Download pdf - 9. NMR Spectra of New Compounds · 7.995 4.000 1.921 1.888 4.419 1.972 1.952 Current Data Parameters NAME nkt666 EXPNO 10 PROCNO 1 F2 - Acquisition Parameters Date_ 20150924

98

76

54

32

10

ppm -0.0000.9050.9190.9331.3321.3361.3481.3501.3621.3641.3741.3771.3801.3831.3871.3901.3961.4001.4081.4141.4251.7011.7141.7301.7441.7571.784

3.8303.8433.856

5.044

6.4986.578

6.8786.8816.8837.098

7.264

7.526

2.963

3.982

1.987

2.009

4.000

0.9581.924

1.8271.831

1.822

Current Data Parameters

NAME nkt-ligand-1

EXPNO 10

PROCNO 1

F2 - Acquisition Parameters

Date_ 20150920

Time 10.30

INSTRUM spect

PROBHD 5 mm CPPBBO BB

PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 16

DS 2

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 31.29

DW 50.000 usec

DE 10.00 usec

TE 300.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W

F2 - Processing parameters

SI 65536

SF 500.1700102 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S36

9. NMR Spectra of New CompoundsElectronic Supplementary Material (ESI) for Green Chemistry.This journal is © The Royal Society of Chemistry 2015

210200

190180

170160

150140

130120

110100

9080

7060

5040

3020

100

ppm

-0.011

13.970

22.398

28.10328.787

50.489

68.191

76.76677.02077.274

113.037

117.797119.270

130.024

137.461138.605

160.285


NAME nkt-ligand-1

EXPNO 11

PROCNO 1


Date_ 20150920

Time 10.33

INSTRUM spect


PULPROG zgpg30

TD 65536

SOLVENT CDCl3

NS 100

DS 4

SWH 29761.904 Hz

FIDRES 0.454131 Hz

AQ 1.1010048 sec

RG 189.66

DW 16.800 usec

DE 11.00 usec

TE 300.2 K

D1 2.00000000 sec

D11 0.03000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 125.7804227 MHz

NUC1 13C

P1 10.00 usec

PLW1 65.00000000 W

======== CHANNEL f2 ========

SFO2 500.1720007 MHz

NUC2 1H

CPDPRG[2 waltz16

PCPD2 80.00 usec

PLW2 13.50000000 W

PLW12 0.30375001 W

PLW13 0.19440000 W


SI 32768

SF 125.7678470 MHz

WDW EM

SSB 0

LB 1.00 Hz

GB 0

PC 1.40

13C N

MR

S37

98

76

54

32

10

ppm

-0.000

1.900

5.384

6.8056.8076.8097.1317.2657.2677.2847.2907.4907.5057.5067.5207.9777.9797.9937.995

4.000

1.921

1.8884.419

1.972

1.952


NAME nkt666

EXPNO 10

PROCNO 1


Date_ 20150924

Time 12.34

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 16

DS 2

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 31.29

DW 50.000 usec

DE 10.00 usec

TE 300.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700104 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S38

210200

190180

170160

150140

130120

110100

9080

7060

5040

3020

100

ppm

-0.004

51.531

76.77777.03177.285

118.786125.811129.753130.329130.557131.591131.684136.061136.792


NAME nkt666

EXPNO 11

PROCNO 1


Date_ 20150924

Time 12.36

INSTRUM spect


PULPROG zgpg30

TD 65536

SOLVENT CDCl3

NS 100

DS 4

SWH 29761.904 Hz

FIDRES 0.454131 Hz

AQ 1.1010048 sec

RG 107.18

DW 16.800 usec

DE 11.00 usec

TE 300.1 K

D1 2.00000000 sec

D11 0.03000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 125.7804227 MHz

NUC1 13C

P1 10.00 usec

PLW1 65.00000000 W

======== CHANNEL f2 ========

SFO2 500.1720007 MHz

NUC2 1H

CPDPRG[2 waltz16

PCPD2 80.00 usec

PLW2 13.50000000 W

PLW12 0.30375001 W

PLW13 0.19440000 W


SI 32768

SF 125.7678470 MHz

WDW EM

SSB 0

LB 1.00 Hz

GB 0

PC 1.40

13C N

MR

S39

98

76

54

32

10

ppm

-0.000

0.8890.9030.9181.2891.3031.3191.3331.5001.5031.5131.5191.5221.5301.5342.121

2.5292.5452.561

5.060

6.7326.8756.8987.095

7.270

7.522

3.117

2.2071.981

1.973

4.000

0.9713.7831.885

1.865


NAME nkt-ligand7r

EXPNO 10

PROCNO 1


Date_ 20150920

Time 13.50

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 16

DS 2

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 31.29

DW 50.000 usec

DE 10.00 usec

TE 300.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700069 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S40

210200

190180

170160

150140

130120

110100

9080

7060

5040

3020

100

ppm

-0.011

13.855

22.319

33.46935.390

50.510

76.79077.04477.297

119.241

123.335

127.164129.978

137.122137.424

144.937


NAME nkt-ligand7r

EXPNO 11

PROCNO 1


Date_ 20150920

Time 13.57

INSTRUM spect


PULPROG zgpg30

TD 65536

SOLVENT CDCl3

NS 100

DS 4

SWH 29761.904 Hz

FIDRES 0.454131 Hz

AQ 1.1010048 sec

RG 189.66

DW 16.800 usec

DE 11.00 usec

TE 300.1 K

D1 2.00000000 sec

D11 0.03000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 125.7804227 MHz

NUC1 13C

P1 10.00 usec

PLW1 65.00000000 W

======== CHANNEL f2 ========

SFO2 500.1720007 MHz

NUC2 1H

CPDPRG[2 waltz16

PCPD2 80.00 usec

PLW2 13.50000000 W

PLW12 0.30375001 W

PLW13 0.19440000 W


SI 32768

SF 125.7678470 MHz

WDW EM

SSB 0

LB 1.00 Hz

GB 0

PC 1.40

13C N

MR

S41

98

76

54

32

10

ppm 1.4751.4801.4861.4881.4921.5001.6471.6511.6561.6661.6721.6821.6881.7051.7181.7361.7441.7581.7631.7701.7741.7801.7871.9871.9912.0022.0082.0112.0132.0162.0202.0232.0262.0312.0442.0462.8852.9002.9052.9202.9352.9402.955

5.064

6.7176.8796.8816.9536.9557.0977.262

7.531

1.9851.8542.7392.1111.955

0.949

4.000

0.9521.8401.9391.891

1.854


NAME nkt-ligand7s

EXPNO 10

PROCNO 1


Date_ 20150920

Time 13.41

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 16

DS 2

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 31.29

DW 50.000 usec

DE 10.00 usec

TE 300.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700113 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S42

210200

190180

170160

150140

130120

110100

9080

7060

5040

3020

100

ppm

-0.010

25.409

34.593

45.673

50.592

76.76077.01477.268

119.256

123.385125.912

129.954

137.087137.429

148.656


NAME nkt-ligand-3

EXPNO 10

PROCNO 1


Date_ 20150920

Time 12.13

INSTRUM spect


PULPROG zgpg30

TD 65536

SOLVENT CDCl3

NS 50

DS 4

SWH 29761.904 Hz

FIDRES 0.454131 Hz

AQ 1.1010048 sec

RG 189.66

DW 16.800 usec

DE 11.00 usec

TE 300.1 K

D1 2.00000000 sec

D11 0.03000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 125.7804227 MHz

NUC1 13C

P1 10.00 usec

PLW1 65.00000000 W

======== CHANNEL f2 ========

SFO2 500.1720007 MHz

NUC2 1H

CPDPRG[2 waltz16

PCPD2 80.00 usec

PLW2 13.50000000 W

PLW12 0.30375001 W

PLW13 0.19440000 W


SI 32768

SF 125.7678470 MHz

WDW EM

SSB 0

LB 1.00 Hz

GB 0

PC 1.40

13C N

MR

S43

98

76

54

32

10

ppm

-0.000

1.853

5.157

6.8906.9197.1177.2637.2907.2927.3677.3787.3817.3847.4087.4217.4247.4347.4387.4547.4567.4667.4707.4737.571

4.000

0.8811.9401.9350.7231.9070.9793.9262.027


NAME nkt-ligand7t

EXPNO 10

PROCNO 1


Date_ 20150920

Time 13.46

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 16

DS 2

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 31.29

DW 50.000 usec

DE 10.00 usec

TE 300.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700109 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S44

210200

190180

170160

150140

130120

110100

9080

7060

5040

3020

100

ppm

-0.005

50.515

76.77877.03177.286

119.262124.614125.849127.121128.102128.984130.162137.470137.852139.599143.124


NAME nkt-ligand-4

EXPNO 10

PROCNO 1


Date_ 20150920

Time 12.30

INSTRUM spect


PULPROG zgpg30

TD 65536

SOLVENT CDCl3

NS 70

DS 4

SWH 29761.904 Hz

FIDRES 0.454131 Hz

AQ 1.1010048 sec

RG 189.66

DW 16.800 usec

DE 11.00 usec

TE 300.1 K

D1 2.00000000 sec

D11 0.03000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 125.7804227 MHz

NUC1 13C

P1 10.00 usec

PLW1 65.00000000 W

======== CHANNEL f2 ========

SFO2 500.1720007 MHz

NUC2 1H

CPDPRG[2 waltz16

PCPD2 80.00 usec

PLW2 13.50000000 W

PLW12 0.30375001 W

PLW13 0.19440000 W


SI 32768

SF 125.7678470 MHz

WDW EM

SSB 0

LB 1.00 Hz

GB 0

PC 1.40

13C N

MR

S45

98

76

54

32

10

ppm

-0.000

2.891

5.021

6.2656.358

6.889

7.080

7.269

7.525

5.979

4.000

0.9361.935

1.8311.869

1.855


NAME nkt-ligand7u

EXPNO 10

PROCNO 1


Date_ 20150920

Time 14.02

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 16

DS 2

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 31.29

DW 50.000 usec

DE 10.00 usec

TE 300.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700079 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S46

210200

190180

170160

150140

130120

110100

9080

7060

5040

3020

100

ppm

-0.005

40.279

50.988

76.79077.04477.298

110.445113.667

119.324

129.799

137.484137.961

151.271


NAME nkt-ligand7u

EXPNO 11

PROCNO 1


Date_ 20150920

Time 14.08

INSTRUM spect


PULPROG zgpg30

TD 65536

SOLVENT CDCl3

NS 100

DS 4

SWH 29761.904 Hz

FIDRES 0.454131 Hz

AQ 1.1010048 sec

RG 189.66

DW 16.800 usec

DE 11.00 usec

TE 300.2 K

D1 2.00000000 sec

D11 0.03000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 125.7804227 MHz

NUC1 13C

P1 10.00 usec

PLW1 65.00000000 W

======== CHANNEL f2 ========

SFO2 500.1720007 MHz

NUC2 1H

CPDPRG[2 waltz16

PCPD2 80.00 usec

PLW2 13.50000000 W

PLW12 0.30375001 W

PLW13 0.19440000 W


SI 32768

SF 125.7678470 MHz

WDW EM

SSB 0

LB 1.00 Hz

GB 0

PC 1.40

13C N

MR

S47

98

76

54

32

10

ppm

-0.000

1.279

1.681

5.115

6.8016.9356.9386.9407.1927.2057.2077.261

8.036

9.050

4.000

0.9531.8891.7741.991

1.896


NAME NKT tbu complex

EXPNO 10

PROCNO 1


Date_ 20140807

Time 19.58

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 16

DS 2

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 31.29

DW 50.000 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700120 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S48

Zinc Complex 8c

210200

190180

170160

150140

130120

110100

9080

7060

5040

3020

100

ppm

-0.007

31.148

34.812

51.371

76.75877.01377.267

119.738124.000125.083128.979

136.035138.611

153.506


NAME NKT tbu complex

EXPNO 11

PROCNO 1


Date_ 20140807

Time 20.04

INSTRUM spect


PULPROG zgpg30

TD 65536

SOLVENT CDCl3

NS 161

DS 4

SWH 29761.904 Hz

FIDRES 0.454131 Hz

AQ 1.1010048 sec

RG 189.66

DW 16.800 usec

DE 11.00 usec

TE 300.0 K

D1 2.00000000 sec

D11 0.03000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 125.7804227 MHz

NUC1 13C

P1 10.00 usec

PLW1 65.00000000 W

======== CHANNEL f2 ========

SFO2 500.1720007 MHz

NUC2 1H

CPDPRG[2 waltz16

PCPD2 80.00 usec

PLW2 13.50000000 W

PLW12 0.30375001 W

PLW13 0.19440000 W


SI 32768

SF 125.7678470 MHz

WDW EM

SSB 0

LB 1.00 Hz

GB 0

PC 1.40

13C N

MR

S49

Zinc Complex 8c

98

76

54

32

10

ppm

-0.000

0.8690.8840.8971.2001.2061.2281.2311.2511.2591.2731.4381.5161.5391.5611.7252.0392.0432.0592.062

3.463

3.764

4.4324.5154.5224.5304.5364.5444.5524.5574.5654.573

7.280

2.2198.7192.205

3.995

0.988

2.968

0.949

1.000


NAME nkt239,240

EXPNO 10

PROCNO 1


Date_ 20140618

Time 21.44

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 4

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 15.99

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700018 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S50

210200

190180

170160

150140

130120

110100

9080

7060

5040

3020

10ppm

28.38329.88130.620

48.381

54.549

75.87176.78277.03677.29079.310

155.191


NAME nkt239,240

EXPNO 11

PROCNO 1


Date_ 20140618

Time 21.48

INSTRUM spect


PULPROG zgpg30

TD 65536

SOLVENT CDCl3

NS 90

DS 4

SWH 29761.904 Hz

FIDRES 0.454131 Hz

AQ 1.1010048 sec

RG 189.66

DW 16.800 usec

DE 11.00 usec

TE 300.0 K

D1 2.00000000 sec

D11 0.03000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 125.7804227 MHz

NUC1 13C

P1 10.00 usec

PLW1 65.00000000 W

======== CHANNEL f2 ========

SFO2 500.1720007 MHz

NUC2 1H

CPDPRG[2 waltz16

PCPD2 80.00 usec

PLW2 13.50000000 W

PLW12 0.30375001 W

PLW13 0.19440000 W


SI 32768

SF 125.7678470 MHz

WDW EM

SSB 0

LB 1.00 Hz

GB 0

PC 1.40

13C N

MR

S51

98

76

54

32

10

ppm -0.0000.9170.9461.3601.3631.3761.3901.3921.4041.4121.4171.4201.4261.4301.4341.4391.4431.4511.4571.5691.6981.7101.7221.7561.7691.7831.7851.7991.812

3.9563.9703.983

4.6544.666

6.8426.922

7.259

2.965

3.995

1.8602.021

2.010

4.000

1.9230.944

0.898


NAME nkt106

EXPNO 10

PROCNO 1


Date_ 20131126

Time 22.04

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 2

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 19.70000076 W


SI 65536

SF 500.1700115 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S52

210200

190180

170160

150140

130120

110100

9080

7060

5040

3020

100

ppm

14.020

22.448

28.20428.963

65.23168.086

76.76377.01677.270

112.190

117.299

142.748

159.740


NAME nkt106(s-2)

EXPNO 10

PROCNO 1


Date_ 20140527

Time 14.49

INSTRUM spect


PULPROG zgpg30

TD 65536

SOLVENT CDCl3

NS 51

DS 4

SWH 29761.904 Hz

FIDRES 0.454131 Hz

AQ 1.1010048 sec

RG 107.18

DW 16.800 usec

DE 11.00 usec

TE 300.0 K

D1 2.00000000 sec

D11 0.03000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 125.7804227 MHz

NUC1 13C

P1 10.00 usec

PLW1 65.00000000 W

======== CHANNEL f2 ========

SFO2 500.1720007 MHz

NUC2 1H

CPDPRG[2 waltz16

PCPD2 80.00 usec

PLW2 13.50000000 W

PLW12 0.30375001 W

PLW13 0.19440000 W


SI 32768

SF 125.7678470 MHz

WDW EM

SSB 0

LB 1.00 Hz

GB 0

PC 1.40

13C N

MR

S53

98

76

54

32

10

ppm

-0.0000.9220.9360.9501.3641.3671.3801.3941.3961.4081.4161.4211.4241.4311.4341.4381.4431.4471.4551.4611.5311.7591.7721.7861.7881.8021.815

3.9543.9673.980

4.537

6.8786.8806.972

7.257

2.935

3.988

1.996

2.025

4.000

1.8640.902

0.561


NAME nkt108

EXPNO 10

PROCNO 1


Date_ 20131128

Time 14.38

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 16

DS 2

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 23.8

DW 50.000 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 19.70000076 W


SI 65536

SF 500.1700127 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S54

210200

190180

170160

150140

130120

110100

9080

7060

5040

3020

10ppm

-0.003

14.010

22.440

28.17728.890

45.867

68.208

76.76477.01977.273

114.685

120.628

139.258

159.666


NAME nkt108(s-3)

EXPNO 10

PROCNO 1


Date_ 20140527

Time 14.44

INSTRUM spect


PULPROG zgpg30

TD 65536

SOLVENT CDCl3

NS 43

DS 4

SWH 29761.904 Hz

FIDRES 0.454131 Hz

AQ 1.1010048 sec

RG 107.18

DW 16.800 usec

DE 11.00 usec

TE 300.0 K

D1 2.00000000 sec

D11 0.03000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 125.7804227 MHz

NUC1 13C

P1 10.00 usec

PLW1 65.00000000 W

======== CHANNEL f2 ========

SFO2 500.1720007 MHz

NUC2 1H

CPDPRG[2 waltz16

PCPD2 80.00 usec

PLW2 13.50000000 W

PLW12 0.30375001 W

PLW13 0.19440000 W


SI 32768

SF 125.7678470 MHz

WDW EM

SSB 0

LB 1.00 Hz

GB 0

PC 1.40

13C N

MR

S55

98

76

54

32

10

ppm

1.532

2.981

4.541

6.6706.6736.752

7.260

4.705

6.182

4.000

1.9580.960

12.170


NAME nkt173

EXPNO 10

PROCNO 1


Date_ 20140310

Time 21.44

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 4

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 19.70000076 W


SI 65536

SF 500.1700136 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S56

210200

190180

170160

150140

130120

110100

9080

7060

5040

3020

10ppm

0.010

40.467

46.640

76.77977.03377.287

112.352

116.556

138.762

150.997


NAME nkt173(s-14)

EXPNO 10

PROCNO 1


Date_ 20140527

Time 14.30

INSTRUM spect


PULPROG zgpg30

TD 65536

SOLVENT CDCl3

NS 39

DS 4

SWH 29761.904 Hz

FIDRES 0.454131 Hz

AQ 1.1010048 sec

RG 107.18

DW 16.800 usec

DE 11.00 usec

TE 300.0 K

D1 2.00000000 sec

D11 0.03000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 125.7804227 MHz

NUC1 13C

P1 10.00 usec

PLW1 65.00000000 W

======== CHANNEL f2 ========

SFO2 500.1720007 MHz

NUC2 1H

CPDPRG[2 waltz16

PCPD2 80.00 usec

PLW2 13.50000000 W

PLW12 0.30375001 W

PLW13 0.19440000 W


SI 32768

SF 125.7678470 MHz

WDW EM

SSB 0

LB 1.00 Hz

GB 0

PC 1.40

13C N

MR

S57

98

76

54

32

10

ppm

-0.000

1.2391.2451.2601.2671.2701.2901.3121.5081.5291.5521.5741.9562.0452.0492.0662.068

3.5123.6533.7694.1004.1144.1284.1434.5214.5294.5374.5434.5504.5584.5644.5724.5794.7014.715

7.297

2.239

2.109

4.317

1.0782.9303.130

0.052

1.0211.000


NAME nkt248

EXPNO 10

PROCNO 1


Date_ 20140625

Time 14.20

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 8

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 13.62

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1699936 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S58

210200

190180

170160

150140

130120

110100

9080

7060

5040

3020

10ppm

29.76030.493

48.74551.93854.556

75.74576.81577.07077.325

155.176156.284


NAME nkt248

EXPNO 20

PROCNO 1


Date_ 20140625

Time 20.52

INSTRUM spect


PULPROG zgpg30

TD 65536

SOLVENT CDCl3

NS 61

DS 4

SWH 29761.904 Hz

FIDRES 0.454131 Hz

AQ 1.1010048 sec

RG 189.66

DW 16.800 usec

DE 11.00 usec

TE 300.0 K

D1 2.00000000 sec

D11 0.03000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 125.7804227 MHz

NUC1 13C

P1 10.00 usec

PLW1 65.00000000 W

======== CHANNEL f2 ========

SFO2 500.1720007 MHz

NUC2 1H

CPDPRG[2 waltz16

PCPD2 80.00 usec

PLW2 13.50000000 W

PLW12 0.30375001 W

PLW13 0.19440000 W


SI 32768

SF 125.7678470 MHz

WDW EM

SSB 0

LB 1.00 Hz

GB 0

PC 1.40

13C N

MR

S59

98

76

54

32

10

ppm -0.0001.2081.2151.2351.2411.2571.2621.2821.2901.4331.4411.4591.4671.4811.4861.4881.5071.5141.9091.9332.0392.0472.0542.0632.0682.0742.4592.7342.7422.7502.7562.7642.7712.7772.7852.7933.4393.4783.7674.5254.5334.5424.5464.5554.5644.5684.5774.585

7.266

2.244

2.520

1.9703.636

1.740

1.122

0.185

3.029

1.000


NAME nkt252

EXPNO 30

PROCNO 1


Date_ 20140701

Time 17.04

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 16

DS 2

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 31.29

DW 50.000 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700095 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S60

210200

190180

170160

150140

130120

110100

9080

7060

5040

3020

10ppm

-0.012

29.924

33.452

49.335

54.541

76.37376.76477.01977.273

155.218


NAME nkt252

EXPNO 31

PROCNO 1


Date_ 20140701

Time 17.07

INSTRUM spect


PULPROG zgpg30

TD 65536

SOLVENT CDCl3

NS 100

DS 4

SWH 29761.904 Hz

FIDRES 0.454131 Hz

AQ 1.1010048 sec

RG 189.66

DW 16.800 usec

DE 11.00 usec

TE 300.0 K

D1 2.00000000 sec

D11 0.03000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 125.7804227 MHz

NUC1 13C

P1 10.00 usec

PLW1 65.00000000 W

======== CHANNEL f2 ========

SFO2 500.1720007 MHz

NUC2 1H

CPDPRG[2 waltz16

PCPD2 80.00 usec

PLW2 13.50000000 W

PLW12 0.30375001 W

PLW13 0.19440000 W


SI 32768

SF 125.7678470 MHz

WDW EM

SSB 0

LB 1.00 Hz

GB 0

PC 1.40

13C N

MR

S61

98

76

54

32

10

ppm

1.4131.4191.4261.4331.4391.4461.4531.4591.4661.4731.4781.4861.4931.5541.5621.5651.5691.5791.5871.5941.5991.6061.6121.6241.6321.7631.7761.7821.7891.7951.8021.8091.8141.8201.8271.9221.9291.9361.9401.9481.9531.9661.9735.0095.0175.0275.0345.0425.0525.060

7.2587.4167.4207.4317.4447.4477.4507.5247.5267.5297.5387.5417.5457.5568.0418.0438.0478.0588.0598.060

1.0972.1113.2472.2582.083

1.000

1.9940.994

1.982


NAME nkt376

EXPNO 30

PROCNO 1


Date_ 20141216

Time 12.32

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 4

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700130 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S62

NMR Spectra of Known Compounds (Products)

98

76

54

32

10

ppm

-0.000

1.562

5.3697.2517.3257.3407.3457.3527.3547.3577.3747.3867.3897.4007.4037.4067.4197.4227.4347.4447.4477.4507.4537.4587.4607.5387.5417.5437.5527.5567.5597.5687.5707.5738.0718.0748.0878.0898.090

2.000

7.764

1.889


NAME nkt209

EXPNO 10

PROCNO 1


Date_ 20140428

Time 17.22

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 4

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700169 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S63

98

76

54

32

10

ppm

1.0661.0901.1131.1201.1231.1281.1371.1481.1551.5331.5381.5441.5551.5571.5611.5671.5681.5741.5791.5851.7161.7211.7401.7441.7501.7561.9521.9571.9661.9711.9801.9852.1142.1192.1262.1302.1342.1382.1432.1502.168

4.9104.9184.9314.9404.9534.962

7.2587.4217.4247.4367.4497.4527.5287.5317.5347.5427.5467.5497.5587.5617.5638.0378.0408.0438.0548.0558.056

3.2247.5582.704

2.4712.3031.1661.303

1.000

1.9951.060

1.932


NAME nkt198

EXPNO 10

PROCNO 1


Date_ 20140414

Time 21.19

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 8

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 19.70000076 W


SI 65536

SF 500.1700134 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S64

98

76

54

32

10

ppm 1.0761.0821.1091.1181.1351.1431.1501.1701.1781.1861.2071.2531.2661.2741.2841.3011.3161.3901.3991.4221.4401.4521.4661.4721.4921.5081.5281.5361.6581.6811.7641.7721.8361.8421.8631.9071.9151.9421.9611.9682.3902.4054.7614.7714.7784.7854.7944.8024.8094.8174.8275.3475.356

7.1897.3467.3617.3777.4597.4737.4887.9667.9667.982

3.4266.6353.141

18.591

7.678

7.209

2.142

1.000

0.984

2.1020.996

2.035


NAME nkt203

EXPNO 10

PROCNO 1


Date_ 20140416

Time 20.40

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 16

DS 2

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 19.70000076 W


SI 65536

SF 500.1700481 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S65

98

76

54

32

10

ppm

1.3401.3821.3871.3911.3961.4081.4111.4161.4201.4321.4361.4411.4451.5691.5761.7311.7401.7501.7741.7831.7901.7981.8071.8141.8221.8311.8382.1172.1262.1362.1442.1522.1622.1712.4482.4552.4572.4642.4682.4762.4842.4922.4962.5022.5052.5125.1065.1115.1135.1175.1265.1315.1335.137

7.2587.4347.4377.4497.4627.4657.5407.5427.5457.5547.5577.5617.5697.5727.5758.0558.0588.0728.074

6.1043.7871.4191.1581.2460.4441.0101.2261.111

1.110

1.000

2.0441.114

2.019


NAME nkt204

EXPNO 10

PROCNO 1


Date_ 20140418

Time 17.07

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 8

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 19.70000076 W


SI 65536

SF 500.1700135 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S66

98

76

54

32

10

ppm

-0.0000.087

1.1211.1381.155

1.553

4.4074.4214.4234.4264.440

7.2587.4177.4207.4327.4457.4487.5277.5297.5327.5417.5447.5598.0298.0328.0368.0468.0488.049

9.044

2.012

2.000

1.9991.006

1.972


NAME ykt607

EXPNO 10

PROCNO 1


Date_ 20131112

Time 15.52

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 1

DS 0

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 31.29

DW 50.000 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 19.70000076 W


SI 65536

SF 500.1700133 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S67

98

76

54

32

10

ppm

-0.000

1.0561.0701.084

2.5362.5512.5652.579

3.475

4.9474.9514.955

7.2627.4377.4407.4537.4657.4687.5597.5617.5647.5767.5918.0608.0638.0678.0778.079

5.971

4.004

1.998

2.000

1.9090.943

1.852


NAME nkt116

EXPNO 10

PROCNO 1


Date_ 20131210

Time 14.58

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 4

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 19.70000076 W


SI 65536

SF 500.1700105 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S68

98

76

54

32

10

ppm

-0.000

1.5521.554

2.606

3.890

5.342

7.2157.2307.2457.2517.3357.3497.3527.3707.3737.3777.3827.3857.3897.3997.4017.4047.4077.4397.4537.4567.9437.959

3.044

0.070

2.000

2.2670.9932.7172.156

0.940


NAME nkt205

EXPNO 10

PROCNO 1


Date_ 20140418

Time 17.13

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 8

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 19.70000076 W


SI 65536

SF 500.1700172 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S69

98

76

54

32

10

ppm

-0.000

0.8950.908

1.5381.5521.8121.8251.8391.8521.8661.8791.8932.4502.464

3.8013.8163.8303.844

5.1885.2165.2385.266

7.0307.0457.0967.1127.1527.1637.1677.1777.2297.2457.2597.5487.5527.5647.5677.5797.583

8.5328.5338.542

6.168

3.325

0.993

2.027

0.940

2.000

0.9531.9550.9942.5540.937

0.891


NAME nkt167

EXPNO 10

PROCNO 1


Date_ 20140304

Time 18.31

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 8

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 19.70000076 W


SI 65536

SF 500.1700137 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S70

98

76

54

32

10

ppm

-0.0000.071

1.649

2.0682.0742.1432.5192.5342.5362.5512.8832.8992.914

7.1877.2027.2527.2597.2737.289

6.071

6.0333.076

2.006

2.000

2.9212.203


NAME ykt531

EXPNO 10

PROCNO 1


Date_ 20130830

Time 19.40

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 1

DS 0

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 23.8

DW 50.000 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 19.70000076 W


SI 65536

SF 500.1700161 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S71

98

76

54

32

10

ppm

-0.000

1.5441.549

5.207

7.2557.3547.3597.3677.3737.3777.381

8.1438.1448.146

2.055

5.073

1.000


NAME ykt584-iso

EXPNO 10

PROCNO 1


Date_ 20140109

Time 21.14

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 1

DS 0

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 31.29

DW 50.000 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 19.70000076 W


SI 65536

SF 500.1700139 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S72

98

76

54

32

10

ppm

0.8860.9000.9180.9330.9470.9630.9771.3591.3741.3891.4041.5481.6111.6241.6402.1462.1612.1712.184

4.1134.1214.1344.1434.1554.2804.2894.2984.307

5.1115.2535.270

7.2597.3177.3277.3347.3437.3597.367

10.680

2.462

2.312

1.200

2.562

1.002

2.532

0.965

5.587


NAME val onbu

EXPNO 2

PROCNO 1


Date_ 20130912

Time 15.13

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 1

DS 0

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 19.70000076 W


SI 65536

SF 500.1700127 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S73

98

76

54

32

10

ppm

-0.0000.071

1.5591.5621.568

5.2045.8375.8395.8575.8606.1426.1636.1776.1976.4316.4346.4666.4687.2557.3187.3217.3247.3287.3327.3367.3407.3457.3537.3547.3587.3707.3747.3807.390

0.0250.0050.226

2.000

0.989

0.943

0.976

4.784


NAME benzyl acrylate

EXPNO 20

PROCNO 1


Date_ 20150106

Time 20.21

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 4

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700146 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S74

98

76

54

32

10

ppm

-0.000

1.9691.9711.9721.974

5.197

5.5815.5845.587

6.1566.1586.1596.161

7.2557.3227.3267.3297.3337.3347.3397.3497.3517.3607.3657.3677.3717.3767.387

3.000

1.987

1.004

0.997

4.831


NAME ykt620-iso

EXPNO 10

PROCNO 1


Date_ 20140109

Time 21.22

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 1

DS 0

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 31.29

DW 50.000 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 19.70000076 W


SI 65536

SF 500.1700139 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S75

98

76

54

32

10

ppm

-0.000

1.5651.6971.711

4.4314.445

5.210

7.2597.3557.3597.3637.3707.3767.3777.3817.382

2.1702.983

0.949

2.000

4.892


NAME ykt500-2cu

EXPNO 10

PROCNO 1


Date_ 20130819

Time 17.24

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 1

DS 0

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 31.29

DW 50.000 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 19.70000076 W


SI 65536

SF 500.1700128 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S76

98

76

54

32

10

ppm 1.3421.3481.3541.3611.3691.3751.3821.3891.3961.4031.4421.4491.4611.4681.4731.4881.4931.5071.5141.5191.5201.5291.5361.5471.5551.5611.5641.5761.7281.7371.7461.7551.7641.7721.7801.8991.9081.9161.9251.9333.7654.5894.5974.6074.6154.6244.6344.642

7.265

3.125

3.4172.0432.042

3.000

0.957


NAME nkt224

EXPNO 20

PROCNO 1


Date_ 20140513

Time 13.57

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 8

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700098 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S77

98

76

54

32

10

ppm

-0.000

1.2441.2581.273

1.542

2.043

3.7974.1004.1144.1284.143

5.166

7.2587.3417.3467.3517.3547.3567.3637.3677.3697.3767.3807.3827.392

0.527

0.248

0.486

2.933

0.325

2.000

4.850


NAME nkt221

EXPNO 10

PROCNO 1


Date_ 20140509

Time 19.23

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 8

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700132 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S78

98

76

54

32

10

ppm

-0.000

1.5511.6591.664

2.1112.1172.194

3.701

7.262

6.175

5.949

3.369

3.000


NAME nkt233tm

EXPNO 10

PROCNO 1


Date_ 20140526

Time 13.10

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 4

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700117 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S79

98

76

54

32

10

ppm

-0.000

1.587

3.7213.7293.7453.7533.7583.7703.7823.7944.4044.4164.4224.4334.5774.5944.6124.9364.9444.9474.9524.9554.9594.9604.9644.9674.9724.9754.983

7.267

2.198

1.0621.050

1.000


NAME nkt222

EXPNO 10

PROCNO 1


Date_ 20140513

Time 14.05

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 8

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700091 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S80

98

76

54

32

10

ppm

-0.001-0.000

1.6163.6123.6133.6193.6203.6343.6353.6413.6423.6793.6883.7013.7103.7994.0284.0304.0394.0414.0534.0564.0584.0644.0694.0724.0744.0874.0894.0984.3904.4024.4074.4194.4874.5044.5214.7994.8074.8114.8154.8194.8234.8274.8314.8354.8435.2225.2435.2725.2735.2745.3065.3075.3095.8365.8485.8585.8695.8815.8925.9035.9135.9147.267

2.181

2.142

1.0821.074

1.015

2.078

1.000


NAME nkt318

EXPNO 10

PROCNO 1


Date_ 20140911

Time 10.52

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 16

DS 2

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 31.29

DW 50.000 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700084 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S81

98

76

54

32

10

ppm

-0.000

1.540

4.1454.1534.1664.1744.2264.2354.2474.2564.5274.5394.5444.5564.6024.6194.6365.0065.0145.0155.0185.0235.0255.0265.0305.0315.0345.0395.0425.0516.9046.9066.9226.9247.0057.0077.0207.0337.0357.2597.2917.2957.2997.3067.3107.3137.3187.3237.3287.332

1.0451.0651.0201.061

1.000

2.0091.024

2.045


NAME nkt322

EXPNO 10

PROCNO 1


Date_ 20141129

Time 17.37

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 4

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.2 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700127 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S82

98

76

54

32

10

ppm

-0.000

1.260

1.6402.5232.5332.5462.5562.5642.5732.5822.5962.6052.6802.6862.6902.6973.6913.7003.7093.7093.7904.2294.2434.2464.2604.5154.5324.5484.7994.8104.8134.8154.8214.8244.8264.8294.8354.8374.8404.8515.0825.302

6.702

6.883

7.0987.1167.267

7.538

4.309

2.156

4.2861.332

1.082

1.033

1.000


NAME nkt319

EXPNO 10

PROCNO 1


Date_ 20140911

Time 11.03

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 16

DS 2

SWH 10000.000 Hz

FIDRES 0.152588 Hz

AQ 3.2767999 sec

RG 31.29

DW 50.000 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730888 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700084 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S83

98

76

54

32

10

ppm

-0.000

1.570

2.8292.8452.8562.8722.8792.8912.9062.9184.0714.0754.0824.0874.0984.1004.1034.1144.1444.1554.1624.1734.4624.4784.4955.106

7.1727.1867.1897.2607.2827.2967.3307.3457.359

2.144

1.0451.053

1.040

1.000

2.0651.8312.035


NAME nkt283

EXPNO 20

PROCNO 1


Date_ 20141129

Time 17.41

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 4

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700120 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S84

98

76

54

32

10

ppm

-0.000

1.551

4.1894.2034.2074.221

4.7304.7474.7654.9394.9554.9705.263

7.2607.3427.3447.3477.3537.3587.3617.3717.3827.3857.4027.4047.4137.4177.430

1.040

1.0601.035

1.000

5.188


NAME nkt317

EXPNO 10

PROCNO 1


Date_ 20140920

Time 16.31

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 8

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.0 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700122 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S85

98

76

54

32

10

ppm

1.2811.2871.3071.3101.3131.3341.3541.3631.4531.5781.5881.6071.6281.6321.6341.6582.0922.1002.110

3.532

4.4634.4694.9104.9184.9264.9314.9394.9474.9524.9604.968

7.2657.4157.4187.4307.4437.4467.5307.5327.5357.5447.5477.5517.5607.5628.0208.0228.0268.0378.0388.039

2.1669.4592.574

4.187

1.013

0.963

1.000

1.9660.996

1.929


NAME nkt235

EXPNO 20

PROCNO 1


Date_ 20141129

Time 17.46

INSTRUM spect


PULPROG zg30

TD 65536

SOLVENT CDCl3

NS 4

DS 1

SWH 8012.820 Hz

FIDRES 0.122266 Hz

AQ 4.0894465 sec

RG 31.29

DW 62.400 usec

DE 10.00 usec

TE 300.1 K

D1 1.00000000 sec

TD0 1

======== CHANNEL f1 ========

SFO1 500.1730010 MHz

NUC1 1H

P1 12.00 usec

PLW1 13.50000000 W


SI 65536

SF 500.1700097 MHz

WDW EM

SSB 0

LB 0.30 Hz

GB 0

PC 1.00

1H N

MR

S86