Download pdf - · 2019-08-14 · 2 CURRICULUM The Curriculum of B.Tech (Chemical Engineering) is designed to fulfil the Program Educational Objectives (PEO) and the Program Outcomes (PO) listed

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Pondicherry Engineering College, Puducherry – 605014 (An Autonomous Institution of Government of Puducherry affiliated to Pondicherry University)

Curriculum and Syllabi

for

B.Tech. (Chemical Engineering) (With Effect from Academic year 2018-19)

(Approved in Fifth Academic Council Meeting held on 6th May 2019)

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CURRICULUM

The Curriculum of B.Tech (Chemical Engineering) is designed to fulfil the Program Educational

Objectives (PEO) and the Program Outcomes (PO) listed below.

PROGRAM EDUCATIONAL OBJECTIVES (PEO)

PEO1 To provide necessary background in science, particularly in advanced mathematics, physics and chemistry that underlie modern chemical engineering and technology.

PEO2 To provide training to solve problems relevant to the general practice of Chemical Engineering and engineering design.

PEO3 To provide students experience in conducting and in planning experiments in modern engineering laboratory including experiments with computers as well as interpreting the significance of resulting data and properly reporting results in well written technical reports.

PEO4 To provide students opportunity to work as part of team on projects pertaining to core and advanced areas of chemical engineering and fostering of important job related skills such as improved oral and written communications.

PEO5 To promote student awareness of life-long learning and to introduce them to professional ethics and codes of professional practice.

PROGRAM OUTCOMES (PO)

PO1 Apply the knowledge of mathematics, science, engineering fundamentals, and an engineering specialization to the solution of complex engineering problems.

PO2 Identify, formulate, review research literature, and analyze complex engineering problems reaching substantiated conclusions using first principles of mathematics, natural sciences, and engineering sciences.

PO3 Design solutions for complex engineering problems and design system components or processes that meet the specified needs with appropriate consideration for the public health and safety, and the cultural, societal, and environmental considerations.

PO4 Use research-based knowledge and research methods including design of experiments, analysis and interpretation of data, and synthesis of the information to provide valid conclusions.

PO5 Create, select, and apply appropriate techniques, resources, and modern engineering and IT tools including prediction and modeling to complex engineering activities with an understanding of the limitations.

PO6 Apply reasoning informed by the contextual knowledge to assess societal, health, safety, legal and cultural issues and the consequent responsibilities relevant to the professional engineering practice.

PO7 Understand the impact of the professional engineering solutions in societal and environmental contexts, and demonstrate the knowledge of, and need for sustainable development.

PO8 Apply ethical principles and commit to professional ethics and responsibilities and norms of the engineering practice.

PO9 Function effectively as an individual, and as a member or leader in diverse teams, and in multidisciplinary settings.

PO10 Communicate effectively on complex engineering activities with the engineering community and with society at large, such as, being able to comprehend and write effective reports and design documentation, make effective presentations, and give and receive clear instructions.

PO11 Demonstrate knowledge and understanding of the engineering and management principles and apply these to one’s own work, as a member and leader in a team, to manage projects and in multidisciplinary environments.

PO12 Recognize the need for, and have the preparation and ability to engage in independent and life-long learning in the broadest context of technological change.

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PROGRAM SPECIFIC OUTCOMES (PSO)

PSO1 Graduates are acquainted well with the concepts and principles of Chemical Engineering required for understanding and solving practical industrial problems of current interests to process industries.

PSO2 Graduates are initiated to work on Innovative Ideas that will eventually motivate them to pursue Higher Studies and Research in Chemical and Allied Engineering.

PSO3 Graduates can function in a Multidisciplinary Environment by being able to associate and integrate their domain knowledge with other disciplines.

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Distribution of credits among the subjects grouped under various categories:

Courses are grouped under various categories and the credits to be earned in each category of courses are as

follows:

Sl. No.

Category Credits Course Category

Code (CCC)

1 Humanities, Social Sciences and Management Courses 6 + 2 / 3 * HSM

2 Basic Science Courses (Mathematics, Physics, Chemistry and Biology)

30.5 BSC

3 Engineering Science Courses (Workshop, Drawing, Basics of Electrical/Mechanical/Computer etc.,)

21.5 ESC

4 Professional Core Courses 63 PCC

5 Professional Elective Courses (from chosen discipline) 15 PEC

6 Open Elective Courses (from other technical/ emerging disciplines)

10 OEC

7 Professional Activity Courses (Project Work, Entrepreneurship, Seminar, Internship, Comprehensive Test)

14 PAC

8 Mandatory non-Credit Courses (Environmental Sciences, Induction, Indian Constitution, Essence of Indian Traditional Knowledge, Professional Ethics)

Non-credit MCC

Total 160

*included in the 10 credits under open elective category

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Semester-wise Courses and Credits

Semester I

Course Code

Course CCC Periods

Credits L T P

FY201 Induction Programme MCC - - - 0

MA201 Mathematics I BSC 3 1 0 4

PH201 Physics BSC 3 1 0 4

CY201 Chemistry BSC 3 1 0 4

HS201 English for Communication HSM 2 0 2 3

ME201 Workshop and Manufacturing Practice ESC 0 0 3 1.5

PH202 Physics Laboratory BSC 0 0 3 1.5

CY202 Chemistry Laboratory BSC 0 0 3 1.5

Total 11 3 11 -

25 19.5

Semester II

Course Code

Course CCC Periods

Credits L T P

MA202 Mathematics II BSC 3 1 0 4

EE201 Basic Electrical Engineering ESC 3 1 0 4

CS201 Programming for Problem Solving ESC 3 0 0 3

ME202 Engineering Graphics and Computer Aided Drawing ESC 2 0 4 3

CE201 Environmental Science MCC 3 0 0 0

EE202 Basic Electrical Engineering Laboratory ESC 0 0 3 1.5

CS202 Programming Laboratory ESC 0 0 3 1.5

Total 14 2 10 -

26 17

6

Semester III

Course Code

Course CCC Periods

Credits L T P

CY203 Chemistry for Chemical Engineering BSC 3 1 4

CE233 Engineering Mechanics and Mechanics of Solids

ESC 3 1 4

CH201 Momentum Transfer PCC 3 1 4

CH202 Process Calculations PCC 3 1 4

SH201 Biology for Engineers BSC 3 - 2

CY204 Chemistry Lab for Chemical Engineering BSC 3 1.5

SH202 Indian Constitution MCC 3 ---

Total 18 4 3

25 19.5

Course Code

Open Elective/ Honors/ Minor Course CCC Periods

Credits L T P

ZZOXX* Open Elective OEC 3 - - 3

CHH01 Introduction to Frontiers of Chemical Engineering

PCC 4 - - 4

CHM01 Process Engineering Principles and Calculations

PCC 3 1 - 4

Semester IV

Course Code

Course CCC Periods

Credits L T P

MA204 Transforms, Partial Differential Equations and Statistics

BSC 3 1 4

CH203 Process Heat Transfer PCC 3 1 4

CH204 Mechanical Operations PCC 3 3

CH205 Chemical Engineering Thermodynamics PCC 3 1 4

CH206 Mass Transfer – I PCC 3 1 4

EC234 Elements of Electronics ESC 3 - 3

CH207 Chemical Engineering Lab – I PCC 3 1.5

Total 18 4 3

25 23.5

Course Code


Credits L T P

ZZOXX* Open Elective OEC 3 - - 3

CHH02 Special Topics in Chemical Engineering – I

PCC 3 1 - 4

CHM02 Fluid Flow and Particle Technology PCC 3 1 - 4

*ZZ in ZZOXX is the Department Code of the department offering Open Elective

7

Semester V

Course Code

Course CCC Periods

Credits L T P

CH208 Mass Transfer – II PCC 3 1 4

CH209 Chemical Reaction Engineering – I PCC 3 1 4

CH210 Chemical Process Industries PCC 3 3

CHYXX Program Elective – I PEC 3 3

CHYXX Program Elective – II PEC 3 3

CH211 Chemical Engineering Lab – II PCC 3 1.5

EP201 Entrepreneurship PAC 3 2

Total 18 2 3

23 20.5

Course Code


Credits L T P

ZZOXX Open Elective OEC 3 - - 3

CHH03 Special Topics in Chemical Engineering – II PCC 3 1 - 4

CHM03 Heat Transfer and Thermodynamics PCC 3 1 - 4

Semester VI

Course Code

Course CCC Periods

Credits L T P

CH212 Chemical Reaction Engineering – II PCC 3 1 4

CH213 Process Dynamics & Control PCC 3 1 4

CHYXX Program Elective –III PEC 3 3

CHYXX Program Elective – IV PEC 3 3

HS202 Industrial Economics and Management HSM 3 3

CH214 Chemical Engineering Lab – III PCC 3 1.5

SH203 Essence of Indian Traditional Knowledge MCC 3

Total 18 2 3

23 18.5

Course Code


Credits L T P


CHH04 Special Topics in Chemical Engineering-III

PCC 3 1 - 4

CHM04 Fundamentals of Mass Transfer and Separations

PCC 3 1 - 4

8

Semester VII

Course Code

Course CCC Periods

Credits L T P

CH215 Transport Phenomena PCC 3 1 - 4

CH216 Computational Methods and Practice in Chemical Engineering

PCC 3 - 2 4

CH217 Process Equipment Design & Practice PCC 3 2 4

CH218 Process Engineering Economics PCC 3 - - 3

CHYXX Program Elective – V PEC 3 - - 3

CH219 Process Control and Simulation Lab PCC 3 1.5

CH220 Seminar PAC 3 1

CH221 Professional Ethics MCC 2

Total 20 1 7

28 20.5

Course Code


Credits L T P


CHH05 Special Topics in Chemical Engineering – IV

PCC 3 1 - 4

CHM05 Process Dynamics and Reaction Engineering

PCC 3 1 - 4

Semester VIII

Course Code

Course CCC Periods

Credits L T P

SWOXX Open Elective through SWAYAM OEC - - - 2

SWOXX Open Elective through SWAYAM OEC - - - 2

CH222 Comprehensive Test PAC - - 2 1

CH223 Internship PAC - - - 2

CH224 Project Work PAC - - 8 8

Total

10 15

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List of Professional Electives Courses (PEC)

Professional Electives Course Code

Course Semester

Professional Elective – I /II

CHY01 Polymer Science and Technology

V

CHY02 Membrane Technology

CHY03 SemiConductor Processing Technology

CHY04 Petrochemical Technology

CHY05 Energy Technology and Management

Professional Elective – III /IV

CHY06 Petroleum Refinery Engineering

VI

CHY07 Nuclear Technology

CHY08 New Separation Techniques

CHY09 Chemical Engineering Practice

CHY10 Fluidization Engineering

Professional Elective – V

CHY11 Risk and safety Management in Process Industries

CHY12 Pollution Control in Process Industries

VII CHY13 Bio Process Engineering

CHY14 Process Optimization

List of Open Electives

Course Code

Course

CHO01 Principles of Process Engineering

CHO02 Green Chemistry and Engineering

CHO03 Energy Engineering

CHO04 Introduction to Semiconductor Processing

10

Courses offered under various categories:

CCC Course Code

Course Semester Credit Total Credit

BSC

MA201 Mathematics – I I 4

30.5

PH201 Physics I 4

CY201 Chemistry I 4

PH202 Physics laboratory I 1.5

CY202 Chemistry Laboratory I 1.5

MA202 Mathematics –II II 4

CY203 Chemistry for Chemical Engineering III 4

SH201 Biology for Engineers III 2

CY204 Chemistry Lab for Chemical Engineering III 1.5


IV 4

ESC

ME201 Workshop and Manufacturing Practice I 1.5

21.5

EE201 Basic Electrical Engineering II 4

CS201 Programming for Problem Solving II 3

ME202 Engineering Graphics & Computer Aided Drawing

II 3

EE202 Electrical Engineering Laboratory II 1.5

CS202 Programming Laboratory II 1.5

CE233 Engineering Mechanics & Mechanics of Solids

III 4

EC234 Elements of Electronics IV 3

PCC

CH201 Momentum Transfer III 4

63

CH202 Process Calculation III 4

CH203 Process Heat Transfer IV 4

CH204 Mechanical Operation IV 3

CH205 Chemical Engineering Thermodynamics IV 4

CH206 Mass Transfer – I IV 4

CH207 Chemical Engineering Lab-I IV 1.5

CH208 Mass Transfer –II V 4

CH209 Chemical Reaction Engineering – I V 4

CH210 Chemical Process Industries V 3

CH211 Chemical Engineering Lab-II V 1.5

CH212 Chemical Reaction Engineering – II VI 4

CH213 Process Dynamics & Control VI 4

CH214 Chemical Engineering Lab – III VI 1.5

CH215 Transport Phenomena VII 4

CH216 Computational Methods & Practice in Chemical Engineering

VII 4

CH217 Process Equipment Design & Practice VII 4

CH218 Process Engineering Economics VII 3

CH219 Process Control and Simulation Lab VII 1.5

PEC

CHY01 Program Elective – I V 3

15

CHY02 Program Elective – II V 3

CHY03 Program Elective – III VI 3

CHY04 Program Elective – IV VI 3

CHY05 Program Elective – V VII 3

OEC ZZOXX

Open Electives offered by other Departments

III - VII 6 10

SWOXX Open Electives offered under SWAYAM - 4

11

PAC

EP201 Entrepreneurship V 2

14

CH220 Seminar VII 1

CH222 Comprehensive Test VIII 1

CH223 Internship VIII 2

CH224 Project Work VIII 8

HSM

HS201 English for Communication I 3

6 + 3*/ 2*

HS202 Industrial Engineering & Economics VI 3

HSOXX Humanities Open Elective offered by HSS Department

- 3*

SWOXX Humanities Open Elective offered under SWAYAM

- 2*

Total 160

*included in the 10 credits under Open Elective category

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Department : Humanities and Social Sciences Programme: B.Tech

Semester : First Course Category Code: MCC Semester Exam Type: -

Course Code Course Periods / Week Credit Maximum Marks

L T P C CA SE TM

FY201 Induction Programme - - - Non-Credit - - -

Prerequisite -

Course Outcome

The course will enable the student to

CO1 Acquire social awareness & knowledge for self-development

CO2 Be aware of nature & environment conscious and of Innovative nature.

CO3 Develop holistic attitude and harmony in the individual, family, and society

CO4 Know about the art and culture, language and literature of this vast secular nation

CO5 Integrating technical Education for betterment of society

UNIT-I Proficiency in English Periods: 12

Communication skills – Diagnostic test on Grammar – Synonyms, Antonyms, Tenses, Sentence Completion, Idioms & Phrases, One word substitution, Homophones, Homonyms, Use of Prepositions, Subject-verb agreement – Writing – Paragraph writing, Letter writing, Essay writing, Story Development.

CO1

UNIT-II Bridge course in Mathematics Periods: 12

Fundamentals of differential and integral calculus: Theory, Practice & Test. Limit of function-Fundamental results on limits-Continuity of a function- Concept of differentiation- Concept of derivative- Slope of a curve-Differentiation Techniques- Derivatives of elementary functions from first principle- Derivatives of inverse functions-Logarithmic differentiation- Method of substitution- Differentiation of parametric functions-Differentiation of implicit functions- Higher order derivatives. Integrals of functions containing linear functions-Method of integration (Decomposition method, method of substitution, integration by parts) - Definite integrals. Simple definite integrals- Properties of Definite integrals- Reduction formulae- Area and volume- Length of curve- surface area of a solid.

CO2

UNIT-III Universal human values Periods: 12

Current Status of the society (Sources of fear)-Reformation through education-Sanskar-What is success (getting good marks, college admission, Job etc)-What is aim of life (happiness, Prosperity and continuity of happiness and prosperity)-What is required for happiness (relationship, physical facilities)-Relationship involves all emotions and feelings-Physical facility-material things required for life-Difference between animal and human consciousness-Animal consciousness-depending on money, accumulating money by wrong means etc.-Human consciousness-right thinking, right understanding, right feeling-Happiness through Harmony in the individual, family, society and nature, leading to fearlessness in the society is the purpose of holistic education or value education.

CO3

UNIT-IV Literary activities Periods: 12

Team building activities – Quiz – Oral Exercises – Group discussion, Debate, Extempore, Role play. CO4

UNIT-V Creative arts Periods: 12

Introduction to painting & renowned artworks – Documentary & Short films – Music – Vocal, Instrumental – Dance – Classical, Cinematic – Mimicry – Mime.

CO5

Lecture Periods: 60 Tutorial Periods: - Practical Periods: - Total Periods: 60

Reference Books

-

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Department : Mathematics Programme: B.Tech.

Semester : First Course Category Code: BSC Semester Exam Type: TY

Course Code Course Name Periods / Week Credit Maximum Marks

L T P C CA SE TM

MA201 Mathematics-I 3 1 - 4 40 60 100

Prerequisite: -

Course Outcome

CO1 To apply differential calculus to notions of curvature, evolutes and involutes and they will

have a basic understanding of Beta and Gamma functions

CO2 The mathematical tools needed in evaluating multiple integrals and their usage.

CO3 The effective mathematical tools for the solutions of differential equations that model

physical processes

CO4 Able to solve simultaneous linear differential equations

CO5 Understands Vector calculus and its applications

UNIT-I Differential Calculus Periods: 12

Curvature, radius of curvature, evolutes and involutes. Beta and Gamma functions and their properties. CO1

UNIT-II Multi variable calculus Periods: 12

Multiple Integrals, change of order of integration in double integrals, Applications: Plane areas (double integration), Change of variables (Cartesian to polar), Double and triple integrations, Volumes by triple integration – Mass, Center of mass and Gravity (constant and variable densities).

CO2

UNIT-III First order Ordinary Differential Equation Periods: 12

Exact equations, First order linear equations, Bernoulli’s equation, Equations not of first degree, equations solvable for p, equations solvable for y, equations solvable for x - Clairaut’s type - simple applications, orthogonal trajectories, growth and decay.

CO3

UNIT-IV Higher Order Ordinary Differential Equation Periods: 12

Linear differential equations of higher order - with constant coefficients, the operator D, Euler’s linear equation of higher order with variable coefficients, simultaneous linear differential equations, solution by variation of parameters method.

CO4

UNIT-V Vector Calculus Periods: 12

Gradient, divergence and curl, their properties and relations. Scalar line integrals, vector line integrals, scalar surface integrals, vector surface integral, Theorems of Green, Stokes and Gauss divergence (without proof). Simple applications involving cubes, sphere and rectangular parallelepipeds.

CO5

Lecture Periods: 45 Tutorial Periods: 15 Practical Periods:- Total Periods: 60

Reference Books:

1. Veerarajan T, Engineering Mathematics I , McGraw-Hill Education(India) Private Limited, 2014 2. Veerarajan T, Engineering Mathematics II , McGraw-Hill Education(India) Private Limited, 2015 3. Venkataraman M.K., Engineering Mathematics, Vol. I&II, The National Publishing Company, Chennai, 2008. 4. Erwin Kreyszig, Advanced Engineering Mathematics (9 th Ed), John Wiley & Sons, New Delhi, 2011. 5. Ramana B.V., Higher Engineering Mathematics, Tata McGraw Hill New Delhi, Eleventh Reprint, 2010. 6. Bali N. and Goyal M., Advanced Engineering Mathematics, Laxmi Publications Pvt. Ltd., New Delhi, 9thEdition,

2011.

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Department : Mathematics Programme : B.Tech

Semester : Second Course Category Code: BSC Semester Exam Type: TY


L T P C CA SE TM

MA202 Mathematics-II 3 1 - 4 40 60 100

Prerequisite: -

Course Outcome

CO1 Understands Matrix theory

CO2 The tool of Fourier series for learning advanced Engineering Mathematics

CO3 The tool of Fourier transform for learning advanced Engineering Mathematics

CO4 The tools of differentiation of functions of a complex variable that are used in various

techniques dealing engineering problems.

CO5 The tools of integration of functions of a complex variable that are used in various

techniques dealing engineering problems.

UNIT-I Matrices Periods: 12

Inverse and rank of a matrix, System of linear equations, Symmetric, Skew Symmetric and Orthogonal matrices, Eigenvalues and Eigenvectors of a real matrix, Characteristic equation, Properties of Eigenvalues. Cayley-Hamilton Theorem (statement only), Diagonalization of matrices.

CO1

UNIT-II Fourier Series Periods: 12

Dirichlet’s conditions - Expansion of periodic functions into Fourier series- Change of interval- Half-range Fourier series. Complex form of Fourier series - Root mean square value - Parseval’s theorem on Fourier coefficients - Harmonic analysis.

CO2

UNIT-III Fourier Transform Periods: 12

Fourier Integral Theorem(statement only)- Fourier transform, Inverse Fourier transform, definition and properties - Evaluation of integrals- Fourier cosine and sine transform, definitions and evaluation of integrals using cosine and sine transforms.

CO3

UNIT-IV Complex Valued function and Conformal Mapping Periods: 12

Definition of a Complex valued function f(z) and its derivative - Analytic functions -Necessary condition for a function f(z) to be analytic (in Cartesian) - Cauchy-Riemann equation - statement of C-R equation in polar form -sufficient condition for f(z) to be analytic(statement only)- harmonic function- Harmonic and orthogonal properties of analytic function – Construction of analytic functions. Conformal mapping – Simple and standard transformations like w = z2, ez, z+c, cz, sinz, 1/z, Bilinear transformation (excluding Schwarz- Christoffel transformation).

CO4

UNIT-V Complex Integration Periods:12

Cauchy’s Integral theorem, Cauchy’s integral formula (without proof) and problems, Taylor’s and Laurent’s theorem (without proof), Classification of singularities. Residues and evaluation of residues – Cauchy’s Residue theorem, Contour integration – Evaluation of real integrals – unit circle and semi-circular contour (excluding poles on boundaries).

CO5

Lecture Periods: 45 Tutorial Periods: 15 Practical Periods: Total Periods: 60

Reference Books:

1. Veerarajan T., Engineering Mathematics II , McGraw-Hill Education(India) Private Limited, 2018 2. Veerarajan T., Transforms and Partial Differential Equations , McGraw-Hill Education(India) Private Limited,

2016 3. Venkataraman M.K., Engineering Mathematics, Vol. II and III, The National Publishing Company, 2008. 4. Erwin Kreyszig, Advanced Engineering Mathematics (Ninth Edition), John Wiley & Sons, New Delhi, 2011 5. Ramana B.V., Higher Engineering Mathematics, Tata McGraw Hill New Delhi, Eleventh Reprint, 2010. 6. Bali N. and Goyal M., Advanced Engineering Mathematics, Laxmi Publications Pvt. Ltd., New Delhi, Ninth

Edition, 2011.

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Department : Physics Programme : B.Tech.(CH)

Semester : First/Second Course Category Code: BSC Semester Exam Type: TY


L T P C CA SE TM

PH201 Physics 3 1 - 4 40 60 100

Prerequisite -

The course will enable the student to:

Course

Outcome

CO1 Understand electric and magnetic field & potential

CO2 Study the basics of dielectric materials and its importance

CO3 Understand the concepts of wave mechanics and its applications

CO4 To study the optical phenomena arising due to interference, diffraction and polarization

CO5 To discuss the fundamentals of Lasers, fiber optics and its real time applications

UNIT-I Electromagnetic theory Periods: 12

Brief review of electrostatics, electric field and potential – divergence and curl of electrostatic field – Gauss

law and its applications, Laplace’s equation in one, two and three dimension.

Brief review of magnetostatics, Biot-Savart law – divergence and curl of static magnetic field – Ampere’s law –

magnetic vector potential – comparison of electrostatics and magnetostatics.

CO1

UNIT-II Dielectrics Periods: 12

Dielectric polarization and its mechanisms – dielectric loss – dielectric breakdown – calculation of electronic

polarizabilities and ionic polarizabilities – temperature and frequency dependence of polarization – internal

field in solids – Clausius-Mossotti relation – ferroelectricity – ferroelectric hysteresis.

CO2

UNIT-III Quantum mechanics Periods: 12

Matter Waves – de Broglie hypothesis – uncertainty principle – Schrödinger wave equations – time dependent

– time independent – physical significance of wave function – application to particle in a one dimensional

potential box – concept of quantum mechanical tunneling (without derivation) – applications of tunneling

(qualitative) to alpha decay, tunnel diode, scanning tunneling microscope.

CO3

UNIT-IV Wave optics Periods: 12

Interference: airwedge – Newton’s rings – Michelson’s interferometer – types of fringes – determination of

wavelength of a light source.

Diffraction: concept of resolution of spectral lines – Rayleigh’s criterion – resolving power of grating, prism &

telescope.

Polarisation: Basic concepts of double refraction – circular and elliptical polarization – quarter and half wave

plates – optical rotation – specific rotatory power – Laurent’s half shade polarimeter.

CO4

UNIT-V Lasers and Fiber optics Periods: 12

Lasers: Principles of laser – spontaneous and stimulated emissions – Einstein’s theory of matter radiation

interaction – A and B coefficients – population inversion and laser action – optical resonators(qualitative) –

types of lasers –Nd:YAG, CO2 laser, GaAs laser – industrial & medical applications of lasers (any two).

Fiber optics: Principle and propagation of light in optical fiber – numerical aperture and acceptance angle –

step index and graded index fiber – qualitative ideas of attenuation in optical fibers – fiber optic

communication (schematic), active and passive fiber optic sensors, endoscope.

CO5

Lecture Periods: 45 Tutorial Periods: 15 Practical Periods: - Total Periods: 60

Reference Books

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1. David Griffiths, Introduction to Electrodynamics, 3rd Edition, Eastern Economy Edition., 2011 2. A.S. Vasudeva, Modern Engineering Physics, S. Chand & Co, 2006. 3. D. J. Griffiths, “Quantum mechanics”, Pearson Education, 2014. 4. V. Rajendran, Engineering Physics, 2nd Edition, TMH, New Delhi 2011 5. Avadhanulu M. N. , Engineering Physics, S. Chand & Co, 2007 6. David Halliday, Robert Resnick and Jearl Walker, Fundamentals of Physics, Wiley publications, 2013 7. H.J. Pain, The physics of vibrations and waves, Wiley publications, 2005 8. Ajoy Ghatak, Optics, 5th Edition TMH, New Delhi, 2012 9. Orazio Svelto, 2nd Edition, plenum Press, Principles of Lasers, 1982. 10. K. Thyagarajan and Ajoy Ghatak, Lasers Fundamentals and Applications, 2nd Edition, Springer 2010.

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Department : Physics Programme : B.Tech.(CH)

Semester : First/Second Course Category Code: BSC Semester Exam Type: LB


L T P C CA SE TM

PH202 Physics Laboratory - - 3 1.5 40 60 100

Prerequisite -

The students will learn to experimentally measure:

Course

Outcome

CO1 Optical parameters related to the concepts included in theoretical curriculum

CO2 Characteristic parameters of Laser and optical fiber

CO3 Thermal conductivity and pressure coefficients

CO4 Magnetic field, electrical conductivity and Hall coefficient

CO5 Young’s modulus, Rigidity modulus and acceleration due to gravity

Choice of 10-12 experiments from the following

1. Radius of curvature of a Lens - Newton’s rings 2. Thickness of a thin object by air – wedge 3. Spectrometer – resolving power of a prism 4. Spectrometer – resolving power of a transmission grating 5. Spectrometer - hollow prism / ordinary & extraordinary rays by calcite prism* 6. Lorent’s Half shade polarimeter – determination of specific rotatory power

CO1

7. Determination of wavelength of a laser source using transmission grating, reflection grating (vernier calipers) & particle size determination

8. Determination of numerical aperture & acceptance angle of an optical fiber 9. Determination of optical absorption coefficient of materials using laser* 10. Michelson’s interferometer*

CO2

11. Coefficient of thermal conductivity - radial flow method

12. Coefficient of thermal conductivity – Lee’s disc method

13. Jolly’s bulb apparatus experiment – determination of α*

CO3

14. Magnetism: I – H curve

15. Field along the axis of a coil carrying current

16. Vibration magnetometer – calculation of magnetic moment & pole strength 17. Electrical conductivity of semiconductor – two probe / four probe method* 18. Hall effect in a semiconductor*

CO4

19. Determination of Young’s modulus and rigidity modulus 20. Acceleration due to gravity - compound pendulum

*Demonstration experiments CO5


Reference Books

1. Physics Practical Observation Manual, Department of Physics, Pondicherry Engineering College.

18

Department : Chemistry Programme : B.Tech

Semester : First/Second Course Category Code: BSC Semester Exam Type: TY


L T P C CA SE TM

CY201 Chemistry 3 1 - 4 40 60 100

Prerequisite: -

Course Outcome


CO1 Analyse microscopic chemistry in terms of orbitals, structure and intermolecular forces

CO2 Rationalize the bulk properties and processes

CO3 Study the concepts of electrochemistry and its applications

CO4 Understand the mechanism of chemical reactions and synthesis of molecules

CO5 Comprehension of the concepts of analytical techniques.

UNIT-I Chemical bonding and isomerism Periods: 12

Chemical bonding-valence bond theory, overlapping of orbitals. Hybridization in carbon compounds-sp, sp2 and sp3. Electron pair repulsion. Hybridization and shape of water and ammonia molecules. Molecular orbital theory-combination of atomic orbitals. Bond order. Molecular orbital diagrams for homonuclear diatomic molecules-(hydrogen to neon). Ionic, dipolar and van der Waals interactions. Structural and stereo isomerism-geometrical isomerism in alkenes. Optical isomerism-optical activity, chiral carbon. Optical isomerism in lactic acid and tartaric acid. Enantiomers, diastereomers and meso compounds. Resolution of racemic mixtures, racemization, asymmetric synthesis, Walden inversion.

CO1

UNIT-II Water chemistry and reaction kinetics Periods: 12

Water chemistry-hard and soft water, removal of hardness by ion exchange and zeolite processes. Determination of hardness by EDTA method. Desalination-Reverse osmosis. Adsorption-adsorption of gases on solids-Freundlich and Langmuir adsorption isotherms. Factors affecting adsorption of gases on solids. Chemical kinetics-rate of a reaction, factors affecting rate of reaction, first and second order rate equations. Half-life of reactions.

CO2

UNIT-III Electrode potential and corrosion Periods: 12

Electrode potential, electromotive force, reference electrodes-hydrogen, Ag/AgCl, calomel and glass electrodes. Nernst equation and applications. Electrolyte concentration cell. Batteries-Primary and secondary batteries. Dry cell, alkaline battery, Ni-Cd battery and lead-acid battery. Fuel cell-Hydrogen-oxygen fuel cell. Corrosion-dry and wet corrosion, mechanism of electrochemical corrosion, galvanic, pitting and concentration cell corrosion. Factors influencing corrosion. Corrosion control by cathodic protection. Anodization.

CO3

UNIT-IV Introduction to reaction mechanism Periods: 12

Introduction to reaction mechanism-factors influencing a reaction, homolytic and heterolytic bond fission. Reaction intermediates-carbonium ion, carbanion, free radicals and carbenes. Electrophiles and nucleophiles. Mechanism of free radical substitution-chlorination of methane. Mechanism of electrophlic substitution-bromination of benzene. Nucleophilic substitution-SN2-hydrolysis of methyl bromide, SN1-hydrolysis of t-butyl bromide. Elimination reactions-E1 and E2. Addition reactions-nucleophilic and electrophilic. Synthesis of aspirin, paracetamol, sulfanilamide and chloroquine.

CO4

UNIT-V Analytical techniques Periods: 12

Absorption and emission of radiation. Beer-Lamberts law. Ultraviolet and visible spectroscopy-basic principles and instrumentation. Basic principles and instrumentation of atomic absorption spectrometry, hollow cathode lamp. Conductivity-equivalent and molar conductance, cell constant. Conductometric titration-types of conductometric titrations. Potentiometry-principle of acid base titration. Chromatography- Principles and instrumentation of gas Chromatograph.

CO5


Reference Books 1. P.C. Jain and Monika Jain, Engineering Chemistry, Dhanpat Rai Publishing Company, New Delhi, 2016. 2. S.S. Dara and S.S Umare, A Textbook of Engineering Chemistry, S. Chand & Co., Ltd. New Delhi, 2013. 3. Arun Bahl, B.S. Bahl and G.D. Tuli, Essentials of Physical Chemistry, S. Chand and Company Ltd, New Delhi, 2016 4. Arun Bahl and B.S. Bahl, A Text Book of Organic Chemistry, S. Chand and Company Ltd, New Delhi, 2011 5. B.R. Puri, L.R. Sharma and K.C Kalia, Principles of Inorganic Chemistry, Milestone Publishers, New Delhi, 2007 6. G.R. Chatwal and S.K. Anand, Instrumental Methods of Chemical Analysis, Himalaya Publishing House Pvt Ltd, New Delhi, 2005

7. D.A. Skoog, F.J. Holler and T.A. Nieman, Principles of Instrumental Analysis, Thomson Asia Pvt. Ltd, Singapore, 2004.

19

Department : Chemistry Programme : B.Tech.(CH)

Semester : First/Second Course Category Code: BSC Semester Exam Type: LB


L T P C CA SE TM

CY202 Chemistry Laboratory - - 3 1.5 40 60 100

Prerequisite -

Course Outcome

The students will learn to:

CO1 Determine rate constants and order of reactions

CO2 Measure molecular/system properties such as surface tension, viscosity, partition coefficient, hardness of water, adsorption, saponification value and acid value

CO3 Analyze quantitatively the contents of samples

CO4 Use conductivity, potentiometric and chromatographic techniques

CO5 Analyse a salt sample

Choice of 10-12 experiments from the following:

1. Kinetic study of acid hydrolysis of ethyl acetate

CO1

2. Determination of surface tension and viscosity 3. Partition of benzoic acid between benzene and water 4. Total hardness of water - Determination by EDTA method 5. Freundlich adsorption isotherm - Adsorption of acetic acid on charcoal 6. Saponification value and acid value of an oil

CO2

7. Chloride content of water - Determination by Mohr’s method 8. Determination of oxalic acid by permanganometry 9. Determination of ferrous by permanganometry 10. Determination of ferrous and ferric by dichrometry 11. Determination of carbonate and bicarbonate in a mixture 12. Beer-Lamberts law - Determination of ferrous by colorimetry 13. Magnesium content in water - Determination by EDTA method 14. Acetic acid content in vinegar 15. Dissolved oxygen content in water - Determination by Winkler’s method. 16. Determination of available chlorine in bleaching powder.

CO3

17. Conductometric titration 18. Potentiometric titration 19. Thin layer chromatography

CO4

20. Chemical analysis of salt for cations and anions CO5

Lecture Periods: Tutorial Periods: - Practical Periods: 45 Total Periods: 45

Reference Books

1. Lab Manual, Department of Chemistry, Pondicherry Engineering College, Puducherry, 2018. 2. V. Venkateswaran, R. Veeraswamy and A.R. Kulandaivelu, Basic Principles of Practical Chemistry, Sultan Chand &

Sons, New Delhi, 2001. 3. J. Mendham, R.C. Denney, J.D. Barnes and M. Thomas, Vogel’s Text Book of Quantitative Chemical Analysis, Pearson

Education, New Delhi, 2002.

20

Department : Humanities and Social Sciences Programme : B.Tech

Semester : First/Second Course Category Code: HSM Semester Exam Type: TY


L T P C CA SE TM

HS201 English for Communication 2 - 2 3 40 60 100

Prerequisite -

Course

Outcome

CO1 To help the learners to develop their technical communication skills

CO2 To equip the learners with skills required for developing their reading prowess.

CO3 To enhance the writing skills of learners by providing practice in writing.

CO4 To instil confidence in learners to develop their speaking skills and enable them to articulate

with ease.

CO5 To facilitate vocabulary enhancement and grammatical correctness in communication.

UNIT-I TECHNICAL COMMUNICATION Periods: 12

Nature of Technical communication – Forms of Technical Communication – General and Technical

Communication – Importance and need –Organization in Technical Communication – Style – ABC of Technical

Communication –Technical Communication Skills.

CO1

UNIT-II COMPREHENSION AND ANALYSIS Periods: 12

Technical and Non-Technical passages – Reading methods – Skimming – Scanning– Extensive and Intensive

reading – Inferring – Contextual meaning – summary – note making. CO2

UNIT-III PRACTICE IN WRITING Periods: 12

Sentence Structures – Use of phrases and clauses in sentences – coherence in writing – principles for paragraph

writing –Essay Writing – describing – defining – classifying – Business letters – memorandum – instructions – E-

mail –reports.

CO3

UNIT-IV SPEAKING PRACTICE Periods: 12

Pronunciation –Basics of Phonetics– Conversations and dialogues –formal presentations – Group Discussions –

Extempore speaking – Debates- Role Plays– interview skills. CO4

UNIT-V GRAMMAR AND VOCABULARY BUILDING Periods: 12

Word formation – root words from foreign languages and their use in English – Prefixes and suffixes –subject-

verb agreement – Articles – voice – preposition– importance of punctuation – Redundancies – synonyms,

Antonyms and standard abbreviations– Indianisms.

CO5

Lecture Periods: 30 Tutorial Periods: - Practical Periods: 30 Total Periods: 60

Reference Books

1. Sudarshana, N.P and C. Savitha. English for Technical Communication. Noida: CUP, 2016. 2. Shoba, K N and Lourdes Joavani Rayen. Communicative English. Chennai: CUP, 2017. 3. Rizvi, Ashraf, M. Effective Technical Communication. New Delhi: McGraw, 2017. 4. Daniel Jones. English Pronouncing Dictionary. Cambridge University Press, 2003. 5. Dutt, Kiranmai P and Geetha Rajeevan. Basic Communication Skills. New Delhi: CUP,2013 6. Sanjay Kumar and Pushpalata. Communication Skills. New Delhi: OUP, 2011. 7. Mohan, Krishna and Meera Banerji. Developing Communication Skills. 2nd edition. Delhi: Macmillan, 2012. 8. Relevant material from newspapers, magazines and journals will be used for integrated practice.

21

Department : Mechanical Engineering Programme : B.Tech

Semester : First/Second Course Category Code: ESC Semester Exam Type: LB


L T P C CA SE TM

ME201 Workshop and Manufacturing Practice 0 0 3 1.5 40 60 100

Prerequisite

Course

Outcome

CO1 To convey the basics of mechanical tools used in carpentry section and establish hands on

experience in making the different carpentry joints

CO2 To gain knowledge on types of tools and machines used in sheet metal shop and perform

some exercises

CO3 To develop basic welding and fitting joints using the hand tools and establish the importance

of joints and fitting in engineering applications

CO4 To gain knowledge of the different machines used in manufacturing processes which are

commonly employed in the industry, to fabricate components using different materials

CO5 To carry out simple manufacturing operations in lathe, drilling and shaping machine

UNIT-I Carpentry Periods: 9

Study of tools and machines in carpentry

Practice on :1.Half Lap joint 2.Corner Mortise joint and 3.Dovetail joint CO1

UNIT-II Sheet Metal Periods: 9

Study of tools and machineries in sheet metal shop

1.Frustum of cone 2.Waste collection tray and 3.Rectangular box CO2

UNIT-III Welding and Fitting Periods: 9

Lectures/demonstrations/videos on Welding and fitting operations with simple exercise. 1. Filing and Job

preparation 2. V-Fitting and 3. Simple lap joint CO3

UNIT-IV Study of tools and machines Periods: 6

Study of tools and machines in manufacturing lab

1. Lathe machine 2.Drilling machine and 3.Shaping machine CO4

UNIT-V Simple Exercises in Lathe/Drilling machine/Shaper Periods: 12

Simple operations in lathe, drilling and shaping

1.Facing and Turning 2.Step Turning 3.Drilling in a flat plate with different drill dimensions and 4.Cube in

Shaping

CO5


Reference Books

1. Hajra Choudhury S.K., Hajra Choudhury A.K. and Nirjhar Roy S.K., “Elements of Workshop technology”, Vol. I 2008 and Vol. II 2010, Media promoters and publishers private limited, Mumbai.

2. Kalpakjian S. And Steven S. Schmid, “Manufacturing Engineering and Technology”, 4th edition, Pearson Education India Edition, 2002.

3. H.N.Gupta, R.C.Gupta and Arun Mittal, Manufacturing Processes, New Age Publications, 2001.

22

Department : Mechanical Engineering Programme : B.Tech

Semester : First/Second Course Category Code: ESC Semester Exam Type: TY


L T P C CA SE TM

ME202 Engineering Graphics and Computer Aided Drawing

2 - 4 3 40 60 100

Prerequisite -

Course Outcome

CO1 Students learn to properly dimension and annotate engineering drawings as per standards of engineering drawing practice.

CO2 Students are made to follow and understand the basics of engineering drawing with simple solids.

CO3 Students can properly apply and produce sectional views.

CO4 Students are able to properly create multi-view orthographic drawings from three dimensional diagrams. Students are able to present a drawing in orthographic and isometric projections.

CO5 Students learn the application of engineering graphics through computer-aided drafting.

UNIT-I Periods: 18

Introduction to Engineering graphics, Standards for Engineering Drawing practice, Lettering, Line work and Dimensioning, Projection of Lines, Projection of Planes

CO1

UNIT-II Periods: 18

Projections of simple solids CO2

UNIT-III Periods: 18

Sections of solids and Development of surfaces CO3

UNIT-IV Periods: 18

Isometric Projections and Orthographic Projections CO4

UNIT-V Periods: 18

Introduction to Computer Graphics and Drafting, Auto CAD, 2-D diagrams of simple geometries using Auto-CAD script.

CO5


Reference Books

1. K.R. Gopalakrishna and Sudhir Gopalakrishna, Engineering Graphics, Inzinc Publishers, 2007. 2. K.Venugopal, Engineering Drawing & Graphics + Auto CAD, 4th edition, New Age Int’lPublication Ltd., 2004. 3. BIS, Engineering Drawing practices for Schools & College, SP 46: 2003. 4. T. Jeyapoovan, Engineering Graphics using AUTOCAD, 7th edition, VIKAS Publishing House (P) Ltd., 2015. 5. N.D. Bhatt, Engineering Drawing, 49th edition, Charotar Publishing House, 2014. 6. K.V. Natarajan, A Text Book of Engineering Drawing, Dhanalakshmi Publishers, 2006. 7. M. B. Shah and B. C. Rana, Engineering Drawing, 2nd edition, Pearson Publications, 2018. 8. Agrawal B. & Agrawal C. M. (2012), Engineering Graphics, TMH Publication 9. http://www.3ds.com/products/catia/ 10. http://en.wikipedia.org/wiki/CATIA

http://www.3ds.com/products/catia/

http://en.wikipedia.org/wiki/CATIA

23

Department : Electrical and Electronics Engineering Programme : B.Tech



L T P C CA SE TM

EE201 Basic Electrical Engineering 3 1 - 4 40 60 100

Prerequisite -

Course Outcome

CO1 To understand the basic concepts of DC circuits and theorems.

CO2 To explain the concepts of AC circuits and resonance.

CO3 To understand the basic concepts of magnetic circuits and transformer.

CO4 To explain the working principle, construction, applications of electrical machines.

CO5 To Gain knowledge of working of power plants and fundamentals of switch gear and

earthing.

UNIT-I DC Circuits Periods: 12

Electrical circuit elements (R, L and C) - Definition of Voltage, Current, Power and Energy – Ohm’s law, Kirchoff current and voltage laws, analysis of simple circuits with DC voltage – Division of current in series and parallel circuits – Star-delta conversion – Node and mesh method of analysis of DC circuits – Network Theorems: Thevenin, Norton and Superposition Theorems.

CO1

UNIT-II AC Circuits Periods: 12

Representation of sinusoidal waveforms, peak and rms values, phasor representation, real power, reactive power, apparent power, power factor. Analysis of single-phase ac circuits consisting of R, L, C, RL, RC, RLC combinations (series and parallel). Resonance: Series and parallel resonance. Three-phase balanced circuits: voltage and current relations in star and delta connections – Power measurement by two Wattmeter method.

CO2

UNIT-III Transformers Periods: 12

Laws of Electromagnetic induction – Ampere’s circuital law, Faraday’s law and Lenz law – Dot rule. Magnetic materials, B-H characteristics. Single phase transformer: Construction and working, losses in transformers, regulation and efficiency. Auto-transformer and three-phase transformer connections.

CO3

UNIT-IV Electrical Machines Periods: 12

Elementary concept of rotating machines – Flemming’s right hand and left hand rule – DC Machines: Construction and working of DC Machines - Generator and Motors – Emf equation of DC generator and back emf of DC motor –characteristics - Types of DC Machines. AC Machines: Construction and working of Single phase & three phase induction motors and synchronous generator (qualitative approach only).

CO4

UNIT-V Power Plants and LT Switch gear Periods: 12

Power Plants: Layout of thermal, hydro and nuclear power generation (block diagram approach only). Components of AC transmission and distribution systems – One-line diagram. Components of LT Switchgear: Switch Fuse Unit (SFU), MCB, ELCB, MCCB, Types of Wires and Cables. Earthing. Elementary calculations for energy consumption.

CO5


Reference Books

1. D. P. Kothari and L. J. Nagrath, “Basic Electrical Engineering”, 3rd Edition, Tata McGraw Hill, 2017. 2. D. C. Kulshreshtha, “Basic Electrical Engineering”, Tata McGraw Hill, 2011. 3. Rajendra Prasad, “Fundamentals of Electrical Engineering”, 3rd Edition, PHI Learning Private Limited, 2014. 4. L. S. Bobrow, “Fundamentals of Electrical Engineering”, Oxford University Press, 2011. 5. E. Hughes, “Electrical and Electronics Technology”, Pearson, 2010. 6. V. D. Toro, “Electrical Engineering Fundamentals”, Prentice Hall India, 1989.

24

Department : Electrical and Electronics Engineering Programme : B.Tech



L T P C CA SE TM

EE202 Basic Electrical Engineering Laboratory - - 3 1.5 40 60 100

Prerequisite -

Course Outcome

CO1 To understand the principles of domestic wiring and electrical components.

CO2 To illustrate handling of measuring instruments and demonstrate the concepts of network theorems

CO3 To analyze RL,RC,RLC circuits

CO4 To introduce concepts of single/three phase circuits

CO5 To demonstrate the working principle of electrical machines

Any 10 experiments

1. Study of: Basic safety precautions. Concepts of domestic wiring- wires, switches, plugs, sockets, fuses and lamp holders.

2. Study of fan and tube light connections and earthing 3. Stair case wiring. 4. Bedroom wiring.

CO1

5. Use of measuring instruments. Verification of Kirchoff’s voltage and current law 6. Verification of Thevenin and Norton theorems 7. Verification of Superposition Theorem.

CO2

8. Impedance calculation of R-L, R-C & R-L-C circuits and verification. 9. Measurement of power & power factor in a single phase AC circuit using three Ammeter Method 10. Resonance: Series and parallel.

CO3

11. Measurement of various line and phase quantities for a three phase star/delta ac circuit. 12. Measurement of three phase power using two wattmeter method. 13. Energy measurement using single phase energy meter.

CO4

14. Load test on a single phase transformer. 15. Load test on a single phase induction motor.

CO5

Lecture Periods: Tutorial Periods: Practical Periods: 45 Total Periods: 45

Reference Books

1. Laboratory Manual, Department of Electrical and Electronics Engineering, Pondicherry Engineering College.

25

Department : Computer Science and Engineering Programme : B.Tech



L T P C CA SE TM

CS201 Programming for Problem Solving 3 - - 3 40 60 100

Prerequisite -

Course Outcome

CO1 Understood the phases of problem solving techniques for simple problems.

CO2 Able to write programs using the basic language constructs.

CO3 Able to build a larger programs using function oriented approaches.

CO4 Could write efficient programs using advanced concepts to optimize the memory.

CO5 Could write programs to access data from the secondary storage efficiently.

UNIT-I Algorithmic Problem Solving Periods: 9

History and Classifications of Computers – Components of Computer – Working Principle of Computer – Hardware – Software and its Types – Applications of Computers. Generations of Programming Languages – Introduction to Number System. Problem solving techniques: Program development life-cycle – Algorithms – building blocks of algorithms - Algorithmic problem solving-Flowchart– Pseudo code.

CO1

UNIT-II Data, Expressions, Statements Periods: 9

Introduction to C –C Program Structure – C Tokens: Keyword, Identifiers, Constants, Variables and Data types (simple and user-defined) – Operators and its types – Operator Precedence – Expression Evaluation – Type Conversion –Managing Input/output operations-Branching Statements – Looping Statements.

CO2

UNIT-III Arrays and Functions Periods: 9

Arrays – Two dimensional arrays, Multidimensional arrays. Character arrays. Functions: Function Prototype, Passing Arguments to Function – Call by Value and Call by Reference – Nested function call – Library Functions – User-defined Functions – Recursion. Strings – String I/O functions, String Library functions – Storage classes.

CO3

UNIT-IV Structures, Unions and Pointers Periods: 9

Structures – Arrays and structures – Nested structures – Structure as argument to functions–Union. Pointers – Declaration, Initialization and Accessing Pointer variable – Pointers and arrays – pointers as argument and return value – Pointers and strings - Pointers and structures.

CO4

UNIT-V File Management Periods: 9

Introduction to File Concepts in C – File types – I/O operations on files – File modes – Random access to files –Command line arguments. Dynamic Memory Allocation: MALLOC, CALLOC, FREE, REALLOC. Introduction to preprocessor: Macro substitution directives – File inclusion directives –Compiler Control directives – Miscellaneous directives.

CO5


Reference Books

1. Balagurusamy. E, “Programming in ANSI C”, Tata McGraw Hill, Seventh Edition, 2017. 2. Byron Gottfried & Jitender Chhabra, “Programming with C”, Schaum's Outlines Series, 2017. 3. Brian W. Kernighan & Dennis Ritchie. “The C Programming Language”, Pearson Education India; Second Edition,

2015. 4. Ashok N Kamthane, “Computer Programming”, Pearson education, Second Edition, 2012.

https://www.amazon.in/s/ref=dp_byline_sr_book_1?ie=UTF8&field-author=Byron+Gottfried&search-alias=stripbooks

https://www.amazon.in/s/ref=dp_byline_sr_book_2?ie=UTF8&field-author=Jitender+Chhabra&search-alias=stripbooks

26

Department : Computer Science and Engineering Programme : B.Tech



L T P C CA SE TM

CS202 Programming Laboratory - - 3 1.5 40 60 100

Prerequisite -

Course Outcome

CO1 Understood the program editing and compilation environment.

CO2 Able to write simple C programs using most frequently used control structures.

CO3 Apply the methods problems using arrays and functions.

CO4 Learnt to handle data processing using structures for simple applications.

CO5 Write programs that could handle file i/o and pointers.

Programming Using C

1. Study of Compilation and execution of simple C programs 2. Basic C Programs

a. Arithmetic Operations b. Area and Circumference of a circle

c. Swapping with and without Temporary Variables

CO1

3. Programs using Branching statements a. To check the number as Odd or Even b. Greatest of Three Numbers c. Counting Vowels d. Grading based on Student’s Mark

4. Programs using Control Structures a. Computing Factorial of a number b. Fibonacci Series generation c. Prime Number Checking

d. Computing Sum of Digit

CO2

5. Programs using Arrays a. Sum of ‘n’ numbers b. Sorting an Array c. Matrix Addition, Subtraction, Multiplication and Transpose

6. Programs using Functions a. Computing nCr b. Factorial using Recursion

c. Call by Value and Call by Reference

CO3

7. Programs using String Operations a. Palindrome Checking b. Searching and Sorting Names

8. Programs using Structure a. Student Information System b. Employee Pay Slip Generation

c. Electricity Bill Generation

CO4

9. Programs using Pointers a. Pointer and Array b. Pointers as argument and return value c. Pointer and Structure

10. Programs using File Operation a. Counting No. of Lines, Characters and Black Spaces b. Content copy from one file to another c. Reading and Writing Data in File

CO5

Lecture Periods: - Tutorial Periods: - Practical Periods: 45 Total Periods: 45

Reference Books

-

27

Department : Civil Engineering Programme : B.Tech

Semester : First/Second Course Category Code: MCC Semester Exam Type: -


L T P C CA SE TM

CE201 Environmental Science 3 - - Non-Credit - - -

Prerequisite -

Course Outcome

CO1 Able to understand about the environment and natural resources

available

CO2 Able to design the Rainwater harvesting and adopting the methods for recycle and reuse

of domestic water

CO3 Able to address the environmental issues namely pollution,

depletion of natural resources and degrading ecosystem

CO4 Able to develop models for resource and energy management,

which are environmental friendly and work for sustainable development of the humanity.

CO5 Able to participate in the Green initiatives in the society i.e. Energy conservation and Tree

plantation.

CO6 Able to make the solid waste segregation and conduct events related environmental

issues.

Activity – 1 Periods: 9

CO1 Water resources- Water Cycle, Distribution, Groundwater flow, Demand for water, Water pollution- causes

and effects, Water Act (1974).


CO2

Rainwater Harvesting-Methodology, components, design of rainwater harvesting system for a single house (as

per IS:15797-2008)


Domestic waste water- Definition, Characteristics, Recycling and Reuse of domestic waste water.


CO3

Air Pollution- definition, classification, causes, Sources, effects and control measures, Air Act (1981)


Solid Waste management – Causes- effects and control measures of Urban and industrial waste, Waste

management initiatives in India for human well-being.

Activity – 6 Periods: 9 CO4

Renewable and non-renewable energy resources- use of alternating energy sources – Energy management.


CO5

Green Buildings- Definition, Importance, building envelope, Problems in existing buildings, Energy use in

Buildings, Greenhouse gas emissions and indoor air pollution, green construction materials, Green building

assessment system, Case study


Importance of Tree Plantation, Display of usefulness of trees, Method of tree planting, Identify the trees

available in the PEC campus, Mass Plantation inside/outside the campus in association with the H2EC /NSS of

PEC, Store the trees to the planted by the dignitaries with the help of horticulture of PEC.


CO6

Collection and segregation of solid waste in the PEC campus in association with the H2EC /NSS of PEC


Invite guest Lectures from the Environmental experts of DSTE (for environmental issues)/REAP (for energy

efficient buildings)/Town and Country Planning/PWD of Puducherry, conducting competitions to students in

28

the topics of slogan making, poster and seminar presentations, debate and observing the important national

and international days on environmental issues to bring awareness among the students and public.

Activity Periods: 45 Tutorial Periods: - Practical Periods: - Total Periods: 45

Reference Books

1. P.Yugananth, R.Kumaravelan, Environmental Science and Engineering, Scitech Publications (Inida) P.Ltd., Delhi, 2017.

2. John Pichtel, Waste Management Practices: Municipal, Hazardous and Industrial, CRC Press,2014 3. V.S.K.V.Harish, Arunkumar, Green Building Energy Simulation and Modeling, Elsevier Science & Technology,2018 4. Anubha Kaushik and C.P.Kaushik, Environmental Science and Engineering, New Age International (P) Ltd., New

Delhi, 2010. 5. S.S.Dara, A text book of Environmental Chemistry and Pollution Control, S.Chand and Company Ltd., New Delhi,

2014. 6. IS:15797:2008, Roof Top Rainwater Harvesting-Guidelines, BIS, New Delhi 7. Energy Conservation Building Code, 2017, Bureau of Energy Efficiency, Ministry of Power, Government of India.

29

Department : Chemistry Programme : B.Tech (CH)

Semester : Third Subject Category: BSC Semester Exam Type: TY


L T P C CA SE TM

CY203 Chemistry for Chemical Engineering 4 - - 4 40 60 100

Prerequisite -

Course Outcome


CO1 Analyse the theories, which offer molecular level explanation to the properties of matter

CO2 Understand the theoretical principles underlying reaction kinetics and catalysis

CO3 Know the fundamental concepts of structure and reactions of carbohydrates

CO4 Become familiar with other biologically important molecules

CO5 Understand the reactions which are relevant to industrial processes

UNIT-I Gaseous state and Colligative properties Periods: 12

Ideal gases, equation of state, Boyle’s law, Charles law, Avogadro’s law, Daltons law, kinetic molecular theory of gases, deduction of gas laws from kinetic gas equation. Maxwell’s distribution of molecular velocities. Deviation from ideal behaviour – van der Waal’s equation of state. Colligative properties – Lowering of vapour pressure, elevation of boiling point, depression of freezing point, molecular weight determination, osmotic pressure.

CO1

UNIT-II Reaction kinetics and Catalysis Periods: 12

Effect of temperature on reaction rates, Arrhenius equation, Energy of activation. Theories of reaction rates-Collision theory, absolute reaction rate theory and Lindemann theory of unimolecular reaction. Catalysis- Characteristics of catalysts, Types of catalysts. homogeneous catalysis – kinetics of acid base catalysis, and enzyme catalysis. Heterogeneous catalysis – Kinetics of unimolecular and bimolecular surface reactions- Langmuir-Rideal – Hinshelwood mechanism.

CO2

UNIT-III Carbohydrates Periods: 12

Classification. Monosaccharides- reaction of Glucose and fructose, open chain and cyclic structures of glucose and fructose, mutarotation, epimerization, Killiani- Fisher synthesis, Ruff degradation, conversion of aldoses to ketoses and Ketoses to aldoses. Disaccharides – properties and structure of sucrose. Polysaccharides – properties and structure of starch and cellulose. Industrial applications of cellulose.

CO3

UNIT-IV Amino acids, Proteins, Enzymes, Oils and Fats Periods: 12

Amino acids-types-methods of synthesis and reactions of α-amino acid. Proteins-composition, classification and isolation of proteins. Physical and chemical properties, structure and uses of proteins. Enzymes-chemical nature, mechanism of enzyme action, factors affecting enzyme action. Applications of enzymes. Oils and fats-occurrence, general physical and chemical characteristics. Soaps and detergents-types

CO4

UNIT-V Polymers and Dyes Periods: 12

Polymers-classification. Types of polymerization- Addition polymerization-mechanism of free radical, anionic, cationic and Ziegler-Natta polymerization. Condensation polymerization-preparation of polyamides, polyesters, epoxy resins and ion-exchange resins. Natural rubber-vulcanization. Dyes – Colour and constitution, Classification of dyes by structure, preparation of azo dyes – methyl orange, congo red, triaryl amine dyes – phenolphthalein, fluorescein, Anthraquinone dyes – alizarin and indigo dye.

CO5

Lecture Periods: 60 Tutorial Periods: Practical Periods: Total Periods: 60

Reference Books:

1. B.R. Puri, L.R. Sharma and M.S. Pathania, Principles of Physical Chemistry, Vishal Publishing Co., New Delhi, 2017. 2. A.S. Negi and S.C. Anand, A Textbook of Physical Chemistry, New Age International (P) Ltd., New Delhi, 2007. 3. ArunBahl, B.S. Bahl and G.D. Tuli, Essentials of Physical Chemistry, S. Chand & Company Ltd, New Delhi, 2012. 4. K.S Tewari and N.K. Vishnoi, A Text Book of Organic Chemistry, Vikas Publishing House Pvt. Ltd, New Delhi 2017. 5. ArunBahl and B.S. Bahl, A Text Book of Organic Chemistry, S. Chand and Company Ltd, New Delhi, 2016 6. Peter Atkins and Julio de Paula, Elements of Physical Chemistry, Oxford University Press, New Delhi, 2017. 7. I.L. Finar, Organic Chemistry, Volume 1, Pearson Education, New Delhi, 2009. 8. P.L. Soni and H.M. Chawla, Text Book of Organic Chemistry, Sultan Chand & Sons, New Delhi, 2010.

9. P.C. Jain and Monika Jain, Engineering Chemistry, Dhanpat Rai Publishing Company, New Delhi, 2016.

30

Department : Civil Engineering Programme : B.Tech (CH)

Semester : Third Course Category Code: PCC

Semester Exam Type: TY


L T P C CA SE TM

CE233 Engineering Mechanics and Mechanics of Solids

3 1 0 4 40 60 100

Prerequisite:

Course Outcome

CO1 Able to Calculate the Resultant of a given force system. Identify the equilibrium of a system.

CO2 Able to draw the free body diagram to find the unknown forces using equilibrium equations

CO3 Able to draw the free body diagram of a various contact problems using Newton’s laws of friction and find the force required to maintain the equilibrium

CO4 Able to calculate the properties of section for both static and dynamic problems

CO5 Able to solve any static problem using virtual work done concepts

CO6 Able to identify the difference between terms particle and rigid body and kinematics and kinetics of the body to solve the various parameters of the dynamic problems

UNIT – I Fundamentals of Mechanics Periods: 12

Mechanics and its relevance, Force System, Definition- Force, Moment and Couple -Principle of Transmissibility, laws of mechanics, Resultant of force system – Concurrent and non-concurrent coplanar forces, Conditions of static equilibrium for coplanar force system, stability and equilibrium, concept of free body diagrams.

CO1

UNIT – II Application of Force System Periods: 12

Types loads and supports – simply supported beams, cantilever beams and plane trusses – reactions (No analysis required). Friction: Laws of friction, Static dry friction, simple contact friction problems, body on inclined planes, ladders, wedges, simple screw jack.

CO2

UNIT – III Properties of Surfaces Periods: 12

Properties of sections – centroids, center of gravity, area moment of inertia, product moment of inertia, polar moment of inertia, radius of gyration, mass moment of inertia. Principle of virtual work – work done – application to simple structural arrangements

CO3

UNIT – IV Kinematics and Kinetics of Particles Periods: 12

Introduction of Dynamics – Types of Motion – D Alembert’s principle – work energy method – work energy equation for translation and – Motion of connected bodies – work done by a spring – Impulse momentum equation – conservation of momentum – Impact of elastic bodies – oblique impart – Loss of kinetic energy.

CO4

UNIT – V Mechanics of solids Periods: 12

Simple stresses and strains-Tension, Compression and Shear stresses-Hooke’s law-Elastic Constants, Relation between elastic constants-Compound stresses-Thermal stresses-Compound bars-Shear force and bending moment for beams and frames-Theory of simple bending-Bending stress distribution at sections-Beams of uniform strength

CO5

Lecture Periods : 45 Tutorials Periods: 15 Practical Periods : - Total Periods : 60

Reference Books:

1. Bhavikatti,S.S and Rajashekarappa,K.G., Engineering Mechanics, New Age International (P) Ltd, New Delhi, 2013.

2. Timoshenko, S., Young, D.H., Rao, J.V. and SukumarPati, Engineering Mechanics, Fifth edition, McGraw Hill Education (India) Pvt. Ltd., 2013.

3. Beer, F.P and Johnson Jr. E.R, Vector Mechanics for Engineers, Vol. 1 Statics and Vol. 2 Dynamics, McGraw – Hill International Edition, 1997.

31

Department : Chemical Engineering Programme : B.Tech (CH)

Semester : Third Course Category Code: PCC Semester Exam Type: TY

Course Code

Course Name

Periods / Week Credit Maximum Marks

L T P C CA SE TM

CH201 Momentum Transfer 3 1 - 4 40 60 100

Prerequisite:

On successful completion of the course, the candidate should be able to:

Course Outcome

CO1 Appreciate the principle of fluid pressure, hydrostatic equilibrium, buoyancy and their applications in gravity and centrifugal separators.

CO2 Explain the basic laws governing the flow of non viscous and viscous fluids and their rheological behaviour

CO3 Write momentum balance equations for different flow geometries and calculate pressure drop and friction factor.

CO4 Have knowledge of various flow measuring devices and pumps used for transportation of fluids

CO5 Appreciate the principle of flow past immersed bodies and drag coefficient and use these concepts in calculating terminal settling velocity and pressure drop in packed and fluidised beds

UNIT-I Fluid Statics Periods: 12

Fluid Statics – Fluid density, compressible and incompressible fluids; Pressure, relationship between pressure and density for ideal gas; Hydrostatic equilibrium in gravitational and centrifugal force fields; Gravity decanters and centrifuge ; Pascal’s law, hydraulic lever; Measurement of fluid pressure, manometers, Archimedes principle and buoyancy

CO1

UNIT-II Fluid Dynamics Periods: 12

Fluid Dynamics – ideal flow of fluids (non-viscous and incompressible fluids), Continuity equation and energy equation (Bernoulli’s equation), applications. Flow of viscous fluids - Shear rate, Shear stress, Newton’s law of fluid motion, Viscosity, concept of momentum transfer, Rheology of fluids - Newtonian and non-Newtonian fluids, laminar and turbulent flow, Reynolds number and transition from laminar to turbulent flow.

CO2

UNIT-III Fluid Dynamics Periods: 12

Momentum balance equation, Hagen-Poiseulle equation , Flow of fluids through circular pipe, Annulus, Flow between parallel plates, , flow through non circular cross section – equivalent diameter, Correction of Bernoulli’s equation for velocity and friction, friction factor, friction factor Vs Reynold’s number for laminar flow, Friction factor correlations for turbulent flow through pipes, Dimensional analysis- Rayliegh’s and Buckinham Pi methods, friction loss across sudden expansion, contraction, valves and fittings.

CO3

UNIT-IV Fluid Transportation Periods: 12

Transportation and metering of fluid - Orifice meter, Venturimeter, Pitot tube, Rotameter, Weirs and Notches, Pumps and Compressors, Performance and characteristics of centrifugal pumps, NPSH, Cavitation , Priming

CO4

UNIT-V Flow past immersed bodies Periods: 12

Flow past immersed bodies - Boundary layer, drag and drag coefficient, Stokes law and terminal settling velocity. Flow of fluids through bed of solids - Darcy’s law, Ergun’s equation, Fluidization, minimum fluidization velocity, pneumatic transport.

CO5


Reference Books:

1. Noel de Nevers, Fluid mechanics for Chemical Engineers, TATA McGraw- Hill edition,3rd Edition 2011. 2. W.L.Mc.Cabe, J.C.Smith and P.Harriot, Unit Operations of Chemical Engineers, McGraw Hill International edition, 7th

Edition, 2009. 3. Coulson J.M and Richardson J.F., Chemical Engineering - Volume 1, Elsevier Press, 6th Edition, 2006.

32

Department : Chemical Engineering Programme : B.Tech (CH)

Semester : Third Course Category Code: PCC


Course Code

Course Name

Periods / Week

Credit Maximum Marks

L T P C CA SE TM

CH202 Process Calculations 3 1 - 4 40 60 100

Prerequisite

On Successful completion of the course, students should be able to:

Course Outcome

CO1 Express various properties in different system of units and understand various process principles.

CO2 Develop material balance equations on various unit operations.

CO3 Perform material balances on systems involving chemical reactions and have knowledge on recycle, purge and bypass operations.

CO4 Perform Energy Balance calculations on various processes in Chemical Engineering

CO5 Write Energy Balances for processes with Chemical Reaction.

UNIT-I Process Principles Periods: 12

Introduction to Chemical engineering calculations, units and dimensions, mole and molecular weight, properties of gases, vapours, liquids, solutions and solids, gas laws, partial pressures, vapour pressures, saturation and equilibria, Raoults law, partial saturation and humidity. Introduction to Material and Energy Balances- Derivation of Steady state and Unsteady state Balance equations for any system

CO1

UNIT-II Material Balances on Nonreactive System Periods: 12

Material balances without chemical reactions, stoichiometry and unit operations-distillation, absorption, stripping, extraction, leaching, crystallization, drying, and psychrometry. Recycle, purge and bypass calculations.

CO2

UNIT-III Material Balances on Reactive system Periods: 12

Material balances involving chemical reactions, simple oxidation reaction, calculations involving combustion of gaseous, liquid and solid fuels. Recycle, purge and bypass calculations. Introduction to unsteady balances , Balances on mixing vessel, Level Systems

CO3

UNIT-IV Energy Balances on Nonreactive System Periods: 12

Energy balance - heat capacity and calculation of enthalpy changes, Enthalpy changes for phase transitions, evaporation, Clausius - Clapeyron equation. CO4

UNIT-V Energy Balances on Reactive Systems Periods: 12

Energy balances with chemical reaction - heat of reaction and adiabatic flame temperature calculations CO5

Lecture Periods: 45 Tutorial Periods: 15 Practical Periods: Total Periods:60

Reference Books:

1. Bhatt and S.M.Vora, Stoichiometry, Tata McGraw Hill, 5th Edition, 2013. 2. David.M.Himmelblau and Riggs , Basic Principles and Calculations in Chemical Engineering, Prentice Hall of India Ltd., 7th Edition, 2004 3. A.Hougen, K.M. Watson and K.A.Ragatz, Chemical Process Principles, Vol 1, CBSE Publisher, 1980. 4. Richard M. Felder, Ronald W.Rousseau, Elementary Principles of Chemical Processes, Wiley Publications, 3rd Edition, 2007. 5. V.Venkataramani, N.Anantharaman and K.M.Meera Sheriffa Begum, Process Calculations, PHI Learning Private Limited, 2nd Edition, 2012. 6. D.C.Sikdar, Chemical Process Calculations, PHI Learning Private Limited, 2nd Edition, 2013.

33

Department : Chemical Engineering Programme : B.Tech

Semester : Third Subject Category: BSC Semester Exam Type: TY


L T P C CA SE TM

SH201 Biology for Engineers 3 - - 2 40 60 100

Prerequisite Nil

Course Outcome

After studying the course, the student will be able to:

CO1 Convey that classification per se is not what biology is all about but highlight the underlying criteria, such as morphological, biochemical and ecological

CO2 Highlight the concepts of recessiveness and dominance during the passage of genetic material from parent to offspring

CO3 Convey that all forms of life have the same building blocks and yet the manifestations are as diverse as one can imagine

CO4 Gain a basic understanding of enzyme action and factors affecting their activity.

CO5 Identify and classify microorganisms.

UNIT-I Classification Periods: 9

Classification outline based on (a) cellularity- Unicellular or multicellular (b) ultrastructure prokaryotes or eukaryotes (c) Energy and Carbon utilisation -Autotrophs, heterotrophs, lithotropes (d) Ammonia excretion – aminotelic, uricoteliec, ureotelic (e) Habitats- acquatic or terrestrial (e) Molecular taxonomy three major kingdoms of life.

CO1

UNIT-II Genetics Periods: 9

Mendel’s laws, Concept of segregation & independent assortment. Concept of allele. Recessiveness, and dominance. Single gene disorders in humans – Sickle cell disease, Phenylketonuria.

CO2

UNIT-III Biomolecules Periods: 9

Carbohydrates: Types, Structural & functional importance. Lipids: Classification - Simple, compound, & derived, Importance of lipid soluble vitamins. Amino acids – general structure, essential amino acids. Proteins - Levels of protein structure, structural & functional importance of proteins, Enzymes- Definition, Enzyme Activity & Units, Specific Activity, Specificity, Factors affecting enzyme activity. Nucleic acids: Types and importance.

CO3

UNIT-IV Metabolism Periods: 9

Introduction: Food chain & energy flow. Definitions - Anabolism & Catabolism. Photosynthesis: Reaction and importance. Glycolysis & TCA cycle. ATP – the energy currency of cells.

CO4

UNIT-V Microbiology Periods: 9

Concept of single celled organisms. Concept of species & strains. Identification & classification of microorganisms. Virus – Definition, types, examples.

CO5


Reference Books:

1. Biology: A global approach: Campbell, N. A.; Reece, J. B.; Urry, Lisa; Cain, M,L.; Wasserman, S. A.; Minorsky, P. V.; Jackson, R. B. Pearson Education Ltd

2. Outlines of Biochemistry, Conn, E.E; Stumpf, P.K; Bruening, G; Doi, R.H. John Wiley and Sons 3. Principles of Biochemistry (V Edition), By Nelson, D. L.; and Cox, M. M.W.H. Freemanand Company 4. Molecular Genetics (Second edition), Stent, G. S.; and Calender, R. W.H. Freeman andcompany, Distributed by

Satish Kumar Jain for CBS Publisher 5. Microbiology, Prescott, L.M J.P. Harley and C.A. Klein 1995. 2nd edition Wm, C.Brown Publishers.

34

Department : Chemistry Programme :B.Tech. (CH)

Semester : Third Subject Category: BSC Semester Exam Type: LB

Course Code Course Name Hours / Week Credit Maximum Marks

L T P C CA SE TM

CY204 Chemistry Lab for Chemical Engineering - - 3 1.5 40 60 100

Prerequisite -

Outcomes

The students will be able to:

CO1 Identify simple organic compounds

CO2 Synthesize small molecules

CO3 Determine physical constants such as boiling point and melting point

Choice of 10-12 experiments from the following:

1. Identification of organic compounds through group detection - Identification of aldehydes, ketones, carboxylic acids, amides, esters, amines, ethers, alcohols, hydrocarbons, carbohydrates, phenols, amino acids, peptides and proteins.

CO1

2. Synthesis of organic compounds involving reactions such as oxidation, reduction, bromination, nitration, acetylation, hydrolysis, esterification and polymerization.

CO2

3. Determination of physical constants: Boiling point, melting point and TG analysis. CO3


Reference Books:

1. Laboratory Manual prepared by Department of Chemistry, Pondicherry Engineering College, Puducherry, 2019. 2. B.S. Furniss, A.J. Hannaford, P.W.G. Smith, A. R. Tatchell, Vogel’s Text Book of Practical Organic Chemistry,

Pearson Education, New Delhi, 2005.

35

Department : Humanities and social Sciences Programme: B.Tech. (CH)

Semester : Third Subject Category: MCC Semester Exam Type: -


L T P C CA SE TM

SH202 Indian Constitution 3 - - - - - -

Prerequisite Nil

Course Outcome

The course will enable the students to:

CO1 understand the essence and significance of the constitution

CO2 recognize ones fundamental duties and rights

CO3 appreciate the structure and functions of legislature, executive and judiciary

CO4 understand the functioning of state governments and union territories

CO5 understand the centre-state relations and functioning of constitutional bodies

UNIT-I Introduction of Indian Constitution Periods: 09

The Making of Indian Constitution - The Constituent Assembly - Sources of Indian Constitution -

Preamble and the Supreme Court’s Judgments on Preamble.

CO1

UNIT-II State, Rights and Duties Periods: 09

State and Union Territories – Citizenship - Fundamental Rights - Directive Principles of State Policy -

Fundamental Duties. CO2

UNIT-III Union Government Periods: 09

Union Government - The Powers and Functions of the President, Vice–President, Council ofMinisters, Prime Minister, Judiciary, Supreme Court - Judicial Review - Judicial Activism- Public InterestLitigation - Power and Functions of the Parliament -Budget Power and Functions of Parliament, Speaker of Lok Sabha.

CO3

UNIT-IV State Governments Periods: 09

State Governments – Governor - State Council of Ministers - Chief Minister- Legislative Assembly- High Courts - Union Territories -Panchayati Raj Institutions - 73th and 74th Constitutional Amendment – Gram Panchayats - Block Panchayats - Municipalities.

CO4

UNIT-V Union- State Relations, Constitutional Bodies Periods: 09

Centre – State Relations - Public Service - Election Commission - NITI Ayog, Emergency Powers of the President- Constitution Amendment Procedure- Right to Information Act - Right to Education. Major Constitutional Amendments and their impact on Indian Political System.

CO5


Reference Books: 1. Austin, Granville. The Indian Constitution: Cornerstone of a Nation. Oxford University Press, 1999. 2. Basu, Durga Das, et al. Introduction to the Constitution of India. 20th ed., Thoroughly Rev, Lexis Nexis

Butterworths Wadhwa Nagpur, 2008. 3. Choudhry, Sujit, et al., editors. The Oxford Handbook of the Indian Constitution. Oxford University Press, 2016. 4. Bakshi, Parvinrai Mulwantrai, and Subhash C. Kashyap, The Constitution of India (Universal Law Publishing,

2016) 5. Bhargava, Rajeev, ‘Politics and Ethics of the Indian Constitution’, 2009 6. Rajeev Bhargava - ‘The Promise of India’s Secular Democracy’, 2010 7. Chakrabarty, Bidyut, India’s Constitutional Identity: Ideological Beliefs and Preferences (Routledge, 2019) 8. Jayal, Niraja Gopal, and Pratap Bhanu Mehta, The Oxford Companion to Politics in India, Oxford University Press,

2010 9. Kashyap, Subhash C., Our Constitution: An Introduction to India’s Constitution and Constitutional Law (NBT

India, 1994) 10. Kashyap, Subhash C. Our Parliament: An Introduction to the Parliament of India. Revised edition, National Book

Trust, India, 2011. 11. Subhash C. Kashyap Our Constitution Paperback –. (NBT India, 2012). 12. Laxmikanth, M. "INDIANPOLITY". McGraw-Hill Education "Constitution of India".

Ministry of Law and Justice, Govt. of India.

36

Department : Mathematics Programme :B.Tech. (CH)

Semester : Fourth Subject Category: BSC Semester Exam Type: TY

Course Code Course Name Hours / Week Credit Maximum Marks

L T P C CA SE TM


3 1 - 4 40 60 100

Prerequisite

Course Outcome

CO1 Understands Transform Calculus

CO2 Understands how to form partial differential equations

CO3 Solve the Partial Differential Equations

CO4 Gain knowledge on solving Boundary Value Problems

CO5 Understand basic statistics and distributions

UNIT-I LAPLACE TRANSFORMS Periods: 12

Definition of Laplace Transform, Inverse Laplace Transform, Linearity property, Laplace transform of unit step function, Unit impulse function and some elementary functions, Change of scale and first shifting property, Derivatives and integrals of Laplace transform, Transform of derivatives and integrals, Application: Solution of single ordinary linear differential equation with constant coefficients-Laplace transform of Periodic functions.

CO1

UNIT-II PARTIAL DIFFERENTIAL EQUATIONS Periods: 12

General and Singular solution of PDE, Complete Solution of First order Non-linear PDE, Lagrange's linear equation of first order, Solution of the simultaneous equations by the method of grouping and multipliers.

CO2

UNIT-III HIGHER ORDER PDE AND BOUNDARY VALUE PROBLEMS Periods: 12

Homogeneous linear PDE of higher order with constant coefficients. Solution of partial differential equation by the method of separation of variables. Application of PDE: Variable separable solutions of the one dimensional wave equation, Transverse vibration of a stretched string.

CO3

UNIT-IV ONE DIMENSIONAL AND TWO DIMENSIONAL HEAT FLOW Periods: 12

Heat Equation, Variable and separable solution of one dimensional heat equation, Temperature distribution with zero and non-zero boundary values, Two dimensional heat flow under steady state conditions(Cartesian).

CO4

UNIT-V PROBABILITY AND STATISTICS Periods: 12

Probability, Events, Sample space, Axioms of probability, Random variable (Discrete and Continuous), Expectation, Probability Distribution: Binomial, Poisson & Normal distribution and statistical parameters of these distributions, Correlation and Regression, Rank correlation.

CO5


Reference Books:

1. Veerarajan T, Engineering Mathematics II, McGraw-Hill Education(India) Private Limited, 2014 2. Veerarajan T, Transforms and Partial Differential Equations, Third Edition, McGraw-Hill Education(India) Private

Limited, 2016. 3. Venkataraman M.K., Engineering Mathematics, Third Year, Part-B, The National Publishing Company, Chennai,

2008. 4. S.C.Gupta and V.K.Kapoor, Fundamentals of Mathematical Statistics, 10th Edition, Sultan Chand &Sons, New

Delhi, 2000. 5. Erwin Kreyszig, Advanced Engineering Mathematics (9 th Ed), John Wiley & Sons, New Delhi, 2011. 6. Ramana B.V., Higher Engineering Mathematics, Tata McGraw Hill New Delhi, Eleventh Reprint, 2010. 7. Bali N. and Goyal M., Advanced Engineering Mathematics, Laxmi Publications Pvt. Ltd., New Delhi, 9thEdition,

2011.

37

Department : Chemical Engineering Programme :B.Tech. (CH)

Semester : Fourth Course Category Code: PCC Semester Exam Type: TY

Course Code

Course Name


L T P C CA SE TM

CH203 Process Heat Transfer 3 1 - 4 40 60 100

Prerequisite


Course Outcome

CO1 Identify the various modes of heat transfer and to carry out conduction calculations for various geometries

CO2 Apply the principles of heat transfer involving no phase changes for various flow systems

CO3 Apply the principles of heat transfer with phase changes for sand ply them in operations like condensation and boiling

CO4 Analyse the systems involving radiation and to solve problems pertaining to them

CO5 Explain the working principle of heat exchange equipments like heat exchangers and evaporators employed in process industries

UNIT-I Conductive Heat Transfer Periods: 12

Steady state conduction – Fourier’s law, thermal conductivity, conduction through composite multilayer plane walls, spherical walls and cylindrical walls, insulation and critical thickness of insulation, heat conduction in rods with heat generation. Heat transfer in extended surfaces - equation for heat transfer in rectangular and cylindrical fins, fin effectiveness and fin efficiency.

CO1

UNIT-II Convective Heat transfer without Phase Change Periods: 12

Principles of heat transfer in fluids - laminar flow and boundary layer theory in heat transfer, heat transfer in turbulent flow, eddy thermal diffusivity, prandtl mixing length theory, analogies between transfer of momentum and heat - Reynold’s analogy, Prandtl and Colburn analogy. Dimensional analysis in heat transfer, Correlations for the calculation of heat transfer coefficients, heat transfer coefficient for flow through a pipe, flow through a non circular conduit, flow past flat plate, flow through packed beds. Heat transfer by natural convection.

CO2

UNIT-III Convective Heat Transfer with Phase Change Periods: 12

Heat transfer to fluids with phase change - heat transfer from condensing vapours, drop wise and film wise condensation, Nusselt equation for vertical and horizontal tubes, condensation of superheated vapours, effect of non-condensable gasses on rate of condensation. Heat transfer to boiling liquids - mechanism of boiling, nucleate boiling and film boiling.

CO3

UNIT-IV Radiative Heat Transfer Periods: 12

Radiation heat transfer - Emissive power, Black body radiation, Emissivity, Stefen - Boltzman law, Plank’s law, radiation between surfaces, View factor calculations - view factor for infinitely parallel grey planes, view factor from a plane to a hemisphere, Radiation in absorbing gases.

CO4

UNIT-V Heat Transfer Equipments Periods: 12

Heat exchange equipments - Double pipe and shell and tube heat exchangers, concept of log mean temperature difference (LMTD), LMTD correction factor, overall heat transfer coefficient, dirt factor, heat exchanger effectiveness. Evaporators - single effect and multiple effect evaporators, boiling point rise, capacity and economy of multiple effect evaporators, evaporation equipments.

CO5


Reference Books:

1. Binay K.Dutta , Heat Transfer, Prentice Hall Publications, 2006. 2. W.L.Mc.Cabe, J.C.Smith and P.Harriot, Unit operations of Chemical Engineers, McGraw Hill International

edition, 7th edition, 1995. 3. Holman.J.P, Heat Transfer, 9 th Edition, McGraw Hill International, 2004. 4. Kern D.Q, Process Heat Transfer, McGraw Hill, 1950. 5. Krieth, Fundamentals of Heat Transfer, Harper and Row Publishers, 6th Edition, 1986. 6. C.J.Geankoplis, Transport Processes and Unit Operations, Prentice Hall, 3rd Edition, 1993. 7. Coulson J.M and Richerdson J.F, Chemical Engineering - Volume 1, Elsevier Press, 6th Edition, 2006.

38


Semester : Fourth Course Category Code: PCC



L T P C CA SE TM

CH204 Mechanical Operations 3 - 3 40 60 100

Prerequisite


Course Outcome

CO1 Explain the techniques involved in particle size analysis and handling methods of solids

CO2 Select suitable size reduction equipment and explain various size enlargement techniques

CO3 Differentiate the various types of classifiers and centrifugal separators

CO4 Illustrate the principles and theory of filtration and thickening techniques and their related equipments

CO5 Explain the principles and theories of froth-flotation, mixing and agitation and able to calculate power required for mixing

UNIT-I Particle Size Analysis and Handling Periods: 9

Particle Size Analysis - Methods of representation of size analysis, shape factor, sub sieve methods of analysis, surface area determination. Industrial screening - Theory of screening, screen efficiency, types of screening equipments , Storage and Conveyance of solids - Bunkers, silos, bins and hoppers, transportation of solids in bulk, conveyer selection, different types of conveyers .

CO1

UNIT-II Particle Size Reduction and Enlargement Periods: 9

Size reduction - Energy relationships in size reduction, size reduction equipment and selection, closed circuit and open circuit operation. Size enlargement - Principle of granulation, briquetting, pelletisation, flocculation,

CO2

UNIT-III Fluid – Solid Separation Periods: 9

Classification - Application of Stoke’s equation, types of classifiers - gravity settling, settling tanks, elutriation, double cone classifier, rake classifier, bowl classifier. Centrifugal separation - Principles, separation of solids from fluids, continuous centrifuges, cyclones and hydro cyclones. Gas cleaning - Gravity and momentum separators, cyclone separators.

CO3

UNIT-IV Filtration and Sedimentation Periods: 9

Solid - Liquid separation-Filtration, flow through filter cake and filter media, compressible and incompressible filter cakes, filtration equipments - selection, operation and design of filters and optimum cycle of operation, filter aids. Thickening - Batch and continuous thickeners, design of continuous thickeners.

CO4

UNIT-V Concentration Techniques & Mixing Periods: 9

Froth flotation - Principles and theories of collection, flotation cell and typical circuit. Sorting (separation of solids) , Principles of jiggers, Types of jiggers, Mixing and agitation - Mixing of liquids without solids, mixing of liquids with solids, mixing of powders, selection of suitable mixers, power requirement for mixing.

CO5

Lecture Periods: 45 Tutorial Periods: - Practical Periods: Total Periods: 45

Reference Books:

1. Anup K Swain, Hemlata Patra and G.K.Roy ,Mechanical Operations, Tata McGraw-Hill Education Private Limited, 2011.

2. Badger and Banchero, Introduction to Chemical Engineering, Tata McGraw-Hill, 2006. 3. McCabe, J.C.Smith and P.Harriot, Unit Operations of Chemical Engineers, McGraw Hill International

Edition, VII edition, 2009. 4. Foust Wenzel, Principle of Unit Operations, John Wiley and sons, II Edition, 1980. 5. Coulson J.M and Richerdson J.F, Chemical Engineering - Volume 2, Elsevier Press, V Edition, 2006.

39



Course Code

Course Name


L T P C CA SE TM

CH205 Chemical Engineering Thermodynamics

3 1 - 4 40 60 100

Prerequisite


Course Outcome

CO1 Explain the PVT behaviour of fluids and the concepts of ideal gas, non ideal gas, compressibility factor, critical properties and to have an idea about equations of state

CO2 Appreciate the principle of first and second laws of thermodynamics and to apply them in solving problems

CO3 Describe various thermodynamic properties and relations between them and know about Maxwell relations, thermodynamic diagrams and their constructions

CO4 Explain the concept of ideal and non-ideal solutions, partial molar properties, chemical potential, fugacity and activity

CO5 Appreciated the fundamentals of VLE and the phase rules

UNIT-I Equations of state Periods: 12

The behaviour of fluids - PVT properties of fluids, equations of state, ideal and non-ideal gas, the and compressibility factor, critical properties, generalized equations of state.

CO1

UNIT-II Laws of Thermodynamics Periods: 12

First law of thermodynamics - Types of energy, work, heat and energy changes, application of first law to different processes. Second law of thermodynamics and its applications - Entropy, reversible and irreversible processes, Carnot cycle, T-S diagrams, enthalpy of mixing and disorder, refrigeration .

CO2

UNIT-III Thermodynamic properties and relations Periods: 12

Thermodynamic properties and relations among them, mathematical relationships among basic properties, Maxwell relations, changes in properties, temperature and pressure effects, thermodynamic diagrams, construction of thermodynamic diagrams.

CO3

UNIT-IV Thermodynamics of solution Periods: 12

Solution properties - partial molal properties and chemical potential, concept of fugacity and activity and their calculations, ideal and non-ideal solutions, Gibbs - Duhem equations, property change of mixing and excess properties.

CO4

UNIT-V Phase Equilibria Periods: 12

Phase equilibria - Phase rule, fundamentals of vapour - liquid equilibrium, Vanlaar, Margules and Wilson equations for binary mixture, liquid - liquid, solid - liquid and solid - vapour equilibria.

CO5


Reference Books:

1. J.Richard Elliot, Carl T Lira, Introductory Chemical thermodynamics, Prentice Hall International Series, 2nd Edition,2012.

2. J.M. Smith,H.C.Van Ness and M.M.Abbot adapted by B.I.Bhatt, Introduction to Chemical Engineering Thermodynamics(In SI Units), McGraw-Hill,7th Edition, 2013.

3. K.V.Narayanan, .A textbook of Chemical Engineering Thermodynamics, PHI learning private limited, 2nd Edition, 2013.

4. B.G.Kyle,Chemical and Process Thermodynamics, PHI learning private limited , 2nd Edition, 1999. 5. Y.V.C.Rao, An Introduction to Thermodynamics, Wiley Eastern, 1994.

40



Course Code

Course Name


L T P C CA SE TM

CH206 Mass Transfer I 3 1 - 4 40 60 100

Prerequisite


Course Outcome

CO1 Measure and determine diffusion coefficients of gas, liquid systems

CO2 Determine mass transfer coefficients and appreciate stage concept

CO3 Perform process design calculations related to absorption and stripping operations

CO4 Perform process design calculations related to adsorption operation

CO5 Perform process design calculations related to humidification operation

UNIT-I Diffusive Mass Transfer Periods: 12

Molecular diffusion in gases and liquids, measurement and calculation of diffusivities, steady state diffusion in multi component mixtures. Diffusion in solids, molecular and Knudsen diffusion in porous solids.

CO1

UNIT-II Turbulent Transfer of Mass and Interface Mass Transfer

Periods: 12

Mass transfer in turbulent flow, eddy diffusion, mass transfer coefficients, estimation of mass transfer coefficient in wetted wall column, correlations for the calculation of mass transfer coefficients. Theory of interface mass transfer, Individual and overall mass transfer coefficients, steady state co-current and counter current mass transfer processes, stages and stage efficiencies, cross flow and counter current cascades of stages, Kremser equations for the calculation of number of theoretical stages. Equipments for gas-liquid contact operations

CO2

UNIT-III Absorption Periods: 12

Gas Absorption - Tray tower absorber, absorption factor, calculation number of theoretical stages, Murphree efficiency - point efficiency, tray efficiency and overall tray efficiency, calculation of actual number of trays. Packed tower absorber - HETP, HTU and NTU calculations Non-isothermal absorber, absorption with chemical reaction.

CO3

UNIT-IV Adsorption Periods: 12

Adsorption – Types of adsorption, nature of adsorbents, adsorption equilibria, effect of pressure and temperature on adsorption isotherms, Freundlich equation. Adsorption operation – stage wise operations, steady state moving bed absorbers, unsteady state fixed bed adsorbers, break through curves, rate of adsorption in fixed beds, design of fixed bed adsorbers.

CO4

UNIT-V Humidification Periods: 12

Humidification - Humidity chart, adiabatic saturation curves, wet bulb temperature and measurement of humidity, Lewis relation, equipments for humidification operations, water cooling towers and spray chambers. Theory and calculation of humidification processes - gas liquid interaction, conditions in the top and bottom of cooling towers, design of cooling towers and dehumidifiers.

CO5

Lecture Periods: 45 Tutorial Periods: 15 Practical Periods: Total Periods:`60

Reference Books:

1. R.E. Treybal, Mass Transfer Operations, McGraw Hill, 3rd Edition, 1981. 2. Binay K Dutta, Principles of Mass Transfer and Separation Process, PHI learning private limited, 2007. 3. C.J.Geankoplis, Transport Processes and Unit Operations, Prentice Hall, 4th Edition, 2003. 4. Badger and Banchero, Introduction to Chemical Engineering, Tata McGraw Hill, 2006. 5. Coulson J.M and Richerdson J.F, Chemical Engineering - Volume 2, Elsevier Press, V Edition, 2006. 6. W.L.McCabe, J.C.Smith and P.Harriot, Unit Operations of Chemical Engineers, McGraw Hill International

Edition, 7th Edition, 2009. 7. A.P.Sinha and Parameswar De, Mass Transfer Principles and Operations, PHI learning private limited,

2012.

41

Department : ECE Programme : B.Tech (CH)

Semester : Fourth Course Category Code: ESC Semester Exam Type: TY

Course Code Course Hours / Week Credit Maximum Marks

L T P C CA SE TM

EC234 Elements of Electronics 3 - - 3 40 60 100

Prerequisite Nil

Course Outcome

CO1 Understanding the basic theory of semiconductors and diodes.

CO2 Knowledge about various transistor configurations and also could comprehend the need for proper biasing of devices.

CO3 Understanding the operation of Field Effect Transistor devices.

CO4 Gain knowledge on Thyristors and optical devices.

CO5 Acquire knowledge on Transducers and Sensors.

UNIT – I Semiconductor Fundamentals and PN junction diode Periods: 9

Introduction to semiconductors – Types of semiconductors -Energy band diagram of semiconductor - Diode equivalent circuit -Diode current equation - Construction, working and VI characteristics of PN junction diode – Energy band structure of open circuited PN junction- Effect of temperature on PN junction diodes - Capacitance effects –Types of breakdown – Zener diode - Application of diode as half wave, full wave and bridge rectifiers, Clipper and Clamper circuits. Regulators - Zener diode as Voltage regulator.

CO1

UNIT-II Bipolar Junction Transistor Periods: 9

Construction- Types of configurations: Operation of NPN and PNP transistors- working and characteristics of CE, CB and CC configurations –Early effect - Thermal runaway – Heat sinks - Need for transistor biasing – dc load line – Q point-Voltage divider bias - Application of BJT as amplifier and switch.

CO2

UNIT-III Field Effect Transistor Periods: 9

Types – Construction and operation of N-channel and P-channel JFET – Characteristics and parameters of JFET- JFET biasing circuits –fixed bias and potential divider bias (derivations not required) Construction ,working and characteristics of E-MOSFET and Depletion MOSFET - Working and application of CMOS as inverter.

CO3

UNIT-IV Thyristors and Optical Devices Periods: 9

Construction, working and characteristics of SCR, DIAC , TRIAC, UJT. Construction, working and characteristics of LED, LASER, PIN diode, APD, Optocoupler. LDR, photo multiplier, LCD.

CO4

UNIT-V Transducers and Sensors Periods: 9

Basic principle – Classification of Transducers – Mechanical Transducers – Displacement to Pressure Transducer – Passive Electrical Transducers – Resistive - Inductive - Capacitive Displacement Transducers – Active Electrical Transducers – Piezoelectric Transducers – Hall Effect Transducers -Photo voltaic -Semiconductor Sensors – Smart Sensor – Hall effect sensor – Thermal Detector Sensor – Ultrasonic sensor – Fiber optic pH and Humidity sensor – Chemical Sensors – Semiconductor Gas Detectors - Biomedical Sensors.

CO5


Reference Books:

1. J.Millman, C.Halkias and Satyabrata ,”Electronic devices and Circuits”, Third edition,McGraw Hill, 2010. 2. Robert L. Boylestead and Louis Nashelsky, “Electron Devices and Circuits Theory ", Prentice Hall of India, 11th

Edition,2013. 3. David A. Bell, "Electronic Devices and Circuits", Prentice Hall of India, 5th Edition, 2008. 4.Theodore F. Bogart, “Electronic Devices and Circuits”, Pearson Education India ,2011.

5. Murthy D. V. S, “Transducers and Instrumentation”, Prentice Hall, 2nd Edition, 2012.

https://www.amazon.in/s/ref=dp_byline_sr_book_1?ie=UTF8&field-author=Theodore+F.+Bogart&search-alias=stripbooks

42

Department : Chemical Engineering Programme : B.Tech.(CH)

Semester : Fourth Course Category Code: PCC Semester Exam Type: LB


L T P C CA SE TM

CH207 Chemical Engineering Lab –I 3 1.5 40 60 100

Prerequisite Momentum Transfer, Mechanical Operations

Course Outcome

On successful completion of the course, the candidate should gain practical knowledge on

CO1 Applying Bernoulli’s equation for calculating friction factor

CO2 Handling equipments for calibration of flow meters and measuring devices

CO3 The methods employed for calculating pressure drop across packed and fluidised bed

CO4 Applying energy laws in estimating energy required for size reduction equipments

CO5 Applying filtration principles for estimating the performance of different filters

(Any 10 of the below experiments)

1. Laminar flow of Newtonian and non Newtonian fluids 2. Flow through pipes and fittings 3. Flow through annulus

CO1

4. Orifice meter 5. Venturi meter 6. Rotameter 7. Weirs and notches 8. Centrifugal Pump Characteristics

CO2

9. Packed bed; 10. Fluidized bed;

CO3

11. Sieve Analysis 12. Ball Mill 13. Jaw Crusher

CO4

14. Plate and Frame Filter Press 15. Vacuum Filter 16. Beaker Decantation

CO5

Lecture Periods: - Tutorial Periods: - Practical Periods: 45 Total Periods: 45

Reference Books

1. Lab Manual, Department of Chemical Engineering, Pondicherry Engineering College, Puducherry, 2018

43


Semester : Fifth Course Category Code: PCC


Course Code

Course Name

Periods / Week


L T P C CA SE TM

CH208 Mass Transfer -II 3 1 - 4 40 60 100

Prerequisite: Nil


Course Outcome

CO1 Understand the concept of vapour-liquid equilibrium and its application in the distillation

CO2 Analyse distillation operations through stage concept

CO3 Analyse extraction and leaching operations through ternary diagrams

CO4 Able to suggest drying time requirements for various devices and design industrial driers.

CO5 Estimate crystal yields for batch and continuous equipments.

UNIT-I Distillation Periods: 12

Vapour liquid equilibria - Raoult’s law, relative volatility, vapour liquid equilibrium diagrams for ideal and non-ideal systems, enthalpy concentration diagrams. Principle of distillation - flash distillation, differential or simple distillation, steam distillation, multistage continuous rectification, calculation of number of ideal stages by Ponchan - Savarit method, Total reflux, minimum reflux ratio, optimum reflux ratio.

CO1

UNIT-II Stage Calculations Periods: 12

Number of ideal stages by McCabe - Thiele method, effect of operating conditions on the number of ideal stages, Murphree stage and overall efficiency, calculation of actual number of stages, batch distillation with reflux, packed bed distillation, NTU and HTU calculations.

CO2

UNIT-III Extraction and Leaching Periods: 12

Liquid - liquid extraction, ternary liquid- liquid equilibrium, solvent characteristics, equipments for liquid-liquid extraction, stage wise contact - cross current and counter current extraction, continuous contact extraction, packed bed extraction with reflux. Leaching - Leaching by percolation through stationary solid beds, moving bed leaching, counter current multiple contact ( shank’s system ), equipments for leaching operation, multi stage continuous cross current and counter current leaching, stage calculations, stage efficiency.

CO3

UNIT-IV Drying Periods: 12

Drying - equipments for batch and continuous drying of solids, principles and theories of drying - drying rate curve, critical and equilibrium moisture content, calculation of drying time under constant drying conditions. Mechanism of batch drying - cross-circulation drying, through circulation drying. Continuous drying - material and energy balances in continuous dryers, rotary dryer - design of rotary dryer.

CO4

UNIT-V Crystallisation Periods: 12

Crystallization - principles of crystallization, types of crystals, nucleation theories, crystal growth and law, particle size distribution of crystals, Yields, heat and material balances in crystallization, equipments for crystallization.

CO5


Reference Books:

1. R.E. Treybal, Mass Transfer Operations, McGraw Hill, 3rd Edition, 1981. 2. Binay K Dutta, Principles of Mass Transfer and Separation Process, PHI learning private limited, 2007. 3. C.J.Geankoplis, Transport Processes and Unit Operations, Prentice Hall, 4th Edition, 2003. 4. W.L.McCabe, J.C.Smith and P.Harriot, Unit Operations of Chemical Engineers, McGraw Hill International

Edition, 7th Edition, 2009. 5. A.Anantharaman and K.M.Meera Sheriffa Begum, Mass Theory and Practice, PHI learning private limited,

2011. 6. A.P.Sinha and Parameswar De, Mass Transfer Principles and Operations, PHI learning private limited,

2012.

44


Semester : Fifth Course Category Code: PCC Semester Exam Type: TY

Course Code

Course Name


L T P C CA SE TM

CH209 Chemical Reaction Engineering- I 3 1 - 4 40 60 100

Prerequisite:


Course Outcome

CO1 Calculate the equilibrium compositions of single and multiple reactions.

CO2 Able to analyse the kinetics of homogeneous reactions using differential and integral methods.

CO3 Able to design ideal batch and flow reactors.

CO4 Able to analyse the performance of ideal reactors connected in series or parallel.

CO5 Evaluate the yield and product distribution of series/parallel reactions carried out in ideal CSTR and PFRs.

UNIT-I Chemical Equilibria Periods: 12

Chemical Equilibria - Free energy and chemical reactions, feasibility of chemical reaction, calculation of free energy of homogeneous reactions, equilibrium constants and evaluation from thermodynamic data, effect of different variables on reaction equilibria, calculation of equilibrium composition for single and multiple reactions, equilibria of heterogeneous reactions.

CO1

UNIT-II Homogeneous Reactions Periods: : 12

Kinetics of homogeneous reactions - introduction, single and multiple reactions, elementary and non-elementary reactions, rate equations, kinetic models for non-elementary reactions, testing kinetic models, temperature dependence of rate - Arrhenius, collision and activated complex theories, Interpretation of batch reactor data for single and complex reactions under constant volume and variable volume conditions, differential and integral analysis, half life period.

CO2

UNIT-III Design of Homogeneous Reactors Periods: : 12

Design of single homogeneous reactors - ideal reactors, design equations for ideal batch reactor, PFR and CSTR, size comparison of single reactors.

CO3

UNIT-IV Multiple Reactor Systems Periods: : 8L+4T

Multiple reactor systems - plug flow reactors in series and / or parallel, CSTRs in series, reactors of different types in series, recycle reactor, auto catalytic reactions, optimum recycle ratio for an auto catalytic reaction.

CO4

UNIT-V Multiple Reactor Systems Periods: : 12

Multiple reaction systems - series and parallel reactions in CSTRs and PFRs, product distribution, fractional yields, maximization of fractional yield in multiple reactions, series - parallel reactions.

CO5


Reference Books:

1. Octave Levenspiel, Chemical Reaction Engineering, John Wiley Publications Ltd., 3rd Edition, 2007. 2. Lanny D. Schmidt, The Engineering of Chemical Reactions, Oxford University Press, 2nd Edition, 2010. 3. H.S.Fogler, Elements of Chemical Reaction Engineering, Prentice Hall of India Ltd., 4th Edition, 2009. 4. J.M.Smith, Chemical Engineering Kinetics, McGraw Hill, III Edition, 1981. 5. S.Sundaramurthy, S Suresh,Green Chemical Engineering: An Introduction to Catalysis, Kinetics, and Chemical

Processes, CRC press, Taylor and Francis group,2014

45




L T P C CA SE TM

CH210 Chemical Process Industries 3 - 3 40 60 100

Prerequisite


Course Outcome

CO1 Enumerate various water conditioning processes and processes for the manufacture of industrial gases.

CO2 Make process flow diagram; identify parameters and engineering problems involved in industrial production of heavy inorganic chemicals.

CO3 Generate process flow diagram, list out the process parameters and identify the engineering problems involved in the manufacturing of various inorganic engineering materials.

CO4 Explain the process involved in manufacture of various organic and inorganic chemicals.

CO5 Identify the parameters, draw process flow diagram and list out the engineering problems involved in the manufacture of various fertilizers.

UNIT-I Water and Industrial gases Periods: 9

Water Conditioning methods, Demineralisation, Precipitation Process. Industrial Gases: Carbon dioxide, Nitrogen, Hydrogen, Oxygen and Acetylene.

CO1

UNIT-II Alkalies and Acids Manufacture Periods: 9

Alkalies : Chlor-alkali Industries: Manufacture of Soda ash, Manufacture of Caustic Soda and chlorine-common salt. Sulphur and Sulphuric acid: Mining of Sulphur and manufacture of Sulphuric acid. Manufacture of hydrochloric acid and Nitric Acid.

CO2

UNIT-III Cement, Glass and Ceramics Periods: 9

Cement, Glass and Paper; Cement: Types and Manufacture of Portland cement, Glass: Manufacture of Glasses and Special Glasses, Ceramics: Refractories

CO3

UNIT-IV Sugar, pulp and pigments Periods: 9

Sugars and Paints: Manufacture of sugar, Manufacture of paints – Pigments. Production of Pulp, Paper and rayon, Vegetable oil by Solvent Extraction.

CO4

UNIT-V Fertiliser Periods: 9

Fertilisers: Nitrogen Fertilisers: Synthetic Ammonia, Urea, Ammonium chloride, CAN, Ammonium Phosphate. Phosphorus fertilizers: Phosphate rock, Phosphoric, Acid, Super Phosphate and Triple Super phosphate –MAP, DAP.

CO5


Reference Books:

1. N.Shreve, Chemical Process Industries, 5th Edition, McGraw Hill, New York, 1984. 2. R.Gopal and M.Sittig, Dryden’s outlines of Chemical Technology, 2nd Edition, 1965. 3. S.D.Shukla and G.N.Pandey,Textbook of Chemical Technology, Volume I, 1977.

46


Semester : Fifth Course Category Code: PCC Semester Exam Type: LB

Course Code

Course Periods / Week Credit Maximum Marks

L T P C CA SE TM

CH211 Chemical Engineering Lab-II 3 1.5 40 60 100

Prerequisite

Course Outcome


CO1 Applying basic laws of heat transfer in conduction, convection and radiation

CO2 Handling heat exchangers and evaluating their performance

CO3 Handling condensers and evaluating their performance

CO4 Estimating the various characteristic properties of fuel

CO5 Applying Fick’s law of diffusion for evaluating diffusivity.


1. Heat Transfer through Composite Wall 2. Transient Heat Conduction 3. Heat Transfer with Natural Convection 4. Heat Transfer by Radiation.

CO1

5. Heat Transfer in a Shell and Tube Heat Exchanger 6. Heat Transfer through Packed Bed 7. Heat Transfer in a Double Pipe Heat Exchanger

CO2

8. Heat Transfer in a Vertical Condenser 9. Heat Transfer in a Horizontal Condenser

CO3

10. Flash and Fire Point of a fuel 11. Redwood viscometer 12. Calorific value of a fuel

CO4

13. Stefan’s tube experiment-diffusivity of vapour in air 14. Liquid- liquid diffusion - Diffusivity of salt in water 15. Surface Evaporation 16. Sublimation of naphthalene ball 17. Vapour Liquid Equilibrium

CO5


Reference Books:

1. Lab Manual, Department of Chemical Engineering, Pondicherry Engineering College, Puducherry, 2018.

47

Department : IEDP Programme: B.Tech. (CH)

Semester : Fifth Course Category Code: PAC Semester Exam Type: TY


L T P C CA SE TM

EP201 Entrepreneurship 3 - - 2 40 60 100

Prerequisite Nil

Course Outcome

CO1 Attain conceptual understanding of entrepreneurship and design thinking

CO2 Understand about business model development and MVP

CO3 Analyze about costing and revenue

CO4 Learn about marketing and sales

CO5 Realize about team formation and compliance requirements

UNIT-I Problem and Customer Periods: 9

Effectuation, Finding the flow. Entrepreneurial style, business opportunity, problems worth solving, methods for finding problems, problem interviews. Design Thinking, Consumer and customer, market types, segmentation and targeting, early adopters, Gains, Pains and Jobs-To be done, Value Proposition Canvas (VPC), Identifying Unique Value Proposition (UVP).

CO1

UNIT-II Business Model and Validation Periods: 9

Types of Business Models, Lean Canvas, Risks. Building solution demo, solution interviews, problem-solution test, competition, Blue Ocean Strategy. MVP- Build-Measure-Learn feedback loop, MVP Interviews, MVP Presentation.

CO2

UNIT-III Revenue and Cost Periods: 9

Revenue Streams-Income, costs, gross and net margins - primary and secondary revenue streams- Different pricing strategies - product costs and Operations costs; Basics of unit costing. Financing New Venture- various sources - investor expectation- Pitching to Investors.

CO3

UNIT-IV Marketing and Sales Periods: 9

Difference between product and brand - positioning statement. Building Digital Presence, Social media- company profile page – Sales Planning - buying decisions, Listening skills, and targets. Unique Sales Proposition (USP), sales pitch, Follow-up and closing a sale.

CO4

UNIT-V Team and Support Periods: 9

Team Building - Shared leadership - role of a good team - team fit - defining roles and responsibilities - collaboration tools and techniques- project management, time management, workflow, delegation of tasks. Business regulations - starting and operating a business - compliance requirements.

CO5


Reference Books

1. Nandan H, Fundamentals of Entrepreneurship, Prentice Hall India, 2013. 2. Khanka S.S, Entrepreneurial Development, S Chand & Company, 2007. 3. Sangeetha Sharma, Entrepreneurship Development, Prentice Hall India, 2017. 4. Anil Kumar.S, Entrepreneurship Development, New Age Publishers, 2003. 5. LearnWISE–Digital learning platform by Wadhwani Foundation, www.learnwise.org.

48

Department : Chemical Engineering Programme: B.Tech. (CH)

Semester : Sixth Course Category Code: PCC


Course Code Course Name Periods /

Week Credit Maximum Marks

L T P C CA SE TM

CH212 Chemical Reaction Engineering- II

3 1 - 4 40 60 100

Prerequisite:

On successful completion of the course, the student should be able to:

Course Outcome

CO1 Appreciate the effect of temperature in reactor performance.

CO2 Able to identify non-ideal fluid mixing and evaluate its impact on reactor performance.

CO3 Design simple heterogeneous non-catalytic reactors for gas-solid reactions

CO4 Design simple heterogeneous non-catalytic reactors for gas-liquid reactions

CO5 Derive global rate equations accounting for diffusion through porous catalyst pellets

UNIT-I Periods: 12

Non-isothermal reactions - temperature effects on chemical reaction rates, design procedures for adiabatic and non-isothermal operation of batch and flow reactors, optimum temperature progression, operating temperature for favourable product distribution in multiple reactions, reactor stability.

CO1

UNIT-II Periods: 12

Non-ideal reactors - Reasons for non-ideal flow behaviours, concept of mixing - micro and macro mixing, residence time distribution (RTD) functions, C, E and F curves, calculation of mean residence time from E and F curves, Tanks in series models, Axial dispersion model, segregated flow model, conversion in non-ideal reactors, introduction to multi-parameter models.

CO2

UNIT-III Periods: 12

Fluid-solid non-catalytic reactions - shrinking core model, determination of the rate controlling step, conversion in reactors with constant fluid composition, fixed bed reactor, Conveyor type /Tubular reactors.

CO3

UNIT-IV Periods: 12

Gas-liquid non-catalytic reactions - models for transfer at gas-liquid interface, enhancement factor, Hatta number, Derivation of overall rate equation for first order irreversible reaction and instantaneous reaction, design of packed bed reactors for gas-liquid non-catalytic reactions (simple cases).

CO4

UNIT-V Periods: 12

Kinetics of solid catalysed reactions - Langmuir-Hinshelwood-Hougen-Watson mechanism, Reaction and diffusion in porous catalysts - effectiveness factor, Thiele modulus, Global rate equations. Introduction to design of catalytic reactors- packed bed, fluidised bed, slurry reactors

CO5


Reference Books:

1. Octave Levenspiel, Chemical Reaction Engineering, John Wiley Sons Ltd., 3rd Edition, 2007. 2. J.M.Smith, Chemical Engineering Kinetics, McGraw Hill, 3rd Edition, 1981. 3. H.S.Fogler, Elements of Chemical Reaction Engineering, PHI learning private limited, 4thEdition, 2012. 4. S.Sundaramurthy, S Suresh, Green Chemical Engineering: An Introduction to Catalysis, Kinetics, and

Chemical Processes, CRC press, Taylor and Francis group,2014 5. G.F.Froment and K.B.Bischoff, Chemical Reactor Analysis and Design, John Wiley and Sons, 3ndEdition 2011.

49


Semester : Sixth Course Category Code: PCC Semester Exam Type: TY

Course Code

Course Name


L T P C CA SE TM

CH213 Process Dynamics and Control 3 1 - 4 40 60 100

Prerequisite

On Successful completion of the course, students should be able to :

Course Outcome

CO1 Appreciate the basic principles of feedback control and application of Laplace transform technique in dynamic modelling

CO2 Derive transfer function models for various systems

CO3 Analyse the transient behaviour of closed loop control systems

CO4 Analyse the stability of control system using root stability criteria and root locus diagrams

CO5 Analyse the stability of feedback control system using Bode Nicholas stability criteria.

UNIT-I Basics of control system Periods: 12

Introduction - Control system, components of a feed back control system, Lags in the control system – transfer lag, transportation lag, Pneumatic PID controller, control valve , valve characteristics. Laplace transforms - properties of Laplace transform, solution of linear differential equations using Laplace transform techniques.

CO1

UNIT-II Dynamic behaviour of systems Periods: 12

Dynamic behaviour of systems - derivation of transfer functions for first and second order systems, liquid level, temperature, pressure, flow and concentration control processes, linearization of nonlinear systems, interacting and non-interacting systems.

CO2

UNIT-III Transient behaviour of closed loop control systems Periods: 12

Transient response of first and second order systems, natural frequency, damping factor, overshoot, decay ratio, rise time and settling time. Transient analysis of control systems - block diagram algebra, overall transfer function of closed loop control systems, regulator and servo problems, transient response of first and second order systems with P, PI and PID controller.

CO3

UNIT-IV Stability of control systems Periods: 12

Definition of stability of control systems, Routh test , limitations of Routh test, Pade’s approximation of time delay systems. Root-locus technique - rules for plotting the root locus diagram, application of root locus to control systems.

CO4

UNIT-V Stability of control systems Periods: 12

Introduction to frequency response - Bode diagrams, Bode diagrams for first and second order systems, P, PI, PID controllers, transportation lag. Bode stability criteria, phase margin and gain margin, Nicholas chart, Ziegler - Nicholas Optimum controller settings. Nyquist stability criteria, Ziegler – Nicholas tuning of PID controller.

CO5


Reference Books: 1. D.R. Coughanour, Process Systems analysis and Control, McGraw Hill Education (India), 3rdEdition, 2013. 2. Stephanopoulos, Chemical Process Control – Theory and Practice, PHI learning private limited, 1984. 3. B.Wayne Bequette, Process Control Modelling, Design and Simulation, PHI learning private limited, 2003. 4. D.W.Seborg, T.F.Edger, and D.A.Millichamp, Process Dynamics and Control, John Wiley and Sons,2nd

Edition, 2004. 5. Thomas E. Marlin, Process Control Designing Processes and Control Systems for Dynamic Performance,

TATA McGraw-Hill, 2nd Edition, 2012. 6. Peter Harriot, Process Control, Tata McGraw Hill Publishing Co., 1964.

50

Department : Humanities & Social Sciences Programme: B.Tech.

Semester : Sixth Course Category Code: HSM Semester Exam Type: TY


L T P C CA SE TM

HS202 Industrial Economics and Management

3 - - 3 40 60 100

Prerequisite

Course Outcome

CO1 Assess the knowledge of mathematics to understand industrial micro economics/macroeconomics

CO2 Implement various management techniques based on the needs

CO3 Implement various investment evaluation based on the needs

CO4 Apply formula and workout problem

CO5 Understand Case studies on General, Production and Financial management

UNIT-I Micro and Macro Economics and its Applications Periods: 9

Nature and Scope of Economic science: Micro – Macro Economics, Economic decisions and Technical decisions. Demand and Supply concepts: Types of Demand, Determinants of Demand and Supply, concept of Equilibrium, Elasticity of Demand, cost components, Concepts of ISO-Quant – Break Even Analysis – Market structure – Price of Product Nature of pricing in different types of competition Small Scale Industries – Role of SSI in Indian Economy. Macro Economics: Nature and functions of Money – National Income – GNP and Savings – Inflation and Deflation concept – Business Cycle – Foreign Trade and Balance of payment.

CO1

UNIT-II Management Techniques Periods: 9

Types and Principles of Management – Elements of Management – Planning, Organising, Staffing, Directing, Coordinating Controlling - Scope of Management – Types of Organization Merits and Demerits – Types of (Ownership) of a firm Merits and Demerits.

CO2

UNIT-III Industrial Finance Periods: 9

Need for Finance – Types of finance – Sources of finance – Types of Investment – Evaluation of Investment – Preparation of Trading, Profit and loss Account and Balance Sheet – types of accounting and significance of each types.

CO3

UNIT-IV Production Management Periods: 9

Theory of Production Function – Types of Production Merits and Demerits – Process Planning – Routing – Scheduling – Material Control Concepts of Productivity – Measurement of Productivity – Inspection and Dispatches.

CO4

UNIT-V Marketing Management Periods: 9

Core Concepts of Marketing -0 Needs – Wants – Demand, Marketing Vs Selling – Products and Markets – Pricing and related factors – Channels of Distribution – Promotion Advertising – Market Research Vs Marketing Research.

CO5


Reference Books

1. Varshney Maheswari, Managerial Economics, S Chand & Co, New Delhi, 2011. 2. Dutt & Sundaram, Indian Economy, S Chand & Co, New Delhi, 2015. 3. Pandey I.M, Elements of Financial Management, Wiley Eastern Ltd, New Delhi, 2015. 4. H.L. Ahuja, Macro Economics for Business and Management, S Chand & Company Ltd, 2011. 5. O.P Khanna, Industrial Engineering and Management, Dhanpat Rai and Sons, 2009. 6. Philip B Kotler, Marketing Management, Mac Millan, New York 2011.

51


Semester : Sixth Course Category Code: PCC Semester Exam Type: LB

Course Code

Course Periods / Week Credit Maximum Marks

L T P C CA SE TM

CH214 Chemical Engineering Lab -III 3 1.5 40 60 100

Prerequisite

Course Outcome


CO1 Handling various mass transfer equipments and evaluating mass transfer coefficients

CO2 Applying distillation principles for evaluating the performance of simple and steam distillation units.

CO3 Applying mass transfer principles to evaluate the extraction efficiency

CO4 Handling CSTRs and PFRs and evaluating their performance

CO5 Determining RTD of a CSTR and a packed bed reactor


1. Packed bed absorber 2. Wetted Wall Column 3. Adsorption isotherm 4. Multistage adsorption

CO1

5.Simple distillation 6. Steam distillation I and II

CO2

7. Liquid - Liquid equilibrium 8. Liquid- Liquid extraction 9. Leaching

CO3

10. Isothermal Batch reactor – Determination of order and reaction rate constant 11. Semi batch reactor- Determination of conversion and reaction rate constant 12. Determination of activation energy 13. CSTR- Determination of conversion and reaction rate constant 14. PFR- Determination of conversion and reaction rate constant; 15. PFR and CSTR in series - Comparison of conversion 16. Three CSTRs in series - Comparison of conversion

CO4

17. Residence Time Distribution in CSTR 18. Residence Time Distribution in packed bed reactor 19. Heterogeneous catalytic reaction

CO5

LecturePeriods: Tutorial Periods: Practical Periods: 45 Total Periods: 45

Reference Books


52

Department : Humanities & Social Sciences Programme : B.Tech.

Semester : Sixth Subject Category: MCC Semester Exam Type: -


L T P C CA SE TM

SH203 Essence of Indian Traditional Knowledge

3 - - - - - -

Prerequisite

Course Outcome


CO1 understand connect up and explain basics of Indian traditional knowledge in modern scientific perspective

UNIT-I Periods: 23

Basic structure of Indian knowledge system, Modern science and Indian knowledge system, Yoga and holistic health care.

CO1 UNIT-II Periods: 22

Philosophical tradition, Indian linguistic tradition, Indian artistic tradition.


Reference Books:

1. N. Sivaramakrishnan (Ed.) Culteral Heritage of India – Course Materal, Bharatiya Vidya Bhavan, Mumbai 5th edition, 2014.

2. Swami Jitatmanand, Modern Physics and Vedanta, Bharatiya Vidya Bhavan. 3. Fritzof Capra, Tao of Physics. 4. Yoga Sutra of Patanjali, Ramakrishna Mission, Kolkatta. 5. R.N. Jha, Science of Conciousness Psychotherapy and yoga Practices, Vidyanidhi Prakashan, Delhi 2016. 6. S.C Chaterjee and D.M Datta, An Introduction to Indian Philosophy, University of Calcutta, 1984. 7. Krishna Chaitanya, Arts of India, Abhinav Publications, 1987

53


Semester : Seventh Course Category Code: PCC Semester Exam Type: TY

Course Code

Course Name


L T P C CA SE TM

CH215 Transport Phenomena 3 1 - 4 40 60 100

Prerequisite

On Successful completion of the course, Student should be able to:

Course Outcome

CO1 Critically evaluate momentum transport phenomena and perform calculations using shell balance for different momentum flow geometries.

CO2 Develop equation of continuity and equation of motion in different coordinate systems.

CO3 Critically evaluate heat transport phenomena and perform calculations using shell balance for different heat flow geometries.

CO4 Apply the equations of change to establish profiles of velocity, temperature and concentration.

CO5 Critically evaluate mass transport phenomena and perform calculations using shell balance with and without reaction.

UNIT-I Fluid Flow Periods: 12

Viscosity, temperature effect on viscosity of gases and liquids, Newton’s law, mechanism of momentum transport, Velocity distribution in laminar flow- shell momentum balance-flow through tubes-surfaces-flow of Newtonian fluid.

CO1

UNIT-II Fluid flow Periods: 12

Equation of change for isothermal process – one dimensional equation of motion and continuity – Euler and Navier Stokes equation

CO2

UNIT-III Heat Transfer Periods: 12

Thermal conductivity, temperature and pressure effect on thermal conductivity of gases and liquids, Fourier’s law, mechanism of energy transport, shell energy balance, temperature distribution in solids and laminar flow with electrical, nuclear, viscous heat source, heat conduction through composite walls, cylinders, spheres, fins, slits.

CO3

UNIT-IV Energy Equations Periods: 12

Energy equations, special forms, use of equations of change CO4

UNIT-V Mass transfer Periods: 12

Diffusivity, temperature and pressure effect, Fick’s law, mechanism of mass transport, theory of diffusion in gases and liquids, shell mass balances, concentration distribution in solids and in laminar flow: Stagnant gas film, heterogeneous and homogeneous chemical reaction systems, falling film, porous catalyst. The equation of continuity, summary of equations of change and fluxes, use of equations of change

CO5


Reference Books:

1. R.B.Bird, W.E.Stewart and E.N.Lightfoot, Transport Phenomena, John Wiley and Sons, 2ndEdition, 2003. 2. Willim Thomas, Introduction to Transport phenomena, Pearson Education, 1st Edition, 2000. 3. R.S.Brodkey and H.C. Herskey, Transport Phenomena, McGraw Hill, 1988. 4. J.R.Welty, C.E.Wicks, R.E.Wilson and Roggers , Fundamentals of Momentum, Heat and Mass transfer, John

Wiley and Sons, 5th Edition, 2007. 5. Willim Deen, Analysis of Transport Phenomena, Oxford University Press, 2nd Edition, 2007.

54

Department : Chemical Engineering Programme: B.Tech.(CH)

Semester : Seventh Course Category Code: PCC Semester Exam Type: LB


L T P C CA SE TM

CH216 Computational Methods and Practice in Chemical Engineering

3 - 2 4 40 60 100

Prerequisite

On successful completion of this course, Students should be able to:

Course Outcome

CO1 Write simple problems in GNU- octave

CO2 Write programs to solve chemical engineering problems represented by linear simultaneous equations

CO3 Write programs to solve chemical engineering problems represented by non-linear algebraic equations.

CO4 Write programs to solve chemical engineering problems represented by ordinary differential equations

CO5 Write programs to solve chemical engineering problems involving numerical integration and interpolation.

UNIT-I Principles of Programming using GNU-Octave Periods: 15

Lectures Principles of Programming using GNU-Octave: Matrices and Matrix operations, Assignment statement, Logical operators and Logical statement (If-Then-Else, switch case), Conditional statements, repetitive loops function scripts (for-loop, while-loop), global and local variable, plotting and display of results. Practice Simple programs to illustrate the concepts-

1. Calculation of vapour pressure and latent heat using Antoine’s equation 2. Calculation of specific heat and enthalpy 3. Reading data from steam table

CO1

UNIT-II Solutions to linear algebraic Equations Periods: 15

Lectures Solutions to linear algebraic Equations : Gauss Elimination iterative methods (Jacobi, Gauss-Seidel), Tri diagonal matrices and Thomas algorithm, Polynomial regression and least square Practice Computer Programs to

1. Solve Material Balance of process flow sheets 2. Fit Mass transfer, heat transfer and friction factor correlations 3. Interstage Composition in multistage absorption column 4. Balanced chemical reaction equations

CO2

UNIT-III Solutions of non -linear algebraic equations Periods: 15

Lectures Solutions of non -linear algebraic equations: Bisection methods, direct substitution (fixed point) method, Picard’s methods, Regula-Falsi Method, Wegstein Method, Newton-Raphson method, system of non-linear equation Practice Computer program to

1. Calculate boiling point at given pressure 2. Bubble point and dew point calculations 3. Flash calculation 4. Calculation of equilibrium conversion and selectivity of multiple reactions 5. Calculating number of ideal stages in binary distillation column

CO3

55

UNIT-IV Solution of Ordinary Differential Equations (Initial value problems)

Periods: 15

Lectures Solution of ordinary differential equations (Initial value problems) : Explicit Euler method, implicit Euler method, predictor- corrector method, Runge- Kutta method (2nd order and 4th order), system of ODEs, stiffness Practice Computer programs to

1. Compute concentration in a batch reactor 2. 2. Obtain dynamic response of a liquid level process 3. Obtain dynamic response of a CSTR. 4. Concentration profile in a PFR 5. Compute temperature profile in steady state heat conduction

CO4

UNIT-V Numerical integration and interpolation Periods: 15

Lectures Numerical integration and interpolation: Trapezoidal Rule, Simpson 1/3 rule, Linear interpolation, quadratic and cubic Spline interpolation Practice Computer programs to

1. Compute Final composition in simple distillation 2. NTU in a Packed bed absorber 3. Mean specific heat over a temperature range 4. Interpolate VLE data 5. Calculate mean residence time and variance from tracer test 6. Interpolate stem-table data

CO5

Note: Semester exam is a practical exam. Students will solve 5 problems (one from each unit) by writing programs using Octave.

Lecture Periods: 45 Tutorial Periods: Practical Periods:30 Total Periods:75

Reference Books:

1. Numerical methods with Chemical Engineering Applications, K.D. Borfmam, P.Daoutidis, Cambridge University Press, 2017.

2. Introduction to Chemical Engineering Computing, B.A.Finlayson, Wiley India 2010 3. Computational Methods in Chemical Engineering, O.T. Hanna, O.C. Sandall, Prentice Hall

1995.

56



Course Code

Course Name


L T P C CA SE TM

CH217 Process Equipment Design & Practice 3 2 4 40 60 100

Prerequisite

On Successful completion of the course, students should be able to :

Course Outcome

CO1 Bridge the theoretical basis in heat transfer to its applications in designing an open ended design problems in heat exchangers and condensers and simulate the same using GNU -OCTAVE.

CO2 Workout detailed process design of multi effect evaporators and carry out simulation using GNU-OCTAVE.

CO3 Designs packed and plate absorption towers and simulate the same using GNU-OCTAVE.

CO4 Work out detailed process design of Distillation columns and simulate using GNU-OCTAVE.

CO5 Carry out detailed process design of dryers, cooling tower and mechanical design of storage tanks, reactors and tall vessels.

UNIT-I Heat Exchangers Periods: 15

Theory Process Design of Heat Exchangers- Double Pipe and Shell and Tube Condensers – Vertical and Horizontal Practice Computer Aided Design and Simulation of Heat Exchangers and Condensers using GNU-OCTAVE

CO1

UNIT-II Evaporators Periods: 15

Theory Process Design of Evaporators – Multiple Effect – Forward feed and Backward feed (with and without boiling point rise Practice Computer Aided Design and Simulation of Multiple effect evaporators (with and without boiling point rise) using GNU-OCTAVE

CO2

UNIT-III Absorption Towers Periods: 15

Theory Process Design of Packed Bed and Plate Type Absorption Towers Practice Computer Aided Design and Simulation of Packed Bed and Plate Type Absorbers using GNU-OCTAVE

CO3

UNIT-IV Distillation columns Periods: 15

Theory Process Design of Packed Bed and Plate Type Distillation columns Practice Computer Aided Design and Simulation of Packed Bed and Plate Type Distillation columns using GNU-OCTAVE

CO4

UNIT-V Dryers and cooling towers Periods: 15

Theory Process Design of the following equipments: Rotary Drier Cooling Tower Mechanical Design of Reactors, Storage Tanks and Tall Columns Practice Computer Aided Design and Simulation of Cooling tower and Rotary drier using GNU-OCTAVE

CO5


Reference Books:

1. S.B.Thakore and BI Bhatt, Introduction to Process Engineering and Design, McGraw-Hill Education (India) Private Limited, 2013.

57

2. Kern D.Q, Process Heat Transfer, McGraw Hill, 1950. 3. J.M.Coulson and J.F.Richardson, Chemical Engineering - Volume VI, Elsevier Press, 6thEdition, 2006. 4. R.H.Perry and Don Green, Chemical Engineer’s Handbook, McGraw Hill, 8th Edition, 2009. 5. R.E. Treybal, Mass Transfer Operations, McGraw Hill, II Edition, 1981.

58




L T P C CA SE TM

CH218 Process Engineering Economics 3 - - 3 40 60 100

Prerequisite

On successful completion of the course, students should be able to:

Course Outcome

CO1 Perform calculations in regard to interest and concept of equivalence formulas.

CO2 Account depreciation and depletion in plant economics calculations.

CO3 Recognize, analyse, solve and compare various cash flow models / methods used for economic selection of alternates

CO4 Enumerate different cost entities in cost estimation and gain knowledge on various project evaluation techniques.

CO5 Perform calculations to obtain optimum solution pertaining to specific unit operations.

UNIT-I Economics in Process Design Periods: 9

Time value of money - simple and compound interest - discrete, nominal and continuous rate of return and their relationships, issue and evaluation of bonds, concept of equivalence.

CO1

UNIT-II Depreciation and Amortization Periods: 9

Depreciation and Amortization - classification of depreciation and methods of uniform, rapid and slow write off techniques and their comparison, depreciation accounting procedures, taxes and insurance, implication of taxes in selecting alternates.

CO2

UNIT-III Selection of Alternates Periods: 9

Economics of selection of alternates - criteria, annual cost, present worth, rate of return, capitalized cost methods, extra investment analysis, mutually exclusive basis, replacement economy.

CO3

UNIT-IV Cost Estimation& Project Evaluation Periods: 9

Cost estimation - equipment costs, cost indices, William’s point sixth rule, methods of estimation of fixed capital, product cost estimation. Bookkeeping - ledgers and journals, financial statements, balance sheet, principles and application of project execution techniques, PERT and CPM, preparation of project feasibility reports, selection of plant location and layout.

CO4

UNIT-V Cost Optimization Periods: 9

Optimization - procedure involving single and two variables, optimum number of units required for maximum profit and minimum cost, determination of optimum parameters in selected unit operations - fluid flow (optimum pipe diameter), heat transfer (optimum thickness of insulation), evaporation, filtration, break-even analysis.

CO5

Lecture Periods: 45 Tutorial Periods: - Practical Periods: Total Periods: 45

Reference Books:

1. Max S. Peters, Klaus D Timmerhaus and Ronald E. West, Plant Design and Economics for Chemical Engineers, McGraw Hill (Indian Edition), 5th Edition 2013.

2. Jelen’s, Cost and Optimization Engineering, McGraw Hill, 2nd Edition, 1992.

59




L T P C CA SE TM

CH219 Process Control and Simulation Lab 3 1.5 40 60 100

Prerequisite

Course Outcome

On successful completion of the course, students will gain practical knowledge on :

CO1 Applying control principles for determining time constant of various systems

CO2 Obtaining transient response of various systems

CO3 Online control of temperature and level controllers

CO4 Developing a flow sheet using DWSIM


1. Time constant of thermometer 2. Time constant of pressure vessel system 3. Two-Tank non interacting system 4. Two -Tank interacting system

CO1

5. Transient response of a mercury manometer 6. Transient response of a mixing vessel

CO2

7. Control valve characteristics 8. On –Off Control system behaviour 9. Level controller 10. Temperature controller

CO3

11. Flow sheeting and Simulation using DWSIM CO4


Reference Books


60


Semester : Seventh Course Category Code: PAC Semester Exam Type: PR

Course Code

Course Name


L T P C CA SE TM

CH220 Seminar 3 1 100 -- 100

Prerequisite

On successful completion of the course, students should be able to :

Course Outcome

CO1 Write technical documents and make oral presentations related to the work completed

CO2 Manage the given assignment in a given time period

C03 Identify, understand and discuss current technologies

C04 Learn and integrate through independent learning and collaborative study

The student will present a seminar on the following

Select on a topic in an emerging area in his/her specialization of Chemical Engineering. Make a presentation for duration of 20 to 25 minutes. Submit a brief report running to 15 or 20 pages for the purpose of evaluation.

CO1 CO2 CO3 CO4


Reference Books

1. Books related to the Seminar title. 2. Papers published in reputed journals and conferences related to the seminar.

61


Semester : Seventh Course Category Code: MCC

Semester Exam Type: -

Course Code

Course Name


L T P C CA SE TM

CH221 Professional Ethics 2 -

Prerequisite

On successful completion of the course, students should be able to :

Course Outcome

CO1 Apply ethical principles and commit to professional ethics in their profession.

CO2 Recognise the need for safety and apply reasoning to assess the safety and consequent responsibilities relevant to the professional engineering practice.

The course should cover the following topics by way of Seminars, Expert Lecturers and Assignments. Engineering Ethics – Moral Issues, Ethical theories and their uses Engineering as Experimentation – Code of Ethics Engineer’s Responsibility for Safety Responsibilities in Rights Global issues of engineering ethics

CO1 CO2

Lecture Periods: 30 Tutorial Periods: Practical Periods: Total Periods:30

Reference Books:

1. R.Subramanian , Professional Ethics, Oxford University Press,2013. 2. Mike Martine and Roland Schinzinger, Ethics in Engineering, McGraw Hill, 2005. 3. Charles E Harris Michael S Pritchard and Michael J Rabins, Engineering Ethics-Concepts and

Cases, Thompson Learning,2000. 4. Charles D.Fleddermann, Engineering Ethics , Prentice Hall, New Mexico, 1999.

62


Semester : Eighth Course Category Code: PAC Semester Exam Type: PR


L T P C CA SE TM

CH222 Comprehensive Test 2 1 100 100

Prerequisite: All professional core courses

On successful completion of the course, students should be able to:

Course Outcome CO1

Demonstrate the knowledge and understanding of the Chemical Engineering Principles and concepts gained during their course period.

CO2 Identify and solve chemical Engineering problems of higher order

The student is required to take a ‘Comprehensive Test’ on a scheduled date in the beginning of the eighth semester. The student will be tested for his/her understanding of the basic principles of the core Chemical Engineering subjects. Comprehensive Test will carry 1 credit. Comprehensive Test is meant for testing the higher order and critical thinking of the student in the respective domain. This test will have the standard of GATE examination. Two comprehensive tests, preferably with objective type questions from all core courses will be conducted of GATE examination standard.

CO1 CO2

Lecture Periods: Tutorial Periods: Practical Periods:30 Total Periods: 30

Reference Books 1. All Books related to the core courses. 2. Papers published in reputed journals and conferences related to the core courses.

63



Course Code

Course Name


L T P C CA SE TM

CH223 Internship - 2 100 100

Prerequisite

On successful completion of this internship, Students should be able to

Course Outcome

CO1 Demonstrate the ability to work in actual work environment


CO3 Function effectively as a member in diverse teams and in multidisciplinary settings

CO4 Apply professional ethics and responsibilities

CO5 Manage a project / assignment within a given time frame

The student is required to undergo ‘internship’ in an chemical industry of repute / research laboratory / higher learning institution for a minimum period of 6 weeks in a maximum of 3 spells during vacations. The internship carries 2 credits. Each spell of internship shall be for a period of not less than 2 weeks. The main purpose of internship is to enhance the general professional outlook and capability of the student to advance his chances of improving the career opportunities. The student should get prior approval from the Head of the Department before undertaking the internship and submit a detailed report after completion for the purpose of assessment.

A committee comprising of two faculty members will assess the internship for 100 marks, by evaluating the internship report and the oral presentation by the student.

CO1 CO2 CO3 CO4 CO5

64




L T P C CA SE TM

CH224 Project work 8 8 60 40 100

Prerequisite

On successful completion of the course, students should be able:

Course Outcome

CO1 Reinforce classroom theory by collecting literature pertaining to the propose project

CO2 Demonstrate the ability to work in teams


CO4 Manage a project within a given time frame

CO5 Apply professional ethics and responsibilities

The objective of the project is to enable the students to work in groups of not more than four members in each group on a project involving analytical, experimental, design or combination of these in the area of Chemical Engineering. The student shall carry out a ‘project work’ in the eighth semester. This project work carries 8 credits. The student is given an option to carry out this project work either in the college or in an industry / research laboratory / higher learning institution. The project work will be carried out under the supervision of a project guide from the department. In the case of student carrying out the project work outside the college, an external guide from the relevant organization shall be assigned in addition to the internal guide from the department. The student is required to do literature survey, formulate the problem and form a methodology of arriving at the solution of the problem. On completion of the work, a project report should be prepared and submitted to the department. The project report will be evaluated by a Project Evaluation committee comprising of the Head of the Department or his nominee (Chairman), Project coordinator (Professor/Associate Professor) and two other faculty members.

CO1 CO2 CO3 CO4 CO5

Lecture Periods: - Tutorial Periods: - Practical Periods: - Total Periods: -

Reference Books

1. Books related to the project title. 2. Papers published in reputed journals and conferences related to the project.

65

Honours Courses

66

Department : Chemical Engineering Programme : B.Tech.(CH)-Honours


Course Code

Course Name


L T P C CA SE TM

CHH01 Introduction to Frontiers of Chemical Engineering

4 - - 4 40 60 100

Prerequisite


Course Outcome

CO1 Have a better grasp of Chemical Engineering history and developments and its frontier areas

CO2 Appreciate the application of nanomaterials in various fields

CO3 Recognise the potential uses of polymer composites and blends as engineering materials

CO4 Appreciate the application of Chemical Engineering in Controlled Drug Delivery Systems

CO5 Apply the fundamentals of chemical Engineering in the fields of Quantitative Biosciences and Tissue Engineering

UNIT-I Overview of Chemical Engineering Periods: 8

History and development of Chemical Engineering, Chemical Engineering present status, Challenges , Frontier areas- An overview

CO1

UNIT-II Nano Technology Periods: 12

Introduction to nanotechnology and nano materials, Synthesis Procedures for nano materials – Physical vapour deposition, Chemical Vapour deposition, Electrochemical deposition,Nano material applications: waste water treatment, nanobiotechnology, nanocomposites, biological nanomaterials, ,nanotechnology in food, medicine and health sciences.

CO2

UNIT-III Polymeric Composite and Polymer blends Periods: 12

Polymer composite materials: Physico-mechanical properties of conventional fibre and particulate polymer composites, advanced polymer composites, polymer nano composites, fillers used for polymer composites, polymer composites structure, characterisation, physical and chemical modification of polymer composites. Polymer blends : Definition of polymer blends and alloys, Advantages of polymer blends over conventional polymers, Thermo dynamical aspects of polymer blend miscibility, mixing, structure, properties and application of polymer blends in emerging technology – photovoltaic , Light emitting diode, supercritical fluids, Lithium battery and fuel cells

CO3

UNIT-IV Controlled Drug Delivery Systems Periods: 12

Polymer basics, Drug delivery systems (reservoir, matrix, bio-erodible systems) Pharmacokinetics and bio distribution of drug delivery systems, Drug elimination and fate, Externally controlled systems, Micro- and nano-particle based delivery Cell and gene delivery, Delivery of vaccines (oral, pulmonary, transdermal) Relevant FDA regulations

CO4

UNIT-V Quantitative Bio Science and Tissue Engineering

Periods: 15

Quantitative Bioscience: Chemistry of biological system, molecular and cellular system, physiology and behaviour, ecology, evolution, earth systems Tissue Engineering: The present and future role of chemical engineering in tissue Engineering, Principle of tissue engineering, Stem cells, Cell matrix, cell-cell interaction, Biologic scaffold for tissue engineering, Natural polymers in tissue engineering applications

CO5

Lecture Periods: 60 Tutorial Periods: Practical Periods: Total Periods:60

Reference Books:

1. Morton M.Denn, Chemical Engineering – An Introduction, Cambridge University Press, 2012. 2. Laurent Simon, Control of biological and drug delivery system for Chemical, biomedical and pharmaceutical Engineering, Wiley ,2013 3. Xiaoling Li, Bhaskara Jasti, Design of controlled release drug delivery systems, Mc graw Hill Chemical

67

Engineering, First Edition,2006. 4. Lloyd M. Robson, Polymer Blends – A comprehensive review, Hanser Publications, 2007. 5. D R Paul and S Newman, Polymer Blends , Vol I & II, Academic Press, 1976 6. G. Lubin, Handbook of composites, second edition, Van Nostrand Reinhold,NY,1982. 7. Brain Munsky, Quantitative Biology: theory, Computational methods and models, MIT Press, 2018. 8. Hayser,Fussenegger, Tissue Engineering, Springer,2017.

68


Semester : Fourth Course Category Code: PCC


Course Code

Course Name

Periods / Week


L T P C CA SE TM

CHH02 Special Topics in Chemical Engineering – I

3 1 - 4 40 60 100

Prerequisite


Course Outcome

CO1 Appreciate the principles involved in process flow sheet calculations.

CO2 Analyse various chemical process synthesis methods.

CO3 Gain an understanding of the flow of compressible fluids.

CO4 Apply the concepts of turbulent flow in velocity profile calculations.

CO5 Formulate power law for non- Newtonian fluids.

UNIT-I Introduction to Chemical Process Synthesis Periods: 12

Choice of raw materials, writing balanced chemical reactions, generation-consumption analysis, Leblanc process, Solvay process, ammonia synthesis, atom economy, process economy process capacities and product values, case study – six carbon chemistry.

CO1

UNIT-II Introduction to Process Flow sheet Calculations Periods: 12

Linear equations and chemical reactions, using matrices to balance chemical reactions, using matrices in generation – consumption analysis, using matrices to find linearly independent chemical reactions, linear models of process flow sheets : mixers, splitters, reactor (single and multiple reactions), separators, process topology, linear models with multiple process units and recycle, tearing algorithm.

CO2

UNIT-III Compressible Fluid flow Periods: 12

Flow of Compressible fluids – Thermodynamics of ideal gas, isentropic process, wave propagation through compressible fluids, sonic velocity, Mach number, flow through variable area conduits (Nozzle), Equations for isentropic flow, Equations for isothermal frictional flow.

CO3

UNIT-IV Turbulent flow Periods: 12

Turbulent flow - Velocity fluctuations in turbulent flow, statistical nature of turbulence, Reynold’s stresses, empirical theories, eddy viscosity, Prandtl’s mixing length theory, Velocity distribution for turbulent flow – 1/7th power law, Logarithmic velocity distribution, Universal velocity distribution; Relationship between friction factor and Reynold’s number, Von karman correlation.

CO4

UNIT-V Non-Newtonian fluids Periods: 12

Laminar flow of non-Newtonian (power law) fluids through circular pipe, friction factor and Reynold’s number for power law fluid, Metzner Reed’s approach, capillary tube experiment, Power Law of fluids and Bingham Plastics

CO5


Reference Books:

1.Introduction to chemical processes – principles, analysis, synthesis, Regina M Murphy, McGraw Hill (India), 2013. Chapter 1, chapter 3. 2. Noel de Nevers, Fluid mechanics for Chemical Engineers, TATA McGraw- Hill Edition, 3rdEdition 2011. 3. W.L.Mc.Cabe, J.C.Smith and P.Harriot, Unit Operations of Chemical Engineers, McGraw Hill International edition, 7th Edition, 2009. 4.Coulson J.M and Richardson J.F., Chemical Engineering - Volume 1, Elsevier Press, 6th Edition, 2006.

69




L T P C CA SE TM

CHH03 Special Topics in Chemical Engineering – II

3 1 - 4 40 60 100

Prerequisite


Course Outcome

CO1 Derive exact analytical solutions for unsteady state conduction and diffusion problems

CO2 Explain various theories of mass transfer and its applications

CO3 Analyse the analogies of heat, mass and momentum and derive Reynold, Prandtl and colburn analogies

CO4 Explain various concepts in statistical thermodynamics

CO5 Estimate thermodynamic properties using equation of state principles

UNIT-I Unsteady state Conduction and Diffusion Periods: 12

Unsteady state heat conduction. Exact analytical solutions and charts, one-dimensional and multidimensional systems-Use of transient heat conduction charts. Unsteady state diffusion mass transfer. Exact analytical solutions and charts. Lumped parameter method of transient analysis.

CO1

UNIT-II Theories of Mass Transfer Periods: 12

Theories of Mass Transfer. film theory, penetration theory, surface renewal theory, and their applications.

CO2

UNIT-III Analogy of Heat, Mass and Momentum Periods: 12

Analogies of Momentum, Heat and Mass Transfer, Reynolds analogy, Prandtl -Taylor analogy and Colburn analogy. Analogy applications.

CO3

UNIT-IV Statistical Thermodynamics Periods: 12

The Statistical Method, The Language of Statistical Thermodynamics, Statistical Thermodynamic formation of the Boltzmann equation, Negative Temperature, Entropy and Third law.

CO4

UNIT-V Property Estimation using Equation of State Periods: 12

Thermodynamic properties from volumetric data. Thermodynamic properties with independent variables P and T. Fugacity of a component in a mixture at moderate pressures. Fugacity of a pure liquid or solid. Thermodynamic properties with independent variables V and T. Fugacity of a component in a mixture according to van der Waals’ equation, phase equilibrium from volumetric properties.

CO5


Reference Books:

1. James Sucec, Heat Transfer, Jaico Publishing House, 1999. 2. C.O.Bennett, J.E.Myers, Momentum, Heat and Mass transfer, McGraw Hill Publication, Third edition,

1981. 3. Anthony L.Hines, Robert N. Maddox, Mass Transfer: Fundamentals and Applications, Prentice Hall,1985. 4. R.E. Treybal, “Mass Transfer Operations”, McGraw Hill, 3rd Edition, 1981. 5. John M.Prausnitz, Rudiger N. Lichtenthaler, edmundo Gomes de Azevedo, ,Molecular Thermodynamics

of Fluid-Phase equilibria, Third Edition, Prentice Hall PTR, New Jersey 6. Terrell L.Hill , An introduction to Statistical Thermodynamics”, 2008, Dover Publications. 7. J.Rajaram, J.C.Kuriacose, Chemical Thermodynamics Classical, Statistical and Irreversible, Pearson, 2013

70



Course Code

Course Name


L T P C CA SE TM

CHH04 Special Topics in Chemical Engineering – III

3 1 - 4 40 60 100

Prerequisite


Course Outcome

CO1 Estimate various physical properties applying group contribution methods

CO2 Solve problems relating to multi component distillation systems

CO3 Appreciate the various principles involved in Semiconductor processing

CO4 Classify various types industrial heat and mass transfer equipments

CO5 Explain the concepts involved in fuel cell and hydrogen energy production

UNIT-I Group Contribution Methods Periods: 12

Group Contribution Methods : Estimation of physical properties, Pure component constants, Critical Properties, Acentric factor, Boiling and freezing points, UNIFAC and UNIQUAC methods

CO1

UNIT-II Multicomponent Distillation Periods: 12

Multicomponent Systems: specific limitations, Key components, minimum reflux ratio, Colburn Method, Underwood method, Total reflux, Fenske’s equation, Feed tray location, Lewis and Matheson calculation

CO2

UNIT-III Semiconductor Processing Periods: 12

Overview of Chip Manufacturing Process, FEOL and BEOL Concepts, Lithography basics, Deposition Techniques - Physical Vapor Deposition (PVD) basics, equipment description and operation details, Electrochemical deposition, Chemical vapor deposition (CVD) basics, Atmospheric pressure (APCVD), low pressure (LPCVD), plasma enhanced (PECVD), mass transfer control and reaction kinetics control, Reactor description and operation

CO3

UNIT-IV Industrial Heat and Mass Transfer Equipments Periods: 12

Principle, Construction and Working of Reboilers, Vapourizers, Plate Heat Exchangers, Finned Tube Heat Exchangers, Air cooled Heat Exchangers, Fired Heaters(Furnaces and Boilers), Absorbers, Molecular Distillation units, Divided wall Distillation columns, Vacuum dryers, Fluidised bed driers, Swenson Walker Crystalliser, MSMPR, Humidifcation and Dehumidification equipments, Industrial extractors, Rotating Disc contactors.

CO4

UNIT-V Fuel Cell and Hydrogen Energy Periods: 12

Need for fuel cell, Overview of fuel cell technology, Components of fuel cell, Basic electrochemistry for fuel cells, Safety issues and cost expectations and life cycle analysis of fuel cells. Hydrogen Energy: Production of Hydrogen from hydrocarbon, nuclear energy and renewable , Hydrogen purification – pressure swing adsorption, Solvent based absorption, membrane separation, Hydrogen storage – Compressed storage , liquid state storage and solid state storage, materials for storage

CO5


Reference Books:

1. Robert C.Reid, John M. Prausnitz, Bruce E.Poling, The Properties of Gases & Liquids, Fourth Editions, Mc graw Hill International Editions, 1988 2. Stanley I. Sandler, Chemical, Biochemical and Engineering Thermodynamics, Wiley Student edition, 2006 3. R.E. Treybal, “Mass Transfer Operations”, McGraw Hill, 3rd Edition, 1981. 4. Charles D.Holland, Fundamentals of Multi-component Distillation, McGraw Hill,1997 5. Bent Serense, Hydrogen and Fuel Cells: Emerging technologies and applications, Academic Press, 2005. 6. Peter Hoffmann, Tomorrow’s energy: Hydrogen, Fuel cells and the prospects for a cleaner planet, MIT press, Cambridge, 2017. 7. Kayode coker, Ludwig's Applied Process Design for Chemical and Petrochemical Plants, 4th edition, Gulf professional publishing, 2007.

71



Course Code

Course Name


L T P C CA SE TM

CHH05 Special Topics in Chemical Engineering – IV

3 1 - 4 40 60 100

Prerequisite

On Successful completion of the course, the student should be able to:

Course Outcome

CO1 Synthesis heat exchanger networks

CO2 Analyse polymer reactions and their performance equations

CO3 Formulate and solve boundary value problems in Chemical Engineering

CO4 Gain an understanding of advanced process control techniques.

CO5 Design and tune PID controllers

UNIT-I Pinch Technology and Heat Exchanger Networks Periods: 12

Heat Exchanger Network – Composite Curves, Energy Targets and Pinch, Skid Diagram, Problem Table Algorithm, Simple Criteria for Design of Heat Exchanger Network Capital And Total Cost Targets , Number Of Units , Heat Exchanger Area , Number Of Shells, Capital Cost and annualization of capital costs – Case Studies. (Students are required to Solve Assignment Problems by writing programs using GNU – Octave)

CO1

UNIT-II Polymerization Reactions and Reactors Periods: 12

Ideal Addition Polymerization – Kinetics , Design Equations for PFR , CSTR ; Chain Reactions and Polymer Size Distribution ; Free - Radical Polymerization – Kinetics , Batch Reactor / PFR Design Equation Catalytic Polymerization , Condensation Polymerization , Fisher –Tropsch Polymerization. (Students are required to Solve Assignment Problems by writing programs using GNU – Octave)

CO2

UNIT-III Boundary value problems in Chemical Engineering Periods: 12

Examples of BVPs in Chemical Engineering – Diffusion and Chemical Reaction in Porous Spherical Catalyst Pellet, Tubular Reactor with Axial Mixing, Conduction Through Cooling Films; Solution to the BVPs – Shooting Method, Finite Difference Method, Orthogonal Collocation Method. (Students are required to Solve Assignment Problems by writing programs using GNU – Octave)

CO3

UNIT-IV Advanced Process Control Periods: 12

Feed forward Control, Ratio Control (Simple Design Problems), Cascade Control (Simple Design Problem) Time Delay Compensation , Inferential Control , Selective / Override Control , Adaptive Control , Model Predictive Control (Introduction).

CO4

UNIT-V Design and Tuning of PID Controllers Periods: 12

Performance Criteria for Closed Loop System, PID Controller Tuning Methods – Direct Synthesis Method, Internal Model Control (IMC) Tuning Relationship, Tuning Relations Based on integral error Criteria, Controllers with two degrees of freedom, On – Line Controller Tuning – Continuous Cycling Method, Delay Auto - Tuning, Step Test Methods, Guidelines for Common Control Loop.

CO5


Reference Books:

1. Robin smith, Chemical process design and integration’ Wiley INDIA, 2005. 2. Lanny.D. Schmidt , Engineering of chemical reactions , , Oxford university press , 2005. 3. D.E.Seborg, T.F.Edgar , D.A.Mellichamp , Process dynamics and control, John Wiley and Sons, 2004. 4. A. Rasmuson, B.Andersson, L. Olsson, R.Andersson, Mathematical Modelling in Chemical Engineering Cambridge University Press, 2014.

72

Minor Courses

73

Department : Chemical Engineering Programme : B.Tech.(CH)-Minor


Course Code

Course Name


L T P C CA SE TM

CHM01 Process Engineering Principles and Calculations

3 1 - 4 40 60 100

Prerequisite


Course Outcome

CO1 Explain the scope and basic concepts of unit operations and unit processes in Chemical Engineering

CO2 Explain the production of important chemicals manufactured in a chemical industry

CO3 Apply various types of unit system and recognise basic process principles.

CO4 Perform material balance calculations on various unit operations and processes

CO5 PerformEnergy balance calculations on various unit operations and processes

Unit -I Introduction to Chemical Engineering Periods: 12

Historical Overview of Chemical Engineering, Concepts of Unit Operations and Unit Processes, Features of organised Chemical Processing- from Chemistry to Chemical Engineering, The Chemical Industry – Scope, Features and Characteristics, Principle of balancing with examples to illustrate differential and integral balance, lumped and distributed balances

CO1

UNIT-II Chemical Technology Periods: 12

Chemical Process Industries- Batch and Continuous mode of operation, Flow sheets, Process flow sheets for manufacture of standard chemicals - urea, sugar, crude distillation, cement, paper and pulp ,Paints, ethylene, acetylene, Rubber,methane, ethylene, polyethylene, acetylene

CO2

UNIT-III Process Principles Periods: 12

Introduction to Chemical Engineering Calculations, units and dimensions, mole and molecular weight, properties of gases, vapors, liquids, solutions and solids, gas laws, partial pressures, vapor pressures, saturation and equilibria, Raoults law, partial saturation and humidity

CO3

UNIT-IV Material Balances Periods: 12

Material balances in simple systems involving physical changes like distillation, mixing, absorbtion, crystallisation and chemical reactions like oxidation and combustion reactions, systems involving recycle , purge and bypass

CO4

UNIT-V Energy Balances Periods: 12

Heat capacity and enthalpy changes, Heat of reaction, Heat of Combustion, Heat of mixing, Sensible heat, Latent heat, Energy Balance calculations in simple systems

CO5


Reference Books:

1. B.I.Bhatt and S.M.Vora, Stoichiometry, Tata McGraw Hill, 5th Edition, 2013. 2. David.M.Himmelblau and Riggs , Basic Principles and Calculations in Chemical Engineering, Prentice Hall of India Ltd., 7th Edition, 2004. 3. A.Hougen, K.M. Watson and K.A.Ragatz, Chemical Process Principles, Vol 1, CBSE Publisher, 1980. 4. Richard M. Felder, Ronald W.Rousseau, Elementary Principles of Chemical Processes, Wiley Publications, 3rd Edition, 2007. 5. V.Venkataramani, N.Anantharaman and K.M.MeeraSheriffa Begum, Process Calculations,PHI Learning Private Limited, 2nd Edition, 2012. 6. N.Shreve, Chemical Process Industries , 5th Edition, McGraw Hill, New York, 1984. 7. R.Gopal and M.Sittig, Dryden’s outlines of Chemical Technology, 2nd Edition, 1965.

74




L T P C CA SE TM

CHM02 Fluid Flow and Particle Technology 3 1 - 4 40 60 100

Prerequisite


Course Outcome

CO1 Explain the principle and application of fluid pressure, buoyancy and basic laws governing the flow of non-viscous fluids

CO2 Understand the concept of flow of viscous fluids and write momentum balance equations

CO3 Explain the working principle of various measuring devices and pumps used for transportation of fluids

CO4 Explain the techniques involved in particle size analysis and reduction

CO5 Identify various equipments involved in classification, separation, centrifugation and filtration

Unit –I Fluid Statics and Dynamics Periods: 12

Fluid Statics – Fluid density, compressible and incompressible fluids; Pressure, relationship between pressure and density for ideal gas; Hydrostatic equilibrium in gravitational and centrifugal force fields; Gravity decanters and centrifuge ; Pascal’s law, hydraulic lever; Measurement of fluid pressure, manometers, Archimedes principle and buoyancy. Fluid Dynamics – ideal flow of fluids (non-viscous and incompressible fluids), Continuity equation and energy equation (Bernoulli’s equation), applications.

CO1

UNIT-II Flow of Viscous Fluids Periods: 12

Flow of viscous fluids - Shear rate, Shear stress, Newton’s law of fluid motion, Viscosity, concept of momentum transfer, Rheology of fluids - Newtonian and non-Newtonian fluids, laminar and turbulent flow, Reynolds number and transition from laminar to turbulent flow, Momentum Balance equations

CO2

UNIT-III Fluid Transportation Periods: 12

Transportation and metering of fluid - Orifice meter, Venturimeter, Pitot tube, Rota meter, Weirs and Notches, Pumps and Compressors, Performance and characteristics of centrifugal pumps, NPSH, Cavitation , Priming

CO3

UNIT-IV Particle Size Analysis and Reduction Periods: 12

Particle Size Analysis - Methods of representation of size analysis, shape factor, sub sieve methods of analysis, surface area determination. Industrial screening - screening, screen efficiency, types of screening equipments , solids storage - Bunkers, silos, bins and hoppers, Size reduction - Energy relationships in size reduction, size reduction equipment and selection, Size enlargement - Principle of granulation, briquetting, pelletisation, flocculation

CO4

UNIT-V Particle Separation Periods: 12

Classification –principle, types of classifiers - gravity settling, settling tanks, elutriation, and bowl classifier. Centrifugal separation - Principles, separation of solids from fluids, continuous centrifuges, cyclones and hydro cyclones. Gas cleaning - Gravity and momentum separators, cyclone separators. Solid - Liquid separation-Filtration- filtration equipments, filter aids. Thickening - Batch and continuous thickeners

CO5


Reference Books:

1. Noel de Nevers, Fluid mechanics for Chemical Engineers, TATA McGraw- Hill edition,3rd Edition 2011. 2. W.L.Mc.Cabe, J.C.Smith and P.Harriot, Unit Operations of Chemical Engineers, McGraw Hill International edition, 7th Edition, 2009. 3. Anup K Swain, Hemlata Patra and G.K.Roy ,Mechanical Operations,Tata McGraw- Hill Education Private Limited, 2011. 4. Badger and Banchero, Introduction to Chemical Engineering, Tata McGraw-Hill, 2006.

75



Course Code

Course Name


L T P C CA SE TM

CHM03 Heat Transfer and Thermodynamics

3 1 - 4 40 60 100

Prerequisite


Course Outcome

CO1 Understand PVT behaviour of the aggregate state of the matter

CO2 Apply first and second laws of thermodynamics to different processes

CO3 Understand the concept of fugacity and activity coefficient and their calculations

CO4 Identify different modes of heat transfer and their related basic laws

CO5 Explain the working principles of various types of heat exchanger and evaporators employed in process industries

Unit –I PVT relations Periods: 12

The behaviour of fluids - PVT properties of fluids, equations of state, ideal and non-ideal gas, compressibility factor, critical properties, generalized equations of state.

CO1

UNIT-II Laws of Thermodynamics Periods: 12

First law of thermodynamics - Types of energy, work, heat and energy changes, application of first law to different processes. Second law of thermodynamics and its applications - Entropy, reversible and irreversible processes, Carnot cycle, T-S diagrams, enthalpy of mixing and disorder, refrigeration ,liquefaction .

CO2

UNIT-III Concept of fugacity and Activity Coefficient Periods: 12

Solution properties - partial molal properties and chemical potential, concept of fugacity and activity and their calculations, ideal and non ideal solutions, Gibbs - Durham equations, property change of

mixing and excess properties.

CO3

UNIT-IV Principles of Heat transfer Periods: 12

Modes of heat transfer–conduction, convection and radiation, Fourier’s law of conduction, Newton’s law of cooling, Stefan Boltzmann law of radiation, heat transfer without and with phase change (evaporation, condensation), heat transfer coefficient.

CO4

UNIT-V Industrial Heat transfer Equipments Periods: 12

Heat Exchangers – Construction and working of double pipe and shell and tube, condensers – vertical and horizontal, Evaporators – Principles, Types , single effect and multiple effect evaporation, Modes of feed arrangement

CO5


Reference Books:

1. J.Richard Elliot, Carl T Lira, Introductory Chemical thermodynamics, Prentice Hall International Series, 2nd Edition,2012. 2. J.M. Smith,H.C.Van Ness and M.M.Abbot adapted by B.I.Bhatt, Introduction to Chemical Engineering Thermodynamics (In SI Units), McGraw-Hill,7th Edition, 2013. 3. K.V.Narayanan, .A textbook of Chemical Engineering Thermodynamics, PHI learning private limited, 2nd Edition, 2013. 4. Y.V.C.Rao, An Introduction to Thermodynamics, Wiley Eastern, 1994. 5. BinayK.Dutta , Heat Transfer, Prentice Hall Publications, 2006. 6. W.L.Mc.Cabe, J.C.Smith and P.Harriot, Unit operations of chemical engineers, McGraw Hill International edition, 7th edition, 1995. 7. Holman.J.P, Heat Transfer, 9th Edition, McGraw Hill International, 2004.

76




L T P C CA SE TM

CHM04 Fundamentals of Mass Transfer and Separations

3 1 - 4 40 60 100

Prerequisite


Course Outcome

CO1 Understand the basics of diffusion in various systems

CO2 Explain the various concepts involved in interface mass transfer.

CO3 Identify different unit operations in mass transfer

CO4 Derive fundamental equations for various unit operations

CO5 Explain different industrial mass transfer equipments

Unit -I Introduction to mass transfer Periods: 12

Basics of diffusion: Gases, liquid and solid system and their Correlations. Introduction to mass transfer coefficient and its measurements and correlations

CO1

UNIT-II Interface mass transfer Periods: 12

Interface mass transfer: individual and overall mass transfer coefficients. Modes of contact and concept of stage. Various stages efficiencies.

CO2

UNIT-III Unit operation in mass transfer Periods: 12

Basic unit operation in mass transfer: Absorption, stripping, adsorption, distillation, extraction, leaching, humidification, dehumidification, drying

CO3

UNIT-IV Stage concepts Periods: 12

Stage concept: Absorption, stripping, adsorption, distillation, extraction, leaching and their Analytical solutions

CO4

UNIT-V Industrial mass transfer equipments Periods: 12

Mass transfer equipment’s: Gas-liquid contactors, liquid-liquid contactors, solid-liquid contactors, Solid-gas contactors.

CO5


Reference Books:

1. R.E. Treybal, Mass Transfer Operations, McGraw Hill, 3rd Edition, 1981. 2. Binay K Dutta, Principles of Mass Transfer and Separation Process, PHI learning private limited, 2007. 3. C.J.Geankoplis, Transport Processes and Unit Operations, Prentice Hall, 4th Edition, 2003. 4. Badger and Banchero, Introduction to Chemical Engineering, Tata Mc Graw Hill, 2006. 5. Coulson J.M and Richerdson J.F, Chemical Engineering - Volume 2, Elsevier Press, V Edition, 2006. 6. W.L.McCabe, J.C.Smith and P.Harriot, Unit Operations of Chemical Engineers, McGraw Hill International Edition, 7th Edition, 2009. 7. A.P.Sinha and Parameswar De, Mass Transfer Principles and Operations, PHI learning private limited, 2012.

77




L T P C CA SE TM

CHM05 Process Dynamics and Reaction Engineering

3 1 - 4 40 60 100

Prerequisite


Course Outcome

CO1 Analyse the kinetics of homogeneous reactions using differential and integral methods.

CO2 Design ideal batch and flow homogenous reactors.

CO3 Classify non catalytic and catalytic reactors and have knowledge on various types

CO4 Appreciate the basic principles of feedback control and application of Laplace transform technique in dynamic modelling

CO5 Derive transfer function models for various systems and Analyse the transient behaviour of closed loop control systems

Unit -I Chemical Kinetics Periods: 12

Kinetics of homogeneous reactions - introduction, single and multiple reactions, elementary and nonelementary reactions, Conversion, Yield, Selectivity, Batch and Continuous flow reactors, rate equations, kinetic models for nonelementary reactions, testing kinetic models, temperature dependence of rate - Arrhenius, collision and activated complex theories.

CO1

UNIT-II Homogenous Reactors Periods: 12

Design of single homogeneous reactors - ideal reactors, Basic design equations for ideal batch reactor, PFR and CSTR, size comparison of single reactors

CO2

UNIT-III Heterogeneous Reactors Periods: 12

Multiphase non-catalytic (gas –solid, gas-liquid) reactors, Catalytic reactors : Solid catalysts - characteristics, classification of catalysts, selection and preparation of industrial catalysts, promoters and inhibitors, Fixed bed , fluidised bed, slurry reactors

CO3

UNIT-IV Control System Periods: 12

Introduction - Control system, components of a feed back control system, Lags in the control system – transfer lag, transportation lag, Pneumatic PID controller, control valve – valve characteristics. Laplace transforms - properties of Laplace transform, solution of linear differential equations using Laplace transform techniques, piecewise continuous functions.

CO4

UNIT-V Control Dynamics Periods: 12

Dynamic behaviour of systems - derivation of transfer functions for first and second order systems, liquid level, temperature, pressure, flow and concentration control processes, linearization of nonlinear systems, interacting and non-interacting systems. Transient response of first and second order systems, natural frequency, damping factor, overshoot, decay ratio, rise time and settling time.

CO5


Reference Books:

1. D.R. Coughanour, Process Systems analysis and Control, Mc Graw Hill Education (India), 3rd Edition, 2013. 2. Stephanopoulos, Chemical Process Control – Theory and Practice, PHI learning private limited, 1984. 3. Peter Harriot, Process Control, Tata McGraw Hill Publishing Co., 1964. 4. Octave Levenspiel, Chemical Reaction Engineering, John Wiley Sons Ltd., 3rd Edition, 2007. 5. J.M.Smith, Chemical Engineering Kinetics, McGraw Hill, 3rd Edition, 1981. 6. H.S.Fogler, Elements of Chemical Reaction Engineering, PHI learning private limited, 4th Edition, 2012

78

Professional Elective Courses

79


Semester : Fifth Course Category Code: PEC Semester Exam Type: TY


L T P C CA SE TM

CHY01 Polymer Science and Technology 3 - 3 40 60 100

Prerequisite


Course Outcome

CO1 Gain knowledge on the structure and properties of polymers.

CO2 Describe various types of polymers, polymerisation reactions, their process.

CO3 Describe various polymerization techniques uses and equipments employed.

CO4 Explain different polymer processing techniques for plastics manufacture

CO5 Enumerate various processing and finishing methods for fibre and elastomers.

UNIT-I Polymer Characterisation Periods: 9

Introduction - Definitions and concepts, polymerisation reactions, polymer structure, functionality, Characterisation of polymers.

CO1

UNIT-II Types and Equipments Periods: 9

Different types of polymers - natural and modified natural products, synthetic polymers and various types of polymerisation reactions.

CO2

UNIT-III Polymerisation Methods Periods: 9

Methods of polymerisation - mass, solution, emulsion and suspension polymerisation processes, various polymer products and their preparations, Degradation of polymers. Equipments used.

CO3

UNIT-IV Polymer processing for plastics Periods: 9

Processing methods for Plastics - Moulding, Extrusion, Casting, Calendaring, Forming, compounding, foaming, Reinforced fibre plastics. Finishing methods for Plastics .Post treatment of plastics. Fillers, Plasticizers, antioxidants, retardants , stablizers.

CO4

UNIT-V Processing and Finishing for fibre Periods: 9

Processing methods for Fibre and Elastomers – Spinning and Vulcanisation. Pre-treatment and post-treatment of elastomers: sintering, scouring, bleaching Finishing methods for fibre and Elastomers: dyeing, sizing, narcerizing, lubrication, curing, cross linking.

CO5


Reference Books:

1. Fred.W.Billmeyer, Text Book of Polymer Science, John Wiley and sons, 1980. 2. V.R.Gowarikar, Polymer Science, New Age International, Second Edition,2006. 3. David J. Williams, Polymer Science and Engineering, Prentice Hall, 1971. 4. Stanley Middleman, Fundamentals of Polymer Processing, McGraw Hill, 1977. 5. Herman S. Kaufman and Joseph J Falcetta, Introduction to Polymer Science and Technology, JohnWiley and

sons, 1977. 6. Rakesh K.Gupta and Anil Kumar, Fundamentals of Polymers, International edition, 1998.

80



Course Code

Course Name


L T P C CA SE TM

CHY02 Membrane Technology 3 - - 3 40 60 100

Prerequisite


Course Outcome

CO1 Appreciate the basic principle of membrane separation and membrane separation processes.

CO2 Identify membrane types, manufacturing methods and their applications in various industries and enumerate the prerequisites required for the design of RO system.

CO3 Design RO module and have grasp on the principle, design and application of nano filtration process.

CO4 Explain the principle, design and application of ultra filtration process.

CO5 Appreciate the concept and applications of microfiltration , dialysis and electro dialysis.

UNIT-I Membrane Principles Periods: 9

Basic principle of membrane separation. Classification of membrane separation processes. Advantages and disadvantages of membrane processes, Retention or rejection coefficient, Factors affecting the separation processes- concentration polarization and fouling.

CO1

UNIT-II Membrane materials and Types Periods: 9

Membrane types, materials and modules. General methods of membrane manufacture. Application of membrane separation processes in pharmaceutical, food, dairy, bioprocess and chemical industry. The concept of reverse osmosis, flux equations. Design and operating parameters, concentration polarization and membrane plugging

CO2

UNIT-III Design of RO Module Periods: 9

Design of an RO Module. Applications of reverse osmosis. The principle of nano filtration, nano filtration membrane, parameters affecting the performance of NF membranes. Industrial applications.

CO3

UNIT-IV Ultrafiltration Periods: 9

The basic principle of ultra filtration, ultra filtration membranes, configuration of UF unit, Types of devices in ultra filtration. Factors affecting the performance of ultra filtration. Fouling and flux decline. Affinity ultra filtration in protein purification and other applications.

CO4

UNIT-V Microfiltration Periods: 9

The basic principle of microfiltration. Cross flow and dead end microfiltration. Microfiltration membranes, mechanism of transport, membrane plugging and throughput, Fouling in microfiltration membranes and factors affecting fouling, Applications of microfiltration. Dialysis, Dialysis membranes, mass transfer in dialysis, applications. Electrodialysis- principles and applications.

CO5


Reference Books:

1. Kaushik Nath , Membrane Separation Processes , PHI learning private limited, 2011. 2. P.C. Wankat, Rate Controlled Processes, Springer Publications, 2005. 3. B.Sivasanker , Bio-separations , PHI learning private limited,2010. 4. R. W. Rousseau, Handbook of separation process technology, John Wiley and Sons, 1987.

81


Semester : Fifth Course Category Code: Semester Exam Type: TY

Course Code

Course Name


L T P C CA SE TM

CHY03 Semiconductor Processing Technology 3 - 3 40 60 100

Prerequisite


Course Outcome

CO1 Explain the concept involved in chip manufacturing process and various terminology related to it

CO2 Enumerate various physical and electrochemical vapour deposition techniques for chip manufacturing.

CO3 Explain the basics of chemical vapour deposition and atomic layer deposition and their deposition techniques

CO4 Describe various removal methods involved in chip manufacturing

CO5 Understand various surface modification methods and characterisation methods

UNIT-I Semiconductor Concepts Periods: 9

Overview of Chip Manufacturing Process, FEOL and BEOL Concepts, Lithography basics, layout, hierarchy vs flat file, levels and layers in layout file, Projection printing, dark field mask, positive resist and its advantages. Process details including resist coating, pre-exposure bake, exposure, soft bake, developing and hard bake, Stepper vs Scanner, Resolution, numerical aperture, Production Issues

CO1

UNIT-II Physical and Electrochemical Vapour Deposition Periods: 9

Deposition Techniques - Physical Vapour Deposition (PVD) basics, equipment description and operation details, RF/magnetron sputtering, long throw, ionized metal plasma (IMP) sputtering, collimated beam, sputtering yield. Electrochemical deposition, Electro-migration vs grain size, conformal, anti conformal and super fill.Suppressor, accelerator, levelers, effect of seed layer, spin on coating.

CO2

UNIT-III Chemical Vapour Deposition Periods: 9

Chemical vapor deposition (CVD) basics, Atmospheric pressure (APCVD), low pressure (LPCVD), plasma enhanced (PECVD), mass transfer control and reaction kinetics control. Reactor description and operation, deposition of silicon, poly silicon, oxide, nitride and tungsten, brief introduction to atomic layer deposition (ALD) and molecular beam epitaxy (MBE).

CO3

UNIT-IV Removal Methods Periods: 9

Wet etching: Isotropic etch, selectivity, anisotropic Si etch in KOH, cleaning, Chemicals for oxide and nitride removal. Dry etching : Plasma, anisotropic etch, equipment details and operation, Reactive ion etching (RIE), veil formation and de-veil, electrostatic discharge (ESD), aluminum etch, Chemical Mechanical planarization (CMP) basics, Front end of line (FEOL) basics, transistor structure and operation.

CO4

UNIT-V Modification methods Periods: 9

Material modification methods (diffusion, ion implantation, oxidation), process integration, testing and yield, relevant tools and techniques (FIB, SEM, AFM, Ellipsometry)

CO5


Reference Books:

1. The Science and Engineering of Microelectronic Fabrication (2nd Edition) by S.A. Campbell, Oxford University Press, 2001. 2. Introduction to Microelectronic Fabrication, Vol. 5 of Modular Series on Solid State Devices (2nd Edition) by Richard C. Jaeger, Prentice Hall, 2001. 3. Microchip Fabrication: (5th Edition) by Peter Van Zant, McGraw Hill, 2004.

82




L T P C CA SE TM

CHY04 Petrochemical Technology 3 - - 3 40 60 100

Prerequisite


Course Outcome

CO1 Appreciate the history, economics, future and limitations of petrochemical industries

CO2 Explain the process, process chemistry and applications of first generation petrochemicals.

CO3 Describe the process, process chemistry and applications of second generation petrochemicals.

CO4 Explain the process, process chemistry and applications of third generation petrochemicals.

CO5 Appreciate the process, process chemistry and applications of miscellaneous petrochemicals.

UNIT-I Sources and Classification Periods: 9

General Introduction - History, economics and future of petrochemicals, energy crisis and petrochemical industry, sources and classification of petrochemicals.

CO1

UNIT-II First Generation petrochemicals Periods: 9

First generation petrochemicals - alkanes - C1, C2, C3, C4 petrochemicals, alkenes - C2,C3,C4 petrochemicals, alkynes - C2,C3,C4 petrochemicals, B-T-X aromatics, diene based petrochemicals.

CO2

UNIT-III Second Generation petrochemicals Periods: 9

Second generation petrochemicals - synthesis gas, methanol, formaldehyde chloromethanes, ethanol, acetaldehyde, acetic acid, acetic anhydride, isopropyl alcohol, ethylene oxide, propylene oxide, acetone, vinyl chloride, phenol, aniline and styrene.

CO3

UNIT-IV Third Generation petrochemicals Periods: 9

Third generation petrochemicals - plastics, rubbers and fibres, olefinic polymers, polyethylene, polypropylene, polyisobutylene, diene polymers - polybutadiene, neoprene, polyisoprene, SBR, synthetic fibres.

CO4

UNIT-V Miscellaneous petrochemicals Periods: 9

Miscellaneous petrochemicals - petroleum proteins, synthetic detergents, resin and rubber chemicals, explosives - TNT and RDX.

CO5


Reference Books:

1. S.Maiti, Introduction to petrochemicals, Oxford and IBH publishing Co., 1992. 2. H.Steines, Introduction to petrochemical Industry, Pergamon, 1961. 3. G.D.Hobson and W.Pohl, Modern Petroleum Technology, Applied Science Publisher,4th Edition, 1975. 4. Richard Frank Goldsten and A.Lawrence Waddams, The Petroleum Chemical Industry, E & FN Spon Ltd.,1967. 5. G.T.Austin, Shreves Chemical Process Industries, 5th Edition, McGraw-Hill, 1986.

83



Course Code

Course Name


L T P C CA SE TM

CHY05 Energy Technology and Management 3 - 3 40 60 100

Prerequisite


Course Outcome

CO1 Appreciate the basic concepts of energy systems and also the classification and processing of solid fuels.

CO2 Explain various types of liquid and gaseous fuels

CO3 Describe various combustion phenomenon and acquire knowledge on solar, wind and tidal energy

CO4 Acquire knowledge on geothermal, MHD and nuclear energy management systems

CO5 Develop basic skills for energy auditing

UNIT-I Solid Fuels Periods: 9

Fuels - Classification, Properties, tests and analysis. Solid Fuels - Coal, origin, classification, storage and handling, carbonization, gasification and briquetting - gasification of biomass.

CO1

UNIT-II Liquid Fuels Periods: 9

Liquid fuels - Petroleum based fuels, synthetic fuels, alcohol and blended fuels, storage and handling. Gaseous fuels - Water gas, carburetted water gas, producer gas, coal gas and natural gas.

CO2

UNIT-III Solar, Wind and Tidal Energy Periods: 9

Various types of combustion equipments for solid, liquid and gaseous fuels. Principle, Storage and Applications of Solar energy, Wind energy, Tidal energy.

CO3

UNIT-IV Energy Management Periods: 9

Geothermal energy, Magneto hydrodynamics, Nuclear energy. Principles, Need , Initiation and Management of Energy Management Program.

CO4

UNIT-V Energy Auditing Periods: 9

Energy audit – elements, and concepts, types of energy audits, energy audit case studies – Sugar industry, Paper industry. Energy Conservation- Principles of Energy Conservation, Cogeneration, Waste Heat Recovery Technologies.

CO5


Reference Books:

1. S.Sarcar, Fuels and combustion, Orient Longman, 1990. 2. G.D.Rai, Non conventional energy sources, Khanna Publishers, IV edition, New Delhi, 2004. 3. S.P.Sharma and ChanderMohan, Fuels and Combustion, Tata McGraw Hill, 2004.

84


Semester : Sixth Course Category Code: PEC Semester Exam Type: TY

Course Code

Course Name


L T P C CA SE TM

CHY06 Petroleum Refinery Engineering 3 - - 3 40 60 100

Prerequisite


Course Outcome

CO1 Recognize the importance of petroleum refining with knowledge on crude oil testing and evaluation

CO2 Describe crude oil separation methods and various petroleum refining techniques

CO3 Appreciate the principle, process chemistry of various breakdown, Rebuilding and reforming processes

CO4 Explain various treatment techniques for removal of sulphur compounds.

CO5 Identify the processes involved in the production of petrochemicals

UNIT-I Periods: 9

Introduction – genesis, occurrence, drilling of crude oil, composition and Evaluation of crude oil. Testing of petroleum products. History of Refining

CO1

UNIT-II Periods: 9

Separation: Pre-treatment of crude oil – Handling – Heating of crudes Refining of petroleum- Atmospheric and vacuum distillation–Design aspects, blending process.

CO2

UNIT-III Periods: 9

Breakdown Process: Cracking, Visbreaking, Coking – types and operation Rebuilding Process: Isomerisation, Alkylation, Polymerisation, Reforming – types and operation Asphalt Technology.

CO3

UNIT-IV Periods: 9

Treatment Techniques for the removal of Sulphur Compounds to improve the performance, storage and stability Product Treatment processes–various solvent treatment processes, Dewaxing , clay treatment, hydro fining.

CO4

UNIT-V Periods: 9

Introduction to Petrochemical – generation, Cracking of Naphtha and gas for the Production of ethylene, propylene, isobutylene and butadiene. Production of acetylene from methane. Extraction of aromatics.

CO5


Reference Books:

1. B.K.Bhaskara Rao, Modern Petroleum Refining processes, 5th Edition, Oxford and IBH Publishing Co.Pvt.Ltd, New Delhi,2008. 2. J.H.Harker and J.R.Backhurst,“Fuel and Energy, Academic Press Inc.(London) Ltd, 1981. 3. W.L.Nelson, Petroleum Refinery Engineering, 4th edition, McGraw Hill, New York, 1985. 4. Robert. A.Meyers, Handbook of Petroleum Refining Processes, McGraw Hill, New York, 1986. 5. G.D.Hobson and W.Phol, Modern Petroleum Technology, Applied Science Publishers, 4thedition, 1975.

85




L T P C CA SE TM

CHY07 Nuclear Technology 3 - - 3 40 60 100

Prerequisite


Course Outcome

CO1 Appreciate the fundamentals and history of Nuclear power

CO2 Gain knowledge on different types of nuclear radiation and its interaction with matter

CO3 Define basic nuclear terminologies and the theories behind functioning of nuclear reactors

CO4 Describe the fundamentals of sustained nuclear chain reaction and fission reactor design

CO5 Define the guiding principles of radiation hazards and reactor safety

UNIT-I Nuclear Energy Fundamentals Periods: 9

Nuclear energy fundamentals: Atomic structure, and radio isotopes, radio activity, nuclear fission, nuclear fission reactors. History of reactor development, reactors for power production.

CO1

UNIT-II Nuclear Radiations Interaction Periods: 9

Nuclear reactions and radiations: Radio activity, interaction of alpha and beta particles, with matter, interaction of beta particles with matter, interaction of neutrons with matter, neutron cross section.

CO2

UNIT-III Nuclear reactor Theory Periods: 9

Nuclear reactor theory: The neutron cycle, critical mass, neutron diffusion, the diffusion equation, slowing down of neutrons, reactor period, transient conditions and reflectors.

CO3

UNIT-IV Engineering Considerations of Nuclear power plant Periods: 9

Engineering Considerations of Nuclear Power: Extension of theory to design, design criteria, selection of materials, reactor fuel, moderator materials, coolant system, reactor control and operation, fuel preparation, reprocessing of spent fuel.

CO4

UNIT-V Radiation hazards and Safety Periods: 9

Environmental effects and safety: Radiation hazards, radiation monitoring, radio waste treatment systems, reactor shielding. General principles of reactor safety, reactor protection system, reliability and risk assessment.

CO5


Reference Books:

1. Samuel Glasstone and Alexander Seasonske, Nuclear reactor engineering , 3rd Edition, CBS Publishers, USA. 2. Glenn Murphy, Elements of Nuclear Engineering, John Wiley and sons Inc., 1961. 3. K.Sriram, Basic Nuclear Engineering, Wiley eastern Ltd., 1990. 4. W.Marshall, Nuclear Power Technology, Vol. 1,2 & 3, Oxford University Press, New York, 1983.

86



Course Code

Course Name


L T P C CA SE TM

CHY08 New Separation Techniques 3 - 3 40 60 100

Prerequisite


Course Outcome

CO1 Gain knowledge on the concepts and fundamentals of adsorption and chromatography techniques.

CO2 Explain the basic concepts, principle and applications of membrane separation and various membrane separations processes.

CO3 Solve problems in design and mathematical modelling of membrane systems.

CO4 Explain the fundamentals of surfactant based separations.

CO5 Explain the basic principle and the fundamentals required for thermodynamic modelling of supercritical fluid extraction.

UNIT-I Adsorption and Chromatography Periods: 9

Adsorption separations - Review of fundamentals, mathematical modelling of column contactors, pressure swing adsorption, ion chromatography, affinity chromatography, gradient chromatography, parametric pumping, counter-current, simulated counter-current and multidimensional chromatography.

CO1

UNIT-II Membranes and Membrane Separations Periods: 9

Membrane separation processes – basic concepts, membrane modules, structure and characteristics of membranes, design considerations of Reverse Osmosis, Ultra Filtration, Electro Dialysis, Gas permeation membranes, Pervaporation, Nano filtration and micro filtration.

CO2

UNIT-III Modelling of Membrane Systems Periods: 9

Detailed theories for membrane separations – concentration polarization, gel formation and fouling, mathematical models for membrane systems with and without concentration polarization, Transport inside the membranes, solution diffusion membranes, porous membranes.

CO3

UNIT-IV Surfactant based Separations Periods: 9

Surfactant based separations - fundamentals of surfactants at surfaces and in solution, liquid membrane permeation, and foam separations, micellar separations.

CO4

UNIT-V Supercritical Fluid Extractions Periods: 9

Supercritical fluid extraction - Physicochemical principles, thermodynamic modelling, process synthesis and energy analysis

CO5


Reference Books:

1. R.T. Yang, Gas Separation by Adsorption Processes, Imperial College Press, 1997. 2. P.C. Wankat, Rate Controlled Processes, Springer Publications, 2005. 3. Seader and Henley, Separation Process Principles, Wiley Publication, Second Edition, 2008. 4. P. C. Wankat, Large scale adsorption and chromatography, CRC Press, 1986. 5. R. W. Rousseau, Handbook of separation process technology, John Wiley and Sons, 1987. 6. M. C. Porter, Handbook of industrial membrane technology, Noyes publication, Park Ridge, New Jersey,

1990. 7. J. F. Scamehorn and J. H. Harwell, Surfactant based separation processes, T. A. Hatton in Vol. 23 of

Surfactant science series, Marcel-Dekker., 1989. 8. M. A. McHugh and V. J. Krukonis, Supercritical fluid extraction, Butterworth, 1985.

87



Course Code

Course Name


L T P C CA SE TM

CHY09 Chemical Engineering Practice 3 - - 3 40 60 100

Prerequisite


Course Outcome

CO1 Explain the importance of process design engineering in plant based operations, modifications and decision making.

CO2 Critically select engineering materials based on their characteristics

CO3 Perform calculations pertaining to the design of pumping systems.

CO4 Perform calculations for economic selection and sizing of pipes and piping system components and also explain various tracing techniques.

CO5 Explain various utilities of a chemical plant.

UNIT-I Process Flowsheets Periods: 9

Role of a process Engineer, Process documentation, flow sheets – types, preparation, flow sheet presentation, symbols, line and equipment symbols, Piping and Equipment identification, Standards and codes, time planning and Scheduling.

CO1

UNIT-II Engineering Materials Periods: 9

Materials selection: mechanical properties, materials- metals, polymeric materials, ceramic materials, graphite, glasses, Corrosion, Factors affecting corrosion, Causes and cures, types, material selection for corrosion resistances, novel engineering materials.

CO2

UNIT-III Pumps, Blowers and Compressors Periods: 9

Pumps classification and types, Pump performance characteristics and selection of pumps, packing and mechanical seals, pumping systems design, pump priming. Fans, blowers, compressor, ejectors and mechanical vacuum systems.

CO3

UNIT-IV Valves and Insulation Periods: 9

Piping calculations, available piping, tubing and other flow conduits, economical sizing of pipe, Valves: types, sizing and selection Thermal insulation, usages for thermal insulation, types of insulation, recommended thickness of insulation, Tracing- steam tracing, electric tracing, jacketing.

CO4

UNIT-V Plant Utilities Periods: 9

Utilities of a chemical plant, Boilers, Cooling tower, DM water plants, Industrial water Treatment, Turbines, Chillers, Process Safety and Pressure relieving devices, Storage tanks.

CO5


Reference Books:

1. Henry J. Sandler, Edward T. Luckiewicz, Practical process engineering – A working approach to plant design, McGraw Hill Book Company,1987.

2. Ernest E. Ludwig, Applied Process Design, Vol. I, II & III, 3rd Edition, Gulf Professional Publishing, 1999.

88




L T P C CA SE TM

CHY10 Fluidization Engineering 3 - - 3 40 60 100

Prerequisite


Course Outcome

CO1 Distinguish various fluidization regimes

CO2 Calculate various hydrodynamic parameters

CO3 Critically analyse solids mixing and segregation

CO4 Quantify heat and mass transfer coefficients through models

CO5 Appreciate various multiphase systems

UNIT-I Introduction Periods: 9

Introduction: Fluidized state, nature of hydrodynamic suspension, regimization of the fluidized state, operating models for fluidization systems

CO1

UNIT-II Hydrodynamics of Fluidisation Periods: 9

Hydrodynamics of Fluidisation Systems: General bed behaviour, pressure drop, empirical correlations for solid holdup, flow models.

CO2

UNIT-III Mixing and Segregation Periods: 9

Solid Mixing and Segregation: Degree of Segregation, operation shifts, reversal points, mixing-segregation equilibrium generalized fluidization of poly systems, liquid phase mixing and gas phase mixing.

CO3

UNIT-IV Heat and Mass Transfer Periods: 9

Heat and Mass Transfer in Fluidization Systems: Mass Transfer-Gas-liquid Mass Transfer, liquid-solid mass transfer and wall to bed mass transfer. Heat Transfer-Column wall to bed Heat Transfer.

CO4

UNIT-V Miscellaneous Systems Periods: 9

Miscellaneous Systems: Moving bed, slurry bubble column, two phase and three phase inverse fluidized bed, typical applications.

CO5


Reference Books:

1. Kunii D and Levenspiel .O, Fluidization Engineering, Elsevier Publication, 2005. 2. Leva M, Fluidization, McGraw Hill Publications, 1959. 3. Davidson J.F and Harrison D, Fluidization, Academic Press, 1971.

89


Semester : Seventh Course Category Code: PEC Semester Exam Type: TY


L T P C CA SE TM

CHY11 Risk and Safety Management in Process Industries

3 - - 3 40 60 100

Prerequisite


Course Outcome

CO1 Conduct hazards and operability studies from the knowledge gained on risk analysis

CO2 Apply appropriate guidelines by identifying various hazards in work place

CO3 Develop awareness and suggest mitigation measures needed in handling hazardous materials.

CO4 Develop safety guidelines for personnel and environmental protection in handling hazardous pollutants in various industries.

CO5 Gain knowledge on safety education and training

UNIT-I Hazard Identification Periods: 9

Hazard identification methodologies, risk assessment methods - PHA, HAZOP, MCA, ETA, FTA, consequence analysis, probit analysis.

CO1

UNIT-II Hazards in work Places Periods: 9

Hazards in work places - nature and type of work places, types of hazards, hazards due to improper house-keeping, hazards due to fire in multi-floor industries and buildings, guidelines and safe methods in the above situations.

CO2

UNIT-III Hazardous Chemicals Periods: 9

Workers’ exposures to hazardous chemicals, TLVs of chemicals, physical and chemical properties of chemicals leading to accidents like fire explosions, ingestion and inhalation, pollution in work places due to dangerous dusts, fumes and vapours, guidelines, fundamentals of pressure relief devices and safe methods in chemicals handling, storage and entry into confined spaces.

CO3

UNIT-IV Industrial Hazards Periods: 9

Hazards peculiar to industries like fertilizer, heavy chemicals, petroleum, pulp and paper, tanneries, dyes, paints, pesticides, glass and ceramics, dairy and sugar industries, guidelines for safeguarding personnel and safeguarding against water, land and air pollution in the above industries.

CO4

UNIT-V Process Safety Periods: 9

Safety education and training - safety management, fundamentals of safety tenets, measuring safety performance, motivating safety performance, legal aspects of industrial safety, safety audit. Process Safety and management Systems

CO5


Reference Books:

1. F. P. Lees, Loss prevention in process industries, 2nded, Butterworth-Heinemann, 1996. 2. W. Handley, Industrial safety handbook, 2nd ed., McGraw-Hill, 1977. 3. S. P. Levine, 1985, Protecting personnel at hazardous waste sites, Martin- Butterworth, 1971. 4. R. P. Blake, Industrial safety, Prentice Hall, 1953. 5. D. Patterson, Techniques of safety management, McGraw-Hill, 1978.

90




L T P C CA SE TM

CHY12 Pollution Control in Process Industries

3 - - 3 40 60 100

Prerequisite


Course Outcome

CO1 Explain the basic concepts of pollution, pollution control and to identify sources, techniques and monitoring of air pollution.

CO2 Assess the degree of treatment required for waste water by analysis its characteristics.

CO3 Identify the sources of solid wastes and to manage them.

CO4 Explain the concepts involved in control techniques of noise pollution and to give in-depth information about laws, policies and acts related to environmental system.

CO5 Carry out case studies on pollution related to various industries

UNIT-I Introduction to Air Pollution Periods: 9

Man and Environment, Types of pollution, Pollution control aspects, Pollution monitoring and analysis of pollutant. Air pollution: Sources and effects, particulate control, control of gaseous pollutants (SOx, NOx, oxides of carbon, hydrocarbon pollutants), Air Quality Management, Carbon Trading.

CO1

UNIT-II Water Pollution Periods: 9

Types of water pollution, sources, water pollution control. Waste water treatment technologies and Recycle.

CO2

UNIT-III Solid waste management Periods: 9

Sources, processing methods, waste disposal methods, energy recovery from solid waste and land pollution.

CO3

UNIT-IV Noise Pollution Periods: 9

Hazardous noise exposure, noise measuring instruments and noise pollution control technology. Regulations: ISO 14000, 9000, pollution Acts and Regulations.

CO4

UNIT-V Case Study Periods: 9

Pollution (Air, Water & Solid) control in the following process industries - Fertilizers, Petroleum Refinery and Petrochemical, Pulp and Paper, Cane Sugar, Tannery, Distilleries and Pharmaceutical Industry .

CO5


Reference Books:

1. S.C. Bhatia, Environmental Pollution and control in chemical process Industries, Khanna Publishers, 1st Edition, 2001.

2. C.S.Rao, Environmental Pollution Control Engineering, Wiley Eastern, 1992. 3. S.P.Mahajan, Pollution control in Process Industries, Tata McGraw Hill, 1990. 4. F. P. Lees, Loss prevention in process industries, 2nd Edition, Butter worth- Heinemann, 1996. 5. Martin Crawford, Pollution Control Theory, McGraw Hill, 1976. 6. Marell, Solid Wastes, John Wiley, 1975.

91



Course Code

Course Name


L T P C CA SE TM

CHY13 Bioprocess Engineering 3 - - 3 40 60 100

Prerequisite


Course Outcome

CO1 Explain the basic concepts cum constraints of biology, biotechnology and microbiology.

CO2 Design enzymatic reaction systems by understanding the biological characteristics and industrial role of different types of enzymes.

CO3 Explain different types, requirements and principles of growth and metabolism of biological cells.

CO4 Explain the principles of fermentation and identify different types of industrial fermenters and bioreactors.

CO5 Appreciate the application of the principles of bio processing for industrial production of commercially important products such as wine, beer, cheese, bio ethanol, bakery yeast and Penicillin..

UNIT-I Introduction Periods: 9

Introduction to bioprocess engineer, story of Penicillin, regulatory constraints of bioprocess engineering, microbial diversity, biomolecules, Recombinant DNA technology, Cell Mutation.

CO1

UNIT-II Enzyme and Enzyme kinetics Periods: 9

Enzymes: Introduction, types, industrially and medically important enzymes, Enzyme kinetics for SSSE system, Methods of Enzyme Immobilisation.

CO2

UNIT-III Metabolic Pathways Periods: 9

Metabolic Pathways: Bioenergetics , glucose metabolism, glucolysis, TCA cycle, Respiration, Anaerobic Metabolism, Batch Cellular growth kinetics, cell growth nutrients.

CO3

UNIT-IV Fermentation Periods: 9

Principles of Fermentation: types of industrial fermentation, fermentation media, sterilization, inoculums development, instrumentation and control of Fermentor, bioreactor types, downstream processing.

CO4

UNIT-V Industrial Products Periods: 9

Traditional Industrial Bioprocess: Ethanol Production, Bakers Yeast production, Penicillin Production, Beer Production, wine production and cheese production.

CO5


Reference Books:

1. Michael Shuler and F.Kargi, Bio Process Engineering Basic Concepts, PHI learning private limited,2nd Edition,2002 .

2. Biswajit Mukherjee, Bio process Engineering, Black Prints, 2012. 3. Doran, Bioprocess Engineering Principles, Elsevier India Private Ltd, 2011.

92


Semester : Seventh Course Category Code: PEC



L T P C CA SE TM

CHY14 Process Optimization 3 1 - 3 40 60 100

Prerequisite

Course Outcome

CO1 Appreciate the theory and concepts of optimisation

CO2 Apply numerical search methods for locating the minima of functions in one variable

CO3 Apply variable search algorithms for finding out the extreme of multivariable functions with and without constraints

CO4 Able to formulate and solve optimisation problems using linear , geometric , dynamic and Integer programming methods

CO5 Formulate and solve optimisation problems in chemical Engineering

UNIT-I Concepts of Optimization Periods: 12

Introduction – General concepts of optimization, classification of optimization problem – single variable and multivariable, constrained and unconstrained, continuous and discrete optimization problems; Mathematical representation, geometrical interpretation, degrees of freedom analysis, formulation of optimization problems – simple illustrations. Theory and concepts of optimization - functions and their properties – unimodal and multimodal functions, local and global minimum; Gradient vector, Hessian matrix, Positive and negative definiteness of symmetric matrix, test of convexity and concavity, Stationary points, Necessary and sufficient conditions for extremum of single and multivariable functions, illustrative problems.

CO1

UNIT-II Linear regression Periods: 12

Linear regression – method of least squares, fitting models to data, factorial design of experiments, illustrative problems. Introduction to one dimensional search – scanning and bracketing algorithms, two point equal interval search, golden section search, quadratic interpolation method, Newton and quasi Newton method, Illustrative problems.

CO2

UNIT-III Constrained optimization Periods: 12

Constrained optimization – Equality constrained optimization, Lagrange multiplier method, inequality constrained optimization, Kun-Tucker necessary condition, sufficient condition for constrained optimization, illustrative examples. Introduction to multivariable search – Gradient descent method (line search), Hessian based search algorithms, Newton’s method, Conjugate gradient method, illustrative problems.

CO3

UNIT-IV Linear Programming Periods: 12

Linear Programming – introduction, illustration of concepts using graphical approach, simplex algorithm, variables unrestricted in sign, degenerate LP problem, illustrative problems. Introduction to geometric programming, dynamic programming, and integer programming (only illustration of concepts and no problems to be asked in the semester examination)

CO4

UNIT-V Application of optimization in chemical engineering

Periods: 12

Application of optimization in chemical engineering – Optimal pipe diameter, optimal thickness of insulation, optimal inter stage pressure in multistage compression, optimal design of shell and tube heat exchanger, optimal reflux ratio in a binary distillation column, optimal batch time in a batch reactor, optimal temperature of progression for exothermic reversible reaction, Optimal scheduling of refinery operation, Optimum recovery of waste heat, optimal design and operation of staged distillation columns.

CO5

Lecture Periods: 45 Tutorial Periods: 15 Practical Periods:- Total Periods: 60

Reference Books:

1. T.F.Edger and D.M.Himmelblau, Optimization of Chemical Processes, McGraw-Hill, 2001. 2. Kalyanmoy Deb, Optimization for Engineering Design, John Wiley, 1995. 3. V.Kafarov, Cybernetic Methods in Chemistry and Chemical Engineering, MIR Publishers, 1976.

93

Open Elective Courses

94

Department : Chemical Engineering Programme: B.Tech

Semester : Third/Fourth/Fifth/Sixth/Seventh Course Category Code: OEC Semester Exam Type: TY


L T P C CA SE TM

CHO01 Process Engineering Principles

3 - 3 40 60 100

Prerequisite


Course Outcome

CO1 Appreciate the importance of chemical Engineering and explain the basic laws of chemical Engineering

CO2 Gain knowledge on the principles involved in fluid flow and mechanical operations

CO3 Identify the basic modes of heat transfer and explain the working principle of industrial heat transfer equipments

CO4 Explain the fundamentals of mass transfer and mass transfer equipments

CO5 Explain the fundamentals of reaction engineering and various reactors

UNIT-I Process Principles Periods: 9

Chemical Process Industries - Batch and Continuous mode of operations–Process Flow Sheets–Material and Energy Balance Principles – Mass – Mole – Volume Conversions (Ideal Gas Law), Sensible and Latent Heat Calculations, Principles of Momentum, Heat and Mass Transport – Rate Laws (Newton’s Law, Fourier’s Law, Fick’s law), Chemical Reactions rate and equilibrium, Phase equilibrium, Vapour Pressures and Humidity.

CO1

UNIT-II Fluid Transport and Mechanical Operation Equipments

Periods: 9

Laminar and Turbulent flow, Flow Characteristics of fluids – Newtonian and Non-Newtonian, Friction factor, Head loss due to fluid friction pumps – different types, pump characteristics, compressors. Size reduction of solids – crushing (Jaw crusher) and grinding (Ball mill), Size separation (screening), solid – liquid separation–filtration, settling and sedimentation, centrifuge.

CO2

UNIT-III Heat Transfer Equipments Periods: 9

Modes of heat transfer–conduction, convection and radiation, heat transfer without and with phase change (evaporation, condensation), heat transfer coefficient. Heat Exchangers – double pipe and shell and tube, condensers – vertical and horizontal, evaporators – single effect and multiple effect, reboilers.

CO3

UNIT-IV Mass transfer Equipments Periods: 9

Molecular and turbulent transport of mass–mass transfer coefficient, mass transfer principles in separation, gas – liquid operations – absorption, distillation, humidification – packed and tray towers. Fluid – solid operations – adsorption, drying, leaching, crystallization. Liquid- liquid operations – extraction.

CO4

UNIT-V Chemical Reactors Periods: 9

Single and multiple reactions–conversion, yield, selectivity batch and flow reactors(PFR,CSTR), catalyses, multiphase non-catalytic (gas – solid, gas – liquid) and catalytic reactors, fixed bed, fluidized bed, slurry reactors. Process flow sheets for manufacture of standard chemicals - urea, sugar, crude distillation, cement, paper and pulp.

CO5


Reference Books:

1. Walter. L Badger and Julius.T.Banchero , Introduction to Chemical Engineering, , Tata McGraw Hill.2001 2. Octave Levenspiel , Chemical Reaction Engineering, Wiley Eastern Ltd., II Edition, 2000. 3. W.L.Mc.Cabe, J.C.Smith and P.Harriot , Unit operations of chemical engineers, , McGraw Hill International Edition, V edition,1998. 4. N.Shreve , Chemical Process Industries,5th edition, McGraw Hill, New York, 1984. 5. Salil K Ghosal, Shyamal K Sanyal and Siddhartha Datta, Introduction to Chemical Engineering, Tata McGraw-

Hill, 1993.

95

Department : Chemical Engineering Programme: B.Tech



L T P C CA SE TM

CHO02 Green Chemistry and Engineering 3 - - 3 40 60 100

Prerequisite Nil


Course Outcome

CO1 Identify and assess various global environmental issues.

CO2 Enumerate , classify and explain the various pollution prevention strategies

CO3 Explain the concept of zero discharge and good work place

CO4 Develop process mass and energy integration steps.

CO5 Analyse the concept of Life cycle Analysis.

UNIT-I Environmental Issues Periods: 9

Overview of Major Environmental Issues, Global Environmental Issues. Air Quality Issues. Water Quality Issues, Ecology, Natural Resources, Description of Risk. Values of Risk Assessment in the Engineering Profession. Risk-Based Environmental Law. Risk Assessment Concepts. Hazard Assessment. Dose-Response. Risk Characterization.

CO1

UNIT-II Current Strategies Periods: 9

Pollution Prevention – Pollution Prevention Concepts and Terminology, Chemical Process Safety. Responsibilities for Environmental Protection. Environmental Persistence. Classifying Environmental Risks Based on Chemical Structure. Exposure Assessment for Chemicals in the Ambient Environment.

CO2

UNIT-III Green Chemistry Periods: 9

Green Chemistry. Green Chemistry Methodologies. Quantitative/Optimization-Based Frameworks for the Design of Green Chemical Synthesis Pathways. Green Chemistry Pollution Prevention in Material Selection for Unit Operations. Pollution Prevention for Chemical Reactors. Pollution Prevention for Separation, Devices, Pollution Prevention Applications for Separative Reactors. Pollution Prevention in Storage Tanks and Fugitive Sources.

CO3

UNIT-IV Process Integration Periods: 9

Process Energy Integration. Process Mass Integration. Case Study of a Process Flow Sheet-Estimation of Environmental Fates of Emissions and Wastes.

CO4

UNIT-V Life Cycle Analysis Periods: 9

Magnitudes of Environmental Costs. A Framework for Evaluating Environmental Costs. Hidden Environmental Costs. Liability Costs. Internal Intangible Costs. External Intangible Costs. Introduction to Product Life Cycle Concepts. Life-Cycle Assessment. Life-Cycle Impact Assessment. Streamlined Life Cycle Assessments. Uses of Life Cycle Studies.

CO5


Reference Books:

1.Allen, D.T., Shonnard, D.R, Green Engineering: Environmentally conscious Design of Chemical Processes, Prentice Hall PTR 2002. 2.MukeshDoble and Anil Kumar Kruthiventi, Green Chemistry and Engineering, Elsevier, Burlington, USA, 2007.

96




L T P C CA SE TM

CHO03 Energy Engineering 3 - 3 40 60 100

Prerequisite


Course Outcome

CO1 Explain the global and Indian energy scenario and identify different forms of energy

CO2 Identify various conventional energy resources and their applications.

CO3 Identify various Renewable energy resources ways of harnessing energy from them along with merits and demerits

CO4 Appreciate Biomass as a source of energy and understand different methods of conversion of biomass into energy

CO5 Apply the basic skills required for energy auditing and to make action plans and conservation policies.

UNIT-I Energy Periods: 9

Introduction to energy- Global energy scene- Indian energy scene- Units of energy, conversion factors, general classification of energy, energy crisis, energy alternatives.

CO1

UNIT-II Conventional Energy Periods: 9

Conventional energy resources, Thermal, hydro and nuclear reactors, thermal, hydro and nuclear power plants, efficiency, merits and demerits of the above power plants, combustion processes, fluidized bed combustion.

CO2

UNIT-III Non Conventional Energy Periods: 9

Solar energy; solar thermal systems; flat plate collectors, focusing collectors, solar water heating, solar thermal power generation, solar energy application in India, energy plantations. Wind energy: types of windmills, types of wind rotors, wind electric power generation, wind power in India, economics of wind farm, Ocean energy: ocean wave energy conversion, ocean thermal energy conversion, tidal energy conversion, geothermal energy.

CO3

UNIT-IV Biomass Energy Periods: 9

Biomass Origin - Resources estimation. Thermo chemical conversion- Biological conversion. Chemical conversion- Hydrolysis & hydrogenation, solvolysis, bio crude, bio diesel power generation gasifier, biogas, integrated gasification.

CO4

UNIT-V Energy Management Periods: 9

Energy Conservation act, Energy Management duties and responsibilities, Energy Audit-Types, methodology and reports. Thermal energy Management.

CO5


Reference Books:

1. Rao,S. and Parulekar, B.B., Energy Technology, Khanna Publishers 2005. 2. Rai, G.D., Non conventional Energy Sources, Khanna Publishers, New Delhi, 1984. 3. Nagpal, G.R., Power Plant Engineering, Khanna Publishers 2008.3. Energy Management, Paul W.O. Callaghan McGraw – Hill, 1993. 4. Nejat Vezirog, Alternate Energy Sources, IT, McGraw Hill, New York, 1981.

97




L T P C CA SE TM

CHO04 Introduction to Microelectronic Fabrication Processes

3 - 3 40 60 100

Prerequisite


Course Outcome

CO1 Explain the concept involved in chip manufacturing process and various terminology related to it

CO2 Enumerate various physical and electrochemical vapour deposition techniques for chip manufacturing.

CO3 Explain the basics of chemical vapour deposition and atomic layer deposition and their deposition techniques

CO4 Describe various removal methods involved in chip manufacturing

CO5 Understand various surface modification methods and characterisation methods

UNIT-I Chip Manufacturing Concepts Periods: 9

Overview of Chip Manufacturing Process, FEOL and BEOL Concepts, Lithography basics, layout, hierarchy vs flat file, levels and layers in layout file, Projection printing, dark field mask, positive resist and its advantages. Process details including resist coating, pre-exposure bake, exposure, soft bake, developing and hard bake, Stepper vs scanner, Resolution, numerical aperture, Production Issues

CO1

UNIT-II Physical and Electrochemical Vapour Deposition Periods: 9

Deposition Techniques - Physical Vapour Deposition (PVD) basics, equipment description and operation details, RF/magnetron sputtering, long throw, ionized metal plasma (IMP) sputtering, collimated beam, sputtering yield. Electrochemical deposition, Electro-migration vs grain size, conformal, anti conformal and super fill. Suppressor, accelerator, levelers, effect of seed layer, spin on coating.

CO2

UNIT-III Chemical Vapour Deposition Periods: 9

Chemical vapor deposition (CVD) basics, Atmospheric pressure (APCVD), low pressure (LPCVD), plasma enhanced (PECVD), mass transfer control and reaction kinetics control. Reactor description and operation, deposition of silicon, poly silicon, oxide, nitride and tungsten, brief introduction to atomic layer deposition (ALD) and molecular beam epitaxy (MBE).

CO3

UNIT-IV Removal Methods Periods: 9

Wet etching: Isotropic etch, selectivity, anisotropic Si etch in KOH, cleaning, Chemicals for oxide and nitride removal Dry etching : Plasma, anisotropic etch, equipment details and operation, Reactive ion etching (RIE), veil formation and de-veil, electrostatic discharge (ESD), aluminum etch, Chemical Mechanical planarization (CMP) basics, Front end of line (FEOL) basics, transistor structure and operation.

CO4

UNIT-V Modification methods Periods: 9

Material modification methods (diffusion, ion implantation, oxidation), process integration, testing and yield, relevant tools and techniques (FIB,SEM,AFM, ellipsometry)

CO5


Reference Books:

1. The Science and Engineering of Microelectronic Fabrication (2nd Edition) by S.A. Campbell, Oxford University Press, 2001.

2. Introduction to Microelectronic Fabrication, Vol. 5 of Modular Series on Solid State Devices (2nd Edition) by Richard C. Jaeger, Prentice Hall, 2001.

3. Microchip Fabrication: (5th Edition) by Peter Van Zant, McGraw Hill, 2004.