www.ateknea.com General meeting, Brussels 5th September 2015
Technical Project Manager Balazs RING
Slide 2
NANOTI - M12 General meeting Friday 6 th of January 2015 13:00
13:15 Welcome by the Coordinator Agenda, Project status up-date
(ATEKNEA) 13:15 14:45 Progress and status update and discussion WP3
Surface treatment procedure development (BME) WP4 Prototype
development - mechanics (BME) WP4 Prototype development -
electronics (ATEKNEA) WP5 examination of the samples (BME) WP6
In-vitro experiments (TUD) 14:45 15:00 Non-technical WPs ATEKNEA
14:45 15:15 Coffee break 15:15 17.15 Preparation for the review
meeting Project overview, status report, deviations, delays,
management issues Work done by the RTDs to meet the SMEs
expectations (incl. major deviations) Objectives of the SME-AGs,
other enterprises / end users: Technical background, expected
output from project, assessment of the current status Commercial
plans Dissemination activities 17.15 18:00 Schedule of next
meetings and any other business (open discussion) 20:00 Dinner -
Aux Armes de Bruxelles (13 rue des Bouchers1000 Bruxelles)
05-02-2015
Slide 3
Project status up-date
Slide 4
Actual issues NANOTI - M12 General meeting Budget shift for BME
approved by REA Periodic report was successfully submitted in
December Ongoing involvement of an external professional for
anodizing PS development * The consortium shall submit a periodic
report to the REA for each reporting period within 60 days after
the end of each respective period ** REA shall evaluate project
reports and deliverables and disburse the corresponding payments
within 90 days of their receipt 05-02-2015
Slide 5
Technology related objectives for RP1 To achieve the optimal
nanosurface on the implant, NANOTI project has to face a number of
challenging and dependent factors: To identify a detailed system
specification, outlining the target technology and the required
instrumentation based on market need, literature search, and the
expertise of partners. (M2). To create the mechanical and
electrical design for the laboratory equipment (Month 5) To
fabricate the laboratory-scale equipment for technology
optimization (Month 5): To prepare samples from the base materials
To get the strong and weak points of the laboratory-scale surface
treatment equipment NANOTI - M12 General meeting 05-02-2015
Slide 6
Scientific objectives for RP1 To optimize the chemical etching
parameters To optimize the electro polishing parameters To optimize
the anodizing parameters To test the scale-up effect with the
laboratory equipment To design and fabricate the prototype of
surface treatment equipment To determine interfacial energy of
implant surfaces NANOTI - M12 General meeting 05-02-2015
Slide 7
List of Workpackages NANOTI - M12 General meeting WP No.
Work-Package title Type of Activity Lead Partner Planned Status of
the WP Actual Status of the WP WP 1System specifications RTDPROTIP
100% WP 2 Development of the laboratory-scale surface treatment
equipment RTDATEKNEA 100% WP 3 Development of surface treatment
procedure RTDBME 100%80% WP 4 Development of the surface treatment
equipment prototype RTDITM 70% WP 5 Non-destructive and destructive
examination of the samples RTDBME 60% WP 6In vitro biological
studyRTD TUD 20% WP 7In vivo biological study RTDTUD 0% WP
8Facilitating the take-up of results OTHERITM 50% WP 9Project
management and coordination MANATEKNEA On going 05-02-2015
Slide 8
Gannt chart NANOTI - M12 General meeting 05-02-2015
Slide 9
Biological characterization, destructive and non-destructive
investigation Technical overview Technology development NANOTI -
M12 General meeting Sample preparation Chemical etching
Electropolishing Anodic oxidation 05-02-2015
Slide 10
Technical overview Prototype development NANOTI - M12 General
meeting 05-02-2015
Slide 11
Remaining WPs, tasks and Deliverables WP3 & WP4
Optimization of anodizing Finalization of surface treatment and
anodizing power supply WP5 Destructive and Non-destructive
examination of the samples (M3-M15) Task 5.1 Fatique test of the
samples (BME) Task 5.2 Corrosion test of the samples (BME) WP6 - In
vitro biological study (M10- M20) Task 6.1 - Study adhesion,
proliferation and differentiation of human mesenchymal stem cells
(TUD) D6.1 Documentation of the bacterial response (September 2015)
Task 6.2 - Study adhesion, proliferation and differentiation of
human mesenchymal stem cells (TUD) D6.2 Documentation of the
attachment, proliferation and differentiation of hMSC (September
2015) D6.3 Results of in vitro study (September 2015) WP7 - In vivo
biological study (M12-M24) Task 7.1 - Ethical approval (TUD) D7.1
Ethical Approval (April 2015) Task 7.2 - Study osseointegration of
dental implants in rat-tail model (TUD) D7.2 Documentation of the
osseointegration and biocompatibility (January 2016) D7.3
Independent professional report (January 2016) NANOTI - M12 General
meeting 05-02-2015
Slide 12
NANOTI - M12 General meeting Friday 6 th of January 2015 13:00
13:15 Welcome by the Coordinator Agenda, Project status up-date
(ATEKNEA) 13:15 14:45 Progress and status update and discussion WP3
Surface treatment procedure development (BME) WP4 Prototype
development - mechanics (BME) WP4 Prototype development -
electronics (ATEKNEA) WP5 examination of the samples (BME) WP6
In-vitro experiments (TUD) 14:45 15:00 Non-technical WPs ATEKNEA
14:45 15:15 Coffee break 15:15 17.15 Preparation for the review
meeting Project overview, status report, deviations, delays,
management issues Work done by the RTDs to meet the SMEs
expectations (incl. major deviations) Objectives of the SME-AGs,
other enterprises / end users: Technical background, expected
output from project, assessment of the current status Commercial
plans Dissemination activities 17.15 18:00 Schedule of next
meetings and any other business (open discussion) 20:00 Dinner -
Aux Armes de Bruxelles (13 rue des Bouchers1000 Bruxelles)
05-02-2015
Slide 13
Progress and results form BME WP3, WP4, WP5 NANOTI - M12
General meeting 05-02-2015
Slide 14
Progress and results form ATEKNEA WP4 NANOTI - M12 General
meeting 05-02-2015
Slide 15
WP2- Laboratory-scale surface treatment equipment NANOTI - M12
General meeting Electrical unit was designed and fabricated based
on the system specification Chemical etching Electrolyte
temperature Ultrasonic agitation Electropolishing Current density
(up to 2A/cm2) Magnetic stirring Process timing Electrolyte
temperature U/I data logging Anodic oxidation DC Voltage (0-250V)
Magnetic stirring Process timing Electrolyte temperature Continious
/ impulse mode U/I data logging 05-02-2015
Slide 16
WP2- Laboratory-scale surface treatment equipment NANOTI - M12
General meeting Component integration Standard 19 wide metal rack
3-phase 32A power inlet, industrial connectors 05-02-2015
Slide 17
WP4- Prototype development NANOTI - M12 General meeting
Modifications due to system revision: LCD display for impulse
length and motor speed New embedded control for linear actuators
and LCD display Improved Ultrasonic performance -> 2x 120W New
agitation method: Linear actuator Centrifugal pump 05-02-2015
Slide 18
Anodizing power supply working characterics Experiments were
performed at BME to compare the behaviour of the old setup with the
electrical system Problem: applied voltage is limited by high
current draw Result: high voltage cannot be achieved in continious
mode Conclusion: its the turn-on transient not the stady state
operation that resulted different oxide layers NANOTI - M12 General
meeting Effect of consecutive pulses 05-02-2015
Slide 19
WP4- Prototype development NANOTI - M12 General meeting Impulse
mode Problems with the 1st gen.(up to 60A) New experimental setup
implemented External energy storage Electronics to isolate the
output of the PS Low-side driver topology with 20 IGBTs Serial slow
diodes to protect the IGBTs 1700uF/1000V capacitor bank, manually
selectable value 1000V / 700A peak performance 05-02-2015
Slide 20
WP4- Prototype development NANOTI - M12 General meeting Impulse
mode final version Problem noticed: Sparks may appear above 450V
!!! hort circuit protection : current limiting serial resistance
Resistance bank: 0.2/1500W Improved performance 1000V/6000A 30 High
power IGBTs (most powerful on the market) New gate driver circuit
Galvanically isolated driver pins Two digital control pins to
enable for integration purposes 05-02-2015
Slide 21
WP4- Prototype development NANOTI - M12 General meeting
Prototype electronics Electrical cabinet integration Simplified
front panel VFDs for electrolyte agitation Soft-PLC solution based
on Beckhoff TWINCAT Built-in control panel with 12 touch screen
EtherCAT coupler + IO modules Power supplies controlled with SCPI
via TCP/IP PID controller communicates via RS485 VFDs controlled
with MODBUS RTU via RS485 Digital outputs for relays, swithces
Digital inputs for safety parts (e.g. limit switch) 05-02-2015
Slide 22
WP4- Prototype development NANOTI - M12 General meeting Control
software Easy-to-use Graphical User Interface Full process control
All main parameters displayed on one screen Parallel process
esecution Editable treatment profiles Logging functions (.csv)
remote access via FTP 05-02-2015
Slide 23
Video NANOTI - M12 General meeting 05-02-2015
Slide 24
Summary and further work NANOTI - M12 General meeting Gained a
better understanding of the electrochemical system behaves The
electrical unit of the prototype has been designed and fabricated
Control software of the prototype has been implemented Integration
of the anodization power supply Electrical and mechanical
integration into the final mechanical unit Testing and fine
adjustment 05-02-2015
Slide 25
Progress and results form TUD NANOTI - M12 General meeting
05-02-2015
Slide 26
Further work NANOTI - M12 General meeting Electrical and
mechanical integration into the final mechanical unit Testing and
fine adjustment 05-02-2015
Slide 27
Vote on RTD performance NANOTI - M12 General meeting
05-02-2015
Slide 28
NANOTI - M12 General meeting Friday 6 th of January 2015 13:00
13:15 Welcome by the Coordinator Agenda, Project status up-date
(ATEKNEA) 13:15 14:45 Progress and status update and discussion WP3
Surface treatment procedure development (BME) WP4 Prototype
development - mechanics (BME) WP4 Prototype development -
electronics (ATEKNEA) WP5 examination of the samples (BME) WP6
In-vitro experiments (TUD) 14:45 15:00 Non-technical WPs ATEKNEA
14:45 15:15 Coffee break 15:15 17.15 Preparation for the review
meeting Project overview, status report, deviations, delays,
management issues Work done by the RTDs to meet the SMEs
expectations (incl. major deviations) Objectives of the SME-AGs,
other enterprises / end users: Technical background, expected
output from project, assessment of the current status Commercial
plans Dissemination activities 17.15 18:00 Schedule of next
meetings and any other business (open discussion) 20:00 Dinner -
Aux Armes de Bruxelles (13 rue des Bouchers1000 Bruxelles)
Slide 29
NANOTI - M12 General meeting Friday 6 th of January 2015 13:00
13:15 Welcome by the Coordinator Agenda, Project status up-date
(ATEKNEA) 13:15 14:45 Progress and status update and discussion WP3
Surface treatment procedure development (BME) WP4 Prototype
development - mechanics (BME) WP4 Prototype development -
electronics (ATEKNEA) WP5 examination of the samples (BME) WP6
In-vitro experiments (TUD) 14:45 15:00 Non-technical WPs ATEKNEA
14:45 15:15 Coffee break 15:15 17.15 Preparation for the review
meeting Project overview, status report, deviations, delays,
management issues Work done by the RTDs to meet the SMEs
expectations (incl. major deviations) Objectives of the SME-AGs,
other enterprises / end users: Technical background, expected
output from project, assessment of the current status Commercial
plans Dissemination activities 17.15 18:00 Schedule of next
meetings and any other business (open discussion) 20:00 Dinner -
Aux Armes de Bruxelles (13 rue des Bouchers1000 Bruxelles)
05-02-2015
Slide 30
Dissemination and exploitation Non-technical WPs
Slide 31
WP9- FACILITATING THE TAKE-UP OF RESULTS Deliverables 4/9/2014
SPABRINK - M12 Pre-review meeting D9.1 Project Website
DevelopmentM3 D9.2 A draft Plan for the Use and Dissemination of
the Foreground M9 D9.3 A final PUDFM22 D9.4 Public dissemination
reportM22 31
Slide 32
Completed dissemination actions I. Project website (submitted
as Deliverable 8.1) www.nanoti.eu Leaflet Continuously updated by
ATEKNEA with news and project related events Contains a document
sharing section for Consortium members => you can find all
project related documents there 4/9/2014 SPABRINK - M12 Pre-review
meeting 32
Slide 33
Review meeting NANOTI - M12 General meeting 05-02-2015
Slide 34
What does REA expect from Us? REA expects to see more than
results! REA wants to see that SMEs: are still behind the project
are interested in the outcome of the project still believe in the
project are also satisfied with the results NANOTI - M12 General
meeting 05-02-2015
Slide 35
What can we expect? Reviewer or officer might ask you (SMEs and
RTDs) directly! You should prepare to give a statement! You should
know about the project results! Internal consortium meeting on the
day before review meeting to update you about the content of the
report and the expected questions. Final periodic report Submitted
in December 2014, All deliverables due up to M9 (end of RP1)
submitted NANOTI - M12 General meeting 05-02-2015
Slide 36
06-02-2015 NANOTI - RP1 Review meeting Friday 6 th of January
2015 10:00 10:10 Welcome and introduction REA, PO 10:10 10:35
Project overview (ATEKNEA) Main goals and objectives Status report
(WPs, deliverables, milestones, scheduling) Deviations, amendments
Risk management Project financing, Use of resources 10.35 11.50 RTD
performance related to DOW and SMEs expectations Progress and
results form ATEKNEA Progress and results from BME Progress and
results from TUD 11.50 12.40 Impact of project for the SMEs
(Technical background, expected output, commercial plans and steps
undertaken, assesment of the current status)
Slide 37
06-02-2015 NANOTI - RP1 Review meeting Friday 5 th of September
2014 12:40 13:00 Impact for USZ (Technical background, expected
output, assesment of the current status, commercial plan) 13:00
13:45 Lunch break 13:45 14:15 Exploitation and Dissemination (incl.
interim Plan for Use and Dissemination of Knowledge) 14:15
15:00Discussion between reviewer and REA 15:00 15:30 Feedback by
REA and the Reviewer
Slide 38
MEDGRUPE NANOTI - M12 General meeting 05-02-2015
Slide 39
PROTIP NANOTI - M12 General meeting 05-02-2015
Slide 40
ITM NANOTI - M12 General meeting 05-02-2015
Slide 41
USZ NANOTI - M12 General meeting 05-02-2015
Slide 42
ITM NANOTI - M12 General meeting 05-02-2015
Slide 43
Overview NANOTI - M12 General meeting ATEKNEA is generally
responsible for the design and fabrication of the electrical
system. WP leader of: WP2 Development of the laboratory-scale
surface treatment equipment Task leader of: T2.2 Design of the
electrical units T4.3 Design and fabrication of the surface
treatment equipment prototype Significant contribution to: T1.1 -
System specification T4.2 Laboratory equipment development for
testing the scale-up effect 05-02-2015
Slide 44
WP2- Laboratory-scale surface treatment equipment NANOTI - M12
General meeting Electrical unit was designed and fabricated based
on the system specification Chemical etching Electrolyte
temperature Ultrasonic agitation Electropolishing Current density
(up to 2A/cm2) Magnetic stirring Process timing Electrolyte
temperature U/I data logging Anodic oxidation Voltage (0-250V)
Magnetic stirring Process timing Electrolyte temperature Continious
/ impulse mode U/I data logging 05-02-2015
Slide 45
WP2- Laboratory-scale surface treatment equipment NANOTI - M12
General meeting Main components of the system: 3x PID controllers
for temperature control with FEP coated sensors Solid State Relay
based power drive stage (up to 40A per channel) DC motors for
stirring (0-300 RPM) Electro-polishing power supply (0-80V, 0-40A)
Anodization power supply (0-360V, 0-15A) 60W ultrasonic generator
Custom-made heating coils Custom-made impulse generator
05-02-2015
Slide 46
WP2- Laboratory-scale surface treatment equipment Impulse
generator Microcontroller-based operation High-power IGBT switching
Variable impulse length: 200us - 100ms Analog impulse length
setting (potentiometer) Manual impulse generation with a pushbutton
Preparation for RS232 control Tested with 30 Ohm/50W load NANOTI -
M12 General meeting 05-02-2015
Slide 47
WP2- Laboratory-scale surface treatment equipment NANOTI - M12
General meeting Component integration Standard 19 wide metal rack
3-phase 32A power inlet, industrial connectors 05-02-2015
Slide 48
WP4- Prototype development NANOTI - M12 General meeting
Modifications due to system revision: LCD display for impulse
length and motor speed New embedded control for linear actuators
and LCD display Improved Ultrasonic performance -> 2x 120W New
agitation method: Linear actuator Centrifugal pump 05-02-2015
Slide 49
WP4- Prototype development NANOTI - M12 General meeting Impulse
mode Problems with the 1st gen.(up to 60A) New experimental setup
implemented External energy storage Electronics to isolate the
output of the PS Low-side driver topology with 20 IGBTs Serial slow
diodes to protect the IGBTs 1700uF/1000V capacitor bank, manually
selectable value 1000V / 700A peak performance 05-02-2015
Slide 50
WP4- Prototype development NANOTI - M12 General meeting Impulse
mode final version Problem noticed: Sparks may appear above 450V
Short circuit protection : current limiting serial resistance
Resistance bank: 0.2/1500W Improved performance 1000V/6000A 30 High
power IGBTs (most powerful on the market) New gate driver circuit
Galvanically isolated driver pins Two digital control pins to
enable for integration purposes 05-02-2015
Slide 51
WP4- Prototype development NANOTI - M12 General meeting
Prototype electronics Electrical cabinet integration Simplified
front panel VFDs for electrolyte agitation Soft-PLC solution based
on Beckhoff TWINCAT Built-in control panel with 12 touch screen
EtherCAT coupler + IO modules Power supplies controlled with SCPI
via TCP/IP PID controller communicates via RS485 VFDs controlled
with MODBUS RTU via RS485 Digital outputs for relays, swithces
Digital inputs for safety parts (e.g. limit switch) 05-02-2015
Slide 52
WP4- Prototype development NANOTI - M12 General meeting Control
software Easy-to-use Graphical User Interface Full process control
All main parameters displayed on one screen Parallel process
esecution Editable treatment profiles Logging functions (.csv)
remote access via FTP 05-02-2015
Slide 53
Further work NANOTI - M12 General meeting Electrical and
mechanical integration into the final mechanical unit Testing and
fine adjustment 05-02-2015
Slide 54
Q&A Thank you for you attention
Slide 55
www.ateknea.com ATEKNEA SOLUTIONS HUNGARY Kft. Ttnyi t 84-86.
HU-1119 BUDAPEST. T. +36 1 787 4024 F. +36 1 787 4390 NANOTI - M12
General meeting Thank you for your attention! +36-1-787-4024 x
338balazs.ring.ateknea Technical Project Coordinator
[email protected] Balazs Ring 05-02-2015
Slide 56
WP4- Prototype development NANOTI - M12 General meeting Power
supply Charge/ discharge control Capacitor bank Electrochemical
cell Power supply Impulse driver Electrochemical cell
05-02-2015