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Vacuum system

Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

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Page 1: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Vacuum system

Page 2: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Principal scheme

Page 3: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa
Page 4: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Vacuum parameters

1 Preliminary vacuum 1*10-2 Pa

2 Melt storage 5*10-4 Pa

3 Crystal annealing 5*10-5 Pa

Page 5: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Mechanical pump.Construction and

principle of operation.

Page 6: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Two Stage Rotary Vane Vacuum Pump

3 phase engine

Inlet and outlet

Oil level

Oil removal

Page 7: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Gas flow in rotary pump

1, 7 –stages, 2,3 – valve, 4 – gas outlet, 5- gas channel, 6 – gas inlet

Page 8: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Vacuum characteristic

Page 9: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Diffusion pump

Page 10: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Structure of diffusion pump

1 – body; 2, 10 – covers; 3, 11 – washer; 4 – oil reflector; 5 – earth; 6 – vapor path; 7 – spiral way; 8 – heater;

Page 11: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Stage

Oil reflector

Cooling water

Page 12: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

10-7 10-6 10-5 10-4 10-3 10-2 10-1100

101

102

103

104

105S

pee

d l

/sec

Input pressure, torr

Vacuum characteristic

Page 13: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Electromagnetic valve. Solenoid principle of operation.

Page 14: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Manual close ring

Engine

Cover

Vacuum lock. Construction and principle of operation.

Page 15: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Structure of lock

Page 16: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Vacuum meter APG. Principle of operation.

1- electric cable, 2- socket,3 – spring ring, 4-vacuum flange, 5-filter

Page 17: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Principle of operation Pirani

TO MEASURE VACUUM BY MEASURING HEAT CONDUCTIVITY OF GAS

Heater wire

Thermocouple

Page 18: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Vacuum meter WRG. Principle of operation.

WRG – combination of inverse magnetron sensor and PiraniWay of measuring is chosen automatically

Page 19: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Principle of operation

Dependence of ionized gas current on pressureCrossed magnetic field make longer path of ions before reach anode

+

-E H

Page 20: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Plant assembly

Page 21: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Vacuum line is fixed to the frame by

Joining crystallizer with 3 bolts Joining right angle tube with 2 bolts Vacuum devices and parts are mutually fixed with clamps and rings

Page 22: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

To set the crystallizer on the frame and to fix it with the bolts

Page 23: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

To join the vacuum tube to crystallizer and frame by means of the bolts

and the studs

Page 24: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

To join the lock and diffusion pump by means of the studs

Page 25: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

To set the side shields and to fix them with the screws

Page 26: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

To set up vacuum devices

Page 27: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

To set up water tube with water collector

Water collector

Pressure meter

Page 28: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Water collector

Page 29: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Water piping1-Valve2-Pressure meter3-12 –Valves of the grower parts13- Diffusion pump14-Thyristor15 – Chamber16 –Bottom17- Small cover18- Big cover19 -Rod20-Cutter21- Current lead 122- Current lead 223-34 –Thermal sensor of the elements35- Funnel

Page 30: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

To set and fix with the bolts the column to the frame

Page 31: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

To set and to fix the computer control board

Page 32: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

To set the supports and to adjust them in order to provide for horizontal

orientation of the grower

Page 33: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Assembly of hot zone inside the crystallizer

Bottom SupportSide shield

W Tube

Page 34: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Checking the center of W-tube and the gap

Page 35: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Mo shield and W-tube

Shield to the current lead

Bottom shield

Page 36: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Bottom shield

Support

Bottom shieldGranules

Page 37: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Al2O3 loading

Page 38: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

To put on and to fix the big cover with the nuts

Page 39: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Heater

Page 40: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Small cover

Lobe

Window

Page 41: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

To set and to fix bus bars with the bolts

Page 42: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

To set and fix the side shields on the frame

Page 43: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

To set the transformer unit

Page 44: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

To set the mechanical vacuum pump

Page 45: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Maintenance

Checking for vacuum seals and junctions Checking of water cooling system Checking for thermal screens and hot

zone elements wear Correction of crucible position

Page 46: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Safety measuresElectrical safetyThere are the following sources of electric safety:

chains of power supply of the component parts of the grower,panels and blocks with electric apparatus and electric equipment, located on the control panel, crystallizer, power cabinet.

Protection of maintenance staff against electrical shock is provided by the doors which can be opened by special key and by protective grounding.

There are grounding bolts with special marks on the doors of the power cabinet and control unit.

Page 47: Vacuum system. Principal scheme Vacuum parameters 1 Preliminary vacuum 1*10 -2 Pa 2 Melt storage 5*10 -4 Pa 3 Crystal annealing 5*10 -5 Pa

Danger of thermal burns.There are the following sources of thermal

burns: the heater, screens and the melt surface at monitoring of crystallization front through non-protected window, therefore after termination of technological process it is allowed to open the grower only after its complete cooling.

To protect the eye of process engineer from thermal irradiation at monitoring of seeding process it is necessary to use the light filter.