Ultrasonic Evaluation of TiAl And40 Cr Diffusion Bonding Quality Based on Time-scale Characteristics Extraction

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  • 8/13/2019 Ultrasonic Evaluation of TiAl And40 Cr Diffusion Bonding Quality Based on Time-scale Characteristics Extraction

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    Ultrasonic evaluation of TiAl and 40Cr diffusion bonding quality based

    on time-scale characteristics extraction

    Yilin Luan a,n, Tao Sun a, Jicai Feng b, Tie Gang c

    a School of Mechatronics Engineering, Harbin Institute of Technology, Harbin, Chinab School of Materials Science & Engineering, Harbin Institute of Technology at Weihai, Weihai, Chinac State Key Lab of Advanced Welding and Jointing, Harbin Institute of Technology, Harbin, China

    a r t i c l e i n f o

    Article history:Received 25 September 2010

    Received in revised form

    12 April 2011

    Accepted 13 July 2011Available online 27 July 2011

    Keywords:

    Ultrasonics

    Diffusion bonding

    Dissimilar materials

    Continuous wavelet transform

    Time-scale amplitude and phase

    a b s t r a c t

    To solve the problem of ultrasonic pulse-echo method in the evaluation of kissing bond and unbond inTiAl and 40Cr diffusion bonding, a characteristics extraction algorithm was proposed. The algorithm was

    based on continuous wavelet transform to convert ultrasonic TiAl and 40Cr diffusion bonding interface

    signals into time-scale domain. The ultrasonic tests were performed by an ultrasonic C-scan imaging

    system using a 10 MHz focused transducer. The time-scale amplitude and phase of the interface signals

    were calculated and analyzed to distinguish the kissing bond and the unbond from the perfectly

    bonded interface. The kissing bond can be detected by the scale-dependent amplitude combined with

    phase variation and the unbond can be measured by the opposite phase. The amplitude and phase

    characteristics were extracted to reconstruct the amplitude and phase characteristics images for TiAl

    and 40Cr diffusion bonding specimens evaluation. The amplitude and phase characteristics images are

    effective in the evaluation of bonding quality.

    & 2011 Elsevier Ltd. All rights reserved.

    1. Introduction

    Diffusion bonding has been considered as a potential welding

    method and increasingly used in the field of aerospace and

    industry, which has many advantages such as high performance,

    significant cost and weight savings, and low requirement for the

    weldability of materials [1,2]. However, imperfections such as

    kissing bond and unbond may occur at the interface due to

    improper surface preparation and upset bonding conditions [3].

    These defects can degrade bonding strength, especially fracture

    toughness and fatigue strength [46]. Thus, it is necessary to

    develop non-destructive evaluation of diffusion bonding.

    The interfacial imperfections are parallel to the specimen

    surface, which is a suitable position for ultrasonic test [7].

    A variety of ultrasonic methods have been applied in the evalua-tion of bonding quality, such as pulse-echo method, laser ultra-

    sonic system[8], guided waves [911], and nonlinear ultrasonic

    measurement [1214]. Pulse-echo method is the most popular

    technique among these ultrasonic methods. Palmer et al. [15]

    described the application of ultrasonic reflectivity for the char-

    acterization of copper diffusion bonds with different bonding

    qualities. Ultrasonic reflection coefficients at 10 MHz were

    correlated with the ultimate tensile strength. Kato and Abe [16]measured diffusion bondings of steel to titanium plates to obtain

    the relationships among bonding strength, state of bonding

    interface, and two major components derived from ultrasonic

    testing. Considerable progress was made by Greenberg et al. [17]

    in developing a real-time system for the monitoring of bonding

    process by analyzing the amplitude ratio and attenuation of

    acoustic waves. In other efforts, the C-scan images at the bonding

    interface were used to calculate the ratio of non-bonded area of

    diffusion bonded joints of mild steel, combined with impact tests

    for threshold level determination [18]. Similar technique was

    applied to field-assisted diffusion bonding joints to assess the

    mechanical quality by increasing the ultrasonic frequency up to

    20 MHz[19].

    In general, the unbonds in similar diffusion bondings arereadily detectable by normal incidence wave since the ultrasonic

    wave will be reflected at the defects whereas passing through the

    perfectly bonded regions. The bonding quality can be assessed by

    the amplitude of the reflected signals. However, the kissing bonds

    are only a few micrometers in size, which result in weak

    reflection. The bonding joints appear to be flawless under ultra-

    sonic inspection [20]. As for the dissimilar diffusion bondings,

    some ultrasonic energy is still reflected from the perfectly bonded

    interface due to the effect of impedance mismatch between

    materials to be bonded[7]. It is difficult to distinguish the defect

    signals from the interface signals so that the bonding quality

    cannot be assessed by the amplitude of the reflected signals.

    Contents lists available at ScienceDirect

    journal homepage: www.elsevier.com/locate/ndteint

    NDT&E International

    0963-8695/$ - see front matter & 2011 Elsevier Ltd. All rights reserved.

    doi:10.1016/j.ndteint.2011.07.008

    n Corresponding author. Tel./fax: 86045186413115.

    E-mail addresses: [email protected] (Y.L. Luan),[email protected] (T. Sun),

    [email protected] (J.C. Feng),[email protected] (T. Gang).

    NDT&E International 44 (2011) 789796

    http://www.elsevier.com/locate/ndteinthttp://localhost/var/www/apps/conversion/tmp/scratch_2/dx.doi.org/10.1016/j.ndteint.2011.07.008mailto:[email protected]:[email protected]:[email protected]:[email protected]://localhost/var/www/apps/conversion/tmp/scratch_2/dx.doi.org/10.1016/j.ndteint.2011.07.008http://localhost/var/www/apps/conversion/tmp/scratch_2/dx.doi.org/10.1016/j.ndteint.2011.07.008http://localhost/var/www/apps/conversion/tmp/scratch_2/dx.doi.org/10.1016/j.ndteint.2011.07.008http://localhost/var/www/apps/conversion/tmp/scratch_2/dx.doi.org/10.1016/j.ndteint.2011.07.008mailto:[email protected]:[email protected]:[email protected]:[email protected]://localhost/var/www/apps/conversion/tmp/scratch_2/dx.doi.org/10.1016/j.ndteint.2011.07.008http://www.elsevier.com/locate/ndteint
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    In this paper, we focus on the evaluation of TiAl and 40Cr

    diffusion bonding quality. A time-scale characteristics extraction

    algorithm is proposed to measure TiAl and 40Cr diffusion bonding

    interfacial imperfections. The algorithm is based on continuous

    wavelet transform to analyze the amplitude and phase variation

    of ultrasonic interface signals in the time-scale domain. The

    authors shall demonstrate that the defects can be assessed by

    the time-scale amplitude and phase characteristics.

    2. Theoretical background

    Classical boundary condition for ultrasonic wave interaction

    with welded or perfectly bonded interface assumes that stress

    and displacement across the interface is continuous. When an

    ultrasonic wave is normally incident to such an interface, the

    reflection coefficient R12 is given by[21]

    R12 Z2Z1Z2 Z1

    1

    whereZ1and Z2 are the acoustic impedances of the materials on

    either side of the interface. Note that the reflection coefficient

    from the perfectly bonded interface is just a function of the

    impedances.

    If the bonding is imperfect and the size of imperfections is

    considerably smaller than the wavelength of ultrasound, the inter-

    face can be modeled by a set of distributed springs. The ultrasonic

    wave interaction with such an interface can be described using

    spring boundary condition. The reflection coefficient of normal

    incidence ultrasonic wave from imperfect interface is given by[22]

    R12 Z2Z1 io=knZ1Z2Z2 Z1io=knZ1Z2

    2

    whereo is the angular frequency of the ultrasonic wave and kn isthe normal interfacial stiffness, which is defined as distributed

    spring contacts per unit area. The normal interfacial stiffness varies

    from infinity when perfectly bonded is achieved, to zero for an

    unbond surface. The normal interfacial stiffness must be much lessthan infinity when kissing bond occurs at the interface.

    The reflection coefficient of the imperfect interface is related to

    three factors: the acoustic impedances of the materials on either

    side of the interface, the ultrasonic frequency, and the normal

    interfacial stiffness. The amplitude and phase of the reflection

    coefficient of TiAl and 40Cr diffusion bonding interface as shown

    in Fig. 1 are calculated to illustrate the relationship among the

    reflection coefficient and the three factors. The acoustic impe-

    dances of TiAl and 40Cr are 2.73 107 and 4.68 107 Pa s m1,

    respectively. As the phase is a periodic function with period p,

    the result is only shown between p/2 and p/2. As kn-N,corresponding to the case of perfectly bonded, the amplitude of

    the reflection coefficient9R9-(Z2Z1)/(Z2Z1) at all frequencies.The phase of the reflection coefficient tends to zero from the

    positive direction, which means the reflected wave and the

    incident wave are in-phase. As kn-0, corresponding to the case

    of unbond, the amplitude of the reflection coefficient9R9-1 andalso no frequency dependence is observed. There is an exception

    to the rule.9R9 tends to (Z2Z1)/(Z2Z1) when fis close to zero.The frequency used in ultrasonic testing is usually greater than2.5 MHz, even greater than 5 MHz. So this tendency has little

    effect on the practical ultrasonic testing. The phase of the

    reflection coefficient tends to zero from the negative direction,

    which is equivalent to F-p. The reflected wave is opposite inphase to the incident wave. As kn is much less than infinity,

    corresponding to the case of kissing bond, part of the ultrasonic

    energy is reflected from the interface and the amplitude of the

    reflection coefficient increases with the frequency. The phase of

    the reflection coefficient is the same at low frequencies and

    opposite at high frequencies. The phase transition occurs when

    F-7p/2.

    3. Experimental

    3.1. Specimens preparation

    TiAl intermetallic compound and 40Cr steel were used in the

    study. The specimens were a rectangular shape of 45 mm 30 mm,

    and the thicknesses of TiAl and 40Cr were 4.2 and 14.8 mm,

    respectively. TiAl specimens were given chemical cleaning by 5%

    hydrofluoric acid, then rinsed in water and finally dried in hot

    airflow. 40Cr specimens were cleaned using acetone. Six specimens

    were then bonded at various temperatures under a constant

    pressure of 1.33 103 Pa in a vacuum furnace. The welding

    temperatures were 900, 950 and 1000 1C to obtain unbond, kissing

    bond, and perfectly bonded joints, respectively. The welding pres-

    sure was 15 MPa for 15 min. A TiAl plate without diffusion bondingwas prepared as reference specimen.

    3.2. Ultrasonic measurement

    Ultrasonic tests were performed using ULTRAPAC C-scan

    immersion system produced by Physical Acoustic Corporation.

    The system consists of an immersion system including a scanning

    frame assemble, motorized axis adjusters, an immersion tank, and

    a computer with ULTRAWIN software to control test and provide

    result display. A broadband focused transducer with central

    Fig. 1. Calculated reflection coefficient of TiAl and40

    Cr diffusion bonding interface: (a) amplitude of reflection coefficient and (b) phase of reflection coefficient.

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    frequency at 10 MHz was used. The ultrasonic wave at normal

    incidence from TiAl side was focused on the TiAl and 40Cr

    diffusion bonding interface. The C-scan images of the specimens

    and the interface A-scan signals were obtained at the same time

    with sampling frequency of 100 MHz. The ultrasonic wave was

    also focused on the bottom of the reference TiAl plate and the

    reference signal was collected from the TiAlair interface, which

    had 99.99% amplitude and opposite phase of the incident wave.

    Phase inversion was performed on the reference signal.

    3.3. Shear test

    The central part of each diffusion bonding specimen was cut to

    obtain 20 shear test specimens with the dimensions of 4 mm

    9 mm 19 mm. A plan view of the shear test specimens cutting

    method are illustrated inFig. 2.The area with section lines was not

    used for shear test to eliminate the edge effect caused by focused

    transducer in the ultrasonic measurement. The numbers were the

    serial number of shear test specimens. The shear test specimens were

    subjected to shear tests at TiAl and 40Cr diffusion bonding interface in

    a universal testing machine, providing information on the shear

    strength of 20 areas of the diffusion bonding specimen. The shear

    strength tbwas obtained by

    tb FbA0

    3

    whereFbis the loading of final failure and A0is the area of shear test

    specimen.

    3.4. Metallographic analysis

    The cross-sections of TiAl and 40Cr bonding joints were

    polished for metallographic analysis. TiAl specimens were lightly

    etched with 2% nitric acid. Micrographs of the diffusion bonding

    interfaces were obtained by an optical microscope.

    4. Time-scale characteristics extraction algorithm

    As we know from Section 2, the ultrasonic amplitude and

    phase after interacting with the interface are affected by the

    bonding quality of the interface. Therefore, the interfacial imper-

    fections can be evaluated by the ultrasonic amplitude and phase

    characteristics. The time-scale characteristics extraction algo-

    rithm is proposed to assess the bonding quality. The algorithm

    procedures are as follows:

    (1) The continuous wavelet transforms are performed on both

    the interface signals and the reference signal according to the

    following equation:

    Wfa,b

    Z 11

    ftca,btdt 1ffiffiffiffiffiffiffi

    9a9q

    Z 11

    ftc tb

    a

    dt

    tA0,n 4

    whereWf(a,b) is the continuous wavelet transform of function

    f(t), f(t) is the interface signal or the reference signal, tis the

    time variable, (0,n] is the sampling interval off(t),c(t) is the

    basic wavelet, andaandbare referred to as the scale and timeparameter, respectively. The complex morlet wavelet is

    employed in the continuous wavelet transform for its simi-

    larity to the ultrasonic signal and linear phase. The complex

    morlet wavelet is defined as

    ct 1ffiffiffiffiffiffiffipfb

    p et2=fb e2ipfct 5wherefb and fcare the bandwidth parameter and the central

    frequency of the basic wavelet, respectively.

    It is necessary to optimize the time-scale resolution and

    determine the scale parameter a and the step of the scale s

    prior to the continuous wavelet transform. The time-scale

    resolution is related to 1=2pfc ffiffiffiffifbp , and therefore, fcis set as1 Hz to adjust fb. The optimal time-scale is obtained when fbequals 0.8. The scale parameter a of the continuous wavelet

    transform is determined by the following equation:

    a fcfs

    fa6

    wherefsis the sampling frequency of the ultrasonic measure-

    ment and fa is the central frequency of the wavelet corre-

    sponding to scale a. As can be seen, the scale is related to fawhenfcand fs are known, which is determined by the useful

    bandwidth of the transducer. The useful bandwidth of the

    transducer is ranging from 6 to 15 MHz. The scale parameter

    is 16.76.7 according to Eq. (6). The scale parameter is

    rounded to integers as 176 and the correspondence band-

    width is ranging from 5.8 to 16.7 MHz. The step of the scale s

    is set as 0.2 considering the computation efficiency.

    (2) The time-scale ratio of the interface signal and the reference

    signal R(a,b) is obtained by

    Ra,b Wfa,binterfaceWfa,breference

    7

    where the subscript interfaceand reference correspond to the

    interface signal and the reference signal, respectively.

    (3) The time-scale amplitude 9R(a,b)9 and the time-scale phaseF(a,b) are obtained by

    Ra,b

    ffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiffiR2Ra,b R

    2I a,b

    q 8

    Fa,b +Ra,b arctan

    RIa,b

    RRa,b 9

    where the subscript R and I correspond to the real and the

    imaginary part of R(a,b), respectively. Concerned only with

    the same or opposite of the time-scale phase, 1 is

    employed to represent the same phase, and 1 is employed

    to represent the opposite phase.

    (4) The time-scale amplitude9R(a,bj)9of every time parameter bjis linear fitted along the scale parameter a decreasing direc-

    tion to obtain the fitting curve yj according to the following

    equation:

    yj Aj9Ra,bj9 Kj, j l, l 1=fs,. . .,m 10

    where Aj and Kj are the fitting slope and the fitting constant

    of the fitting curve yj, respectively, and l and m are the

    scope of the time parameter b, respectively. The amplitude

    1 2 3 4

    5 6 7 8

    9 10 11 12

    13 14 15 16

    17 18 19 20

    45

    30

    4

    9

    Fig. 2. Plan view of the shear test specimens.

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    characteristicCR is obtained by

    CR Xmj l

    Aj 11

    (5) The phase characteristic CF is calculated by

    CF s

    vu s

    1

    mfslf

    s1 X

    v

    i uX

    m

    j l

    Fai,bj

    i u,u s,. . .,v, j l, l 1=fs,. . .,m 12

    where u and v represent the scope of the scale parameter a,

    F(ai,bj) is the time-scale phase of every scale parameter ai and

    every time parameter bj. The reason of amplitude and phase

    characteristics extraction will be explained in results and discus-

    sion section.

    5. Results and discussion

    Fig. 3 shows the reflected signals of the perfectly bonded

    interface, the kissing bond, and the unbond and the correspond-ing shear strengths of the joints are 246.1, 44.7, and 6.7 MPa,

    respectively. As can be seen, there are reflected signals not only

    from the kissing bond and the unbond but also from the perfectly

    bonded interface due to the effect of impedances mismatch (the

    reflectivity of the TiAl and 40Cr diffusion bonding interface is

    26.3%). Moreover, there is no apparent difference between signals

    from the perfectly bonded interface and from the kissing bond. It

    is difficult to detect the kissing bond by the signals and the

    bonding quality cannot be accessed by the amplitude of the

    reflected signals.

    Differences are illustrated clearly after the signals are pro-

    cessed by the algorithm described in Section 4. Fig. 4 shows

    the time-scale amplitude of the signals shown in Fig. 3. The

    signal-to-noise ratio of time-scale amplitude is low when time is

    less than 0.1 ms and greater than 0.4 ms, so that the signal analysis

    was performed at the interval of [0.1ms, 0.4 ms]. Four time

    parameters were extracted and the curves of the amplitude

    changing with the scale were illustrated on the right side of

    the time-scale amplitude. The extracted time parameters were

    0.1, 0.2, 0.3, and 0.4 ms. As can be seen from Fig. 4(a), the

    amplitude was low and remained roughly constant from 0.1 to0.4 ms at every time parameter for the perfectly bonded interface.

    This phenomenon was confirmed by the extracted time para-

    meters for the curves of the amplitude changing with the scale

    were almost straight lines. As the scale is related to the frequency,

    the amplitude does not vary with the frequency. For the kissing

    bond as shown inFig. 4(b), the amplitude increased with the scale

    decreasing at every time parameter. According to (6), the scale is

    in inverse proportion to the central frequency of the wavelet, that

    is to say, the amplitude increases with the frequency. The

    amplitude was high and did not vary with the scale for the

    unbond as shown in Fig. 4(c). The reason of the scale-dependent

    amplitude may be explained as follows. The length of the kissing

    bond is much smaller than the wavelength of the ultrasonic wave.

    The ultrasonic wave of low scale (high frequency) is much more

    sensitive to the interfacial imperfection than that of high scale

    (low frequency). The lower the scale (the higher the frequency is),

    the higher the amplitude after interacting with the defect. Thus,

    the scale-dependent amplitude is observed for the kissing bond.

    Though the kissing bond cannot be detected by the amplitude of

    the reflected signals, one can reliably identify the defect using the

    scale-dependent amplitude.

    As for the kissing bond, the time-scale amplitude 9R(a,bj)9 ofevery time parameter bj increased with the decrease in scale ,

    whereas that of the unbond and the perfectly bonded interface

    did not vary with the scale. Therefore, the fitting slope Aj of the

    fitting curveyjalong the scale decreasing direction was chosen to

    0.0-1.0

    -0.5

    0.0

    0.5

    1.0

    Normalizedamplitude

    Time (s)

    0.0-1.0

    -0.5

    0.0

    0.5

    1.0

    Normalizedamplitude

    Time (s)

    0.1 0.2 0.3 0.4 0.5 0.1 0.2 0.3 0.4 0.5

    -1.0

    -0.5

    0.0

    0.5

    1.0

    Normalized

    amplitude

    Time (s)

    0.0 0.1 0.2 0.3 0.4 0.5

    Fig. 3. Ultrasonic signals reflected from TiAl and40

    Cr diffusion bonding interface: (a) perfectly bonded interface, (b) kissing bond, and (c) unbond.

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    represent the scale-dependent feature of 9R(a,bj)9. The fittingslopes Aj were then summed as the amplitude characteristic CR.

    The calculated amplitude characteristics were 6.30, 0.02, and

    0.01 for the kissing bond, the unbond, and the perfectly

    bonded interface, respectively. The kissing bond was distin-

    guished from the unbond and the perfectly bonded interface by

    the extracted amplitude characteristics.

    A special phenomenon for the unbond was observed in the

    experiment as shown in Fig. 5. The time-scale amplitude of theunbond decreased with the scale at every time parameter when

    the ultrasonic signal was too high to overflow the oscilloscope. This

    was because the signal was distorted by the saturated sampling.

    However, this phenomenon has no effect to distinguish the unbond

    from the kissing bond and the perfectly bonded interface.

    Fig. 6shows the time-scale phase of the signals reflected from

    the perfectly bonded interface, the kissing bond, and the unbond.

    As can be seen fromFig. 6, the phase was almost the same for the

    perfectly bonded interface at the interval of [0.1 ms, 0.4 ms]; the

    time-scale phase presented the same at high scale whereas

    opposite at low scale for the kissing bond; the time-scale phase

    was opposite for the unbond. The opposite phase can be

    explained by considering the difference in the acoustic impe-

    dances on either side of the interface. The phase is the same after

    the ultrasonic wave interacting with the interface in the case of

    the acoustic impedance of the top material is less than that of the

    bottom material, whereas the phase is opposite in the case of the

    acoustic impedance of the top material is greater than that of

    the bottom material. The acoustic impedance of the interface

    layer is much less than that of the upper materials for the kissing

    bond and the unbond, so that the opposite phase occurs. Although

    the bonding quality is difficult to be evaluated by the amplitude

    of the reflected signal, the kissing bond can be detected by thephase variation, and the unbond could be measured by the

    opposite phase. The time-scale phase becomes another useful

    tool to assess the kissing bond and the unbond.

    The extraordinary feature of the time-scale phase of different

    bonding quality was the same and opposite differences. The mean

    value of the time-scale phase was able to represent the phase

    differences. This is the reason for selecting the mean value as the

    phase characteristic. The phase characteristic CR of the kissing

    bond predicted to be between 1 and 1 for the time-scale

    phaseF(ai,bj) presented the same at high scale whereas opposite

    at low scale. The time-scale phase F(ai,bj) for the unbond and the

    perfectly bonded interface were opposite and the same, so that

    the predicted phase characteristics CR should be 1 and 1.

    The calculation result showed that phase characteristics were

    Time (s)

    Scale

    0 0.1 0.2 0.3 0.4 0.5

    17

    15

    13

    11

    9

    7

    0

    0.5

    1

    170.0

    0.2

    0.4

    0.6

    0.8

    1.0

    Amplitude

    Scale

    t=0.1s

    t=0.2s

    t=0.3s

    t=0.4s

    Time (s)

    Scale

    0 0.1 0.2 0.3 0.4 0.5

    17

    15

    13

    11

    9

    70

    0.5

    1

    0.0

    0.2

    0.4

    0.6

    0.8

    1.0

    Amplitude

    Scale

    Time (s)

    Scale

    0 0.1 0.2 0.3 0.4 0.5

    17

    15

    13

    11

    9

    7

    0

    0.5

    1

    0.0

    0.2

    0.4

    0.6

    0.8

    1.0

    Amplitude

    Scale

    16 15 14 13 12 11 10 9 8 7 6

    17 16 15 14 13 12 11 10 9 8 7 6

    17 16 15 14 13 12 11 10 9 8 7 6

    t=0.1s

    t=0.2s

    t=0.3s

    t=0.4s

    t=0.1s

    t=0.2s

    t=0.3s

    t=0.4s

    Fig. 4. Time-scale amplitude of signals from TiAl and 40Cr diffusion bonding interface: (a) perfectly bonded interface, (b) kissing bond, and (c) unbond.

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    0.68, 0.99, and 0.97 for the kissing bond, the unbond, and

    the perfectly bonded interface, respectively. The extracted phase

    characteristics distinguished the kissing bond and the unbonded

    from the perfect bonded interface.

    The characteristics extraction was performed on the diffusion

    bonding specimens. The amplitude and phase characteristics

    images were reconstructed according to the position of the ultra-

    sonic C-scan images using color indicating their values. Results of

    one specimen are shown in Fig. 7. Fig. 7(a)(d) are the ultrasonicC-scan image, the shear strength of 20 areas of the specimen, the

    amplitude characteristics image, and the phase characteristics

    image, respectively. The lines on Fig. 7(b) were manually added

    according to the dimension of the shear test specimens. The

    elliptical regions A, B, and C were discussed. The amplitude of the

    C-scan image is approximately 40% in region A, which is close to

    region C. However, the shear strength of region C is 173.1 MPa,

    whereas that of region A is averagely 19.5 MPa. There must be some

    imperfections on the interface and their characteristics match those

    of the kissing bonds. However, it is too difficult to identify the

    kissing bonds by the ultrasonic C-scan image. Differences are

    illustrated clearly in the amplitude and phase characteristics

    images. The amplitude characteristics approach to 5 and the phase

    characteristics are approximately 0.7 in region A. The amplitude

    and phase characteristics of region C are approximately 0.02 and

    0.98. The amplitude of the ultrasonic C-scan image in region B is

    too high to overflow the oscilloscope and the shear strength is zero.

    These defects belong to the unbond. The amplitude characteristics

    are less than zero due to signal saturation sampling and the phase

    characteristics are approximately 1.

    The microstructures of the regions A and B are shown in Fig. 8.

    Small areas with the length of a few micrometers in which

    diffusion process is inhibited can be seen at the kissing bondinterface; and a narrow long gap with the width of approximately

    89 mm is located at the unbond interface. The amplitude and

    phase characteristics images are effective to assess the kissing

    bonds and the unbonds in the TiAl and 40Cr diffusion bonding

    specimens. Analogous signal analyses were performed on five

    other specimens, and the same results were obtained.

    6. Conclusions

    Ultrasonic interface signals of the TiAl and 40Cr diffusion

    bondings are transformed in the time-scale domain to analyze

    the time-scale amplitude and phase and extract characteristics for

    the bonding quality assessment. The algorithm proposed by the

    0.0-1.0

    -0.5

    0.0

    0.5

    1.0

    No

    rmalized

    amplitude

    Time (s) Time (s)

    Scale

    0 0.1 0.2 0.3 0.4 0.5

    17

    15

    13

    11

    9

    7

    0

    0.5

    1

    0.1 0.2 0.3 0.4 0.5

    Fig. 5. Saturated sampling signal from unbond interface and corresponding time-scale amplitude: (a) saturated sampling signal and (b) time-scale amplitude.

    Time (s)

    Scale

    0 0.1 0.2 0.3 0.4 0.5

    17

    15

    13

    11

    9

    7-1

    -0.5

    0

    0.5

    1

    Time (s)

    Scale

    0 0.1 0.2 0.3 0.4 0.5

    17

    15

    13

    11

    9

    7-1

    -0.5

    0

    0.5

    1

    Time (s)

    Scale

    0 0.1 0.2 0.3 0.4 0.5

    17

    15

    13

    11

    9

    7

    -1

    -0.5

    0

    0.5

    1

    Fig. 6. Time-scale phase of signals from TiAl and 40Cr diffusion bonding interface: (a) perfectly bonded interface, (b) kissing bond, and (c) unbond.

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    paper differs from conventional ultrasonic evaluation for it

    utilizes the scale-dependent amplitude instead of the amplitude

    of the reflected signal. Another difference of the algorithm is the

    application of the phase information. From the above study we

    arrive at the conclusion that the kissing bond can be detected by

    the scale-dependent amplitude combined with phase variation

    and the unbond can be measured by the opposite phase. The

    kissing bonds and the unbonds exist not only in diffusion

    bondings but also in other solid-state welding methods, such as

    high-frequency induction brazing and friction welding. The algo-

    rithm shall be applied in other solid-state welding methods toanalyze its universaliability in our further study.

    Acknowledgment

    The authors are grateful to all the members of non-destructive

    testing research team of the State Key Lab of Advanced Welding

    Production Technology in the Harbin Institute of Technology for

    their help.

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    -5

    0

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    [%]

    100

    50

    0

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