Ultrasonic Application 1

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    APPLICATION 1:APPLICATION 1:

    ULTRASONIC TUBE CLEANINGULTRASONIC TUBE CLEANING

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    CONTENTS OF PRESENTATIONCONTENTS OF PRESENTATION

    1.0 Theory of Ultrasonic Cleaning

    2.0 Ultrasonic Cleaning (Scale Removal)

    3.0 Applications in The Plant Operations

    4.0 Dynamics Ultrasonic Cleaning System

    5.0 Heat Echanger!Re"oiler T#"e Cleaning

    6.0 $#estion an% Ans&er

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    What is U!t"as#$i%s&

    Ultrasonics is the science of sound waves above the limits of humanaudibility. Ultrasound is a sound with a pitch so high that it can not be

    heard by the human ear.

    + Frequencies above 18 Kilohert ! Ultrasonic. "anging from

    #$%$$$ cycles per second or &ilohert 'K() to over

    1$$%$$$ K(.

    + *ommonly used frequencies between #$ K( and $K(.

    ,

    T'EOR( OF ULTRASONIC CLEANING

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    Principles

    + -f increased sound amplitude is applied to nonelastic media such

    as water or other liquids%the liquid tends to fracture because of

    the negative pressure% causing a phenomenon &nown as

    cavitation.

    + s the wave fronts pass% the cavitation /bubbles/ oscillate and

    grow to an unstable sie. Finally% the violent collapse of the

    cavitation /bubbles/ results in implosions% which cause shoc&

    waves to be radiated from the sites of the collapse

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    ULTRASONIC CLEANING

    (Scale Removal)

    PRODUCT CODE : SBB UC 500

    REPRESENTATIVE

    SAMPLING

    LABORATORY

    ANALYSIS

    CHEMICAL

    SELECTION

    DEVELOP

    PROCEDURES

    CAVITATION Loosing out t! s"#$! %on&ing

    CHEMICAL ' Boost u( u$t)#soni" i))#&i#tion #n&

    BOOSTING su%st)#t! "$!#ning*

    SCRUBING B)!#+ing out t! $oosing s"#$!ULTRASONIC

    PRINCIPLES

    +SCALING

    ,IELD

    APPLICATION

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    Ultrasonics Spee%s Cleaning "y Dissol#tion

    + *avitation and implosion as a result of ultrasonic activity displace

    and remove loosely held contaminants such as dust from surfaces.

    For this to be effective% it is necessary that the coupling medium be

    capable of wetting the particles to be removed.

    + 0ome contaminants are comprised of insoluble particles loosely

    attached and held in place by ionic or cohesive forces. he effect of

    ultrasonics is substantially the same in these cases.

    + he mechanical micro!agitation helps speed the dissolution ofsoluble contaminants and brea& the attractive forces of insoluble

    particles

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    'a) 2irty 0urface

    Fi)*"+ 2 ,+!#- i!!*st"at+s th+ s*"a%+ # th+ /a"t ,+i$)

    %!+a$+ has ,++$ "+/"+s+$t+ as a !at.

    'b) *leaning 3rocess

    'c) 4echanical *leaning

    i.e brushing

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    are needed to see this picture.Maximizing the Ulta!onic Cleaning "oce!!Maximizing the Ulta!onic Cleaning "oce!!

    P"#%+ss Pa"a+t+"s

    aiii$) Caitati#$

    *hemical

    ime

    emperature cavitation intensity

    emperature

    viscosity of a liquid

    dissolved gas

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    Maximizing the Ulta!onic Cleaning "oce!!

    I/#"ta$%+ # i$iii$)

    iss#!+ Gas

    2uring compression portion of the sound

    wave% any gas which diffused into the

    bubble is compressed and diffuse across

    the boundary again to re!enter the liquid

    s a result% cavitation bubbles formed in

    liquids containing gas do not collapse all

    the way to implosion

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    Overall Cleaning Effect

    (ighly wettedformulations

    compatible with

    the base metal

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    So$utions Us!& -it U$t)#soni" C$!#ning O. V#)ious P#)ts /1

    M#t!)i#$ o. "onst)u"tion T2(!s o. (#)ts Cont#3in#nts Suit#%$! "$!#ning #g!nt

    I)on4 St!!$4 St#in$!ss st!!$ C#stings4 st#3(ing4

    3#"in!& (#)ts4 &)#n

    i)!4 &i!s!$ .u!$ in6!"to)s

    Ci(s4 $u%)i"#nts4 $igt

    o7i&!s

    Hig "#usti" it

    "!$#ting #g!nts

    I)on4 St!!$4 St#in$!ss st!!$ Oi$'8u!n"!&4 us!&

    #uto3oti9! (#)ts .in!

    3!s #n& sint!)!& .i$t!)s

    C#)%oni;!& oi$ g)!#s!4

    "#)%on s3ut4 !#92 g)i3!

    &!(osits

    Hig "#usti"4 si$i"#t!&

    I)on4 St!!$4 St#in$!ss st!!$ B!#)ing )ings4 (u3(

    (#)ts4 +ni.! %$#&!s4 &)i$$t#(s4 9#$9!s

    Ci(s g)in&ing4 $#((ing

    #n& oning "o3(oun&soi$s #7!s #n& #%)#si9!s

    Mo&!)#t!$2 #$+#$in!

    I)on4 St!!$4 St#in$!ss st!!$ Ro$$!) %!#)ings4

    !$!"t)oni" "o3(on!nts

    t#t #)! #..!"t!& %2 #t!)

    o) (os! &)2!) ()o%$!3s4

    +ni.! %$#&!s4 sint!)!&

    .i$t!)s

    Bu..ing #n& (o$ising

    "o3(oun&s

    3is"!$$#n!ous 3#"ining4

    so( #n& ot!) soi$s

    C$o)in#t!&'so$9!nt

    &!g)!#s!) /ini%it!&

    t)i"$o)o!t2$!n!4 .o)

    !7#3($!1

    A$u3inu3 #n& ;in" C#stings4 o(!n'3!s #i)

    .i$t!)s4 us!& #uto3oti9!

    "#)%u)!to) (#)ts4 9#$9!s4

    sit" "o3(on!nts4

    &)#n i)!

    Ci(s4 $u%)i"#nts #n&

    g!n!)#$ g)i3!

    Mo&!)#t!$2 #$+#$in!4

    s(!"i#$$2 ini%it!& to

    ()!9!nt !t"ing o. 3!t#$4

    o) n!ut)#$ s2nt!ti"

    /usu#$$2 in $i8ui& .o)31

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    So$utions Us!& -it U$t)#soni" C$!#ning O. V#)ious P#)ts /

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    So$utions Us!& -it U$t)#soni" C$!#ning O. V#)ious P#)ts /=1

    P$#sti"s L!ns!s4 tu%ing4 ($#t!s4

    sit" "o3(on!nts

    Ci(s4 .ing!)()ints4 $int4

    so( &i)t

    Mo&!)#t!$2 #$+#$in! o)

    n!ut)#$ s2nt!ti"

    V#)ious 3!t#$s4 ($#sti"s

    /n2$on4 T!.$on4 !(o724 !t"*14

    #n& o)g#ni" "o#tings !n

    #t!) so$utions "#nnot %!

    to$!)#t!&

    P)!"ision g!#)s4 %!#)ings4

    sit"!s4 (#int!& ousings4

    ()int!& "i)"uit %o#)&s4

    3ini#tu)! s!)9o3oto)s4

    "o3(ut!) "o3(on!nts

    Lint4 ot!) (#)ti"u$#t!

    3#tt!)4 #n& ot!) $igt oi$s

    T)i"$o)ot)i.$uo)o!t#n!

    /.$uo)o"#)%on so$9!nt14

    soni"'9#(o) &!g)!#s!)

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    Procedure

    The cleaning liquideither aqueous orsolvent is flled in thetank

    The transducer mountedat the bottom o the tankor generation oultrasonic !ave

    The vibrations are

    transerred into theliquid medium throughthe stainless steel tank"cavitations ormation#

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    APPLICATIONS IN T'EAPPLICATIONS IN T'E

    PLANT OPERATIONPLANT OPERATION

    'ii) Filter *leaning

    ! to remove plugging materials in filter pores.

    'i) ube53late *leaning 'reboiler% heat e6changer% condenser

    and column pac&ing)

    ! to remove scale and fouling materials

    +/+$i$) #$ #/+"ati#$ "+7*i"++$t8 *!t"as#$i% t+%h$i7*+

    has -i+ a//!i%ati#$s /a"ti%*!a"!9 t# i/"#+ /"#%+ss

    +i%i+$%98 "+t+$ti#$ ti+ a$ %#st. '#-++" #" %!+a$i$)

    a$ ai$t+$a$%+ /*"/#s+s8 th+ t+%h$i7*+ is +"9 *s+*!#":

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    P"#%+*"+s # U!t"as#$i% C!+a$i$)

    4aterial

    *ompatibility

    0cale

    nalysis3lanning

    *hemical

    0election

    2esign7ayout

    7ayoutpproval

    2evelop3rocedure

    2evelop0

    9undle

    "emoval

    9undle

    -nstallation

    :quipment

    -nstallation

    *hemical

    0oa&ing

    *leaning ;

    4onitoring

    0cale

    nalysis

    9undle

    7ifting

    9undle

    "insing

    1st. 0tage

    #nd 0tage

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    A.A. 9$ai%s U!t"as#$i% C!+a$i$) S9st+UCS;9$ai%s U!t"as#$i% C!+a$i$) S9st+UCS;

    F!#- S+7*+$%+s P

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    System Specification

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    S(STE CONFIGURATIONS(STE CONFIGURATION

    Fi+ ai$ s+%ti#$ # UCS8 %#/"is+s #:

    1; Li7*i %#$tai$+"

    ! U>F accumulation tan&

    ! =? 2iameter @ A? (eight! 4ade of 00

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    2; Pi/+ itti$)s s+%ti#$

    !4aBor piping and overflow piping is fabricated from 1C 00

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    3; U!t"as#$i% Bath S9st+ S+%ti#$

    ! ' *onsist of custom made flanges% drive shaft% pipe soc&ets% rabbitclamps and fle6ible hose.

    2U*0 custom made parts at

    outlet flow loop were install

    together with e6isting U0 bath.

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    4; P*/i$) S+%ti#$' *onsist of one *entrifugal 3ump and 2iaphragm pump that used

    to pump the U>F to the UCSand to recycle overflow of U>F bac& to

    the accumulation tan& respectively.

    *entrifugal 3ump

    2iaphragm 3ump

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    5; I$st"*+$tati#$ S+%ti#$!*onsist of :lectromagnetic Flowmeter% 3ressure 0ensors%

    overflow level sensor and analog pressure gauges.

    3*E

    >utlet 3ressure

    ransducer

    -nlet 3ressure

    ransducer

    -nlet :lectromagnetic

    Flowmeter

    3ressure auge

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    Tube Bundleafter cleaning

    Tube Bundlecleaning skid

    Chemicalholding tank

    Cleaning Bath

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    Tube Bundleduring

    cleaningprocess

    CleaningBath

    Chemical

    TubeBundleafter

    cleaning

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    'OTOR* C+EA* PER,OR'ACE

    During the cleaning operation, parameters such as inlet and outlet pressures of

    the bundle, pump flowrate and air intake for diaphragm were monitored closelyand recorded. There are three level of cleaning can be observed from theflowrate profile.

    (i) Fillup period

    - Accumulation of UOF in the system and

    establishment of flow regime

    (ii) Removal and Cleaning period

    - the period where plugged catalyst is being removed

    either by chemical or shear effect.

    - cleaning will take place 10-20 hours dependingon the nature of bundle and UOF solution.

    (iii) Stabilization and Flux Measurement Period`

    - the cleaning is complete

    - Measurement of average bundle permeability and flux

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    E-A+UATO O, C+EAED .UD+E

    :valuation is divided into three methods.

    'i) 3ermeability and Flu6 4easurement

    ! records inlet flowrate% flu6% and pressure from the cleaning

    ! use 2arcy?s equation to calculate the final permeability.

    ! plot flu6 profile on semilog graph to verify the quality tube bundle.! compare the final flu6 and calculated permeability to original

    values from manufacturer.

    ! updated the latest values in the process flow sheet.

    ,

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    Evaluation of Cleaning Effectiveness

    (i) Permeability and Flux Measurement

    F!*3 P"#.i!+

    $.$1

    $.1

    1

    1$

    $ + 1$ 1+ #$ #+

    (ours

    9undle

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    'ii) 3ore >bservation

    ! his is a microscopic evaluation of cleaning effectiveness.

    ! 0mall specimens from tube samples of each bundle are

    prepared for the analysis.

    ! For each tube sample% small specimens diameter

    appro6imately !A mm are prepared for the 0canning:lectron 4icroscope '0:4) and :lemental 2iffraction @!"ay

    ':2@) nalysis.

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    Figure below show photos of pores structure

    before and after cleaning. he photos wereta&en at $$ times magnification.

    9efore fter

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    Figure below shows configuration of plugging

    ta&e place in the tube.

    $$6 4agnification #$$$6 4agnification

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    Figure below shows the characteristic of

    damaged tube bundle.

    9efore *lean fter *lean

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    'iii) U>F :lemental nalysis

    ! >bBectives of the analysis are

    'i) to determine the content of copper chromite in thesolution during cleaning.

    'ii) to determine the reactivity of solution with filter

    materials

    'iii) to identify the lifetime of U>F solution

    :lemental analysis was conducted on used U>F samples after

    cleaning process of every tube bundle completed.

    Four elements shall be analyed

    'i) copper '*u)%'ii) Jic&el 'Ji)%

    'iii) *hromium '*r)

    'iv) Ferrous 'Fe).

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    Table : Quantitative Analysis Report of UOF Solution

    Sa/!+ I C#//+")>L;

    Ni%?+!)>L;

    Ch"#i*)>L;

    F+""#*s)>L;

    >riginal U>F $.$#'927) $.$#'927) $.1'927) $.1$'927)

    U>F1 9undleLF# 9undleLF= 9undleL#= #A=.#8 $.# $.H1 1=.IA

    U>F 9undleL1I

    #8

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    BENEFITS

    "educes costs of cleaning% manpower% new bundles

    and maintenance.

    :stimated saving "4# millions a year

    0horten period of maintenance from H days to 18 hours.

    "educes of ris& e6posed to to6ic and haardous chemicals.

    he technique used friendly chemical i.e. U>F "emover

    Used U>F "emover has moderate properties that meet

    :0 specification.

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    B. '+at E%ha$)+"> R+,#i!+" T*,+ Et+"$a!>I$t+"$a! C!+a$i$);

    "eboiler ube

    3ortable un

    ransducer

    Ultrasonicsenerator

    7iquid 'water)

    Frequency

    *onverter

    ransducer

    'immersed)

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    Sta,i!i+" R+,#i!+" T*,+ Et+"$a!>I$t+"$a! C!+a$i$);

    = P+t"#$as P+$a/isa$ +!a?a; S$. Bh.'M.*ontinue)

    -nlet :lectromagnetic

    Flowmeter

    4anager

    >perator holding

    3ortable ransducer

    (arness. 'ood 3ractices)

    "uptured bubbles

    'cavitation)

    *leaned

    0ection

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    Sta,i!i+" R+,#i!+" T*,+ Et+"$a!>I$t+"$a! C!+a$i$);

    = P+t"#$as P+$a/isa$ +!a?a; S$. Bh.'M.*ontinue)

    9undle cleaned with

    ultrasonic and U>F

    chemical

    *lose!up view

    7ifting from Nater 9ath. "eady

    for (ydroBet '"inse)

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    Sta,i!i+" R+,#i!+" T*,+ Et+"$a!>I$t+"$a! C!+a$i$);

    = P+t"#$as P+$a/isa$ +!a?a; S$. Bh.'M.*ontinue)

    7oosen 0cale

    4odel Faces

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    BENEFITS

    "educes costs of cleaning% manpower and maintenance.

    :stimated saving =$O of ordinary cleaning cost

    0horten period of maintenance to 8 hours.

    -ncrease heat transfer efficiency up to $O. "educesflowing pressure drop up to =$O.

    "educes of ris& e6posed to to6ic and haardous chemicals.

    he technique used friendly chemical i.e. >6ide5*o&e "emover

    Used U>F "emover has moderate properties that meet

    :0 specification.

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    C. ULTRASONIC APPLICATIONS

    'i) Ultrasonic *avitation '*lamping ype)

    $ % & P E '

    $ % & P E '

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    C. ULTRASONIC APPLICATIONS

    /ii1 U$t)#soni" C#9it#tion /I33!)si%$! T2(!1

    $ % & P E '

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    C. ULTRASONIC APPLICATIONS

    'iii) Ultrasonic *avitation '3lug!in ype)

    $ % & P E '

    $ % & P E '

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