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1 Dr. Thomas W. Scharf Professor Department of Materials Science and Engineering University of North Texas P.O. BOX 305310 Denton, TX 76203-5310 (940) 891-6837 e-mail: [email protected] EDUCATION B.S. Ceramic Science and Engineering, The Pennsylvania State University, University Park, PA, 1994. Thesis title, “The Effects of Oxidation on the Strength Behavior of SiC Fibers” under Dr. Richard E. Tressler. M.S. Metallurgical and Materials Engineering, The University of Alabama, Tuscaloosa, AL, 1997. Thesis title, “Structural, Tribo-Mechanical, and Thermal Characterization of Sputtered Diamond-Like Carbon and Nitrogenated Diamond-Like Carbon Thin Films” under Dr. John A. Barnard. Ph.D. Metallurgical and Materials Engineering, The University of Alabama, Tuscaloosa, AL, 2000. Dissertation title, “Growth, Structure, and Mechanical Wear Strength of Ultra-Thin Ion Beam and Sputter Deposited Hard Coatings” under Dr. John A. Barnard. PROFESSIONAL EXPERIENCE 5/14-present: Professor, Department of Materials Science and Engineering, University of North Texas, Denton, TX. 5/10-5/14: Associate Professor, Department of Materials Science and Engineering, University of North Texas, Denton, TX. 9/05-5/10: Assistant Professor, Department of Materials Science and Engineering, University of North Texas, Denton, TX. •Established a materials tribology laboratory to measure friction, wear and lubrication processes by in situ and ex situ methods. •Constructed a viscous flow atomic layer/chemical vapor deposition reactor to synthesize solid lubricant and wear resistant coatings for moving mechanical assembly applications. •Secured several external federal grants (listed under current funding). •Developed two new courses: Bonding, Structure and Crystallography and Tribology of Materials. 6/06-8/06; 7/07-8/07; 7/09-9/09; 6/11-7/11, 7/12-8/12, 6/13-8/13 & 6/14-8/14: University Summer Faculty, Microsystems Materials, Tribology, & Technology (2006 & 2007), Multiscale Metallurgical Science &

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Page 1: Thomas W. Scharf - Amazon S3 · 2019-04-16 · 1 Dr. Thomas W. Scharf Professor Department of Materials Science and Engineering University of North Texas P.O. BOX 305310 Denton, TX

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Dr. Thomas W. Scharf

Professor

Department of Materials Science and Engineering

University of North Texas

P.O. BOX 305310

Denton, TX 76203-5310

(940) 891-6837

e-mail: [email protected]

EDUCATION B.S. Ceramic Science and Engineering, The Pennsylvania State

University, University Park, PA, 1994. Thesis title, “The Effects of Oxidation on the Strength Behavior of SiC Fibers” under Dr. Richard E. Tressler.

M.S. Metallurgical and Materials Engineering, The University of

Alabama, Tuscaloosa, AL, 1997.

Thesis title, “Structural, Tribo-Mechanical, and Thermal

Characterization of Sputtered Diamond-Like Carbon and

Nitrogenated Diamond-Like Carbon Thin Films” under Dr. John

A. Barnard.

Ph.D. Metallurgical and Materials Engineering, The University of

Alabama, Tuscaloosa, AL, 2000.

Dissertation title, “Growth, Structure, and Mechanical Wear

Strength of Ultra-Thin Ion Beam and Sputter Deposited Hard

Coatings” under Dr. John A. Barnard. PROFESSIONAL EXPERIENCE 5/14-present: Professor, Department of Materials Science and Engineering,

University of North Texas, Denton, TX. 5/10-5/14: Associate Professor, Department of Materials Science and

Engineering, University of North Texas, Denton, TX. 9/05-5/10: Assistant Professor, Department of Materials Science and

Engineering, University of North Texas, Denton, TX. •Established a materials tribology laboratory to measure friction,

wear and lubrication processes by in situ and ex situ methods. •Constructed a viscous flow atomic layer/chemical vapor deposition reactor to synthesize solid lubricant and wear resistant coatings for moving mechanical assembly applications. •Secured several external federal grants (listed under current funding). •Developed two new courses: Bonding, Structure and Crystallography and Tribology of Materials.

6/06-8/06; 7/07-8/07; 7/09-9/09; 6/11-7/11, 7/12-8/12, 6/13-8/13 & 6/14-8/14: University Summer Faculty, Microsystems Materials, Tribology, & Technology (2006 & 2007), Multiscale Metallurgical Science &

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Technology (2009, 2011 & 2012), and Materials Aging and Reliability Departments (2013 & 2014), Sandia National Laboratories, Albuquerque, NM. •Investigated solid lubrication mechanisms in diamond-like carbon, lubricious oxides and MoS2/Sb2O3/Au nanocomposite coatings for applications in moving mechanical assemblies, such as weapon system components, microsystems, and space (satellite) components. •Studied high temperature wear behavior and mechanisms of Tantalum- and Cobalt-based alloys.

6/03-9/05: Limited Term Member of the Technical Staff, Microsystems

Materials, Tribology, and Technology, Sandia National Laboratories, Albuquerque, NM. •Co-developed a new process for the deposition of crystalline tungsten disulphide (WS2) solid lubricant coatings with monolayer precision by atomic layer deposition (ALD) for potential applications in moving mechanical assemblies such as MEMS (SMM and LIGA) and rolling element bearings. •Investigated the coverage, friction, and wear behavior of PECVD diamond-like carbon (DLC) and diamond-like nanocomposite (DLN) coatings for potential applications in low mass mechanisms and LIGA technology. •Characterized the self-mated tribology of ultrananocrystalline diamond (UNCD) thin films for potential applications to MEMS resonators.

6/00-6/03: Postdoctoral Research Associate, Tribology Section, Naval

Research Laboratory, Washington, D.C. •Investigated the friction and wear life under dry sliding of amorphous diamond-like carbon (DLC) coatings using the NRL homebuilt in situ Raman tribometer. •Developed a model for quantifying the thickness of thin coatings and wear scars using Raman spectra in spot and line modes. The calculated thickness compared well with stylus profilometry values and complement it by determining thickness, not physical height. •Investigated lubricated sliding wear of DLC in Krytox lubricant with in situ Raman tribometry. The Raman carbon (DLC coating) and silicon (substrate) signals were monitored during sliding using a line scan attachment. It was determined the coating wears linearly until failure based on increasing Si:C intensity ratios. The in situ Raman line map profiles inside the wear track showed the coating wore unevenly based on mapping Si to C intensities, and there were no detectable transfer films inside the contact, just a hydrodynamic boundary film.

1/95-6/00: Research Assistant/Teaching Assistant, Department of Metallurgical and Materials Engineering, The University of Alabama. •Designed and constructed a dual ion beam assist technique in high vacuum to deposit ultrathin hard coatings and solid lubricant films. •Demonstrated experimentally that discrete amounts of substitutional nitrogen incorporated into dc/rf sputtered and ion beam deposited diamondlike carbon thin films dramatically improve the resistance to wear, resistance to plastic deformation, and lower the friction coefficient.

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•Determined that depth-sensing reciprocating scratch tests on protective overcoats can produce repeatable and accurate wear and friction properties down to 20 Å film thickness. •Performed the first set of experiments to compare different contact loading regimes on the wear and friction properties of ultrathin films using Nanoindenter II nanoscratch option and an IBM home-built microwear scan technique. •Developed a technique to measure ultrathin (<50 Å) film coverage of underlying magnetic media using Angle-Resolved XPS. •Conducted extensive depth-sensing nanoindentation measurements of many mechanical properties of thin films including hardness, elastic modulus, and strain-rate sensitivity. •Experienced in many structural characterization techniques including high and low angle x-ray diffraction, FE-SEM with EDXS, AFM, spectroscopic ellipsometry, XPS/VBXPS/AES, Raman spectroscopy, and Fourier transform IR spectroscopy.

1/99-6/99: Research Scientist/Engineer, IBM, Almaden Research Center, San Jose, CA.

•Conducted extensive wear testing using an unique IBM built system on 10 (first time reported) to 60 Å thick protective overcoats on rigid disks, e.g., ion beam deposited CHx, CHxNy, CNx, sputtered CHx, CNx, BCx, BCxNy, SiNx. •Established a new wear rate ranking methodology for sub 60 Å thick overcoats with 1 Å resolution using Auger electron spectroscopy measurements within the wear track. •Analyzed the effects of biasing, ion energy, nitrogen concentration and depositing seed layers on mechanical wear strength and friction. •Determined experimentally by AFM and HRSEM that the failure mechanisms are different for ultrathin 10 and 20 Å sputtered overcoats. •Ascertained correlations between the adhesion strength and microstructural measurements, namely density (XRR) and sp3 content (NMR), of ultrathin overcoats.

6/97-8/97: Project Engineer, Eastman Kodak Co., San Diego Laboratories.

•Assisted in the design and development of innovative head/flexible media interfaces used primarily in the Advanced Photo System (APS) camera film. •Performed tribological studies of sliding surfaces including compliance, wear, and reliability testing. •Conducted experiments involving the contouring of MR read and inductive write heads.

8/94-1/95: Quality Control Engineer, The Martin Guitar Co. Inc., Nazareth,

PA •Developed a comprehensive set of specifications for guitar strings used for incoming inspection of materials. •Conducted material characterization tests using an Instron mechanical tensile testing machine.

5/94-8/94: Laboratory assistant, Department of Ceramic Science and Engineering, The Pennsylvania State University.

•Assisted graduate students on the characterization of Carborundum SiC fibers to be used in fiber-reinforced ceramic matrix composites.

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AWARDS AND HONORS 2017 Society of Tribologists and Lubrication Engineers (STLE) Al Sonntag

Award for Best Paper in Solid Lubricants

2016 Teacher Scholar Award - University of North Texas

2016 Division Editor for ASM Vol. 18, 2nd edition, “Friction, Lubrication and

Wear Technology”

2015-2018 Elected to Board of Directors Society of Tribologists and Lubrication

Engineers (STLE)

2013-2019 Elected to Board of Directors Wear of Materials, Inc. that organizes

Wear of Materials International Conferences

2013 Peter J. Blau Award for Best Poster Presentation at the 19th International

Conference on Wear of Materials

2012 Gordon Research Conference on Tribology, Waterville, ME, Chairman’s

Fund Award (Speaker)

2011 Distinguished Alumni Award, Department of Metallurgical and Materials

Engineering, The University of Alabama.

2011 Society of Tribologists and Lubrication Engineers (STLE) Al Sonntag

Award for Best Paper in Solid Lubricants.

2010 Gordon Research Conference on Tribology, Waterville, ME, Chairman’s

Fund Award (Session Chair)

2009 UNT Top External Funding Recipient Number 3 (out of 1064 Professors).

2008 Gordon Research Conference on Tribology, Waterville, ME, Chairman’s

Fund Award (Speaker)

2007 New Faculty Grant, ACS-Petroleum Research Fund

2003 invited article, “Role of Third Bodies in Friction and Wear of Protective

Coatings” in the special issue of Journal and Vacuum Science and Technology A

devoted to the 50th anniversary of the American Vacuum Society (AVS).

Best paper awards and scholarship awards with graduate students:

o 2010 Society of Vacuum Coaters (SVC) Helen and Rolf Illsley

Scholarship Fund of the SVC (Hamidreza Mohseni, PhD student);

o 2010 and 2011 Society of Tribologists and Lubrication Engineers (STLE)

65th and 66th Annual Meetings & Exhibitions, No. 1 student poster

presentation for superior scientific and presentation quality (Hamidreza

Mohseni, PhD student).

o 2012 Society of Tribologists and Lubrication Engineers (STLE) 67th

Annual Meeting & Exhibitions, No. 3 student poster presentation for

superior scientific and presentation quality (Kyle Roget, PhD student); co-

advised with Prof. Srinivasan Srivilliputhur.

o 2013 Society of Vacuum Coaters (SVC) Jane and Frank Warchol

Scholarship Fund of the SVC (Victor Ageh, PhD student)

o 2017 Society of Tribologists and Lubrication Engineers (STLE) E. Richard

Booser Scholarship Award (Tyler Torgerson, BSc student)

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o 2017 Society of Tribologists and Lubrication Engineers (STLE) 72nd

Annual Meeting & Exhibitions, No. 3 student poster presentation for

superior scientific and presentation quality (Tyler Torgerson, BSc student);

Alpha Sigma Mu

PUBLICATIONS (current Google scholar h-index=27 and current ISI Web of Science and Scopus h-

index=23)

Journals (peer-reviewed) 1) J.A. Barnard, H. Fujiwara, V.R. Inturi, J.D. Jarratt, T.W. Scharf, and J.L. Weston, “Nanostructured Magnetic Networks,” Applied Physics Letters 69(18), 2758-2760, (1996). 2) T.W. Scharf, H. Deng, and J.A. Barnard, “Mechanical and Fracture Toughness Studies of Amorphous SiC-N Hard Coatings Using Nanoindentation,” Journal of Vacuum Science and Technology A15(3), 963-967, (1997). 3) T.W. Scharf, H. Deng, and J.A. Barnard, “Nanowear/nanomechanical Testing and the Role of Stress in Sputtered CNx Overcoats,” Journal of Applied Physics 81(8), 5393-5395, (1997). 4) H. Deng, T.W. Scharf, and J.A. Barnard, “Adhesion Assessment of Silicon Carbide, Carbon, and Carbon Nitride Ultrathin Overcoats by Nanoscratch Techniques,” Journal of Applied Physics 81(8), 5396-5398, (1997). 5) J.A. Barnard, V.R. Inturi, J.D. Jarratt, T.W. Scharf, and J.L. Weston, “High Coercivity Nanostructured Networks,” Journal of Applied Physics 81(8), 5467-5469, (1997). 6) H. Deng, T.W. Scharf, and J.A. Barnard, “Determining Critical Loads for Ultra-Thin Overcoats Using a Depth Sensing Nanoindentation Multiple Sliding Technique,” IEEE Transactions on Magnetics 33(5), 3151-3153, (1997). 7) T.W. Scharf and J.A. Barnard, “Nanotribology of Ultrathin a:SiC/SiC-N Overcoats Using a Depth Sensing Nanoindentation Multiple Sliding Technique,” Thin Solid Films 308-309(1-2), 340-344, (1997). 8) R.D. Ott, T.W. Scharf, D. Yang, and J.A. Barnard, “Tribological and Mechanical Properties of CN Ultra-Thin Overcoat Films,” IEEE Transactions on Magnetics 34(4), 1735-1737, (1998). 9) T.W. Scharf, R.D. Ott, D. Yang, and J.A. Barnard, “Structural and Tribological Characterization of Protective a:C and a:CNx Overcoats for Next Generation Hard Disks,” Journal of Applied Physics, 85(6), 3142-3154 (1999).

150 current Scientific Citation Index Times Cited 10) T.W. Scharf and J.A. Barnard, “Coverage and Mechanical Wear Assessment of ≤50 Å Thick Dual Ion Beam Deposited and Sputtered Protective Overcoats”, Journal of Information Storage and Processing Systems, 2, 185-192 (2000). Note: In 2002, this journal merged with Microsystem Technologies (Micro- and Nanosystems Information Storage and Processing Systems).

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11) T.W. Wu, V. Deline, T.W. Scharf, B.K. Yen, J.A. Barnard, “Wear of Ultrathin Carbon Overcoat Characterized by Microwear Scan and Auger Electron Spectroscopy,” Journal of Vacuum Science and Technology A, 19(3) 986-992 (2001). 12) T.W. Scharf, T.W. Wu, B.K. Yen, B. Marchon, J.A. Barnard, “Mechanical Strength and Wear Resistance of 5 nm IBD Carbon Overcoats for Magnetic Disks,” IEEE Transactions on Magnetics, 37(4) 1792-1794 (2001). 13) G. Wei, T.W. Scharf, J.N. Zhou, F. Huang, M.L. Weaver, J.A. Barnard, “Nanotribology Studies of Cr, Cr2N and CrN Thin Films Using Constant and Ramped Load Nanoscratch Techniques,” Surface and Coatings Technology 146 357-362 (2001). 14) T.W. Scharf, J. Gong, G. Zangari, J.A. Barnard, “Assessing Defect Density and Wear Resistance of Ultrathin Diamond-like Carbon Films,” Applied Physics A-Materials Science and Processing 74(6) 827-829 (2002). 15) T.W. Scharf and I.L. Singer, “Role of Third Bodies in Friction Behavior of Diamond-like Nanocomposite Coatings Studied by In Situ Tribometry,” Tribology Transactions 45(3) 363-371 (2002). 16) T.W. Scharf and I.L. Singer, “Monitoring Transfer Films and Friction Instabilities with In Situ Raman Tribometry,” Tribology Letters 14(1) 3-8 (2003). 17) T.W. Scharf and I.L. Singer, “Quantification of the Thickness of Carbon Transfer Films Using Raman Tribometry,” Tribology Letters 14(2) 137-145 (2003). 18) T.W. Scharf and I.L. Singer, “Thickness of Diamond-like Carbon Coatings Quantified with Raman Spectra,” Thin Solid Films, 440 138-144 (2003). 19) (Invited 50th anniversary of AVS article) I.L. Singer, S.D. Dvorak, K.J. Wahl and T.W. Scharf, “Role of Third Bodies in Friction and Wear of Protective Coatings,” Journal of Vacuum Science and Technology A, 21(5) S232-S240 (2003). 20) J. Neidhardt, L. Hultman, E. Broitman, T.W. Scharf, and I.L. Singer, “Structural, Mechanical and Tribological Behavior of Fullerene-like and Amorphous Carbon Nitride Coatings Synthesized by DC Reactive Magnetron Sputtering,” Diamond and Related Materials, 13 1882-1888 (2004). 21) T.W. Scharf, S. V. Prasad, T. M. Mayer, R. S. Goeke, and M. T. Dugger, “Atomic Layer Deposition of Tungsten Disulphide Solid Lubricant Coatings,” Journal of Materials Research, 19 3443-3446 (2004).

________________________________________________________________________

Joined UNT, August, 2005 22) T.W. Scharf, S. V. Prasad, M. T. Dugger, P.G. Kotula, R. S. Goeke, and R.K. Grubbs, “Growth, Structure, and Tribological Behavior of Atomic Layer Deposited Tungsten Disulphide Solid Lubricant Coatings with Applications to MEMS,” Acta Materialia, 54, 4731-4743 (2006). 23) T.W. Scharf, J.A. Ohlhausen, D.R. Tallant, and S.V. Prasad, “Mechanisms of Friction in Diamond-like Nanocomposite Coatings,” Journal of Applied Physics, 101, 063521-1 -063521-11, (2007).

This article was selected for the April 9, 2007 issue (Volume 15, Issue 14) of Virtual Journal of Nanoscale Science & Technology covering a focused area of frontier research on nanometer-scale structures.

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24) R.E. Stallcup II, Y. Mo, T.W. Scharf, and J.M. Perez, “Formation of nanometer-size high-density pits on epitaxial diamond (100) films,” Diamond and Related Materials, 16 1727–1731 (2007). 25) D.S. Grierson, A.V. Sumant, A.R. Konicek, M. Abrecht, J. Birrell, O. Auciello, J.A. Carlisle, T.W. Scharf, M.T. Dugger, P.U.P.A. Gilbert, and R.W. Carpick, “Tribochemistry and Material Transfer for the Ultrananocrystalline Diamond-Silicon Nitride Interface by X-PEEM Spectromicroscopy,” Journal of Vacuum Science and Technology B, 25(5) 1700-1705 (2007). 26) S. Samuel, S. Nag, T.W. Scharf, and R. Banerjee, “Wear Resistance of Laser-Deposited Boride Reinforced Ti-Nb-Zr-Ta Alloy Composites for Orthopedic Implants,” Materials Science and Engineering C: Biomimetic Materials, Sensors and Systems, 28, 414-420 (2008). 27) M.C. Romanes, N.A. D’Souza, D. Coutinho, K.J. Balkus, Jr. , and T.W. Scharf, “Surface and Subsurface Characterization of Epoxy-Mesoporous Silica Composites to Clarify Tribological Properties,” Wear, 265, 88-96 (2008). 28) J.Y. Hwang, A. Neira, T.W. Scharf, J. Tiley, and, R. Banerjee, “Laser-deposited Carbon Nanotube Reinforced Nickel Matrix Composites,” Scripta Materialia, 59, 487-490 (2008). 29) T.W. Scharf, M.C. Romanes, K. Mahdak, J.Y. Hwang R. Banerjee, R.D. Evans and G.L. Doll, “Atomic-scale Structure and Composition of Tungsten Carbide Reinforced Diamond-like Carbon Films,” Applied Physics Letters, 93, 151909 (2008).

This article was selected for the October 27, 2008 issue (Volume 18, Issue 17) of Virtual Journal of Nanoscale Science & Technology covering a focused area of frontier research on nanometer-scale structures.

30) T.W. Scharf, D. R. Diercks, B. P. Gorman, S. V. Prasad, and M. T. Dugger, “Atomic Layer Deposition of Tungsten Disulphide Solid Lubricant Nanocomposite Coatings on Rolling Element Bearings,” Tribology Transactions, 52, 284-292 (2009). 31) S. V. Prasad, T.W. Scharf, P. G. Kotula, J. R. Michael, and T. R. Christenson, “Application of Diamond-Like Nanocomposite Coatings on LIGA Microsystem Parts,” Journal of Microelectromechanical Systems, 18, 695-704 (2009). 32) T.W. Scharf, A. Rajendran, R. Banerjee, and F. Sequeda, “Growth, Structure and Friction Behavior of Titanium Doped Tungsten Disulphide (Ti-WS2) Coatings,” Thin Solid Films, 517, 5666-5675 (2009). 33) W. Brostow, W. Chonkaew; K.P. Menard, and T.W. Scharf, “Modification of an Epoxy Resin with a Fluoroepoxy Oligomer for Improved Mechanical and Tribological Properties,” Materials Science and Engineering A, 507, 241-251 (2009). 34) T.W. Scharf, A. Neira, J.Y. Hwang, J. Tiley and R. Banerjee, “Solid Lubrication of Laser Deposited Carbon Nanotube Reinforced Nickel Matrix Nanocomposites, Journal of Applied Physics, 106, 013508-1 - 013508-7 (2009).

This article was selected for the July 20, 2009 issue (Volume 20, Issue 3) of Virtual Journal of Nanoscale Science & Technology covering a focused area of frontier research on nanometer-scale structures.

35) T.W. Scharf and I.L. Singer, “Role of the Transfer Film on the Friction and Wear of Metal Carbide Reinforced Amorphous Carbon Coatings during Run-in," Tribology Letters, 36, 43-53 (2009).

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36) G.L. Doll, B.A. Mensah, H. Mohseni and T.W. Scharf, “Chemical Vapor Deposition and Atomic Layer Deposition of Coatings for Mechanical Applications,” Journal of Thermal Spray Technology, 19,510-516 (2010). 37) T.W. Scharf, P.G. Kotula and S.V. Prasad, “Friction and Wear Mechanisms in MoS2/Sb2O3/Au Nanocomposite Coatings,” Acta Materialia, 58, 4100-4109 (2010). 38) F.L. Kuo, M.-T. Lin, B.A. Mensah, T.W. Scharf and N.D. Shepherd, “A Comparative Study of the Photoluminescence and Conduction Mechanisms of Low Temperature Pulsed Laser Deposited and Atomic Layer Deposited Zinc Oxide Thin Films,” Physica Status Solidi A, 207, 2487–2491 (2010). 39) H. Mohseni and T.W. Scharf, “Tribological Improvement of Carbon/Carbon Composites by Infiltration of ZnO/Al2O3/ZrO2 Solid Lubricant Coatings,” Tribology and Lubrication Technology, 66(8), 20-21 (2010). 40) A.R.P. Singh, J.Y. Hwang, T.W. Scharf, J. Tiley and R. Banerjee, “Bulk Nickel-Carbon Nanotube Nanocomposites by Laser Deposition,” Materials Science and Technology, 26, 1393–1400 (2010). 41) S. Gopagoni, A. R. P. Singh, J. Y. Hwang, N. Bunce, B.A. Mensah, T. W. Scharf, J. Tiley, and R. Banerjee, “Microstructural evolution in laser deposited nickel-titanium-carbon in situ metal matrix composites,” Journal of Alloys and Compounds, 509, 1255–1260 (2011). 42) H. Mohseni and T.W. Scharf, “Atomic Layer Deposition of ZnO/Al2O3/ZrO2 Nanolaminates for Improved Thermal and Wear Resistance in Carbon-Carbon Composites” Journal of Vacuum Science and Technology A, 30(1) 01A149-1 - 01A149-12 (2012).

The X-ray tomography images from this article were selected for the April 2012 Images of the Month on the Micro Photonics, Inc. website: https://www.microphotonics.com/default.aspx?pageid=1495

43) H. Mohseni, B.A. Mensah, N. Gupta, S.G. Srinivasan, and T.W. Scharf, “On Tailoring the Nanocrystalline Structure of ZnO to Achieve Low Friction,” Tribology and Lubrication Technology, 68(1), 17-19 (2012). 44) (Invited article) R.R. Chromik, H.W. Strauss and T.W. Scharf, “Materials Phenomena Revealed by In situ Tribometry,” JOM, 64(1), 35-43 (2012). 45) H. Mohseni, P.C. Collins, and T. W. Scharf, “Nanocrystalline Orientation and Phase Mapping of Textured Coatings Revealed by Precession Electron Diffraction,” Nanomaterials and Energy, 1(6), 318-323 (2012). 46) (Invited review article) T.W. Scharf and S.V. Prasad, “Solid Lubricants: A Review,” Journal of Materials Science 48(2), 511-531 (2013). 47) D.S. Stone, S. Harbin, H. Mohseni, J.-E. Mogonye, T.W. Scharf, C. Muratore, A.A. Voevodin, A. Martini, and S.M. Aouadi, “Lubricious Silver Tantalate Films for Extreme Temperature Applications,” Surface and Coatings Technology 217, 140-146 (2013). 48) A. Sondhi, C. Morandi, R.F. Reidy, and T.W. Scharf, “Theoretical and Experimental Investigations on the Mechanism of Carbothermal Reduction of Zirconia,” Ceramics International 39, 4489–4497 (2013).

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49) H. Gao, D.S. Stone, H. Mohseni, S.M. Aouadi, T.W. Scharf, and A. Martini, “Mechanistic Studies of High Temperature Friction Reduction in Silver Tantalate,” Applied Physics Letters 102, 121603-1 (2013). 50) K. Roget, S.G. Srinivasan, and T.W. Scharf, “Molecular Dynamics Simulations of Frictional Behavior in FCC Copper and HCP Magnesium,” Tribology and Lubrication Technology, 69(7), 16-19 (2013). 51) A. Sondhi, R.F. Reidy, and T.W. Scharf, “Understanding the Mechanism of Zirconia to Zirconium Carbide Conversion for Ultra-high Temperature Ceramic Applications,” American Ceramics Society Bulletin, 92(6), 56 (2013). 52) H. Gao, S.M. Aouadi, T.W. Scharf, and A. Martini, “High-Temperature Tribological Properties of Silver Tantalate,” Tribology and Lubrication Technology, 69(10), 16-19 (2013). 53) V. Ageh, H. Mohseni, and T.W. Scharf, “Lubricious Zinc Titanate Coatings for High Temperature Applications,” Surface and Coatings Technology, 237, 241–247 (2013). 54) T.W. Scharf, R.S. Goeke, P.G. Kotula, and S.V. Prasad, “Synthesis of Au-MoS2 Nanocomposites: Thermal and Friction-Induced Changes to the Structure,” ACS Applied Materials and Interfaces, 5(22), 11762–11767 (2013). 55) V. Shaikh, N. Boubekri, and T.W. Scharf, “Microlubrication Effects during End Milling AISI 1018 Steel,” International Journal of Manufacturing, Materials, and Mechanical Engineering, 3(4), 14-29, (2013). 56) V. Ageh, H. Mohseni, and T.W. Scharf, “Processing-Structure-Tribological Property Interrelationships of Zinc Titanate Thin Films Grown by Atomic Layer Deposition,” Surface and Coatings Technology, 241, 112-117 (2014). 57) D.S. Stone, H. Gao, C. Chantharangsi, C. Paksunchai, M. Bischof, D. Jaeger, A. Martini, T.W. Scharf, S.M. Aouadi, “Load-dependent High Temperature Tribological Properties of Silver Tantalate Coatings,” Surface and Coatings Technology 244, 37-44 (2014). 58) V. Ageh, R.S Rajamure, Y.H. Ho, and T.W. Scharf, “Nanocrystalline Zinc Titanate Coatings for Corrosion Protection,” Nanomaterials and Energy 3(2), 47-52 (2014). 59) T. Borkar, J. Hwang, J.Y. Hwang, T.W. Scharf, J. Tiley, S.H. Hong, R. Banerjee, “Strength versus Ductility in Carbon Nanotube Reinforced Nickel Matrix Nanocomposites,” Journal of Materials Research 29, 761-769 (2014). 60) V. Shaikh, N. Boubekri, and T.W. Scharf, “Analyzing the Effectiveness of Microlubrication using a Vegetable Oil-based Metal Working Fluid during End Milling AISI 1018 Steel," International Journal of Manufacturing Engineering Vol. 2014, 1-13, http://dx.doi.org/10.1155/2014/261349 (2014). 61) T. Borkar, J. Sosa, J.Y. Hwang, T.W. Scharf, J. Tiley, H. Fraser, and R. Banerjee, “Laser Deposited in situ TiC-Reinforced Nickel Matrix Composites: 3D Microstructure and Tribological Properties,” JOM, 66(6), 935-942 (2014). 62) M.T. Dugger, T.W. Scharf, and S.V. Prasad, “Materials in Space: Exploring the Effect of Low Earth Orbit on Thin Film Solid Lubricants,” Advanced Materials and Processes 172(5), 32-35 (2014).

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63) A. Sondhi, O. Okobiah, S. Chattopadhyay, T. Shibata, T.W. Scharf and R. F. Reidy, “X-ray Absorption Spectroscopy (XAS) Studies on the Carbothermal Reduction Reaction Products of 3 mol% Yttria Stabilized Zirconia,” Journal of Applied Crystallography 47, 1512-1519 (2014). 64) W. Sun, V. Ageh, H. Mohseni, T.W Scharf, and J. Du, “Experimental and Computational Studies on Stacking Faults in Zinc Titanate,” Applied Physics Letters, 104(24), 241903-1 – 241903-5 (2014). 65) (Invited review article) S.M. Aouadi, H. Gao, A. Martini, T.W. Scharf, and C. Muratore, “Lubricious Oxide Coatings for Extreme Temperature Applications: A Review,” Surface and Coatings Technology 257, 266-277 (2014). 66) J.-E. Mogonye, K. Hattar, P.G. Kotula, T.W. Scharf, and S.V. Prasad “He Implantation for Improved Tribological Performance in Au Electrical Contacts,” Journal of Materials Science 50, 382-392 (2015). 67) H. Mohseni, P. Nandwana, A. Tsoi, R. Banerjee, and T.W. Scharf, “In Situ Nitrided Titanium Alloys: Microstructural Evolution during Solidification and Wear,” Acta Materialia 83, 61–74 (2015). 68) H. Mohseni, B.A. Mensah, N. Gupta, S.G. Srinivasan, and T.W. Scharf, “Exceptional Friction Mitigation via Subsurface Plastic Shear in Defective Nanocrystalline Ceramics,” Materials Research Letters 3, 23-29 (2015). 69) H. Singh, K.C. Mutyala, H. Mohseni, T.W. Scharf, R.D. Evans, and G.L. Doll, “Tribological Behavior of Ti Containing MoS2 in Sliding and Rolling Contact,” Tribology and Lubrication Technology, 71(1), 22-24 (2015). 70) N. Argibay, J.E. Mogonye, J.R. Michael, R.S. Goeke, P.G. Kotula, T.W. Scharf, M.T. Dugger, and S.V. Prasad, “On the Thermal Stability of Physical Vapor Deposited Oxide-Hardened Nanocrystalline Gold Thin Films,” Journal of Applied Physics, 117, 145302-1 - 145302-13 (2015).

This was the featured article and front cover art in this issue. 71) T.W. Scharf, S.V. Prasad, P.G. Kotula, J.R. Michael, and C.V. Robino, “Elevated Temperature Tribology of Cobalt and Tantalum-based Alloys,” Wear 330-331, 199-208 (2015). 72) V. Ageh, D. Choudhuri, and T.W. Scharf, “High Frequency Reciprocating Sliding Wear Behavior and Mechanisms of Quaternary Metal Oxide Coatings,” Wear 330-331, 390-399 (2015). 73) H. Mohseni and T.W. Scharf, “Role of Atomic Layer Deposited Solid Lubricants in the Sliding Wear Reduction of Carbon–Carbon Composites at Room and Higher Temperatures,” Wear 332-333, 1303-1313 (2015). 74) H. Singh, K.C. Mutyala, H. Mohseni, T.W. Scharf, R.D. Evans, and G.L. Doll, “Tribological Performance and Coating Characteristics of Sputter Deposited Ti-Doped MoS2 in Rolling and Sliding Contact,” Tribology Transactions 58, 767-777 (2015). 75) T. Borkar, H. Mohseni, J. Hwang, T.W. Scharf, J.S. Tiley, S.H. Hong, and R. Banerjee, “Excellent Strength-Ductility Combination in Nickel-Graphite Nanoplatelet (GNP/Ni) Nanocomposites,” Journal of Alloys and Compounds 646, 135-144 (2015).

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76) A. Ayyagari, T.W. Scharf, and S. Mukherjee, “Dry Reciprocating Sliding Wear Behavior and Mechanisms of Bulk Metallic Glass Composites,” Wear 350-351, 56-62 (2016). 77) O.O. Tinubu, S. Das, A. Dutt, J.E. Mogonye, V. Ageh R. Xu, J. Forsdike, R.S. Mishra, and T.W. Scharf, “Friction Stir Processing of A-286 Stainless Steel: Microstructural Evolution during Wear,” Wear 356-357, 94-100 (2016). 78) J.E. Mogonye, A. Srivastava, S. Gopagoni, R. Banerjee, and T.W. Scharf, “Solid/self-lubrication Mechanisms of an Additively Manufactured Ni-Ti-C Metal Matrix Composite,” Tribology Letters, 64, 37 (2016). 79) J.E. Mogonye and T.W. Scharf, Tribological Properties and Mechanisms of Self-mated Ultrafine-Grained Titanium,” Wear 376-377, 931-939 (2017). 80) J.E. Mogonye, N. Argibay, R.S. Goeke, P.G. Kotula, T.W. Scharf, and S.V. Prasad, “Tribology and Sliding Electrical Contact Resistance of E-beam Hard Au: Effects of Annealing,” Wear 376-377, 1662-1672 (2017). 81) V.A. Shaikh, T.W. Scharf, and N. Boubekri, “Microlubrication Machining of 1018 Steel: The Effect of a Biodegradable Lubricant on the Microstructural Integrity, Lubrication Science accepted (2017). 82) B. Gwalani, A. Ayyagari, D. Choudhuri, T.W. Scharf, S. Mukherjee, M. Gibson, and R. Banerjee, “Microstructure and Wear Resistance of an Intermetallic-based Al0.25Ti0.75CoCrFeNi High Entropy Alloy,” Materials Chemistry and Physics accepted (2017). 83) A. Ayyagari, B. Gwalani, T.W. Scharf, R. Banerjee, and S. Mukherjee, “Reciprocating Sliding Wear Behavior of High Entropy Alloys in Dry and Marine Environments,” Materials Chemistry and Physics accepted (2017). Conference Proceedings (peer-reviewed) 1) T.W. Scharf, R.B. Inturi, and J.A. Barnard, “Characterization of the Mechanical and Tribological Properties of Sputtered a:SiC Thin Films,” Materials Research Society Symposium Proceedings 436, 311-316, (1997). 2) R.D. Ott, T.W. Scharf, D. Yang, and J.A. Barnard, “Tribological and Mechanical Properties of CN Ultra-Thin Overcoat Films and Their Influence on the Underlying Magnetic Media,” The Minerals, Metals, and Materials Society Symposium Proceedings, Hard Coatings based on Borides, Carbides, and Nitrides 99-108 (1998). 3) T.W. Scharf, R.D. Ott, D. Yang, and J.A. Barnard, “Observations of Depth-Sensing Reciprocating Scratch Tests of DLC and Nitrogenated-DLC Overcoats on Magnetic Disks,” Materials Research Society Symposium Proceedings , 517, 389-394 (1998). 4) T.-W. Wu, T.W. Scharf, and H. Zhang, “Micro-wear Scan Test on Carbon Overcoats as Thin as 6 nm or Less,” Materials Research Society Symposium Proceedings, 593, 409-414(1999). 5) T.W. Scharf, R.M. Mowery, and I.L. Singer, “In Situ Raman Tribometry of Diamond-like Carbon Coatings and Transfer Films in Dry and Lubricated Contacts,” Symposium on Rolling Element Bearings (ASTM, West Conshohocken, PA, 2002) pp. 7-16.

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6) I.L. Singer, S.D. Dvorak, K.J. Wahl and T.W. Scharf, “Third Body Processes and Friction of Solid Lubricants Studied by In Situ Optical and Raman Tribometry,” Proceedings of the 28th Leeds-Lyon Symposium on Tribology, Edited by D. Dowson, M. Priest, G. Dalmaz, A.A. Lubrecht, Tribology series. 40 (Elsevier Scientific Pub. Co. London UK, 2002) pp.327-336.

________________________________________________________________________

Joined UNT, August, 2005 7) G.L. Doll and T.W. Scharf, “Chemical Vapor Deposition and Atomic Layer Deposition of Coatings for Mechanical Applications,” Proceedings of the International Thermal Spray Conference, Las Vegas, NV, p. 1072-1077 (2009). Technical Reports (peer-reviewed) 1) T.W. Scharf and S. V. Prasad, “Diamond-Like Nanocomposite Coatings for LIGA-Fabricated Nickel Alloy Parts,” Report No. SAND2005-1004, Sandia National Laboratories, Albuquerque, NM, (2005). 2) T.M. Mayer, T.W. Scharf, S. V. Prasad, M. T. Dugger, P.G. Kotula, R.K. Grubbs, and R. S. Goeke, “Atomic Layer Deposition of Highly Conformal Tribological Coatings,” Report No. SAND2005-5742, Sandia National Laboratories, Albuquerque, NM, (2005).

________________________________________________________________________

Joined UNT, August, 2005

3) R.S. Goeke, S. V. Prasad, T.W. Scharf, and P.G. Kotula, “Synthesis of MoS2-Au Nanocomposite Films by Sputter Deposition,” Report No. SAND2012-5081, Sandia National Laboratories, Albuquerque, NM, (2012). Book Chapters (all invited) (peer-reviewed):

________________________________________________________________________

Joined UNT, August, 2005 1) T.W. Scharf and I.L. Singer, “Third Bodies and Tribochemistry of DLC Coatings,” in Tribology of Diamond-like Carbon Films: Fundamentals and Applications, eds. A. Erdemir and C. Donnet, Springer, pp. 201-236 (2007). 2) T.W. Scharf, “Wear of Metals,” in Handbook of Lubrication and Tribology, Volume II: Theory and Design, Second Edition, ed. R.W. Bruce, CRC Press, pp. 35-1 – 35-18 (2012). 3) T.W. Scharf, “Low Friction Coatings,” in Handbook of Lubrication and Tribology, Volume II: Theory and Design, Second Edition, ed. R.W. Bruce, CRC Press, pp. 39-1 – 39-16 (2012). 4) T.W. Scharf, “Transition Metal Dichalcogenide-based (MoS2, WS2) Coatings.” in Friction, Lubrication and Wear Technology, Vol. 18, Second Edition, ed. G.E. Totten, accepted (2017). Patents ___________________________________________________________________ Joined UNT, August, 2005 1) T.W. Scharf, H. Mohseni, and J. Tiley, “Anti-fretting Wear Coating for Substrates,” Patent Number US 9,228,145. Date of Patent January 5, 2016.

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Utility Patent Filed ___________________________________________________________________ Joined UNT, August, 2005 1) S. Gopagoni, T.W. Scharf, R. Banerjee, and J. Tiley, “Solid Lubricating, Hard and Fracture Resistant Composites for Surface Engineering Applications,” Filed 2/18/2013 with U.S. Patent Application number 13/769,787 and U.S.P.T.O. Publication number US 2013/0252859. 2) N. Argibay and T.W. Scharf, “Monolithic MAX Phase Ternary Alloys for Sliding Electrical Contacts,” Filed 5/28/2015 with U.S. Patent Application number 13/769,787 and U.S.P.T.O. Publication number US 2013/0252859.

JOURNAL EDITORIAL BOARDS Tribology Transactions (2016-present) Associate Editor

(http://www.tandfonline.com/loi/utrb20)

Wear (2015-present) (http://www.journals.elsevier.com/wear/editorial-board)

Lubrication Science (2013-present)

(http://onlinelibrary.wiley.com/journal/10.1002/(ISSN)1557-6833)

Lubricants (2012-present) (http://www.mdpi.com/journal/lubricants/editors)

Nanomaterials and Energy (2012-present) Associate Editor

(http://www.icevirtuallibrary.com/page/jnaen/editorialpanel) PRESENTATIONS SUMMARY Since joining UNT in September 2005

23 invited talks (including 2008 and 2012 Gordon Conference on Tribology)

81 contributed talks at national and international conferences ADVISING PhD students and current job Maia Romanes (PhD 2008) Post-doctoral Researcher at UNT Benedict Mensah (PhD 2010) Group Leader, Intel Corporation, Chandler, AZ Hamidreza Mohseni (PhD 2011) Senior Advanced Product Development

Engineer, Robert Bosch LLC Vasim Shaikh (PhD 2013) – co-advised with Nourredine Boubekri

Assistant Professor, Department of Production Engineering, Fr. Conceicao Rodrigues College of Engineering, Mumbai, India

Anchal Sondhi (PhD 2014) – co-advised with Richard Reidy Process Engineer, Intel Corporation, Hillsboro, OR

Victor Ageh (PhD 2014) Post-doctoral Researcher at UNT Jon-Erik Mogonye (PhD 2016) Post-doctoral Researcher at Army Research

Lab, Aberdeen, MD Masters students and current job

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Anjana Rajendran (MS 2007) Business System Analyst with Service Solutions Tooling at American Express, Phoenix, AZ

Rick Moser (MS 2007) Process Engineer, Texas Instruments, Richardson, TX

Wei-Lun Tu (MS 2009) Process Engineer, Hangzhou Perfect-Tech Co., Ltd., China

Jon-Erik Mogonye (MS 2012) Post-doctoral Researcher at Army Research Lab, Aberdeen, MD

Kyle Roget (MS 2013) – co-advised with Srinivasan Srivilliputhur PhD student, University of Texas at Arlington Doug Kinkenon (MS 2013) Engineer, Cree, Inc., Durham, NC Segun Tinubu (MS 2015) Universal American, Houston, TX Jonova Thomas (MS 2016) PhD Graduate Student, Purdue University, IN Nneoma Mojekwu (MS 2015) Dheyaa Fahad Kadhim (MS 2016) Post-doctoral Researchers Maia Romanes (2008-2009) Hamidreza Mohseni (2011-2013)

EXTERNAL COLLOBORATORS Somuri V. Prasad (Sandia National Laboratories, NM), Ronald S. Goeke (Sandia National Laboratories, NM), Irwin Singer (Naval Research Laboratories, Washington, DC), Jamie Tiley (Wright-Patterson Air Force Base, OH), Ashlie Martini (University of California – Merced, CA), Gregory Sawyer (University Florida, FL), Robert Carpick (University of Pennsylvania, PA), Gary Doll (University of Akron, OH), Miladin Radovic (TAMU, College Station, TX), Federico Sequeda (Universidad del Valle, Cali, Colombia), Ryan Evans (Timken Co., Canton, OH).

PROFESSIONAL AFFILIATIONS

Alpha Sigma Mu, The Minerals, Metals, and Materials Society (TMS), American

Vacuum Society (AVS), Society of Tribologists and Lubrication Engineers (STLE).

FUNDING

Total external funding generated at UNT as PI or co-PI during the period

Sept. 2005 – present = $ 2,943,411.

Total external funding generated since tenure May 2010 = $ 1,920,964

PI grants are from National Science Foundation, Air Force Office of

Scientific Research, Air Force Research Laboratory, American Chemical

Society, Army Research Laboratory, and industry.

INSTRUCTIONAL ACTIVITIES SUMMARY

Since joining UNT in September 2005 Taught total of 26 classes/courses (5 core undergraduate course, 8 core

undergraduate lab modules, 2 core undergraduate/graduate courses, 1 core

graduate course, and 4 elective graduate courses) with instructor evaluation scores

of all highly effective averaging. Student comments for all the courses are very

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strong. I developed two of the courses: Bonding, Structure, Crystallography;

Tribology of Materials; and developed core undergraduate ceramics lab module.

Graduated 6 PhD students (4 major advisor and 2 co-advisor), 6 MS students (5

major advisor and 1 co-advisor); currently advising 1 PhD student and 2 MS

students.

Mentored 7 UG students on Senior Projects and 2 UNT SUPER students

An UG student, Jefferson Helstad, performing research in my laboratory was

awarded in June, 2009 the American Society of Engineering Education (ASEE)

Science, Mathematics and Research for Transformation (SMART) scholarship.

SERVICE

Since joining UNT in September 2005 Service activities have been divided into three primary categories, to the Materials

Science and Engineering department, to the University/College of Engineering, and to the

overall Materials Science and Engineering community.

To the Department

Undergraduate advisor for the Bachelor of Science Degree in Materials Science

and Engineering (MSE) from 2007-2012.

Helped develop the MSE departmental undergraduate curriculum for the new BS

program.

Modified guidelines and rules for new Graduate qualifying examinations. Also, I

am in charge of coordination and monitoring of all exams.

MSE Promotion and Tenure Committee Chair (2014-ongoing)

Member of the MSE undergraduate and graduate curriculum committee to revise

the core curriculum.

Member of MSE ABET committee.

Member of MSE strategic planning committee.

Chair of MSE committee revising P&T and Merit Policies.

MSE cohort advisor.

Member of several departmental hiring committees – Chair & Assistant Professor

in electron microscopy and spectroscopy.

Co-developed Undergraduate poster and brochure for recruitment.

Advisor of Ed Walter, part time machinist. Constructed and coordinated work

order request forms.

To the College of Engineering

Member of College of Engineering reappointment committee for Dr. Bryant

Member of the College of Engineering Curriculum Committee from 2007-2012 –

oversaw the introduction of new courses in the Graduate program and creation of

new courses in the Undergraduate program. Currently, member of the College of

Engineering undergraduate curriculum committee.

Member of College of Engineering hiring committee – PACCAR chair in

Mechanical and Energy Engineering.

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Coordinated hands-on materials demonstrations during the College of Engineering

Homecoming week.

To the University

Assistant Director of CART (Center for Advanced Research and Technology), a

University of North Texas center.

Member of the Goldwater Scholarship nominating committee.

Member of Distinguished Teaching Award Committee.

Co-chair of UNT cluster “Multi-scale Surface Engineering for Enhanced

Performance and Extended Lifetimes”

To the Community Outside the University

Elected to Board of Directors for Wear of Materials, Inc. which plans and runs the

Wear of Materials (WOM) conference held every two years since 1977. Current

role is Secretary and will be Conference Chairman in 2019. Also elected as a

member of the WOM steering committee.

Active in the Society of Tribologists and Lubrication Engineers (STLE) –

Member and voted in as President of Solid Lubricant Technical Committee for

2007-2008, nominated Paper Solicitation Chair of Surface Engineering Technical

Committee in 2008-2009, member of awards committee (2009-present), and

current president of Materials Tribology committee

Symposium Chairman for the Tribology and Mechanical Behavior of Coatings

and Engineered Surfaces at the International Conference on Metallurgical

Coatings and Thin Films (ICMCTF) from 2011-present. Session organizer for Materials Tribology at 2010 and 2013 Materials Science and

Technology (MS&T) Conference conferences

Session Chair at numerous international conferences such as International

Conference on Metallurgical Coatings and Thin Films: San Diego, CA (2006-

present); Society of Tribologists and Lubrication Engineers Annual Meeting:

(2005-present), Materials Science and Technology (MS&T) Conference,

Cincinnati, OH (2006, 2010, 2013).

Served on several National Science Foundation (NSF) panel reviews: Materials

Design and Surface Engineering 2007, 2008, 2009, 2010, 2011, 2012; Major

Research Instrumentation (MRI) Program for Primarily Undergraduate Institutions

(PUI) 2008.

Proposal reviewer for: National Science Foundation (NSF), Air Force Office of

Scientific Research (AFOSR), American Chemical Society (ACS), and U.S.

Civilian Research and Development Foundation (CRDF).

Manuscript reviewer for peer-reviewed journals: Acta Materialia, Nature

Materials, Applied Physics Letters, ACS Applied Materials and Interfaces, Journal

of Applied Physics, Journal of Materials Research, Journal of Tribology, Surface

Coatings and Technology, Thin Solid Films, Tribology Transactions, Tribology

Letters, Tribology International, and Wear.

Presented several formal talks at recruiting functions (North Texas Preview night

and Materials Day) to high school students on what Materials Scientists and

Engineers do.

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Coordinated and edited article “Solid Lubricants for Aerospace Applications” for

Society of Tribologists and Lubrication Engineers (STLE) Magazine - Tribology

and Lubrication Technology (TLT) May 2009 issue.