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Thesis Summary Dynamic Tensile Failure of Rocks Subjected to Simulated In Situ Stresses Bangbiao Wu Department of Civil Engineering University of Toronto Submitted to ISRM Rocha Medal Tianjin China, 2017

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Page 1: Thesis Summary Dynamic Tensile Failure of Rocks Subjected ... · Thesis Summary Dynamic Tensile Failure of Rocks Subjected to Simulated In Situ Stresses Bangbiao Wu Department of

Thesis Summary

Dynamic Tensile Failure of Rocks Subjected to Simulated In Situ Stresses

Bangbiao Wu

Department of Civil Engineering University of Toronto

Submitted to ISRM Rocha Medal

Tianjin China, 2017

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Abstract

Tensile failure of rocks is a main problem in underground engineering projects, in which rocks

are subjected to dynamic disturbances while under high in situ stresses. When disturbed by

dynamic loads from blasting, seismicity or rockbursts, the underground structures would be

vulnerable to tensile failure. Depending on the distance from the underground opening, the in-

situ stress states change from hydrostatic in the far-field, to triaxial in the intermediate distance,

and to the pre-tension nearby the opening.

Dynamic mechanical properties of engineering materials have been investigated for many years

and various devices are used to conduct experiments on these materials. One of the most

frequently used techniques is the split Hopkinson pressure bar (SHPB) system. Using the SHPB

technique, dynamic mechanical properties such as compressive strength, tensile strength and

fracture toughness have been studied on engineering materials, mostly under uniaxial loading

conditions. However, underground rocks are subjected to in situ stresses and occasional dynamic

loadings. Thus, the SHPB testing system is further adjusted with confining pressure system for

dynamic response of rocks under pre-stress state.

In the experiment, the Brazilian disc rock specimens made from Canadian Laurentian granite are

first subjected to pre-stresses simulating in-situ stresses underground (including pre-tension,

hydrostatic confinement, and triaxial confinement) and then loaded dynamically using the

modified SHPB system. The dependence of dynamic tensile strength of the rock material on the

static pre-stress and loading rate is established. A theoretical model is adopted to predict the

dynamic tensile strength of the rock material under different pre-stress states; the results

demonstrate the applicability of the model because the error is less than 5% with reasonable

values for of the parameters.

These experimental results and the calibrated theoretical model will be of great importance in the

design and safety of underground rock engineering projects.

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1 Introduction

1.1 Background

Tensile failure is a main mode of rock failure and it is meaningful and necessary to investigate

the dynamic tensile failure of rocks subjected to pre-stress simulating the underground stress

states. Research has been conducted under quasi static situations, however, the tensile tests under

dynamic loadings have just been proposed in recent years (Xia 2009). Ross, Thompson et al.

(1989) first adopted Brazilian disc specimens to get the dynamic tensile properties of concrete in

SHPB system. Cai, Kaiser et al. (2007) then studied the dynamic behavior of the Meuse/Haute-

Marne argillite and obtained the tensile properties under different strain rates. Zhao and Li (2000)

investigated the dynamic tensile properties of granite by using a dynamic loading machine and 3-

point flexural test method. Wang, Jia et al. (2004) and Wang, Li et al. (2009) proposed flattened

Brazilian disc specimens for the determination of dynamic tensile strength of rocks.

Depending on the distance from the underground opening, the in-situ stress states change from

hydrostatic in the far-field, to triaxial in the intermediate distance, and to the pre-tension nearby

the opening. Take deep mining as an example, the bending of the roof and the buckling of the

pillar would induce static tensile stress state. When disturbed by dynamic loads from blasting,

seismicity or rockbursts, the structures would be vulnerable to tensile failure. From microscopic

perspective, pores and microcracks in rock materials are potential sources of tensile failure

because of stress concentration. Even though the far-field load is compressive, the local stresses

around these inhomogeneities may be tensile. Dynamic disturbance would promote the

generation, propagation and nucleation of defects, and lead to the tensile failure of the rock

materials.

In previous research, there are not many results of tensile experiments on pre-stressed rocks, and

if so, all of them are under quasi-static stress states. Some researchers conducted Brazilian disc,

shear and torsion tests on rocks under hydrostatic pressure (Robertson 1955, Jaeger and Hoskins

1966) and they found that the strength of rock increases with the hydrostatic pressure. Vasarhelyi

(1997) investigated the influence of confinement on the mode I fracture of Gneiss and they

concluded that the fracture toughness also increases with the confining pressure. Al-Shayea,

Khan et al. (2000) tested straight notched Brazilian disk (SNBD) specimens under diametrical

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compression to study the influence of confinement on fracture toughness of limestone. Chen and

Zhang (2004) studied the influence of confinement on rock fracture toughness using notch-hole

combined Brazilian disc specimens and Funatsu, Seto et al. (2004) did the same tests on notched

semi-circular bend (NSCB) specimens and they found the same increasing trend with confining

pressure.

To sum up, there have been many improvements in rock dynamic testing; however, the research

concerning dynamic response of rock subjected to pre-stress is still deficient, which can be listed

here:

1. The loading method for pre-stress pressure is not reasonable enough to represent the state of

the deep rocks. Deep rock is mainly subjected to hydrostatic pressure, with differential stress

components, which is mainly tension in rock mass near free surface such as mined-out areas.

However, in research regarding to the dynamic failure of rocks, researchers either have ignored

the effects of confinement, or have only considered the lateral confinement or hydrostatic pre-

stress at most.

2. The fact that the main failure mode of rock is tension (Kaiser, Kim et al. 2010) is not taken

into consideration in many studies. Instead, most of the studies are focused on the dynamic

failure in compression, rarely on tensile or fracture. But in deep underground engineering

projects, rock fails mainly in tension except the sliding failure of large joints.

3. Some studies did not investigate and verify the accuracy and reliability of the testing methods.

In most experiments related to dynamic tension and fracture, the strength and the fracture

toughness are obtained directly from the static formulas, regardless of the applicability. This

situation has been greatly improved with the presence of the ISRM suggested method, which

provides the specimen preparation, experimental procedure and detailed data processing method

for dynamic tests. However, it still needs to be modified to take confining pressure into

consideration.

4. Although the dynamic failure of rock under different pre-stress situations has been

investigated, there is no ready-made conclusion about the behavior. And the tests were

conducted under different situations by different researchers using different materials and

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apparatus. Thus, it is necessary to systematically investigate the dynamic behavior of pre-

stressed rock.

1.2 Research Objectives and Approach

The research work presented in this thesis is aimed at understanding dynamic tensile failure of

pre-stressed rocks and trying to predict such failure under specific circumstances, such as the

failure of underground rocks under certain loading rate at certain depth. To study and predict

blasting-induced damage, the research uses its correlation with loading rate. Thus, the Split

Hopkinson Pressure Bar (SHPB) is adopted to conduct dynamic tests on rock materials with

different loading rate, and the SHPB system is modified to provide different pre-stress states for

the rock specimens to simulate the in-situ stress states before being subjected to dynamic

loadings. After achieving the correlation between the tensile strength and the loading conditions,

the statistical crack mechanics is used to predict the tensile failure of rock under different loading

conditions and compare the results with that from the lab tests. The specific objectives of this

research are as follows:

• Investigate the nature of stress waves generated by the SHPB impact.

• Study the mechanisms of wave propagation and rock tensile failure for Brazilian Disc

tests under different pre-stress states.

• Evaluate the performance of a theoretical modelling on reproducing the tensile failure

process under certain loading rates.

• Seek a correlation between the dynamic tensile strength and the loading rate and pre-

stress state.

• Design and establish a fully functional SHPB system for rock dynamic tests with pre-

stress, to simulate pre-stress state of deep rocks.

• Understand the influence of the pre-stress, loading rate on the dynamic tensile properties

of the rock.

• Establish a failure model for the dynamic failure of rocks subjected to pre-stress, and

improve the model by referring to engineering activities.

The technical route is as shown in Figure 1.1; the first step is to set up a multifunctional SHPB

system which can provide pre-stress to the specimens. The bars and the pressure cylinders will

be sealed for the confining pressure system, which would lead to the high frictional resistance.

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This will be fully considered in the design, and we will use soft rubber for the sealing to reduce

the friction. Tests will be conducted on Laurentian granite without pre-stress to standardize the

whole system and to provide reference for the following tests.

Figure 1.1 Technical route of the whole project

The whole system is composed of the SHPB loading system and the pre-stress subsystem. The

loading system contains the striker bar, the incident bar and the transmitted bar, which are all 1.5

inch in diameter as shown in Figure 1.2. Before the test, the specimen would be sandwiched

between the incident bar and the transmitted bar. The two parts for confinement are connected by

two steel rods, to provide the desired pre-stress by adjusting the pressure of the two chambers.

This system can be used for all the desired pre-stress state of the specimens.

Figure 1.2 Schematic of the Brazilian test under hydrostatic confining pressure on SHPB

system

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Figure 1.3 Schematic diagram of the approach and methodology employed in this research

Goal:

Provide guidelines for the

development of a reliable

method to predict blast-induced

tensile failure and design tool

for blasting operations

A. STUDY OF

DYNAMIC FAILURE

OF ROCK MATERIAL

B. EFFECT OF IN SITU

STRESS ON DYNAMIC

TENSILE STREGNTH OF

ROCK MATERAILS

C. THEORETICAL

STUDY- STATISTICAL

MECHANICS

SHPB Test

Pulse Shaper

Technique

Micro-CT scan

SEM

Pre-tension Hydrostatic Confinement

SCRAM

ISO-SCRAM

DCA

Underground

Opening Far Field Rock

Failure

Triaxial Stress State

Penny Shaped Crack

Homogenous and

Isotropic Medium

Random Distribution

Mechanical Properties under In situ stress states

Rate Dependency

Failure Pattern

Different Failure Modes of Different Rocks under Pre-stress Conditions

• Compressive Failure

• Tensile Failure

• Fracture Toughness

Take Temperature into Consideration

• Pre-heat Treated

• In situ Heating

Further Applications of Statistical Mechanics in Predicting

• Measurement of damage

• Predicting strength under confinement with different loading rates

On time observation of rock failure under Micro-CT

• 4D imaging technique

D. FUTURE WORK

Intermediate

Zone Failure

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2 Experimental Techniques

2.1 Specimen Preparation

Figure 2.1 illustrates the procedures for preparing Brazilian disc specimens for dynamic tensile

tests. Rock cores with a nominal diameter of 40 mm are first drilled from a rock block, and then

sliced to obtain disc specimens with an average thickness of 16 mm. All of the disc specimens

are polished afterwards until the surface roughness is less than 0.5% of the specimen thickness.

During the procedure of specimen preparation, different parameters are measured and compared

with the results by Nasseri and Mohanty (2008). Table 2.1 shows the P-wave velocities of the

LG block before drilling. Basically, the P-wave velocity measurement is to decide the bedding

direction of the block and then drill the specimens from the bedding direction, which is the XY

plane direction shown in Table 2.1.

Table 2.1 P-wave velocity of Laurentian granite in this study

Direction Nasseri and Mohanty (2008) Current study

XY plane 4115 ± 14 (m/s) 4172 ± 42 (m/s)

XZ plane 4448 ± 46 (m/s) 4635 ± 72 (m/s)

YZ plane 4513 ± 42 (m/s) 4683 ± 45 (m/s)

Figure 2.1 Procedure for the preparing the Brazilian disc specimen of Laurentian granite

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In order to further investigate the mineral component of the Laurentian granite specimen, a thin

section was made to observe under the scanning electron microscope (SEM). The SEM result is

shown in 错误!未找到引用源。, which indicates different components by different colors. To

sum up, the percentages of Quartz, Feldspar and Biotite are 22.5%, 71.6% and 2.3% respectively,

which is different from that reported by Nasseri, Mohanty et al. (2005) that the percentages are

33%, 60% and 3-5%, respectively. It seems that the ‘gap’ between the two results is large.

However, a possible reason is that the rock specimens are not from the same block although they

are the same type of rock. Another reason is that the thin section is too small compare to a block,

makes it impossible to represent the volume percentage of each mineral of the whole block.

According to Dietrich and Skinner (1979), the component percentages are normally 20-60 % of

Quartz, 35-90 % of alkali feldspar, 10-65 % of plagioclase and 5-20 % of Mafic (Biotite,

Hornbende etc.) So both of the results are reasonable.

Figure 2.2 Mineral and microcracks traced from three orthogonal planes for Laurentian granite

(Nasseri and Mohanty (2008))

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Table 2.2 Mineral composition of Laurentian Granite

Direction

Quartz Feldspar Biotite

Average Grain

Size (mm) % Average Grain

Size (mm) % Average Grain

Size (mm) %

XY plane 0.39 33% 0.37 59% 0.25 5%

XZ plane 0.56 34% 0.51 60% 0.41 3%

YZ plane 0.54 30% 0.40 64% 0.28 3%

2.2 Split Hopkinson Pressure Bar (SHPB)

A general SHPB system consists of three major components: a loading device, bar components

and a data acquisition and recording system, as schematically shown in Figure 2.3. The most

common method of loading is to launch a striker impacting on the incident bar. The striker bar is

launched by a sudden release of the compressed air the gas gun and accelerates in the long gun

barrel until it impacts on the end of the incident bar. This kind of striker launch mechanism

produces a controllable and repeatable impact of the incident bar, the striking speed can be

simply controlled by changing the pressure of the compressed gas of the depth of the striker

inside the gun barrel.

The impact of the striker bar on the free end of the incident bar induces a longitudinal

compressive wave propagating in both directions. The left-propagating wave is fully released at

the free end of the striker bar and forms the trailing edge of the incident compressive pulse i

(Figure 2.3). Thus, the duration of i depends on the length and longitudinal wave velocity in

the striker. Upon reaching the bar-specimen interface, part of the incident wave is reflected as the

reflected wave r and the remainder passes through the specimen to the transmitted bar as the

transmitted wave t . Strain gauges are used to record the stress wave pulse on both incident bar

and transmitted bar.

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Figure 2.3 The x-t diagram of stress waves propagation in SHPB (after Xia, Dai et al. (2011))

The diameter of the bars is governed by the diameter of rock specimen, which should be at least

10 times the average grain size of the rock (Dai, Huang et al. 2010, Zhou, Xia et al. 2012). Based

on the one dimensional stress wave theory, the dynamic forces (Figure 2.3) on the incident end

(P1) and the transmitted end (P2) of the specimen are (Kolsky 1949, Kolsky 1953):

1 ( )i rP AE (2-1)

2 tP AE (2-2)

where E is the Young’s Modulus, A is the cross-sectional area of the bars. For a Brazilian disc

test, when the quasi-static state is achieved in the specimen (P1 = P2), the dynamic tensile

strength is determined by the following equation:

2 f

t

P

BD

(2-3)

where t is the tensile strength of the specimen, fP is the load when the failure occurs, B and

D are the thickness and the diameter of the specimen, respectively.

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2.3 Modified SHPB System for Pre-stress Conditions

The modified SHPB apparatus for tri-axial stress state includes the three bars (a striker bar, an incident

bar, and a transmitted bar) (Zhou, Xia et al. 2012) and a hydraulic system, as shown in Figure 2.4. The

elastic bars are made of the same material as that for the pre-tension test. The hydraulic system is mainly

composed of a cylinder that applies lateral confinement to the rock specimens (Cylinder 1), and a pressure

chamber that provides axial preload (Cylinder 2) to the bars and specimen.

Figure 2.4 Schematics of the modified SHPB system for Tri-axial test

Huang, Xia et al. (2013) employed X-ray Micro CT method and strain control ring in the SHPB

tests to observe microscopic damage accumulation in brittle solids subjected to dynamic

compressive loading. X-ray Micro CT with high resolution was used to examine the 3D

microcrack inside the recovered rock specimen under various strains.

To sum up, this section reviews the microscopic characterization and microstructure of

Laurentian granite, demonstrating that the Laurentian granite can be considered as a homogenous

rock material, and introduces the SHPB apparatus for dynamic experimental studies.

3 Dominant Crack Algorithm (DCA)

In rock engineering problems such as blasting, earthquakes and rockbursts, it is common that

rocks may be subjected to dynamic loads and fail suddenly. It is thus critical to understand the

dynamic response of rocks for ensuring safety and maximizing profit in engineering projects.

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Theoretical modeling has been proposed to investigate the failure process of rock material, under

both static and dynamic loading conditions.

Zuo, Addessio et al. (2006) proposed the dominant crack algorithm (DCA) for the damage of

brittle materials under dynamic loading. The rate-dependent damage evolution in the DCA

model is based on the strain energy release rate associated with the critical crack orientation,

which is defined as the most unstable orientation for cracks that are isotropically distributed in

the material. To illustrate the features of the DCA model, the authors simulated several standard

load paths such as hydrostatic, uniaxial strain, and pure shear on Sic ceramic. The strain rate and

loading history of the uniaxial strain response and the pure shear response are similar to the

hydrostatic simulation. Recently the authors (Zuo, Disilvestro et al. 2010) improved the physics

of the model by incorporating plasticity and a nonlinear equation of state (Deganis and Zuo

2011), and applied it to study damage in concrete.

3.1 Constitutive Relations with Damage

In Dominant Crack Algorithm (DCA), the crack number density function is approximated by an

exponential function, which has been indicated by experiments (Seaman, Curran et al. 1976,

Curran, Seaman et al. 1987, Curran and Seaman 1996, Scholz 2002):

0 ( )n( , , ) exp( / ( , ))

( , )

Nc t c c t

c t

nn n

n (3-1)

where ( , )c tn is the average crack radius, 0 ( )N n is the initial crack number density per solid

angle for crack orientation n . The number of cracks per unit volume

is0 0

ˆ ( , , ) ( )c

N n c t dcd N d

n n , which remains constant over time (i.e., there is no

crack nucleation or coalescence during deformation). It follows from Eq. (3-1) that for a given

orientation n , the number density of cracks with radius larger than c is

0( , , ) ( , , ) ( ) exp( / ( , ))c

N c t n c t dc N c c t

n n n n , which decreases exponentially with the crack

radius.

Substituting ( , )b n and n( , , )c tn into Eq. (3-1) and carrying out the integrations over the crack

radius c gives the total crack strain as

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3

30

30

0

3

0

3

0

( , ) ( , ) ( , , )

( )8(1 )exp( / ( , )) ( , )

3 (2 ) ( , )

( )8(1 )( exp( / ( , )) ( , ) )

3 (2 ) ( , )

16(1 )( ) ( , ) ( , )

(2 )

16(1 )( ) (

e

cc

c

t c n c t dcd

Nc c t c dcd

G c t

Nc c t c dc d

G c t

N c t dG

N cG

b n n

nn b n

n

nn b n

n

n n b n

n

3

0

, )

16(1 )( ) ( , ) ( ) ( ) 2( )

(2 )

t d

N c t dG

n n n n n

n n n n n n n n n n

(3-2)

According to Zuo, Addessio et al. (2006), the total crack strain can be divided into two parts, the

open crack strain and the shear crack strain,

( , ) ( , ) ( , )o s

c c ct t t (3-3)

With the opening crack strain and shear crack strain given by

3

0

16( , ) (1 ) ( ) ( , )o

c t N c t dG

n n n n n n (3-4)

s 3

0

16(1 )( , ) = ( ) ( , ) ( ) ( ) 2( )

(2 )c t N c t d

G

n n n n n n n n n n (3-5)

s ( , )c t is a deviatoric tensor (i.e., str ( , )=0c t ), i.e., the sliding of crack faces does not

contribute to dilatancy. With the assumption of an isotropic distribution of crack, Addessio and

Johnson (1990) found the analytical expression for shear crack strains by carrying out the

integration over all crack orientations,

s 3

0

64 (1 )( , )=

5 (2 )

d

c c N cG

(3-6)

Where d p I and ( ) / 3p tr are the stress deviator and pressure, respectively; I being

the second order identity tensor. It is noted that the explicit dependency of crack strain on time

( )t has been replaced by the dependency on the mean crack size c , which evolves with time.

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Similarly, the crack opening strain is found by carrying out the integration in Eq. (3-6) over all

crack orientations. The result can be written as:

3

0

64 1( , ) (1 ) ( ( ) )

15 2

o

c c N c trG

I (3-7)

In the DCA model, strain of the characteristic volume can be considered to be composed by two

parts, the elastic strain ij

e and the crack strain ij

c , as shown in Figure 3.1.

ij ij

e c

ij ( i , j =1, 2, 3) (3-8)

Figure 3.1 The schematics of the DCA constitutive model

The elastic strain can be divided into the volumetric strain tensor and the deviatoric tensor,

1

2ij

e

ije SG

(3-9)

1

3kk

e

kkK

( k =1, 2, 3) (3-10)

where ijS is the deviatoric stress tensor, G is the Shear modulus, and K is the bulk modulus.

Generally, the damage of the characteristic volume can be expressed as a function of the crack

size

3 3

0 ( )c

D AN ca

(3-11)

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where D is the damage function, A is a constant value, 0N is the crack number density, c is

the crack size, and a is the size of the characteristic volume. According to Eq.(3-11), the

evolution of the damage is

3 2

0 0( 3 )D A N c N c c (3-12)

According to the assumption that the crack number density is constant during the failure process,

0 0N , so the damage evolution can be expresses as

22

0 3

33

c cD AN c c

a (3-13)

Addessio and Johnson (1990) established the relation between the deviatoric strain tensor and the

deviatoric stress tensor

3

ij

c e

ije c S (3-14)

where e is a parameter related to the shear modulus and the crack number density by

0 3

12 eG AN

a (3-15)

From Eqs. (3-14) and (3-15), we can get that

32 ( )c

ij ij

cGe S

a (3-16)

Taking the derivative of the equation with respect to time leads to the relation between the crack

strain and the stress tensor.

2 31[3( ) ( ) ]

2

c

ij ij ij

c c ce S S

G a a a (3-17)

And the relation between the strain of the whole model and the stress tensor can be expresses as

2 31[3( ) ( ) ]

2 2

ije c

ij ij ij ij ij

S c c ce e e S S

G G a a a (3-18)

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where c is the crack velocity, G is the shear modulus, ijS is the deviatoric stress tensor.

3.2 Crack Propagation Criterion

In order to describe the opening and propagation of the microcracks, it is assumed that the

propagation velocity is related to the stress intensity factor (Dienes 1996). The classic theory of

crack instability and growth assumes that the cracks grow at a high speed when the applied stress

exceeds a critical level. According to Freund (1998), when the local stress is really high, the

crack propagation velocity at the crack tip can be close to Rayleigh wave speed of the material,

and the empirical expression for the crack velocity is

2

max[1 ( ) ]ICKc v

K (3-19)

where maxv is the terminal crack speed as the energy release rate increases, which is near the

Rayleigh wave speed of the material Rv (Chen, Xia et al. 2009), and

ICK is the initiation fracture

toughness, K is the local stress intensity factor.

According to Evans (1974), when the crack local stress intensity factor is lower than the critical

value, the crack still propagates with a relatively low speed and the process is quasi-static rather

than dynamic. The crack velocity is expressed as

max

1

( )mKc v

K (3-20)

where m is a factor related to the crack propagation velocity, which is typically between 5 and 10

(Dienes, Zuo et al. 2006). 1K is a constant parameter determined by the continuity condition at

the transition point. Consider the continuity condition of Eqs. (3-19) and (3-20), the crack

velocity and acceleration should be both equal to each other at the transition point (suppose the

corresponding fracture toughness is K ), leading to,

2

1

1 ( ) ( )mICK K

K K

(3-21)

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2

1

3

1 1

12 ( )IC m

K Km

K K K

(3-22)

Solve Eqs. (3-21) and (3-22), the transition fracture toughness and the constant parameter can be

determined,

21ICK K

m (3-23)

1

1

21 (1 )

2m

IC

mK K

m (3-24)

So the crack propagation velocity can be described as

max

1

( )mKc v

K

21ICK K

m (3-25)

2

max[1 ( ) ]ICKc v

K

21ICK K

m (3-26)

The local stress intensity factor K is calculated using the effective stress

effK c (3-27)

where the effective stress can be written as the form of the deviatoric stress according to Von

Mises law

3

2eff ij ijS S (3-28)

The statistical crack mechanics modeling method is introduced and the dominant crack algorithm

(DCA) is adopted to model the dynamic tensile failure of the Laurentian granite in this study.

The constitutive equations in the DCA modeling and the crack propagation criterion are

developed.

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4 Dynamic Tensile Tests with Pre-Tension

4.1 BD Experimental Results under Pre-tension

Five groups of Laurentian granite BD specimens (with static tensile strength of 12.8 MPa) under

the pre-tension of 0 MPa, 2 MPa, 4 MPa, 8 MPa, and 10 MPa are tested under different loading

rates.

Figure 4.1 BD specimens sandwiched between the incident and transmitted bars

Based on the one dimensional stress wave theory, and assuming stress equilibrium during

loading (Zhou, Xia et al. 2012) (i.e.,i r t ), the history of the force on the specimen is:

0( ) ( )dP t P P t (3-1)

where 0P is the static preload on the bars, ( )dP t is the dynamic force history on the bars after the

impact. The tensile stress history at the center of the disc specimen can be determined as:

0 00

( )( ) ( ) t

d

A E tt t

RB

(3-2)

where 0 is the pre-tension at the center of the disc, and

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00

P

RB

(3-3)

Figure 4.2 and Figure 4.3 illustrate the dynamic tensile strength versus loading rate and total

tensile strength versus loading rate, respectively. It is obvious that the dynamic strength increases

with the loading rate, revealing the phenomenon of rate dependency that is common for

engineering materials, such as rock (Zhang and Zhao 2013), concrete (Fujikake, Senga et al.

2006, Cusatis 2011), ceramic (Brar and Rosenberg 1988, Zhang, Liu et al. 2008).

Figure 4.2 The dynamic strength versus loading rate for different pre-tensions

Apart from the rate dependency mentioned above, what can be seen from Figure 4.2 is that the

dynamic tensile strength of the rock decreases with the increase of the pre-tension when

subjected to the same loading rate. The decrease of dynamic tensile strength is caused by the

opening of microcracks when the specimen bears the pre-tension stress. Which is consistent to

the results reported by Xia et al. that the microstructures affect the dynamic stress of rock

specimens (Xia, Nasseri et al. 2008).

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Figure 4.3 Total tensile strength versus loading rate for different pre-tensions

Figure 4.3 shows some examples of the total tensile strength versus loading rates for different

pre-tensions. It presents that the total tensile strength of the rock specimens is almost the same

under the same loading rate, no matter how much pre-tension is applied to the specimen before

impact. The result in Figure 4.3 thus indicate that more microcracks are generated and activated

under higher pre-tension, resulting in a more viscous material that is more sensitive to the

loading rate.

The failure pattern of specimens can be an important indicator in revealing the failure

mechanism of rocks, so it would be useful to analyze the failure pattern of the recovered

specimens. Figure 4.4 shows three typical recovered specimens from dynamic tests and one

specimen from static BD test for comparison. The specimen 0-0 is damaged by the static BD test,

it is obvious that the failure is along the loading axis. Figure 4.4 shows that all the specimens

were fractured diametrically into two halves. Specimen 2-2 and specimen 4-2 are both broken

with two pieces of fragments fractured from the center, which reveals the rate dependence of the

rock strength. Both specimen 4-2 and specimen 4-9 have a small wedge shaped crushed zone,

which is a result of secondary fracture after the main fracture from the center of the disc as

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discussed in the literature (Dai, Huang et al. 2010). The secondary fracture is mainly caused by

the further movement of the incident bar towards the transmitted bar after the initial impact. With

the increase of the loading rate, the impact velocity of the striker bar on the incident bar gets

higher, leading to higher moving velocity of the incident bar.

Figure 4.4 Typical failure patterns of the tested specimens

4.2 DCA Modeling for the Dynamic Tensile Failure of Rock under Pre-tension

The DCA algorithm process is basically involved in the calculation at the dominant crack tip for

the local stress and fracture toughness. With the propagation of the crack, the damage evolves

until the propagation velocity reaches the critical value, while the modeling material fails

suddenly.

The stress and strain are composed of the volumetric tensor and the deviatoric tensor,

ij m ij ijS (3-4)

ij m ij ije (4-6)

which can be written in the form of components in different directions:

where

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11 22 33

1 1( )

3 3m kk (3-5)

11 22 33

1 1( )

3 3m kk (3-6)

m is the mean stress, m is the mean strain,

kk is the volumetric strain, ij is the Kronecker

delta. When the crack propagates under the effect of far field stress, the local stress intensity

factor is:

effK c (3-7)

where the effective stress can be written as the form of the deviatoric stress according to Von

Mises law

2

33

2eff ij ijJ S S (3-8)

So the local stress intensity factor can also be expressed as:

2 2 3

2eff ij ijK c cS S (3-9)

At certain calculation step, the stress and can be obtained from the stress in previous step and the

strain rate,

(t t) (t)ij ij ij (3-10)

where ij is the increment of the stress, (t)ij is the stress component at the previous step, and

ij m ij ijS (3-11)

m V kkK (3-12)

Where VK is the bulk modulus, the increment of the volumetric strain kk is constant in each

step, ijS is the increment of the deviatoric stress during the time step.

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Figure 4.5 Flow chart of the DCA modeling

Modeling parameters , , , ,a c m N

Initial stress, strain conditions at 0t t

3(t) (t) (t)

2ij ijK cS S

21ICK K

m

YES

2

max[1 ( ) ]ICKc v

K

max

1

( )mKc v

K

NO

( t) Nn

YES

Stop calculation, Strength=Max( 1 2, .., N )

NO

2 31[3( ) ( ) ]

2

c

ij ij ij

c c ce S S

G a a a

(t t) (t)ij ij V kk ij ijK S

(t t) (t)ij ij t

t t t

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Is current fitness value

better than pBest?

Target or maximum

epochs reached?

The particle swarm optimization (PSO), which is a relatively recent heuristic search method

similar to the Genetic Algorithm (GA) but more computationally efficient, is adopted to search

for the best values for the parameters a , 0c , and m that works for the modeling.

Figure 4.6 Flow diagram illustrating the particle swarm optimization algorithm

Initialize Particles

Calculate fitness values for each particle

YES

Assignment current

fitness as new pBest

NO

NO

Assign best particle’s pBest value to gBest

Keep previous pBest

Calculate velocity for each particle

Use each particle’s velocity value to update its data value

End YES

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Figure 4.7 Experimental and modeling results with different loading rates under 0 MPa pre-

tension, with parameters 6.74a mm, 0 1.45c mm and 10.33m

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Figure 4.8 Relationship between pre-tension and the ratio of initial crack size over characteristic

volume size

Figure 4.8 illustrates how the ratio of initial crack size over the characteristic volume size 0 /c a

is related to the pre-tension the rock specimen bears. Basically, the ratio of 0 /c a increases with

the pre-tension, which is easy to understand because higher pre-tension means more damage

made in the specimen and more microcracks generation and coalescence, leading to a larger

initial crack size.

According to the correlation between the ratio 0 /c a and the static pre-tension

0 , a polynomial

function is used to fit the data, as in Figure 4., the function is expressed as:

2

0 00

0 0

0.221 0.00424 0.00199/c a

(3-13)

where 0 is the static pre-tension at the center of the specimen, ( 1 )MPa is a reference stress

to valid the dimension of the equation. From Eq.(3-13), we can predict the dynamic tensile

strength when the desired pre-tension is given, so Eq.(3-13) can be considered as the bridge

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between the macroscopic loading conditions to the microscopic characteristics, which can be

used in DCA to predict the dynamic tensile strength of rock materials.

After we get the optimized values for the parameters under different pre-tension stresses, the

DCA model can be carried out to predict the dynamic tensile strength for each case, the

parameters used for the DCA model is listed in Table 4.1.

Table 4.1 Parameters used in DCA for the prediction of the dynamic tensile strength

E(GPa) a(mm) vmax(m/s)

46 4.0 300

υ m KIC(MPa·m1/2)

0.21 5.0 1.37

5 Dynamic Tensile Tests Under Hydrostatic Stress

5.1 BD Test under Hydrostatic Confinement

In this program, five groups of specimens are tested under the hydrostatic confinements of 0

MPa, 5 MPa, 10 MPa, 15 MPa, and 20 MPa. Figure 5.1 illustrates the correlation between tensile

strength and the loading rate when the rock specimens are under 10 MPa hydrostatic stress. It

can be observed that the tensile strength increases with the loading rate almost linearly, revealing

the phenomenon of rate dependency that is common for engineering materials.

Based on the correlation between the tensile strength and the loading rate as shown in Figure 5.1,

and that between the strength and the hydrostatic confinement as in Figure 5.2, an empirical

equation is proposed to fit the testing results and explain the dynamic tensile behaviour of rocks

under hydrostatic confinement:

0

0 0

(1 ln(1 ))(1 ( ) )n

tot

PS S

P

(5-1)

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where totS denotes the dynamic tensile strength of the test rock materials,

0S (= 12.8 MPa) is the

static BD strength of the rock material. P is the hydrostatic confinement, 0P (=1 MPa) is the

reference hydrostatic confinement; is the loading rate of each impact test, 0 (=1 GPa/s) is

the reference loading rate. , and n are fitting parameters.

Figure 5.1 Dynamic tensile strength of confined rock specimen under 10MPa hydrostatic stress

Figure 5.2 Dynamic tensile testing results under different loading rates and hydrostatic pre-stress,

and data fitting of the results

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The physical meaning of the equation is that, when the loading rate is 0 and there is no

confinement, the strength of the rock is the static tensile strength S; the dynamic tensile strength

of the rock logarithmically increases with the hydrostatic confinement. The data fitting based on

Eq. (5-1) and the experimental result leads to the values of the parameters as: =0.1804 ,

0.0436 , and 0.5257n . Figure 5.3 is obtained to show how the dynamic tensile strength is

related to the hydrostatic confinement and the loading rate, which fits well to the data points.

Based on the fitted curves, a 3D plot is obtained to show the dynamic tensile strength of rocks

with loading rate and hydrostatic confinement, as in

Figure 5.3. It is obvious that the dynamic tensile strength increases with both the hydrostatic

stress and the loading rate. It can be also seen from the 3D plot that the increment of the dynamic

tensile strength decreases with the loading rate and the hydrostatic stress.

Figure 5.3 The 3D plot of the dynamic tensile strength with loading rate and hydrostatic pre-

stress

Figure 5.4 shows some recovered specimens with different hydrostatic confinement and loading

rate to study the failure pattern of the BD specimens under such loading conditions, revealing the

rate dependence because higher loading rate means less time for the propagation and coalescence

of microcracks before failure, thus more microcracks are involved in the failure process, leading

to higher apparent strength of the rock specimens.

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b

a

c

d e

Figure 5.4 Recovered specimens under different loading rates and hydrostatic pre-stress

5.2 The DCA Prediction of the Dynamic Tensile Strength of LG

Subjected to Hydrostatic Confinement

The PSO is adopted to do the iterations for the values of the parameters for the DCA modeling.

The parameters are found first to match each case with different confining pressure.

Table 5.1 Modeling error for 20 MPa confining pressure with parameters 3.46a mm,

0 0.24c mm and 9.12m

Loading rate

(GPa/s)

Experimental Strength

(MPa)

Modeling strength

(MPa) Error

686.2 48.22 46.83 2.88%

926.75 51.48 52.71 2.39%

1024.64 52.86 54.18 2.50%

1205.83 56.37 56.85 0.85%

1351.49 59.48 59.42 0.10%

1749.28 67.47 64.58 4.28%

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Figure 5.5 Experimental and modeling results with different loading rates under 20 MPa

hydrostatic confining pressure, with parameters 3.46a mm, 0 0.24c mm and 9.12m

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Similar to the case when the confining pressure is 20 MPa, the DCA modeling is carried out with

the PSO algorithm for the cases when the confining pressure is 0 MPa, 5 MPa, 10 MPa, and 15

MPa. Table 5.2 lists the optimized parameters and the error for each hydrostatic confinement

condition.

Table 5.2 Optimized parameters for different hydrostatic confinement conditions by the PSO

Hydrostatic Stress

(MPa)

a

mm 0c

mm 0 /c a m

Max

Error

0 3.81 1.00 0.26 5.00 4.55%

5 4.21 0.60 0.14 9.41 3.27%

10 2.00 0.21 0.11 10.0 3.12%

15 2.79 0.17 0.06 5.04 3.24%

20 3.46 0.24 0.07 9.12 4.28%

After the optimization of all the cases including the pre-tension, triaxial stress and hydrostatic

confining pressure, the characteristic volume size is 4 mm, the parameter m is 5, then the PSO is

adopted again for the initial crack size 0c for each case, and the results are listed in Table 5.3.

Table 5.3 Optimized value for initial crack size under different hydrostatic confinement

Hydrostatic Stress

(MPa)

a

mm 0c

mm 0 /c a m

Max

Error

0 4.00 0.89 0.22 5.00 2.33%

5 4.00 0.45 0.11 5.00 3.82%

10 4.00 0.35 0.09 5.00 3.97%

15 4.00 0.21 0.05 5.00 3.32%

20 4.00 0.16 0.04 5.00 1.71%

To sum up, five groups of Laurentian granite specimen were impacted with different loading

rates under the hydrostatic stress of 0 MPa, 5 MPa, 10 MPa, 15 MPa and 20MPa. Besides the

experiments, the DCA model with the PSO algorithm is adopted to predict the dynamic tensile

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strength under different hydrostatic confining pressures, which is reflected on the value of the

ratio of the initial crack size to the characteristic volume size. The experimental result reveals that

there is a significant enhancement in tensile strength with the increase of the loading rate, which is the

rate dependency for many engineering materials. The dynamic tensile strength increases with the

hydrostatic confinement due to the restraint of opening and propagation of discontinuities by

confinement. Another important finding is that the increment of the tensile strength decreases as the

hydrostatic confinement becomes higher, which is the same as the static strength under confining

pressure. The DCA modeling is carried out and the comparison of the results with the experimental ones

demonstrates its capability for the prediction of the dynamic tensile strength of rock materials.

6 Dynamic Tensile Test under Triaxial Stress States

6.1 BD Test under Triaxial Stress States

After the calculation of the stress on the specimen, the stress exerted on the bar is then

determined to achieve the pre-stress conditions before the impact is launched. Through the

correlation between the tensile stress on the specimen and the stress at the bar specimen interface,

the load needed on the bar can be determined.

Hydrostatic Stress: 5 MPa, 10 MPa Pretension: 20%, 40%, 60%, 80% of the strength

Figure 6.1 Experimental design with different hydrostatic stress and pretension

+

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Figure 6.2 Dynamic tensile strength of confined rock specimen under 5MPa hydrostatic stress

Figure 6.3 Dynamic tensile strength of confined rock specimen under 10MPa hydrostatic stress

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Four groups of specimens are tested under the hydrostatic confinements of 5 MPa and 10 MPa.

Figure 6.2 and Figure 6.3 illustrate the correlation between tensile strength and the loading rate

when the rock specimens are under 5 MPa and 10 MPa hydrostatic stress respectively. It can be

observed that the tensile strength increases with the loading rate almost linearly, revealing the

phenomenon of rate dependency that is common for engineering materials.

Besides the rate dependency mentioned above, it is also obvious that the dynamic tensile strength

of the rock decreases with the pre-tension, which is also observed from the pre-tension tests. The

total tensile strength of LG is illustrated in Figure 6.4 under 5 MPa hydrostatic confinement and

different pre-tensile stresses. Based on the similar fitting for the total tensile strength under pre-

tension without any hydrostatic confinement, the empirical equation as in Eq.(6-1) is proposed to

fit the data and explain the dynamic tensile behavior of rock under triaxial stress states.

0

σ(1 ( ) )n

totS S

(6-1)

where totS denotes the total tensile strength, S (= 17.8 MPa) is the static tensile strength of the

specimen under 5 MPa hydrostatic confining pressure. σ is the loading rate of each impact test,

(=1 GPa/s) is the reference loading rate. and n are fitting parameters. The physical meaning

of the equation is that, when there is no dynamic loading, the strength of the rock is the static

tensile strength S, the second term represents the rate dependence effect. The data fitting based

on Eq.(6-1) and the experimental result leads to the values of the parameters as 0.0628 MPa

and 0.4931n . It is seen that the function fits well with the experimental data points. The result

in Figure 6.4 thus indicates that more microcracks are generated and activated under higher pre-

tension, resulting in a more viscous material that is more sensitive to the loading rate. This

augmented rate sensitivity compensates the pre-tension weakening effect, leading to a roughly

pre-tension independency of the total tensile strength.

The total tensile strength of LG under 10 MPa hydrostatic confining pressure is illustrated in

Figure 6.5. The data fitting based on Eq.(6-1) and the experimental result leads to the values of

the parameters as: 0.0636 MPa, and 0.4454n .

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Figure 6.4 Total strength of rock specimen under 5MPa hydrostatic stress and pre-tension

Figure 6.5 Total strength of rock specimen under 10 MPa hydrostatic stress and pre-tension

Figure 6.6 shows some recovered specimens with different hydrostatic confinement and

pretension to study the failure pattern of the BD specimens under such loading conditions. The

photos at the top are the specimens under 5 MPa hydrostatic confining pressure, followed by the

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specimens under 10 MPa in the middle, and the pattern schematics at the bottom. Type I is

failure pattern is the diametrical split. Figure 6.6a are the specimens with cracks at center and

break neatly into two halves. Type II has central cracking with crushed wedges. In this case, the

specimen fails along its central line but small wedge-shaped pieces can be found in the crumbs,

as shown in Figure 6.6b. Type III shows failure with a crushed strap where a diametrically

distributed crushed zone can be found in the specimen center, as illustrated in Figure 6.6c.

Figure 6.6 Failure pattern of specimens: (a) diametrical split, (b) central cracking with crushed

wedges, (c) failure with crushed strap. The photos at top are the specimens under 5 MPa

confining pressure and in the middle are the specimens under 10 MPa confining pressure.

(a)

(a) (b)

(b)

(c)

(c)

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6.2 The DCA Prediction of the Dynamic Tensile Strength of LG

Subjected to Triaxial Stress State

Same as the preceding chapters, the PSO is adopted to do the iterations for the values of the

parameters for the DCA modeling. Similarly, the parameters are found first to match each case

with different confining pressure. For example, the iterations for confining pressure 5 MPa with

3.56 MPa (20% of tensile strength) pretension is illustrated in Figure 6.7, the iterations for

confining pressure 10 MPa with 4.56 MPa (20% of tensile strength) pretension is illustrated in

Figure 6.8.

Figure 6.7 Iterations for DCA modeling parameters with 5 MPa hydrostatic pressure and 3.56

MPa (20% of tensile strength) pre-tension

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Figure 6.8 Iterations for DCA modeling parameters with 10 MPa hydrostatic pressure and 4.56

MPa (20% of tensile strength) pre-tension

The iteration number is 450 to convergent when the rock is subjected 5 MPa hydrostatic

confining pressure and 3.56 MPa pre-tension, the corresponding values of the parameters are

10.0a mm, 0 0.51c mm and 6.03m ; It takes 462 iterations for the DCA modeling to

converge when the rock specimen are subjected to traixial stress with 10 MPa hydrostatic

confining pressure and 4.56 MPa pre-tension, and the parameters are 4.79a mm,

0 0.25c mm and 7.05m . Results of the DCA modeling under 10 MPa confinement and

several loading rates are illustrated in Figure 6.9.

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Figure 6.9 Experimental and modeling results with different loading rates under 10 MPa

hydrostatic confining pressure and 20% pretension, with parameters 4.79a mm, 0 0.25c mm

and 7.05m

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Similar to the cases when the rocks are subjected to either pure pre-tension or hydrostatic

confinement, the PSO algorithm is adopted in the DCA modeling to achieve the group

optimization of the parameters. Table 6.1 lists the optimized parameters and the error of each

superposed pre-stress conditions.

Table 6.1 Optimized parameters for different hydrostatic confinement conditions by the PSO

Hydrostatic

(MPa) Pre-tension

a

mm 0c

mm 0 /c a m Max Error

5

20% 4.00 0.19 0.05 5.00 2.92%

40% 4.00 0.23 0.06 5.00 4.77%

60% 4.00 0.35 0.09 5.00 2.53%

80% 4.00 0.52 0.13 5.00 4.12%

10

20% 4.00 0.17 0.04 5.00 2.58%

40% 4.00 0.33 0.08 5.00 3.32%

60% 4.00 0.45 0.11 5.00 2.08%

80% 4.00 0.70 0.18 5.00 2.14%

It is obvious that under both hydrostatic confinement conditions, the ratio of 0 /c a decreases

with the increasing pre-tension, which is the same as when the rocks are subjected to pure pre-

tension. After the determination of the parameters, the DCA modeling is carried out and the

dynamic tensile stress history of the specimens under each superposed loading condition is

obtained.

To sum up, the modified SHPB system with hydraulic cylinders is adopted to measure the

dynamic tensile strength under triaixal stress states. The confining pressure are set as 5 MPa and

10 MPa, the pre-tension is 20%, 40%, 60% or 80% of the static tensile strength under the current

hydrostatic confining pressure. Similarly, the DCA model with the PSO algorithm is used to

predict the dynamic tensile strength under different pre-stress conditions, which is reflected on

the value of the ratio of the initial crack size to the characteristic volume size.

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7 Concluding Remarks

This thesis investigated the dynamic tensile failure of Laurentian granite under different pre-

stress conditions with a wide range of loading rates, and explored the relationship between the

dynamic tensile strength of the rock material and the pre-tension, the hydrostatic confining

pressure and the loading rate. The following paragraphs summarize the main items completed in

this thesis and the major conclusions. The experimental results and the DCA modeling

performance can be used as a guideline for the development of a reliable method to predict blast-

induced tensile failure and design tool for blasting operations.

1. The dynamic experimental methodology involving experimentation and calculation equations

using the modified dynamic testing system, i.e. SHPB system, are developed to measure the

dynamic tensile strength of Laurentian granite under different pre-stress conditions. The main

achievement is the modification of the SHPB system to exert static pre-tension and

hydrostatic confining pressure to the rock specimens before the dynamic test is conducted.

2. The dynamic tensile strength of Laurentian granite under different pre-stress conditions are

obtained with respect to the loading rate.

3. The micro-CT technique is used to observe the crack distribution and to exam the failure

pattern of the rock specimens under hydrostatic confinement. It is observed that the failure is

always an extension fracture in the loaded diametral plane as long as the test is valid. The

micro-CT images demonstrate that with higher loading rates, there are more cracks at the

vicinity of the loading diameter direction, which is consistent to the material rate dependency.

4. The development of the Dominant Crack Algorithm (DCA) in the use of prediction for the

dynamic tensile strength of the rock materials. The DCA modeling is carried out and it shows

that it is most sensitive to the ratio of initial crack size over the characteristic volume size

0 /c a , and less sensitive to the characteristic volume size a and the crack velocity related

parameter m .

5. The adoption of Particle Swarm Optimization (PSO) for the optimized values of the

parameters in the DCA modeling for the dynamic tensile failure of LG under different pre-

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tension stresses. With the PSO algorithm, the optimized value for the characteristic volume

size a is determined as 4 mm and the crack velocity related parameter m is determined as 5.

Then, the PSO iteration is used again for the optimized value of the initial crack size for each

case with different pre-stress conditions.

Selected References

Addessio, F. L. and J. N. Johnson (1990). "A Constitutive Model for the Dynamic-Response of Brittle Materials." Journal of Applied Physics 67(7): 3275-3286.

Al-Shayea, N. A., K. Khan and S. N. Abduljauwad (2000). "Effects of confining pressure and temperature on mixed-mode (I-II) fracture toughness of a limestone rode." International Journal of Rock Mechanics and Mining Sciences 37(4): 629-643.

Brar, N. S. and Z. Rosenberg (1988). "Brittle Failure of Ceramic Rods under Dynamic Compression." Journal De Physique 49(C-3): 607-612.

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