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WHEAT Technical specifications DSTU 3768:2010 NATIONAL STANDARD OF UKRAINE Canada-Ukraine Grain Project “Grain Quality and Rural Agriculture Credit Systems in Ukraine – phase II” The State Centre for Certification and Expertise of Grain and Products of its Processing Free translation from Ukrainian

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Page 1: The State Centre for NATIONAL STANDARD OF UKRAINE ... · NATIONAL STANDARD OF UKRAINE Canada-Ukraine Grain Project “Grain Quality and Rural Agriculture Credit Systems in Ukraine

WHEATTechnical specifications

DSTU 3768:2010

NATIONAL STANDARD OF UKRAINE

Canada-Ukraine Grain Project “Grain Quality and Rural

Agriculture Credit Systems in Ukraine – phase II”

The State Centre for Certification and Expertise of Grain and Products of its

Processing

Free translation from Ukrainian

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«HARMONIZATION» ?!!!

USDA U.S. DEPARTMENT OF AGRICULTURECOMMISSION REGULATION (EU) No. 1272/2009

ISO 7970:2000 (Wheat (Triticum aestivum L.) – Specification) ISO 11051:1994 (Durum wheat (Triticum durum Desf.) – Specification)

A considerable quantity of standards, requirements of the various countries and the external economic contracts

Operational experience with acting national standard and GOST

To have possibility for more harmonious conversion from quality parameters of the national standard to quality parameters of theexternal economic contracts and the international standards

To take into consideration internal specificity and also interests of all sectors of the market (in particular the baking industry)

Free translation from Ukrainian

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1. SCOPE

The present standard applies to Common wheat and Durum wheat destined for use in food and nonfood purpose and for export.Wheat types distribution is expounded in a Table 1; parameters, characteristicsand norms of wheat quality as per Grades – in Tables 2 and 3;obligatory requirements for wheat grain, which guarantee human and animals life and environment — in sections 5.2 (grain condition, odor, color, pests infestation), 6.1 (toxic elements, mycotoxines and pesticides), 6.2 (safety and productive sanitation requirements), 6.3 та 6.4 (environment protection).

1.1 The present standard applies to Common wheat (Triticum aestivum L.) and Durum wheat (Triticum durum Desf.) destined for use in food and nonfood purpose and for trade.1.2 Obligatory requirements for wheat grain, which guarantee human and animals life and health safety and preservation of the environment are stated in sections 4 (4.9, 4.10, 4.11) and 5.

2004

2009-2010

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2. NORMATIVE REFERENCES

Having regard to thecancellation of old DSTU

and GOST versions normative references were

revised

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3. TERMS AND DEFINITIONS

Terminology and correspondent definitions are used in the standard in accordance with DSTU 2422 and other documents acting in Ukraine.Grain warehouseLegal entity which on the right of ownership has a warehouse(s) and certificateon accordance of storage services of grain and foods of his processingGrain impuritiesDefective grains of wheat and other cultivated plants, which in accordance withstandards for them are included in Grain impurities3.1 DockageImpurities of an organic and inorganic origin, which should be eliminated from wheat in case of his end use. Impurities are divided on Grain and Wasteimpurities.

Terminology and correspondent definitions are used in the standard in accordance with DSTU 2422 and other normative legal documents acting in Ukraine, in particular: ImpuritiesImpurities of an organic and inorganic origin, which are divided on Grain and Waste impurities and affecting wheat quality

2004

2009-2010

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3.1.1 Grain impurities include:3.1.1.1 broken grainsGrain bits, which are generated as a result of mechanical activity 3.1.1.3 pressed grainsGrains strained, flattened as a result of mechanical activity

3.1 Grain impurities3.1.1 broken grainsAll grains whose endosperm is partially uncovered or grains from which the germ has been removed as a result of mechanical activity

2009-2010

2004

3. TERMS AND DEFINITIONS

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3.1.1.2 shrunken grainsGrains unadulterated, contracted, light-weight, strained as a result ofadverse conditions of development and maturing3.1.1.5 grains damaged by frostGrains damaged by frost during maturing period, with changed color (whitish or darkened) 3.1.1.8 unripe grainsGrains which did not come to complete maturity; with greenish shade, simply strained by pressure

3.1.2 shrivelled grainsGrains damaged by frost and unripe grains (green), as well as small and shrunken grains, which, after elimination from the sample of all other matter referred to Grain and Waste impurities, pass through a sieve with long rounded apertures of the following dimensions: 2.0 x 20.0 mm for common wheat and 1.9 x 20.0 mm for durum wheat

2004

2010

3. TERMS AND DEFINITIONS

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3.1.1.4 sprouted grainsGrains in which the radicle or plumule exceeded the seed coat bounds or with plumule which tore, but did not come out the seed coat surface, and grains from which the radicle or plumule have been removed

3.1.3 sprouted grainsGrains in which the radicle or plumule exceeded the seed coat bounds; grains from which the radicle or plumule have been removed, with clearly visible deformation and changed seed coat color in the germ area

2004

2009-2010

3. TERMS AND DEFINITIONS

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3.1.4 grains overheated during dryingGrains with changed seed coat color and sound endosperm, which color has not undergone changes during drying

3.1.4 overheated grainsGrains with changed seed coat color due to heating during drying or spontaneous heat generation and sound endosperm, which color has not undergone changes

2004

3.1.1.6 damaged grainsGrains with changed seed coat color and endosperm from creamy to light brown due to spontaneous heat generation, drying and morbid affection

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2010

3. TERMS AND DEFINITIONS

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3.1.1.7 eaten grainsGrains eaten by pests irrespective of the stage of their damage

3.1.5 grains eaten by pestsGrains eaten by pests irrespective of the stage of their damage

2004

2009-2010

3. TERMS AND DEFINITIONS

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3.1.6 grains of cerealsWhole and not spoiled grains of rye, triticale and barley

3.1.6 grains of cerealsNot spoiled grains of rye, triticale and barley

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2010

3. TERMS AND DEFINITIONS

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3.1.7 grains in which the germ is discoloredGrains with normal and not sprouted germ and seed coat at the germ area colored brown to brownish black. This discoloration (darkening as a result of fungus or bacterial affection) is located at the germ area and extends (from one side at least) into the grains crease (Annex D)

2010

3. TERMS AND DEFINITIONS

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Annex D (informative)EXTERNAL SIGNS OF GRAINS IN WHICH THE GERM IS DISCOLORED

1 – The minimum area and intensity of darkening at the germ area (view from above);

2 – The minimum level of coverage by continuous band that extends around thecheek (width and darkening intensity of the band is irrelevant);

3 – The minimum degree of darkening of the continuous band required (amount of the band darkening area is irrelevant).

Grain shall be considered as grains in which the germ is discolored in case of simultaneous presence of sign 1 with sign 2 or with sign 3, which are obligatory.

2009-2010

2010

2009Hard copy

version

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3.1.2 Waste impurities include:3.1.2.1 mineral impuritiesLimitedly possible impurities of mineral origin (sand, lumps of earth, pebble, etc.) 3.1.2.2 organic impurutiesPhytogenous impurities (fragments of stems, leaves, ears, awns, chaff, etc.), fragments of pests, seeds of non-toxic weeds

3.2 Waste impurities3.2.1 mineral impuritiesImpurities of inorganic origin (sand, lumps of earth, pebble, etc.) retained by a sieve with long rounded apertures of 1.0 x 20.0 mm and all matter of organic and inorganic origin passing through the mentioned sieve (fines)3.2.2 organic impuritiesAll organic components other than grains of wheat, grains of cereals and harmful impurities: fragments of stems, leaves, ears, awns, chaff, fragments of pests, seeds of weeds and other cultivated plants, etc.

2010

2004

3. TERMS AND DEFINITIONS

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3.1.2.3 harmful impuritiesPhytogenous impurities which are harmful for humans and animals health

3.2.3 harmful impuritiesPhytogenous impurities, which if present in the certain quantities, have a harmful and dangerous effect for humans and animals health, organoleptic properties or technological performance: smut, ergot, harmful and toxic seeds according to Annex E

2004

2010

3. TERMS AND DEFINITIONS

Free translation from Ukrainian

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Annex E (informative)INDICATIVE LIST OF

HARMFUL AND TOXIC SEEDS

Botanical name Common name in Ukrainian

Common name in English

Toxic seeds Acroptilon repens (L.) DC. Гірчак повзучий Hardheads, Russian Knapweed Agrostemma githago L. Кукіль звичайний Corn-cockle Conium maculatum L. Болиголов плямистий Spotted hemlock Coronilla varia L. В’язіль різнокольоровий Coronilla, Crown vetch Crotalaria spp. Кроталярія Crotalaria Datura fastuosa L. Дурман індійський Downy thorn-apple, hoary thorn-

apple Datura stramonium L. Дурман звичайний Stamony, Thorn apple Heliotropium lasiocarpum Fisher et C. A. Meyer

Геліотроп опушеноплідний Heliotrope

Lolium temulentum L. Пажитниця п’янка Darnel Ricinus communis L. Рицина звичайна Castor-oil plant Sophora alopecuroides L. Софора лисохвоста Stagger bush, Russian centaury Sophora pachycarpa Schrank ex C. A. Meyer

Софора товстоплідна Siberian Pachycarpa

Thermopsis montana Термопсис гірський Buffalo pen Thermopsis lanceolata R. Br. in Aiton

Термопсис ланцетоподібний, мишатник

False Lupin, Golden Banner

Trichodesma incanum Триходесма сива Harmful seeds Allium sativum L. Часник Garlic Cephalaria syriaca (L.) Roemer et Shultes

Ворсянка, цефалярія сірійська

Teasel

Melampyrum arvense L. Мар’янник польовий Cow-cockle Melilotus spp. Донник Melilot, Sweet clover Sorghum halepense (L.) Pers. Сорго алепське Johnson grass Trigonella foenum-graecum L. Пажитник сінний Fenugreek

2009-2010

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1. Acroptilon repens (L.) DC.Hardheads, Russian KnapweedГірчак повзучий

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

ISO 7970:2000

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2. Agrostemma githago L.Corn-cockleКукіль звичайний

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

ISO 7970:2000

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3. Conium maculatum L.Spotted hemlockБолиголов плямистий

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

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4. Coronilla varia L.Coronilla, Crown vetchВ’язіль різнокольоровий

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

ISO 7970:2000

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5. Crotalaria spp.CrotalariaКроталярія

ISO 7970:2000

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

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6. Datura Fastuosa L. (syn. Datura metel)Downy thorn-apple, Hoary thorn-appleДурман індійський

ISO 7970:2000

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

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7. Datura stramonium L.Stramony, Thorn apple Дурман звичайний

ISO 7970:2000

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

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8. Heliotropium lasiocarpum Fisher et C. A. MeyerHeliotropeГеліотроп опушеноплідний

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

ISO 7970:2000

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9. Lolium temulentum L.DarnelПажитниця п’янка

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

ISO 7970:2000

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10. Ricinus communis L.Castor-oil plant Рицина звичайна

ISO 7970:2000

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

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11. Sophora alopecuroides L.Stagger bush, Russian centauryСофора лисохвоста

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

ISO 7970:2000

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12. Sophora pachycarpa Schrank ex C. A. Meyer Siberian PachycarpaСофора товстоплідна

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

ISO 7970:2000

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13. Thermopsis montanaBuffalo penТермопсис гірський

ISO 7970:2000

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

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14. Thermopsis lanceolata R. Br. in AitonFalce Lupin, Golden bannerТермопсис ланцетоподібний, мишатник

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

ISO 7970:2000

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15. Trichodesma incanum

Триходесма сива

ISO 7970:2000

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

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1. Allium sativum L.GarlicЧасник

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

ISO 7970:2000

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2. Cephalaria syriaca (L.) Roemer et ShultesTeaselВорсянка, цефалярія сірійська

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

ISO 7970:2000

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3. Melampyrum arvense L.Cow-cockleМар’янник польовий

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

ISO 7970:2000

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4. Melilotus spp.Melilot, Sweet cloverДонник

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

ISO 7970:2000

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5. Sorghum halepense (L.) Pers. Johnson grassСорго алепське

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

ISO 7970:2000

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6. Trigonella foenum-graecumFenugreekПажитник сінний

DSTU 3768:2010 INDICATIVE LIST OF HARMFUL AND TOXIC SEEDS

ISO 7970:2000

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3.1.2.4 fusarium affected grainsGrains contaminated by the Fusarium disease, whitish, sometimes with salmon spots, light, shrunken, unviable3.1.2.5 spoiled grainsGrains with decidedly spoiled endosperm from brown to black in color and grains which scatter in case of pressing.

3.2.4 spoiled grainsGrains presenting specks of rottenness, mould, downy mildew, bacterial or other damage; with changed seed coat and endosperm color due to spontaneous heat generation or too extreme heating during drying and/or with crumbly endosperm.Fusarium affected grains also belong to this group – grains contaminated by the Fusarium disease, whitish, chalky with complete loss of shine, sometimes with salmon spots, shrunken, unviable

2009-2010

2004

3. TERMS AND DEFINITIONS

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Annex C (normative)EXTERNAL SIGNS OF FUSARIUM AFFECTED

WHEAT GRAINS AND DISCOLOURED AND PINK NON-FUSARIUM AFFECTED GRAINS

Characteristics Fusarium affected grains Discoloured grains

(Discoloration Level 3)

Pink Non-Fusarium affected grains

External appearance

Grain is whitish, chalky, with complete loss of shine. Pink-crimson or cream-pink stains can be observed on some grains

Grain is cream-white with complete or partial loss of shine

On the background of typically colored grain coats there are pink-red stains on the whole surface of grains, mainly near the germ, which cannot be scraped off. Natural shine.

Kernel structure Porous, crumbly endosperm of floury consistency; in case of lingering Fusarium affect – from floury to partially vitreous

Structure of endosperm is similar to typically coloured grain

Vitreuesness of endosperm is the same as in typically coloured grain

Form and fullness

Most grains are wrinkled and stunted; with pointed cheeks and dashed in crease. In case lingering Fusarium affect form and size of the crease are similar to that in sound grains, sometimes grains are swollen, with pilled off coats

Not differ from typically coloured grains. Coat may be slightly wrinkled on the back of the grain.

Not differ from typically coloured grains. Pink coloured coat and endosperm are tightly joined.

Fungi infection and germ viability

Germ is not viable, black coloured at cut. Fungus mycelium is present on the crease and in the germ

Germ is viable, primrose at cut. No fungus mycelium and sporodochium on the crease and the germ

Germ is viable, primrose at cut. No fungus mycelium and sporodochium on the crease and in the germ

2004-2009-2010

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Annex B (normative)DETERMINATION OF FUSARIUM AFFECTED GRAINS CONTENT

2004-2009-2010

B.1 Apparatus:Laboratory balances of accuracy class 3, maximum weighing

limit of 1 kg in accordance with GOST 24104.4.5 magnifying glass in accordance with GOST 25706.Laboratory plate in accordance with the normative document

currently in force.Scalpel or razor blade in accordance with the normative

document currently in force. Scoop in accordance with the normative document currently in

force.Laboratory cup for test sample in accordance with the

normative document currently in force.

B.2 Sampling:Sampling is carried out according to GOST 13586.3. An average

sample of not less than 2 kg shall be combined from increment samples drawn. A test sample of (50.0 ±0.1) g shall be extracted from the average sample after the coarse waste impurities removal.

B.3 Determination:Grains which exhibit fusarium affect (according to Annex C) shall

be removed from the (50.0 ±0.1) g test portion under good lighting conditions. If uncertain grains, which can be classified as Discoloured grains of the Discoloration Level 3 or Pink Non-Fusarium affectedgrains, are observed, their germ and crease shall be checked foravailability of mycelium and sporodochium using the magnifying glass, the germ shall be cut and its colour shall be determined. The grains shall be considered as Fusarium affected grains in case the aggregatecharacteristics indicated in Annex C are observed. Weigh Fusariumaffected grains to the nearest 0.01 g.

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2004-2009-2010

B.4 Processing of the results:Content of Fusarium affected grains is expressed in

percents, where total weight of the Fusarium damaged kernels detected in test sample of 50 g is multiplied by 2. In case the third decimal digit is 5 or more, the second decimal digit shallbe increased by one.

B.5 Control of the results:Discrepancy between results of control determinations’

should not exceed mentioned permissible values:

Fusarium affected grains content, %

Permissible difference between results of control

determinations, % Up to 0.30 inclusive 0.15

Over 0.30 up to 0.60 inclusive 0.25 » 0.60 » 1.00 » 0.35 » 1.00 » 3.00 » 0.55 » 3.00 » 6.00 » 0.85

» 6.00 » 10.00 » 1.25

Annex B (normative)DETERMINATION OF FUSARIUM AFFECTED GRAINS CONTENT

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3.3 Bug-ridden grainsGrains with black point at the surface as a result of bug (Eurygaster integricepsPut) nibble with clearly visible bright-yellow spot of round or irregular shape situated around the point; grains with the same spot on the surface with impression or wrinkle at the spot area without nibble point; grains with the same spot at the germ area without impression or wrinkle and without nibble point; in all cases endosperm consistence under the spot is easily crumbled, pulverized, or reduced to powder

GOST 30483-97 2009-2010

3. TERMS AND DEFINITIONS

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3.3 smutty grainsGrains with brush or part of the surface covered with smut spores.

3.4 Smutty grainsGrains with brush, crease or part of the surface covered with smut spores, which appearance at first to be determined visually and if necessary to be confirmed by mycological examination 2009-2010

2004

3. TERMS AND DEFINITIONS

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3.2. Wheat of unimpaired quality, Grain and Waste impurities composition3.2.1 Wheat of unimpaired quality includes:– whole and damaged wheat grains which are not included by the nature of their damage in Grain and Waste impurities;– small grains — whole wheat grains which pass through a sieve with long rounded apertures 1.7 x 20.0 mm;– for wheat of Class 6 — grains and seeds of other cereal and pulse crops which are not included by the nature of their damage in Grain and Waste impurities in accordance with standards for these plants.

3.5 Wheat of unimpaired quality, Grain and Waste impurities3.5.1 Wheat of unimpaired quality includes:– whole and damaged wheat grains which are not included by the nature of their damage in Grain and Waste impurities;– for common and durum wheat — grains in which the germ is discolored less than 8 %;– for wheat of Class 6 — grains and seeds of other cereal and pulse crops which are not included by the nature of their damage in Grain and Waste impurities in accordance with standards for these plants.

2004

2009

3. TERMS AND DEFINITIONS

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Modifying order No. 272 of Derzhspozhyvchstandart of Ukraine dd. 29/07/2009Amendment No.2 DSTU 3768:2009

Section No. 3. Item 3.5.1 “Wheat of unimpaired quality includes:”to complement paragraph in such redaction:"For common wheat shrivelled grains in the amount of 50 % of their mass"

2009

3. TERMS AND DEFINITIONS

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3.5 Wheat of unimpaired quality, Grain and Waste impurities3.5.1 Wheat of unimpaired quality includes:– whole and damaged wheat grains which are not included by the nature of their damage in Grain and Waste impurities;– for common and durum wheat — grains in which the germ is discolored less than 8 %;– for common wheat shrivelled grains in the amount of 50 % of their mass;– for wheat of Class 6 — grains and seeds of other cereal and pulse crops which are not included by the nature of their damage in Grain and Waste impurities in accordance with standards for these plants.

3.5 Wheat of unimpaired quality, Grain and Waste impurities composition3.5.1 Wheat of unimpaired quality includes:– whole and damaged wheat grains, which are not included by the nature of their damage in Grain and Waste impurities;– grains in which the germ is discolored: for common wheat of Group A not more than 8 %, for common wheat of Group B and Grade 6 – not more than 30 %;– for wheat of Grade 6 - grains and seeds of other cereal and pulse crops which are not included by the nature of their damage in Grain and Waste impurities in accordance with standards for these plants

2009

2010

3. TERMS AND DEFINITIONS

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3.2.2 Grain impurities include:for common and durum wheat of all Grades:– grains of wheat pressed, shrunken, sprouted, damaged by frost, damaged due to spontaneous heat generation or during drying, unripe, broken and eaten irrespective of the stage of their damage;– whole and damaged grains of rye, triticale and barley which are not included by the nature of their damage in Waste impurities in accordance with standards for these plants;for common wheat of Grade 6:– grains and seeds of other cereal and pulse crops which are included by the nature of their damage in Grain impurities in accordance with standards for these plants.

____________________________________________

3.5.2 Grain impurities include:– grains of wheat shrivelled, sprouted, overheated during drying;– grains in which the germ is discolored (the difference between 8 % and their content);– grains of wheat broken and damaged by pests irrespective of the stage of their damage;– grains of other cereals which are not included by the nature of their damage in Waste impurities in accordance with standards for these plants;– for wheat of Grade 6 - grains and seeds of other cereal and pulse crops which are included by the nature of their damage in Grain impurities in accordance with standards for these plants

2004

2009

Free translation from Ukrainian

3. TERMS AND DEFINITIONS

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Modifying order No. 272 of Derzhspozhyvchstandart of Ukraine dd. 29/07/2009Amendment No.2 DSTU 3768:2009

Section No. 3. Item 3.5.2 “Wheat of unimpaired quality includes:”to expound the first paragraph in such redaction:"Grains of wheat shrivelled in the amount of 50 % of their mass, sprouted, overheated during drying;"

2009

3. TERMS AND DEFINITIONS

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3.5.2 Grain impurities include:– grains of wheat shrivelled in the amount of 50 % of their mass, sprouted, overheated during drying.– grains in which the germ is discolored (the difference between 8 % and their content)– grains of wheat broken and damaged by pests irrespective of the stage of their damage– grains of other cereals which are not included by the nature of their damage in Waste impurities in accordance with standards for these plants.– for wheat of Grade 6 - grains and seeds of other cereal and pulse crops which are included by the nature of their damage in Grain impurities in accordance with standards for these plants.

3.5.2 Grain impurities include:– grains of wheat shrivelled, sprouted, overheated;– grains in which the germ is discolored: for durum wheat – all grains, for common wheat of Group A – more than 8 %, for common wheat of Group B and Grade 6 – more than 30 %;– grains of wheat broken and eaten by pests irrespective of the stage of their damage;– grains of other cereals, which are not included by the nature of their damage in Waste impurities in accordance with standards for these plants;– for wheat of Grade 6 - grains and seeds of other cereal and pulse crops which are included by the nature of their damage in Grain impurities in accordance with standards for these plants

2009

2010

3. TERMS AND DEFINITIONS

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3.2.3 Waste impurities include:– all matter (the same as harmful impurities components) passing through a sieve with a1.0 mm round mesh; – from the matter retained by a sieve with 1.0 mm round mesh: mineral, organic and harmful impurities; weed seeds; spoiled grains of wheat, rye, triticale and barley with decidedly spoiled endosperm from brown to black in color;– Fusarium affected grains;– for common and durum wheat of all Grades — grains and seeds of other cultivated plants, excluding non-spoiled grains of rye, triticale and barley, and different oilseeds;– fragments of wheat, rye and barley grains with completely eaten away endosperm.

3.5.3 Waste impurities include:– all matter (the same as harmful impurities components) passing through a sieve with long rounded apertures of 1.0 x 20.0 mm, which should be included in mineral impurities; from the matter retained by a sieve with long rounded apertures of 1.0 x 20.0 mm:– mineral, organic and harmful impurities; spoiled grains of wheat, rye, triticale and barley;– fragments of wheat, rye, triticale and barley grains with completely eaten awayendosperm.

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3. TERMS AND DEFINITIONS

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4. TECHNICAL SPECIFICATIONS

5 GENERAL TECHNICAL SPECIFICATIONS5.1 Common wheat is divided into six Grades and Durum wheat into five Grades based on quality parameters values. Corresponding quality requirements for each wheat Grade are included in tables 2 and 3.5.5 Common wheat of Grade 6 can be used for food and nonfood purpose. М’якупшеницю 6 класу можна використовувати для продовольчих та непродовольчихпотреб. If such wheat is used for food purpose it have to be with Natural weight not less than 710 g/l and Protein content (on dry matter basis) not less than 10 %. __________________________________________________________________________________________________________________________________________________________

4 TECHNICAL SPECIFICATIONS4.1 Common wheat is divided into six Grades (Grades 1-3 – Group A, Grades 4-5 –Group B and Grade 6) based on quality parameters values. Durum wheat is divided into five Grades based on quality parameters values. Corresponding quality requirementsfor each wheat Grade are included in tables 1 and 2.Common wheat of Group A to be used in food purpose (mainly for flour-milling and baking industry) and for export. Common wheat of Group B and Grade 6 to be used in food and nonfood purpose and for export. As per customer’s requirement other non-class-generating quality parameters (Wet gluten content and quality, W, sedimentation index, etc.) can be analyzed in accordance with internationally recognized and approved methods.

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D escr ip tio n and lim its fo r C o m mo n wh eat Grad es P aram eters

1 2 3 4 5 6 Pro te in co n tent (o n dr y m at ter ba s is) , % , no t le ss than

14 .0 13 .0 12 .0 11 .0 10 .0 N ot lim ited

W et glu ten c on te nt , % , not les s tha n 30 27 23 18 18 N o t lim ited G luten q uality :

g roup І І- II І-I I І-I I І-I II N o t lim ited IDK un its 45 -75 45-100 45-100 20-100 20-110 N ot lim ited

R em a rk : W et glu te n co nte nt an d Q ua lity o f glu ten a re n ot ob lig ato ry pa ra m e te rs for d eter m in atio n of w h ea t Gr ad e. Lim its fo r the m ar e ind icate d for u se in con tr ac ts for w h ea t in -tak e to f lou r m a nu fac tur es on ly .

D u rin g the d ete rm i na tio n o f w h ea t c l ass the p rio rity is gi ve n to fa llin g n um b er a ga in s t co nten t o f sp ro ute d gr ain s .

Table 1 — Common wheat quality parametersD e s c r ip t io n a n d l im its fo r

C o m m o n w h e a t G r o u p s a n d G r a d e s А B P a r a m e te r s

1 2 3 4 5 6 P r o t e in c o n t e n t ( o n d r y m a t t e r b a s is ) , % , n o t le s s th a n

1 4 .0

1 2 .5

1 1 .0

1 2 .5

1 0 .5

N o t lim ite d

W e t g lu te n c o n te n t , % , n o t le s s th a n

2 8 .0 2 3 .0 1 8 .0 N o t l im ite d

G lu te n q u a l ity : g r o u p ID K u n its

І - І І 4 5 -1 0 0

І - І І 4 5 -1 0 0

І - І І 2 0 -1 0 0

N o t l im ite d

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11,0 % - 200945-100 - 2009

4. TECHNICAL SPECIFICATIONS

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Table 2 — Common wheat quality parameters

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5.2 Wheat of all Grades should be in sound condition, notperspired and without heat damage during drying, with normal smell intrinsical to sound grain of this type (without musty, malty, moldy, other foreign smells); of normal color; grain pestsinfestation is not allowed (except mites infestation of not more than the second degree).4.2 Common and Durum wheat of each Grade should be in sound condition, not perspired and without heat damage; with smell intrinsical to sound grain (without musty, malty, moldy, putrid, wormwood, smutty, oil products and other foreign smells); of typical color; grain pests infestation is not permitted.

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TYPES

4.1 Wheat is divided into Types in accordance with botanical and biological features, color and vitreousness.Table 1 — Wheat Types

Content of wheat of other types, %, not more than Types Vitreuesness, %

total including I Hard red spring wheat Not less than 40 10 5 % of Durum wheat II Hard red winter wheat Not less than 40 10 5 % of Durum wheat III Hard white spring wheat Not less than 60 10 Does not take into account IV Hard white winter wheat Not limited 10 Does not take into account V Spring durum wheat Not less than 40 10 10 % of white wheat VI Winter durum wheat Not less than 40 10 5 % of white wheat VII Unclassified Wheat which do not meet any of the above mentioned

requirements (Types mixture)

2004

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4.2 Wheat, which have lost its natural colour as a result of adverse conditions during ripening, harvesting or storage at presence of dark tints is classified as “Darkening” or as “Discoloured” with mentioned Discoloration Level (GOST10967).5.3 Discoloration Level 1 is permitted for Common and Durum wheat of grades 1 and 2, Levels 1-2 – for Grade 3 and any Discoloration and Darkening Level –for common wheat of Grade 6.

4.3 Wheat, which have lost its natural colour as a result of adverse conditions during ripening, harvesting or storage is classified as “Discoloured” with mentioned Discoloration Level. Discoloration Level 1 is permitted for Common wheat of Group A, Levels 1-2 – for Common wheat of Group B and any Discoloration Level – for Grade 6.The order on use of wheat consignments with percentage of grains in which the germ is discolored more than 20% for Common wheat and more than 8% for durum wheat gives the Central enforcement authority concerning an agrarian policy of Ukraine.

TYPES. TECHNICAL SPECIFICATIONS 2004

2009

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Modifying order No. 272 of Derzhspozhyvchstandart of Ukraine dd. 29/07/2009Amendment No.2 DSTU 3768:2009Section No. 4. Item 4.3 to expound the first paragraph in such redaction:“Wheat, which have lost its natural colour as a result of adverse conditions during ripening, harvesting or storage, is classified as “Discoloured” with mentioned Discoloration Level. Discoloration Levels 1-2 are permitted for Common wheat of Groups A and B and any Discoloration Grade – for Grade 6.”

4.3 Wheat, which have lost its natural colour as a result of adverse conditions during ripening, harvesting or storage, is classified as “Discoloured” with mentioned Discoloration Level. Discoloration Levels 1-2 are permitted for Common wheat of Groups A and B, and any Discoloration Level – for Grade 6.The order on use of wheat consignments with percentage of grains in which the germ is discolored more than 20% for Common wheat and more than 8% for durum wheat gives the Central enforcement authority concerning an agrarian policy of Ukraine.

2009

2009-2010

TYPES. TECHNICAL SPECIFICATIONS

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5.4 In case of mismatch even of one parameter to wheat requirements, wheat should be transferred into the corresponding lower Grade.5.6 At the consent of grain silos and other subjects of enterprise activity wheat moisture and impurities content suppose to be above the requirements limits, under posiibility of further processing of such grain to the quality parameters noted in tables 2 and 3.____________________________________________________________________________________________________________________________________________________________

4.4 In case of mismatch even of one parameter to Common wheat requirements, Common wheat should be transferred into the corresponding Grade. In case of mismatch of gluten quantity and quality parameters to minimal requirements of Group A common wheat should be transferredinto group B under condition that other parameters to be in conformity with the quality requirements. In case of mismatch even of one common wheat parameter to Groups A and B requirements Common wheat should be transferred into Grade 6.4.5 In case of mismatch even of one parameter to Durum wheat requirements, Durum wheat should be transferred into the corresponding quality Grade.4.6 At the consent of grain silos and other subjects of enterprise activity wheat moisture and impurities content suppose to be above the requirements limits, under condition of further processing of such grain by them to the quality parameters noted in tables 1 and 2.

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4. TECHNICAL SPECIFICATIONS

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5.7 Wheat, which is prepared for export, should be in sound condition, with normal smell and color, without grain pests infestation and in accordance with requirements of Table 4.

Table 4 – The main quality parameters for common and durum wheat for export

Import and export requirements to wheat quality for Types composition, Grain and Waste impurities, wet Gluten, other parameters to be established in the contract between the supplier and the buyer.

Parameters Wheat for food purpose

Wheat for feed and other purpose

Natural weight, g/l Not less than 730 Not limited Moisture content, % Not more than 14,5 Not more than 14,5 Protein content, on dry matter basis, % Not less than 10,0 Up to 10,0

4.7 Import and export requirements to wheat quality parameters to beestablished in the contract between the supplier and the buyer.

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2009

4. TECHNICAL SPECIFICATIONS

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4.7 Import and export requirements to wheat quality parameters to beestablished in the contract between the supplier and the buyer.

4.7 In case of mismatch even of one parameter to minimal requirements of Grade 6 for common wheat and Grade 5 for durum wheat, it should be classified for account as “Non-standard” with mentioned mismatched parameter/parameters.4.8 Import and export requirements to wheat quality parameters to beestablished in the contract between the supplier and the buyer.

2009

2010

4. TECHNICAL SPECIFICATIONS

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Description and limits for Common wheat Grades Parameters

1 2 3 4 5 6 Types composition Types І - IV Types І - IV, permitted Type VIINatural weight, g/l, not less than 760 755 730 710 710 Not limited Moisture content, %, not more than 14.5 14.5 14.5 14.5 14.5 14.5

Description and limits for Common wheat Groups and Grades

А B Parameters

1 2 3 4 5 6 Natural weight, g/l, not less than 760 740 730 720 710 Not limited Vitreuesness,%, not less than 50 40 30 Not limited Moisture content, %, not more than 14.0 14.0 14.0 14.0 14.0 14.0

2004

2009Table 1 — Common wheat quality parameters

Table 2 — Common wheat quality parameters

4. TECHNICAL SPECIFICATIONS

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2009

Modifying order No. 258 of Derzhspozhyvchstandart of Ukraine dd. 15/07/2009Amendment No.1 DSTU 3768:2009Section No. 4. Item 4.4 to complement with paragraph in such redaction:“Common wheat with Natural weight of 690-710 g/l, Protein content not less than 11.0 % and Wet gluten content not less than 18 % should be transferred into Class 5. As per other parameters this wheat should meet minimal requirements of Class 5. Wheat with above mentioned quality should be stored separately.” “

2010Table 1 — Common wheat quality parametersDescription and limits for

Common wheat Groups and Grades А B Parameters

1 2 3 4 5 6 Natural weight, g/l, not less than 760 740 730 710 690 Not limited Vitreuesness,%, not less than 50 40 Not limited Moisture content, %, not more than 14.0 14.0 14.0 14.0 14.0 14.0

4. TECHNICAL SPECIFICATIONS

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Description and limits for Common wheat Grades Parameters

1 2 3 4 5 6 Grain impurities, %, not more than 5.0 5.0 8.0 10.0 15.0 15.0 In particular sprouted grains 1.0 1.0 3.0 3.0 5.0 In limits for

Grain impurities Falling number, sec, more than 200 200 150 100 less than

100 Not limited

Remark: During the determination of wheat Grade the priority is given to Falling number against sprouted grains content.

D e s c rip t ion a n d lim it s for C om m on w he a t G ro up s a n d G ra d e s

А B P a ra m e te rs

1 2 3 4 5 6 G ra i n i m p u rit ie s , % , n ot m o re th a n 5 .0 8 .0 8 .0 1 0 .0 1 2 .0 1 5 .0 I n p a r ti c ul a r: o th e r c e re a l s

4 .0

4 .0

4 .0

4 .0

4 .0

In lim its fo r

G ra in im p u ri tie s

s p r ou te d g ra in s 2 .0 3 .0 4 .0 4 .0 4 .0 In lim its fo r G ra in

im p u ri tie s F a ll ing n u m be r, s e c , n ot l e s s th a n 2 2 0 1 8 0 1 5 0 1 5 0 1 3 0 N o t l im i te d

2009

20044. TECHNICAL SPECIFICATIONS

Free translation from Ukrainian

Table 1 — Common wheat quality parameters

Table 2 — Common wheat quality parameters

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Description and limits for Common wheat Groups and Grades

А B Parameters

1 2 3 4 5 6 Grain impurities, %, not more than 5.0 8.0 8.0 10.0 12 .0 15.0 In particular: b roken grains

5.0

5.0

5.0

In limits for Gra in impurities

g rains of cereals 4.0 4.0 4.0 4.0 4.0 In limits for Grain impurit ies sprouted grains 2.0 3.0 3.0 4.0 4.0 In limits for Grain impurit ies Fall ing number, sec, not less than 220 180 150 150 130 Not lim ited

2009

2010

4. TECHNICAL SPECIFICATIONS

Free translation from Ukrainian

Table 1 — Common wheat quality parameters

Table 1 — Common wheat quality parametersD e s c rip t ion a n d lim it s for

C om m on w he a t G ro up s a n d G ra d e s А B P a ra m e te rs

1 2 3 4 5 6 G ra i n i m p u rit ie s , % , n ot m o re th a n 5 .0 8 .0 8 .0 1 0 .0 1 2 .0 1 5 .0 I n p a r ti c ul a r: o th e r c e re a l s

4 .0

4 .0

4 .0

4 .0

4 .0

In lim its fo r

G ra in im p u ri tie s

s p r ou te d g ra in s 2 .0 3 .0 4 .0 4 .0 4 .0 In lim its fo r G ra in

im p u ri tie s F a ll ing n u m be r, s e c , n ot l e s s th a n 2 2 0 1 8 0 1 5 0 1 5 0 1 3 0 N o t l im i te d

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D e s c r ip tio n a n d lim its fo r C o m m o n w h e a t G ra d e s P a ra m e te rs

1 2 3 4 5 6 W a s te im p u r it ie s , % , n o t m o re th a n 1 .5 2 .0 3 .0 4 .0 5 .0 5 .0

In p a r t ic u la r: s p o ile d g ra in s 0 .2 0 .2 0 .5 0 .5 1 .0 1 .0 fu s a r iu m a ffe c te d g ra in s 0 .3 0 .5 1 .0 1 .0 1 .0 1 .0 c o rn -c o c k le 0 .3 0 .5 0 .5 0 .5 0 .5 0 .5 m in e ra l im p u r it ie s , o u t o f w h ic h : 0 .3 0 .3 0 .5 1 .0 1 .0 1 .0 - p e b b le , s la g , o re 0 .1 5 0 .1 5 0 .2 0 .3 In lim its fo r

m in e ra l im p u r it ie s

Description and limits for Common wheat Groups and Grades А B Parameters

1 2 3 4 5 6 W aste impurities, %, not more than 1.0 2.0 2.0 2.0 2 .0 5.0 In particular: mineral impurities, out of which:

0.3

0.5

0.5

0.5

0 .5

1.0

- pebb le, slag, ore 0.15 0.15 0.2 0.15 0 .2 In limits for mineral impurities

spoiled grains, out of which: 0.3 0.3 0.5 0.3 0 .5 1.0 - fusarium affected grains In limits for spoiled grains

2004

2009-2010

4. TECHNICAL SPECIFICATIONS

Free translation from Ukrainian

Table 1 — Common wheat quality parameters

Table 2 — Common wheat quality parameters

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D e s c r ip t io n a n d l im i ts f o r C o m m o n w h e a t G r a d e s P a r a m e te r s

1 2 3 4 5 6 h a r m fu l im p u r it i e s , o u t o f w h ic h : 0 .2 0 .3 0 .5 0 .5 0 .5 0 .5

s m u t a n d e r g o t 0 .0 5 0 .0 5 0 .1 0 .1 0 .1 0 .1 H a r d h e a d s , D a r n e l , S ta g g e r b u s h , F a ls e L u p in ( in to ta l ) 0 .0 5 0 .0 5 0 .1 0 .1 0 .1 0 .1 C o r o n ill a 0 .1 0 .1 0 .1 0 .1 0 .1 0 .1 H e li o t r o p e 0 .1 0 .1 0 .1 0 .1 0 .1 0 .1 T ri c h o d e s m a i n c a n u m N o t p e rm i t te d

Descrip tion and lim its for Com mon wheat Gr oups and G rades

А B P aram eters

1 2 3 4 5 6 harmful impurit ies, out of whic h: 0.2 0 .2 0.2 0.2 0.2 0.5 - s mut and ergot 0.05 0. 05 0.05 0.05 0.05 0.1 - T richod esma incanum Not permit ted - Corn-c ock le In lim its for harmf ul imp uri ties - each of any other t oxic se eds 0.05 0. 05 0.05 0.05 0.05 0.1

2004

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4. TECHNICAL SPECIFICATIONS

Free translation from Ukrainian

Table 1 — Common wheat quality parameters

Table 2 — Common wheat quality parameters

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Description and limits for Common wheat Groups and G rades

А B Para meters

1 2 3 4 5 6 S mutty grains, %, not m ore than 5.0 5.0 8.0 5.0 8.0 10.0

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4. TECHNICAL SPECIFICATIONS

Free translation from Ukrainian

Table 1 — Common wheat quality parameters

Table 2 — Common wheat quality parameters

Param eters Description and lim its for Com m on w heat G rades

1 2 3 4 5 6 Sm utty grains, % , not m ore than 5.0 5.0 5.0 8.0 8.0 10.0

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2009-2010D escri ption an d l im its for

D u ru m w h eat G rad es Param eter s 1 2 3 4 5

C om m on w h eat gra in s, % , no t m ore than 4 4 8 10 Not l im i ted N atur a l w eigh t , g /l, no t l es s t ha n 750 750 730 710 Not l im i ted M oi stu re c onte nt, % , no t m ore than 14 .5 14 .5 14 .5 14 .5 14 .5 V itre ue sn es s,% , no t les s t han 70 60 50 40 Not l im i ted G r ain im p uri ties , % , no t m ore t han 5 .0 5 .0 8 .0 10 .0 15 .0 In part icu la r: sp rou ted g rai ns

1 .0

1 .0

3 .0

3 .0

In l im it s fo r

Grai n im purit ies W aste im p ur itie s, % , no t m ore than 2 .0 2 .0 2 .0 5 .0 5 .0 In part icu la r: m ineral im purit ies , ou t o f w hi ch :

0 .3

0 .3

0 .5

0 .5

1 .0

- pebb l e, sl ag , o re 0 .15 0 .15 0 .2 0 .3 In l im it s fo r m i neral i m puriti es

spo il ed g rains , ou t o f whi ch : 0 .2 0 .2 0 .5 1 .0 1 .0 - fusarium a ffecte d g rains In li m it s fo r spo ile d gra ins harm fu l im puri tie s, ou t o f w h ich : 0 .2 0 .3 0 .5 0 .5 0 .5 - sm ut a nd e rgot 0 .05 0 .05 0 .1 0 .1 0 .1 - Tri chodesm a in canum Not perm it ted - C orn-cock l e In lim its fo r harm fu l im purit ies - ea ch of any o ther t ox ic s eeds 0 .05 0 .05 0 .05 0 .05 0 .1 S m u tty gra in s , % , no t m ore t han 5 .0 5 .0 5 .0 5 .0 10 .0 P rotei n con ten t (on d ry m atte r b as is ), % , n o t l es s t han

14 .0

13 .0

12 .0

11 .0

No t l im i ted

F all in g n um b er , se c, not le ss t han 200 200 150 100 Not l im i ted

Table 2 — Durum wheat quality parameters

4. TECHNICAL SPECIFICATIONS

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4.9 Pesticides residues content in wheat should not exceed the norms stipulated in МBP&СН 5061 [1] and DSanPiN 8.8.1.2.3.4-000 [2].4.10 Radionuclides content in wheat should not exceed levels established in GN 6.6.1.1-130 [3].4.11 Poisonous materials content in wheat should not exceed maximum admissible levels noted in table 3.

P a r a m e t e r N o r m M e t h o d T o x i c e l e m e n t s , m g / k g :

L e a d 0 . 5 I n a c c o r d a n c e w it h G O S T 2 6 9 3 2 a n d G O S T 3 0 5 3 8 C a d m iu m 0 . 1 I n a c c o r d a n c e w it h G O S T 2 6 9 3 3 a n d G O S T 3 0 5 3 8 A r s e n i c 0 . 2 I n a c c o r d a n c e w it h G O S T 2 6 9 3 0 a n d G O S T 3 0 5 3 8 M e r c u r y 0 . 0 3 I n a c c o r d a n c e w it h G O S T 2 6 9 2 7 a n d G O S T 3 0 5 3 8 C o p p e r 1 0 . 0 I n a c c o r d a n c e w it h G O S T 2 6 9 3 1 a n d G O S T 3 0 5 3 8 Z in c 5 0 . 0 I n a c c o r d a n c e w it h G O S T 2 6 9 3 4 a n d G O S T 3 0 5 3 8 M y c o to x i n e s , m g / k g A f l a t o x i n В 1 0 . 0 0 5 I n a c c o r d a n c e w it h М Р 2 2 7 3 [ 4 ] , М Р 4 0 8 2 [ 5 ] , D S T U Е N 1 2 9 5 5Z e a ra l e n o n e 1 . 0 I n a c c o r d a n c e w it h М Р 2 9 6 4 [ 6 ]

Т -2 t o x in 0 . 1 I n a c c o r d a n c e w it h М P 3 1 8 4 [ 7 ]

D e o x y n iv a le n o l ( V o m it o x in ) 0 . 5 I n a c c o r d a n c e w it h М P 3 9 4 0 [ 8 ] , М U 5 1 7 7 [ 9 ]

O c h r a t o x i n А 0 . 0 0 5 I n a c c o r d a n c e w it h D S T U Е N І S О 1 5 1 4 1 - 1 , D S T U Е N І S О 1 5 1 4 1 - 2

R a d io n u c li d e s , B q / k g :

S t r o n t i u m - 9 0 C a e s iu m - 1 3 7

2 0 5 0

М U № 5 7 7 8 [ 1 0 ] М U № 5 7 7 9 [ 1 1 ]

P e s t i c i d e s T h e l is t o f p e s t ic i d e s , w h i c h c o n t e n t t o b e c o n t r o ll e d in w h e a t , d e p e n d s o n t h e ir u s e in c e r t a i n t e r r i t o ry a n d t o b e a p p ro v e d b y t h e a u t h o r it i e s o f M in is t r y o f H e a l t h a n d V e t e r i n a r y M e d ic in e o f U k r a in e

Table 3 – Maximum admissible levels of toxic elements, mycotoxines, radionuclides and pesticides content

2009-20104. TECHNICAL SPECIFICATIONS

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5.1 Control over the emission of noxious pollutants to the atmosphere is to be exercised according to GOST 17.2.3.02, DSP 201 [12].

5.2 The environmental protection requirements at grain acceptance, transportation and storage of wheat should be observed in accordance with GOST 12.1.005, requirements laid down in “Rules of Accident Prevention and Industrial Sanitation on Storing and Processing Enterprises of the Ministry of bread products of the USSR”, №99 [13], other normative and legal documents in force.

5.3 Soil protection against contamination with consumer and production waste is to be performed according to SanPiN 42-128-4690 [14].

5. SAFETY AND ENVIRONMENT PROTECTION REQUIREMENTS

2009-2010

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7.1 Acceptance control rules are in accordance with GOST 13586.3.7.2 Wheat condition, smell, color, vitreuesness, types composition, natural weight, moisture, grain and waste impurities content, insects infestation, protein and wet gluten content, wet gluten quality and falling number to be determined in each wheat consignment.7.3 Wheat in which the content of other cereals and pulses is over 15 % from the total grain mass, to be accepted as a mixture of wheat with other cultivated plants with its composition mentioned in percents.

6.1 Acceptance control rules are in accordance with GOST 13586.3.Extraneous subjects (stones, pieces of metal, wood, etc.) have been observed during intake, outtake and storage should be withdrawn.6.2 Wheat condition, smell, color, vitreuesness, natural weight, moisture, grain and wasteimpurities content, insects infestation, bug-ridden grains, smutty grains, protein and wet gluten content, wet gluten quality and falling number to be determined in each wheat consignment. Safety parameters to be determined in accumulated consignments.6.3 Wheat in which the content of other cereals and pulses is over 15 % from the total grain mass together with impurities, to be accepted as a mixture of wheat with other cultivated plants with its composition mentioned in percents.

6. ACCEPTANCE CONTROL RULES2004

2010

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7.4 Control and periodicity of the toxic elements, mycotoxines and pesticides content control in wheat used for food, technical purpose and for export is provided in accordance with Procuderal Direction “Order and periodicity of food raw materials and foodstuff control for safety parameters” [6], and for feed purpose in accordance with Procuderal Guidelines “Order and periodicity of mixed fodders and mix fodder raw materials control for safety parameters” [7].7.5 Each wheat cinsignment to be accompanied with (except for for commodity producers) with pesticides, toxic elements, mycotoxines and radionuclides content certificate.

6.4 Control of the toxic elements, mycotoxines, pesticides residues and radiologicalparameters content is carried out by state structures in accordance with current legislation and determinate order.6.5 Periodicity of the toxic elements, mycotoxines, pesticides residues and radiologicalparameters content control – in accordance with МР 4.4.4-108 [15].6.6 If wheat consignment, by results of visual or acceptance control, does not meet specified quality requirements and can not be divided into homogeneous parts, it should be returned.6.7 In case of unsatisfactory results of analysis even on one of parameters, re-testing on thedouble quantity of the samples, drawn from the same wheat consignment, to be provided. Results of re-testing are final and apply to the total consignment. 2010

2004

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6. ACCEPTANCE CONTROL RULES

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7. METHODS OF QUALITY PARAMETERS DETERMINATION

Having regard to the adoption of new and cancellationof old DSTU and GOST versions section references

were revised and modified in accordance with normative documents currently in force

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7.1 Grain sampling shall be carried out in accordance with DSTU 3355, DSTU ISO 13690, and GOST 13586.3.

7.2 Odor, color and grain discoloration shall be determined in accordance with GOST 10967.

7.3 Hectolitre weight shall be determined in accordance with DSTU 4233, DSTU 4234, GOST 10840 (arbitral).

7.4 Vitreuesness shall be determined in accordance with GOST 10987.7.5 Moisture content shall be determined in accordance with DSTU 4117,

DSTU GOST 29144, GOST 29143, GOST 13586.5 (arbitral).7.6 Grain, waste, harmful impurities, smutty grains and bug-ridden grains

content shall be determined in accordance with GOST 30483 and Annexes A and B.

2010

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7. METHODS OF QUALITY PARAMETERS DETERMINATION

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Annex А (normative)THE ORDER OF WHEAT TESTING FOR IMPURITIES CONTENT

A.1 A test portion of 250 g shall be passed for half a minute through the sieve with long rounded apertures of 1.0 x 20.0 mm in accordance with GOST 30483 (3.1.2).

The matter that passing through the sieve shall be weighed and included in mineral impurities.

A.2 Broken grains, overheated grains, grains of cereals, sprouted grains, grains eaten by pests, grains in which the germ is discolored, grains damaged by frost and unripe grains (green), mineral, organic, harmful impurities and spoiled grains must be extracted from the matter retained by the sieve.

A.3 After elimination from the sample of all the above mentioned matter the partial sample shall be passed for half a minute through a sieve with long rounded apertures of 2.0 x 20.0 mm.

All the matter which passes through the sieve with long rounded apertures of 2.0 x 20.0 mm shall be weighed and considered as small and shrunken grains.

A.4 Shrivelled grains content shall be determined as sum of grains damaged by frost, unripe grains (green), small and shrunken grains content in percents.

A.5 Smutty grains and bug-ridden grains shall be determined in accordance with GOST 30483 requirements.

2010

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2010

Annex А (normative)

Test portion of 50 g

The first sieving (30 seconds)

Fines (to minera l im purities)

In the matter r etained:

– minera l im purities;

– organic impurities;

– harmful impurities;

– spoiled grains

The second sieving (30 seconds)

The matter passed (small and shrunken grains)

sieve 1.0 х 20.0 mm In the matter r etained:

– broken grains;

– sprouted grains;

– overheated grains;

– grains of cerea ls;

– grains eaten by pests;

– gra ins in which the germ is

discolored ;

– grains damaged by frost;

– unripe grains (green )

sieve 2.0 х 20.0 mm

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7.7 Protein content shall be determined in accordance with DSTU 4117, GOST 10846 (arbitral).

7.8. Gluten quantity and quality (IDK) shall be determined in accordance with DSTU 4117, DSTU ISO 21415-1, DSTU ISO 21415- 2, GOST 13586.1(arbitral).

7.9 Falling number shall be determined in accordance with GOST 30498(arbitral), GOST 27676.

7.10 Grains infestation by pests shall be determined in accordance with DSTU ISO 6639-1, DSTU ISO 6639-2, DSTU ISO 6639-3, DSTU ISO 6639-4, GOST 13586.4.

7.11 Toxic elements, mycotoxines, radionuclides and pesticides content shall be determined in accordance with normative documents listed in Table 3 and in accordance with other methods, approved by the Central Executive Authority in the field of health protection.

Decomposition of sample for toxic elements determination shall be carried out in accordance with GOST 26929.

2010

7. METHODS OF QUALITY PARAMETERS DETERMINATION

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8 TRANSPORTATION AND STORAGE8.1 Wheat is transported in bulk using any type of transport means in accordance with the transportation rules requirements to the particular type of transport selected. 8.2 Transport means should be clean, without any foreign odour. Wheat grain should be protected against precipitations during loading, transportation and unloading.8.3. Wheat is to be placed and stored in clean and dry granaries, which are free from foreign odour and infestation and correspond to operating sanitary rules approved in accordance with established procedure, and storage conditions mentioned in “Instructions on grain, oilseeds, flour and groats storage” [16].

9. SUPPLIER’S WARRANTEESSupplier shall guarantee conformance of wheat to requirements of the present standard if storing and transportation conditions are met.

2010

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Annex F (informative)BIBLIOGRAPHY

References were modified in accordance with revision of normative documents currently in force

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THANKS FOR THANKS FOR YOUR YOUR ATTENTIONATTENTION!!