Tests of Soil and Bitumen

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    MATERIAL TESTING AND THEIR SIGNIFICANCE

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    Soil1.Grain Size Analysis2.Atterbergs Limit3.Compaction Test4.Free Swell Index5.Direct Shear6.

    California Bearing Ratio

    7.Tri-Axial Compression Test

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    Grain Size Analysis(IS 2720: part 4)

    PURPOSE

    The commonly used properties for classification of soil are the grain

    size distribution and atterbergs limits which are also used to determine

    the suitability of soil as a sub-grade material and other purposes.

    The soils are generally divided into four groups based on their particle

    size Gravel: coarser particles of rock and sand between 80mm and

    4.75mm

    Sand: smaller fraction of particles between 4.75mm and 75micron Silt: soil fractions smaller than 75 micron are called fines which

    consist of silt and clay.75 micron to 2 micron is silt

    Sand: microscopic and sub-microscopic particles lower than 2micron is clayey particles.

    Dry sieve analysis is generally carried out on coarse aggregates or sandy

    soil either retained or passing through 4.75 mm sieve if they are

    cohesion less and without lumps. Otherwise wet sieve analysis is

    conducted.

    Wet sieve analysis is carried if the sample contains cohesive lumps and

    it is not possible to break them into their respective grain size by any

    pulverizing methods. Soils with fractions which are likely to causeflocculation are added with 2 gm of sodiumhexameta-phoshate or 1 gm

    of sodium hydroxide / sodium carbonate as a dispersing agent and left

    for soaking.

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    Uniformity coefficient U, is expressed as (D60 /D10 ), where D60 and D10

    are particle size corresponding to 60 % and 10% fines in the grain size

    distribution curve. A high value of uniformity coefficient such as U

    greater than 4 or 5 indicates the presence of wide range of particle sizeor soil is well graded. A low U of the order of lower than 2 indicates

    uniformly graded soil

    Soil classification

    Ordinarily sieve analysis (dry/wet) will be quite sufficient along with the

    tests for consistency limits for identifying and classifying soil.

    Proportioning soils for mixed designThe principle of mechanical soil stabilization is to mix two or more

    number of selected soils and gravels or aggregates in a suitable

    proportion that a desired grain size distribution is obtained for the

    combined materials as per mix design

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    ATTERBERG`S LIMIT(IS 2720 PART 5 & 6)

    PURPOSE

    The physical properties of fine grained soils, especially of clayey soils

    differ considerably at different water contents present in soil. The tests

    for determination of consistency limits are all empirical.

    Liquid Limit: It is defined as the minimum water content at which the

    soil will flow under the application of a very small shearing force.

    Plastic Limit: It is defined as the minimum water content at which soil

    remains in a plastic state and posses moulding characteristics.

    Shrinkage Limit: it is defined as the maximum water content at which

    further reduction in water content does not cause reduction in volume.

    LIQUID LIMIT TEST (By cone penetration one point method)

    In the case of soils whose liquid limit exceeds by 120% in case of one

    point method mechanical method should be used.

    PRINCIPLE

    Since the depth of penetration is in an indirect reflection of shear

    strength at different water contents, it has been found, within the

    framework of a scientific base that W/WL against logD or D is unique

    and is independent of soil type. The resulting linear relation enables to

    determine liquid limit water content at specified penetration of 20 mm

    depth.

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    CALCULATION

    The water content is determined for any accepted trial and the liquid

    limit water content is calculated by any one of the following

    relationships.

    WL = WN / 0.77 LogD

    WL = WN / (0.65 + 0.0175 D)

    The liquid limit of the sample shall be reported to first decimal place

    and history of the sample that is natural state, oven dried, or any

    pretreatment done should be mentioned.

    Shrinkage Limit of remoulded sample, Ws = w (v- vo/wo)100

    where

    Ws = shrinkage limit in percent,

    w = moisture content of wet soil pat

    V = volume of wet soil pat in ml,

    Vo = volume of dry soil pat in ml, and

    Wo - weight of oven-dry soil pat in g.

    Application of consistency limits

    Identification and classification of soils

    Compressibility

    Plasticity index

    Application of data in the construction of highway material

    Group index method of classifying sub grade soil

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    COMPACTION TEST

    PURPOSE

    Compaction of a soil is a mechanical process by which the soil particles

    are constrained to be packed more closely together by reducing air

    voids. Soil compaction decreases air voids and consequently increases

    dry density. This may result in increase in shear strength. The possibility

    of future settlement or compressibility decreases and also the tendency

    for subsequent changes in moisture content decreases.

    Light compaction is done filling the mould in three equal layers and

    compacted by 2.6 kg hammer with 25 blows in small mould and 55

    blows in large mould of 150 mm diameter

    Heavy compaction is done by filling the mould in 5 layers and

    compacting by 4.9 kg hammer with 25 blows each in small mould of

    100 mm diameter and 55 blows in large mould of 150 mm diameter.

    RESULT

    Moisture- dry density graph is plotted with moisture content on the X

    axis and dry density on Y axis and a smooth curve is drawn connectingthe points, which is called compaction curve.

    From this curve, the maximum density is noted and the corresponding

    value of moisture content is taken as optimum moisture content OMC

    DISCUSSION

    The objective of the compaction test is to determine the relationship

    between compacting moisture content and dry density achieved for the

    soil keeping the compacting energy per unit volume constant.

    Therefore to increase the accuracy of results the volume to be struck

    off from the collar should not be very different in each case and it

    should be like 6 mm of soil should be there after removing the collar to

    be struck off to get good reproducibility.

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    APPLICATION OF COMPACTION TEST

    In field compaction the compacting effort is first controlled at OMC and

    the adequacy of compaction is checked by checking the dry density

    achieved

    The results are used for quality control in the construction of

    pavements as IRC and MORTH recommends achieving 97% of the dry

    density achieved in heavy compaction in sub-grade layer and 95% in

    compacted embankments.

    Suitability of the soil to be used in highway work is based on the

    specified minimum value of dry density achieved in compaction test. As

    per MORTH for deciding suitability of soil to be used as sub-grade, themaximum dry density should not be less than 1.75 g/cc

    The maximum dry density indicates the strength property of the soil,

    lower the dry density it indicates weaker is the soil although it is just

    qualitative idea quantification is done by conducting strength tests.

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    SHEAR TESTS ON SOILS(IS 2720 part 11, 12, 13)

    PURPOSE

    The strength parameters namely the cohesion and the angle of internalfriction or shearing resistance of soils are usually found from the shear

    tests. Two commonly used methods are direct shear test and triaxial

    compression test

    DIRECT SHEAR TEST

    In this test the soil specimen is placed in the shear box between two

    halves and a normal load is applied. Then a longitudinal displacementor the shear force is applied and its magnitude is increased until the

    specimen fails along the predetermined horizontal plane between the

    two halves of shear box

    By repeating the direct shear test at different magnitudes of normal

    load, a graph is plotted with normal stress values on the X-axis and the

    shear stress values on Y-axis. The value of cohesion C, and the

    magnitude of angle of internal friction are obtained from the graph

    DISCUSSION

    The main advantage of direct shear test is its simplicity and less time

    consuming in comparison to tri axial. But it is also associated with some

    disadvantages as follows

    The failure is forced to take place along pre determined horizontalplane not the weakest plane

    The area of cross section of specimen progressively decreases during

    the test.

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    There is no uniform shear stress distribution within the failure plane

    and drainage conditions are not controlled

    TRI-AXIAL COMPRESSION TEST

    In triaxial test the load applied is mostly transient and it is carried out

    on the soil having more cohesive properties

    APPLICATIONS

    The shear strength parameters C and internal friction can be found and

    thus shearing resistance can be found out

    Elastic modulus values or modulus of deformation values of sub grade

    and other pavement layer materials are determined from tri axial test.

    The unconfined compression test is considered to be the special case in

    which lateral confining pressure is zero.

    FREE SWELL INDEX

    PURPOSE

    Free swell index is conducted on soils which have the potential to swell.

    It is desirable to carry out further detailed investigations on soils with

    high free swell index.

    DISCUSSION

    The volume of the soil sample in the jar is noted as Vk and water as Vw

    than FSI = 100* (Vw - Vk )/Vk

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    CALIFORNIA BEARING RATIO

    PURPOSE

    The CBR test denotes a measure of resistance to penetration of a soil orflexible pavement material of standard plunger under controlled test

    conditions. It is a method for evaluating the strength of sub grade soil

    and other pavement materials for the design and construction of

    flexible pavements.

    DISCUSSION ON RESULTS

    The CBR values at 2.5 and 5.0 mm penetration levels are calculated foreach specimen from the corresponding graphs. Generally the CBR value

    at 2.5 mm penetration is higher but if the value is higher at 5.0 mm

    than test is repeated and If still it is higher than higher value is adopted.

    The initial concavity of the load penetration curve calling for the

    correction may be due to one or more of the following reasons:

    The top layer of soaked soil specimen is too soft or slushy after soakingin water.

    The top surface of the specimen is not even.

    The penetration plunger of the loading machine is not vertical result in

    bottom surface of plunger not being horizontal and fully in contact with

    the top surface of specimen.

    APPLICATIONS

    Based on CBR data collected, empirical design charts were developed

    by the California state highway department, correlating the CBR value

    and pavement thickness requirement.

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    AGGREGATES1.Aggregate Impact test2.Los Angeles Abrasion test

    3.Specific gravity and water absorption test

    4.Shape test

    5.Soundness test

    6.Stripping value test

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    Aggregate Impact test(IS 2386 Part 4)

    PURPOSE

    Toughness is the property of the material to resist impact. During the

    construction process of pavement layers, particularly compaction by

    heavy rollers and also due to movement of heavy wheel loads of traffic,

    the road aggregates are subjected to impact therefore stone aggregates

    should therefore be sufficiently tough to resist fracture under impact

    loads.

    DISCUSSION

    Aggregate impact value test of a sample not only depends on

    toughness and strength parameters it also depends on the shape

    factors such as flakiness and elongation of the aggregates

    APPLICATION

    The aggregate impact test is considered to be an important test to

    assses the suitability of the aggregated as regards the toughness for usein various constructional purpose mainly highway.

    RESULTS

    It is expressed as percentage of finer material passing 2.36 mm IS sieve

    after test to original weight.

    Aggregate impact value Toughness property

    Less than 10 Exceptionally strong/tough

    10 to 20 Very tough

    20 to 30 Good for pavement construction

    Above 35 Weak for pavement construction

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    LOS ANGELES ABRASION TEST(IS 2386 part 4)

    PURPOSE

    Due to movement of traffic, the road stones are used in the surfacingcourse of pavements are subjected to wearing action at the top surface.

    Resistance to wear or hardness is hence a essential property for road

    aggregates especially when used in wearing course. Thus road stones

    should be hard enough to resist the wearing under heavy traffic loads.

    RESULT

    The result is expressed as a percentage wear and the average value of

    the two test. Percentage wear is the amount of fines to the originalweight passing through 1.70 mm IS sieve

    DISCUSSION

    Los angeles test is very commonly used to evaluate the quality of

    aggregates for use in pavement construction, especially to decide

    hardness of aggregate M

    Maximum allowable los angeles abrasion value of aggregates given by

    MORTH for different layers is given in the tableTypes of pavement layer Los angeles abrasion value,

    maximum

    WBM sub-base, WBM, WMM and

    CRM base course

    40Bituminous macadam and binder

    course

    Dense graded bituminous

    macadam binder

    Dense graded bituminous

    macadam binder course 35

    Cement concrete pavement

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    SPECIFIC GRAVITY AND WATER ABSORPTION(IS 2386 PART 4)

    PURPOSE

    The specific gravity of an aggregate is considered to be measure ofstrength or quality of the material. Stone having low specific gravity are

    generally weaker than those with higher specific gravity values. The

    specific gravity is made to use in weight-volume conversions.

    CALCULATION

    Specific gravity, apparent specific gravity and water

    Absorption shall be calculated as follows:

    Specific gravity= (dry weight of aggregate)/(weight of equal volume of

    water)

    Water absorption (percent of dry weight) = % by weight of water

    absorbed in terms of oven dried weight of aggregates

    DISCUSSION AND APPLICATION

    The water absorption test does not always gives reproducible results inaggregates with high porosity.

    The specific gravity of coarse aggregates used in road construction

    ranges from 2.5 to 3.2 with an avg value of 2.70.

    Water absorption is accepted as measure of its porosity. Sometimes

    this value is even considered as a measure of its resistance to frost

    action though not has been confirmed by adequate research.

    Water absorption of about 0.1 to 2.0 percent for coarse aggregates

    normally used in road construction.

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    SHAPE TEST(IS 2386 part 1)

    PURPOSE

    The shape of aggregate particle is determined by the percentage of

    flaky and elongated particles contained in it. Presence of flaky particles

    in the construction is undesirable as they may cause weakness with

    possibilities of breaking down under loads.

    APPLICATION

    In the road construction work MORTH has specified the limits of

    flakiness index and elongation index. Though elongated shape of

    aggregates also gets broken down under heavy rollers duringcompaction and also during compaction under heavy traffic load.

    MORTH has specified the maximum permissible value of combined

    flakiness and elongation index of coarse aggregates as 30% for WMM

    base course and other

    SOUNDNESS TEST

    (IS 2386 PART 5)PURPOSE

    Soundness test is intended to study the resistance of course and fine

    aggregates to weathering action. In the absence of adequate

    information the laboratory test simulation accelerated weathering

    condition is carried out to judge the durability or the soundness of the

    course aggregates.

    DISCUSSIONIf the sample contains less than 5% of any of the sizes specified under

    procedure that size should not be tested, but for the purpose of testing

    it shall be considered to have the loss in sodium sulphate or magnesium

    sulphate treatment as the avg of next smaller or next greater size

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    APPLICATION

    The soundness test is useful to asses the resistance of the aggregates to

    weathering. For cement concrete likely to be exposed to the action of

    frost, coarse, and fine aggregates should pass an accelerated soundness

    test. As a general rule, it may be taken that the avg loss of weight after

    10 cycles should not exceed 12% with sodium sulphate and 18% with

    magnesium sulphate

    Indian road congress has specified maximum permissible loss in weight

    in soundness test after 5 cycles as 12% with sodium sulphate and 18%

    with magnesium sulphate for the aggregates to be used in bituminous

    binder course and surfacing of road pavements.

    STRIPPING VALUE(IS 6241)

    PURPOSE

    Stripping of coated binder or detachment of a portion of bitumen

    coating from the aggregate due to the presence of water. So to

    measure and deal with this problem test is conducted to calculate

    stripping value. The stripping is due to the fact that those aggregateshave higher affinity towards water than bituminous binders and this

    displacement of bituminous coating from the aggregates depends on

    the physio-chemical forces acting on the system. Most road aggregates

    are electrically charged for example silica, a common constituent of

    igneous rock posses a weak negative charge and hence have a higher

    affinity for polar compounds like water

    DISCUSSIONThe stripping value is the ratio of uncovered area observed visually to

    the total area of aggregates in each test, expressed as percentage.

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    BITUMEN1.Penetration Test

    2.Ductility Test

    3.Viscosity Test

    4.Softening Point Test

    5.Flash and Fire Point Test

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    PENETRATION TEST(IS 1203)

    PURPOSE

    Determination of absolute viscosity is not so simple therefore theconsistency of these materials are determined by indirect methods.

    Penetration test is indirect method to determine consistency by

    measuring the depth to which a standard needle will penetrate

    vertically under its own weight. Thus the basic principle of the

    penetration test is the measurement of the penetration.

    DISCUSSION

    It may be noted that the penetration value is influenced by anyaccuracy as regards of following factors

    Pouring temperature, size of needle, weight placed on needle, test

    temperature, duration of releasing the penetration needle, period of

    cooling etc.

    APPLICATION

    It is most commonly adopted test to determine the grade of the

    material in terms of its hardness.Penetration test is empirical test and there is no direct relation to the

    fundamental properties of binder.

    DUCTILITY TEST(IS 1208)

    PURPOSE

    It is desirable that the bitumen binders used in the bituminous mixes

    form ductile thin films around the aggregates. The binder material

    which posses sufficient ductility would crack and thus provide pervious

    pavement surface

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    DISCUSSION

    The ductility value gets seriously affected if any of the following factors

    are varied

    1.Test temperature2.Pouring temperature3.Diameter of briquette, particularly the cross section at the

    minimum width should be 10x10 mm

    4. Improper level of briquette placement or the stretched thread ofspecimen touching the top or bottom surface of water bath

    5.Rate of pulling6.Period of cooling

    APPLICATIONS

    A certain minimum ductility is considered essential because of the temp

    change in the bitumen mix and the repeated deformations that occur. If

    the bitumen is low in ductility pavement may crack and lead to failure.

    VISCOSITY TEST(IS 1206 PART I, II, III)

    Viscosity of a liquid is the property that retards its flow due to internal

    friction and it is a measure of resistance to flow of the liquid. The

    viscosity is of two types as

    ABSOLUTE VISCOSITY: the ratio between the applied shear stress and

    the rate of shear is called the absolute viscosity measured in poise.

    KINEMATIC VISCOSITY: it is the ratio of the absolute viscosity to the

    density of the liquid, both at the same temperature measured instokes.

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    APPLICATIONS OF ABSOLUTE AND KINEMATIC VISCOSITIES

    Previously grading of bitumen is done as per the penetration test but

    now more rational methods are available to categorize bitumen

    material known as VISCOSITY GRADING (VS)

    SOFTENING POINT TEST(IS 1205)

    PURPOSE

    Bitumen does not suddenly change from solid to liquid state, but as the

    temperature increases it becomes softer until it flows readily.the

    softening point is the temperature at which the substance attains

    particular degree of softening under specified condition of test. And asall bitumen mixes are required to be soft and flowable so as to make

    possible their mixing with aggregates

    DISCUSSION

    To ensure the credibility of the test the following conditions should be

    taken care of:

    1.Quality and type pf liquid in the bath2.Weight of balls3.Distance between bottom ring and bottom base plate4.Rate of heating

    APPLICATIONS

    Softening point thus gives an idea of the temperature at which the

    bituminous material attains a certain viscosity. Bitumen with higher

    softening point may be preferred in warmer places.it is also used to

    sometimes specify hard bitumens and pitches

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    FLASH AND FIRE POINT TEST(IS 1209)

    PURPOSE

    Flash point test gives an indication of the critical temperature at andabove which suitable precautions should be taken while heating the

    bitumen.

    FLASH POINT: it is the minimum temperature at which bituminous

    binder starts emitting the volatile vapours and these volatile vapours

    can momentarily catch fire though the binder does not burn itself.

    FIRE POINT: on further heating it is the lowest temperature at which

    application of test flame causes the binder material to ignite and burn

    atleast for 5 seconds under specified conditions.