Teledyne Analyser

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    Series 6000

    Ultraviolet Photometric Analyzer

    Built for Reliability and Performance

    TELEDYNEANALYTICAL INSTRUMENTS

    T

    eledynes Series 6000 Microprocessor Controlled

    Ultraviolet Photometer is designed to provide

    continuous on-line analytical data of critical processconditions and eliminate time consuming laboratory

    analysis. This analyzer can be configured to

    measure at any wavelength within the ultraviolet

    or visible portions of the electromagnetic energy

    spectrum.

    Since numerous gases and liquids have a useful

    absorbance peak in the ultraviolet region, a wide

    variety of applications are possible.

    Advantages Dependable microprocessor-controlled analysis

    Auto calibration and auto ranging

    Continuous real time analysis

    Eliminates time-consuming lab analysis

    Features

    Microprocessor based, high resolution, ultra stable

    electronics (no potentiometers)

    Three user-selectable ranges

    Signal & Range ID output: 0-1 VDC and 4-20 mADC

    (isolated)

    Programmable auto ranging

    Range ID contacts (quantity 4) Form A normally open

    contacts, 3A@250 VAC resistive

    Two adjustable concentration alarm set points with

    programmable relay function Form C contacts,

    3A@250 VAC resistive

    Programmable auto calibration with mode ID Form A

    normally open contacts

    Remotely operated calibration (customer suppliedvalves and 24 VDC signal)

    Self diagnostics with Form C failure contacts

    Full duplex RS232 communication link

    Alphanumeric VF display for set-up and diagnostics

    Power: 115/230 VAC 50/60 Hz

    Principle of Operation

    The analyzers optical path (figure 1) consists of a

    UV source, sample cell, and detector. A filter wheel

    located in front of the detector continuously rotates

    a reference and measuring filter in and out of the

    optical path.

    The material of interest continuously flows through

    the sample cell where the optical energy is absorbed

    at the various wavelengths in accordance with its

    composition. The analyzer utilizes the reference

    wavelength to compensate for extraneous

    phenomena (turbidity, dirt on optics, source drift,

    etc.) thereby producing a high degree of stability

    over long periods.

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    Flourescence ProbeOil-in-Water Analyzer

    MODEL 6650Flourescence ProbeOil-in-Water Analyzer

    TELEDYNEANALYTICAL INSTRUMENTS

    Built for Reliability and Performance

    Teledynes Model 6650is comprised ofa versatile transmitter and probe

    for monitoring oil-in-water in

    various reneries, power plants,

    and offshore platforms. The

    system incorporates state-of-

    the-art electronics and a ber

    optic based, in-situ probe thatdetects oil-in-water.

    Detection of oil-in-water

    in process boilers, cooling

    towers, reneries, and offshore

    platforms is an important

    measurement from an economic

    and environmental standpoint.

    This new technology from Teledyne makes

    this measurement simple, and reduces the

    cost of ownership. Because of its in-situ

    measurement capabilities, the Model 6650

    analyzer offers real time analysis within a

    second.

    Features

    * Direct measurement; no interference from

    turbidity

    No spare part replacements required for

    3 years

    Long life UV lamp

    Virtually no drift

    No inner lter error effects

    Fiber Optic Probe

    The Model 6650 uses a ber optic

    based, in-situ probe that monitors actual

    concentrations of oil-in-water using UV

    uorescence technology. TAI also offers an automatic

    retractor as an option for cleaning the probe,

    depending upon the application.

    Model 6650 Transmitter

    Teledynes 6650 uses a highly versatile

    transmitter that measures the signal fromour probe and sends the signal back to the

    transmitter. This reading is based on the

    amount of optical attenuation from the ber

    optic in-situ probe.

    The transmitter is compact and designed

    to connect to the probe via two ber optic

    cables. A local digital display is provided and the

    transmitter offers a 4-20 mA output signal to other

    devices. In addition,

    the transmitter

    is equipped with

    automatic calibration

    checking. A reference

    lter is inserted into

    the measuring beam

    either locally or

    remotely to verify operation of the transmitter.

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    Model 6650 Oil-In-Water Analyzer

    2005 Teledyne Analytical Instruments, A Teledyne Technologies Company.All rights reserved. Printed in the USA. 11/05LD

    Warranty

    Instrument is warranted for 1 year against defects in materialor workmanship

    NOTE: Specifications and features will vary with application. The above are establishedand validated during design, but are not to be construed as test criteria for every product.All specifications and features are subject to change without notice.

    TELEDYNE

    ANALYTICAL INSTRUMENTSA Teledyne Technologies Company16830 Chestnut StreetCity of Industry, California 91748, USA

    TEL: 626-934-1500 or 888-789-8168

    FAX: 626-934-1651 EMAIL: [email protected]

    www.teledyne-ai.com

    User Display & Control

    Type of display: LED display

    Display format: 3-1/2 digits in user defined engineering

    units

    Electrical

    Power requirement: 24 VDC (9 - 32 VDC) if 110 / 220 VAC

    is available (optional) AC / DC power

    supply

    Power consumption: 0.48 Watts

    Analog outputs: 4 - 20 mA isolated

    Analog loop resistance: 500 Ohms, nominally @ 24V

    Alarms: Optional

    Area classification: Z-purge for Class I, Division 2;

    X-purge for Class I, Division 1

    Mechanical

    Transmitter weight: 1.5 lbs

    Enclosure construction: Extruded aluminum (NEMA

    enclosures optional)

    8 H x 3 - 7/8 W x 71 - 1/2 D

    Probe

    Materials: 316 SS or Hastelloy C

    Temperature rating: 315.5 C (600 F)Pressure rating: 10,000 psig

    Probe options: 1. 6, 12 or 24 in length

    2. Temperature controlled

    3. Temperature thermistor

    4. Pressure strain gauge

    APPLICATIONS

    Pollution abatement programs involving effluent

    from refineries, chemical / petrochemical plants,

    oil fields, steel mills, automotive production, food

    processing, and other industries

    Offshore drilling platforms, produced water, oil

    field water flooding, steam injection operations On-board shipping (fast analysis required

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    MODEL 6600Oil in Water Analyzer System

    Redesigned with modularity and lower cost in mind

    Rack or cabinet mounted

    General purpose or explosion proof

    Teledynes Model 660/661 has been the industry standard inoil-in-water analysis for 30 years. The microprocessor based6600 / 6610 improves upon our proven analog circuitry and the

    sample handling system. The new, compact modern design

    incorporates many new features at a significantly reduced cost.

    Critical features include:

    Folded optical system optimized for excellent signal-to-noise

    ratio and stability

    Increased reliability by eliminating many moving parts

    New sonicator homogenizes oil (in-line) in water instantly (less

    than one second)

    Improved auto-zero filter system prepares zero fluid

    for calibration and zeroing without long sparging cycle

    Specially developed software with auto calibration features

    Automatic self-cleaning sample cell suitable for high pressure

    and temperature

    Manual calibrations done easily with collected zero

    fluid from sample system using the gravity fed reservoir

    Manual or automatic span sensitivity easily checked with

    internal span flag once field calibrated

    Faster response time

    Modular design configured to meet specific application

    requirements

    The 6600 utilizes the ultraviolet absorption principle to detect

    and continuously measure oil concentration in water with a

    reproducibility that exceeds standard laboratory techniques.

    Teledyne Analytical Instruments

    Oil in Water Analyzer System

    The automated analysis system includes a single beam,

    dual wavelength, UV photometric analyzer that compensates

    for turbidity, algae, cell window coatings, and other optical

    attenuation.

    To assure accuracy, a unique conditioning system delivers a

    sample representative of the true oil content of the stream.

    A continuous ultrasonic homogenizer (figure 2) disperses all

    suspended oil droplets and oil absorbed into foreign matter so

    the sample, to the analyzer, appears to be uniform and in true

    solution.

    OIL DETECTION AND ANALYSIS

    The basic oil detection UV analyzers offered by other

    manufacturers are single wavelength photometers a "go / no

    go" instrument without a sample conditioning system.

    Teledyne feels these lack the sophistication necessary for reliable

    oil detection monitoring, preferring a dual wavelength design.Attenuation of energy transmission by turbidity and cell window

    deposits can then be distinguished from absorption despite the

    presence of oil.

    With sample conditioning (figure 1) and automatic zeroing, our

    analyzers produce a truly representative solution for analysis and

    can compensate for background absorption found in most oil-in-

    water applications.

    DUAL WAVELENGTH

    Recognizing the importance of eliminating the effects of turbidity

    and inherent electro-optical interferences, Teledyne developed a

    single sample cell, chopped beam, dual-wavelength photometric

    analyzer unmatched in reliability and accuracy.The 6600 has been extensively field tested to show excellent

    correlation with the EPA gravemetric reference method 413.1.

    The system utilizes optical filters to isolate and make energy

    measurements at two specific wavelength bands. The UV

    measuring band (centered at 254 nanometers) is extremely

    narrow to avoid side-band interference.

    A reference signal is generated at a selected wavelength region

    where oil does not absorb significantly. This signal is effected by

    the aforementioned interference as well as by absorption due to

    the presence of oil.

    Components contributing to total absorption in a typical water

    effluent sample are shown in figure three. Turbidity and electro-optical interferences are removed by the analyzers design, and

    non-oil background is zeroed out.

    Since both the measuring and reference wavelengths are

    generated at the end of the transmission system, electro-optical

    interference (cell window coating, variations in source lamp,

    aging of detector and other electronics) effects each signal

    equally. The output signal is obtained by electronically generating

    the logarithm of the ratio of the measuring signal to the reference

    signal. Therefore, the output signal, linear with absorption, shows

    little or no affect from turbidity. Additionally, electro-optical stability

    is enhanced by the dual wavelength design.

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    APPLICATIONS

    Pollution abatement programs involving effluents from refineries,

    chemical / petrochemical plants, oil fields, steel mills, automotive

    production, food processing, and other industries

    Offshore drilling platforms, produced water, oil field water flooding,

    steam injection operations

    On-board shipping (fast analysis required < 10 seconds)

    On-shore deballasting discharges and ballast treatment facilities

    Boiler return, feedwater, steam condensate, cooling water, leak

    detection

    Monitoring of airport runoff, municipal water treatment plants

    Wastewater and sewage treatment plants

    Process stream monitoring

    Aromatic hydrocarbons like benzene, toluene, styrene, xylenes in

    water

    FEATURES

    Specific to oil (correlates to EPA 413.1)

    Microprocessor based electronics

    Auto calibration

    Remotely initiated cal / zero via customer supplied 24 VDC signal

    Self-diagnostics with Form C relay contacts

    Ratio measurement

    Continuous measurement

    Total oil readout standard, undissolved oil readout possible (with

    autozero filtering option)

    Integral alarms

    Self-cleaning cell

    Automatic turbidity compensation

    Full duplex RS-232 communication link

    Process pressure up to 150 PSIG (higher pressure possible

    application dependent)

    Sample temperature to 120C (higher temperatures possible,

    application dependent)

    Response time under 5 seconds possible (application dependent)

    NEMA-4x (stainless steel standard) mounted control unit

    AUTOMATIC ZERO MODE

    The 6600 offers an automatic zeroing feature, permitting a continuous

    analysis specific for oil without interference. The zeroing mode

    technique (application dependent) is accomplished by the automatic

    preparation (filtering) and periodic analysis of an oil-free fluid which

    contains the compounds contributing to background absorption. When

    this fluid is analyzed, the background absorption is measured and

    then zeroed out. The cycle is automatically repeated once each hour

    to update the oil analysis by correcting for fluctuations. This allows for a

    more accurate analysis of oil and grease content specifically separated

    from other non-oil organics that many times are also present in effluents.

    For very clean processes like steam or boiler return condensates, only

    oil free nitrogen (N2) gas or air can be used for electro-optical energy

    background variations such as from normal source or detector anomalies

    over time.

    UNHOMOGENIZED HOMOGENIZED

    FIGURE 2

    Homogenizer Function The effect of homogenization on the sample is

    illustrated above. Both the particulate oil and the compounds representing

    turbidity are of random size. Homogenization causes the oil droplets to be

    dispersed to such a particle size that, to the analyzer, they appear to be in

    true solution. Oil absorbed upon or contained within the portion represented

    by turbidity is also placed into solution along with the particulate oil. Turbidity

    has no characteristic absorption and is ratioed to zero by the analyzer.

    NON-OILORGANIC

    BACKGROUND

    DISSOLVED OIL

    UNDISSOLVED OIL

    TURBIDITY

    ZERO FLUID

    "ZERO"

    PURE

    H2

    0

    HOMOGENIZED

    SAMPLE

    FIGURE 3

    Fractions contributing to total absorption in typical water effluen

    The homogenized sample contains all components of the effluent stream

    The UV analyzer measures the stream fractions as non-oil background

    dissolved oil, and non-dissolved oil. Turbidity will be ratioed out and give

    no reading. The analyzer will measure the zero fluid as the non-oil fraction

    Turbidity and oil have been removed from the zero fluid by coarse and ultra

    fine filtering. Coarse filtering removes the non-dissolved oil, while ultra-fine

    filtering removes the lighter dissolved oils. During the zero cycle, the

    analyzer is automatically adjusted to read zero. The non-oil UV absorbing

    background is subtracted from the total UV reading.

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    SAMPLE CONDITIONING

    Factors associated with undissolved oil and background absorption are

    eliminated by sample conditioning. The 6600 incorporates conditioning

    components that prepare the sample so both undissolved and dissolved

    oils are detected and measured.

    A new, in-line, high frequency (20 kHz) ultrasonic homogenizer

    minimizes the size of the oil droplets suspended while dispersing

    them into a more uniform molecular level in the sample so they can

    be measured accurately. For any photometric analytical technique

    measuring oil in water above 20 ppm oil requires this homogenization.Oil absorbed onto the particulate matter in the sample is also dispersed

    by the homogenizer.

    Since the response of particulate matter as a possible attenuator is

    automatically neutralized by the optical system and ratioed to zero by

    the electronics of the photometer, the characteristic absorption of the

    total oil can be measured. The output signal or meter readout is linearly

    proportional with total oil concentration.

    OIL AND GREASE

    Many environmental applications (as monitored by regulatory agencies)

    allow certain minimal levels of dissolved oil to remain in the water

    measured. The 6600 (when ordered specifically to do so) can monitor

    for total oil and grease recoverable or be easily switched to monitor

    the undissolved oil portion only. This minimizes the customers

    costly requirement in energy to process water below a minimum oil

    concentration as dictated by local regulations before out-flowing the

    water as an effluent.

    COMPENSATION FOR BACKGROUND

    Many applications require compensation for background absorption

    due to the presence of non-oil organic and inorganic compounds that

    absorb UV energy. Furthermore, the concentration of these compounds

    will likely fluctuate, specifically in applications with multiple non-oil

    organics and inorganic compounds present in the background. In

    order to obtain an analysis specific to oil, the background absorption

    contributed by these compounds must be eliminated and zeroed out.

    The 6600 does exactly this.

    Sample Conditioning System A sample is fed through a V1 sample / utility valve, then through a split tee; one side as a bypass loop, the other through

    an inline ultrasonic homogenizer. This disperses any oil in the sample before measurement including small or large oil droplets and oil absorbed on foreign

    particles. A portion of the stream is conditioned to remove all oil, both dissolved and undissolved, without altering the background (boiler additives or other

    inorganic compounds.) When this portion is delivered to the analyzer (through SV3), the analyzer subtracts the background from the total and reads out

    total oil only. The analyzer is manually calibrated with a known standard on a one time basis through the indicated zero and span inlet reservoir. The

    specially designed sample cell can interface with process fluids up to 150 psig and 120C (248F)

    BY-PASSF2BY-PASS

    FLOWMETER0-110 LPH

    V10HOMOGENIZER

    FC1

    FLOW

    CONTROLLER

    F1

    SAMPLE

    FLOWMETER

    0-30 LPH

    SAFETY BLOCK

    VALVE

    ZERO & SPAN IN

    C C C C

    V5

    V7

    V6

    CELL BLOCK

    V13-WAYVALVE

    C

    C

    V4

    V8V9C

    IN

    BACK PRESSURE

    REGULATOR

    20-50 PSI

    PUMP(2-5 LPM)30-80 GPH

    FILTER0,2 MICRON

    FILTER3.0 MICRON

    V3

    IN

    PV2

    BPR1

    SAMPLE IN(2-5 LPM)30-80 GPH

    15' WATER VACUUM

    UTILITY

    GRABSAMPLE

    N2 OR AIR

    90 TO 100 PSIG

    RETURN

    SAFE VENT

    SV3

    SV4

    F2 F3

    F1

    IN

    OUT

    SV1SV2

    NOTES: UNLESS OTHERWISE SPECIFIED.

    1. USE HOMOGENIZER AND FILTER ASSEMBLIES FOR HIGH RANGE,

    HIGH BACKGROUND

    2. USE FILTER ASSEMBLY FOR LOW RANGE, HIGH BACKGROUND

    3.

    USE BACKFLUSH SOLENOIDS FOR LOW RANGE, VERY LOW BACKGROUND

    4. USE PUMP ASSEMBLY FOR LOW PRESSURE OR NO GRAVITY FEED

    FIGURE 1

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    OPTIONAL MODULES

    Homogenizer Module A high frequency (20 kHz) ultrasonic

    homogenizer is used to minimize the size of the oil droplets

    while dispensing them in the sample so they can be measured

    accurately. Measuring samples above 20 ppm typically require this

    module.

    Filter Assembly Module required for applications with highbackground interference

    Pump Module required for applications with low pressure or no

    gravity feed

    Purge Module Z purge unit or X purge unit

    CONFIGURATIONS

    General purpose

    Class I, Div. 2, Groups B, C & D

    Class I, Div. 1, Groups B, C & D

    CE mark, CENELEC certified

    OIL IN WATER ANALYZER SYSTEM SERIES 6600-6610

    SPECIFICATIONS

    Range: 0-10 ppm up to 0-200 ppm oil in water

    (application dependent)

    Noise: Less than 1% of full scale

    Zero drift: Corrected by automatic zero

    Accuracy: Dependent upon variability of oil composition;

    2% of full scale when calibrated against

    same oil as being analyzed

    Reproducibility: 1% of full scale or better

    Linearity: 1% of full scale or better

    Power 115 VAC 50/60 Hz; requirements: 230 VAC,

    50/60Hz (specify)

    Ambient 0 to 50C; may be heated or cooled to

    temperature: operate in other temperatures

    Sample 1 to 120C, nominal (non-freezing),temperature: lower temperatures possible

    with salt waters

    Sample 0 to 150 PSIG (an optional pump can be

    pressure: supplied when no gravity feed or

    sample pressure is available)

    Signal output: Analytical measurement, 0-1 VDC and

    isolated 4-20 mADC

    Alarms: Dual fully adjustable concentration alarm set

    points with programmable relay function.

    Form C contacts, 3A resistive; self-diagnostics with Form C failure alarm contact

    Data lines: Bi-directional RS-232C serial interface

    Readout: Two line alphanumeric vacuum florescent

    display0-10 ppm oil-in-water

    monitoring system for boiler /

    steam condensate application

    2005 Teledyne Analytical Instruments, A Teledyne Technologies Company.All rights reserved. Printed in the USA. 11/05LD

    WarrantyInstrument is warranted for 1 year against defects in material

    or workmanshipNOTE: Specifications and features will vary with application. The above are establishedand validated during design, but are not to be construed as test criteria for every product.All specifications and features are subject to change without notice.

    TELEDYNEANALYTICAL INSTRUMENTSA Teledyne Technologies Company

    16830 Chestnut StreetCity of Industry, California 91748, USA

    TEL: 626-934-1500 or 888-789-8168

    FAX: 626-934-1651 EMAIL: [email protected]

    www.teledyne-ai.com

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    Features

    Ranges are 0-50 ppb to 0-20 ppm, user selectable

    Dual ranges and auto ranging

    Microprocessor controlled for versatility

    Multi-tasking software allows viewing test variables while

    operating

    Continuous self checking with alarms

    Dual bi-directional RS-232 ports for remote operation

    (optional RS-485 or Ethernet)

    Digital status outputs indicate instrument operating condition

    Adaptive signal filtering optimizes response time

    Temperature and pressure compensation

    Internal Zero & Span check (optional)

    Internal data logging with 1 min to 365 day multiple

    averages

    Critical orifices provide flow stability

    Teledyne Analytical Instruments

    6400

    E

    U V F l u o r e s c e n c e S O 2 A n a l y z e r

    Teledynes 6400E uses a proven UV fluorescenceprinciple coupled with state-of-the-art microprocessortechnology to provide accurate and dependable

    measurements of low level S02.

    Exceptional stability is achieved with the use of an opticalshutter to compensate for PMT drift and a reference

    detector to correct for changes in UV lamp intensity.

    A hydrocarbon kicker and advanced optical design

    combine to prevent inaccuracies due to interferents. The

    multi-tasking software gives real time indication of many

    operational parameters and provides automatic alarms if

    diagnostic limits are exceeded.

    Advanced Performance

    The 6400E includes a built-in data acquisition capability

    using the analyzers own internal memory. This allows the logging

    of multiple parameters including averaged or instantaneousconcentration values, calibration data and operating parameters

    such as flow, pressure and lamp intensity.

    Stored data are easily retrieved through the serial port or optional

    Ethernet port via our software or from the front panel, allowing

    operators to perform predictive diagnostics and enhanced data

    analysis by tracking parameter trends.

    The 6400E combines lighter weight, rugged construction, ease

    of use, powerful diagnostics, modular design and outstanding

    performance to meet air monitoring requirements.

    Applications

    Detect low trace levels of SO2 in medical air and medical

    oxygen to satisfy USA and European pharmacopeiarequirements.

    Detect trace levels of H2S in methane-rich Bio-Gas streams

    used as the feed for fuel cell power generation devices. The

    H2S impurities, which can poison the platinum based catalyst,

    are converted into SO2 on a 1:1 basis via Teledynes THC

    converter. The resultant converted sample gas is then fed to the

    6400E for continuous analysis purposes.

    6400E Schematic6400E Schematic

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    6400E FLUORESCENT SO2 ANALYZER

    SPECIFICATIONS

    Ranges: 0-50 ppb to 0-20,000 ppb full scale, user

    selectable; dual ranges and auto ranging

    supported

    Units: ppb, ppm, g/m3, mg/m3

    Zero noise:

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    TELEDYNEANALYTICAL INSTRUMENTS

    Total

    Sulphides

    Analyzer

    FOR CO2 Purity Quality Monitoring

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    The need to continuously detect for suldes

    in carbon dioxide has become increasingly

    important within the food and beverage market.

    Gas suppliers must ensure that the CO2 they provide

    for use in the preservation of food and drink related

    products meet todays exacting standards. The

    contamination of carbon dioxide can emanate from

    many sources and therefore it is essential that the

    CO2 used for such purposes be monitored at theCO2 generator facility, at the beverage producer

    facility, or both.

    PRINCIPLE OF OPERATION

    The Model 6200E Total Suldes Analyzer utilizes

    proven UV uorescent technology to continuously

    detect suldes found in inert gas streams. An

    internal, quartz catalytic converter is employed to

    convert the suldes, when mixed with scrubbed

    ambient air, into SO2 via high temperature oxidation.

    An internal vacuum pump is employed to draw boththe sample and the ambient air into the converter.

    The converted sample gas is fed to the uorescence

    chamber where it is then exposed to ultra-violet

    radiation.

    The measurement process in the reaction cell is

    described by the following equation:

    SO2 + hu1dSO2*

    SO2*dSO2 + hu2

    Where hu1 is the incident UV energy at 214nm andhu2 is the resultant uorescence, which is directly

    proportional to the SO2 concentration in the reaction

    cell.

    The uorescence emission is in turn sensed by

    the photo-multiplier tube (PMT) and amplied to

    provide an analog output. The result is a continuous

    measurement of total suldes (i.e. H2S, CS2, COS,

    mercaptans, etc.) as SO2 from 0-50 ppb to 0-20

    ppm.

    Model 6200E basic configuration

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    ELECTRONICS PLATFORM

    The 6200E combines the proven UV uorescence

    principle with state of the art microprocessor

    technology to provide accurate and dependable

    measurement of trace levels of total suldes. Long

    term stability is obtained by the use of an optical

    shutter to compensate for zero drift, coupled with

    lamp reference detector to correct for lamp drift.

    The multi-tasking microprocessor allows easy eld

    ranging from 50 ppb to 20 ppm as well as providing

    on-line indication of instrument status. The 6200E

    is continuously checking operating parameters and

    provides alarms on out of specication conditions,

    including electrical and optical parameters.

    The easy to read display, intuitive menu structure,

    and ease of operation combine to make the

    6200E the instrument of choice for Total Suldes

    applications.

    The instrument includes a built-in data acquisitioncapability, utilizing the analyzers internal RAM.

    This allows logging of the measured variable

    concentration as well as other parameters such as

    calibration data, ow rates, lamp intensities or a

    variety of other congurable parameters.

    This provides the operator the ability to perform

    predictive diagnostics by tracking parameters over

    time. This stored data is available through an RS-

    232C port on either an automatic timed or manual

    manner.

    THE COMPONENTS

    The 6200E comes complete with three 19 inch relay

    rack modules - the Sample Converter Module, the

    Analysis Module, and a Calibration Module.

    The Sample Converter Modulecomes with an

    SO2 scrubber, sample / ambient air lters, high

    temperature dilution control orice box, and Total

    Reduced Sulfur (TRS) converter.

    The Analysis Moduleconsists of the UV

    uorescence analyzer, pressure and ow

    transducers, and vacuum pump.

    The Calibration Moduleconsists of restrictor /

    orice ow regulators and ow control system,

    all provided in a temperature controlled setting to

    ensure accurate performance.

    The two inlet ports allow use of two independent

    calibration gases which may be diluted to provide

    the required span gas concentration. Dilution ratios

    from 20:1 to 300:1 are manually set from the frontpanel.

    FEATURES

    High sensitivity with user selectable ranges

    from 0-50 ppb to 0-20 ppm

    Microprocessor controlled, providing

    advanced user interface capabilities

    Built-in data acquisition capability using the

    analyzers own RAM

    Extremely high-end self diagnostic capability

    providing continuous self checking with

    continuous warning alarms

    Bi-directional RS-232C for remote operation

    Critical orices provide ow sensitivity

    High temperature TRS converter

    Digital status outputs provide instrument

    condition

    Easy to read display

    Proven UV uorescence technique

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    2006 Teledyne Analytical Instruments, A Teledyne Technologies Company.All rights reserved. Printed in the USA. 05/06LD

    Warranty

    Instrument is warranted for 1 year against defects in materialor workmanship

    NOTE: Specifications and features will vary with application. The above are establishedand validated during design, but are not to be construed as test criteria for every product. Allspecifications and features are subject to change without notice.

    6200E Total Sulphides Analyzer

    SPECIFICATIONS

    Ranges: 0 - 50 ppb to 0 - 20,000 ppb full-scale, user

    selectable

    Dual ranges and auto-ranging supported

    Zero noise: < 0.2 ppbSpan noise: < 0.5% of reading (above 50 ppb)

    LDL: 0.4 ppb

    Zero drift**: < 0.5 reading / 24hrs; 1 ppb / 7 days

    Span drift**: < 0.5% reading / 24 hrs; 1% of reading / 7

    days

    Lag time: 20 secs

    Rise time (95%): < 120 secs

    Linearity: 1% of full scale

    Sample flow rate: 700 cc/min 10%

    Converter temperature: 1000C

    Converter efficiency: > 98% above 0C dewpoint

    Converter life: 3000 ppm hours

    SOx scrubber efficiency: > 98%

    SOx scrubber life: > 1000 ppm hours

    Analyzer operating temperature: 5 to 40C

    Power: 100 Vac 240 Vac, 50/60 Hz (user

    specified)

    Outputs: Analog: 10 V, 5 V, 1 V, 100 mV (selectable)

    (4-20mA isolated output optional)

    RS232 (I/O): Standard DB9

    Digital status: 12 contact closure outputs

    TELEDYNE

    ANALYTICAL INSTRUMENTSA Teledyne Technologies Company

    16830 Chestnut StreetCity of Industry, California 91748, USA

    TEL: 626-934-1500 or 888-789-8168

    FAX: 626-934-1651 EMAIL: [email protected]

    www.teledyne-ai.com

    Size (H x W x D):

    Model 6200E analyzer:

    (7 x 17 x 23.5)

    (177.8 x 432 x 596.9 mm)

    Dilutor / Converter module:

    (7 x 17 x 23.5)(177.8 x 432 x 596.9 mm)

    Calibration module:

    (5.25x 17 x 23.5)

    (133.3 x 432 x 596.9 mm)

    **At constant conditions

    ADDITIONAL OPTIONS

    Fluorocarbon zero / span valves

    19 rack mount brackets

    19 rack mount with chassis sliders

    2 to 5 year warranty

    Contact Teledyne for details on our Carbon Dioxide

    Quality Control (CDQC), which is a turn-key

    system capable of detecting:

    Total Sulphides (UV

    Total Hydrocarbons Trace Moisture (AI2 O3)

    Trace Oxygen (Electrochemical)

    CO2 Purity (NDIR)

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    Process Photometers

    PUV3402 and PIR3502

    AnalyzeIT

    FieldIT

    ControlIT

    EngineerIT

    FieldIT

    InformIT

    OperateIT

    PowerIT

    IndustrialIT

    Continuous Measurements

    VistaNET Connectivity

    Multiple Component Samples

    Measures Vapor or Liquid Samples

    Operates in IR, NIR, UV and VIS Regions

    Fiber Optic Option for NIR Applications

    Multiple Interference Compensation Capability

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    UV/VIS/NIR Fiber Optics

    Option

    The PFO3502 Multiwave offers a fiber optic option

    for applications that require remote sampling capa-

    bility. With this option, light is transmitted via one

    waveguide to the remote sample cell. A second

    waveguide is used to return the sample-modified

    light to the detector.

    This Fiber Optics option is effective in

    UV/Visible/NIR applications where:

    The sample stream is highly toxic.

    Corrosive products are analyzed.

    Fast response time is required.

    The sample is at high pressure.

    Cell-In-Oven Sample

    System

    The Multiwave Cell-In-Oven designprovides a simple and effective pack-age for high temperature applications.The major benefit of this design is thatthe sample cell and sample handlingcomponents are together in one com-

    mon temperature controlled enclosure.The elimination of heat trace require-ments for sampling lines minimizesthe risk of cold spots. This designalso offers excellent accessibility forfast cell removal during maintenance.

    Performance Specifications

    Precision: 1% of full scale

    Noise:

    1% of full scale at 0.02 absorption units 0.5% of full scale at 0.20 absorption units

    Linearity:Standard 2% of full scale

    Zero Drift: 0.5% of full scale per day for IR; 1.0% of full scale per/day for UV

    Response Time:Programmable

    Ambient Electronic Stability: 1% of full scale for 18F (10C) in 4 hours

    Operating Specifications

    Wavelength Range:Ultraviolet 200400 nm

    Visible 400800 nmNear Infrared 8002500 nmFundamental Infrared 2.5014.50 um.

    Ambient Temperature Range:32 to 113F (045C)

    Max. Cell Heat:302F (150C)

    Electric Cell Heat:Power Consumption 450 watts maximum(temperature is application dependant)

    Sample Flow Rate:Typical 20500 cc/min for vapors;5120 cc/min for liquids

    Sample Pressure:0500 PSIG (034 bar)

    Voltage Input Variation:10% fluctuation without causing anoutput variation of 0.05% of full scale

    Electrical Power To Analyzer:100/115/220/230 VAC, 4566 HZ,150W, Maximum Power Consumption600W With Electric Heat

    Instrument Air Supply for Enclosure Purge

    (Safety):Pressure 4080 psi (36 bars)Flow Rate 0.5 CFM (15L/min.)

    Optical Purge, typically nitrogen:Pressure @ 1530 psi (12 bar)

    Flow Rate 1015 cc/min

    General Installation

    Protect the instrument from direct sunlight andrain at operating temperature between 32113 F(045C)

    Dimensions

    Weight:

    approximately 80 lbs (36.28 kg)Height:13.5 inches (342.9 mm)

    Depth:10.5 inches (266.7 mm)

    Width:10 inches (254 mm) per module

    Overall Length:(based on cell pathlength)

    Minimum26.8 inches (681.4 mm) for 0.5 to 16 mm cell

    Maximum65.5 inches (1665 mm) for 1 meter cell

    Tube Fittings

    Sample Inlet/Outlet:

    Metallic Cells Teflon Cell

    Size: 1/4" 1/8"

    Brand: Standard Gyrolok Gallek or Fluorocarb(Swagelok available)

    Material: 316 SS TeflonHastelloy C, Monel

    Purge Inlet and Outlet:Metal Cell Size: 1/4" NPT-F

    Brand: Gyrolok

    Material: 316 SS

    Power:Size: 18 AWG, 3/4" Conduit Hub

    Type: 3 conductors each

    Output Signals

    Analog Outputs:4 ea. 4-20 mA isolated into 600 ohms max.

    Contact Closures:2 ea. Relay, 3W at 0.25 A or 28 VDC, 5 ea.isolated solid state. Both relay and solid statecontact closures N.O. or N.C.

    Digital Inputs:8 ea., 2 ea. are dedicated

    Digital Outputs:4 ea., 110 VDC, 25 watts ea., max. standard,110 VDC, 24 VDC optional.

    Area Classification

    NEC Class I, Groups B, C, D, Division 2 withoutenclosure purge; Division 1 with type Y-Purge;CSA Class I, Groups B, C, D, Division 2 with typZ-Purge;Division1 withtype X-Purge (CSA 15549CE Zone 2, II3G; EEx pz IIB+H2 T4 to T2;

    CE Zone 1, II2G; EEx pd [ib] IIB+H2 T4 to T2(LCIE 03 ATEX 6007X)

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    Process Photometers

    PUV3402andPIR3502...

    The Next Generation of On-Line

    Process Photometers.

    MultiwaveProcess Photometers

    are designed to provide on-line meas-

    urements of gas or liquid components,

    in simple or complex process streams,

    for process control, product quality

    assurance, safety, catalyst protection

    and area monitoring.

    The Multiwave is a fixed filter photo-

    meter that utilizes optical filters to

    make continuous measurements. The

    single beam, dual wavelength concept

    used in the Multiwave compensates

    for source and detector aging and the

    obstruction of cell windows, while

    allowing the sample cell to be isolated

    from the electronics.

    The Multiwave design takes the single

    beam, dual wavelength concept one

    important step further, by adding up

    to eight filters to the filter wheel. Thisimproved method provides more meas-

    urement solutions than a conventional

    single component process photometer.

    The use of multiple wavelengths ena-

    bles the Multiwave to compensate

    for numerous interferences and per-

    form multiple component applications.

    The newMultiwaveProcess Photo-

    meters offer even more performance,

    operating efficiency and versatility to

    the user. The Multiwave line features

    two basic models, each offering a wide

    range of applications capability.

    PIR3502 Multiwave Photometers

    can be applied to Infrared and Near

    Infraredmeasurements.

    PUV3402 Multiwave Photometers

    are designed for theUltraviolet and

    Visible spectral regions.

    Optical Schematic

    Multiwave Photometers can be con-

    nected to ABB AnalyticalsVistaNET

    Process Analyzer Network, enabling

    data interchange from the analyzer tothe DCS, seamless connectivity to the

    Plant LAN and remote user access.

    With the addition of VistaNET, all

    operator functions may be performed

    at the analyzer or from a remote PC.

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    MultiwaveTM Process Photometer

    VistaNET

    Connectivity

    The VistaNET Process Analyzer

    Network is a local area network that

    supports data interchange from

    process analyzers to the Distributed

    Control System (DCS), in a dedicated

    and secured manner. VistaNET also

    provides seamless connectivity to the

    plant operating system (Plant LAN).

    Through the Multiwave Remote

    User Interface, the user can configure,

    operate, or troubleshoot the operation

    of the analyzer from a remote PC.

    With this remote access capability all

    operator functions may be performed.

    Remote configuration and observa-

    tion of the Multiwave photometer,

    enabling technicians to use their

    time more efficiently.

    Graphic display of Absorbance vs.

    Concentration data, allowing the

    user to check the validity and

    linearity of calibration samples.

    Remotemaintenance viamodem

    multiple users can view datasimultaneously and work together

    in troubleshooting activities.

    Reports and Tables can be printed

    and reviewed at remote locations.

    And VistaNet is designed for use

    with widely used and accepted PC

    hardware and operating systems,

    including Windows 95, 98 and NT,

    TCP/IP and other protocols. Connect-

    ing to other network operating sys-

    tems is simple and very economical*.

    *Consult our VistaNET Brochure for more details.

    Multiwave Spectral Regions

    Infrared (IR) 2.5014.5 um

    Near Infrared (NIR) 8002500 nmVisible (VIS) 400800 nmUltraviolet (UV) 200400 nm

    Multiwave Process Photometers Leading Applications*

    PIR3502

    Infrared: Isocyanate in chloroaromatic solventAmbient air monitoringMulticomponent monomers in polymer process

    Near Infrared: Measurement of Hydrogenic Compounds (C-H, N-H, O-H)Water in organics, such as Ethylene Dichloride (EDC)Caustic in Acid Gas Scrubbers

    PUV3402

    Visible: Color Measurements (ASTM, APHA, Saybolt Color Units)Ultraviolet: %T @ Multiple Wavelengths in Glycol Process

    Chlorine in Phosgene

    *Consult our Multiwave Applications Brochure

    for more details.

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    MultiwaveTM Process Photometer

    Designed for Reliability

    and Performance

    PUV3402 and PIR3502 Multiwave Process Photo-meters are designed to meet all the significantchallenges of the process environment, includingambient temperature variation, moisture, corrosiveand explosive stream compositions, electricalhazards, dust and vibration.

    Accessibility Every major component may

    be easily removed and replaced, significantly

    reducing maintenance time.

    Solid State Detectors The PIR3502 and PUV3402

    use solid state detectors. These detectors are

    thermally stable and insensitive to vibration.

    They require no mechanical adjustment and

    minimal interconnecting circuitry. They provide

    excellent linearity and long service life.

    Brushless Chopper Motor Provides good

    mechanical reliability and long service life.

    Linearizer Circuit with Up to 8 Points Ensures

    a 2% of full scale linearity and allows the user

    to select the best accuracy for a specific range.

    Isolated Sample Cell Prevents flammable andcorrosive streams from contacting electronics,

    permits cell heating to optimum sample condi-

    tions, allows easy access and optimum optical

    pathlength selection.

    Self-Aligning Optics Saves time during

    maintenance operations.

    Temperature Controlled Filter Assembly Eliminates temperature effects on filters,

    improving long term stability.

    Electric Cell Heating Concept The first ever

    Division 1/Zone 1 electrically heated sample cell.

    Employs a unique heat pipe concept that reduces

    temperature gradients across the cell, providing

    a more stable output and accurate temperature

    control.

    Data validation to ensure the reliability of

    Multiwave data.

    Self-diagnostics to aid in troubleshooting

    operations.

    Functional User Interface Direct user interface

    at the analyzer is simple and easy using the

    Multiwave's front panel keyboard and display

    screen. And with built-in VistaNET capability,

    all operator functions may also be performed

    from a remotePC.

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    ABB Inc.

    843 N. Jefferson Street

    Lewisburg

    WV 24901

    USA

    Office: 304.647.4358

    Fax: 304.645.4236

    The IndustrialIT

    wordmark and all mentioned product names

    in the form XXXXXXIT

    are registered or pending trademarks of ABB.

    ABB has Sales & Customer Support expertise in over

    100 countries worldwide.

    The Companys policy is one of continuous

    product improvement and the right

    is reserved to modify the information

    contained herein without notice.

    2005 ABB Inc. BUASC 3-2-105

    www.abb.com/analytical

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    Series 6000

    Ultraviolet Photometric Analyzer

    Series 6000

    Ultraviolet Photometric Analyzer

    CONFIGURATIONS

    6000: General purpose wall mount

    6020: Totally explosion proof suitable for use in

    Class I, Division 1, Groups B, C & D

    Alternate configurations are available; contact the

    factory.

    SPECIFICATIONS

    Noise: < 1%

    Drift: Less than 1% per day

    Diurnal: Less than 1% per 20F

    Accuracy: 1% of full scale

    Ambient: 32F to 122F

    (0-50C) non-condensing

    Sample cell: Stainless steel with quartz windowstandard. Other materials available.

    Cell length: .01 to 40 inches

    (application dependent)

    Flow rate: 50 to 1500 cc/min

    Light source: Tungsten lamp, mercury, deuterium

    arc (application dependent)

    Power rating: 115/230 VAC, 50/60Hz volts,approximately 200 watts

    Sensitivity: .02 to 3 absorbance units

    Optical System (figure 1)

    SOURCELENSSAMPLE IN

    FILTER WHEEL

    DETECTOR

    SAMPLE OUT

    MOTOR

    Reproducibility: 1% of scale or better

    Electronic response: 90% in 1 second

    Filter wavelength: 210 to 1000 nano-meters

    Sample pressure: Quartz window - 30 psig

    Sapphire - 40 psig

    Enclosure:

    (6000)General purpose - sheet steel

    (6020) Hazardous duty - condulet

    Readout: 2-line alphanumeric vacuum

    fluorescent display (VFD)

    2005 Teledyne Analytical Instruments, A Teledyne Technologies Company.All rights reserved. Printed in the USA. 11/05LD

    Warranty

    Instrument is warranted for 1 year against defects in materialor workmanship

    NOTE: Specifications and features will vary with application. The above are establishedand validated during design, but are not to be construed as test criteria for every product.All specifications and features are subject to change without notice.

    TELEDYNE

    ANALYTICAL INSTRUMENTSA Teledyne Technologies Company16830 Chestnut StreetCity of Industry, California 91748, USA

    TEL: 626-934-1500 or 888-789-8168

    FAX: 626-934-1651 EMAIL: [email protected]

    www.teledyne-ai.com