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TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
June 22, 2009
NELAP Accredited #100226
Samples are analyzed on an as received basis unless otherwise requested and documented. The sample results contained in this report relate only to the requested analytes of interest as directed on the chain of custody. IL ELAP and NELAP accredited fields of testing are indicated by the letters NELAP under the Certification column.
All quality control criteria applicable to the test methods employed for this project have been satisfactorily met and are in accordance with NELAP except where noted. The following report shall not be reproduced, except in full, without the written approval of Teklab, Inc.
If you have any questions regarding these tests results, please feel free to call.
Sincerely,
WorkOrder: 09060783A831-735002-012901-225/Ameren Champaign 62403053
RE:
Dear Pete Sazama:
TEKLAB, INC received 3 samples on 6/18/2009 5:55:00 PM for the analysis presented in the following report.
210 West Sand Bank RoadColumbia, IL 62236-0230
(618) 281-7173(618) 281-5120
TEL:FAX:
Pete SazamaPSC Industrial Outsourcing, LP
Heather A. WhiteProject Manager
(618)344-1004 ex 20
IL ELAP and NELAP Accredited - Accreditation #100226 Page 1 of 54
Project: A831-735002-012901-225/Ameren Champaign 62403053Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
SAMPLE SUMMARY
Report Date: 22-Jun-09
Lab Sample ID Client Sample ID Collection Date
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
Fractions
09060783-001 CBA-01 6/18/2009 1:30:00 PM6
09060783-002 CBA-02 6/18/2009 1:50:00 PM6
09060783-003 CBA-03 6/18/2009 2:10:00 PM6
IL ELAP and NELAP Accredited - Accreditation #100226 Page 2 of 54
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
A831-735002-012901-225/Ameren Champaign 624030530906078322-Jun-09
Project:LabOrder:
Client:
Report Date:
CASE NARRATIVEPSC Industrial Outsourcing, LP
Cooler Receipt Temp: 4.2 °C
State accreditations:
KS: NELAP #E-10347 | KY: UST #0073 | MO: DNR #00930 | AR: ADEQ #70-028-0
Qualifiers
- Analyte detected below reporting limits
- Analyte detected in the associated Method Blank
- Spike Recovery outside accepted recovery limits
- RPD outside accepted recovery limits- Not Detected at the Reporting Limit - Value above quantitation range
- Value exceeds Maximum Contaminant Level
- Reporting Limit
- Dilution Factor
- Too numerous to count ( > 200 CFU )
- Diluted out of sample
- Holding time exceeded- Surrogate Standard added by lab
- Matrix interference
- IL Dept. of Public Health- IL ELAP and NELAP Accredited Field of Testing
DF
RL
TNTC
Surr
IDPH
B
J
R
S
X
NELAP
E
MI
H
ND
D
- Did not igniteDNI- Unknown hydrocarbon#- QC criteria failed or noncompliant CCVQ
- Client requested RL below PQLC
IL ELAP and NELAP Accredited - Accreditation #100226 Page 3 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 1:30:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-001
Client Sample ID: CBA-01
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
ASTM D2974Percent Moisture 6/18/2009 7:00:00 PM0.1 % 122.9 MAB
STANDARD METHODS 18TH ED. 2540 GTotal Solids 6/18/2009 7:00:00 PM0.1 % 177.1 MAB
SW-846 3050B, 6010B, METALS BY ICPArsenic 6/19/2009 1:14:06 PM2.36 mg/Kg-dry 15.04 LALNELAP
Barium 6/19/2009 1:14:06 PM0.47 mg/Kg-dry 1124 LALNELAP
Cadmium 6/19/2009 1:14:06 PM0.19 mg/Kg-dry 10.35 LALNELAP
Chromium 6/19/2009 1:14:06 PM0.94 mg/Kg-dry 119.8 LALNELAP
Lead 6/19/2009 1:00:26 PM3.77 mg/Kg-dry 116.8 LALNELAP
Silver 6/19/2009 1:14:06 PM0.52 mg/Kg-dry 1< 0.52 LALNELAP
SW-846 3050B, METALS BY GFAASelenium 7740 J 6/19/20090.556 mg/Kg-dry 10.33 MEKNELAP
SW-846 3550B, 8081A, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
4,4´-DDE 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
4,4´-DDT 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
Alachlor 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
Aldrin 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
alpha-BHC 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
alpha-Chlordane 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
beta-BHC 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
Chlordane 6/19/2009 9:40:00 PM4.27 µg/Kg-dry 1ND HENELAP
delta-BHC 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
Dieldrin 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
Endosulfan I 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
Endosulfan II 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
Endosulfan sulfate 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
Endrin 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
Endrin aldehyde 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
Endrin ketone 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
gamma-BHC 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
gamma-Chlordane 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HE
Heptachlor 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
Heptachlor epoxide 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
Methoxychlor 6/19/2009 9:40:00 PM2.14 µg/Kg-dry 1ND HENELAP
Toxaphene 6/19/2009 9:40:00 PM38.4 µg/Kg-dry 1ND HENELAP
Surr: Decachlorobiphenyl 6/19/2009 9:40:00 PM48-149 %REC 153.6 HE
Surr: Tetrachloro-m-xylene 6/19/2009 9:40:00 PM19-145 %REC 129.7 HE
IL ELAP and NELAP Accredited - Accreditation #100226 Page 4 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 1:30:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-001
Client Sample ID: CBA-01
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 6/19/2009 10:25:00 AM47.9 µg/Kg-dry 1ND MAMNELAP
Aroclor 1221 6/19/2009 10:25:00 AM47.9 µg/Kg-dry 1ND MAMNELAP
Aroclor 1232 6/19/2009 10:25:00 AM47.9 µg/Kg-dry 1ND MAMNELAP
Aroclor 1242 6/19/2009 10:25:00 AM47.9 µg/Kg-dry 1ND MAMNELAP
Aroclor 1248 6/19/2009 10:25:00 AM47.9 µg/Kg-dry 1ND MAMNELAP
Aroclor 1254 6/19/2009 10:25:00 AM47.9 µg/Kg-dry 1ND MAMNELAP
Aroclor 1260 6/19/2009 10:25:00 AM47.9 µg/Kg-dry 1ND MAMNELAP
Surr: Decachlorobiphenyl 6/19/2009 10:25:00 AM5-156 %REC 159.6 MAM
Surr: Tetrachloro-meta-xylene 6/19/2009 10:25:00 AM7.35-123 %REC 128.5 MAM
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 1ND MAMNELAP
Acenaphthylene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 1ND MAMNELAP
Anthracene J 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.004 MAMNELAP
Benzo(a)anthracene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.036 MAMNELAP
Benzo(a)pyrene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.042 MAMNELAP
Benzo(b)fluoranthene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.063 MAMNELAP
Benzo(g,h,i)perylene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.032 MAMNELAP
Benzo(k)fluoranthene R 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.023 MAMNELAP
Bis(2-ethylhexyl)phthalate S 6/19/2009 10:54:00 AM0.087 mg/Kg-dry 10.166 MAMNELAP
Chrysene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.049 MAMNELAP
Dibenzo(a,h)anthracene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.007 MAMNELAP
Fluoranthene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.111 MAMNELAP
Fluorene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 1ND MAMNELAP
Indeno(1,2,3-cd)pyrene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.027 MAMNELAP
Naphthalene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 1ND MAMNELAP
Phenanthrene R 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.039 MAMNELAP
Pyrene 6/19/2009 10:54:00 AM0.004 mg/Kg-dry 10.088 MAMNELAP
Surr: 2-Fluorobiphenyl 6/19/2009 10:54:00 AM10-131 %REC 147.5 MAM
Surr: Nitrobenzene-d5 6/19/2009 10:54:00 AM10-132 %REC 150.1 MAM
Surr: p-Terphenyl-d14 6/19/2009 10:54:00 AM30.6-131 %REC 168.5 MAM
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
1,2-Dichlorobenzene 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
1,3-Dichlorobenzene 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
1,4-Dichlorobenzene 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
2,4,5-Trichlorophenol 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
2,4,6-Trichlorophenol 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
2,4-Dichlorophenol 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 5 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 1:30:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-001
Client Sample ID: CBA-01
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS2,4-Dimethylphenol 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
2,4-Dinitrophenol 6/20/2009 2:55:00 PM6.52 mg/Kg-dry 5ND DMHNELAP
2,4-Dinitrotoluene 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
2,6-Dinitrotoluene 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
2-Chloronaphthalene 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
2-Chlorophenol 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
2-Methoxy-4-methylphenol 6/20/2009 2:55:00 PM4.24 mg/Kg-dry 5ND DMH
2-Methylnaphthalene 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
2-Nitroaniline 6/20/2009 2:55:00 PM6.52 mg/Kg-dry 5ND DMHNELAP
2-Nitrophenol 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
3,3´-Dichlorobenzidine 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
3-Nitroaniline 6/20/2009 2:55:00 PM6.52 mg/Kg-dry 5ND DMHNELAP
4,6-Dinitro-2-methylphenol 6/20/2009 2:55:00 PM6.52 mg/Kg-dry 5ND DMHNELAP
4-Bromophenyl phenyl ether 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
4-Chloro-3-methylphenol 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
4-Chloroaniline 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
4-Chlorophenyl phenyl ether 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
4-Nitroaniline 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
4-Nitrophenol 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
Aniline 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
Azobenzene 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMH
Benzidine 6/20/2009 2:55:00 PM6.89 mg/Kg-dry 5ND DMHNELAP
Benzoic acid 6/20/2009 2:55:00 PM9.78 mg/Kg-dry 5ND DMHNELAP
Benzyl alcohol 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
Bis(2-chloroethoxy)methane 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
Bis(2-chloroethyl)ether 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
Bis(2-chloroisopropyl)ether 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
Butyl benzyl phthalate 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
Carbazole 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMH
Dibenzofuran 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
Diethyl phthalate 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
Dimethyl phthalate 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
Di-n-butyl phthalate 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
Di-n-octyl phthalate 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
Hexachlorobenzene 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
Hexachlorobutadiene 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
Hexachlorocyclopentadiene 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
Hexachloroethane 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 6 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 1:30:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-001
Client Sample ID: CBA-01
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSIsophorone 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
m,p-Cresol 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
Nitrobenzene 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
N-Nitrosodimethylamine 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
N-Nitroso-di-n-propylamine 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
N-Nitrosodiphenylamine 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
o-Cresol 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
Pentachlorophenol 6/20/2009 2:55:00 PM13.0 mg/Kg-dry 5ND DMHNELAP
Phenol 6/20/2009 2:55:00 PM2.28 mg/Kg-dry 5ND DMHNELAP
Pyridine 6/20/2009 2:55:00 PM3.26 mg/Kg-dry 5ND DMHNELAP
1,2-Diphenylhydrazine 6/20/2009 2:55:00 PM5.48 mg/Kg-dry 5ND DMH
Surr: 2,4,6-Tribromophenol 6/20/2009 2:55:00 PM32.7-130 %REC 569.0 DMH
Surr: 2-Fluorobiphenyl 6/20/2009 2:55:00 PM34.1-116 %REC 556.9 DMH
Surr: 2-Fluorophenol 6/20/2009 2:55:00 PM30.5-99 %REC 565.0 DMH
Surr: Nitrobenzene-d5 6/20/2009 2:55:00 PM34.1-101 %REC 562.9 DMH
Surr: Phenol-d5 6/20/2009 2:55:00 PM34.9-110 %REC 569.3 DMH
Surr: p-Terphenyl-d14 6/20/2009 2:55:00 PM41.7-124 %REC 574.7 DMH
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,1,1-Trichloroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,1,2,2-Tetrachloroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,1,2-Trichloro-1,2,2-trifluoroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSA
1,1,2-Trichloroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,1-Dichloro-2-propanone 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSA
1,1-Dichloroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,1-Dichloroethene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,1-Dichloropropene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,2,3-Trichlorobenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,2,3-Trichloropropane 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP
1,2,3-Trimethylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSA
1,2,4-Trichlorobenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,2,4-Trimethylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,2-Dibromo-3-chloropropane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,2-Dibromoethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,2-Dichlorobenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,2-Dichloroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,2-Dichloropropane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,3,5-Trimethylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 7 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 1:30:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-001
Client Sample ID: CBA-01
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,3-Dichlorobenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,3-Dichloropropane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1,4-Dichlorobenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
1-Chlorobutane J 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 11.6 JSANELAP
2,2-Dichloropropane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
2-Butanone 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP
2-Chlorotoluene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
2-Hexanone 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP
2-Nitropropane 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP
4-Chlorotoluene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
4-Methyl-2-pentanone 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP
Acetone J 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 130 JSANELAP
Acrolein 6/18/2009 7:17:00 PM109 µg/Kg-dry 1ND JSANELAP
Acrylonitrile 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP
Allyl chloride 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Benzene 6/18/2009 7:17:00 PM1.1 µg/Kg-dry 1ND JSANELAP
Bromobenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Bromochloromethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Bromodichloromethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Bromoform 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Bromomethane 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP
Carbon disulfide 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Carbon tetrachloride 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Chlorobenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Chloroethane 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP
Chloroform 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Chloromethane 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP
cis-1,2-Dichloroethene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
cis-1,3-Dichloropropene 6/18/2009 7:17:00 PM4.4 µg/Kg-dry 1ND JSANELAP
Cyclohexanone 6/18/2009 7:17:00 PM109 µg/Kg-dry 1ND JSA
Dibromochloromethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Dibromomethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Dichlorodifluoromethane 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP
Ethyl acetate 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP
Ethyl ether 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Ethyl methacrylate 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Ethylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Heptane 6/18/2009 7:17:00 PM21.9 µg/Kg-dry 1ND JSA
IL ELAP and NELAP Accredited - Accreditation #100226 Page 8 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 1:30:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-001
Client Sample ID: CBA-01
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachlorobutadiene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Hexachloroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Iodomethane 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP
Isopropylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
m,p-Xylenes 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Methacrylonitrile 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP
Methyl Methacrylate 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Methyl tert-butyl ether 6/18/2009 7:17:00 PM2.2 µg/Kg-dry 1ND JSANELAP
Methylacrylate 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSA
Methylene chloride J 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 12.3 JSANELAP
Naphthalene 6/18/2009 7:17:00 PM10.9 µg/Kg-dry 1ND JSANELAP
n-Butylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
n-Hexane J 6/18/2009 7:17:00 PM21.9 µg/Kg-dry 12.5 JSA
Nitrobenzene 6/18/2009 7:17:00 PM109 µg/Kg-dry 1ND JSANELAP
n-Propylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
o-Xylene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Pentachloroethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
p-Isopropyltoluene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Propionitrile 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP
sec-Butylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Styrene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
tert-Butylbenzene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Tetrachloroethene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Tetrahydrofuran 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP
Toluene J 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 12.1 JSANELAP
trans-1,2-Dichloroethene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
trans-1,3-Dichloropropene 6/18/2009 7:17:00 PM4.4 µg/Kg-dry 1ND JSANELAP
Trichloroethene 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Trichlorofluoromethane 6/18/2009 7:17:00 PM5.5 µg/Kg-dry 1ND JSANELAP
Vinyl acetate 6/18/2009 7:17:00 PM54.7 µg/Kg-dry 1ND JSANELAP
Vinyl chloride 6/18/2009 7:17:00 PM2.2 µg/Kg-dry 1ND JSANELAP
Surr: 1,2-Dichloroethane-d4 6/18/2009 7:17:00 PM61-128 %REC 1122.5 JSA
Surr: 4-Bromofluorobenzene S 6/18/2009 7:17:00 PM78.2-117 %REC 171.3 JSA
Surr: Dibromofluoromethane 6/18/2009 7:17:00 PM66.6-130 %REC 1110.0 JSA
Surr: Toluene-d8 6/18/2009 7:17:00 PM80.1-122 %REC 1117.4 JSA
SW-846 7471AMercury 6/19/20090.013 mg/Kg-dry 10.041 MEKNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 9 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 1:30:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-001
Client Sample ID: CBA-01
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
Sample NarrativeSW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS
Elevated reporting limit due to high levels of target and/or non-target analytes.SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS
Matrix spike and RPD did not recover within control limits because of sample composition.SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS
Surrogate and Internal recoveries were outside QC limits due to matrix interference.
IL ELAP and NELAP Accredited - Accreditation #100226 Page 10 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 1:50:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-002
Client Sample ID: CBA-02
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
ASTM D2974Percent Moisture 6/18/2009 7:00:00 PM0.1 % 120.5 MAB
STANDARD METHODS 18TH ED. 2540 GTotal Solids 6/18/2009 7:00:00 PM0.1 % 179.5 MAB
SW-846 3050B, 6010B, METALS BY ICPArsenic 6/19/2009 1:20:54 PM2.45 mg/Kg-dry 16.95 LALNELAP
Barium 6/19/2009 1:20:54 PM0.49 mg/Kg-dry 1130 LALNELAP
Cadmium 6/19/2009 1:20:54 PM0.20 mg/Kg-dry 10.39 LALNELAP
Chromium 6/19/2009 1:20:54 PM0.98 mg/Kg-dry 120.5 LALNELAP
Lead 6/19/2009 1:03:31 PM3.92 mg/Kg-dry 167.6 LALNELAP
Silver 6/19/2009 1:20:54 PM0.54 mg/Kg-dry 1< 0.54 LALNELAP
SW-846 3050B, METALS BY GFAASelenium 7740 6/19/20090.600 mg/Kg-dry 1< 0.600 MEKNELAP
SW-846 3550B, 8081A, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
4,4´-DDE 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
4,4´-DDT 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
Alachlor 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
Aldrin 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
alpha-BHC 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
alpha-Chlordane 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
beta-BHC 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
Chlordane 6/19/2009 10:05:00 PM102 µg/Kg-dry 25ND HENELAP
delta-BHC 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
Dieldrin 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
Endosulfan I 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
Endosulfan II 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
Endosulfan sulfate 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
Endrin 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
Endrin aldehyde 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
Endrin ketone 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
gamma-BHC 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
gamma-Chlordane 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HE
Heptachlor 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
Heptachlor epoxide 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
Methoxychlor 6/19/2009 10:05:00 PM51.0 µg/Kg-dry 25ND HENELAP
Toxaphene 6/19/2009 10:05:00 PM916 µg/Kg-dry 25ND HENELAP
Surr: Decachlorobiphenyl 6/19/2009 10:05:00 PM48-149 %REC 2573.7 HE
Surr: Tetrachloro-m-xylene 6/19/2009 10:05:00 PM19-145 %REC 2565.6 HE
IL ELAP and NELAP Accredited - Accreditation #100226 Page 11 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 1:50:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-002
Client Sample ID: CBA-02
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 6/19/2009 10:42:00 AM45.8 µg/Kg-dry 1ND MAMNELAP
Aroclor 1221 6/19/2009 10:42:00 AM45.8 µg/Kg-dry 1ND MAMNELAP
Aroclor 1232 6/19/2009 10:42:00 AM45.8 µg/Kg-dry 1ND MAMNELAP
Aroclor 1242 6/19/2009 10:42:00 AM45.8 µg/Kg-dry 1ND MAMNELAP
Aroclor 1248 6/19/2009 10:42:00 AM45.8 µg/Kg-dry 1ND MAMNELAP
Aroclor 1254 6/19/2009 10:42:00 AM45.8 µg/Kg-dry 1ND MAMNELAP
Aroclor 1260 6/19/2009 10:42:00 AM45.8 µg/Kg-dry 1ND MAMNELAP
Surr: Decachlorobiphenyl 6/19/2009 10:42:00 AM5-156 %REC 171.7 MAM
Surr: Tetrachloro-meta-xylene 6/19/2009 10:42:00 AM7.35-123 %REC 162.9 MAM
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 2ND MAMNELAP
Acenaphthylene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 2ND MAMNELAP
Anthracene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 20.011 MAMNELAP
Benzo(a)anthracene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 20.054 MAMNELAP
Benzo(a)pyrene 6/19/2009 3:57:00 PM0.009 mg/Kg-dry 20.082 MAMNELAP
Benzo(b)fluoranthene 6/19/2009 3:57:00 PM0.009 mg/Kg-dry 20.122 MAMNELAP
Benzo(g,h,i)perylene 6/19/2009 3:57:00 PM0.009 mg/Kg-dry 20.038 MAMNELAP
Benzo(k)fluoranthene 6/19/2009 3:57:00 PM0.009 mg/Kg-dry 20.042 MAMNELAP
Bis(2-ethylhexyl)phthalate 6/19/2009 2:44:00 PM0.168 mg/Kg-dry 2ND MAMNELAP
Chrysene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 20.076 MAMNELAP
Dibenzo(a,h)anthracene 6/19/2009 3:57:00 PM0.009 mg/Kg-dry 20.009 MAMNELAP
Fluoranthene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 20.158 MAMNELAP
Fluorene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 2ND MAMNELAP
Indeno(1,2,3-cd)pyrene 6/19/2009 3:57:00 PM0.009 mg/Kg-dry 20.027 MAMNELAP
Naphthalene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 2ND MAMNELAP
Phenanthrene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 20.064 MAMNELAP
Pyrene 6/19/2009 2:44:00 PM0.009 mg/Kg-dry 20.124 MAMNELAP
Surr: 2-Fluorobiphenyl 6/19/2009 2:44:00 PM10-131 %REC 248.3 MAM
Surr: Nitrobenzene-d5 6/19/2009 2:44:00 PM10-132 %REC 263.1 MAM
Surr: p-Terphenyl-d14 6/19/2009 2:44:00 PM30.6-131 %REC 273.9 MAM
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
1,2-Dichlorobenzene 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
1,3-Dichlorobenzene 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
1,4-Dichlorobenzene 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
2,4,5-Trichlorophenol 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
2,4,6-Trichlorophenol 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
2,4-Dichlorophenol 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 12 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 1:50:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-002
Client Sample ID: CBA-02
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS2,4-Dimethylphenol 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
2,4-Dinitrophenol 6/20/2009 3:25:00 PM6.11 mg/Kg-dry 5ND DMHNELAP
2,4-Dinitrotoluene 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
2,6-Dinitrotoluene 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
2-Chloronaphthalene 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
2-Chlorophenol 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
2-Methoxy-4-methylphenol 6/20/2009 3:25:00 PM3.97 mg/Kg-dry 5ND DMH
2-Methylnaphthalene 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
2-Nitroaniline 6/20/2009 3:25:00 PM6.11 mg/Kg-dry 5ND DMHNELAP
2-Nitrophenol 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
3,3´-Dichlorobenzidine 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
3-Nitroaniline 6/20/2009 3:25:00 PM6.11 mg/Kg-dry 5ND DMHNELAP
4,6-Dinitro-2-methylphenol 6/20/2009 3:25:00 PM6.11 mg/Kg-dry 5ND DMHNELAP
4-Bromophenyl phenyl ether 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
4-Chloro-3-methylphenol 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
4-Chloroaniline 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
4-Chlorophenyl phenyl ether 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
4-Nitroaniline 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
4-Nitrophenol 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
Aniline 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
Azobenzene 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMH
Benzidine 6/20/2009 3:25:00 PM6.46 mg/Kg-dry 5ND DMHNELAP
Benzoic acid 6/20/2009 3:25:00 PM9.17 mg/Kg-dry 5ND DMHNELAP
Benzyl alcohol 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
Bis(2-chloroethoxy)methane 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
Bis(2-chloroethyl)ether 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
Bis(2-chloroisopropyl)ether 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
Butyl benzyl phthalate 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
Carbazole 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMH
Dibenzofuran 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
Diethyl phthalate 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
Dimethyl phthalate 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
Di-n-butyl phthalate 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
Di-n-octyl phthalate 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
Hexachlorobenzene 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
Hexachlorobutadiene 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
Hexachlorocyclopentadiene 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
Hexachloroethane 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 13 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 1:50:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-002
Client Sample ID: CBA-02
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSIsophorone 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
m,p-Cresol 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
Nitrobenzene 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
N-Nitrosodimethylamine 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
N-Nitroso-di-n-propylamine 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
N-Nitrosodiphenylamine 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
o-Cresol 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
Pentachlorophenol 6/20/2009 3:25:00 PM12.2 mg/Kg-dry 5ND DMHNELAP
Phenol 6/20/2009 3:25:00 PM2.14 mg/Kg-dry 5ND DMHNELAP
Pyridine 6/20/2009 3:25:00 PM3.06 mg/Kg-dry 5ND DMHNELAP
1,2-Diphenylhydrazine 6/20/2009 3:25:00 PM5.14 mg/Kg-dry 5ND DMH
Surr: 2,4,6-Tribromophenol 6/20/2009 3:25:00 PM32.7-130 %REC 568.2 DMH
Surr: 2-Fluorobiphenyl 6/20/2009 3:25:00 PM34.1-116 %REC 562.7 DMH
Surr: 2-Fluorophenol 6/20/2009 3:25:00 PM30.5-99 %REC 566.0 DMH
Surr: Nitrobenzene-d5 6/20/2009 3:25:00 PM34.1-101 %REC 561.3 DMH
Surr: Phenol-d5 6/20/2009 3:25:00 PM34.9-110 %REC 569.6 DMH
Surr: p-Terphenyl-d14 6/20/2009 3:25:00 PM41.7-124 %REC 571.9 DMH
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,1,1-Trichloroethane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,1,2,2-Tetrachloroethane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,1,2-Trichloro-1,2,2-trifluoroethane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSA
1,1,2-Trichloroethane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,1-Dichloro-2-propanone 6/18/2009 7:44:00 PM49.9 µg/Kg-dry 1ND JSA
1,1-Dichloroethane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,1-Dichloroethene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,1-Dichloropropene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,2,3-Trichlorobenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,2,3-Trichloropropane 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP
1,2,3-Trimethylbenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSA
1,2,4-Trichlorobenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,2,4-Trimethylbenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,2-Dibromo-3-chloropropane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,2-Dibromoethane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,2-Dichlorobenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,2-Dichloroethane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,2-Dichloropropane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,3,5-Trimethylbenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 14 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 1:50:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-002
Client Sample ID: CBA-02
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,3-Dichlorobenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,3-Dichloropropane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1,4-Dichlorobenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
1-Chlorobutane J 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 11.5 JSANELAP
2,2-Dichloropropane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
2-Butanone 6/18/2009 7:44:00 PM49.9 µg/Kg-dry 1ND JSANELAP
2-Chlorotoluene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
2-Hexanone 6/18/2009 7:44:00 PM49.9 µg/Kg-dry 1ND JSANELAP
2-Nitropropane 6/18/2009 7:44:00 PM49.9 µg/Kg-dry 1ND JSANELAP
4-Chlorotoluene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
4-Methyl-2-pentanone 6/18/2009 7:44:00 PM49.9 µg/Kg-dry 1ND JSANELAP
Acetone J 6/18/2009 7:44:00 PM49.9 µg/Kg-dry 142 JSANELAP
Acrolein 6/18/2009 7:44:00 PM99.8 µg/Kg-dry 1ND JSANELAP
Acrylonitrile 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP
Allyl chloride 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Benzene 6/18/2009 7:44:00 PM1.0 µg/Kg-dry 11.3 JSANELAP
Bromobenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Bromochloromethane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Bromodichloromethane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Bromoform 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Bromomethane 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP
Carbon disulfide J 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 13.2 JSANELAP
Carbon tetrachloride 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Chlorobenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Chloroethane 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP
Chloroform 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Chloromethane 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP
cis-1,2-Dichloroethene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
cis-1,3-Dichloropropene 6/18/2009 7:44:00 PM4.0 µg/Kg-dry 1ND JSANELAP
Cyclohexanone 6/18/2009 7:44:00 PM99.8 µg/Kg-dry 1ND JSA
Dibromochloromethane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Dibromomethane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Dichlorodifluoromethane 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP
Ethyl acetate 6/18/2009 7:44:00 PM49.9 µg/Kg-dry 1ND JSANELAP
Ethyl ether 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Ethyl methacrylate 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Ethylbenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Heptane 6/18/2009 7:44:00 PM20.0 µg/Kg-dry 1ND JSA
IL ELAP and NELAP Accredited - Accreditation #100226 Page 15 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 1:50:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-002
Client Sample ID: CBA-02
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachlorobutadiene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Hexachloroethane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Iodomethane 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP
Isopropylbenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
m,p-Xylenes 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Methacrylonitrile 6/18/2009 7:44:00 PM49.9 µg/Kg-dry 1ND JSANELAP
Methyl Methacrylate 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Methyl tert-butyl ether 6/18/2009 7:44:00 PM2.0 µg/Kg-dry 1ND JSANELAP
Methylacrylate 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSA
Methylene chloride J 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 12.6 JSANELAP
Naphthalene 6/18/2009 7:44:00 PM10 µg/Kg-dry 1ND JSANELAP
n-Butylbenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
n-Hexane J 6/18/2009 7:44:00 PM20.0 µg/Kg-dry 12.1 JSA
Nitrobenzene 6/18/2009 7:44:00 PM99.8 µg/Kg-dry 1ND JSANELAP
n-Propylbenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
o-Xylene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Pentachloroethane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
p-Isopropyltoluene J 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 11.2 JSANELAP
Propionitrile 6/18/2009 7:44:00 PM49.9 µg/Kg-dry 1ND JSANELAP
sec-Butylbenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Styrene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
tert-Butylbenzene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Tetrachloroethene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Tetrahydrofuran 6/18/2009 7:44:00 PM49.9 µg/Kg-dry 1ND JSANELAP
Toluene J 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 12.4 JSANELAP
trans-1,2-Dichloroethene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
trans-1,3-Dichloropropene 6/18/2009 7:44:00 PM4.0 µg/Kg-dry 1ND JSANELAP
Trichloroethene 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Trichlorofluoromethane 6/18/2009 7:44:00 PM5.0 µg/Kg-dry 1ND JSANELAP
Vinyl acetate 6/18/2009 7:44:00 PM49.9 µg/Kg-dry 1ND JSANELAP
Vinyl chloride 6/18/2009 7:44:00 PM2.0 µg/Kg-dry 1ND JSANELAP
Surr: 1,2-Dichloroethane-d4 6/18/2009 7:44:00 PM61-128 %REC 1124.8 JSA
Surr: 4-Bromofluorobenzene S 6/18/2009 7:44:00 PM78.2-117 %REC 168.5 JSA
Surr: Dibromofluoromethane 6/18/2009 7:44:00 PM66.6-130 %REC 1113.0 JSA
Surr: Toluene-d8 6/18/2009 7:44:00 PM80.1-122 %REC 1121.1 JSA
SW-846 7471AMercury 6/19/20090.012 mg/Kg-dry 10.043 MEKNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 16 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 1:50:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-002
Client Sample ID: CBA-02
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
Sample NarrativeSW-846 3550B, 8081A, Chlorinated Pesticides by GC/ECD
Elevated reporting limit due to high levels of target and/or non-target analytes.SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS
Elevated reporting limit due to high levels of target and/or non-target analytes.SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS
Perylene-d12 was outside of QC limits due to matrix interference, subsequent analysis showed same results.Elevated reporting limit due to high levels of target and/or non-target analytes.
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS
Surrogate and Internal recoveries were outside QC limits due to matrix interference.
IL ELAP and NELAP Accredited - Accreditation #100226 Page 17 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 2:10:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-003
Client Sample ID: CBA-03
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
ASTM D2974Percent Moisture 6/18/2009 7:00:00 PM0.1 % 115.7 MAB
STANDARD METHODS 18TH ED. 2540 GTotal Solids 6/18/2009 7:00:00 PM0.1 % 184.3 MAB
SW-846 3050B, 6010B, METALS BY ICPArsenic 6/19/2009 1:27:39 PM2.40 mg/Kg-dry 16.56 LALNELAP
Barium 6/19/2009 1:27:39 PM0.48 mg/Kg-dry 196.9 LALNELAP
Cadmium 6/19/2009 1:27:39 PM0.19 mg/Kg-dry 10.33 LALNELAP
Chromium 6/19/2009 1:27:39 PM0.96 mg/Kg-dry 120.1 LALNELAP
Lead 6/19/2009 1:06:35 PM3.85 mg/Kg-dry 113.7 LALNELAP
Silver 6/19/2009 1:27:39 PM0.53 mg/Kg-dry 1< 0.53 LALNELAP
SW-846 3050B, METALS BY GFAASelenium 7740 6/19/20090.577 mg/Kg-dry 1< 0.577 MEKNELAP
SW-846 3550B, 8081A, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
4,4´-DDE 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
4,4´-DDT 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
Alachlor 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
Aldrin 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
alpha-BHC 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
alpha-Chlordane 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
beta-BHC 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
Chlordane 6/19/2009 10:29:00 PM96.8 µg/Kg-dry 25ND HENELAP
delta-BHC 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
Dieldrin 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
Endosulfan I 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
Endosulfan II 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
Endosulfan sulfate 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
Endrin 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
Endrin aldehyde 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
Endrin ketone 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
gamma-BHC 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
gamma-Chlordane 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HE
Heptachlor 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
Heptachlor epoxide 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
Methoxychlor 6/19/2009 10:29:00 PM48.4 µg/Kg-dry 25ND HENELAP
Toxaphene 6/19/2009 10:29:00 PM870 µg/Kg-dry 25ND HENELAP
Surr: Decachlorobiphenyl 6/19/2009 10:29:00 PM48-149 %REC 2575.6 HE
Surr: Tetrachloro-m-xylene 6/19/2009 10:29:00 PM19-145 %REC 2544.5 HE
IL ELAP and NELAP Accredited - Accreditation #100226 Page 18 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 2:10:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-003
Client Sample ID: CBA-03
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 6/19/2009 11:34:00 AM43.5 µg/Kg-dry 1ND MAMNELAP
Aroclor 1221 6/19/2009 11:34:00 AM43.5 µg/Kg-dry 1ND MAMNELAP
Aroclor 1232 6/19/2009 11:34:00 AM43.5 µg/Kg-dry 1ND MAMNELAP
Aroclor 1242 6/19/2009 11:34:00 AM43.5 µg/Kg-dry 1ND MAMNELAP
Aroclor 1248 6/19/2009 11:34:00 AM43.5 µg/Kg-dry 1ND MAMNELAP
Aroclor 1254 6/19/2009 11:34:00 AM43.5 µg/Kg-dry 1ND MAMNELAP
Aroclor 1260 6/19/2009 11:34:00 AM43.5 µg/Kg-dry 1ND MAMNELAP
Surr: Decachlorobiphenyl 6/19/2009 11:34:00 AM5-156 %REC 167.6 MAM
Surr: Tetrachloro-meta-xylene 6/19/2009 11:34:00 AM7.35-123 %REC 135.2 MAM
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 2ND MAMNELAP
Acenaphthylene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 2ND MAMNELAP
Anthracene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 2ND MAMNELAP
Benzo(a)anthracene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 20.015 MAMNELAP
Benzo(a)pyrene 6/19/2009 4:34:00 PM0.008 mg/Kg-dry 20.017 MAMNELAP
Benzo(b)fluoranthene 6/19/2009 4:34:00 PM0.008 mg/Kg-dry 20.026 MAMNELAP
Benzo(g,h,i)perylene 6/19/2009 4:34:00 PM0.008 mg/Kg-dry 20.012 MAMNELAP
Benzo(k)fluoranthene 6/19/2009 4:34:00 PM0.008 mg/Kg-dry 20.009 MAMNELAP
Bis(2-ethylhexyl)phthalate 6/19/2009 3:20:00 PM0.160 mg/Kg-dry 2ND MAMNELAP
Chrysene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 20.011 MAMNELAP
Dibenzo(a,h)anthracene 6/19/2009 4:34:00 PM0.008 mg/Kg-dry 2ND MAMNELAP
Fluoranthene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 20.029 MAMNELAP
Fluorene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 2ND MAMNELAP
Indeno(1,2,3-cd)pyrene 6/19/2009 4:34:00 PM0.008 mg/Kg-dry 2ND MAMNELAP
Naphthalene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 2ND MAMNELAP
Phenanthrene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 20.012 MAMNELAP
Pyrene 6/19/2009 3:20:00 PM0.008 mg/Kg-dry 20.024 MAMNELAP
Surr: 2-Fluorobiphenyl 6/19/2009 3:20:00 PM10-131 %REC 243.5 MAM
Surr: Nitrobenzene-d5 6/19/2009 3:20:00 PM10-132 %REC 260.7 MAM
Surr: p-Terphenyl-d14 6/19/2009 3:20:00 PM30.6-131 %REC 279.4 MAM
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
1,2-Dichlorobenzene 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
1,3-Dichlorobenzene 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
1,4-Dichlorobenzene 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
2,4,5-Trichlorophenol 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
2,4,6-Trichlorophenol 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
2,4-Dichlorophenol 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 19 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 2:10:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-003
Client Sample ID: CBA-03
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS2,4-Dimethylphenol 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
2,4-Dinitrophenol S 6/20/2009 3:55:00 PM5.86 mg/Kg-dry 5ND DMHNELAP
2,4-Dinitrotoluene 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
2,6-Dinitrotoluene 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
2-Chloronaphthalene 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
2-Chlorophenol 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
2-Methoxy-4-methylphenol 6/20/2009 3:55:00 PM3.81 mg/Kg-dry 5ND DMH
2-Methylnaphthalene 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
2-Nitroaniline 6/20/2009 3:55:00 PM5.86 mg/Kg-dry 5ND DMHNELAP
2-Nitrophenol 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
3,3´-Dichlorobenzidine 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
3-Nitroaniline 6/20/2009 3:55:00 PM5.86 mg/Kg-dry 5ND DMHNELAP
4,6-Dinitro-2-methylphenol 6/20/2009 3:55:00 PM5.86 mg/Kg-dry 5ND DMHNELAP
4-Bromophenyl phenyl ether 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
4-Chloro-3-methylphenol 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
4-Chloroaniline 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
4-Chlorophenyl phenyl ether 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
4-Nitroaniline 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
4-Nitrophenol 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
Aniline 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
Azobenzene 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMH
Benzidine 6/20/2009 3:55:00 PM6.19 mg/Kg-dry 5ND DMHNELAP
Benzoic acid 6/20/2009 3:55:00 PM8.79 mg/Kg-dry 5ND DMHNELAP
Benzyl alcohol 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
Bis(2-chloroethoxy)methane 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
Bis(2-chloroethyl)ether 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
Bis(2-chloroisopropyl)ether 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
Butyl benzyl phthalate 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
Carbazole 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMH
Dibenzofuran 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
Diethyl phthalate 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
Dimethyl phthalate 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
Di-n-butyl phthalate 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
Di-n-octyl phthalate 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
Hexachlorobenzene 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
Hexachlorobutadiene 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
Hexachlorocyclopentadiene 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
Hexachloroethane 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 20 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 2:10:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-003
Client Sample ID: CBA-03
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSIsophorone 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
m,p-Cresol 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
Nitrobenzene 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
N-Nitrosodimethylamine 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
N-Nitroso-di-n-propylamine 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
N-Nitrosodiphenylamine 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
o-Cresol 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
Pentachlorophenol S 6/20/2009 3:55:00 PM11.7 mg/Kg-dry 5ND DMHNELAP
Phenol 6/20/2009 3:55:00 PM2.05 mg/Kg-dry 5ND DMHNELAP
Pyridine 6/20/2009 3:55:00 PM2.93 mg/Kg-dry 5ND DMHNELAP
1,2-Diphenylhydrazine 6/20/2009 3:55:00 PM4.92 mg/Kg-dry 5ND DMH
Surr: 2,4,6-Tribromophenol 6/20/2009 3:55:00 PM32.7-130 %REC 569.9 DMH
Surr: 2-Fluorobiphenyl 6/20/2009 3:55:00 PM34.1-116 %REC 562.7 DMH
Surr: 2-Fluorophenol 6/20/2009 3:55:00 PM30.5-99 %REC 569.7 DMH
Surr: Nitrobenzene-d5 6/20/2009 3:55:00 PM34.1-101 %REC 565.5 DMH
Surr: Phenol-d5 6/20/2009 3:55:00 PM34.9-110 %REC 573.6 DMH
Surr: p-Terphenyl-d14 6/20/2009 3:55:00 PM41.7-124 %REC 583.6 DMH
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,1,1-Trichloroethane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,1,2,2-Tetrachloroethane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,1,2-Trichloro-1,2,2-trifluoroethane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSA
1,1,2-Trichloroethane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,1-Dichloro-2-propanone 6/18/2009 8:11:00 PM45.6 µg/Kg-dry 1ND JSA
1,1-Dichloroethane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,1-Dichloroethene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,1-Dichloropropene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,2,3-Trichlorobenzene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,2,3-Trichloropropane 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSANELAP
1,2,3-Trimethylbenzene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSA
1,2,4-Trichlorobenzene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,2,4-Trimethylbenzene J 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 11.7 JSANELAP
1,2-Dibromo-3-chloropropane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,2-Dibromoethane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,2-Dichlorobenzene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,2-Dichloroethane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,2-Dichloropropane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,3,5-Trimethylbenzene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 21 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 2:10:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-003
Client Sample ID: CBA-03
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,3-Dichlorobenzene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,3-Dichloropropane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1,4-Dichlorobenzene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
1-Chlorobutane J 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 13.0 JSANELAP
2,2-Dichloropropane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
2-Butanone 6/18/2009 8:11:00 PM45.6 µg/Kg-dry 1ND JSANELAP
2-Chlorotoluene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
2-Hexanone 6/18/2009 8:11:00 PM45.6 µg/Kg-dry 1ND JSANELAP
2-Nitropropane 6/18/2009 8:11:00 PM45.6 µg/Kg-dry 1ND JSANELAP
4-Chlorotoluene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
4-Methyl-2-pentanone 6/18/2009 8:11:00 PM45.6 µg/Kg-dry 1ND JSANELAP
Acetone J 6/18/2009 8:11:00 PM45.6 µg/Kg-dry 137 JSANELAP
Acrolein 6/18/2009 8:11:00 PM91.1 µg/Kg-dry 1ND JSANELAP
Acrylonitrile 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSANELAP
Allyl chloride 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Benzene 6/18/2009 8:11:00 PM0.9 µg/Kg-dry 12.4 JSANELAP
Bromobenzene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Bromochloromethane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Bromodichloromethane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Bromoform 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Bromomethane J 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 12.2 JSANELAP
Carbon disulfide 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Carbon tetrachloride 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Chlorobenzene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Chloroethane 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSANELAP
Chloroform 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Chloromethane 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSANELAP
cis-1,2-Dichloroethene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
cis-1,3-Dichloropropene 6/18/2009 8:11:00 PM3.6 µg/Kg-dry 1ND JSANELAP
Cyclohexanone 6/18/2009 8:11:00 PM91.1 µg/Kg-dry 1ND JSA
Dibromochloromethane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Dibromomethane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Dichlorodifluoromethane 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSANELAP
Ethyl acetate 6/18/2009 8:11:00 PM45.6 µg/Kg-dry 1ND JSANELAP
Ethyl ether 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Ethyl methacrylate 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Ethylbenzene J 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 11.4 JSANELAP
Heptane 6/18/2009 8:11:00 PM18.2 µg/Kg-dry 1ND JSA
IL ELAP and NELAP Accredited - Accreditation #100226 Page 22 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 2:10:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-003
Client Sample ID: CBA-03
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachlorobutadiene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Hexachloroethane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Iodomethane 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSANELAP
Isopropylbenzene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
m,p-Xylenes J 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 12.0 JSANELAP
Methacrylonitrile 6/18/2009 8:11:00 PM45.6 µg/Kg-dry 1ND JSANELAP
Methyl Methacrylate 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Methyl tert-butyl ether 6/18/2009 8:11:00 PM1.8 µg/Kg-dry 1ND JSANELAP
Methylacrylate 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSA
Methylene chloride J 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 12.1 JSANELAP
Naphthalene 6/18/2009 8:11:00 PM9.1 µg/Kg-dry 1ND JSANELAP
n-Butylbenzene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
n-Hexane J 6/18/2009 8:11:00 PM18.2 µg/Kg-dry 15.5 JSA
Nitrobenzene 6/18/2009 8:11:00 PM91.1 µg/Kg-dry 1ND JSANELAP
n-Propylbenzene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
o-Xylene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Pentachloroethane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
p-Isopropyltoluene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Propionitrile 6/18/2009 8:11:00 PM45.6 µg/Kg-dry 1ND JSANELAP
sec-Butylbenzene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Styrene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
tert-Butylbenzene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Tetrachloroethene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Tetrahydrofuran 6/18/2009 8:11:00 PM45.6 µg/Kg-dry 1ND JSANELAP
Toluene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 14.8 JSANELAP
trans-1,2-Dichloroethene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
trans-1,3-Dichloropropene 6/18/2009 8:11:00 PM3.6 µg/Kg-dry 1ND JSANELAP
Trichloroethene 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Trichlorofluoromethane 6/18/2009 8:11:00 PM4.6 µg/Kg-dry 1ND JSANELAP
Vinyl acetate 6/18/2009 8:11:00 PM45.6 µg/Kg-dry 1ND JSANELAP
Vinyl chloride 6/18/2009 8:11:00 PM1.8 µg/Kg-dry 1ND JSANELAP
Surr: 1,2-Dichloroethane-d4 6/18/2009 8:11:00 PM61-128 %REC 1124.7 JSA
Surr: 4-Bromofluorobenzene S 6/18/2009 8:11:00 PM78.2-117 %REC 174.7 JSA
Surr: Dibromofluoromethane 6/18/2009 8:11:00 PM66.6-130 %REC 1111.0 JSA
Surr: Toluene-d8 6/18/2009 8:11:00 PM80.1-122 %REC 1114.3 JSA
SW-846 7471AMercury 6/19/20090.012 mg/Kg-dry 10.025 MEKNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 23 of 54
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 6/18/2009 2:10:00 PM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 22-Jun-09
LABORATORY RESULTS
WorkOrder: 09060783
Lab ID: 09060783-003
Client Sample ID: CBA-03
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
Sample NarrativeSW-846 3550B, 8081A, Chlorinated Pesticides by GC/ECD
Elevated reporting limit due to high levels of target and/or non-target analytes.SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS
Matrix spike did not recover within control limits because of sample dilution.Elevated reporting limit due to high levels of target and/or non-target analytes.
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS
Perylene-d12 was outside of QC limits due to matrix interference, subsequent analysis showed same results.Elevated reporting limit due to high levels of target and/or non-target analytes.
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS
Surrogate and Internal recoveries were outside QC limits due to matrix interference.
IL ELAP and NELAP Accredited - Accreditation #100226 Page 24 of 54
Sample ID Client Sample ID Collection Date MatrixAnalysis
Date/Time
DATES REPORT
Lab Order: 09060783
Client: PSC Industrial Outsourcing, LPProject: A831-735002-012901-225/Ameren Champaign 62403053
Test NamePrep
Date/Time
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
22-Jun-09Report Date:
09060783-001A CBA-01 6/18/2009 Solid SW-846 3550B, 8081A, Chlorinated Pesticides by GC/ECD
6/19/2009 9:40:00 PM
6/18/2009 7:44:41 PM
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD
6/19/2009 10:25:00 AM
6/18/2009 7:44:41 PM
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS
6/19/2009 10:54:00 AM
6/18/2009 6:53:02 PM
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS
6/20/2009 2:55:00 PM
6/18/2009 6:15:00 PM
09060783-001B SW-846 3050B, 6010B, Metals by ICP 6/19/2009 1:00:26 PM
6/19/2009 7:18:14 AM
SW-846 3050B, 6010B, Metals by ICP 6/19/2009 1:14:06 PM
6/19/2009 7:18:14 AM
SW-846 3050B, Metals by GFAA 6/19/20096/19/2009 7:17:04 AM
SW-846 7471A 6/19/20096/19/2009 8:31:07 AM
09060783-001C ASTM D2974 6/18/2009 7:00:00 PM
Standard Methods 18th Ed. 2540 G 6/18/2009 7:00:00 PM
09060783-001F SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS
6/18/2009 7:17:00 PM
6/18/2009 6:25:00 PM
09060783-002A CBA-02 SW-846 3550B, 8081A, Chlorinated Pesticides by GC/ECD
6/19/2009 10:05:00 PM
6/18/2009 7:44:41 PM
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD
6/19/2009 10:42:00 AM
6/18/2009 7:44:41 PM
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS
6/19/2009 1:31:00 PM
6/18/2009 6:53:02 PM
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS
6/19/2009 2:44:00 PM
6/18/2009 6:53:02 PM
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS
6/19/2009 3:57:00 PM
6/18/2009 6:53:02 PM
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS
6/20/2009 3:25:00 PM
6/18/2009 6:15:00 PM
09060783-002B SW-846 3050B, 6010B, Metals by ICP 6/19/2009 1:03:31 PM
6/19/2009 7:18:14 AM
SW-846 3050B, 6010B, Metals by ICP 6/19/2009 1:20:54 PM
6/19/2009 7:18:14 AM
SW-846 3050B, Metals by GFAA 6/19/20096/19/2009 7:17:04 AM
SW-846 7471A 6/19/20096/19/2009 8:31:07 AM
09060783-002C ASTM D2974 6/18/2009 7:00:00 PM
Page 25 of 54IL ELAP and NELAP Accredited - Accreditation #100226
Sample ID Client Sample ID Collection Date MatrixAnalysis
Date/Time
DATES REPORT
Lab Order: 09060783
Client: PSC Industrial Outsourcing, LPProject: A831-735002-012901-225/Ameren Champaign 62403053
Test NamePrep
Date/Time
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
22-Jun-09Report Date:
09060783-002C CBA-02 6/18/2009 Solid Standard Methods 18th Ed. 2540 G 6/18/2009 7:00:00 PM
09060783-002F SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS
6/18/2009 7:44:00 PM
6/18/2009 6:25:00 PM
09060783-003A CBA-03 SW-846 3550B, 8081A, Chlorinated Pesticides by GC/ECD
6/19/2009 10:29:00 PM
6/18/2009 7:44:41 PM
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD
6/19/2009 11:34:00 AM
6/18/2009 7:44:41 PM
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS
6/19/2009 2:08:00 PM
6/18/2009 6:53:02 PM
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS
6/19/2009 3:20:00 PM
6/18/2009 6:53:02 PM
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS
6/19/2009 4:34:00 PM
6/18/2009 6:53:02 PM
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS
6/20/2009 3:55:00 PM
6/18/2009 6:15:00 PM
09060783-003B SW-846 3050B, 6010B, Metals by ICP 6/19/2009 1:06:35 PM
6/19/2009 7:18:14 AM
SW-846 3050B, 6010B, Metals by ICP 6/19/2009 1:27:39 PM
6/19/2009 7:18:14 AM
SW-846 3050B, Metals by GFAA 6/19/20096/19/2009 7:17:04 AM
SW-846 7471A 6/19/20096/19/2009 8:31:07 AM
09060783-003C ASTM D2974 6/18/2009 7:00:00 PM
Standard Methods 18th Ed. 2540 G 6/18/2009 7:00:00 PM
09060783-003F SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS
6/18/2009 8:11:00 PM
6/18/2009 6:25:00 PM
Page 26 of 54IL ELAP and NELAP Accredited - Accreditation #100226
TEKLAB, INC 5445 HORSESHOE LAKE ROADCOLLINSVILLE, ILLINOIS 62234
ANALYTICAL QC SUMMARY REPORT
Qualifiers
- Analyte detected below reporting limits
- Analyte detected in the associated Method Blank
- Spike Recovery outside accepted recovery limits
- RPD outside accepted recovery limits- Not Detected at the Reporting Limit - Value above quantitation range
- Value exceeds Maximum Contaminant Level
- Reporting Limit
- Dilution Factor
- Too numerous to count ( > 200 CFU )
- Diluted out of sample
- Holding time exceeded- Surrogate Standard added by lab
- Matrix interference
- IL Dept. of Public Health
- IL ELAP and NELAP Accredited
DF
RL
TNTC
Surr
IDPH
B
J
R
S
X NELAP
E
MI
H
ND
D - Did not igniteDNI
- Unknown hydrocarbon#
- QC criteria failedQ
- Client requested RL below PQLC
CCV
DF
DUP
ICV
LCS
MS
MSD
MDL
MB/LCB
PQL
RL
RPD
Continuing calibration verification is a check of a standard to determine the state of calibration of an instrument between recalibration.
Dilution factor is the dilution performed during analysis only and does not take into account any dilutions made during sample preparation. The reported result is final and includes all dilutions factors.Laboratory duplicate is an aliquot of a sample taken from the same container under laboratory conditions for independent processing and analysis independently of the original aliquot. (NELAC)Initial calibration verification is a check of a standard to determine the state of calibration of an instrument before sample analysis is initiated.
Laboratory control sample, spiked with verified known amounts of analytes, is analyzed exactly like a sample to establish intra-laboratory or analyst specific precision and bias or to assess the performance of all or a portion of the measurement system. (NELAC) The acceptable recovery range is listed in this report.Matrix spike is an aliquot of matrix fortified (spiked) with known quantities of specific analytes that is subjected to the entire analytical procedures in order to determine the effect of the matrix on an approved test method’s recovery system. The acceptable recovery range is listed in this report.Matrix spike duplicate means a replicate matrix spike that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in this report.Method detection limit or limit of detection (LOD) means the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type containing the analyte.Method blank or lab control blank is a sample of a matrix similar to the batch of associated sample (when available) that is free from the analytes of interest and is processed simultaneously with and under the same conditions as samples through all steps of the analytical procedures, and in which no target analytes or interferences are present at concentrations that impact the analytical results for sample analyses. (NELAC)Practical quantitation limit or limit of quantitation (LOQ) means the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine laboratory operation conditions. The acceptable recovery range is listed in this report.The reporting limit the lowest level that the data is displayed in the final report. The reporting limit may vary according to customer request or sample dilution. The reporting limit may not be less than the MDL.Relative percent difference is a calculated difference between two recoveries (ie. MS/MSD). The acceptable recovery limit is listed in this report.
SPK The spike is a known mass of target analyte added to a blank sample or sub-sample; used to determine recovery deficiency or for other quality control purposes. (NELAC)
Surr Surrogates are an organic compound which is similar to the analytes of interest in chemical composition and behavior in the analytical process, but which is not normally found in environmental samples.
Key QC concepts:
Page 27 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: I_TS_M_MT
22-Jun-09Report Date:
Sample ID: LCS-R123687
Batch ID: R123687 Analysis Date: 6/18/2009
Prep Date:
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: %
PQL
Client ID: ZZZZZZ
RunNo: 123687
SeqNo: 2312130
LCSSampType:
Total Solids 1.000 100 90 1100.1 01.0
Sample ID: LCSQC
Batch ID: R123687 Analysis Date: 6/18/2009
Prep Date:
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: %
PQL
Client ID: ZZZZZZ
RunNo: 123687
SeqNo: 2312131
LCSQCSampType:
Total Solids 1.000 100 90 1100.1 01.0
Sample ID: 09060783-001CDUP
Batch ID: R123687 Analysis Date: 6/18/2009
Prep Date:
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: %
PQL
Client ID: CBA-01DUP
RunNo: 123687
SeqNo: 2312152
DUPSampType:
Total Solids 150.1 77.14 0.94277.9
Page 28 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: M_HG_SOLID
22-Jun-09Report Date:
Sample ID: MB-53683
Batch ID: 53683 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123669
SeqNo: 2311746
MBLKSampType:
SOP 3063
Mercury 0.01000 30.0 -100 100 J0.010 00.003
Sample ID: LCS-53683
Batch ID: 53683 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123669
SeqNo: 2311747
LCSSampType:
SOP 3063
Mercury 0.2500 97.0 85 1150.010 00.243
Sample ID: 09060783-001BMS
Batch ID: 53683 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-01MS
RunNo: 123669
SeqNo: 2311749
MSSampType:
SOP 3063
Mercury 0.3201 93.2 75 1250.013 0.040970.339
Sample ID: 09060783-001BMSD
Batch ID: 53683 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-01MSD
RunNo: 123669
SeqNo: 2311750
MSDSampType:
SOP 3063
Mercury 0.3201 92.2 75 125 150.013 0.04097 0.3393 0.9480.336
Page 29 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: M_SOLID_GF
22-Jun-09Report Date:
Sample ID: MB-53674
Batch ID: 53674 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 123678
SeqNo: 2311985
MBLKSampType:
SOP 3042
Selenium 7740 0.6000 0 -100 1000.600 0< 0.600
Sample ID: LCS-53674
Batch ID: 53674 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 123678
SeqNo: 2311986
LCSSampType:
SOP 3042
Selenium 7740 3.000 105.4 80 1200.600 03.16
Sample ID: 09060783-002BMS
Batch ID: 53674 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-02MS
RunNo: 123678
SeqNo: 2311988
MSSampType:
SOP 3042
Selenium 7740 3.000 83.6 70 1300.600 02.51
Sample ID: 09060783-002BMSD
Batch ID: 53674 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-02MSD
RunNo: 123678
SeqNo: 2311989
MSDSampType:
SOP 3042
Selenium 7740 3.000 79.8 70 130 200.600 0 2.507 4.632.39
Page 30 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: M_SOLIDS_ICP
22-Jun-09Report Date:
Sample ID: MB-53675
Batch ID: 53675 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 123642
SeqNo: 2311887
MBLKSampType:
SOP 3032
Lead 4.000 0 -100 1004.00 0< 4.00
Sample ID: LCS-53675
Batch ID: 53675 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 123642
SeqNo: 2311888
LCSSampType:
SOP 3032
Lead 50.00 93.9 85 1154.00 047.0
Sample ID: 09060783-003BMS
Batch ID: 53675 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-03MS
RunNo: 123642
SeqNo: 2311893
MSSampType:
SOP 3032
Lead 48.08 82.6 75 1253.85 13.6953.4
Sample ID: 09060783-003BMSD
Batch ID: 53675 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-03MSD
RunNo: 123642
SeqNo: 2311894
MSDSampType:
SOP 3032
Lead 48.08 97.2 75 125 203.85 13.69 53.39 12.360.4
Sample ID: MB-53675
Batch ID: 53675 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 123641
SeqNo: 2311908
MBLKSampType:
SOP 3032
Arsenic 2.500 0 -100 1002.50 0< 2.50
Barium 0.5000 0 -100 1000.50 0< 0.50
Cadmium 0.2000 0 -100 1000.20 0< 0.20
Chromium 1.000 0 -100 1001.00 0< 1.00
Silver 1.000 0 -100 1000.55 0< 0.55
Page 31 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: M_SOLIDS_ICP
22-Jun-09Report Date:
Sample ID: LCS-53675
Batch ID: 53675 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 123641
SeqNo: 2311909
LCSSampType:
SOP 3032
Arsenic 200.0 102.0 85 1152.50 0204
Barium 200.0 111.0 85 1150.50 0222
Cadmium 5.000 102.2 85 1150.20 05.11
Chromium 20.00 112.7 85 1151.00 022.5
Silver 5.000 94.2 85 1150.55 04.71
Sample ID: 09060783-003BMS
Batch ID: 53675 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-03MS
RunNo: 123641
SeqNo: 2311914
MSSampType:
SOP 3032
Arsenic 192.3 93.9 75 1252.40 6.558187
Barium 192.3 90.4 75 1250.48 96.92271
Cadmium 4.808 86.4 75 1250.19 0.32694.48
Chromium 19.23 97.0 75 1250.96 20.1438.8
Silver 4.808 105.8 75 1250.53 05.09
Sample ID: 09060783-003BMSD
Batch ID: 53675 Analysis Date: 6/19/2009
Prep Date: 6/19/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-03MSD
RunNo: 123641
SeqNo: 2311915
MSDSampType:
SOP 3032
Arsenic 192.3 96.2 75 125 202.40 6.558 187.2 2.34192
Barium 192.3 95.7 75 125 200.48 96.92 270.7 3.73281
Cadmium 4.808 89.0 75 125 200.19 0.3269 4.481 2.754.61
Chromium 19.23 116.2 75 125 200.96 20.14 38.80 9.0842.5
Silver 4.808 102.6 75 125 200.53 0 5.087 3.074.93
Page 32 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8081S_S
22-Jun-09Report Date:
Sample ID: MB-53670
Batch ID: 53670 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123709
SeqNo: 2312609
MBLKSampType:
SW3550B
4,4´-DDD 1.67ND
4,4´-DDE 1.67ND
4,4´-DDT 1.67ND
Alachlor 1.67ND
Aldrin 1.67ND
alpha-BHC 1.67ND
alpha-Chlordane 1.67ND
beta-BHC 1.67ND
Chlordane 3.34ND
delta-BHC 1.67ND
Dieldrin 1.67ND
Endosulfan I 1.67ND
Endosulfan II 1.67ND
Endosulfan sulfate 1.67ND
Endrin 1.67ND
Endrin aldehyde 1.67ND
Endrin ketone 1.67ND
gamma-BHC 1.67ND
gamma-Chlordane 1.67ND
Heptachlor 1.67ND
Heptachlor epoxide 1.67ND
Methoxychlor 1.67ND
Toxaphene 30.0ND
Surr: Decachlorobiphenyl 8.330 88.7 73.5 1507.39
Surr: Tetrachloro-m-xylene 8.330 78.3 14.4 1136.52
Sample ID: LCSPST-53670
Batch ID: 53670 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123709
SeqNo: 2312610
LCSSampType:
SW3550B
4,4´-DDD 8.330 91.4 36 2081.67 07.61
Page 33 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8081S_S
22-Jun-09Report Date:
Sample ID: LCSPST-53670
Batch ID: 53670 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123709
SeqNo: 2312610
LCSSampType:
SW3550B
4,4´-DDE 8.330 101.4 26 1911.67 08.45
4,4´-DDT 8.330 107.3 3 2151.67 08.94
Alachlor 8.330 87.2 30 1701.67 07.27
Aldrin 8.330 86.9 46 1731.67 07.24
alpha-BHC 8.330 83.5 37 1791.67 06.96
alpha-Chlordane 8.330 97.9 38 1871.67 08.16
beta-BHC 8.330 94.7 51 1851.67 07.88
delta-BHC 8.330 61.1 46 1661.67 05.09
Dieldrin 8.330 94.6 26 2161.67 07.88
Endosulfan I 8.330 97.9 31 2051.67 08.16
Endosulfan II 8.330 78.1 42 1871.67 06.51
Endosulfan sulfate 8.330 102.8 29 2301.67 08.56
Endrin 8.330 98.0 30 2151.67 08.16
Endrin aldehyde 8.330 59.3 42 2021.67 04.94
Endrin ketone 8.330 71.9 19 2441.67 05.99
gamma-BHC 8.330 86.4 55 1661.67 07.20
gamma-Chlordane 8.330 96.5 23 1861.67 08.04
Heptachlor 8.330 94.7 43 1721.67 07.89
Heptachlor epoxide 8.330 95.7 39 2041.67 07.97
Methoxychlor 8.330 110.9 3 2211.67 09.24
Surr: Decachlorobiphenyl 8.330 90.9 50.4 1767.57
Surr: Tetrachloro-m-xylene 8.330 76.3 10 1076.36
Sample ID: LCSPSTD-53670
Batch ID: 53670 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123709
SeqNo: 2312611
LCSDSampType:
SW3550B
4,4´-DDD 8.330 87.5 36 208 401.67 0 7.612 4.377.29
4,4´-DDE 8.330 96.5 26 191 401.67 0 8.449 4.978.04
4,4´-DDT 8.330 102.8 3 215 401.67 0 8.939 4.268.57
Alachlor 8.330 92.8 30 170 401.67 0 7.266 6.167.73
Page 34 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8081S_S
22-Jun-09Report Date:
Sample ID: LCSPSTD-53670
Batch ID: 53670 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123709
SeqNo: 2312611
LCSDSampType:
SW3550B
Aldrin 8.330 79.8 46 173 401.67 0 7.242 8.516.65
alpha-BHC 8.330 76.1 37 179 401.67 0 6.957 9.336.34
alpha-Chlordane 8.330 93.1 38 187 401.67 0 8.159 5.067.76
beta-BHC 8.330 89.9 51 185 401.67 0 7.885 5.127.49
delta-BHC 8.330 57.7 46 166 401.67 0 5.091 5.764.81
Dieldrin 8.330 90.7 26 216 401.67 0 7.879 4.217.55
Endosulfan I 8.330 93.1 31 205 401.67 0 8.159 5.067.76
Endosulfan II 8.330 74.3 42 187 401.67 0 6.507 4.946.19
Endosulfan sulfate 8.330 97.8 29 230 401.67 0 8.560 4.978.15
Endrin 8.330 93.0 30 215 401.67 0 8.164 5.247.75
Endrin aldehyde 8.330 55.7 42 202 401.67 0 4.942 6.274.64
Endrin ketone 8.330 68.6 19 244 401.67 0 5.991 4.665.72
gamma-BHC 8.330 79.7 55 166 401.67 0 7.197 8.126.64
gamma-Chlordane 8.330 91.7 23 186 401.67 0 8.035 5.097.64
Heptachlor 8.330 87.5 43 172 401.67 0 7.885 7.917.29
Heptachlor epoxide 8.330 93.6 39 204 401.67 0 7.968 2.227.79
Methoxychlor 8.330 106.4 3 221 401.67 0 9.237 4.148.86
Surr: Decachlorobiphenyl 8.330 89.6 50.4 176 4007.46
Surr: Tetrachloro-m-xylene 8.330 74.0 10 107 4006.16
Page 35 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8082S_S
22-Jun-09Report Date:
Sample ID: MB-53670
Batch ID: 53670 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123671
SeqNo: 2311838
MBLKSampType:
SW3550B
Aroclor 1016 37.5ND
Aroclor 1221 37.5ND
Aroclor 1232 37.5ND
Aroclor 1242 37.5ND
Aroclor 1248 37.5ND
Aroclor 1254 37.5ND
Aroclor 1260 37.5ND
Surr: Decachlorobiphenyl 8.300 113.2 47.2 1289.4
Surr: Tetrachloro-meta-xylene 8.300 85.9 21 98.97.1
Sample ID: LCSPCB-53670
Batch ID: 53670 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123671
SeqNo: 2311839
LCSSampType:
SW3550B
Aroclor 1016 166.7 116.0 54.9 12137.5 0193
Aroclor 1260 166.7 115.5 65.5 13337.5 0192
Surr: Decachlorobiphenyl 8.300 116.6 47.2 1289.7
Surr: Tetrachloro-meta-xylene 8.300 94.7 21 98.97.9
Sample ID: 09060783-002AMS
Batch ID: 53670 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg-dry
PQL
Client ID: CBA-02MS
RunNo: 123671
SeqNo: 2311842
MSSampType:
SW3550B
Aroclor 1016 208.8 104.4 35.8 14347.0 0218
Aroclor 1260 208.8 97.5 22.3 15247.0 0204
Surr: Decachlorobiphenyl 10.40 91.0 5 1569.5
Surr: Tetrachloro-meta-xylene 10.40 86.0 7.35 1238.9
Page 36 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8082S_S
22-Jun-09Report Date:
Sample ID: 09060783-002AMSD
Batch ID: 53670 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg-dry
PQL
Client ID: CBA-02MSD
RunNo: 123671
SeqNo: 2311843
MSDSampType:
SW3550B
Aroclor 1016 212.7 103.9 35.8 143 4047.9 0 218.0 1.34221
Aroclor 1260 212.7 91.4 22.3 152 4047.9 0 203.7 4.58195
Surr: Decachlorobiphenyl 10.59 86.5 5 156 4009.2
Surr: Tetrachloro-meta-xylene 10.59 83.1 7.35 123 4008.8
Page 37 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S
22-Jun-09Report Date:
Sample ID: MB-53651
Batch ID: 53651 Analysis Date: 6/20/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123696
SeqNo: 2312251
MBLKSampType:
SW3550B
1,2,4-Trichlorobenzene 0.500ND
1,2-Dichlorobenzene 0.500ND
1,3-Dichlorobenzene 0.500ND
1,4-Dichlorobenzene 0.500ND
2,4,5-Trichlorophenol 0.350ND
2,4,6-Trichlorophenol 0.350ND
2,4-Dichlorophenol 0.500ND
2,4-Dimethylphenol 0.500ND
2,4-Dinitrophenol 1.00ND
2,4-Dinitrotoluene 0.350ND
2,6-Dinitrotoluene 0.350ND
2-Chloronaphthalene 0.350ND
2-Chlorophenol 0.500ND
2-Methoxy-4-methylphenol 0.650ND
2-Methylnaphthalene 0.350ND
2-Nitroaniline 1.00ND
2-Nitrophenol 0.350ND
3,3´-Dichlorobenzidine 0.350ND
3-Nitroaniline 1.00ND
4,6-Dinitro-2-methylphenol 1.00ND
4-Bromophenyl phenyl ether 0.350ND
4-Chloro-3-methylphenol 0.500ND
4-Chloroaniline 0.500ND
4-Chlorophenyl phenyl ether 0.350ND
4-Nitroaniline 0.500ND
4-Nitrophenol 0.350ND
Acenaphthene 0.350ND
Acenaphthylene 0.350ND
Aniline 0.500ND
Anthracene 0.350ND
Azobenzene 0.350ND
Page 38 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S
22-Jun-09Report Date:
Sample ID: MB-53651
Batch ID: 53651 Analysis Date: 6/20/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123696
SeqNo: 2312251
MBLKSampType:
SW3550B
Benzidine 1.06ND
Benzo(a)anthracene 0.350ND
Benzo(a)pyrene 0.350ND
Benzo(b)fluoranthene 0.350ND
Benzo(g,h,i)perylene 0.350ND
Benzo(k)fluoranthene 0.350ND
Benzoic acid 1.50ND
Benzyl alcohol 0.500ND
Bis(2-chloroethoxy)methane 0.350ND
Bis(2-chloroethyl)ether 0.500ND
Bis(2-chloroisopropyl)ether 0.350ND
Bis(2-ethylhexyl)phthalate 0.350ND
Butyl benzyl phthalate 0.350ND
Carbazole 0.500ND
Chrysene 0.350ND
Dibenzo(a,h)anthracene 0.350ND
Dibenzofuran 0.350ND
Diethyl phthalate 0.500ND
Dimethyl phthalate 0.350ND
Di-n-butyl phthalate 0.350ND
Di-n-octyl phthalate 0.350ND
Fluoranthene 0.350ND
Fluorene 0.350ND
Hexachlorobenzene 0.350ND
Hexachlorobutadiene 0.500ND
Hexachlorocyclopentadiene 0.350ND
Hexachloroethane 0.500ND
Indeno(1,2,3-cd)pyrene 0.350ND
Isophorone 0.350ND
m,p-Cresol 0.500ND
Naphthalene 0.350ND
Page 39 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S
22-Jun-09Report Date:
Sample ID: MB-53651
Batch ID: 53651 Analysis Date: 6/20/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123696
SeqNo: 2312251
MBLKSampType:
SW3550B
Nitrobenzene 0.500ND
N-Nitrosodimethylamine 0.500ND
N-Nitroso-di-n-propylamine 0.500ND
N-Nitrosodiphenylamine 0.500ND
o-Cresol 0.500ND
Pentachlorophenol 2.00ND
Phenanthrene 0.350ND
Phenol 0.350ND
Pyrene 0.500ND
Pyridine 0.500ND
1,2-Diphenylhydrazine 0.840ND
Surr: 2,4,6-Tribromophenol 1.670 86.8 52.1 1131.45
Surr: 2-Fluorobiphenyl 0.8350 92.6 46.3 1060.773
Surr: 2-Fluorophenol 1.670 80.8 50.6 891.35
Surr: Nitrobenzene-d5 0.8350 80.5 42.4 99.20.672
Surr: Phenol-d5 1.670 83.1 55.9 98.51.39
Surr: p-Terphenyl-d14 0.8350 93.4 45.5 1150.780
Sample ID: LCS-53651
Batch ID: 53651 Analysis Date: 6/20/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123696
SeqNo: 2312252
LCSSampType:
SW3550B
1,2,4-Trichlorobenzene 1.670 89.4 43.9 92.20.500 01.49
1,4-Dichlorobenzene 1.670 72.3 43.8 84.10.500 01.21
2,4,5-Trichlorophenol 3.330 95.8 38.6 1230.350 03.19
2,4,6-Trichlorophenol 3.330 88.8 35.9 1230.350 02.96
2,4-Dimethylphenol 3.330 56.4 38.3 880.500 01.88
2,4-Dinitrophenol 3.330 77.0 1.88 1621.00 02.56
2,4-Dinitrotoluene 1.670 93.0 48.6 1020.350 01.55
2-Chlorophenol 3.330 74.5 46.6 840.500 02.48
4-Chloro-3-methylphenol 3.330 86.5 51.5 94.90.500 02.88
Page 40 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S
22-Jun-09Report Date:
Sample ID: LCS-53651
Batch ID: 53651 Analysis Date: 6/20/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123696
SeqNo: 2312252
LCSSampType:
SW3550B
4-Nitrophenol 3.330 85.4 53.2 1040.350 02.84
Acenaphthene 1.670 84.7 50.8 1130.350 01.41
Acenaphthylene 1.670 122.6 52.8 121 S0.350 02.05
Anthracene 1.670 80.4 53.3 1150.350 01.34
Benzo(a)anthracene 1.670 77.9 62.3 1100.350 01.30
Benzo(a)pyrene 1.670 84.0 58.2 1090.350 01.40
Benzo(b)fluoranthene 1.670 73.4 51.8 1070.350 01.23
Benzo(g,h,i)perylene 1.670 89.4 49.6 1210.350 01.49
Benzo(k)fluoranthene 1.670 94.8 63.1 1290.350 01.58
Bis(2-ethylhexyl)phthalate 1.670 79.5 56.3 1090.350 01.33
Chrysene 1.670 96.3 58.4 1150.350 01.61
Dibenzo(a,h)anthracene 1.670 88.2 54.9 1200.350 01.47
Diethyl phthalate 3.330 81.3 51.7 1060.500 02.71
Dimethyl phthalate 3.330 86.7 58.8 1040.350 02.89
Di-n-butyl phthalate 1.670 84.7 54.3 1050.350 01.41
Fluoranthene 1.670 84.8 61.6 1130.350 01.42
Fluorene 1.670 87.7 52.2 1160.350 01.46
Hexachlorobenzene 3.330 84.9 55.9 1060.350 02.83
Hexachlorobutadiene 3.330 91.2 35.7 1000.500 03.04
Hexachloroethane 3.330 73.1 38.9 89.90.500 02.43
Indeno(1,2,3-cd)pyrene 1.670 87.5 52.7 1150.350 01.46
m,p-Cresol 1.670 70.6 37.6 93.70.500 01.18
Naphthalene 1.670 74.9 45.7 1010.350 01.25
Nitrobenzene 3.330 75.7 51.8 1040.500 02.52
N-Nitroso-di-n-propylamine 1.670 74.2 49.1 94.50.500 01.24
o-Cresol 1.670 73.4 43 1010.500 01.23
Pentachlorophenol 3.330 77.8 42.2 1022.00 02.59
Phenanthrene 1.670 87.0 52.9 1130.350 01.45
Phenol 3.330 70.9 41.6 81.30.350 02.36
Pyrene 1.670 93.2 60.7 1150.500 01.56
Pyridine 3.330 49.3 3.61 74.30.500 01.64
Page 41 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S
22-Jun-09Report Date:
Sample ID: LCS-53651
Batch ID: 53651 Analysis Date: 6/20/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123696
SeqNo: 2312252
LCSSampType:
SW3550B
Surr: 2,4,6-Tribromophenol 1.670 84.2 52.1 1131.41
Surr: 2-Fluorobiphenyl 0.8350 84.0 46.3 1060.701
Surr: 2-Fluorophenol 1.670 68.2 50.6 891.14
Surr: Nitrobenzene-d5 0.8350 71.0 42.4 99.20.593
Surr: Phenol-d5 1.670 71.0 55.9 98.51.19
Surr: p-Terphenyl-d14 0.8350 85.3 45.5 1150.713
Sample ID: 09060783-003AMS
Batch ID: 53651 Analysis Date: 6/20/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-03MS
RunNo: 123696
SeqNo: 2312256
MSSampType:
SW3550B
1,2,4-Trichlorobenzene 1.974 78.2 35.9 102 J2.96 01.5
1,4-Dichlorobenzene 1.974 56.8 29.8 95.5 J2.96 01.1
2,4,5-Trichlorophenol 3.937 73.2 38.6 1232.07 02.88
2,4,6-Trichlorophenol 3.937 74.5 35.9 1232.07 02.93
2,4-Dimethylphenol 3.937 64.3 38.3 88 J2.96 02.5
2,4-Dinitrotoluene 1.974 67.8 37.5 107 J2.07 01.3
2-Chlorophenol 3.937 60.5 22.6 108 J2.96 02.4
4-Chloro-3-methylphenol 3.937 71.9 19.3 131 J2.96 02.8
4-Nitrophenol 3.937 65.8 27.6 1232.07 02.59
Benzoic acid 0 0 0 08.87 0ND
Diethyl phthalate 3.937 72.5 51.7 106 J2.96 02.8
Dimethyl phthalate 3.937 73.5 58.8 1042.07 02.90
Di-n-butyl phthalate 1.974 73.1 54.3 105 J2.07 01.4
Hexachlorobenzene 3.937 81.2 55.9 1062.07 03.20
Hexachlorobutadiene 3.937 80.2 35.7 1002.96 03.16
Hexachloroethane 3.937 53.6 38.9 89.9 J2.96 02.1
m,p-Cresol 1.974 66.8 37.6 93.7 J2.96 01.3
Nitrobenzene 3.937 68.6 51.8 104 J2.96 02.7
N-Nitroso-di-n-propylamine 1.974 66.4 45.5 99.1 J2.96 01.3
o-Cresol 1.974 63.7 43 101 J2.96 01.3
Page 42 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S
22-Jun-09Report Date:
Sample ID: 09060783-003AMS
Batch ID: 53651 Analysis Date: 6/20/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-03MS
RunNo: 123696
SeqNo: 2312256
MSSampType:
SW3550B
Phenol 3.937 61.7 20.8 1102.07 02.43
Pyridine 3.937 40.8 3.61 74.3 J2.96 01.6
Surr: 2,4,6-Tribromophenol 1.974 62.0 32.7 1301.22
Surr: 2-Fluorobiphenyl 0.9871 44.9 34.1 1160.443
Surr: 2-Fluorophenol 1.974 55.6 30.5 991.10
Surr: Nitrobenzene-d5 0.9871 57.9 34.1 1010.571
Surr: Phenol-d5 1.974 59.5 34.9 1101.17
Surr: p-Terphenyl-d14 0.9871 68.9 41.7 1240.680
Sample ID: 09060783-003AMSD
Batch ID: 53651 Analysis Date: 6/20/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-03MSD
RunNo: 123696
SeqNo: 2312257
MSDSampType:
SW3550B
1,2,4-Trichlorobenzene 1.944 81.4 35.9 102 40 J2.91 0 1.544 01.6
1,4-Dichlorobenzene 1.944 68.0 29.8 95.5 40 J2.91 0 1.122 01.3
2,4,5-Trichlorophenol 3.876 81.2 38.6 123 402.04 0 2.884 8.773.15
2,4,6-Trichlorophenol 3.876 79.3 35.9 123 402.04 0 2.934 4.623.07
2,4-Dimethylphenol 3.876 67.2 38.3 88 40 J2.91 0 2.530 02.6
2,4-Dinitrotoluene 1.944 70.3 37.5 107 40 J2.04 0 1.339 01.4
2-Chlorophenol 3.876 63.2 22.6 108 40 J2.91 0 2.380 02.4
4-Chloro-3-methylphenol 3.876 72.0 19.3 131 40 J2.91 0 2.830 02.8
4-Nitrophenol 3.876 66.7 27.6 123 402.04 0 2.591 0.1742.59
Benzoic acid 0 0 0 0 08.73 0 0 0ND
Diethyl phthalate 3.876 75.4 51.7 106 402.91 0 2.853 2.392.92
Dimethyl phthalate 3.876 76.4 58.8 104 402.04 0 2.895 2.322.96
Di-n-butyl phthalate 1.944 76.7 54.3 105 40 J2.04 0 1.444 01.5
Hexachlorobenzene 3.876 81.9 55.9 106 402.04 0 3.198 0.7513.17
Hexachlorobutadiene 3.876 82.4 35.7 100 402.91 0 3.157 1.133.19
Hexachloroethane 3.876 62.9 38.9 89.9 40 J2.91 0 2.111 02.4
m,p-Cresol 1.944 68.6 37.6 93.7 40 J2.91 0 1.318 01.3
Nitrobenzene 3.876 73.2 51.8 104 40 J2.91 0 2.701 02.8
Page 43 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S
22-Jun-09Report Date:
Sample ID: 09060783-003AMSD
Batch ID: 53651 Analysis Date: 6/20/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-03MSD
RunNo: 123696
SeqNo: 2312257
MSDSampType:
SW3550B
N-Nitroso-di-n-propylamine 1.944 66.7 45.5 99.1 40 J2.91 0 1.312 01.3
o-Cresol 1.944 65.4 43 101 40 J2.91 0 1.257 01.3
Phenol 3.876 63.2 20.8 110 402.04 0 2.427 0.9762.45
Pyridine 3.876 44.8 3.61 74.3 40 J2.91 0 1.604 01.7
Surr: 2,4,6-Tribromophenol 1.944 65.8 32.7 130 4001.28
Surr: 2-Fluorobiphenyl 0.9720 62.9 34.1 116 4000.611
Surr: 2-Fluorophenol 1.944 58.9 30.5 99 4001.14
Surr: Nitrobenzene-d5 0.9720 47.1 34.1 101 4000.458
Surr: Phenol-d5 1.944 62.2 34.9 110 4001.21
Surr: p-Terphenyl-d14 0.9720 75.8 41.7 124 4000.737
Page 44 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S_SIMS
22-Jun-09Report Date:
Sample ID: MB-53669
Batch ID: 53669 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123660
SeqNo: 2311601
MBLKSampType:
SW3550B
Acenaphthene 0.003ND
Acenaphthylene 0.003ND
Anthracene 0.003ND
Benzo(a)anthracene 0.003ND
Benzo(a)pyrene 0.003ND
Benzo(b)fluoranthene 0.003ND
Benzo(g,h,i)perylene 0.003ND
Benzo(k)fluoranthene 0.003ND
Bis(2-ethylhexyl)phthalate 0.067ND
Chrysene 0.003ND
Dibenzo(a,h)anthracene 0.003ND
Fluoranthene 0.003ND
Fluorene 0.003ND
Indeno(1,2,3-cd)pyrene 0.003ND
Naphthalene 0.003ND
Phenanthrene 0.003ND
Pyrene 0.003ND
Surr: 2-Fluorobiphenyl 0.1670 68.7 17.5 1230.115
Surr: Nitrobenzene-d5 0.1670 66.9 35 1050.112
Surr: p-Terphenyl-d14 0.1670 92.2 53.6 1220.154
Sample ID: 09060783-001AMS
Batch ID: 53669 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-01MS
RunNo: 123660
SeqNo: 2311715
MSSampType:
SW3550B
Acenaphthene 0.2176 48.3 36 1350.004 00.105
Acenaphthylene 0.2176 53.0 17.2 1670.004 00.115
Anthracene 0.2176 49.3 39.3 1240.004 0.0043600.112
Benzo(a)anthracene 0.2176 55.7 10 1830.004 0.036300.157
Benzo(a)pyrene 0.2176 69.2 10 2040.004 0.042260.193
Benzo(b)fluoranthene 0.2176 71.9 10.6 1780.004 0.063330.220
Page 45 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S_SIMS
22-Jun-09Report Date:
Sample ID: 09060783-001AMS
Batch ID: 53669 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-01MS
RunNo: 123660
SeqNo: 2311715
MSSampType:
SW3550B
Benzo(g,h,i)perylene 0.2176 57.6 10 1680.004 0.031560.157
Benzo(k)fluoranthene 0.2176 66.0 27.6 1810.004 0.022840.167
Bis(2-ethylhexyl)phthalate 0.2176 -14.1 50 150 S0.087 0.16620.136
Chrysene 0.2176 62.2 10 1760.004 0.048910.184
Dibenzo(a,h)anthracene 0.2176 54.6 12.2 1560.004 0.0072520.126
Fluoranthene 0.2176 74.6 10 2270.004 0.11060.273
Fluorene 0.2176 49.8 35.2 1480.004 00.108
Indeno(1,2,3-cd)pyrene 0.2176 63.1 10 1640.004 0.027150.164
Naphthalene 0.2176 43.3 14.7 1280.004 00.094
Phenanthrene 0.2176 58.1 32.8 1430.004 0.038510.165
Pyrene 0.2176 71.5 10 1800.004 0.088190.244
Surr: 2-Fluorobiphenyl 0.2176 44.9 10 1310.098
Surr: Nitrobenzene-d5 0.2176 43.1 10 1320.094
Surr: p-Terphenyl-d14 0.2176 59.9 30.6 1310.130
Sample ID: LCS-53669
Batch ID: 53669 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123660
SeqNo: 2311874
LCSSampType:
SW3550B
Acenaphthene 0.1670 62.8 56.3 1150.003 00.105
Acenaphthylene 0.1670 66.6 60.3 1430.003 00.111
Anthracene 0.1670 61.1 52.1 1090.003 00.102
Benzo(a)anthracene 0.1670 62.0 52.8 1120.003 00.104
Benzo(a)pyrene 0.1670 67.7 40.8 1270.003 00.113
Benzo(b)fluoranthene 0.1670 73.9 50.1 1500.003 00.123
Benzo(g,h,i)perylene 0.1670 68.1 52.8 1450.003 00.114
Benzo(k)fluoranthene 0.1670 73.6 52 1530.003 00.123
Bis(2-ethylhexyl)phthalate 0.1670 77.2 50 1500.067 00.129
Chrysene 0.1670 68.0 60.8 1280.003 00.114
Dibenzo(a,h)anthracene 0.1670 70.9 54.9 1500.003 00.118
Fluoranthene 0.1670 73.6 58.7 1250.003 00.123
Page 46 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S_SIMS
22-Jun-09Report Date:
Sample ID: LCS-53669
Batch ID: 53669 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123660
SeqNo: 2311874
LCSSampType:
SW3550B
Fluorene 0.1670 66.9 57.8 1250.003 00.112
Indeno(1,2,3-cd)pyrene 0.1670 73.7 52 1470.003 00.123
Naphthalene 0.1670 59.0 54.8 1130.003 00.099
Phenanthrene 0.1670 66.8 60.4 1210.003 00.112
Pyrene 0.1670 76.1 57.9 1290.003 00.127
Surr: 2-Fluorobiphenyl 0.1670 68.9 35.3 1130.115
Surr: Nitrobenzene-d5 0.1670 65.5 33.9 1080.109
Surr: p-Terphenyl-d14 0.1670 87.2 58.4 1220.146
Sample ID: 09060783-001AMSD
Batch ID: 53669 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-01MSD
RunNo: 123660
SeqNo: 2311875
MSDSampType:
SW3550B
Acenaphthene 0.2150 69.7 36 135 49.70.004 0 0.1051 35.10.150
Acenaphthylene 0.2150 70.8 17.2 167 33.30.004 0 0.1153 27.70.152
Anthracene 0.2150 76.0 39.3 124 51.10.004 0.004360 0.1117 40.20.168
Benzo(a)anthracene 0.2150 91.7 10 183 40.60.004 0.03630 0.1575 38.80.233
Benzo(a)pyrene 0.2150 110.5 10 204 56.40.004 0.04226 0.1929 36.80.280
Benzo(b)fluoranthene 0.2150 139.6 10.6 178 49.70.004 0.06333 0.2198 49.20.363
Benzo(g,h,i)perylene 0.2150 58.7 10 168 36.50.004 0.03156 0.1569 0.5580.158
Benzo(k)fluoranthene 0.2150 110.6 27.6 181 42.6 R0.004 0.02284 0.1665 44.10.261
Bis(2-ethylhexyl)phthalate 0.2150 14.4 50 150 60.3 S0.086 0.1662 0.1356 37.00.197
Chrysene 0.2150 105.3 10 176 45.10.004 0.04891 0.1842 39.60.275
Dibenzo(a,h)anthracene 0.2150 60.1 12.2 156 39.90.004 0.007252 0.1259 8.010.136
Fluoranthene 0.2150 155.9 10 227 66.20.004 0.1106 0.2729 48.10.446
Fluorene 0.2150 72.7 35.2 148 65.60.004 0 0.1084 36.20.156
Indeno(1,2,3-cd)pyrene 0.2150 70.2 10 164 36.50.004 0.02715 0.1644 7.980.178
Naphthalene 0.2150 64.1 14.7 128 39.60.004 0 0.09411 37.70.138
Phenanthrene 0.2150 114.4 32.8 143 35.4 R0.004 0.03851 0.1649 53.20.284
Pyrene 0.2150 140.8 10 180 60.10.004 0.08819 0.2437 46.40.391
Surr: 2-Fluorobiphenyl 0.2150 61.1 10 131 4000.131
Page 47 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S_SIMS
22-Jun-09Report Date:
Sample ID: 09060783-001AMSD
Batch ID: 53669 Analysis Date: 6/19/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: CBA-01MSD
RunNo: 123660
SeqNo: 2311875
MSDSampType:
SW3550B
Surr: Nitrobenzene-d5 0.2150 65.3 10 132 4000.140
Surr: p-Terphenyl-d14 0.2150 81.6 30.6 131 4000.176
Page 48 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: V_8260S_S
22-Jun-09Report Date:
Sample ID: LCS-F090618-2
Batch ID: 53680 Analysis Date: 6/18/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123640
SeqNo: 2311283
LCSSampType:
SW5035
1,1,1-Trichloroethane 50.00 105.1 77.5 1215.0 052.5
1,1-Dichloroethene 50.00 103.5 52 1335.0 051.8
1,2-Dibromoethane 50.00 101.2 85.2 1195.0 050.6
1,2-Dichlorobenzene 50.00 107.9 84.2 1225.0 054.0
1,2-Dichloroethane 50.00 108.9 71.1 1255.0 054.5
1,3-Dichlorobenzene 50.00 110.2 83.3 1255.0 055.1
1,4-Dichlorobenzene 50.00 107.0 81.9 1285.0 053.5
2-Butanone 100.0 56.0 39.1 10550.0 056.0
Benzene 50.00 104.4 77.9 1231.0 052.2
Bromodichloromethane 50.00 115.9 87.9 1195.0 057.9
Carbon tetrachloride 50.00 112.4 77.5 1285.0 056.2
Chlorobenzene 50.00 108.2 87.8 1205.0 054.1
Chloroform 50.00 100 81.5 1195.0 050.0
Dibromochloromethane 50.00 109.6 88.6 1195.0 054.8
Ethylbenzene 50.00 108.7 80.9 1195.0 054.4
m,p-Xylenes 50.00 104.9 77.6 1205.0 052.5
Methyl tert-butyl ether 50.00 104.6 69.8 1212.0 052.3
Methylene chloride 50.00 99.3 71.5 1245.0 049.7
Naphthalene 50.00 118.1 75.7 12310 059.0
o-Xylene 50.00 101.2 82.4 1245.0 050.6
Tetrachloroethene 50.00 96.3 74.2 1135.0 048.2
Toluene 50.00 104.4 80.2 1155.0 052.2
Trichloroethene 50.00 105.3 83.3 1185.0 052.6
Surr: 1,2-Dichloroethane-d4 50.00 109.3 61 12854.6
Surr: 4-Bromofluorobenzene 50.00 96.5 78.2 11748.3
Surr: Dibromofluoromethane 50.00 102.6 66.6 13051.3
Surr: Toluene-d8 50.00 93.9 80.1 12247.0
Page 49 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: V_8260S_S
22-Jun-09Report Date:
Sample ID: LCSD-F090618-2
Batch ID: 53680 Analysis Date: 6/18/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123640
SeqNo: 2311284
LCSDSampType:
SW5035
1,1,1-Trichloroethane 50.00 102.8 77.5 121 205.0 0 52.53 2.1951.4
1,1-Dichloroethene 50.00 98.9 52 133 205.0 0 51.75 4.5149.5
1,2-Dibromoethane 50.00 97.2 85.2 119 205.0 0 50.58 4.0148.6
1,2-Dichlorobenzene 50.00 103.5 84.2 122 205.0 0 53.96 4.1851.8
1,2-Dichloroethane 50.00 107.0 71.1 125 205.0 0 54.47 1.8353.5
1,3-Dichlorobenzene 50.00 105.6 83.3 125 205.0 0 55.08 4.2652.8
1,4-Dichlorobenzene 50.00 102.7 81.9 128 205.0 0 53.52 4.1851.3
2-Butanone 100.0 51.5 39.1 105 2050.0 0 55.95 8.2451.5
Benzene 50.00 101.6 77.9 123 201.0 0 52.20 2.7650.8
Bromodichloromethane 50.00 113.4 87.9 119 205.0 0 57.93 2.1656.7
Carbon tetrachloride 50.00 109.0 77.5 128 205.0 0 56.19 3.0954.5
Chlorobenzene 50.00 106.0 87.8 120 205.0 0 54.11 2.0353.0
Chloroform 50.00 98.2 81.5 119 205.0 0 49.99 1.7649.1
Dibromochloromethane 50.00 106.7 88.6 119 205.0 0 54.78 2.6353.4
Ethylbenzene 50.00 105.7 80.9 119 205.0 0 54.36 2.7852.9
m,p-Xylenes 50.00 103.3 77.6 120 205.0 0 52.46 1.5851.6
Methyl tert-butyl ether 50.00 99.7 69.8 121 202.0 0 52.32 4.8449.8
Methylene chloride 50.00 97.0 71.5 124 205.0 0 49.67 2.3848.5
Naphthalene 50.00 110.5 75.7 123 2010 0 59.05 6.6155.3
o-Xylene 50.00 99.4 82.4 124 205.0 0 50.59 1.7349.7
Tetrachloroethene 50.00 92.4 74.2 113 205.0 0 48.17 4.1546.2
Toluene 50.00 102.8 80.2 115 205.0 0 52.21 1.5451.4
Trichloroethene 50.00 101.6 83.3 118 205.0 0 52.64 3.5850.8
Surr: 1,2-Dichloroethane-d4 50.00 108.5 61 128 0054.2
Surr: 4-Bromofluorobenzene 50.00 97.3 78.2 117 0048.6
Surr: Dibromofluoromethane 50.00 102.2 66.6 130 0051.1
Surr: Toluene-d8 50.00 94.5 80.1 122 0047.2
Page 50 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: V_8260S_S
22-Jun-09Report Date:
Sample ID: MBLK-F090618-2
Batch ID: 53680 Analysis Date: 6/18/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123640
SeqNo: 2311285
MBLKSampType:
SW5035
1,1,1,2-Tetrachloroethane 5.0ND
1,1,1-Trichloroethane 5.0ND
1,1,2,2-Tetrachloroethane 5.0ND
1,1,2-Trichloro-1,2,2-trifluoroethane 5.0ND
1,1,2-Trichloroethane 5.0ND
1,1-Dichloro-2-propanone 50.0ND
1,1-Dichloroethane 5.0ND
1,1-Dichloroethene 5.0ND
1,1-Dichloropropene 5.0ND
1,2,3-Trichlorobenzene 5.0ND
1,2,3-Trichloropropane 10ND
1,2,3-Trimethylbenzene 5.0ND
1,2,4-Trichlorobenzene 5.0ND
1,2,4-Trimethylbenzene 5.0ND
1,2-Dibromo-3-chloropropane 5.0ND
1,2-Dibromoethane 5.0ND
1,2-Dichlorobenzene 5.0ND
1,2-Dichloroethane 5.0ND
1,2-Dichloropropane 5.0ND
1,3,5-Trimethylbenzene 5.0ND
1,3-Dichlorobenzene 5.0ND
1,3-Dichloropropane 5.0ND
1,4-Dichlorobenzene 5.0ND
1-Chlorobutane 5.0ND
2,2-Dichloropropane 5.0ND
2-Butanone 50.0ND
2-Chlorotoluene 5.0ND
2-Hexanone 50.0ND
2-Nitropropane 50.0ND
4-Chlorotoluene 5.0ND
4-Methyl-2-pentanone 50.0ND
Page 51 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: V_8260S_S
22-Jun-09Report Date:
Sample ID: MBLK-F090618-2
Batch ID: 53680 Analysis Date: 6/18/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123640
SeqNo: 2311285
MBLKSampType:
SW5035
Acetone 50.0ND
Acrolein 100ND
Acrylonitrile 10ND
Allyl chloride 5.0ND
Benzene 1.0ND
Bromobenzene 5.0ND
Bromochloromethane 5.0ND
Bromodichloromethane 5.0ND
Bromoform 5.0ND
Bromomethane 10ND
Carbon disulfide 5.0ND
Carbon tetrachloride 5.0ND
Chlorobenzene 5.0ND
Chloroethane 10ND
Chloroform 5.0ND
Chloromethane 10ND
cis-1,2-Dichloroethene 5.0ND
cis-1,3-Dichloropropene 4.0ND
Cyclohexanone 100ND
Dibromochloromethane 5.0ND
Dibromomethane 5.0ND
Dichlorodifluoromethane 10ND
Ethyl acetate 50.0ND
Ethyl ether 5.0ND
Ethyl methacrylate 5.0ND
Ethylbenzene 5.0ND
Heptane 20.0ND
Hexachlorobutadiene 5.0ND
Hexachloroethane 5.0ND
Iodomethane 10ND
Isopropylbenzene 5.0ND
Page 52 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
ANALYTICAL QC SUMMARY REPORTTestCode: V_8260S_S
22-Jun-09Report Date:
Sample ID: MBLK-F090618-2
Batch ID: 53680 Analysis Date: 6/18/2009
Prep Date: 6/18/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 123640
SeqNo: 2311285
MBLKSampType:
SW5035
m,p-Xylenes 5.0ND
Methacrylonitrile 50.0ND
Methyl Methacrylate 5.0ND
Methyl tert-butyl ether 2.0ND
Methylacrylate 10ND
Methylene chloride 5.0ND
Naphthalene 10ND
n-Butylbenzene 5.0ND
n-Hexane 20.0ND
Nitrobenzene 100ND
n-Propylbenzene 5.0ND
o-Xylene 5.0ND
Pentachloroethane 5.0ND
p-Isopropyltoluene 5.0ND
Propionitrile 50.0ND
sec-Butylbenzene 5.0ND
Styrene 5.0ND
tert-Butylbenzene 5.0ND
Tetrachloroethene 5.0ND
Tetrahydrofuran 50.0ND
Toluene 5.0ND
trans-1,2-Dichloroethene 5.0ND
trans-1,3-Dichloropropene 4.0ND
Trichloroethene 5.0ND
Trichlorofluoromethane 5.0ND
Vinyl acetate 50.0ND
Vinyl chloride 2.0ND
Surr: 1,2-Dichloroethane-d4 50.00 110.2 61 12855.1
Surr: 4-Bromofluorobenzene 50.00 96.8 78.2 11748.4
Surr: Dibromofluoromethane 50.00 103.7 66.6 13051.9
Surr: Toluene-d8 50.00 96.3 80.1 12248.1
Page 53 of 54
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053Client: PSC Industrial Outsourcing, LP
Lab Order: 09060783
RECEIVING CHECK LIST
Report Date: 22-Jun-09
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
Received By: EAHCarrier: Zach Pearce
Completed by: Reviewed by:
On:
18-Jun-09
On:
19-Jun-09
Shipping container/cooler in good condition? Yes No Not Present
Chain of custody present? Yes No
Chain of custody signed when relinquished and received? Yes No
Chain of custody agrees with sample labels? Yes No
Samples in proper container/bottle? Yes No
Sample containers intact? Yes No
Sufficient sample volume for indicated test? Yes No
All samples received within holding time? Yes No
Container/Temp Blank temperature in compliance? Yes No
Temp °C 4.2
When thermal preservation is required, samples are compliant with a temperature between 0.1°C - 6.0°C, or when samples are received on ice the same day as collected.
Any No responses must be detailed below or on the COC.
Water - VOA vials have zero headspace? Yes No No VOA vials submitted
Water - pH acceptable upon receipt? Yes No
Type of thermal preservation? None Ice Blue Ice Dry Ice
Chain of custody 1 Extra pages included 0
Reported field parameters measured: Field Lab NA
Pages to follow:
Elizabeth A. Hurley Heather A. White
IL ELAP and NELAP Accredited - Accreditation #100226 Page 54 of 54
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
August 18, 2009
NELAP Accredited #100226
Samples are analyzed on an as received basis unless otherwise requested and documented. The sample results contained in this report relate only to the requested analytes of interest as directed on the chain of custody. IL ELAP and NELAP accredited fields of testing are indicated by the letters NELAP under the Certification column.
All quality control criteria applicable to the test methods employed for this project have been satisfactorily met and are in accordance with NELAP except where noted. The following report shall not be reproduced, except in full, without the written approval of Teklab, Inc.
If you have any questions regarding these tests results, please feel free to call.
Sincerely,
WorkOrder: 09080556A831-735002-012901-225/Ameren Champaign 62403053
RE:
Dear Pete Sazama:
TEKLAB, INC received 2 samples on 8/14/2009 4:45:00 PM for the analysis presented in the following report.
210 West Sand Bank RoadColumbia, IL 62236-0230
(618) 281-7173(618) 281-5120
TEL:FAX:
Pete SazamaPSC Industrial Outsourcing, LP
Heather A. WhiteProject Manager
(618)344-1004 ex 20
IL ELAP and NELAP Accredited - Accreditation #100226 Page 1 of 21
Project: A831-735002-012901-225/Ameren Champaign 62403053Client: PSC Industrial Outsourcing, LP
Lab Order: 09080556
SAMPLE SUMMARY
Report Date: 18-Aug-09
Lab Sample ID Client Sample ID Collection Date
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
Fractions
09080556-001 JH-1 8/14/2009 10:45:00 AM6
09080556-002 JH-2 8/14/2009 11:20:00 AM6
IL ELAP and NELAP Accredited - Accreditation #100226 Page 2 of 21
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
A831-735002-012901-225/Ameren Champaign 624030530908055618-Aug-09
Project:LabOrder:
Client:
Report Date:
CASE NARRATIVEPSC Industrial Outsourcing, LP
Cooler Receipt Temp: 2.8 °C
State accreditations:
KS: NELAP #E-10347 | KY: UST #0073 | MO: DNR #00930 | AR: ADEQ #70-028-0
Qualifiers
- Analyte detected below reporting limits
- Analyte detected in the associated Method Blank
- Spike Recovery outside accepted recovery limits
- RPD outside accepted recovery limits- Not Detected at the Reporting Limit - Value above quantitation range
- Value exceeds Maximum Contaminant Level
- Reporting Limit
- Dilution Factor
- Too numerous to count ( > 200 CFU )
- Diluted out of sample
- Holding time exceeded- Surrogate Standard added by lab
- Matrix interference
- IL Dept. of Public Health- IL ELAP and NELAP Accredited Field of Testing
DF
RL
TNTC
Surr
IDPH
B
J
R
S
X
NELAP
E
MI
H
ND
D
- Did not igniteDNI- Unknown hydrocarbon#- QC criteria failed or noncompliant CCVQ
- Client requested RL below PQLC
IL ELAP and NELAP Accredited - Accreditation #100226 Page 3 of 21
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 8/14/2009 10:45:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 18-Aug-09
LABORATORY RESULTS
WorkOrder: 09080556
Lab ID: 09080556-001
Client Sample ID: JH-1
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
ASTM D2974Percent Moisture 8/14/2009 6:00:00 PM0.1 % 118.2 MAB
STANDARD METHODS 18TH ED. 2540 GTotal Solids 8/14/2009 6:00:00 PM0.1 % 181.8 MAB
SW-846 3050B, 6010B, METALS BY ICPArsenic 8/17/2009 2:02:35 PM2.50 mg/Kg-dry 12.85 LALNELAP
Barium 8/17/2009 2:02:35 PM0.50 mg/Kg-dry 1116 LALNELAP
Cadmium 8/17/2009 2:02:35 PM0.20 mg/Kg-dry 1< 0.20 LALNELAP
Chromium 8/17/2009 2:02:35 PM1.00 mg/Kg-dry 123.3 LALNELAP
Lead 8/17/2009 2:02:35 PM4.00 mg/Kg-dry 113.3 LALNELAP
Silver 8/17/2009 2:02:35 PM0.55 mg/Kg-dry 1< 0.55 LALNELAP
SW-846 3050B, METALS BY GFAASelenium 7740 8/17/2009 2:26:04 PM0.556 mg/Kg-dry 1< 0.556 JMWNELAP
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Acenaphthylene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Anthracene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Benzo(a)anthracene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Benzo(a)pyrene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Benzo(b)fluoranthene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Benzo(g,h,i)perylene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Benzo(k)fluoranthene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Bis(2-ethylhexyl)phthalate 8/17/2009 9:07:00 PM0.080 mg/Kg-dry 1ND MAMNELAP
Chrysene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Dibenzo(a,h)anthracene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Fluoranthene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Fluorene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Indeno(1,2,3-cd)pyrene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Naphthalene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Phenanthrene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Pyrene 8/17/2009 9:07:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Surr: 2-Fluorobiphenyl 8/17/2009 9:07:00 PM10-131 %REC 149.9 MAM
Surr: Nitrobenzene-d5 8/17/2009 9:07:00 PM10-132 %REC 153.2 MAM
Surr: p-Terphenyl-d14 8/17/2009 9:07:00 PM30.6-131 %REC 176.4 MAM
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSBenzene 8/17/2009 1:50:00 PM1.0 µg/Kg-dry 1ND JSANELAP
Ethylbenzene 8/17/2009 1:50:00 PM4.8 µg/Kg-dry 1ND JSANELAP
Toluene J 8/17/2009 1:50:00 PM4.8 µg/Kg-dry 11.1 JSANELAP
Xylenes, Total J 8/17/2009 1:50:00 PM4.8 µg/Kg-dry 12.0 JSANELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 4 of 21
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 8/14/2009 10:45:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 18-Aug-09
LABORATORY RESULTS
WorkOrder: 09080556
Lab ID: 09080556-001
Client Sample ID: JH-1
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
Sample Narrative
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: 1,2-Dichloroethane-d4 8/17/2009 1:50:00 PM61-128 %REC 196.7 JSA
Surr: 4-Bromofluorobenzene 8/17/2009 1:50:00 PM78.2-117 %REC 191.1 JSA
Surr: Dibromofluoromethane 8/17/2009 1:50:00 PM66.6-130 %REC 198.4 JSA
Surr: Toluene-d8 8/17/2009 1:50:00 PM80.1-122 %REC 1100.6 JSA
SW-846 7471AMercury 8/14/20090.012 mg/Kg-dry 10.037 ALUNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 5 of 21
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 8/14/2009 11:20:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 18-Aug-09
LABORATORY RESULTS
WorkOrder: 09080556
Lab ID: 09080556-002
Client Sample ID: JH-2
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
ASTM D2974Percent Moisture 8/14/2009 6:00:00 PM0.1 % 116.0 MAB
STANDARD METHODS 18TH ED. 2540 GTotal Solids 8/14/2009 6:00:00 PM0.1 % 184.0 MAB
SW-846 3050B, 6010B, METALS BY ICPArsenic 8/17/2009 2:09:23 PM2.36 mg/Kg-dry 12.95 LALNELAP
Barium 8/17/2009 2:09:23 PM0.47 mg/Kg-dry 1161 LALNELAP
Cadmium 8/17/2009 2:09:23 PM0.19 mg/Kg-dry 10.32 LALNELAP
Chromium 8/17/2009 2:09:23 PM0.94 mg/Kg-dry 120.9 LALNELAP
Lead 8/17/2009 2:09:23 PM3.77 mg/Kg-dry 111.3 LALNELAP
Silver 8/17/2009 2:09:23 PM0.52 mg/Kg-dry 1< 0.52 LALNELAP
SW-846 3050B, METALS BY GFAASelenium 7740 8/17/2009 2:29:28 PM0.588 mg/Kg-dry 1< 0.588 JMWNELAP
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Acenaphthylene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Anthracene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Benzo(a)anthracene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Benzo(a)pyrene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Benzo(b)fluoranthene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Benzo(g,h,i)perylene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Benzo(k)fluoranthene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Bis(2-ethylhexyl)phthalate 8/17/2009 10:52:00 PM0.081 mg/Kg-dry 1ND MAMNELAP
Chrysene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Dibenzo(a,h)anthracene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Fluoranthene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Fluorene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Indeno(1,2,3-cd)pyrene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Naphthalene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Phenanthrene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Pyrene 8/17/2009 10:52:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Surr: 2-Fluorobiphenyl 8/17/2009 10:52:00 PM10-131 %REC 157.8 MAM
Surr: Nitrobenzene-d5 8/17/2009 10:52:00 PM10-132 %REC 157.0 MAM
Surr: p-Terphenyl-d14 8/17/2009 10:52:00 PM30.6-131 %REC 176.7 MAM
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSBenzene 8/17/2009 2:17:00 PM0.9 µg/Kg-dry 12.5 JSANELAP
Ethylbenzene J 8/17/2009 2:17:00 PM4.7 µg/Kg-dry 11.8 JSANELAP
Toluene 8/17/2009 2:17:00 PM4.7 µg/Kg-dry 15.4 JSANELAP
Xylenes, Total J 8/17/2009 2:17:00 PM4.7 µg/Kg-dry 14.0 JSANELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 6 of 21
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 8/14/2009 11:20:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 18-Aug-09
LABORATORY RESULTS
WorkOrder: 09080556
Lab ID: 09080556-002
Client Sample ID: JH-2
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
Sample Narrative
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: 1,2-Dichloroethane-d4 8/17/2009 2:17:00 PM61-128 %REC 1102.3 JSA
Surr: 4-Bromofluorobenzene 8/17/2009 2:17:00 PM78.2-117 %REC 190.5 JSA
Surr: Dibromofluoromethane 8/17/2009 2:17:00 PM66.6-130 %REC 1103.4 JSA
Surr: Toluene-d8 8/17/2009 2:17:00 PM80.1-122 %REC 1101.2 JSA
SW-846 7471AMercury 8/14/20090.011 mg/Kg-dry 10.028 ALUNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 7 of 21
Sample ID Client Sample ID Collection Date MatrixAnalysis
Date/Time
DATES REPORT
Lab Order: 09080556
Client: PSC Industrial Outsourcing, LPProject: A831-735002-012901-225/Ameren Champaign 62403053
Test NamePrep
Date/Time
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
18-Aug-09Report Date:
09080556-001A JH-1 8/14/2009 Solid SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS
8/17/2009 9:07:00 PM
8/17/2009 8:49:43 AM
09080556-001B SW-846 3050B, 6010B, Metals by ICP 8/17/2009 2:02:35 PM
8/17/2009 8:39:34 AM
SW-846 3050B, Metals by GFAA 8/17/2009 2:26:04 PM
8/17/2009 8:37:02 AM
SW-846 7471A 8/14/20098/14/2009 5:30:00 PM
09080556-001C ASTM D2974 8/14/2009 6:00:00 PM
Standard Methods 18th Ed. 2540 G 8/14/2009 6:00:00 PM
09080556-001F SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS
8/17/2009 1:50:00 PM
09080556-002A JH-2 SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS
8/17/2009 10:52:00 PM
8/17/2009 8:49:43 AM
09080556-002B SW-846 3050B, 6010B, Metals by ICP 8/17/2009 2:09:23 PM
8/17/2009 8:39:35 AM
SW-846 3050B, Metals by GFAA 8/17/2009 2:29:28 PM
8/17/2009 8:37:02 AM
SW-846 7471A 8/14/20098/14/2009 5:30:00 PM
09080556-002C ASTM D2974 8/14/2009 6:00:00 PM
Standard Methods 18th Ed. 2540 G 8/14/2009 6:00:00 PM
09080556-002F SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS
8/17/2009 2:17:00 PM
Page 8 of 21IL ELAP and NELAP Accredited - Accreditation #100226
TEKLAB, INC 5445 HORSESHOE LAKE ROADCOLLINSVILLE, ILLINOIS 62234
ANALYTICAL QC SUMMARY REPORT
Qualifiers
- Analyte detected below reporting limits
- Analyte detected in the associated Method Blank
- Spike Recovery outside accepted recovery limits
- RPD outside accepted recovery limits- Not Detected at the Reporting Limit - Value above quantitation range
- Value exceeds Maximum Contaminant Level
- Reporting Limit
- Dilution Factor
- Too numerous to count ( > 200 CFU )
- Diluted out of sample
- Holding time exceeded- Surrogate Standard added by lab
- Matrix interference
- IL Dept. of Public Health
- IL ELAP and NELAP Accredited
DF
RL
TNTC
Surr
IDPH
B
J
R
S
X NELAP
E
MI
H
ND
D - Did not igniteDNI
- Unknown hydrocarbon#
- QC criteria failedQ
- Client requested RL below PQLC
CCV
DF
DUP
ICV
LCS
MS
MSD
MDL
MB/LCB
PQL
RL
RPD
Continuing calibration verification is a check of a standard to determine the state of calibration of an instrument between recalibration.
Dilution factor is the dilution performed during analysis only and does not take into account any dilutions made during sample preparation. The reported result is final and includes all dilutions factors.Laboratory duplicate is an aliquot of a sample taken from the same container under laboratory conditions for independent processing and analysis independently of the original aliquot. (NELAC)Initial calibration verification is a check of a standard to determine the state of calibration of an instrument before sample analysis is initiated.
Laboratory control sample, spiked with verified known amounts of analytes, is analyzed exactly like a sample to establish intra-laboratory or analyst specific precision and bias or to assess the performance of all or a portion of the measurement system. (NELAC) The acceptable recovery range is listed in this report.
Matrix spike is an aliquot of matrix fortified (spiked) with known quantities of specific analytes that is subjected to the entire analytical procedures in order to determine the effect of the matrix on an approved test method’s recovery system. The acceptable recovery range is listed in this report.Matrix spike duplicate means a replicate matrix spike that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in this report.Method detection limit or limit of detection (LOD) means the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type containing the analyte.Method blank or lab control blank is a sample of a matrix similar to the batch of associated sample (when available) that is free from the analytes of interest and is processed simultaneously with and under the same conditions as samples through all steps of the analytical procedures, and in which no target analytes or interferences are present at concentrations that impact the analytical results for sample analyses. (NELAC)Practical quantitation limit or limit of quantitation (LOQ) means the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine laboratory operation conditions. The acceptable recovery range is listed in this report.The reporting limit the lowest level that the data is displayed in the final report. The reporting limit may vary according to customer request or sample dilution. The reporting limit may not be less than the MDL.Relative percent difference is a calculated difference between two recoveries (ie. MS/MSD). The acceptable recovery limit is listed in this report.
SPK The spike is a known mass of target analyte added to a blank sample or sub-sample; used to determine recovery deficiency or for other quality control purposes. (NELAC)
Surr Surrogates are an organic compound which is similar to the analytes of interest in chemical composition and behavior in the analytical process, but which is not normally found in environmental samples.
Key QC concepts:
LCSD Laboratory control sample duplicate is a replicate laboratory control sample that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in this report.
Page 9 of 21
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09080556
ANALYTICAL QC SUMMARY REPORTTest Number: M2540 G
18-Aug-09Report Date:
Sample ID: LCS-R125818
Batch ID: R125818 Analysis Date: 8/14/2009
Prep Date:
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: %
PQL
Client ID: ZZZZZZ
RunNo: 125818
SeqNo: 2361452
LCSSampType:
Total Solids 1.000 100 90 1100.1 01.0
Sample ID: LCSQC
Batch ID: R125818 Analysis Date: 8/14/2009
Prep Date:
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: %
PQL
Client ID: ZZZZZZ
RunNo: 125818
SeqNo: 2361453
LCSQCSampType:
Total Solids 1.000 100 90 1100.1 01.0
Sample ID: 09080556-001CDUP
Batch ID: R125818 Analysis Date: 8/14/2009
Prep Date:
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: %
PQL
Client ID: JH-1DUP
RunNo: 125818
SeqNo: 2361492
DUPSampType:
Total Solids 150.1 81.75 0.30681.5
Page 10 of 21
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09080556
ANALYTICAL QC SUMMARY REPORTTest Number: SW6010B
18-Aug-09Report Date:
Sample ID: MB-54890
Batch ID: 54890 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 125822
SeqNo: 2362135
MBLKSampType:
SOP 3032
Arsenic 2.500 0 -100 1002.50 0< 2.50
Barium 0.5000 0 -100 1000.50 0< 0.50
Cadmium 0.2000 0 -100 1000.20 0< 0.20
Chromium 1.000 0 -100 1001.00 0< 1.00
Lead 4.000 0 -100 1004.00 0< 4.00
Silver 1.000 0 -100 1000.55 0< 0.55
Sample ID: LCS-54890
Batch ID: 54890 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 125822
SeqNo: 2362136
LCSSampType:
SOP 3032
Arsenic 200.0 102.4 85 1152.50 0205
Barium 200.0 104.2 85 1150.50 0208
Cadmium 5.000 102.4 85 1150.20 05.12
Chromium 20.00 104.4 85 1151.00 020.9
Lead 50.00 103.0 85 1154.00 051.5
Silver 5.000 89.8 85 1150.55 04.49
Sample ID: 09080556-002BMS
Batch ID: 54890 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: JH-2MS
RunNo: 125822
SeqNo: 2362140
MSSampType:
SOP 3032
Arsenic 188.7 99.7 75 1252.36 2.953191
Barium 188.7 98.2 75 1250.47 161.4347
Cadmium 4.717 97.6 75 1250.19 0.32084.92
Chromium 18.87 111.1 75 1250.94 20.9241.9
Lead 47.17 95.8 75 1253.77 11.3356.5
Silver 4.717 90.6 75 1250.52 04.27
Page 11 of 21
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09080556
ANALYTICAL QC SUMMARY REPORTTest Number: SW6010B
18-Aug-09Report Date:
Sample ID: 09080556-002BMSD
Batch ID: 54890 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: JH-2MSD
RunNo: 125822
SeqNo: 2362141
MSDSampType:
SOP 3032
Arsenic 188.7 95.4 75 125 202.36 2.953 191.1 4.34183
Barium 188.7 99.1 75 125 200.47 161.4 346.7 0.489348
Cadmium 4.717 94.4 75 125 200.19 0.3208 4.925 3.114.77
Chromium 18.87 102.7 75 125 200.94 20.92 41.88 3.8640.3
Lead 47.17 92.2 75 125 203.77 11.33 56.54 3.0754.8
Silver 4.717 84.8 75 125 200.52 0 4.274 6.614.00
Page 12 of 21
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09080556
ANALYTICAL QC SUMMARY REPORTTest Number: SW7000 G
18-Aug-09Report Date:
Sample ID: MB-54889
Batch ID: 54889 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 125859
SeqNo: 2362160
MBLKSampType:
SOP 3042
Selenium 7740 0.6000 0 -100 1000.600 0< 0.600
Sample ID: LCS-54889
Batch ID: 54889 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 125859
SeqNo: 2362161
LCSSampType:
SOP 3042
Selenium 7740 3.000 99.9 80 1200.600 03.00
Sample ID: 09080556-002BMS
Batch ID: 54889 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: JH-2MS
RunNo: 125859
SeqNo: 2362167
MSSampType:
SOP 3042
Selenium 7740 2.941 86.7 70 1301.18 02.55
Sample ID: 09080556-002BMSD
Batch ID: 54889 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: JH-2MSD
RunNo: 125859
SeqNo: 2362168
MSDSampType:
SOP 3042
Selenium 7740 2.941 86.1 70 130 201.18 0 2.551 0.7422.53
Page 13 of 21
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09080556
ANALYTICAL QC SUMMARY REPORTTest Number: SW7471 A
18-Aug-09Report Date:
Sample ID: MB-54887
Batch ID: 54887 Analysis Date: 8/14/2009
Prep Date: 8/14/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 125846
SeqNo: 2361957
MBLKSampType:
SOP 3063
Mercury 0.01000 0 -100 1000.010 0< 0.010
Sample ID: LCS-54887
Batch ID: 54887 Analysis Date: 8/14/2009
Prep Date: 8/14/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 125846
SeqNo: 2361958
LCSSampType:
SOP 3063
Mercury 0.2500 94.8 85 1150.010 00.237
Sample ID: 09080556-002BMS
Batch ID: 54887 Analysis Date: 8/14/2009
Prep Date: 8/14/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: JH-2MS
RunNo: 125846
SeqNo: 2361961
MSSampType:
SOP 3063
Mercury 0.2800 100 75 1250.011 0.028000.308
Sample ID: 09080556-002BMSD
Batch ID: 54887 Analysis Date: 8/14/2009
Prep Date: 8/14/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: JH-2MSD
RunNo: 125846
SeqNo: 2361962
MSDSampType:
SOP 3063
Mercury 0.2800 106.4 75 125 150.011 0.02800 0.3080 5.650.326
Page 14 of 21
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09080556
ANALYTICAL QC SUMMARY REPORTTest Number: SW8260B
18-Aug-09Report Date:
Sample ID: LCS-G090817-1
Batch ID: 54900 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 125856
SeqNo: 2362109
LCSSampType:
SW5035
Benzene 50.00 79.8 77.9 1231.0 039.9
Toluene 50.00 83.4 80.2 1155.0 041.7
Ethylbenzene 50.00 86.7 80.9 1195.0 043.4
Xylenes, Total 100.0 81.5 77.6 1245.0 081.5
Surr: 1,2-Dichloroethane-d4 50.00 91.4 61 12845.7
Surr: 4-Bromofluorobenzene 50.00 97.4 78.2 11748.7
Surr: Dibromofluoromethane 50.00 97.6 66.6 13048.8
Surr: Toluene-d8 50.00 98.1 80.1 12249.0
Sample ID: LCSD-G090817-1
Batch ID: 54900 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 125856
SeqNo: 2362110
LCSDSampType:
SW5035
Benzene 50.00 84.4 77.9 123 201.0 0 39.90 5.6342.2
Toluene 50.00 86.8 80.2 115 205.0 0 41.69 4.0043.4
Ethylbenzene 50.00 89.0 80.9 119 205.0 0 43.35 2.6444.5
Xylenes, Total 100.0 84.7 77.6 124 205.0 0 81.51 3.8084.7
Surr: 1,2-Dichloroethane-d4 50.00 90.2 61 128 0045.1
Surr: 4-Bromofluorobenzene 50.00 98.0 78.2 117 0049.0
Surr: Dibromofluoromethane 50.00 96.1 66.6 130 0048.1
Surr: Toluene-d8 50.00 97.7 80.1 122 0048.9
Sample ID: MBLK-G090817-1
Batch ID: 54900 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 125856
SeqNo: 2362112
MBLKSampType:
SW5035
Benzene 1.0ND
Toluene 5.0ND
Ethylbenzene 5.0ND
Xylenes, Total 5.0ND
Page 15 of 21
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09080556
ANALYTICAL QC SUMMARY REPORTTest Number: SW8260B
18-Aug-09Report Date:
Sample ID: MBLK-G090817-1
Batch ID: 54900 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 125856
SeqNo: 2362112
MBLKSampType:
SW5035
Surr: 1,2-Dichloroethane-d4 50.00 95.2 61 12847.6
Surr: 4-Bromofluorobenzene 50.00 100.3 78.2 11750.2
Surr: Dibromofluoromethane 50.00 98.6 66.6 13049.3
Surr: Toluene-d8 50.00 94.4 80.1 12247.2
Page 16 of 21
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09080556
ANALYTICAL QC SUMMARY REPORTTest Number: SW8270C
18-Aug-09Report Date:
Sample ID: MB-54886
Batch ID: 54886 Analysis Date: 8/17/2009
Prep Date: 8/14/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 125866
SeqNo: 2362345
MBLKSampType:
SW3550B
Acenaphthene 0.003ND
Acenaphthylene 0.003ND
Anthracene 0.003ND
Benzo(a)anthracene 0.003ND
Benzo(a)pyrene 0.003ND
Benzo(b)fluoranthene 0.003ND
Benzo(g,h,i)perylene 0.003ND
Benzo(k)fluoranthene 0.003ND
Bis(2-ethylhexyl)phthalate 0.067ND
Chrysene 0.003ND
Dibenzo(a,h)anthracene 0.003ND
Fluoranthene 0.003ND
Fluorene 0.003ND
Indeno(1,2,3-cd)pyrene 0.003ND
Naphthalene 0.003ND
Phenanthrene 0.003ND
Pyrene 0.003ND
Surr: 2-Fluorobiphenyl 0.8330 82.8 17.5 1230.690
Surr: Nitrobenzene-d5 0.8330 80.3 35 1050.669
Surr: p-Terphenyl-d14 0.8330 78.4 53.6 1220.653
Sample ID: LCS-54886
Batch ID: 54886 Analysis Date: 8/17/2009
Prep Date: 8/14/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 125866
SeqNo: 2362346
LCSSampType:
SW3550B
Acenaphthene 0.1670 63.3 56.3 1150.003 00.106
Acenaphthylene 0.1670 69.0 60.3 1430.003 00.115
Anthracene 0.1670 62.4 52.1 1090.003 00.104
Benzo(a)anthracene 0.1670 63.4 52.8 1120.003 00.106
Benzo(a)pyrene 0.1670 67.9 40.8 1270.003 00.113
Page 17 of 21
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09080556
ANALYTICAL QC SUMMARY REPORTTest Number: SW8270C
18-Aug-09Report Date:
Sample ID: LCS-54886
Batch ID: 54886 Analysis Date: 8/17/2009
Prep Date: 8/14/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 125866
SeqNo: 2362346
LCSSampType:
SW3550B
Benzo(b)fluoranthene 0.1670 74.2 50.1 1500.003 00.124
Benzo(g,h,i)perylene 0.1670 74.6 52.8 1450.003 00.124
Benzo(k)fluoranthene 0.1670 75.4 52 1530.003 00.126
Bis(2-ethylhexyl)phthalate 0.1670 96.0 50 1500.067 00.160
Chrysene 0.1670 70.7 60.8 1280.003 00.118
Dibenzo(a,h)anthracene 0.1670 71.3 54.9 1500.003 00.119
Fluoranthene 0.1670 70.5 58.7 1250.003 00.118
Fluorene 0.1670 67.9 57.8 1250.003 00.113
Indeno(1,2,3-cd)pyrene 0.1670 73.6 52 1470.003 00.123
Naphthalene 0.1670 65.6 54.8 1130.003 00.110
Phenanthrene 0.1670 67.0 60.4 1210.003 00.112
Pyrene 0.1670 71.5 57.9 1290.003 00.119
Surr: 2-Fluorobiphenyl 0.8330 68.9 35.3 1130.574
Surr: Nitrobenzene-d5 0.8330 65.7 33.9 1080.547
Surr: p-Terphenyl-d14 0.8330 77.8 58.4 1220.648
Sample ID: 09080556-001AMS
Batch ID: 54886 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: JH-1MS
RunNo: 125866
SeqNo: 2362348
MSSampType:
SW3550B
Acenaphthene 0.2048 68.4 36 1350.004 00.140
Acenaphthylene 0.2048 71.7 17.2 1670.004 00.147
Anthracene 0.2048 62.5 39.3 1240.004 00.128
Benzo(a)anthracene 0.2048 63.6 10 1830.004 00.130
Benzo(a)pyrene 0.2048 66.8 10 2040.004 00.137
Benzo(b)fluoranthene 0.2048 79.1 10.6 1780.004 00.162
Benzo(g,h,i)perylene 0.2048 73.8 10 1680.004 00.151
Benzo(k)fluoranthene 0.2048 81.5 27.6 1810.004 00.167
Bis(2-ethylhexyl)phthalate 0.2048 104.6 50 1500.082 00.214
Chrysene 0.2048 79.6 10 1760.004 00.163
Page 18 of 21
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09080556
ANALYTICAL QC SUMMARY REPORTTest Number: SW8270C
18-Aug-09Report Date:
Sample ID: 09080556-001AMS
Batch ID: 54886 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: JH-1MS
RunNo: 125866
SeqNo: 2362348
MSSampType:
SW3550B
Dibenzo(a,h)anthracene 0.2048 73.7 12.2 1560.004 00.151
Fluoranthene 0.2048 67.7 10 2270.004 00.139
Fluorene 0.2048 69.8 35.2 1480.004 00.143
Indeno(1,2,3-cd)pyrene 0.2048 77.1 10 1640.004 00.158
Naphthalene 0.2048 42.7 14.7 1280.004 00.088
Phenanthrene 0.2048 67.4 32.8 1430.004 00.138
Pyrene 0.2048 70.0 10 1800.004 00.143
Surr: 2-Fluorobiphenyl 1.022 61.5 10 1310.628
Surr: Nitrobenzene-d5 1.022 60.5 10 1320.618
Surr: p-Terphenyl-d14 1.022 80.8 30.6 1310.826
Sample ID: 09080556-001AMSD
Batch ID: 54886 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: JH-1MSD
RunNo: 125866
SeqNo: 2362349
MSDSampType:
SW3550B
Acenaphthene 0.1984 71.3 36 135 49.70.004 0 0.1402 0.9230.141
Acenaphthylene 0.1984 76.8 17.2 167 33.30.004 0 0.1468 3.750.152
Anthracene 0.1984 67.7 39.3 124 51.10.004 0 0.1280 4.910.134
Benzo(a)anthracene 0.1984 68.2 10 183 40.60.004 0 0.1303 3.750.135
Benzo(a)pyrene 0.1984 74.2 10 204 56.40.004 0 0.1368 7.320.147
Benzo(b)fluoranthene 0.1984 82.2 10.6 178 49.70.004 0 0.1620 0.6230.163
Benzo(g,h,i)perylene 0.1984 80.2 10 168 36.50.004 0 0.1512 5.080.159
Benzo(k)fluoranthene 0.1984 85.3 27.6 181 42.60.004 0 0.1668 1.450.169
Bis(2-ethylhexyl)phthalate 0.1984 106.9 50 150 60.30.080 0 0.2142 1.000.212
Chrysene 0.1984 87.3 10 176 45.10.004 0 0.1631 5.980.173
Dibenzo(a,h)anthracene 0.1984 78.3 12.2 156 39.90.004 0 0.1509 2.910.155
Fluoranthene 0.1984 76.6 10 227 66.20.004 0 0.1388 9.050.152
Fluorene 0.1984 71.1 35.2 148 65.60.004 0 0.1430 1.380.141
Indeno(1,2,3-cd)pyrene 0.1984 79.7 10 164 36.50.004 0 0.1580 0.1180.158
Naphthalene 0.1984 61.0 14.7 128 39.60.004 0 0.08753 32.10.121
Page 19 of 21
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053
Client: PSC Industrial Outsourcing, LP
Lab Order: 09080556
ANALYTICAL QC SUMMARY REPORTTest Number: SW8270C
18-Aug-09Report Date:
Sample ID: 09080556-001AMSD
Batch ID: 54886 Analysis Date: 8/17/2009
Prep Date: 8/17/2009
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: JH-1MSD
RunNo: 125866
SeqNo: 2362349
MSDSampType:
SW3550B
Phenanthrene 0.1984 74.8 32.8 143 35.40.004 0 0.1380 7.210.148
Pyrene 0.1984 74.1 10 180 60.10.004 0 0.1433 2.570.147
Surr: 2-Fluorobiphenyl 0.9896 62.9 10 131 4000.622
Surr: Nitrobenzene-d5 0.9896 61.9 10 132 4000.613
Surr: p-Terphenyl-d14 0.9896 79.2 30.6 131 4000.784
Page 20 of 21
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 62403053Client: PSC Industrial Outsourcing, LP
Lab Order: 09080556
RECEIVING CHECK LIST
Report Date: 18-Aug-09
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
Received By: EAHCarrier: J. Crompton
Completed by: Reviewed by:
On:
14-Aug-09
On:
17-Aug-09
Shipping container/cooler in good condition? Yes No Not Present
Chain of custody present? Yes No
Chain of custody signed when relinquished and received? Yes No
Chain of custody agrees with sample labels? Yes No
Samples in proper container/bottle? Yes No
Sample containers intact? Yes No
Sufficient sample volume for indicated test? Yes No
All samples received within holding time? Yes No
Container/Temp Blank temperature in compliance? Yes No
Temp °C 2.8
When thermal preservation is required, samples are compliant with a temperature between 0.1°C - 6.0°C, or when samples are received on ice the same day as collected.
Any No responses must be detailed below or on the COC.
Water - VOA vials have zero headspace? Yes No No VOA vials submitted
Water - pH acceptable upon receipt? Yes No
Type of thermal preservation? None Ice Blue Ice Dry Ice
Chain of custody 1 Extra pages included 0
Reported field parameters measured: Field Lab NA
Pages to follow:
Marvin L. Darling Heather A. White
IL ELAP and NELAP Accredited - Accreditation #100226 Page 21 of 21
P2-Borrow 2
Date Collected 10/20/2009 2:45:00 PM
Sample P2-Borrow 2
Analyte Unit
Cyanide, Amenable to Chlorination mg/Kg-dry < Interference
Cyanide mg/Kg-dry < 0.61
Total Solids % 84.1
Mercury mg/Kg-dry 0.024
Selenium mg/Kg-dry < 0.6
Arsenic mg/Kg-dry 5.87
Barium mg/Kg-dry 114
Cadmium mg/Kg-dry 0.28
Chromium mg/Kg-dry 24.3
Lead mg/Kg-dry 16.5
Silver mg/Kg-dry < 0.55
Percent Moisture % 15.9
1,2,4-Trichlorobenzene mg/Kg-dry < 0.582
1,2-Dichlorobenzene mg/Kg-dry < 0.582
1,2-Diphenylhydrazine mg/Kg-dry < 0.978
1,3-Dichlorobenzene mg/Kg-dry < 0.582
1,4-Dichlorobenzene mg/Kg-dry < 0.582
2,4,5-Trichlorophenol mg/Kg-dry < 0.407
2,4,6-Trichlorophenol mg/Kg-dry < 0.407
2,4-Dichlorophenol mg/Kg-dry < 0.582
2,4-Dimethylphenol mg/Kg-dry < 0.582
2,4-Dinitrophenol mg/Kg-dry < 1.16
2,4-Dinitrotoluene mg/Kg-dry < 0.407 S
2,6-Dinitrotoluene mg/Kg-dry < 0.407
2-Chloronaphthalene mg/Kg-dry < 0.407
2-Chlorophenol mg/Kg-dry < 0.582
2-Methoxy-4-methylphenol mg/Kg-dry < 0.757
2-Methylnaphthalene mg/Kg-dry < 0.407
2-Nitroaniline mg/Kg-dry < 1.16
2-Nitrophenol mg/Kg-dry < 0.407
3,3´-Dichlorobenzidine mg/Kg-dry < 0.407
3-Nitroaniline mg/Kg-dry < 1.16
4,6-Dinitro-2-methylphenol mg/Kg-dry < 1.16
4-Bromophenyl phenyl ether mg/Kg-dry < 0.407
4-Chloro-3-methylphenol mg/Kg-dry < 0.582
4-Chloroaniline mg/Kg-dry < 0.582
4-Chlorophenyl phenyl ether mg/Kg-dry < 0.407
4-Nitroaniline mg/Kg-dry < 0.582
4-Nitrophenol mg/Kg-dry < 0.407
Aniline mg/Kg-dry < 0.582
Azobenzene mg/Kg-dry < 0.407
Benzidine mg/Kg-dry < 1.23
Benzoic acid mg/Kg-dry < 1.75
Benzyl alcohol mg/Kg-dry < 0.582
Bis(2-chloroethoxy)methane mg/Kg-dry < 0.407
Bis(2-chloroethyl)ether mg/Kg-dry < 0.582
Bis(2-chloroisopropyl)ether mg/Kg-dry < 0.407
Butyl benzyl phthalate mg/Kg-dry < 0.407
Result
Page 5
P2-Borrow 2
Carbazole mg/Kg-dry < 0.582
Dibenzofuran mg/Kg-dry < 0.407
Diethyl phthalate mg/Kg-dry < 0.582
Dimethyl phthalate mg/Kg-dry < 0.407
Di-n-butyl phthalate mg/Kg-dry < 0.407
Di-n-octyl phthalate mg/Kg-dry < 0.407
Hexachlorobenzene mg/Kg-dry < 0.407
Hexachlorobutadiene mg/Kg-dry < 0.582
Hexachlorocyclopentadiene mg/Kg-dry < 0.407
Hexachloroethane mg/Kg-dry < 0.582
Isophorone mg/Kg-dry < 0.407
m,p-Cresol mg/Kg-dry < 0.582
Nitrobenzene mg/Kg-dry < 0.582
N-Nitrosodimethylamine mg/Kg-dry < 0.582
N-Nitroso-di-n-propylamine mg/Kg-dry < 0.582
N-Nitrosodiphenylamine mg/Kg-dry < 0.582
o-Cresol mg/Kg-dry < 0.582
Pentachlorophenol mg/Kg-dry < 2.33
Phenol mg/Kg-dry < 0.407
Pyridine mg/Kg-dry < 0.582
Acenaphthene mg/Kg-dry < 0.004
Acenaphthylene mg/Kg-dry < 0.004
Anthracene mg/Kg-dry < 0.004
Benzo(a)anthracene mg/Kg-dry 0.019
Benzo(a)pyrene mg/Kg-dry 0.033
Benzo(b)fluoranthene mg/Kg-dry 0.037
Benzo(g,h,i)perylene mg/Kg-dry 0.036
Benzo(k)fluoranthene mg/Kg-dry 0.011
Bis(2-ethylhexyl)phthalate mg/Kg-dry < 0.078
Chrysene mg/Kg-dry 0.024
Dibenzo(a,h)anthracene mg/Kg-dry 0.007
Fluoranthene mg/Kg-dry 0.041
Fluorene mg/Kg-dry < 0.004
Indeno(1,2,3-cd)pyrene mg/Kg-dry 0.018
Naphthalene mg/Kg-dry < 0.004
Phenanthrene mg/Kg-dry 0.013
Pyrene mg/Kg-dry 0.039
1,1,1,2-Tetrachloroethane µg/Kg-dry < 4.9
1,1,1-Trichloroethane µg/Kg-dry < 4.9
1,1,2,2-Tetrachloroethane µg/Kg-dry < 4.9
1,1,2-Trichloro-1,2,2-trifluoroethane µg/Kg-dry < 4.9
1,1,2-Trichloroethane µg/Kg-dry < 4.9
1,1-Dichloro-2-propanone µg/Kg-dry < 48.7
1,1-Dichloroethane µg/Kg-dry < 4.9
1,1-Dichloroethene µg/Kg-dry < 4.9
1,1-Dichloropropene µg/Kg-dry < 4.9
1,2,3-Trichlorobenzene µg/Kg-dry < 4.9
1,2,3-Trichloropropane µg/Kg-dry < 9.7
1,2,3-Trimethylbenzene µg/Kg-dry < 4.9
1,2,4-Trichlorobenzene µg/Kg-dry < 4.9
1,2,4-Trimethylbenzene µg/Kg-dry < 4.9
1,2-Dibromo-3-chloropropane µg/Kg-dry < 4.9
Page 6
P2-Borrow 2
1,2-Dibromoethane µg/Kg-dry < 4.9
1,2-Dichlorobenzene µg/Kg-dry < 4.9
1,2-Dichloroethane µg/Kg-dry < 4.9
1,2-Dichloropropane µg/Kg-dry < 4.9
1,3,5-Trimethylbenzene µg/Kg-dry < 4.9
1,3-Dichlorobenzene µg/Kg-dry < 4.9
1,3-Dichloropropane µg/Kg-dry < 4.9
1,4-Dichlorobenzene µg/Kg-dry < 4.9
1-Chlorobutane µg/Kg-dry < 4.9
2,2-Dichloropropane µg/Kg-dry < 4.9
2-Butanone µg/Kg-dry < 48.7
2-Chlorotoluene µg/Kg-dry < 4.9
2-Hexanone µg/Kg-dry < 48.7
2-Nitropropane µg/Kg-dry < 48.7
4-Chlorotoluene µg/Kg-dry < 4.9
4-Methyl-2-pentanone µg/Kg-dry < 48.7
Acetone µg/Kg-dry < 48.7
Acrolein µg/Kg-dry < 97.3
Acrylonitrile µg/Kg-dry < 9.7
Allyl chloride µg/Kg-dry < 4.9
Benzene µg/Kg-dry < 1
Bromobenzene µg/Kg-dry < 4.9
Bromochloromethane µg/Kg-dry < 4.9
Bromodichloromethane µg/Kg-dry < 4.9
Bromoform µg/Kg-dry < 4.9
Bromomethane µg/Kg-dry < 9.7
Carbon disulfide µg/Kg-dry < 4.9
Carbon tetrachloride µg/Kg-dry < 4.9
Chlorobenzene µg/Kg-dry < 4.9
Chloroethane µg/Kg-dry < 9.7
Chloroform µg/Kg-dry < 4.9
Chloromethane µg/Kg-dry 2.8 J
cis-1,2-Dichloroethene µg/Kg-dry < 4.9
cis-1,3-Dichloropropene µg/Kg-dry < 3.9
Cyclohexanone µg/Kg-dry < 97.3
Dibromochloromethane µg/Kg-dry < 4.9
Dibromomethane µg/Kg-dry < 4.9
Dichlorodifluoromethane µg/Kg-dry < 9.7
Ethyl acetate µg/Kg-dry < 48.7
Ethyl ether µg/Kg-dry < 4.9
Ethyl methacrylate µg/Kg-dry < 4.9
Ethylbenzene µg/Kg-dry < 4.9
Heptane µg/Kg-dry < 19.5
Hexachlorobutadiene µg/Kg-dry < 4.9
Hexachloroethane µg/Kg-dry < 4.9
Iodomethane µg/Kg-dry < 9.7
Isopropylbenzene µg/Kg-dry < 4.9
m,p-Xylenes µg/Kg-dry 1.1 J
Methacrylonitrile µg/Kg-dry < 48.7
Methyl Methacrylate µg/Kg-dry < 4.9
Methyl tert-butyl ether µg/Kg-dry < 1.9
Methylacrylate µg/Kg-dry < 9.7
Page 7
P2-Borrow 2
Methylene chloride µg/Kg-dry 1.4 J
Naphthalene µg/Kg-dry < 9.7
n-Butylbenzene µg/Kg-dry < 4.9
n-Hexane µg/Kg-dry < 19.5
Nitrobenzene µg/Kg-dry < 97.3
n-Propylbenzene µg/Kg-dry < 4.9
o-Xylene µg/Kg-dry < 4.9
Pentachloroethane µg/Kg-dry < 4.9
p-Isopropyltoluene µg/Kg-dry < 4.9
Propionitrile µg/Kg-dry < 48.7
sec-Butylbenzene µg/Kg-dry < 4.9
Styrene µg/Kg-dry < 4.9
tert-Butylbenzene µg/Kg-dry < 4.9
Tetrachloroethene µg/Kg-dry < 4.9
Tetrahydrofuran µg/Kg-dry < 48.7
Toluene µg/Kg-dry < 4.9
trans-1,2-Dichloroethene µg/Kg-dry < 4.9
trans-1,3-Dichloropropene µg/Kg-dry < 3.9
Trichloroethene µg/Kg-dry < 4.9
Trichlorofluoromethane µg/Kg-dry < 4.9
Vinyl acetate µg/Kg-dry < 48.7
Vinyl chloride µg/Kg-dry < 1.9
Page 8
P2-Borrow 1
Date Collected 10/20/2009 2:30:00 PM
Sample P2-Borrow 1
Analyte Unit
Cyanide, Amenable to Chlorination mg/Kg-dry < 0.597
Cyanide mg/Kg-dry < 0.6 R
Total Solids % 83.8
Mercury mg/Kg-dry 0.019
Selenium mg/Kg-dry < 0.545
Arsenic mg/Kg-dry 6.29
Barium mg/Kg-dry 106
Cadmium mg/Kg-dry 0.29
Chromium mg/Kg-dry 26
Lead mg/Kg-dry 16.5
Silver mg/Kg-dry < 0.55
Percent Moisture % 16.2
1,2,4-Trichlorobenzene mg/Kg-dry < 0.59
1,2-Dichlorobenzene mg/Kg-dry < 0.59
1,2-Diphenylhydrazine mg/Kg-dry < 0.992
1,3-Dichlorobenzene mg/Kg-dry < 0.59
1,4-Dichlorobenzene mg/Kg-dry < 0.59
2,4,5-Trichlorophenol mg/Kg-dry < 0.413
2,4,6-Trichlorophenol mg/Kg-dry < 0.413
2,4-Dichlorophenol mg/Kg-dry < 0.59
2,4-Dimethylphenol mg/Kg-dry < 0.59
2,4-Dinitrophenol mg/Kg-dry < 1.18
2,4-Dinitrotoluene mg/Kg-dry < 0.413
2,6-Dinitrotoluene mg/Kg-dry < 0.413
2-Chloronaphthalene mg/Kg-dry < 0.413
2-Chlorophenol mg/Kg-dry < 0.59
2-Methoxy-4-methylphenol mg/Kg-dry < 0.767
2-Methylnaphthalene mg/Kg-dry < 0.413
2-Nitroaniline mg/Kg-dry < 1.18
2-Nitrophenol mg/Kg-dry < 0.413
3,3´-Dichlorobenzidine mg/Kg-dry < 0.413
3-Nitroaniline mg/Kg-dry < 1.18
4,6-Dinitro-2-methylphenol mg/Kg-dry < 1.18
4-Bromophenyl phenyl ether mg/Kg-dry < 0.413
4-Chloro-3-methylphenol mg/Kg-dry < 0.59
4-Chloroaniline mg/Kg-dry < 0.59
4-Chlorophenyl phenyl ether mg/Kg-dry < 0.413
4-Nitroaniline mg/Kg-dry < 0.59
4-Nitrophenol mg/Kg-dry < 0.413
Aniline mg/Kg-dry < 0.59
Azobenzene mg/Kg-dry < 0.413
Benzidine mg/Kg-dry < 1.25
Benzoic acid mg/Kg-dry < 1.77
Benzyl alcohol mg/Kg-dry < 0.59
Bis(2-chloroethoxy)methane mg/Kg-dry < 0.413
Bis(2-chloroethyl)ether mg/Kg-dry < 0.59
Bis(2-chloroisopropyl)ether mg/Kg-dry < 0.413
Butyl benzyl phthalate mg/Kg-dry < 0.413
Result
Page 1
P2-Borrow 1
Carbazole mg/Kg-dry < 0.59
Dibenzofuran mg/Kg-dry < 0.413
Diethyl phthalate mg/Kg-dry < 0.59
Dimethyl phthalate mg/Kg-dry < 0.413
Di-n-butyl phthalate mg/Kg-dry < 0.413
Di-n-octyl phthalate mg/Kg-dry < 0.413
Hexachlorobenzene mg/Kg-dry < 0.413
Hexachlorobutadiene mg/Kg-dry < 0.59
Hexachlorocyclopentadiene mg/Kg-dry < 0.413
Hexachloroethane mg/Kg-dry < 0.59
Isophorone mg/Kg-dry < 0.413
m,p-Cresol mg/Kg-dry < 0.59
Nitrobenzene mg/Kg-dry < 0.59
N-Nitrosodimethylamine mg/Kg-dry < 0.59
N-Nitroso-di-n-propylamine mg/Kg-dry < 0.59
N-Nitrosodiphenylamine mg/Kg-dry < 0.59
o-Cresol mg/Kg-dry < 0.59
Pentachlorophenol mg/Kg-dry < 2.36
Phenol mg/Kg-dry < 0.413
Pyridine mg/Kg-dry < 0.59
Acenaphthene mg/Kg-dry < 0.004
Acenaphthylene mg/Kg-dry < 0.004
Anthracene mg/Kg-dry < 0.004
Benzo(a)anthracene mg/Kg-dry 0.006
Benzo(a)pyrene mg/Kg-dry 0.004
Benzo(b)fluoranthene mg/Kg-dry 0.006
Benzo(g,h,i)perylene mg/Kg-dry 0.004
Benzo(k)fluoranthene mg/Kg-dry < 0.004
Bis(2-ethylhexyl)phthalate mg/Kg-dry < 0.079
Chrysene mg/Kg-dry 0.004
Dibenzo(a,h)anthracene mg/Kg-dry < 0.004
Fluoranthene mg/Kg-dry 0.008
Fluorene mg/Kg-dry < 0.004
Indeno(1,2,3-cd)pyrene mg/Kg-dry < 0.004
Naphthalene mg/Kg-dry < 0.004
Phenanthrene mg/Kg-dry < 0.004
Pyrene mg/Kg-dry 0.007
1,1,1,2-Tetrachloroethane µg/Kg-dry < 4.1
1,1,1-Trichloroethane µg/Kg-dry < 4.1
1,1,2,2-Tetrachloroethane µg/Kg-dry < 4.1
1,1,2-Trichloro-1,2,2-trifluoroethane µg/Kg-dry < 4.1
1,1,2-Trichloroethane µg/Kg-dry < 4.1
1,1-Dichloro-2-propanone µg/Kg-dry < 41.4
1,1-Dichloroethane µg/Kg-dry < 4.1
1,1-Dichloroethene µg/Kg-dry < 4.1
1,1-Dichloropropene µg/Kg-dry < 4.1
1,2,3-Trichlorobenzene µg/Kg-dry < 4.1
1,2,3-Trichloropropane µg/Kg-dry < 8.3
1,2,3-Trimethylbenzene µg/Kg-dry < 4.1
1,2,4-Trichlorobenzene µg/Kg-dry < 4.1
1,2,4-Trimethylbenzene µg/Kg-dry < 4.1
1,2-Dibromo-3-chloropropane µg/Kg-dry < 4.1
Page 2
P2-Borrow 1
1,2-Dibromoethane µg/Kg-dry < 4.1
1,2-Dichlorobenzene µg/Kg-dry < 4.1
1,2-Dichloroethane µg/Kg-dry < 4.1
1,2-Dichloropropane µg/Kg-dry < 4.1
1,3,5-Trimethylbenzene µg/Kg-dry < 4.1
1,3-Dichlorobenzene µg/Kg-dry < 4.1
1,3-Dichloropropane µg/Kg-dry < 4.1
1,4-Dichlorobenzene µg/Kg-dry < 4.1
1-Chlorobutane µg/Kg-dry < 4.1
2,2-Dichloropropane µg/Kg-dry < 4.1
2-Butanone µg/Kg-dry < 41.4
2-Chlorotoluene µg/Kg-dry < 4.1
2-Hexanone µg/Kg-dry < 41.4
2-Nitropropane µg/Kg-dry < 41.4
4-Chlorotoluene µg/Kg-dry < 4.1
4-Methyl-2-pentanone µg/Kg-dry < 41.4
Acetone µg/Kg-dry 31 J
Acrolein µg/Kg-dry < 82.8
Acrylonitrile µg/Kg-dry < 8.3
Allyl chloride µg/Kg-dry < 4.1
Benzene µg/Kg-dry < 0.8
Bromobenzene µg/Kg-dry < 4.1
Bromochloromethane µg/Kg-dry < 4.1
Bromodichloromethane µg/Kg-dry < 4.1
Bromoform µg/Kg-dry < 4.1
Bromomethane µg/Kg-dry < 8.3
Carbon disulfide µg/Kg-dry < 4.1
Carbon tetrachloride µg/Kg-dry < 4.1
Chlorobenzene µg/Kg-dry < 4.1
Chloroethane µg/Kg-dry < 8.3
Chloroform µg/Kg-dry < 4.1
Chloromethane µg/Kg-dry < 8.3
cis-1,2-Dichloroethene µg/Kg-dry < 4.1
cis-1,3-Dichloropropene µg/Kg-dry < 3.3
Cyclohexanone µg/Kg-dry < 82.8
Dibromochloromethane µg/Kg-dry < 4.1
Dibromomethane µg/Kg-dry < 4.1
Dichlorodifluoromethane µg/Kg-dry < 8.3
Ethyl acetate µg/Kg-dry < 41.4
Ethyl ether µg/Kg-dry < 4.1
Ethyl methacrylate µg/Kg-dry < 4.1
Ethylbenzene µg/Kg-dry < 4.1
Heptane µg/Kg-dry < 16.6
Hexachlorobutadiene µg/Kg-dry < 4.1
Hexachloroethane µg/Kg-dry < 4.1
Iodomethane µg/Kg-dry < 8.3
Isopropylbenzene µg/Kg-dry < 4.1
m,p-Xylenes µg/Kg-dry 1 J
Methacrylonitrile µg/Kg-dry < 41.4
Methyl Methacrylate µg/Kg-dry < 4.1
Methyl tert-butyl ether µg/Kg-dry < 1.7
Methylacrylate µg/Kg-dry < 8.3
Page 3
P2-Borrow 1
Methylene chloride µg/Kg-dry 1.2 J
Naphthalene µg/Kg-dry < 8.3
n-Butylbenzene µg/Kg-dry < 4.1
n-Hexane µg/Kg-dry 1.9 J
Nitrobenzene µg/Kg-dry < 82.8
n-Propylbenzene µg/Kg-dry < 4.1
o-Xylene µg/Kg-dry < 4.1
Pentachloroethane µg/Kg-dry < 4.1
p-Isopropyltoluene µg/Kg-dry < 4.1
Propionitrile µg/Kg-dry < 41.4
sec-Butylbenzene µg/Kg-dry < 4.1
Styrene µg/Kg-dry < 4.1
tert-Butylbenzene µg/Kg-dry < 4.1
Tetrachloroethene µg/Kg-dry < 4.1
Tetrahydrofuran µg/Kg-dry < 41.4
Toluene µg/Kg-dry < 4.1
trans-1,2-Dichloroethene µg/Kg-dry < 4.1
trans-1,3-Dichloropropene µg/Kg-dry < 3.3
Trichloroethene µg/Kg-dry < 4.1
Trichlorofluoromethane µg/Kg-dry < 4.1
Vinyl acetate µg/Kg-dry < 41.4
Vinyl chloride µg/Kg-dry < 1.7
Page 4
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
April 21, 2010
NELAP Accredited #100226
Samples are analyzed on an as received basis unless otherwise requested and documented. The sample results contained in this report relate only to the requested analytes of interest as directed on the chain of custody. IL ELAP and NELAP accredited fields of testing are indicated by the letters NELAP under the Certification column.
All quality control criteria applicable to the test methods employed for this project have been satisfactorily met and are in accordance with NELAP except where noted. The following report shall not be reproduced, except in full, without the written approval of Teklab, Inc.
If you have any questions regarding these tests results, please feel free to call.
Sincerely,
WorkOrder: 10040597A831-735002-012901-225/Ameren Champaign 6249080120
RE:
Dear Pete Sazama:
TEKLAB, INC received 2 samples on 4/15/2010 3:00:00 PM for the analysis presented in the following report.
210 West Sand Bank RoadColumbia, IL 62236-0230
(618) 281-7173(618) 281-5120
TEL:FAX:
Pete SazamaPSC Industrial Outsourcing, LP
Shelly A. HennessyProject Manager
(618)344-1004 ex 36
IL ELAP and NELAP Accredited - Accreditation #100226 Page 1 of 53
Project: A831-735002-012901-225/Ameren Champaign 6249080120Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
SAMPLE SUMMARY
Report Date: 21-Apr-10
Lab Sample ID Client Sample ID Collection Date
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
Fractions
10040597-001 P4-Borrow #1 4/14/2010 10:00:00 AM5
10040597-002 P4 Borrow #2 4/14/2010 10:15:00 AM5
IL ELAP and NELAP Accredited - Accreditation #100226 Page 2 of 53
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
A831-735002-012901-225/Ameren Champaign 62490801201004059721-Apr-10
Project:LabOrder:
Client:
Report Date:
CASE NARRATIVEPSC Industrial Outsourcing, LP
Cooler Receipt Temp: 1.4 °C
State accreditations:
KS: NELAP #E-10347 | KY: UST #0073 | MO: DNR #00930 | AR: ADEQ #70-028-0
Qualifiers
- Analyte detected below reporting limits
- Analyte detected in the associated Method Blank
- Spike Recovery outside accepted recovery limits
- RPD outside accepted recovery limits- Not Detected at the Reporting Limit - Value above quantitation range
- Value exceeds Maximum Contaminant Level
- Reporting Limit
- Dilution Factor
- Too numerous to count ( > 200 CFU )
- Diluted out of sample
- Holding time exceeded- Surrogate Standard added by lab
- Matrix interference
- IL Dept. of Public Health- IL ELAP and NELAP Accredited Field of Testing
DF
RL
TNTC
Surr
IDPH
B
J
R
S
X
NELAP
E
MI
H
ND
D
- Did not igniteDNI- Unknown hydrocarbon#- QC criteria failed or noncompliant CCVQ
- Client requested RL below PQLC
IL ELAP and NELAP Accredited - Accreditation #100226 Page 3 of 53
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 4/14/2010 10:00:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 21-Apr-10
LABORATORY RESULTS
WorkOrder: 10040597
Lab ID: 10040597-001
Client Sample ID: P4-Borrow #1
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 4/15/2010 4:10:00 PM0.1 % 111.2 JMT
STANDARD METHODS 18TH ED. 2540 GTotal Solids 4/15/2010 4:10:00 PM0.1 % 188.8 JMT
SW-846 3050B, 6010B, METALS BY ICPArsenic 4/16/2010 1:43:07 PM2.40 mg/Kg-dry 16.54 LALNELAP
Barium 4/16/2010 1:43:07 PM0.48 mg/Kg-dry 139.9 LALNELAP
Cadmium J 4/16/2010 2:29:18 PM0.19 mg/Kg-dry 10.13 LALNELAP
Chromium 4/16/2010 1:43:07 PM0.96 mg/Kg-dry 117.8 LALNELAP
Lead 4/16/2010 1:43:07 PM3.85 mg/Kg-dry 116.1 LALNELAP
Silver 4/16/2010 1:43:07 PM0.53 mg/Kg-dry 1< 0.53 LALNELAP
SW-846 3050B, METALS BY GFAASelenium 7740 4/16/2010 1:41:26 PM0.556 mg/Kg-dry 1< 0.556 MEKNELAP
SW-846 3550B, 8081A, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
4,4´-DDE 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
4,4´-DDT 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
Alachlor 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
Aldrin 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
alpha-BHC 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
alpha-Chlordane 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
beta-BHC 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
Chlordane 4/16/2010 10:51:00 AM3.85 µg/Kg-dry 1ND HENELAP
delta-BHC 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
Dieldrin 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 13.89 HENELAP
Endosulfan I 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
Endosulfan II 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
Endosulfan sulfate 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
Endrin 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
Endrin aldehyde 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
Endrin ketone 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
gamma-BHC 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
gamma-Chlordane 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
Heptachlor 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
Heptachlor epoxide 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
Methoxychlor 4/16/2010 10:51:00 AM1.92 µg/Kg-dry 1ND HENELAP
Toxaphene 4/16/2010 10:51:00 AM34.5 µg/Kg-dry 1ND HENELAP
Surr: Decachlorobiphenyl 4/16/2010 10:51:00 AM48-149 %REC 188.9 HE
Surr: Tetrachloro-m-xylene 4/16/2010 10:51:00 AM19-145 %REC 182.5 HE
IL ELAP and NELAP Accredited - Accreditation #100226 Page 4 of 53
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 4/14/2010 10:00:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 21-Apr-10
LABORATORY RESULTS
WorkOrder: 10040597
Lab ID: 10040597-001
Client Sample ID: P4-Borrow #1
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 4/16/2010 10:47:00 AM43.2 µg/Kg-dry 1ND HENELAP
Aroclor 1221 4/16/2010 10:47:00 AM43.2 µg/Kg-dry 1ND HENELAP
Aroclor 1232 4/16/2010 10:47:00 AM43.2 µg/Kg-dry 1ND HENELAP
Aroclor 1242 4/16/2010 10:47:00 AM43.2 µg/Kg-dry 1ND HENELAP
Aroclor 1248 4/16/2010 10:47:00 AM43.2 µg/Kg-dry 1ND HENELAP
Aroclor 1254 4/16/2010 10:47:00 AM43.2 µg/Kg-dry 1ND HENELAP
Aroclor 1260 4/16/2010 10:47:00 AM43.2 µg/Kg-dry 1ND HENELAP
Surr: Decachlorobiphenyl 4/16/2010 10:47:00 AM5-156 %REC 195.8 HE
Surr: Tetrachloro-meta-xylene 4/16/2010 10:47:00 AM7.35-123 %REC 175.3 HE
SW-846 3550B, 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE
2,4,5-TP (Silvex) 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE
2,4-D 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE
2,4-DB 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE
3,5-Dichlorobenzoic Acid 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE
4-Nitrophenol 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE
Bentazon 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE
Chloramben 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE
Dalapon 4/16/2010 4:36:00 PM161 µg/Kg-dry 1ND HE
DCPA 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE
Dicamba 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE
Dichlorprop 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE
MCPA 4/16/2010 4:36:00 PM1610 µg/Kg-dry 1ND HE
MCPP 4/16/2010 4:36:00 PM1610 µg/Kg-dry 1ND HE
Pentachlorophenol 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE
Picloram 4/16/2010 4:36:00 PM16.1 µg/Kg-dry 1ND HE
Surr: 2,4-Dichlorophenylacetic acid 4/16/2010 4:36:00 PM18.1-118 %REC 147.6 HE
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 1ND MAMNELAP
Acenaphthylene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 1ND MAMNELAP
Anthracene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.005 MAMNELAP
Benzo(a)anthracene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.015 MAMNELAP
Benzo(a)pyrene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.013 MAMNELAP
Benzo(b)fluoranthene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.020 MAMNELAP
Benzo(g,h,i)perylene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.010 MAMNELAP
Benzo(k)fluoranthene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.007 MAMNELAP
Bis(2-ethylhexyl)phthalate 4/16/2010 11:39:00 AM0.075 mg/Kg-dry 1ND MAMNELAP
Chrysene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.018 MAMNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 5 of 53
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 4/14/2010 10:00:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 21-Apr-10
LABORATORY RESULTS
WorkOrder: 10040597
Lab ID: 10040597-001
Client Sample ID: P4-Borrow #1
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSDibenzo(a,h)anthracene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 1ND MAMNELAP
Fluoranthene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.046 MAMNELAP
Fluorene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 1ND MAMNELAP
Indeno(1,2,3-cd)pyrene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.008 MAMNELAP
Naphthalene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 1ND MAMNELAP
Phenanthrene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.030 MAMNELAP
Pyrene 4/16/2010 11:39:00 AM0.004 mg/Kg-dry 10.036 MAMNELAP
Surr: 2-Fluorobiphenyl 4/16/2010 11:39:00 AM10-131 %REC 163.4 MAM
Surr: Nitrobenzene-d5 4/16/2010 11:39:00 AM10-132 %REC 165.5 MAM
Surr: p-Terphenyl-d14 4/16/2010 11:39:00 AM30.6-131 %REC 178.8 MAM
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
1,2-Dichlorobenzene 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
1,3-Dichlorobenzene 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
1,4-Dichlorobenzene 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
2,4,5-Trichlorophenol 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
2,4,6-Trichlorophenol 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
2,4-Dichlorophenol 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
2,4-Dimethylphenol S 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
2,4-Dinitrophenol 4/16/2010 10:03:00 AM1.12 mg/Kg-dry 1ND DMHNELAP
2,4-Dinitrotoluene 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
2,6-Dinitrotoluene 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
2-Chloronaphthalene 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
2-Chlorophenol 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
2-Methoxy-4-methylphenol 4/16/2010 10:03:00 AM0.725 mg/Kg-dry 1ND DMH
2-Methylnaphthalene 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
2-Nitroaniline 4/16/2010 10:03:00 AM1.12 mg/Kg-dry 1ND DMHNELAP
2-Nitrophenol 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
3,3´-Dichlorobenzidine 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
3-Nitroaniline 4/16/2010 10:03:00 AM1.12 mg/Kg-dry 1ND DMHNELAP
4,6-Dinitro-2-methylphenol 4/16/2010 10:03:00 AM1.12 mg/Kg-dry 1ND DMHNELAP
4-Bromophenyl phenyl ether 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
4-Chloro-3-methylphenol 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
4-Chloroaniline 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
4-Chlorophenyl phenyl ether 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
4-Nitroaniline 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
4-Nitrophenol 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
Aniline 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 6 of 53
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 4/14/2010 10:00:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 21-Apr-10
LABORATORY RESULTS
WorkOrder: 10040597
Lab ID: 10040597-001
Client Sample ID: P4-Borrow #1
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAzobenzene 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMH
Benzidine 4/16/2010 10:03:00 AM1.18 mg/Kg-dry 1see note DMHNELAP
Benzoic acid 4/16/2010 10:03:00 AM1.67 mg/Kg-dry 1ND DMHNELAP
Benzyl alcohol 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
Bis(2-chloroethoxy)methane 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
Bis(2-chloroethyl)ether 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
Bis(2-chloroisopropyl)ether 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
Butyl benzyl phthalate 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
Carbazole 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMH
Dibenzofuran 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
Diethyl phthalate 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
Dimethyl phthalate 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
Di-n-butyl phthalate 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
Di-n-octyl phthalate 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
Hexachlorobenzene 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
Hexachlorobutadiene 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
Hexachlorocyclopentadiene 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
Hexachloroethane 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
Isophorone 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
m,p-Cresol 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
Nitrobenzene 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
N-Nitrosodimethylamine 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
N-Nitroso-di-n-propylamine 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
N-Nitrosodiphenylamine 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
o-Cresol 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
Pentachlorophenol 4/16/2010 10:03:00 AM2.23 mg/Kg-dry 1ND DMHNELAP
Phenol 4/16/2010 10:03:00 AM0.390 mg/Kg-dry 1ND DMHNELAP
Pyridine 4/16/2010 10:03:00 AM0.558 mg/Kg-dry 1ND DMHNELAP
1,2-Diphenylhydrazine 4/16/2010 10:03:00 AM0.937 mg/Kg-dry 1ND DMH
Surr: 2,4,6-Tribromophenol 4/16/2010 10:03:00 AM32.7-130 %REC 174.0 DMH
Surr: 2-Fluorobiphenyl 4/16/2010 10:03:00 AM34.1-116 %REC 164.8 DMH
Surr: 2-Fluorophenol 4/16/2010 10:03:00 AM30.5-99 %REC 166.2 DMH
Surr: Nitrobenzene-d5 4/16/2010 10:03:00 AM34.1-101 %REC 160.9 DMH
Surr: Phenol-d5 4/16/2010 10:03:00 AM34.9-110 %REC 172.3 DMH
Surr: p-Terphenyl-d14 4/16/2010 10:03:00 AM41.7-124 %REC 179.6 DMH
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,1,1-Trichloroethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 7 of 53
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 4/14/2010 10:00:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 21-Apr-10
LABORATORY RESULTS
WorkOrder: 10040597
Lab ID: 10040597-001
Client Sample ID: P4-Borrow #1
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,2,2-Tetrachloroethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,1,2-Trichloro-1,2,2-trifluoroethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWE
1,1,2-Trichloroethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,1-Dichloro-2-propanone 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWE
1,1-Dichloroethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,1-Dichloroethene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,1-Dichloropropene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,2,3-Trichlorobenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,2,3-Trichloropropane 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP
1,2,3-Trimethylbenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWE
1,2,4-Trichlorobenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,2,4-Trimethylbenzene J 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 10.8 RWENELAP
1,2-Dibromo-3-chloropropane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,2-Dibromoethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,2-Dichlorobenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,2-Dichloroethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,2-Dichloropropane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,3,5-Trimethylbenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,3-Dichlorobenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,3-Dichloropropane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1,4-Dichlorobenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
1-Chlorobutane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
2,2-Dichloropropane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
2-Butanone 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP
2-Chlorotoluene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
2-Hexanone 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP
2-Nitropropane 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP
4-Chlorotoluene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
4-Methyl-2-pentanone 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP
Acetone 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP
Acrolein 4/16/2010 1:26:00 PM81.5 µg/Kg-dry 1ND RWENELAP
Acrylonitrile 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP
Allyl chloride 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Benzene 4/16/2010 1:26:00 PM0.8 µg/Kg-dry 11.8 RWENELAP
Bromobenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Bromochloromethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Bromodichloromethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Bromoform 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 8 of 53
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 4/14/2010 10:00:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 21-Apr-10
LABORATORY RESULTS
WorkOrder: 10040597
Lab ID: 10040597-001
Client Sample ID: P4-Borrow #1
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSBromomethane 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP
Carbon disulfide J 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 12.5 RWENELAP
Carbon tetrachloride 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Chlorobenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Chloroethane 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP
Chloroform 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Chloromethane 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP
cis-1,2-Dichloroethene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
cis-1,3-Dichloropropene 4/16/2010 1:26:00 PM3.3 µg/Kg-dry 1ND RWENELAP
Cyclohexanone 4/16/2010 1:26:00 PM81.5 µg/Kg-dry 1ND RWE
Dibromochloromethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Dibromomethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Dichlorodifluoromethane 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP
Ethyl acetate 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP
Ethyl ether 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Ethyl methacrylate 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Ethylbenzene J 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 11.1 RWENELAP
Heptane 4/16/2010 1:26:00 PM16.3 µg/Kg-dry 1ND RWE
Hexachlorobutadiene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Hexachloroethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Iodomethane 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP
Isopropylbenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
m,p-Xylenes J 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 12.7 RWENELAP
Methacrylonitrile 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP
Methyl Methacrylate 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Methyl tert-butyl ether 4/16/2010 1:26:00 PM1.6 µg/Kg-dry 1ND RWENELAP
Methylacrylate 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWE
Methylene chloride J 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 10.9 RWENELAP
Naphthalene 4/16/2010 1:26:00 PM8.1 µg/Kg-dry 1ND RWENELAP
n-Butylbenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
n-Hexane J 4/16/2010 1:26:00 PM16.3 µg/Kg-dry 13.4 RWE
Nitrobenzene 4/16/2010 1:26:00 PM81.5 µg/Kg-dry 1ND RWENELAP
n-Propylbenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
o-Xylene J 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 11.0 RWENELAP
Pentachloroethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
p-Isopropyltoluene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Propionitrile 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP
sec-Butylbenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 9 of 53
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 4/14/2010 10:00:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 21-Apr-10
LABORATORY RESULTS
WorkOrder: 10040597
Lab ID: 10040597-001
Client Sample ID: P4-Borrow #1
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
Sample NarrativeSW-846 3550B, 8151A, Chlorinated Herbicides by GC/ECD
Method blank show some PCP contamination, Result are below clients limits.SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.2,4-Dimethylphenol, 4-Nitrophenol, and 4-Chloro-3-methylphenol were outside upper QC limits in the LCS. Sample results are below reporting limit - data is reportable.2,4-Dimethylphenol was outside upper QC limits in the MS.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSStyrene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
tert-Butylbenzene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Tetrachloroethene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Tetrahydrofuran 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP
Toluene J 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 13.6 RWENELAP
trans-1,2-Dichloroethene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
trans-1,3-Dichloropropene 4/16/2010 1:26:00 PM3.3 µg/Kg-dry 1ND RWENELAP
Trichloroethene 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Trichlorofluoromethane 4/16/2010 1:26:00 PM4.1 µg/Kg-dry 1ND RWENELAP
Vinyl acetate 4/16/2010 1:26:00 PM40.7 µg/Kg-dry 1ND RWENELAP
Vinyl chloride 4/16/2010 1:26:00 PM1.6 µg/Kg-dry 1ND RWENELAP
Surr: 1,2-Dichloroethane-d4 4/16/2010 1:26:00 PM72.2-131 %REC 198.5 RWE
Surr: 4-Bromofluorobenzene 4/16/2010 1:26:00 PM82.1-116 %REC 183.0 RWE
Surr: Dibromofluoromethane 4/16/2010 1:26:00 PM77.7-120 %REC 1101.7 RWE
Surr: Toluene-d8 4/16/2010 1:26:00 PM86-116 %REC 1115.7 RWE
SW-846 7471AMercury 4/16/20100.011 mg/Kg-dry 10.020 JMWNELAP
SW-846 9012A (TOTAL)Cyanide 4/20/20100.53 mg/Kg-dry 1< 0.53 MVSNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 10 of 53
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 4/14/2010 10:15:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 21-Apr-10
LABORATORY RESULTS
WorkOrder: 10040597
Lab ID: 10040597-002
Client Sample ID: P4 Borrow #2
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 4/15/2010 4:10:00 PM0.1 % 19.9 JMT
STANDARD METHODS 18TH ED. 2540 GTotal Solids 4/15/2010 4:10:00 PM0.1 % 190.1 JMT
SW-846 3050B, 6010B, METALS BY ICPArsenic 4/16/2010 1:49:54 PM2.36 mg/Kg-dry 15.09 LALNELAP
Barium 4/16/2010 1:49:54 PM0.47 mg/Kg-dry 124.0 LALNELAP
Cadmium J 4/16/2010 1:49:54 PM0.19 mg/Kg-dry 10.12 LALNELAP
Chromium 4/16/2010 1:49:54 PM0.94 mg/Kg-dry 116.8 LALNELAP
Lead 4/16/2010 1:49:54 PM3.77 mg/Kg-dry 111.5 LALNELAP
Silver 4/16/2010 1:49:54 PM0.52 mg/Kg-dry 10.54 LALNELAP
SW-846 3050B, METALS BY GFAASelenium 7740 S 4/16/2010 1:44:48 PM0.588 mg/Kg-dry 1< 0.588 MEKNELAP
SW-846 3550B, 8081A, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
4,4´-DDE 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
4,4´-DDT 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
Alachlor 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
Aldrin 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
alpha-BHC 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
alpha-Chlordane 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
beta-BHC 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
Chlordane 4/16/2010 12:04:00 PM3.67 µg/Kg-dry 1ND HENELAP
delta-BHC 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
Dieldrin 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 12.49 HENELAP
Endosulfan I 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
Endosulfan II 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
Endosulfan sulfate 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
Endrin 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
Endrin aldehyde 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
Endrin ketone 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
gamma-BHC 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
gamma-Chlordane 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
Heptachlor 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
Heptachlor epoxide 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
Methoxychlor 4/16/2010 12:04:00 PM1.83 µg/Kg-dry 1ND HENELAP
Toxaphene 4/16/2010 12:04:00 PM32.9 µg/Kg-dry 1ND HENELAP
Surr: Decachlorobiphenyl 4/16/2010 12:04:00 PM48-149 %REC 165.6 HE
Surr: Tetrachloro-m-xylene 4/16/2010 12:04:00 PM19-145 %REC 165.3 HE
IL ELAP and NELAP Accredited - Accreditation #100226 Page 11 of 53
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 4/14/2010 10:15:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 21-Apr-10
LABORATORY RESULTS
WorkOrder: 10040597
Lab ID: 10040597-002
Client Sample ID: P4 Borrow #2
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 4/16/2010 11:05:00 AM41.1 µg/Kg-dry 1ND HENELAP
Aroclor 1221 4/16/2010 11:05:00 AM41.1 µg/Kg-dry 1ND HENELAP
Aroclor 1232 4/16/2010 11:05:00 AM41.1 µg/Kg-dry 1ND HENELAP
Aroclor 1242 4/16/2010 11:05:00 AM41.1 µg/Kg-dry 1ND HENELAP
Aroclor 1248 4/16/2010 11:05:00 AM41.1 µg/Kg-dry 1ND HENELAP
Aroclor 1254 4/16/2010 11:05:00 AM41.1 µg/Kg-dry 1ND HENELAP
Aroclor 1260 4/16/2010 11:05:00 AM41.1 µg/Kg-dry 1ND HENELAP
Surr: Decachlorobiphenyl 4/16/2010 11:05:00 AM5-156 %REC 172.0 HE
Surr: Tetrachloro-meta-xylene 4/16/2010 11:05:00 AM7.35-123 %REC 160.7 HE
SW-846 3550B, 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE
2,4,5-TP (Silvex) 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE
2,4-D 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE
2,4-DB 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE
3,5-Dichlorobenzoic Acid 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE
4-Nitrophenol 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE
Bentazon 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE
Chloramben 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE
Dalapon 4/16/2010 5:08:00 PM158 µg/Kg-dry 1ND HE
DCPA 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE
Dicamba 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE
Dichlorprop 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE
MCPA 4/16/2010 5:08:00 PM1580 µg/Kg-dry 1ND HE
MCPP 4/16/2010 5:08:00 PM1580 µg/Kg-dry 1ND HE
Pentachlorophenol 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE
Picloram 4/16/2010 5:08:00 PM15.8 µg/Kg-dry 1ND HE
Surr: 2,4-Dichlorophenylacetic acid 4/16/2010 5:08:00 PM18.1-118 %REC 156.6 HE
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Acenaphthylene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Anthracene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Benzo(a)anthracene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Benzo(a)pyrene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Benzo(b)fluoranthene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Benzo(g,h,i)perylene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Benzo(k)fluoranthene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Bis(2-ethylhexyl)phthalate 4/16/2010 1:24:00 PM0.074 mg/Kg-dry 1ND MAMNELAP
Chrysene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 12 of 53
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 4/14/2010 10:15:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 21-Apr-10
LABORATORY RESULTS
WorkOrder: 10040597
Lab ID: 10040597-002
Client Sample ID: P4 Borrow #2
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSDibenzo(a,h)anthracene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Fluoranthene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Fluorene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Indeno(1,2,3-cd)pyrene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Naphthalene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Phenanthrene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Pyrene 4/16/2010 1:24:00 PM0.004 mg/Kg-dry 1ND MAMNELAP
Surr: 2-Fluorobiphenyl 4/16/2010 1:24:00 PM10-131 %REC 164.6 MAM
Surr: Nitrobenzene-d5 4/16/2010 1:24:00 PM10-132 %REC 169.2 MAM
Surr: p-Terphenyl-d14 4/16/2010 1:24:00 PM30.6-131 %REC 178.7 MAM
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
1,2-Dichlorobenzene 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
1,3-Dichlorobenzene 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
1,4-Dichlorobenzene 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
2,4,5-Trichlorophenol 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
2,4,6-Trichlorophenol 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
2,4-Dichlorophenol 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
2,4-Dimethylphenol 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
2,4-Dinitrophenol 4/16/2010 10:32:00 AM1.11 mg/Kg-dry 1ND DMHNELAP
2,4-Dinitrotoluene 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
2,6-Dinitrotoluene 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
2-Chloronaphthalene 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
2-Chlorophenol 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
2-Methoxy-4-methylphenol 4/16/2010 10:32:00 AM0.720 mg/Kg-dry 1ND DMH
2-Methylnaphthalene 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
2-Nitroaniline 4/16/2010 10:32:00 AM1.11 mg/Kg-dry 1ND DMHNELAP
2-Nitrophenol 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
3,3´-Dichlorobenzidine 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
3-Nitroaniline 4/16/2010 10:32:00 AM1.11 mg/Kg-dry 1ND DMHNELAP
4,6-Dinitro-2-methylphenol 4/16/2010 10:32:00 AM1.11 mg/Kg-dry 1ND DMHNELAP
4-Bromophenyl phenyl ether 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
4-Chloro-3-methylphenol 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
4-Chloroaniline 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
4-Chlorophenyl phenyl ether 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
4-Nitroaniline 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
4-Nitrophenol 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
Aniline 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 13 of 53
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 4/14/2010 10:15:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 21-Apr-10
LABORATORY RESULTS
WorkOrder: 10040597
Lab ID: 10040597-002
Client Sample ID: P4 Borrow #2
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAzobenzene 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMH
Benzidine 4/16/2010 10:32:00 AM1.17 mg/Kg-dry 1see note DMHNELAP
Benzoic acid 4/16/2010 10:32:00 AM1.66 mg/Kg-dry 1ND DMHNELAP
Benzyl alcohol 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
Bis(2-chloroethoxy)methane 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
Bis(2-chloroethyl)ether 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
Bis(2-chloroisopropyl)ether 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
Butyl benzyl phthalate 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
Carbazole 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMH
Dibenzofuran 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
Diethyl phthalate 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
Dimethyl phthalate 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
Di-n-butyl phthalate 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
Di-n-octyl phthalate 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
Hexachlorobenzene 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
Hexachlorobutadiene 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
Hexachlorocyclopentadiene 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
Hexachloroethane 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
Isophorone 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
m,p-Cresol 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
Nitrobenzene 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
N-Nitrosodimethylamine 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
N-Nitroso-di-n-propylamine 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
N-Nitrosodiphenylamine 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
o-Cresol 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
Pentachlorophenol 4/16/2010 10:32:00 AM2.22 mg/Kg-dry 1ND DMHNELAP
Phenol 4/16/2010 10:32:00 AM0.388 mg/Kg-dry 1ND DMHNELAP
Pyridine 4/16/2010 10:32:00 AM0.554 mg/Kg-dry 1ND DMHNELAP
1,2-Diphenylhydrazine 4/16/2010 10:32:00 AM0.931 mg/Kg-dry 1ND DMH
Surr: 2,4,6-Tribromophenol 4/16/2010 10:32:00 AM32.7-130 %REC 179.5 DMH
Surr: 2-Fluorobiphenyl 4/16/2010 10:32:00 AM34.1-116 %REC 170.0 DMH
Surr: 2-Fluorophenol 4/16/2010 10:32:00 AM30.5-99 %REC 166.7 DMH
Surr: Nitrobenzene-d5 4/16/2010 10:32:00 AM34.1-101 %REC 166.7 DMH
Surr: Phenol-d5 4/16/2010 10:32:00 AM34.9-110 %REC 169.9 DMH
Surr: p-Terphenyl-d14 4/16/2010 10:32:00 AM41.7-124 %REC 179.7 DMH
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,1,1-Trichloroethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 14 of 53
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 4/14/2010 10:15:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 21-Apr-10
LABORATORY RESULTS
WorkOrder: 10040597
Lab ID: 10040597-002
Client Sample ID: P4 Borrow #2
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,2,2-Tetrachloroethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,1,2-Trichloro-1,2,2-trifluoroethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWE
1,1,2-Trichloroethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,1-Dichloro-2-propanone 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWE
1,1-Dichloroethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,1-Dichloroethene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,1-Dichloropropene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,2,3-Trichlorobenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,2,3-Trichloropropane 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP
1,2,3-Trimethylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 121.9 RWE
1,2,4-Trichlorobenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,2,4-Trimethylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 123.5 RWENELAP
1,2-Dibromo-3-chloropropane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,2-Dibromoethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,2-Dichlorobenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,2-Dichloroethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,2-Dichloropropane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,3,5-Trimethylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,3-Dichlorobenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,3-Dichloropropane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1,4-Dichlorobenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
1-Chlorobutane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
2,2-Dichloropropane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
2-Butanone 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP
2-Chlorotoluene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
2-Hexanone 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP
2-Nitropropane 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP
4-Chlorotoluene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
4-Methyl-2-pentanone 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP
Acetone 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP
Acrolein 4/16/2010 1:54:00 PM97.4 µg/Kg-dry 1ND RWENELAP
Acrylonitrile 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP
Allyl chloride 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Benzene 4/16/2010 1:54:00 PM1.0 µg/Kg-dry 12.7 RWENELAP
Bromobenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Bromochloromethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Bromodichloromethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Bromoform 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 15 of 53
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 4/14/2010 10:15:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 21-Apr-10
LABORATORY RESULTS
WorkOrder: 10040597
Lab ID: 10040597-002
Client Sample ID: P4 Borrow #2
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSBromomethane 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP
Carbon disulfide 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Carbon tetrachloride 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Chlorobenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Chloroethane 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP
Chloroform 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Chloromethane 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP
cis-1,2-Dichloroethene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
cis-1,3-Dichloropropene 4/16/2010 1:54:00 PM3.9 µg/Kg-dry 1ND RWENELAP
Cyclohexanone 4/16/2010 1:54:00 PM97.4 µg/Kg-dry 1ND RWE
Dibromochloromethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Dibromomethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Dichlorodifluoromethane 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP
Ethyl acetate 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP
Ethyl ether 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Ethyl methacrylate 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Ethylbenzene J 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 11.6 RWENELAP
Heptane 4/16/2010 1:54:00 PM19.5 µg/Kg-dry 1ND RWE
Hexachlorobutadiene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Hexachloroethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Iodomethane 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP
Isopropylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
m,p-Xylenes J 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 14.2 RWENELAP
Methacrylonitrile 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP
Methyl Methacrylate 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Methyl tert-butyl ether 4/16/2010 1:54:00 PM1.9 µg/Kg-dry 1ND RWENELAP
Methylacrylate 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWE
Methylene chloride 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Naphthalene 4/16/2010 1:54:00 PM9.7 µg/Kg-dry 1ND RWENELAP
n-Butylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
n-Hexane J 4/16/2010 1:54:00 PM19.5 µg/Kg-dry 13.7 RWE
Nitrobenzene 4/16/2010 1:54:00 PM97.4 µg/Kg-dry 1ND RWENELAP
n-Propylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 19.3 RWENELAP
o-Xylene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 18.6 RWENELAP
Pentachloroethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
p-Isopropyltoluene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Propionitrile 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP
sec-Butylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 16 of 53
Client Project: A831-735002-012901-225/Ameren C
Collection Date: 4/14/2010 10:15:00 AM
Matrix: SOLID
Client: PSC Industrial Outsourcing, LP
Report Date: 21-Apr-10
LABORATORY RESULTS
WorkOrder: 10040597
Lab ID: 10040597-002
Client Sample ID: P4 Borrow #2
Analyses Result Units Date AnalyzedRL DF AnalystCertification Qual
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
Sample NarrativeSW-846 9012A (Total)
RPD was outside of QC limit.Matrix interference present in sample.
SW-846 3050B, Metals by GFAA
Se- Matrix interference present in sample.SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.2,4-Dimethylphenol, 4-Nitrophenol, and 4-Chloro-3-methylphenol were outside upper QC limits in the LCS. Sample results are below reporting limit - data is reportable.
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS
Surrogate recovery was outside QC limits due to matrix interference.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSStyrene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
tert-Butylbenzene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Tetrachloroethene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Tetrahydrofuran 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP
Toluene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 15.8 RWENELAP
trans-1,2-Dichloroethene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
trans-1,3-Dichloropropene 4/16/2010 1:54:00 PM3.9 µg/Kg-dry 1ND RWENELAP
Trichloroethene 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Trichlorofluoromethane 4/16/2010 1:54:00 PM4.9 µg/Kg-dry 1ND RWENELAP
Vinyl acetate 4/16/2010 1:54:00 PM48.7 µg/Kg-dry 1ND RWENELAP
Vinyl chloride 4/16/2010 1:54:00 PM1.9 µg/Kg-dry 1ND RWENELAP
Surr: 1,2-Dichloroethane-d4 4/16/2010 1:54:00 PM72.2-131 %REC 1101.5 RWE
Surr: 4-Bromofluorobenzene S 4/16/2010 1:54:00 PM82.1-116 %REC 176.8 RWE
Surr: Dibromofluoromethane 4/16/2010 1:54:00 PM77.7-120 %REC 1104.4 RWE
Surr: Toluene-d8 S 4/16/2010 1:54:00 PM86-116 %REC 1124.9 RWE
SW-846 7471AMercury 4/16/20100.011 mg/Kg-dry 10.011 JMWNELAP
SW-846 9012A (TOTAL)Cyanide SR 4/20/20100.56 mg/Kg-dry 1< 0.56 MVSNELAP
IL ELAP and NELAP Accredited - Accreditation #100226 Page 17 of 53
Sample ID Client Sample ID Collection Date MatrixAnalysis
Date/Time
DATES REPORT
Lab Order: 10040597
Client: PSC Industrial Outsourcing, LPProject: A831-735002-012901-225/Ameren Champaign 6249080120
Test NamePrep
Date/Time
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
21-Apr-10Report Date:
10040597-001A P4-Borrow #1 4/14/2010 Solid SW-846 3550B, 8081A, Chlorinated Pesticides by GC/ECD
4/16/2010 10:51:00 AM
4/15/2010 6:43:00 PM
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD
4/16/2010 10:47:00 AM
4/15/2010 6:43:00 PM
SW-846 3550B, 8151A, Chlorinated Herbicides by GC/ECD
4/16/2010 4:36:00 PM
4/15/2010 4:56:37 PM
SW-846 3550B, 8151A, Chlorinated Herbicides by GC/ECD
4/19/2010 3:18:00 PM
4/15/2010 4:56:37 PM
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS
4/16/2010 11:39:00 AM
4/15/2010 4:57:58 PM
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS
4/16/2010 10:03:00 AM
4/15/2010 4:57:22 PM
10040597-001B EPA SW846 3550C, 5035A, ASTM D2974 4/15/2010 4:10:00 PM
Standard Methods 18th Ed. 2540 G 4/15/2010 4:10:00 PM
SW-846 3050B, 6010B, Metals by ICP 4/16/2010 1:43:07 PM
4/16/2010 8:03:41 AM
SW-846 3050B, 6010B, Metals by ICP 4/16/2010 2:29:18 PM
4/16/2010 8:03:41 AM
SW-846 3050B, Metals by GFAA 4/16/2010 1:41:26 PM
4/16/2010 8:01:46 AM
SW-846 7471A 4/16/20104/16/2010 8:45:49 AM
SW-846 9012A (Total) 4/20/2010
10040597-001E SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS
4/16/2010 1:26:00 PM
10040597-002A P4 Borrow #2 SW-846 3550B, 8081A, Chlorinated Pesticides by GC/ECD
4/16/2010 12:04:00 PM
4/15/2010 6:43:00 PM
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD
4/16/2010 11:05:00 AM
4/15/2010 6:43:00 PM
SW-846 3550B, 8151A, Chlorinated Herbicides by GC/ECD
4/16/2010 5:08:00 PM
4/15/2010 4:56:37 PM
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS
4/16/2010 1:24:00 PM
4/15/2010 4:57:58 PM
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS
4/16/2010 10:32:00 AM
4/15/2010 4:57:22 PM
10040597-002B EPA SW846 3550C, 5035A, ASTM D2974 4/15/2010 4:10:00 PM
Standard Methods 18th Ed. 2540 G 4/15/2010 4:10:00 PM
SW-846 3050B, 6010B, Metals by ICP 4/16/2010 1:49:54 PM
4/16/2010 8:03:41 AM
Page 18 of 53IL ELAP and NELAP Accredited - Accreditation #100226
Sample ID Client Sample ID Collection Date MatrixAnalysis
Date/Time
DATES REPORT
Lab Order: 10040597
Client: PSC Industrial Outsourcing, LPProject: A831-735002-012901-225/Ameren Champaign 6249080120
Test NamePrep
Date/Time
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
21-Apr-10Report Date:
10040597-002B P4 Borrow #2 4/14/2010 Solid SW-846 3050B, Metals by GFAA 4/16/2010 1:44:48 PM
4/16/2010 8:01:46 AM
SW-846 7471A 4/16/20104/16/2010 8:45:49 AM
SW-846 9012A (Total) 4/20/2010
10040597-002E SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS
4/16/2010 1:54:00 PM
Page 19 of 53IL ELAP and NELAP Accredited - Accreditation #100226
TEKLAB, INC 5445 HORSESHOE LAKE ROADCOLLINSVILLE, ILLINOIS 62234
ANALYTICAL QC SUMMARY REPORT
Qualifiers
- Analyte detected below reporting limits
- Analyte detected in the associated Method Blank
- Spike Recovery outside accepted recovery limits
- RPD outside accepted recovery limits- Not Detected at the Reporting Limit - Value above quantitation range
- Value exceeds Maximum Contaminant Level
- Reporting Limit
- Dilution Factor
- Too numerous to count ( > 200 CFU )
- Diluted out of sample
- Holding time exceeded- Surrogate Standard added by lab
- Matrix interference
- IL Dept. of Public Health
- IL ELAP and NELAP Accredited
DF
RL
TNTC
Surr
IDPH
B
J
R
S
X NELAP
E
MI
H
ND
D - Did not igniteDNI
- Unknown hydrocarbon#
- QC criteria failedQ
- Client requested RL below PQLC
CCV
DF
DUP
ICV
LCS
MS
MSD
MDL
MB/LCB
PQL
RL
RPD
Continuing calibration verification is a check of a standard to determine the state of calibration of an instrument between recalibration.
Dilution factor is the dilution performed during analysis only and does not take into account any dilutions made during sample preparation. The reported result is final and includes all dilutions factors.Laboratory duplicate is an aliquot of a sample taken from the same container under laboratory conditions for independent processing and analysis independently of the original aliquot. (NELAC)Initial calibration verification is a check of a standard to determine the state of calibration of an instrument before sample analysis is initiated.
Laboratory control sample, spiked with verified known amounts of analytes, is analyzed exactly like a sample to establish intra-laboratory or analyst specific precision and bias or to assess the performance of all or a portion of the measurement system. (NELAC) The acceptable recovery range is listed in this report.
Matrix spike is an aliquot of matrix fortified (spiked) with known quantities of specific analytes that is subjected to the entire analytical procedures in order to determine the effect of the matrix on an approved test method’s recovery system. The acceptable recovery range is listed in this report.Matrix spike duplicate means a replicate matrix spike that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in this report.Method detection limit or limit of detection (LOD) means the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type containing the analyte.Method blank or lab control blank is a sample of a matrix similar to the batch of associated sample (when available) that is free from the analytes of interest and is processed simultaneously with and under the same conditions as samples through all steps of the analytical procedures, and in which no target analytes or interferences are present at concentrations that impact the analytical results for sample analyses. (NELAC)Practical quantitation limit or limit of quantitation (LOQ) means the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine laboratory operation conditions. The acceptable recovery range is listed in this report.The reporting limit the lowest level that the data is displayed in the final report. The reporting limit may vary according to customer request or sample dilution. The reporting limit may not be less than the MDL.Relative percent difference is a calculated difference between two recoveries (ie. MS/MSD). The acceptable recovery limit is listed in this report.
SPK The spike is a known mass of target analyte added to a blank sample or sub-sample; used to determine recovery deficiency or for other quality control purposes. (NELAC)
Surr Surrogates are an organic compound which is similar to the analytes of interest in chemical composition and behavior in the analytical process, but which is not normally found in environmental samples.
Key QC concepts:
LCSD Laboratory control sample duplicate is a replicate laboratory control sample that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in this report.
Page 20 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: A_TCND_S_MT_9012A
21-Apr-10Report Date:
Sample ID: MB-R134671
Batch ID: R134671 Analysis Date: 4/20/2010
Prep Date:
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134671
SeqNo: 2586402
MBLKSampType:
Cyanide 0.01< 0.01
Sample ID: LCS-R134671
Batch ID: R134671 Analysis Date: 4/20/2010
Prep Date:
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134671
SeqNo: 2586403
LCSSampType:
Cyanide 0.1000 96.9 85 1150.01 00.10
Sample ID: 10040597-002BMS
Batch ID: R134671 Analysis Date: 4/20/2010
Prep Date:
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: P4 Borrow #2MS
RunNo: 134671
SeqNo: 2586406
MSSampType:
Cyanide 2.775 37.5 75 125 S0.56 01.04
Sample ID: 10040597-002BMSD
Batch ID: R134671 Analysis Date: 4/20/2010
Prep Date:
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: P4 Borrow #2MSD
RunNo: 134671
SeqNo: 2586407
MSDSampType:
Cyanide 2.775 59.0 75 125 15 SR0.56 0 1.042 44.41.64
Page 21 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: I_TS_M_MT
21-Apr-10Report Date:
Sample ID: LCS-R134542
Batch ID: R134542 Analysis Date: 4/15/2010
Prep Date:
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: %
PQL
Client ID: ZZZZZZ
RunNo: 134542
SeqNo: 2581567
LCSSampType:
Total Solids 1.000 100 90 1100.1 01.0
Sample ID: 10040597-002BDUP
Batch ID: R134542 Analysis Date: 4/15/2010
Prep Date:
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: %
PQL
Client ID: P4 Borrow #2DUP
RunNo: 134542
SeqNo: 2581622
DUPSampType:
Total Solids 150.1 90.08 1.5688.7
Sample ID: LCSQC
Batch ID: R134542 Analysis Date: 4/15/2010
Prep Date:
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: %
PQL
Client ID: ZZZZZZ
RunNo: 134542
SeqNo: 2581625
LCSQCSampType:
Total Solids 1.000 100 90 1100.1 01.0
Page 22 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: M_HG_SOLID
21-Apr-10Report Date:
Sample ID: MB-59794
Batch ID: 59794 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134501
SeqNo: 2580526
MBLKSampType:
SOP 3063
Mercury 0.01000 0 -100 1000.010 0< 0.010
Sample ID: LCS-59794
Batch ID: 59794 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134501
SeqNo: 2580527
LCSSampType:
SOP 3063
Mercury 0.2500 105.6 85 1150.010 00.264
Sample ID: 10040597-002BMS
Batch ID: 59794 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: P4 Borrow #2MS
RunNo: 134501
SeqNo: 2580532
MSSampType:
SOP 3063
Mercury 0.2708 107.8 75 1250.011 0.011370.303
Sample ID: 10040597-002BMSD
Batch ID: 59794 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: P4 Borrow #2MSD
RunNo: 134501
SeqNo: 2580533
MSDSampType:
SOP 3063
Mercury 0.2708 103.8 75 125 150.011 0.01137 0.3033 3.640.292
Page 23 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: M_SOLID_GF
21-Apr-10Report Date:
Sample ID: MB-59792
Batch ID: 59792 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 134537
SeqNo: 2581516
MBLKSampType:
SOP 3042
Selenium 7740 0.6000 0 -100 1000.600 0< 0.600
Sample ID: LCS-59792
Batch ID: 59792 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 134537
SeqNo: 2581517
LCSSampType:
SOP 3042
Selenium 7740 3.000 83.8 80 1200.600 02.51
Sample ID: 10040597-002BMS
Batch ID: 59792 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: P4 Borrow #2MS
RunNo: 134537
SeqNo: 2581520
MSSampType:
SOP 3042
Selenium 7740 2.941 38.4 70 130 JS1.18 01.1
Sample ID: 10040597-002BMSD
Batch ID: 59792 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: P4 Borrow #2MSD
RunNo: 134537
SeqNo: 2581521
MSDSampType:
SOP 3042
Selenium 7740 2.941 38.8 70 130 20 JS1.18 0 1.130 01.1
Page 24 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: M_SOLIDS_ICP
21-Apr-10Report Date:
Sample ID: MB-59793
Batch ID: 59793 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 134503
SeqNo: 2581304
MBLKSampType:
SOP 3032
Arsenic 2.500 0 -100 1002.50 0< 2.50
Barium 0.5000 0 -100 1000.50 0< 0.50
Cadmium 0.2000 0 -100 1000.20 0< 0.20
Chromium 1.000 0 -100 1001.00 0< 1.00
Lead 4.000 0 -100 1004.00 0< 4.00
Silver 1.000 0 -100 1000.55 0< 0.55
Sample ID: LCS-59793
Batch ID: 59793 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 134503
SeqNo: 2581305
LCSSampType:
SOP 3032
Arsenic 200.0 109.8 85 1152.50 0220
Barium 200.0 105.0 85 1150.50 0210
Cadmium 5.000 106.4 85 1150.20 05.32
Chromium 20.00 113.4 85 1151.00 022.7
Lead 50.00 109.6 85 1154.00 054.8
Silver 5.000 108.2 85 1150.55 05.41
Sample ID: 10040597-002BMS
Batch ID: 59793 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: P4 Borrow #2MS
RunNo: 134503
SeqNo: 2581309
MSSampType:
SOP 3032
Arsenic 188.7 100.8 75 1252.36 5.094195
Barium 188.7 87.7 75 1250.47 23.99190
Cadmium 4.717 88.8 75 1250.19 0.12264.31
Chromium 18.87 111.0 75 1250.94 16.8137.7
Lead 47.17 89.3 75 1253.77 11.5453.7
Silver 4.717 102.2 75 1250.52 0.53775.36
Page 25 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: M_SOLIDS_ICP
21-Apr-10Report Date:
Sample ID: 10040597-002BMSD
Batch ID: 59793 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: P4 Borrow #2MSD
RunNo: 134503
SeqNo: 2581408
MSDSampType:
SOP 3032
Arsenic 188.7 100.2 75 125 202.36 5.094 195.3 0.630194
Barium 188.7 85.0 75 125 200.47 23.99 189.5 2.72184
Cadmium 4.717 88.2 75 125 200.19 0.1226 4.311 0.6594.28
Chromium 18.87 100.7 75 125 200.94 16.81 37.75 5.2835.8
Lead 47.17 87.2 75 125 203.77 11.54 53.65 1.8652.7
Silver 4.717 102.6 75 125 200.52 0.5377 5.358 0.3515.38
Sample ID: MB-59793
Batch ID: 59793 Analysis Date: 4/19/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 134602
SeqNo: 2583846
MBLKSampType:
SOP 3032
Chromium 1.000 58.0 -100 100 J1.00 00.58
Sample ID: LCS-59793
Batch ID: 59793 Analysis Date: 4/19/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 134602
SeqNo: 2583847
LCSSampType:
SOP 3032
Chromium 20.00 101.2 85 1151.00 020.2
Sample ID: MB-59793
Batch ID: 59793 Analysis Date: 4/19/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 134602
SeqNo: 2584281
MBLKSampType:
SOP 3032
Lead 4.000 0 -100 1004.00 0< 4.00
Sample ID: LCS-59793
Batch ID: 59793 Analysis Date: 4/19/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: ZZZZZZ
RunNo: 134602
SeqNo: 2584282
LCSSampType:
SOP 3032
Lead 50.00 101.2 85 1154.00 050.6
Page 26 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8081S_S
21-Apr-10Report Date:
Sample ID: MB-59787
Batch ID: 59787 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134530
SeqNo: 2581259
MBLKSampType:
SW3550B
4,4´-DDD 1.67ND
4,4´-DDE 1.67ND
4,4´-DDT 1.67ND
Alachlor 1.67ND
Aldrin 1.67ND
alpha-BHC 1.67ND
alpha-Chlordane 1.67ND
beta-BHC 1.67ND
Chlordane 3.34ND
delta-BHC 1.67ND
Dieldrin 1.67ND
Endosulfan I 1.67ND
Endosulfan II 1.67ND
Endosulfan sulfate 1.67ND
Endrin 1.67ND
Endrin aldehyde 1.67ND
Endrin ketone 1.67ND
gamma-BHC 1.67ND
gamma-Chlordane 1.67ND
Heptachlor 1.67ND
Heptachlor epoxide 1.67ND
Methoxychlor 1.67ND
Toxaphene 30.0ND
Surr: Decachlorobiphenyl 8.330 88.9 73.5 1507.41
Surr: Tetrachloro-m-xylene 8.330 67.2 14.4 1135.60
Sample ID: LCSPST-59787
Batch ID: 59787 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134530
SeqNo: 2581260
LCSSampType:
SW3550B
4,4´-DDD 8.330 96.7 36 2081.67 08.06
Page 27 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8081S_S
21-Apr-10Report Date:
Sample ID: LCSPST-59787
Batch ID: 59787 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134530
SeqNo: 2581260
LCSSampType:
SW3550B
4,4´-DDE 8.330 94.1 26 1911.67 07.84
4,4´-DDT 8.330 102.8 3 2151.67 08.57
Alachlor 8.330 109.8 30 1701.67 09.14
Aldrin 8.330 84.8 46 1731.67 07.06
alpha-BHC 8.330 77.1 37 1791.67 06.43
alpha-Chlordane 8.330 102.1 38 1871.67 08.51
beta-BHC 8.330 97.9 51 1851.67 08.15
delta-BHC 8.330 95.2 46 1661.67 07.93
Dieldrin 8.330 93.2 26 2161.67 07.76
Endosulfan I 8.330 88.8 31 2051.67 07.39
Endosulfan II 8.330 97.5 42 1871.67 08.12
Endosulfan sulfate 8.330 103.6 29 2301.67 08.63
Endrin 8.330 99.0 30 2151.67 08.25
Endrin aldehyde 8.330 92.5 42 2021.67 07.70
Endrin ketone 8.330 102.9 19 2441.67 08.57
gamma-BHC 8.330 87.2 55 1661.67 07.26
gamma-Chlordane 8.330 92.8 23 1861.67 07.73
Heptachlor 8.330 86.7 43 1721.67 07.22
Heptachlor epoxide 8.330 98.1 39 2041.67 08.17
Methoxychlor 8.330 107.2 3 2211.67 08.93
Surr: Decachlorobiphenyl 8.330 95.5 50.4 1767.95
Surr: Tetrachloro-m-xylene 8.330 69.7 10 1075.81
Sample ID: 10040597-001AMS
Batch ID: 59787 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg-dry
PQL
Client ID: P4-Borrow #1MS
RunNo: 134530
SeqNo: 2581262
MSSampType:
SW3550B
4,4´-DDD 9.251 91.8 36 2081.85 08.49
4,4´-DDE 9.251 83.8 26 1911.85 07.75
4,4´-DDT 9.251 95.5 3 2151.85 08.83
Alachlor 9.251 117.1 30 1701.85 010.8
Page 28 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8081S_S
21-Apr-10Report Date:
Sample ID: 10040597-001AMS
Batch ID: 59787 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg-dry
PQL
Client ID: P4-Borrow #1MS
RunNo: 134530
SeqNo: 2581262
MSSampType:
SW3550B
Aldrin 9.251 79.3 46 1731.85 07.34
alpha-BHC 9.251 74.6 37 1791.85 06.90
alpha-Chlordane 9.251 89.4 38 1871.85 08.27
beta-BHC 9.251 86.6 51 1851.85 08.01
delta-BHC 9.251 83.6 46 1661.85 07.74
Dieldrin 9.251 73.9 26 2161.85 3.89010.7
Endosulfan I 9.251 83.0 31 2051.85 07.67
Endosulfan II 9.251 86.2 42 1871.85 07.98
Endosulfan sulfate 9.251 84.1 29 2301.85 07.78
Endrin 9.251 88.5 30 2151.85 08.18
Endrin aldehyde 9.251 82.0 42 2021.85 07.59
Endrin ketone 9.251 99.0 19 2441.85 09.16
gamma-BHC 9.251 82.6 55 1661.85 07.64
gamma-Chlordane 9.251 84.5 23 1861.85 07.82
Heptachlor 9.251 81.1 43 1721.85 07.51
Heptachlor epoxide 9.251 89.1 39 2041.85 08.25
Methoxychlor 9.251 93.5 3 2211.85 08.65
Surr: Decachlorobiphenyl 9.251 79.3 48 1497.34
Surr: Tetrachloro-m-xylene 9.251 73.9 19 1456.84
Sample ID: 10040597-001AMSD
Batch ID: 59787 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg-dry
PQL
Client ID: P4-Borrow #1MSD
RunNo: 134530
SeqNo: 2581263
MSDSampType:
SW3550B
4,4´-DDD 9.200 98.0 36 208 401.84 0 8.493 5.949.01
4,4´-DDE 9.200 90.0 26 191 401.84 0 7.753 6.598.28
4,4´-DDT 9.200 98.0 3 215 401.84 0 8.830 2.099.02
Alachlor 9.200 107.3 30 170 401.84 0 10.83 9.299.87
Aldrin 9.200 83.0 46 173 401.84 0 7.339 4.027.64
alpha-BHC 9.200 76.4 37 179 401.84 0 6.902 1.847.03
alpha-Chlordane 9.200 95.0 38 187 401.84 0 8.266 5.588.74
Page 29 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8081S_S
21-Apr-10Report Date:
Sample ID: 10040597-001AMSD
Batch ID: 59787 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg-dry
PQL
Client ID: P4-Borrow #1MSD
RunNo: 134530
SeqNo: 2581263
MSDSampType:
SW3550B
beta-BHC 9.200 90.7 51 185 401.84 0 8.008 4.108.34
delta-BHC 9.200 89.1 46 166 401.84 0 7.738 5.798.20
Dieldrin 9.200 81.5 26 216 401.84 3.890 10.73 5.9711.4
Endosulfan I 9.200 87.1 31 205 401.84 0 7.674 4.288.01
Endosulfan II 9.200 90.4 42 187 401.84 0 7.977 4.168.32
Endosulfan sulfate 9.200 87.1 29 230 401.84 0 7.782 2.988.02
Endrin 9.200 92.8 30 215 401.84 0 8.183 4.298.54
Endrin aldehyde 9.200 85.7 42 202 401.84 0 7.587 3.877.89
Endrin ketone 9.200 102.7 19 244 401.84 0 9.159 3.149.45
gamma-BHC 9.200 85.1 55 166 401.84 0 7.638 2.447.83
gamma-Chlordane 9.200 90.0 23 186 401.84 0 7.816 5.798.28
Heptachlor 9.200 86.9 43 172 401.84 0 7.505 6.277.99
Heptachlor epoxide 9.200 93.0 39 204 401.84 0 8.246 3.738.56
Methoxychlor 9.200 97.0 3 221 401.84 0 8.648 3.128.92
Surr: Decachlorobiphenyl 9.200 69.5 48 149 4006.39
Surr: Tetrachloro-m-xylene 9.200 71.2 19 145 4006.55
Page 30 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8082S_S
21-Apr-10Report Date:
Sample ID: MB-59787
Batch ID: 59787 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134528
SeqNo: 2581179
MBLKSampType:
SW3550B
Aroclor 1016 37.5ND
Aroclor 1221 37.5ND
Aroclor 1232 37.5ND
Aroclor 1242 37.5ND
Aroclor 1248 37.5ND
Aroclor 1254 37.5ND
Aroclor 1260 37.5ND
Surr: Decachlorobiphenyl 8.300 93.3 47.2 1287.7
Surr: Tetrachloro-meta-xylene 8.300 73.4 21 98.96.1
Sample ID: LCSPCB-59787
Batch ID: 59787 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134528
SeqNo: 2581180
LCSSampType:
SW3550B
Aroclor 1016 166.7 107.7 54.9 12137.5 0180
Aroclor 1260 166.7 117.1 65.5 13337.5 0195
Surr: Decachlorobiphenyl 8.300 104.9 47.2 1288.7
Surr: Tetrachloro-meta-xylene 8.300 76.3 21 98.96.3
Sample ID: 10040597-002AMS
Batch ID: 59787 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg-dry
PQL
Client ID: P4 Borrow #2MS
RunNo: 134528
SeqNo: 2581183
MSSampType:
SW3550B
Aroclor 1016 185.0 88.7 35.8 14341.6 0164
Aroclor 1260 185.0 101.3 22.3 15241.6 0187
Surr: Decachlorobiphenyl 9.211 89.9 5 1568.3
Surr: Tetrachloro-meta-xylene 9.211 66.0 7.35 1236.1
Page 31 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8082S_S
21-Apr-10Report Date:
Sample ID: 10040597-002AMSD
Batch ID: 59787 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg-dry
PQL
Client ID: P4 Borrow #2MSD
RunNo: 134528
SeqNo: 2581184
MSDSampType:
SW3550B
Aroclor 1016 182.4 91.9 35.8 143 4041.0 0 164.1 2.09168
Aroclor 1260 182.4 100.9 22.3 152 4041.0 0 187.3 1.80184
Surr: Decachlorobiphenyl 9.081 89.3 5 156 4008.1
Surr: Tetrachloro-meta-xylene 9.081 66.2 7.35 123 4006.0
Page 32 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8151S_S
21-Apr-10Report Date:
Sample ID: MB-59782
Batch ID: 59782 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134530
SeqNo: 2583232
MBLKSampType:
SW8151A
2,4,5-T 10.0ND
2,4,5-TP (Silvex) 10.0ND
2,4-D 10.0ND
2,4-DB 10.0ND
3,5-Dichlorobenzoic Acid 10.0ND
4-Nitrophenol 10.0ND
Bentazon 10.0ND
Chloramben 10.0ND
Dalapon 100ND
DCPA 10.0ND
Dicamba 10.0ND
Dichlorprop 10.0ND
MCPA 1000ND
MCPP 1000ND
Pentachlorophenol 10.0ND
Picloram 10.0ND
Surr: 2,4-Dichlorophenylacetic acid 13.33 60.0 18.1 1187.99
Sample ID: LCS-59782
Batch ID: 59782 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134530
SeqNo: 2583233
LCSSampType:
SW8151A
2,4,5-T 13.33 66.1 34.9 160 J10.0 08.8
2,4,5-TP (Silvex) 13.33 73.8 30.2 161 J10.0 09.8
2,4-D 13.33 71.5 27.4 139 J10.0 09.5
2,4-DB 13.33 68.7 13.6 174 J10.0 09.2
3,5-Dichlorobenzoic Acid 13.33 56.4 18.4 146 J10.0 07.5
4-Nitrophenol 13.33 62.5 18.6 153 J10.0 08.3
Bentazon 13.33 103.7 29.2 15710.0 013.8
Chloramben 13.33 50.3 10.6 130 J10.0 06.7
Dalapon 133.3 19.6 5 56.4 J100 026
Page 33 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8151S_S
21-Apr-10Report Date:
Sample ID: LCS-59782
Batch ID: 59782 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134530
SeqNo: 2583233
LCSSampType:
SW8151A
DCPA 13.33 68.3 10 171 J10.0 09.1
Dicamba 13.33 54.9 23.4 136 J10.0 07.3
Dichlorprop 13.33 80.6 19.5 14110.0 010.7
MCPA 1333 88.6 9.86 1811000 01180
MCPP 1333 63.9 4.61 171 J1000 0850
Pentachlorophenol 13.33 39.9 29.7 128 J10.0 05.3
Picloram 13.33 107.1 33.3 13810.0 014.3
Surr: 2,4-Dichlorophenylacetic acid 13.33 51.9 18.1 1186.92
Sample ID: LCSD-59782
Batch ID: 59782 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134530
SeqNo: 2583234
LCSDSampType:
SW8151A
2,4,5-T 13.33 70.1 34.9 160 30 J10.0 0 8.818 09.3
2,4,5-TP (Silvex) 13.33 79.9 30.2 161 3010.0 0 9.838 7.9410.7
2,4-D 13.33 77.6 27.4 139 3010.0 0 9.539 8.0710.3
2,4-DB 13.33 79.6 13.6 174 3010.0 0 9.158 14.710.6
3,5-Dichlorobenzoic Acid 13.33 56.5 18.4 146 30 J10.0 0 7.522 07.5
4-Nitrophenol 13.33 69.7 18.6 153 30 J10.0 0 8.333 09.3
Bentazon 13.33 85.2 29.2 157 3010.0 0 13.83 19.711.4
Chloramben 13.33 55.4 10.6 130 30 J10.0 0 6.707 07.4
Dalapon 133.3 22.3 5 56.4 30 J100 0 26.15 030
DCPA 13.33 77.7 10 171 3010.0 0 9.112 12.810.4
Dicamba 13.33 60.6 23.4 136 30 J10.0 0 7.324 08.1
Dichlorprop 13.33 79.6 19.5 141 3010.0 0 10.74 1.1910.6
MCPA 1333 99.7 9.86 181 301000 0 1182 11.71330
MCPP 1333 63.6 4.61 171 30 J1000 0 851.6 0850
Pentachlorophenol 13.33 45.3 29.7 128 30 J10.0 0 5.325 06.0
Picloram 13.33 113.7 33.3 138 3010.0 0 14.28 5.9515.2
Surr: 2,4-Dichlorophenylacetic acid 13.33 53.6 18.1 118 3007.15
Page 34 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8151S_S
21-Apr-10Report Date:
Sample ID: 10040597-002AMS
Batch ID: 59782 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg-dry
PQL
Client ID: P4 Borrow #2MS
RunNo: 134530
SeqNo: 2583237
MSSampType:
SW8151A
2,4,5-T 43.07 64.9 34.9 16016.2 027.9
2,4,5-TP (Silvex) 43.07 73.6 30.2 16116.2 031.7
2,4-D 43.07 71.2 27.4 13916.2 030.7
2,4-DB 43.07 82.2 13.6 17416.2 035.4
3,5-Dichlorobenzoic Acid 43.07 45.9 18.4 14616.2 019.8
Bentazon 43.07 57.1 29.2 15716.2 024.6
Chloramben 43.07 44.3 10.6 13016.2 019.1
Dalapon 430.7 20.7 5 56.4 J162 089
DCPA 43.07 72.1 10 17116.2 031.1
Dicamba 43.07 57.1 23.4 13616.2 024.6
Dichlorprop 43.07 73.8 19.5 14116.2 031.8
MCPA 4307 102.5 9.86 1811620 04410
MCPP 4307 57.6 4.61 1711620 02480
Picloram 43.07 102.7 33.3 13816.2 044.2
Surr: 2,4-Dichlorophenylacetic acid 43.07 48.6 18.1 11820.9
Sample ID: 10040597-002AMSD
Batch ID: 59782 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg-dry
PQL
Client ID: P4 Borrow #2MSD
RunNo: 134530
SeqNo: 2583238
MSDSampType:
SW8151A
2,4,5-T 42.45 57.3 34.9 160 015.9 0 27.94 13.824.3
2,4,5-TP (Silvex) 42.45 63.8 30.2 161 015.9 0 31.71 15.827.1
2,4-D 42.45 59.0 27.4 139 015.9 0 30.67 20.225.0
2,4-DB 42.45 78.9 13.6 174 015.9 0 35.40 5.5433.5
3,5-Dichlorobenzoic Acid 42.45 42.7 18.4 146 015.9 0 19.77 8.8118.1
Bentazon 42.45 45.1 29.2 157 015.9 0 24.61 24.919.2
Chloramben 42.45 44.1 10.6 130 015.9 0 19.10 2.0418.7
Dalapon 424.5 18.2 5 56.4 0 J159 0 89.34 077
DCPA 42.45 46.3 10 171 015.9 0 31.06 45.019.7
Dicamba 42.45 52.5 23.4 136 015.9 0 24.61 9.9822.3
Dichlorprop 42.45 51.3 19.5 141 015.9 0 31.78 37.421.8
Page 35 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8151S_S
21-Apr-10Report Date:
Sample ID: 10040597-002AMSD
Batch ID: 59782 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg-dry
PQL
Client ID: P4 Borrow #2MSD
RunNo: 134530
SeqNo: 2583238
MSDSampType:
SW8151A
MCPA 4245 117.2 9.86 181 01590 0 4415 11.94980
MCPP 4245 57.2 4.61 171 01590 0 2483 2.142430
Picloram 42.45 92.2 33.3 138 015.9 0 44.23 12.239.1
Surr: 2,4-Dichlorophenylacetic acid 42.45 42.1 18.1 118 0017.9
Page 36 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S
21-Apr-10Report Date:
Sample ID: MB-59753
Batch ID: 59753 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134531
SeqNo: 2581283
MBLKSampType:
SW3550B
1,2,4-Trichlorobenzene 0.500ND
1,2-Dichlorobenzene 0.500ND
1,3-Dichlorobenzene 0.500ND
1,4-Dichlorobenzene 0.500ND
2,4,5-Trichlorophenol 0.350ND
2,4,6-Trichlorophenol 0.350ND
2,4-Dichlorophenol 0.500ND
2,4-Dimethylphenol 0.500ND
2,4-Dinitrophenol 1.00ND
2,4-Dinitrotoluene 0.350ND
2,6-Dinitrotoluene 0.350ND
2-Chloronaphthalene 0.350ND
2-Chlorophenol 0.500ND
2-Methoxy-4-methylphenol 0.650ND
2-Methylnaphthalene 0.350ND
2-Nitroaniline 1.00ND
2-Nitrophenol 0.350ND
3,3´-Dichlorobenzidine 0.350ND
3-Nitroaniline 1.00ND
4,6-Dinitro-2-methylphenol 1.00ND
4-Bromophenyl phenyl ether 0.350ND
4-Chloro-3-methylphenol 0.500ND
4-Chloroaniline 0.500ND
4-Chlorophenyl phenyl ether 0.350ND
4-Nitroaniline 0.500ND
4-Nitrophenol 0.350ND
Acenaphthene 0.350ND
Acenaphthylene 0.350ND
Aniline 0.500ND
Anthracene 0.350ND
Azobenzene 0.350ND
Page 37 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S
21-Apr-10Report Date:
Sample ID: MB-59753
Batch ID: 59753 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134531
SeqNo: 2581283
MBLKSampType:
SW3550B
Benzidine 1.06ND
Benzo(a)anthracene 0.350ND
Benzo(a)pyrene 0.350ND
Benzo(b)fluoranthene 0.350ND
Benzo(g,h,i)perylene 0.350ND
Benzo(k)fluoranthene 0.350ND
Benzoic acid 1.50ND
Benzyl alcohol 0.500ND
Bis(2-chloroethoxy)methane 0.350ND
Bis(2-chloroethyl)ether 0.500ND
Bis(2-chloroisopropyl)ether 0.350ND
Bis(2-ethylhexyl)phthalate 0.350ND
Butyl benzyl phthalate 0.350ND
Carbazole 0.500ND
Chrysene 0.350ND
Dibenzo(a,h)anthracene 0.350ND
Dibenzofuran 0.350ND
Diethyl phthalate 0.500ND
Dimethyl phthalate 0.350ND
Di-n-butyl phthalate 0.350ND
Di-n-octyl phthalate 0.350ND
Fluoranthene 0.350ND
Fluorene 0.350ND
Hexachlorobenzene 0.350ND
Hexachlorobutadiene 0.500ND
Hexachlorocyclopentadiene 0.350ND
Hexachloroethane 0.500ND
Indeno(1,2,3-cd)pyrene 0.350ND
Isophorone 0.350ND
m,p-Cresol 0.500ND
Naphthalene 0.350ND
Page 38 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S
21-Apr-10Report Date:
Sample ID: MB-59753
Batch ID: 59753 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134531
SeqNo: 2581283
MBLKSampType:
SW3550B
Nitrobenzene 0.500ND
N-Nitrosodimethylamine 0.500ND
N-Nitroso-di-n-propylamine 0.500ND
N-Nitrosodiphenylamine 0.500ND
o-Cresol 0.500ND
Pentachlorophenol 2.00ND
Phenanthrene 0.350ND
Phenol 0.350ND
Pyrene 0.500ND
Pyridine 0.500ND
1,2-Diphenylhydrazine 0.840ND
Surr: 2,4,6-Tribromophenol 1.670 77.2 52.1 1131.29
Surr: 2-Fluorobiphenyl 0.8350 70.1 46.3 1060.585
Surr: 2-Fluorophenol 1.670 74.9 50.6 891.25
Surr: Nitrobenzene-d5 0.8350 69.7 42.4 99.20.582
Surr: Phenol-d5 1.670 76.8 55.9 98.51.28
Surr: p-Terphenyl-d14 0.8350 82.0 45.5 1150.685
Sample ID: LCS-59753
Batch ID: 59753 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134531
SeqNo: 2581284
LCSSampType:
SW3550B
1,2,4-Trichlorobenzene 1.670 78.7 43.9 92.20.500 01.31
1,4-Dichlorobenzene 1.670 64.2 43.8 84.10.500 01.07
2,4,5-Trichlorophenol 3.330 102.4 38.6 1230.350 03.41
2,4,6-Trichlorophenol 3.330 112.1 35.9 1230.350 03.73
2,4-Dimethylphenol 3.330 97.0 38.3 88 S0.500 03.23
2,4-Dinitrophenol 3.330 84.5 1.88 1621.00 02.81
2,4-Dinitrotoluene 1.670 72.2 48.6 1020.350 01.21
2-Chlorophenol 3.330 81.7 46.6 840.500 02.72
4-Chloro-3-methylphenol 3.330 99.1 51.5 94.9 S0.500 03.30
Page 39 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S
21-Apr-10Report Date:
Sample ID: LCS-59753
Batch ID: 59753 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134531
SeqNo: 2581284
LCSSampType:
SW3550B
4-Nitrophenol 3.330 105.9 53.2 104 S0.350 03.53
Acenaphthene 1.670 78.9 50.8 1130.350 01.32
Acenaphthylene 1.670 83.5 52.8 1210.350 01.39
Anthracene 1.670 77.9 53.3 1150.350 01.30
Benzo(a)anthracene 1.670 77.5 62.3 1100.350 01.30
Benzo(a)pyrene 1.670 82.8 58.2 1090.350 01.38
Benzo(b)fluoranthene 1.670 85.9 51.8 1070.350 01.43
Benzo(g,h,i)perylene 1.670 102.5 49.6 1210.350 01.71
Benzo(k)fluoranthene 1.670 91.0 63.1 1290.350 01.52
Bis(2-ethylhexyl)phthalate 1.670 84.5 56.3 1090.350 01.41
Chrysene 1.670 84.9 58.4 1150.350 01.42
Dibenzo(a,h)anthracene 1.670 97.8 54.9 1200.350 01.63
Diethyl phthalate 3.330 93.9 51.7 1060.500 03.13
Dimethyl phthalate 3.330 90.8 58.8 1040.350 03.02
Di-n-butyl phthalate 1.670 83.1 54.3 1050.350 01.39
Fluoranthene 1.670 87.3 61.6 1130.350 01.46
Fluorene 1.670 74.7 52.2 1160.350 01.25
Hexachlorobenzene 3.330 94.4 55.9 1060.350 03.14
Hexachlorobutadiene 3.330 84.5 35.7 1000.500 02.82
Hexachloroethane 3.330 76.8 38.9 89.90.500 02.56
Indeno(1,2,3-cd)pyrene 1.670 100.3 52.7 1150.350 01.68
m,p-Cresol 1.670 86.1 37.6 93.70.500 01.44
Naphthalene 1.670 73.9 45.7 1010.350 01.23
Nitrobenzene 3.330 78.0 51.8 1040.500 02.60
N-Nitroso-di-n-propylamine 1.670 83.6 49.1 94.50.500 01.40
o-Cresol 1.670 73.3 43 1010.500 01.22
Pentachlorophenol 3.330 85.7 42.2 1022.00 02.86
Phenanthrene 1.670 83.1 52.9 1130.350 01.39
Phenol 3.330 77.3 41.6 81.30.350 02.57
Pyrene 1.670 83.6 60.7 1150.500 01.40
Pyridine 3.330 45.7 3.61 74.30.500 01.52
Page 40 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S
21-Apr-10Report Date:
Sample ID: LCS-59753
Batch ID: 59753 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134531
SeqNo: 2581284
LCSSampType:
SW3550B
Surr: 2,4,6-Tribromophenol 1.670 78.7 52.1 1131.31
Surr: 2-Fluorobiphenyl 0.8350 70.0 46.3 1060.584
Surr: 2-Fluorophenol 1.670 67.4 50.6 891.13
Surr: Nitrobenzene-d5 0.8350 74.1 42.4 99.20.619
Surr: Phenol-d5 1.670 80.0 55.9 98.51.34
Surr: p-Terphenyl-d14 0.8350 82.8 45.5 1150.691
Sample ID: 10040597-001AMS
Batch ID: 59753 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: P4-Borrow #1MS
RunNo: 134531
SeqNo: 2581287
MSSampType:
SW3550B
1,2,4-Trichlorobenzene 1.885 74.3 35.9 1020.564 01.40
1,4-Dichlorobenzene 1.885 62.8 29.8 95.50.564 01.18
2,4,5-Trichlorophenol 3.759 90.8 38.6 1230.395 03.41
2,4,6-Trichlorophenol 3.759 103.8 35.9 1230.395 03.90
2,4-Dimethylphenol 3.759 97.2 38.3 88 S0.564 03.65
2,4-Dinitrophenol 3.759 54.1 1.88 1621.13 02.03
2,4-Dinitrotoluene 1.885 73.3 37.5 1070.395 01.38
2-Chlorophenol 3.759 81.0 22.6 1080.564 03.04
4-Chloro-3-methylphenol 3.759 96.8 19.3 1310.564 03.64
4-Nitrophenol 3.759 95.3 27.6 1230.395 03.58
Diethyl phthalate 3.759 92.4 51.7 1060.564 03.47
Dimethyl phthalate 3.759 93.2 58.8 1040.395 03.50
Di-n-butyl phthalate 1.885 83.1 54.3 1050.395 01.57
Hexachlorobutadiene 3.759 80.5 35.7 1000.564 03.03
Hexachlorocyclopentadiene 0 0 0 00.395 0ND
Hexachloroethane 3.759 77.1 38.9 89.90.564 02.90
m,p-Cresol 1.885 86.4 37.6 93.70.564 01.63
Nitrobenzene 3.759 75.3 51.8 1040.564 02.83
N-Nitroso-di-n-propylamine 1.885 85.6 45.5 99.10.564 01.61
o-Cresol 1.885 75.8 43 1010.564 01.43
Page 41 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S
21-Apr-10Report Date:
Sample ID: 10040597-001AMS
Batch ID: 59753 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: P4-Borrow #1MS
RunNo: 134531
SeqNo: 2581287
MSSampType:
SW3550B
Pentachlorophenol 3.759 72.5 18.5 1132.26 02.72
Phenol 3.759 77.1 20.8 1100.395 02.90
Pyridine 3.759 61.1 3.61 74.30.564 02.30
Surr: 2,4,6-Tribromophenol 1.885 74.6 32.7 1301.41
Surr: 2-Fluorobiphenyl 0.9425 58.4 34.1 1160.551
Surr: 2-Fluorophenol 1.885 70.1 30.5 991.32
Surr: Nitrobenzene-d5 0.9425 67.5 34.1 1010.636
Surr: Phenol-d5 1.885 75.7 34.9 1101.43
Surr: p-Terphenyl-d14 0.9425 74.5 41.7 1240.702
Sample ID: 10040597-001AMSD
Batch ID: 59753 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: P4-Borrow #1MSD
RunNo: 134531
SeqNo: 2581288
MSDSampType:
SW3550B
1,2,4-Trichlorobenzene 1.870 79.6 35.9 102 400.560 0 1.401 6.011.49
1,4-Dichlorobenzene 1.870 66.8 29.8 95.5 400.560 0 1.184 5.291.25
2,4,5-Trichlorophenol 3.729 93.9 38.6 123 400.392 0 3.415 2.513.50
2,4,6-Trichlorophenol 3.729 103.2 35.9 123 400.392 0 3.902 1.433.85
2,4-Dimethylphenol 3.729 104.2 38.3 88 40 S0.560 0 3.653 6.133.88
2,4-Dinitrophenol 3.729 58.1 1.88 162 401.12 0 2.032 6.392.17
2,4-Dinitrotoluene 1.870 74.6 37.5 107 400.392 0 1.382 1.011.40
2-Chlorophenol 3.729 83.6 22.6 108 400.560 0 3.043 2.433.12
4-Chloro-3-methylphenol 3.729 94.7 19.3 131 400.560 0 3.639 3.033.53
4-Nitrophenol 3.729 98.4 27.6 123 400.392 0 3.583 2.383.67
Diethyl phthalate 3.729 90.1 51.7 106 400.560 0 3.471 3.223.36
Dimethyl phthalate 3.729 91.2 58.8 104 400.392 0 3.504 2.953.40
Di-n-butyl phthalate 1.870 95.7 54.3 105 400.392 0 1.567 13.31.79
Hexachlorobutadiene 3.729 84.3 35.7 100 400.560 0 3.025 3.803.14
Hexachlorocyclopentadiene 0 0 0 0 00.392 0 0 0ND
Hexachloroethane 3.729 79.2 38.9 89.9 400.560 0 2.898 1.902.95
m,p-Cresol 1.870 89.8 37.6 93.7 400.560 0 1.628 3.051.68
Page 42 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S
21-Apr-10Report Date:
Sample ID: 10040597-001AMSD
Batch ID: 59753 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: P4-Borrow #1MSD
RunNo: 134531
SeqNo: 2581288
MSDSampType:
SW3550B
Nitrobenzene 3.729 80.9 51.8 104 400.560 0 2.829 6.483.02
N-Nitroso-di-n-propylamine 1.870 86.4 45.5 99.1 400.560 0 1.615 0.05301.62
o-Cresol 1.870 75.6 43 101 400.560 0 1.430 1.141.41
Pentachlorophenol 3.729 77.6 18.5 113 402.24 0 2.725 6.082.90
Phenol 3.729 76.9 20.8 110 400.392 0 2.900 1.132.87
Pyridine 3.729 57.3 3.61 74.3 400.560 0 2.298 7.352.14
Surr: 2,4,6-Tribromophenol 1.870 67.5 32.7 130 4001.26
Surr: 2-Fluorobiphenyl 0.9350 59.8 34.1 116 4000.560
Surr: 2-Fluorophenol 1.870 65.3 30.5 99 4001.22
Surr: Nitrobenzene-d5 0.9350 66.1 34.1 101 4000.618
Surr: Phenol-d5 1.870 71.1 34.9 110 4001.33
Surr: p-Terphenyl-d14 0.9350 67.9 41.7 124 4000.635
Page 43 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S_SIMS
21-Apr-10Report Date:
Sample ID: MB-59754
Batch ID: 59754 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134462
SeqNo: 2580336
MBLKSampType:
SW3550B
2-Methylnaphthalene 0.003ND
Acenaphthene 0.003ND
Acenaphthylene 0.003ND
Anthracene 0.003ND
Benzo(a)anthracene 0.003ND
Benzo(a)pyrene 0.003ND
Benzo(b)fluoranthene 0.003ND
Benzo(g,h,i)perylene 0.003ND
Benzo(k)fluoranthene 0.003ND
Bis(2-ethylhexyl)phthalate 0.067ND
Chrysene 0.003ND
Dibenzo(a,h)anthracene 0.003ND
Diethyl phthalate 0.034ND
Dimethyl phthalate J0.0340.014
Di-n-butyl phthalate 0.034ND
Fluoranthene 0.003ND
Fluorene 0.003ND
Indeno(1,2,3-cd)pyrene 0.003ND
m,p-Cresol 0.010ND
Naphthalene 0.003ND
o-Cresol 0.003ND
Phenanthrene 0.003ND
Pyrene 0.003ND
Surr: 2-Fluorobiphenyl 0.8330 51.0 17.5 1230.425
Surr: 2-Fluorophenol 1.670 53.3 23 1170.890
Surr: Nitrobenzene-d5 0.8330 54.2 35 1050.451
Surr: Phenol-d5 1.670 60.6 33.2 1251.01
Surr: p-Terphenyl-d14 0.8330 62.8 53.6 1220.523
Page 44 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S_SIMS
21-Apr-10Report Date:
Sample ID: LCS-59754
Batch ID: 59754 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134462
SeqNo: 2580337
LCSSampType:
SW3550B
2-Methylnaphthalene 0.1670 69.1 50 1500.003 00.115
Acenaphthene 0.1670 74.3 56.3 1150.003 00.124
Acenaphthylene 0.1670 69.3 60.3 1430.003 00.116
Anthracene 0.1670 73.7 52.1 1090.003 00.123
Benzo(a)anthracene 0.1670 65.4 52.8 1120.003 00.109
Benzo(a)pyrene 0.1670 74.6 40.8 1270.003 00.125
Benzo(b)fluoranthene 0.1670 81.7 50.1 1500.003 00.136
Benzo(g,h,i)perylene 0.1670 76.7 52.8 1450.003 00.128
Benzo(k)fluoranthene 0.1670 81.8 52 1530.003 00.137
Bis(2-ethylhexyl)phthalate 0.1670 92.0 50 1500.067 00.154
Chrysene 0.1670 77.4 60.8 1280.003 00.129
Dibenzo(a,h)anthracene 0.1670 77.8 54.9 1500.003 00.130
Diethyl phthalate 0.1670 79.2 50 1500.034 00.132
Dimethyl phthalate 0.1670 95.0 50 1500.034 00.159
Di-n-butyl phthalate 0.1670 89.7 50 1500.034 00.150
Fluoranthene 0.1670 80.4 58.7 1250.003 00.134
Fluorene 0.1670 73.6 57.8 1250.003 00.123
Indeno(1,2,3-cd)pyrene 0.1670 78.3 52 1470.003 00.131
m,p-Cresol 0.1670 75.6 50 1500.010 00.126
Naphthalene 0.1670 64.8 54.8 1130.003 00.108
o-Cresol 0.1670 74.6 50 1500.003 00.125
Phenanthrene 0.1670 72.5 60.4 1210.003 00.121
Pyrene 0.1670 80.9 57.9 1290.003 00.135
Surr: 2-Fluorobiphenyl 0.8330 71.0 35.3 1130.591
Surr: 2-Fluorophenol 1.670 72.8 13.6 1231.22
Surr: Nitrobenzene-d5 0.8330 69.5 33.9 1080.579
Surr: Phenol-d5 1.670 84.7 33.7 1291.41
Surr: p-Terphenyl-d14 0.8330 83.5 58.4 1220.695
Page 45 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S_SIMS
21-Apr-10Report Date:
Sample ID: 10040597-001AMS
Batch ID: 59754 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: P4-Borrow #1MS
RunNo: 134536
SeqNo: 2581316
MSSampType:
SW3550B
Acenaphthene 0.1896 74.5 36 1350.004 00.141
Acenaphthylene 0.1896 70.2 17.2 1670.004 00.133
Anthracene 0.1896 74.7 39.3 1240.004 0.0049080.147
Benzo(a)anthracene 0.1896 61.4 10 1830.004 0.015280.132
Benzo(a)pyrene 0.1896 74.9 10 2040.004 0.013160.155
Benzo(b)fluoranthene 0.1896 74.4 10.6 1780.004 0.019520.161
Benzo(g,h,i)perylene 0.1896 73.1 10 1680.004 0.010110.149
Benzo(k)fluoranthene 0.1896 76.6 27.6 1810.004 0.0070640.152
Bis(2-ethylhexyl)phthalate 0.1896 93.3 50 1500.076 00.177
Chrysene 0.1896 70.9 10 1760.004 0.017990.152
Dibenzo(a,h)anthracene 0.1896 76.4 12.2 1560.004 00.145
Fluoranthene 0.1896 60.9 10 2270.004 0.046100.162
Fluorene 0.1896 71.8 35.2 1480.004 00.136
Indeno(1,2,3-cd)pyrene 0.1896 75.2 10 1640.004 0.0076960.150
Naphthalene 0.1896 64.8 14.7 1280.004 00.123
Phenanthrene 0.1896 61.0 32.8 1430.004 0.029560.145
Pyrene 0.1896 68.0 10 1800.004 0.036170.165
Surr: 2-Fluorobiphenyl 0.9459 66.8 10 1310.632
Surr: Nitrobenzene-d5 0.9459 69.4 10 1320.657
Surr: p-Terphenyl-d14 0.9459 78.1 30.6 1310.739
Sample ID: 10040597-001AMSD
Batch ID: 59754 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: P4-Borrow #1MSD
RunNo: 134536
SeqNo: 2581317
MSDSampType:
SW3550B
Acenaphthene 0.1860 78.5 36 135 49.70.004 0 0.1413 3.340.146
Acenaphthylene 0.1860 74.4 17.2 167 33.30.004 0 0.1331 3.980.138
Anthracene 0.1860 78.0 39.3 124 51.10.004 0.004908 0.1466 2.270.150
Benzo(a)anthracene 0.1860 62.9 10 183 40.60.004 0.01528 0.1317 0.4560.132
Benzo(a)pyrene 0.1860 77.5 10 204 56.40.004 0.01316 0.1552 1.310.157
Benzo(b)fluoranthene 0.1860 77.7 10.6 178 49.70.004 0.01952 0.1606 2.180.164
Page 46 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: SV_8270S_S_SIMS
21-Apr-10Report Date:
Sample ID: 10040597-001AMSD
Batch ID: 59754 Analysis Date: 4/16/2010
Prep Date: 4/15/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: mg/Kg-dry
PQL
Client ID: P4-Borrow #1MSD
RunNo: 134536
SeqNo: 2581317
MSDSampType:
SW3550B
Benzo(g,h,i)perylene 0.1860 67.2 10 168 36.50.004 0.01011 0.1488 9.590.135
Benzo(k)fluoranthene 0.1860 80.6 27.6 181 42.60.004 0.007064 0.1523 2.970.157
Bis(2-ethylhexyl)phthalate 0.1860 96.7 50 150 60.30.075 0 0.1769 1.660.180
Chrysene 0.1860 71.6 10 176 45.10.004 0.01799 0.1524 0.8690.151
Dibenzo(a,h)anthracene 0.1860 74.8 12.2 156 39.90.004 0 0.1448 4.020.139
Fluoranthene 0.1860 66.1 10 227 66.20.004 0.04610 0.1616 4.530.169
Fluorene 0.1860 77.2 35.2 148 65.60.004 0 0.1362 5.310.144
Indeno(1,2,3-cd)pyrene 0.1860 72.3 10 164 36.50.004 0.007696 0.1504 5.650.142
Naphthalene 0.1860 69.0 14.7 128 39.60.004 0 0.1228 4.400.128
Phenanthrene 0.1860 66.9 32.8 143 35.40.004 0.02956 0.1452 5.840.154
Pyrene 0.1860 75.1 10 180 60.10.004 0.03617 0.1650 6.380.176
Surr: 2-Fluorobiphenyl 0.9279 66.9 10 131 4000.621
Surr: Nitrobenzene-d5 0.9279 69.9 10 132 4000.648
Surr: p-Terphenyl-d14 0.9279 85.4 30.6 131 4000.792
Page 47 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: V_8260S_S
21-Apr-10Report Date:
Sample ID: LCS-G100416-1
Batch ID: 59830 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134558
SeqNo: 2582007
LCSSampType:
SW5035
1,1,1-Trichloroethane 50.00 100 85.6 1245.0 050.0
1,1-Dichloroethene 50.00 80.6 60.1 1315.0 040.3
1,2-Dibromoethane 50.00 95.3 86.9 1195.0 047.7
1,2-Dichlorobenzene 50.00 97.0 88 1195.0 048.5
1,2-Dichloroethane 50.00 89.2 73 1175.0 044.6
1,3-Dichlorobenzene 50.00 99.4 85.8 1255.0 049.7
1,4-Dichlorobenzene 50.00 99.7 84.5 1245.0 049.8
2-Butanone 100.0 55.9 45.3 13650.0 055.9
Benzene 50.00 88.0 73.9 1091.0 044.0
Bromodichloromethane 50.00 101.6 91.3 1265.0 050.8
Carbon tetrachloride 50.00 100.1 83.3 1275.0 050.0
Chlorobenzene 50.00 97.8 85.8 1165.0 048.9
Chloroform 50.00 94.6 80 1135.0 047.3
Dibromochloromethane 50.00 90.7 89.1 1195.0 045.4
Ethylbenzene 50.00 97.0 84.1 1155.0 048.5
m,p-Xylenes 50.00 94.9 79.1 1115.0 047.5
Methyl tert-butyl ether 50.00 97.7 80 1282.0 048.8
Methylene chloride 50.00 88.1 73.9 1165.0 044.0
Naphthalene 50.00 80.2 73.1 13510 040.1
o-Xylene 50.00 93.7 82 1175.0 046.8
Tetrachloroethene 50.00 88.9 74.6 1155.0 044.5
Toluene 50.00 88.8 79.1 1125.0 044.4
Trichloroethene 50.00 92.5 81 1115.0 046.2
Surr: 1,2-Dichloroethane-d4 50.00 95.3 72.2 13147.6
Surr: 4-Bromofluorobenzene 50.00 102.1 82.1 11651.1
Surr: Dibromofluoromethane 50.00 100.8 77.7 12050.4
Surr: Toluene-d8 50.00 99.1 86 11649.6
Page 48 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: V_8260S_S
21-Apr-10Report Date:
Sample ID: LCSD-G100416-1
Batch ID: 59830 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134558
SeqNo: 2582008
LCSDSampType:
SW5035
1,1,1-Trichloroethane 50.00 100.4 85.6 124 205.0 0 50.01 0.39950.2
1,1-Dichloroethene 50.00 80.2 60.1 131 205.0 0 40.32 0.57240.1
1,2-Dibromoethane 50.00 100.6 86.9 119 205.0 0 47.66 5.3550.3
1,2-Dichlorobenzene 50.00 98.3 88 119 205.0 0 48.51 1.3549.2
1,2-Dichloroethane 50.00 91.1 73 117 205.0 0 44.58 2.1145.5
1,3-Dichlorobenzene 50.00 99.1 85.8 125 205.0 0 49.70 0.34349.5
1,4-Dichlorobenzene 50.00 99.5 84.5 124 205.0 0 49.83 0.12049.8
2-Butanone 100.0 61.5 45.3 136 2050.0 0 55.88 9.5661.5
Benzene 50.00 88.4 73.9 109 201.0 0 44.01 0.40844.2
Bromodichloromethane 50.00 103.4 91.3 126 205.0 0 50.82 1.6851.7
Carbon tetrachloride 50.00 99.2 83.3 127 205.0 0 50.05 0.86349.6
Chlorobenzene 50.00 97.8 85.8 116 205.0 0 48.91 048.9
Chloroform 50.00 95.0 80 113 205.0 0 47.30 0.44347.5
Dibromochloromethane 50.00 92.7 89.1 119 205.0 0 45.37 2.1846.4
Ethylbenzene 50.00 96.4 84.1 115 205.0 0 48.51 0.60048.2
m,p-Xylenes 50.00 93.5 79.1 111 205.0 0 47.46 1.5346.7
Methyl tert-butyl ether 50.00 102.6 80 128 202.0 0 48.84 4.8951.3
Methylene chloride 50.00 89.2 73.9 116 205.0 0 44.04 1.2644.6
Naphthalene 50.00 86.7 73.1 135 2010 0 40.10 7.8143.4
o-Xylene 50.00 93.0 82 117 205.0 0 46.85 0.75046.5
Tetrachloroethene 50.00 89.1 74.6 115 205.0 0 44.47 0.20244.6
Toluene 50.00 88.4 79.1 112 205.0 0 44.41 0.45144.2
Trichloroethene 50.00 92.5 81 111 205.0 0 46.24 046.2
Surr: 1,2-Dichloroethane-d4 50.00 96.8 72.2 131 0048.4
Surr: 4-Bromofluorobenzene 50.00 102.5 82.1 116 0051.3
Surr: Dibromofluoromethane 50.00 101.0 77.7 120 0050.5
Surr: Toluene-d8 50.00 98.9 86 116 0049.4
Page 49 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: V_8260S_S
21-Apr-10Report Date:
Sample ID: MBLK-G100416-1
Batch ID: 59830 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134558
SeqNo: 2582009
MBLKSampType:
SW5035
1,1,1,2-Tetrachloroethane 5.0ND
1,1,1-Trichloroethane 5.0ND
1,1,2,2-Tetrachloroethane 5.0ND
1,1,2-Trichloro-1,2,2-trifluoroethane 5.0ND
1,1,2-Trichloroethane 5.0ND
1,1-Dichloro-2-propanone 50.0ND
1,1-Dichloroethane 5.0ND
1,1-Dichloroethene 5.0ND
1,1-Dichloropropene 5.0ND
1,2,3-Trichlorobenzene 5.0ND
1,2,3-Trichloropropane 10ND
1,2,3-Trimethylbenzene 5.0ND
1,2,4-Trichlorobenzene 5.0ND
1,2,4-Trimethylbenzene 5.0ND
1,2-Dibromo-3-chloropropane 5.0ND
1,2-Dibromoethane 5.0ND
1,2-Dichlorobenzene 5.0ND
1,2-Dichloroethane 5.0ND
1,2-Dichloropropane 5.0ND
1,3,5-Trimethylbenzene 5.0ND
1,3-Dichlorobenzene 5.0ND
1,3-Dichloropropane 5.0ND
1,4-Dichlorobenzene 5.0ND
1-Chlorobutane 5.0ND
2,2-Dichloropropane 5.0ND
2-Butanone 50.0ND
2-Chlorotoluene 5.0ND
2-Hexanone 50.0ND
2-Nitropropane 50.0ND
4-Chlorotoluene 5.0ND
4-Methyl-2-pentanone 50.0ND
Page 50 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: V_8260S_S
21-Apr-10Report Date:
Sample ID: MBLK-G100416-1
Batch ID: 59830 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134558
SeqNo: 2582009
MBLKSampType:
SW5035
Acetone 50.0ND
Acrolein 100ND
Acrylonitrile 10ND
Allyl chloride 5.0ND
Benzene 1.0ND
Bromobenzene 5.0ND
Bromochloromethane 5.0ND
Bromodichloromethane 5.0ND
Bromoform 5.0ND
Bromomethane 10ND
Carbon disulfide 5.0ND
Carbon tetrachloride 5.0ND
Chlorobenzene 5.0ND
Chloroethane 10ND
Chloroform 5.0ND
Chloromethane 10ND
cis-1,2-Dichloroethene 5.0ND
cis-1,3-Dichloropropene 4.0ND
Cyclohexanone 100ND
Dibromochloromethane 5.0ND
Dibromomethane 5.0ND
Dichlorodifluoromethane 10ND
Ethyl acetate 50.0ND
Ethyl ether 5.0ND
Ethyl methacrylate 5.0ND
Ethylbenzene 5.0ND
Heptane 20.0ND
Hexachlorobutadiene 5.0ND
Hexachloroethane 5.0ND
Iodomethane 10ND
Isopropylbenzene 5.0ND
Page 51 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120
Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
ANALYTICAL QC SUMMARY REPORTTestCode: V_8260S_S
21-Apr-10Report Date:
Sample ID: MBLK-G100416-1
Batch ID: 59830 Analysis Date: 4/16/2010
Prep Date: 4/16/2010
Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual
Units: µg/Kg
PQL
Client ID: ZZZZZZ
RunNo: 134558
SeqNo: 2582009
MBLKSampType:
SW5035
m,p-Xylenes 5.0ND
Methacrylonitrile 50.0ND
Methyl Methacrylate 5.0ND
Methyl tert-butyl ether 2.0ND
Methylacrylate 10ND
Methylene chloride 5.0ND
Naphthalene 10ND
n-Butylbenzene 5.0ND
n-Hexane 20.0ND
Nitrobenzene 100ND
n-Propylbenzene 5.0ND
o-Xylene 5.0ND
Pentachloroethane 5.0ND
p-Isopropyltoluene 5.0ND
Propionitrile 50.0ND
sec-Butylbenzene 5.0ND
Styrene 5.0ND
tert-Butylbenzene 5.0ND
Tetrachloroethene 5.0ND
Tetrahydrofuran 50.0ND
Toluene 5.0ND
trans-1,2-Dichloroethene 5.0ND
trans-1,3-Dichloropropene 4.0ND
Trichloroethene 5.0ND
Trichlorofluoromethane 5.0ND
Vinyl acetate 50.0ND
Vinyl chloride 2.0ND
Surr: 1,2-Dichloroethane-d4 50.00 96.2 72.2 13148.1
Surr: 4-Bromofluorobenzene 50.00 101.6 82.1 11650.8
Surr: Dibromofluoromethane 50.00 97.9 77.7 12048.9
Surr: Toluene-d8 50.00 98.4 86 11649.2
Page 52 of 53
IL ELAP and NELAP Accredited - Accreditation #100226
Project: A831-735002-012901-225/Ameren Champaign 6249080120Client: PSC Industrial Outsourcing, LP
Lab Order: 10040597
RECEIVING CHECK LIST
Report Date: 21-Apr-10
TEKLAB, INC.ENVIRONMENTAL TESTING LABORATORY
5445 HORSESHOE LAKE ROAD
COLLINSVILLE, ILLINOIS 62234
TEL: 618-344-1004
FAX: 618-344-1005
Received By: MLDCarrier: Susan Duffe
Completed by: Reviewed by:
On:
15-Apr-10
On:
15-Apr-10
Shipping container/cooler in good condition? Yes No Not Present
Chain of custody present? Yes No
Chain of custody signed when relinquished and received? Yes No
Chain of custody agrees with sample labels? Yes No
Samples in proper container/bottle? Yes No
Sample containers intact? Yes No
Sufficient sample volume for indicated test? Yes No
All samples received within holding time? Yes No
Container/Temp Blank temperature in compliance? Yes No
Temp °C 1.4
When thermal preservation is required, samples are compliant with a temperature between 0.1°C - 6.0°C, or when samples are received on ice the same day as collected.
Any No responses must be detailed below or on the COC.
Water - VOA vials have zero headspace? Yes No No VOA vials
Water - pH acceptable upon receipt? Yes No
Type of thermal preservation? None Ice Blue Ice Dry Ice
Chain of custody 1 Extra pages included 0
Reported field parameters measured: Field Lab NA
Pages to follow:
Water - TOX containers have zero headspace? Yes No No TOX containers
Marvin L. Darling Heather A. White
IL ELAP and NELAP Accredited - Accreditation #100226 Page 53 of 53
http://www.teklabinc.com/
July 14, 2011
WorkOrder: 11070042A831-735002-012901-225Ameren Champaign 62409080120
RE:
Dear Pete Sazama:
TEKLAB, INC received 5 samples on 7/1/2011 3:50:00 PM for the analysis presented in the following report.
Samples are analyzed on an as received basis unless otherwise requested and documented. The sample results contained in this report relate only to the requested analytes of interest as directed on the chain of custody. NELAP accredited fields of testing are indicated by the letters NELAP under the Certification column.
All tests are performed in the Collinsville, IL laboratory unless otherwise noted in the Case Narrative.
All quality control criteria applicable to the test methods employed for this project have been satisfactorily met and are in accordance with NELAP except where noted. The following report shall not be reproduced, except in full, without the written approval of Teklab, Inc.
If you have any questions regarding these tests results, please feel free to call.
Sincerely,
210 West Sand Bank RoadColumbia, IL 62236-0230
(618) 281-7173(618) 281-5120
TEL:FAX:
Pete SazamaPSC Industrial Outsourcing, LP
Heather A. WhiteProject Manager(618)344-1004 ex [email protected]
Page 1 of 58
This reporting package includes the following:
Report Contents
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Cover Letter 1
Report Contents 2
Definitions 3
Case Narrative 4
Laboratory Results 5
Sample Summary 35
Dates Report 36
Quality Control Results 39
Receiving Check List 58
Chain of Custody Appended
Page 2 of 58
____TeklabHdrP
Definitions
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Abbr DefinitionCCV Continuing calibration verification is a check of a standard to determine the state of calibration of an instrument between recalibration.
DF Dilution factor is the dilution performed during analysis only and does not take into account any dilutions made during sample preparation. The reported result is final and includes all dilutions factors.
DNI Did not ignite
DUP Laboratory duplicate is an aliquot of a sample taken from the same container under laboratory conditions for independent processing and analysis independently of the original aliquot.
ICV Initial calibration verification is a check of a standard to determine the state of calibration of an instrument before sample analysis is initiated.
IDPH IL Dept. of Public Health
LCS Laboratory control sample, spiked with verified known amounts of analytes, is analyzed exactly like a sample to establish intra-laboratory or analyst specific precision and bias or to assess the performance of all or a portion of the measurement system. The acceptable recovery range is in the QC Package (provided upon request).
LCSD Laboratory control sample duplicate is a replicate laboratory control sample that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in the QC Package (provided upon request).
MB Method blank is a sample of a matrix similar to the batch of associated sample (when available) that is free from the analytes of interest and is processed simultaneously with and under the same conditions as samples through all steps of the analytical procedures, and in which no target analytes or interferences should present at concentrations that impact the analytical results for sample analyses.
MDL Method detection limit means the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type containing the analyte.
MS Matrix spike is an aliquot of matrix fortified (spiked) with known quantities of specific analytes that is subjected to the entire analytical procedures in order to determine the effect of the matrix on an approved test method’s recovery system. The acceptable recovery range is listed in the QC Package (provided upon request).
MSD Matrix spike duplicate means a replicate matrix spike that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in the QC Package (provided upon request).
MW Molecular weight
ND Not Detected at the Reporting Limit
NELAP NELAP Accredited
PQL Practical quantitation limit means the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine laboratory operation conditions. The acceptable recovery range is listed in the QC Package (provided upon request).
RL The reporting limit the lowest level that the data is displayed in the final report. The reporting limit may vary according to customer request or sample dilution. The reporting limit may not be less than the MDL.
RPD Relative percent difference is a calculated difference between two recoveries (ie. MS/MSD). The acceptable recovery limit is listed in the QC Package (provided upon request).
SPK The spike is a known mass of target analyte added to a blank sample or sub-sample; used to determine recovery deficiency or for other quality control purposes.
Surr Surrogates are compounds which are similar to the analytes of interest in chemical composition and behavior in the analytical process, but which are not normally found in environmental samples.
TNTC Too numerous to count ( > 200 CFU )
Qualifiers# - Unknown hydrocarbon B - Analyte detected in associated Method Blank
E - Value above quantitation range H - Holding times exceeded
M - Manual Integration used to determine area response ND - Not Detected at the Reporting Limit
R - RPD outside accepted recovery limits S - Spike Recovery outside recovery limits
X - Value exceeds Maximum Contaminant Level
Page 3 of 58
Case Narrative
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Cooler Receipt Temp: 5.4 °C
Herbicide analysis performed by Keystone Laboratories, Inc. See attached report for QC data.
NELAPState Cert # Exp Date LabDept
Locations and Accreditations
____________________________________Collinsville
Address 5445 Horseshoe Lake Road
Collinsville, IL 62234-7425
Phone (618) 344-1004
Fax (618) 344-1005
Email [email protected]
____________________________________Springfield
Address 3920 Pintail Dr
Springfield, IL 62711-9415
Phone (217) 698-1004
Fax (217) 698-1005
Email [email protected]
____________________________________Kansas City
Address 8421 Nieman Road
Lenexa, KS 66214
Phone (913) 541-1998
Fax (913) 541-1998
Email [email protected]
Illinois 100226 1/31/2012 CollinsvilleNELAPIEPA
Kansas E-10374 1/31/2012 CollinsvilleNELAPKDHE
Louisiana 166493 6/30/2012 CollinsvilleNELAPLDEQ
Louisiana 166578 6/30/2012 SpringfieldNELAPLDEQ
Arkansas 88-0966 3/14/2012 CollinsvilleADEQ
Illinois 17584 4/30/2012 CollinsvilleIDPH
Kentucky 0073 5/26/2012 CollinsvilleUST
Missouri 00930 4/13/2013 CollinsvilleMDNR
Oklahoma 9978 8/31/2011 CollinsvilleODEQ
Page 4 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/29/2011 16:00
Lab ID: 11070042-001 Client Sample ID: SBA-C3-01 (5-6)
Matrix: SOLID
Batch
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 07/01/2011 16:000.1 % 120.6 R151546
STANDARD METHODS 18TH ED. 2540 GTotal Solids 07/01/2011 16:000.1 % 179.4 R151526
SW-846 9012A (TOTAL)Cyanide 07/02/2011 12:170.63 mg/Kg-dry 1< 0.63NELAP R151533
SW-846 3050B, 6010B, METALS BY ICPArsenic 07/05/2011 12:252.50 mg/Kg-dry 111.3NELAP 69348
Barium 07/05/2011 12:250.50 mg/Kg-dry 1130NELAP 69348
Cadmium 07/05/2011 12:250.20 mg/Kg-dry 10.24NELAP 69348
Chromium 07/05/2011 12:251.00 mg/Kg-dry 123.2NELAP 69348
Lead 07/05/2011 12:254.00 mg/Kg-dry 120.4NELAP 69348
Silver 07/05/2011 12:250.55 mg/Kg-dry 1< 0.55NELAP 69348
SW-846 3050B, METALS BY GFAASelenium 7740 07/05/2011 11:550.577 mg/Kg-dry 1< 0.577NELAP 69349
SW-846 7471AMercury 07/05/2011 12:220.012 mg/Kg-dry 10.024NELAP 69355
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel 07/04/2011 12:426.28 mg/Kg-dry 1NDNELAP 69330
Kerosene 07/04/2011 12:426.28 mg/Kg-dry 1NDNELAP 69330
Mineral Spirits 07/04/2011 12:426.28 mg/Kg-dry 1NDNELAP 69330
Motor Oil 07/04/2011 12:426.28 mg/Kg-dry 1NDNELAP 69330
Surr: n-Tetracontane 07/04/2011 12:4250.6-140 %REC 178.3 69330
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
4,4´-DDE 07/05/2011 23:062.10 µg/Kg-dry 16.64NELAP 69344
4,4´-DDT J 07/05/2011 23:062.10 µg/Kg-dry 11.4NELAP 69344
Alachlor 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
Aldrin 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
alpha-BHC 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
alpha-Chlordane 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
beta-BHC 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
Chlordane 07/05/2011 23:064.20 µg/Kg-dry 1NDNELAP 69344
delta-BHC 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
Dieldrin 07/05/2011 23:062.10 µg/Kg-dry 14.12NELAP 69344
Endosulfan I 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
Endosulfan II 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
Endosulfan sulfate 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
Endrin 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
Endrin aldehyde 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
Endrin ketone 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
gamma-BHC 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
gamma-Chlordane 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
Heptachlor 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
Heptachlor epoxide 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
Methoxychlor 07/05/2011 23:062.10 µg/Kg-dry 1NDNELAP 69344
Toxaphene 07/05/2011 23:0637.8 µg/Kg-dry 1NDNELAP 69344
Page 5 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/29/2011 16:00
Lab ID: 11070042-001 Client Sample ID: SBA-C3-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD Surr: Decachlorobiphenyl 07/05/2011 23:0648-149 %REC 198.4 69344
Surr: Tetrachloro-m-xylene 07/05/2011 23:0619-145 %REC 175.4 69344
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/05/2011 10:2547.2 µg/Kg-dry 1NDNELAP 69344
Aroclor 1221 07/05/2011 10:2547.2 µg/Kg-dry 1NDNELAP 69344
Aroclor 1232 07/05/2011 10:2547.2 µg/Kg-dry 1NDNELAP 69344
Aroclor 1242 07/05/2011 10:2547.2 µg/Kg-dry 1NDNELAP 69344
Aroclor 1248 07/05/2011 10:2547.2 µg/Kg-dry 1NDNELAP 69344
Aroclor 1254 07/05/2011 10:2547.2 µg/Kg-dry 1NDNELAP 69344
Aroclor 1260 07/05/2011 10:2547.2 µg/Kg-dry 1NDNELAP 69344
Surr: Decachlorobiphenyl 07/05/2011 10:255-156 %REC 199.3 69344
Surr: Tetrachloro-meta-xylene 07/05/2011 10:257.35-123 %REC 174.2 69344
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/05/2011 9:280.004 mg/Kg-dry 1NDNELAP 69347
Acenaphthylene 07/05/2011 9:280.004 mg/Kg-dry 1NDNELAP 69347
Anthracene 07/05/2011 9:280.004 mg/Kg-dry 10.005NELAP 69347
Benzo(a)anthracene 07/05/2011 9:280.004 mg/Kg-dry 10.022NELAP 69347
Benzo(a)pyrene 07/05/2011 9:280.004 mg/Kg-dry 10.025NELAP 69347
Benzo(b)fluoranthene 07/05/2011 9:280.004 mg/Kg-dry 10.033NELAP 69347
Benzo(g,h,i)perylene 07/05/2011 9:280.004 mg/Kg-dry 10.019NELAP 69347
Benzo(k)fluoranthene 07/05/2011 9:280.004 mg/Kg-dry 10.012NELAP 69347
Bis(2-ethylhexyl)phthalate J 07/05/2011 9:280.084 mg/Kg-dry 10.043NELAP 69347
Chrysene 07/05/2011 9:280.004 mg/Kg-dry 10.026NELAP 69347
Dibenzo(a,h)anthracene 07/05/2011 9:280.004 mg/Kg-dry 10.005NELAP 69347
Fluoranthene 07/05/2011 9:280.004 mg/Kg-dry 10.054NELAP 69347
Fluorene 07/05/2011 9:280.004 mg/Kg-dry 1NDNELAP 69347
Indeno(1,2,3-cd)pyrene 07/05/2011 9:280.004 mg/Kg-dry 10.015NELAP 69347
Naphthalene 07/05/2011 9:280.004 mg/Kg-dry 1NDNELAP 69347
Phenanthrene 07/05/2011 9:280.004 mg/Kg-dry 10.029NELAP 69347
Pyrene 07/05/2011 9:280.004 mg/Kg-dry 10.048NELAP 69347
Surr: 2-Fluorobiphenyl 07/05/2011 9:2810-131 %REC 188.4 69347
Surr: Nitrobenzene-d5 07/05/2011 9:2810-132 %REC 176.9 69347
Surr: p-Terphenyl-d14 07/05/2011 9:2880.2-138 %REC 1122.5 69347
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
1,2-Dichlorobenzene 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
1,3-Dichlorobenzene 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
1,4-Dichlorobenzene 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
2,4,5-Trichlorophenol 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
2,4,6-Trichlorophenol 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
2,4-Dichlorophenol 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
2,4-Dimethylphenol 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
2,4-Dinitrophenol 07/05/2011 15:101.26 mg/Kg-dry 1NDNELAP 69346
2,4-Dinitrotoluene 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
2,6-Dinitrotoluene 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
2-Chloronaphthalene 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
2-Chlorophenol 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
Page 6 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/29/2011 16:00
Lab ID: 11070042-001 Client Sample ID: SBA-C3-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS2-Methoxy-4-methylphenol 07/05/2011 15:100.818 mg/Kg-dry 1ND 69346
2-Methylnaphthalene 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
2-Nitroaniline 07/05/2011 15:101.26 mg/Kg-dry 1NDNELAP 69346
2-Nitrophenol 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
3,3´-Dichlorobenzidine 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
3-Nitroaniline 07/05/2011 15:101.26 mg/Kg-dry 1NDNELAP 69346
4,6-Dinitro-2-methylphenol 07/05/2011 15:101.26 mg/Kg-dry 1NDNELAP 69346
4-Bromophenyl phenyl ether 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
4-Chloro-3-methylphenol 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
4-Chloroaniline 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
4-Chlorophenyl phenyl ether 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
4-Nitroaniline 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
4-Nitrophenol 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
Aniline 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
Azobenzene 07/05/2011 15:100.441 mg/Kg-dry 1ND 69346
Benzidine 07/05/2011 15:101.33 mg/Kg-dry 1See noteNELAP 69346
Benzoic acid 07/05/2011 15:101.89 mg/Kg-dry 1NDNELAP 69346
Benzyl alcohol 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
Bis(2-chloroethoxy)methane 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
Bis(2-chloroethyl)ether 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
Bis(2-chloroisopropyl)ether 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
Butyl benzyl phthalate 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
Carbazole 07/05/2011 15:100.629 mg/Kg-dry 1ND 69346
Dibenzofuran 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
Diethyl phthalate 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
Dimethyl phthalate 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
Di-n-butyl phthalate 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
Di-n-octyl phthalate 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
Hexachlorobenzene 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
Hexachlorobutadiene 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
Hexachlorocyclopentadiene 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
Hexachloroethane 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
Isophorone 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
m,p-Cresol 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
Nitrobenzene 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
N-Nitrosodimethylamine 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
N-Nitroso-di-n-propylamine 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
N-Nitrosodiphenylamine 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
o-Cresol 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
Pentachlorophenol 07/05/2011 15:102.52 mg/Kg-dry 1NDNELAP 69346
Phenol 07/05/2011 15:100.441 mg/Kg-dry 1NDNELAP 69346
Pyridine 07/05/2011 15:100.629 mg/Kg-dry 1NDNELAP 69346
1,2-Diphenylhydrazine 07/05/2011 15:101.06 mg/Kg-dry 1ND 69346
Surr: 2,4,6-Tribromophenol 07/05/2011 15:1032.7-130 %REC 194.9 69346
Surr: 2-Fluorobiphenyl 07/05/2011 15:1034.1-116 %REC 182.1 69346
Surr: 2-Fluorophenol 07/05/2011 15:1030.5-99 %REC 176.5 69346
Surr: Nitrobenzene-d5 07/05/2011 15:1034.1-101 %REC 183.9 69346
Page 7 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/29/2011 16:00
Lab ID: 11070042-001 Client Sample ID: SBA-C3-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: Phenol-d5 07/05/2011 15:1034.9-110 %REC 175.8 69346
Surr: p-Terphenyl-d14 07/05/2011 15:1041.7-124 %REC 199.8 69346
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.LCS was outside upper QC limits. Sample was ND.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,1,1-Trichloroethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,1,2,2-Tetrachloroethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,1,2-Trichloro-1,2,2-trifluoroethane 07/05/2011 11:514.9 µg/Kg-dry 1ND 69368
1,1,2-Trichloroethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,1-Dichloro-2-propanone 07/05/2011 11:5149.1 µg/Kg-dry 1ND 69368
1,1-Dichloroethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,1-Dichloroethene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,1-Dichloropropene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,2,3-Trichlorobenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,2,3-Trichloropropane 07/05/2011 11:519.8 µg/Kg-dry 1NDNELAP 69368
1,2,3-Trimethylbenzene J 07/05/2011 11:514.9 µg/Kg-dry 11.4 69368
1,2,4-Trichlorobenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,2,4-Trimethylbenzene J 07/05/2011 11:514.9 µg/Kg-dry 13.5NELAP 69368
1,2-Dibromo-3-chloropropane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,2-Dibromoethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,2-Dichlorobenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,2-Dichloroethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,2-Dichloropropane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,3,5-Trimethylbenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,3-Dichlorobenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,3-Dichloropropane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1,4-Dichlorobenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
1-Chlorobutane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
2,2-Dichloropropane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
2-Butanone 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368
2-Chlorotoluene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
2-Hexanone 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368
2-Nitropropane 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368
4-Chlorotoluene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
4-Methyl-2-pentanone 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368
Acetone 07/05/2011 11:5149.1 µg/Kg-dry 163.7NELAP 69368
Acrolein 07/05/2011 11:5198.3 µg/Kg-dry 1NDNELAP 69368
Acrylonitrile 07/05/2011 11:519.8 µg/Kg-dry 1NDNELAP 69368
Allyl chloride 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Benzene 07/05/2011 11:511.0 µg/Kg-dry 12.1NELAP 69368
Bromobenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Bromochloromethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Bromodichloromethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Bromoform 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Bromomethane 07/05/2011 11:519.8 µg/Kg-dry 1NDNELAP 69368
Carbon disulfide 07/05/2011 11:514.9 µg/Kg-dry 15.3NELAP 69368
Page 8 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/29/2011 16:00
Lab ID: 11070042-001 Client Sample ID: SBA-C3-01 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSCarbon tetrachloride 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Chlorobenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Chloroethane 07/05/2011 11:519.8 µg/Kg-dry 1NDNELAP 69368
Chloroform 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Chloromethane 07/05/2011 11:519.8 µg/Kg-dry 1NDNELAP 69368
cis-1,2-Dichloroethene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
cis-1,3-Dichloropropene 07/05/2011 11:513.9 µg/Kg-dry 1NDNELAP 69368
Cyclohexanone 07/05/2011 11:5198.3 µg/Kg-dry 1ND 69368
Dibromochloromethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Dibromomethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Dichlorodifluoromethane 07/05/2011 11:519.8 µg/Kg-dry 1NDNELAP 69368
Ethyl acetate 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368
Ethyl ether 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Ethyl methacrylate 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Ethylbenzene J 07/05/2011 11:514.9 µg/Kg-dry 11.8NELAP 69368
Heptane 07/05/2011 11:5119.7 µg/Kg-dry 1ND 69368
Hexachlorobutadiene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Hexachloroethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Iodomethane 07/05/2011 11:519.8 µg/Kg-dry 1NDNELAP 69368
Isopropylbenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
m,p-Xylenes J 07/05/2011 11:514.9 µg/Kg-dry 13.3NELAP 69368
Methacrylonitrile 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368
Methyl Methacrylate 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Methyl tert-butyl ether 07/05/2011 11:512.0 µg/Kg-dry 1NDNELAP 69368
Methylacrylate 07/05/2011 11:519.8 µg/Kg-dry 1ND 69368
Methylene chloride 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Naphthalene J 07/05/2011 11:519.8 µg/Kg-dry 12.5NELAP 69368
n-Butylbenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
n-Hexane J 07/05/2011 11:5119.7 µg/Kg-dry 111 69368
Nitrobenzene 07/05/2011 11:5198.3 µg/Kg-dry 1NDNELAP 69368
n-Propylbenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
o-Xylene J 07/05/2011 11:514.9 µg/Kg-dry 11.3NELAP 69368
Pentachloroethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
p-Isopropyltoluene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Propionitrile 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368
sec-Butylbenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Styrene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
tert-Butylbenzene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Tetrachloroethene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Tetrahydrofuran 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368
Toluene J 07/05/2011 11:514.9 µg/Kg-dry 14.4NELAP 69368
trans-1,2-Dichloroethene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
trans-1,3-Dichloropropene 07/05/2011 11:513.9 µg/Kg-dry 1NDNELAP 69368
Trichloroethene 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Trichlorofluoromethane 07/05/2011 11:514.9 µg/Kg-dry 1NDNELAP 69368
Vinyl acetate 07/05/2011 11:5149.1 µg/Kg-dry 1NDNELAP 69368
Vinyl chloride 07/05/2011 11:512.0 µg/Kg-dry 1NDNELAP 69368
Page 9 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/29/2011 16:00
Lab ID: 11070042-001 Client Sample ID: SBA-C3-01 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: 1,2-Dichloroethane-d4 07/05/2011 11:5172.2-131 %REC 1105.6 69368
Surr: 4-Bromofluorobenzene 07/05/2011 11:5182.1-116 %REC 189.5 69368
Surr: Dibromofluoromethane 07/05/2011 11:5177.7-120 %REC 1102.4 69368
Surr: Toluene-d8 07/05/2011 11:5186-116 %REC 1103.0 69368
Marginal Exceedance for trichloroethene in LCS is verified per Volume 1 Module 4 section 1.7.4.2 of the 2009 TNI standard.
SW-846 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875
2,4,5-TP (Silvex) 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875
2,4-D 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875
2,4-DB 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875
3,5-Dichlorobenzoic Acid 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875
Acifluorfen 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875
Bentazon 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875
Chloramben 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875
Dalapon 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875
DCPA 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875
Dicamba 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875
Dichlorprop 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875
Dinoseb 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875
Pentachlorophenol 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875
Picloram 07/11/2011 16:550.05 mg/Kg-dry 1NDNELAP R151875
Surr: DCAA 07/11/2011 17:4224-140 %REC 171.7 R151875
The blank spike recovery and/or blank spike duplicate recovery were outside the established acceptance limits for 3,5-Dichlorobenzoic Acid and 2,4,5-T. Batch was accepted based on acceptable MS/MSD/RPD results.
Page 10 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 8:00
Lab ID: 11070042-002 Client Sample ID: SBA-B4-01 (5-6)
Matrix: SOLID
Batch
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 07/01/2011 16:000.1 % 117.4 R151546
STANDARD METHODS 18TH ED. 2540 GTotal Solids 07/01/2011 16:000.1 % 182.6 R151526
SW-846 9012A (TOTAL)Cyanide 07/02/2011 12:170.60 mg/Kg-dry 1< 0.60NELAP R151533
SW-846 3050B, 6010B, METALS BY ICPArsenic 07/05/2011 12:422.27 mg/Kg-dry 19.56NELAP 69348
Barium 07/05/2011 12:420.45 mg/Kg-dry 1110NELAP 69348
Cadmium J 07/05/2011 12:420.18 mg/Kg-dry 10.17NELAP 69348
Chromium 07/05/2011 12:420.91 mg/Kg-dry 124.9NELAP 69348
Lead 07/05/2011 12:423.64 mg/Kg-dry 117.6NELAP 69348
Silver 07/05/2011 12:420.50 mg/Kg-dry 1< 0.50NELAP 69348
SW-846 3050B, METALS BY GFAASelenium 7740 07/05/2011 11:580.545 mg/Kg-dry 1< 0.545NELAP 69349
SW-846 7471AMercury 07/05/2011 12:220.012 mg/Kg-dry 10.019NELAP 69355
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel 07/04/2011 13:006.03 mg/Kg-dry 1NDNELAP 69330
Kerosene 07/04/2011 13:006.03 mg/Kg-dry 1NDNELAP 69330
Mineral Spirits 07/04/2011 13:006.03 mg/Kg-dry 1NDNELAP 69330
Motor Oil 07/04/2011 13:006.03 mg/Kg-dry 1NDNELAP 69330
Surr: n-Tetracontane 07/04/2011 13:0050.6-140 %REC 179.0 69330
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
4,4´-DDE 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
4,4´-DDT J 07/05/2011 23:302.01 µg/Kg-dry 11.0NELAP 69344
Alachlor 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
Aldrin 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
alpha-BHC 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
alpha-Chlordane 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
beta-BHC 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
Chlordane 07/05/2011 23:304.02 µg/Kg-dry 1NDNELAP 69344
delta-BHC 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
Dieldrin S 07/05/2011 23:302.01 µg/Kg-dry 123.7NELAP 69344
Endosulfan I 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
Endosulfan II 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
Endosulfan sulfate 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
Endrin 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
Endrin aldehyde 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
Endrin ketone 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
gamma-BHC 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
gamma-Chlordane 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
Heptachlor 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
Heptachlor epoxide 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
Methoxychlor 07/05/2011 23:302.01 µg/Kg-dry 1NDNELAP 69344
Toxaphene 07/05/2011 23:3036.1 µg/Kg-dry 1NDNELAP 69344
Page 11 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 8:00
Lab ID: 11070042-002 Client Sample ID: SBA-B4-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD Surr: Decachlorobiphenyl 07/05/2011 23:3048-149 %REC 1103.1 69344
Surr: Tetrachloro-m-xylene 07/05/2011 23:3019-145 %REC 176.9 69344
Matrix spike and matrix spike duplicate did not recover within control limits for dieldrin because of sample composition.
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/05/2011 11:2345.1 µg/Kg-dry 1NDNELAP 69344
Aroclor 1221 07/05/2011 11:2345.1 µg/Kg-dry 1NDNELAP 69344
Aroclor 1232 07/05/2011 11:2345.1 µg/Kg-dry 1NDNELAP 69344
Aroclor 1242 07/05/2011 11:2345.1 µg/Kg-dry 1NDNELAP 69344
Aroclor 1248 07/05/2011 11:2345.1 µg/Kg-dry 1NDNELAP 69344
Aroclor 1254 07/05/2011 11:2345.1 µg/Kg-dry 1NDNELAP 69344
Aroclor 1260 07/05/2011 11:2345.1 µg/Kg-dry 1NDNELAP 69344
Surr: Decachlorobiphenyl 07/05/2011 11:235-156 %REC 1102.1 69344
Surr: Tetrachloro-meta-xylene 07/05/2011 11:237.35-123 %REC 178.9 69344
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
Acenaphthylene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
Anthracene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
Benzo(a)anthracene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
Benzo(a)pyrene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
Benzo(b)fluoranthene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
Benzo(g,h,i)perylene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
Benzo(k)fluoranthene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
Bis(2-ethylhexyl)phthalate 07/05/2011 10:030.081 mg/Kg-dry 1NDNELAP 69347
Chrysene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
Dibenzo(a,h)anthracene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
Fluoranthene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
Fluorene 07/05/2011 10:030.004 mg/Kg-dry 10.015NELAP 69347
Indeno(1,2,3-cd)pyrene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
Naphthalene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
Phenanthrene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
Pyrene 07/05/2011 10:030.004 mg/Kg-dry 1NDNELAP 69347
Surr: 2-Fluorobiphenyl 07/05/2011 10:0310-131 %REC 187.8 69347
Surr: Nitrobenzene-d5 07/05/2011 10:0310-132 %REC 177.9 69347
Surr: p-Terphenyl-d14 07/05/2011 10:0380.2-138 %REC 1117.2 69347
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
1,2-Dichlorobenzene 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
1,3-Dichlorobenzene 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
1,4-Dichlorobenzene 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
2,4,5-Trichlorophenol 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
2,4,6-Trichlorophenol 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
2,4-Dichlorophenol 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
2,4-Dimethylphenol 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
2,4-Dinitrophenol 07/05/2011 13:271.20 mg/Kg-dry 1NDNELAP 69346
2,4-Dinitrotoluene 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
2,6-Dinitrotoluene 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
2-Chloronaphthalene 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
Page 12 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 8:00
Lab ID: 11070042-002 Client Sample ID: SBA-B4-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS2-Chlorophenol 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
2-Methoxy-4-methylphenol 07/05/2011 13:270.782 mg/Kg-dry 1ND 69346
2-Methylnaphthalene 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
2-Nitroaniline 07/05/2011 13:271.20 mg/Kg-dry 1NDNELAP 69346
2-Nitrophenol 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
3,3´-Dichlorobenzidine 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
3-Nitroaniline 07/05/2011 13:271.20 mg/Kg-dry 1NDNELAP 69346
4,6-Dinitro-2-methylphenol 07/05/2011 13:271.20 mg/Kg-dry 1NDNELAP 69346
4-Bromophenyl phenyl ether 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
4-Chloro-3-methylphenol 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
4-Chloroaniline 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
4-Chlorophenyl phenyl ether 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
4-Nitroaniline 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
4-Nitrophenol 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
Aniline 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
Azobenzene 07/05/2011 13:270.421 mg/Kg-dry 1ND 69346
Benzidine 07/05/2011 13:271.27 mg/Kg-dry 1See noteNELAP 69346
Benzoic acid 07/05/2011 13:271.81 mg/Kg-dry 1NDNELAP 69346
Benzyl alcohol 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
Bis(2-chloroethoxy)methane 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
Bis(2-chloroethyl)ether 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
Bis(2-chloroisopropyl)ether 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
Butyl benzyl phthalate 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
Carbazole 07/05/2011 13:270.602 mg/Kg-dry 1ND 69346
Dibenzofuran 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
Diethyl phthalate 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
Dimethyl phthalate 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
Di-n-butyl phthalate 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
Di-n-octyl phthalate 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
Hexachlorobenzene 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
Hexachlorobutadiene 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
Hexachlorocyclopentadiene 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
Hexachloroethane 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
Isophorone 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
m,p-Cresol 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
Nitrobenzene 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
N-Nitrosodimethylamine 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
N-Nitroso-di-n-propylamine 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
N-Nitrosodiphenylamine 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
o-Cresol 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
Pentachlorophenol 07/05/2011 13:272.41 mg/Kg-dry 1NDNELAP 69346
Phenol 07/05/2011 13:270.421 mg/Kg-dry 1NDNELAP 69346
Pyridine 07/05/2011 13:270.602 mg/Kg-dry 1NDNELAP 69346
1,2-Diphenylhydrazine 07/05/2011 13:271.01 mg/Kg-dry 1ND 69346
Surr: 2,4,6-Tribromophenol 07/05/2011 13:2732.7-130 %REC 195.7 69346
Surr: 2-Fluorobiphenyl 07/05/2011 13:2734.1-116 %REC 179.2 69346
Surr: 2-Fluorophenol 07/05/2011 13:2730.5-99 %REC 178.7 69346
Page 13 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 8:00
Lab ID: 11070042-002 Client Sample ID: SBA-B4-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: Nitrobenzene-d5 07/05/2011 13:2734.1-101 %REC 178.5 69346
Surr: Phenol-d5 07/05/2011 13:2734.9-110 %REC 179.2 69346
Surr: p-Terphenyl-d14 07/05/2011 13:2741.7-124 %REC 196.4 69346
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.LCS was outside upper QC limits. Sample was ND.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,1,1-Trichloroethane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,1,2,2-Tetrachloroethane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,1,2-Trichloro-1,2,2-trifluoroethane 07/05/2011 12:244.4 µg/Kg-dry 1ND 69368
1,1,2-Trichloroethane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,1-Dichloro-2-propanone 07/05/2011 12:2444.4 µg/Kg-dry 1ND 69368
1,1-Dichloroethane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,1-Dichloroethene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,1-Dichloropropene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,2,3-Trichlorobenzene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,2,3-Trichloropropane 07/05/2011 12:248.9 µg/Kg-dry 1NDNELAP 69368
1,2,3-Trimethylbenzene J 07/05/2011 12:244.4 µg/Kg-dry 11.3 69368
1,2,4-Trichlorobenzene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,2,4-Trimethylbenzene J 07/05/2011 12:244.4 µg/Kg-dry 13.3NELAP 69368
1,2-Dibromo-3-chloropropane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,2-Dibromoethane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,2-Dichlorobenzene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,2-Dichloroethane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,2-Dichloropropane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,3,5-Trimethylbenzene J 07/05/2011 12:244.4 µg/Kg-dry 11.0NELAP 69368
1,3-Dichlorobenzene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,3-Dichloropropane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1,4-Dichlorobenzene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
1-Chlorobutane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
2,2-Dichloropropane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
2-Butanone 07/05/2011 12:2444.4 µg/Kg-dry 1NDNELAP 69368
2-Chlorotoluene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
2-Hexanone 07/05/2011 12:2444.4 µg/Kg-dry 1NDNELAP 69368
2-Nitropropane 07/05/2011 12:2444.4 µg/Kg-dry 1NDNELAP 69368
4-Chlorotoluene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
4-Methyl-2-pentanone 07/05/2011 12:2444.4 µg/Kg-dry 1NDNELAP 69368
Acetone J 07/05/2011 12:2444.4 µg/Kg-dry 120NELAP 69368
Acrolein 07/05/2011 12:2488.8 µg/Kg-dry 1NDNELAP 69368
Acrylonitrile 07/05/2011 12:248.9 µg/Kg-dry 1NDNELAP 69368
Allyl chloride 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Benzene 07/05/2011 12:240.9 µg/Kg-dry 11.8NELAP 69368
Bromobenzene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Bromochloromethane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Bromodichloromethane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Bromoform 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Bromomethane 07/05/2011 12:248.9 µg/Kg-dry 1NDNELAP 69368
Page 14 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 8:00
Lab ID: 11070042-002 Client Sample ID: SBA-B4-01 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSCarbon disulfide 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Carbon tetrachloride 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Chlorobenzene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Chloroethane 07/05/2011 12:248.9 µg/Kg-dry 1NDNELAP 69368
Chloroform 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Chloromethane 07/05/2011 12:248.9 µg/Kg-dry 1NDNELAP 69368
cis-1,2-Dichloroethene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
cis-1,3-Dichloropropene 07/05/2011 12:243.6 µg/Kg-dry 1NDNELAP 69368
Cyclohexanone 07/05/2011 12:2488.8 µg/Kg-dry 1ND 69368
Dibromochloromethane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Dibromomethane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Dichlorodifluoromethane 07/05/2011 12:248.9 µg/Kg-dry 1NDNELAP 69368
Ethyl acetate 07/05/2011 12:2444.4 µg/Kg-dry 1NDNELAP 69368
Ethyl ether 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Ethyl methacrylate 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Ethylbenzene J 07/05/2011 12:244.4 µg/Kg-dry 11.7NELAP 69368
Heptane 07/05/2011 12:2417.8 µg/Kg-dry 1ND 69368
Hexachlorobutadiene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Hexachloroethane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Iodomethane 07/05/2011 12:248.9 µg/Kg-dry 1NDNELAP 69368
Isopropylbenzene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
m,p-Xylenes J 07/05/2011 12:244.4 µg/Kg-dry 13.0NELAP 69368
Methacrylonitrile 07/05/2011 12:2444.4 µg/Kg-dry 1NDNELAP 69368
Methyl Methacrylate 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Methyl tert-butyl ether 07/05/2011 12:241.8 µg/Kg-dry 1NDNELAP 69368
Methylacrylate 07/05/2011 12:248.9 µg/Kg-dry 1ND 69368
Methylene chloride 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Naphthalene J 07/05/2011 12:248.9 µg/Kg-dry 11.8NELAP 69368
n-Butylbenzene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
n-Hexane J 07/05/2011 12:2417.8 µg/Kg-dry 15.4 69368
Nitrobenzene 07/05/2011 12:2488.8 µg/Kg-dry 1NDNELAP 69368
n-Propylbenzene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
o-Xylene J 07/05/2011 12:244.4 µg/Kg-dry 11.1NELAP 69368
Pentachloroethane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
p-Isopropyltoluene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Propionitrile 07/05/2011 12:2444.4 µg/Kg-dry 1NDNELAP 69368
sec-Butylbenzene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Styrene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
tert-Butylbenzene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Tetrachloroethene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Tetrahydrofuran 07/05/2011 12:2444.4 µg/Kg-dry 1NDNELAP 69368
Toluene J 07/05/2011 12:244.4 µg/Kg-dry 13.8NELAP 69368
trans-1,2-Dichloroethene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
trans-1,3-Dichloropropene 07/05/2011 12:243.6 µg/Kg-dry 1NDNELAP 69368
Trichloroethene 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Trichlorofluoromethane 07/05/2011 12:244.4 µg/Kg-dry 1NDNELAP 69368
Vinyl acetate 07/05/2011 12:2444.4 µg/Kg-dry 1NDNELAP 69368
Page 15 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 8:00
Lab ID: 11070042-002 Client Sample ID: SBA-B4-01 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSVinyl chloride 07/05/2011 12:241.8 µg/Kg-dry 1NDNELAP 69368
Surr: 1,2-Dichloroethane-d4 07/05/2011 12:2472.2-131 %REC 1104.9 69368
Surr: 4-Bromofluorobenzene 07/05/2011 12:2482.1-116 %REC 194.6 69368
Surr: Dibromofluoromethane 07/05/2011 12:2477.7-120 %REC 199.8 69368
Surr: Toluene-d8 07/05/2011 12:2486-116 %REC 1104.1 69368
Marginal Exceedance for trichloroethene in LCS is verified per Volume 1 Module 4 section 1.7.4.2 of the 2009 TNI standard.
SW-846 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 07/11/2011 18:300.05 mg/Kg-dry 1NDNELAP R151875
2,4,5-TP (Silvex) 07/11/2011 18:300.05 mg/Kg-dry 1NDNELAP R151875
2,4-D 07/11/2011 18:300.05 mg/Kg-dry 1NDNELAP R151875
2,4-DB 07/11/2011 18:300.05 mg/Kg-dry 1NDNELAP R151875
3,5-Dichlorobenzoic Acid 07/11/2011 18:300.05 mg/Kg-dry 1NDNELAP R151875
Acifluorfen 07/11/2011 18:300.05 mg/Kg-dry 1NDNELAP R151875
Bentazon 07/11/2011 18:300.05 mg/Kg-dry 1NDNELAP R151875
Chloramben 07/11/2011 18:300.05 mg/Kg-dry 1NDNELAP R151875
Dalapon 07/11/2011 18:300.05 mg/Kg-dry 1NDNELAP R151875
DCPA 07/11/2011 18:300.05 mg/Kg-dry 1NDNELAP R151875
Dicamba 07/11/2011 18:300.05 mg/Kg-dry 1NDNELAP R151875
Dichlorprop 07/11/2011 18:300.05 mg/Kg-dry 1NDNELAP R151875
Dinoseb 07/11/2011 18:300.05 mg/Kg-dry 1NDNELAP R151875
Pentachlorophenol 07/11/2011 18:300.05 mg/Kg-dry 1NDNELAP R151875
Picloram 07/11/2011 17:420.05 mg/Kg-dry 1NDNELAP R151875
Surr: DCAA 07/11/2011 18:3024-140 %REC 164.0 R151875
The blank spike recovery and/or blank spike duplicate recovery were outside the established acceptance limits for 3,5-Dichlorobenzoic Acid and 2,4,5-T. Batch was accepted based on acceptable MS/MSD/RPD results.
Page 16 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 9:00
Lab ID: 11070042-003 Client Sample ID: SBA-D5-01 (5-6)
Matrix: SOLID
Batch
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 07/01/2011 16:000.1 % 115.1 R151546
STANDARD METHODS 18TH ED. 2540 GTotal Solids 07/01/2011 16:000.1 % 184.9 R151526
SW-846 9012A (TOTAL)Cyanide 07/02/2011 12:170.59 mg/Kg-dry 1< 0.59NELAP R151533
SW-846 3050B, 6010B, METALS BY ICPArsenic 07/05/2011 12:482.36 mg/Kg-dry 17.12NELAP 69348
Barium 07/05/2011 12:480.47 mg/Kg-dry 147.2NELAP 69348
Cadmium J 07/05/2011 12:480.19 mg/Kg-dry 10.13NELAP 69348
Chromium 07/05/2011 12:480.94 mg/Kg-dry 115.8NELAP 69348
Lead 07/05/2011 12:483.77 mg/Kg-dry 114.3NELAP 69348
Silver 07/05/2011 12:480.52 mg/Kg-dry 1< 0.52NELAP 69348
SW-846 3050B, METALS BY GFAASelenium 7740 07/05/2011 12:010.556 mg/Kg-dry 1< 0.556NELAP 69349
SW-846 7471AMercury J 07/05/2011 12:220.011 mg/Kg-dry 10.005NELAP 69355
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel 07/04/2011 13:175.86 mg/Kg-dry 1NDNELAP 69330
Kerosene 07/04/2011 13:175.86 mg/Kg-dry 1NDNELAP 69330
Mineral Spirits 07/04/2011 13:175.86 mg/Kg-dry 1NDNELAP 69330
Motor Oil 07/04/2011 13:175.86 mg/Kg-dry 1NDNELAP 69330
Surr: n-Tetracontane 07/04/2011 13:1750.6-140 %REC 173.1 69330
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
4,4´-DDE 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
4,4´-DDT 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
Alachlor 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
Aldrin 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
alpha-BHC 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
alpha-Chlordane 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
beta-BHC 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
Chlordane 07/06/2011 0:443.91 µg/Kg-dry 1NDNELAP 69344
delta-BHC 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
Dieldrin 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
Endosulfan I 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
Endosulfan II 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
Endosulfan sulfate 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
Endrin 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
Endrin aldehyde 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
Endrin ketone 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
gamma-BHC 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
gamma-Chlordane 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
Heptachlor 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
Heptachlor epoxide 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
Methoxychlor 07/06/2011 0:441.96 µg/Kg-dry 1NDNELAP 69344
Toxaphene 07/06/2011 0:4435.1 µg/Kg-dry 1NDNELAP 69344
Page 17 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 9:00
Lab ID: 11070042-003 Client Sample ID: SBA-D5-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD Surr: Decachlorobiphenyl 07/06/2011 0:4448-149 %REC 1104.4 69344
Surr: Tetrachloro-m-xylene 07/06/2011 0:4419-145 %REC 180.3 69344
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/05/2011 11:4243.9 µg/Kg-dry 1NDNELAP 69344
Aroclor 1221 07/05/2011 11:4243.9 µg/Kg-dry 1NDNELAP 69344
Aroclor 1232 07/05/2011 11:4243.9 µg/Kg-dry 1NDNELAP 69344
Aroclor 1242 07/05/2011 11:4243.9 µg/Kg-dry 1NDNELAP 69344
Aroclor 1248 07/05/2011 11:4243.9 µg/Kg-dry 1NDNELAP 69344
Aroclor 1254 07/05/2011 11:4243.9 µg/Kg-dry 1NDNELAP 69344
Aroclor 1260 07/05/2011 11:4243.9 µg/Kg-dry 1NDNELAP 69344
Surr: Decachlorobiphenyl 07/05/2011 11:425-156 %REC 199.4 69344
Surr: Tetrachloro-meta-xylene 07/05/2011 11:427.35-123 %REC 181.6 69344
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/05/2011 10:390.004 mg/Kg-dry 10.052NELAP 69347
Acenaphthylene 07/05/2011 10:390.004 mg/Kg-dry 1NDNELAP 69347
Anthracene 07/05/2011 10:390.004 mg/Kg-dry 10.201NELAP 69347
Benzo(a)anthracene 07/05/2011 10:390.004 mg/Kg-dry 10.524NELAP 69347
Benzo(a)pyrene 07/05/2011 10:390.004 mg/Kg-dry 10.540NELAP 69347
Benzo(b)fluoranthene 07/05/2011 10:390.004 mg/Kg-dry 10.776NELAP 69347
Benzo(g,h,i)perylene 07/05/2011 10:390.004 mg/Kg-dry 10.358NELAP 69347
Benzo(k)fluoranthene 07/05/2011 10:390.004 mg/Kg-dry 10.285NELAP 69347
Bis(2-ethylhexyl)phthalate J 07/05/2011 10:390.078 mg/Kg-dry 10.040NELAP 69347
Chrysene 07/05/2011 10:390.004 mg/Kg-dry 10.566NELAP 69347
Dibenzo(a,h)anthracene 07/05/2011 10:390.004 mg/Kg-dry 10.091NELAP 69347
Fluoranthene 07/05/2011 10:390.004 mg/Kg-dry 11.14NELAP 69347
Fluorene 07/05/2011 10:390.004 mg/Kg-dry 10.066NELAP 69347
Indeno(1,2,3-cd)pyrene 07/05/2011 10:390.004 mg/Kg-dry 10.337NELAP 69347
Naphthalene 07/05/2011 10:390.004 mg/Kg-dry 10.021NELAP 69347
Phenanthrene 07/05/2011 10:390.004 mg/Kg-dry 10.803NELAP 69347
Pyrene 07/05/2011 10:390.004 mg/Kg-dry 10.971NELAP 69347
Surr: 2-Fluorobiphenyl 07/05/2011 10:3910-131 %REC 184.7 69347
Surr: Nitrobenzene-d5 07/05/2011 10:3910-132 %REC 175.4 69347
Surr: p-Terphenyl-d14 07/05/2011 10:3980.2-138 %REC 1116.4 69347
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
1,2-Dichlorobenzene 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
1,3-Dichlorobenzene 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
1,4-Dichlorobenzene 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
2,4,5-Trichlorophenol 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
2,4,6-Trichlorophenol 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
2,4-Dichlorophenol 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
2,4-Dimethylphenol 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
2,4-Dinitrophenol 07/05/2011 12:301.17 mg/Kg-dry 1NDNELAP 69346
2,4-Dinitrotoluene 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
2,6-Dinitrotoluene 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
2-Chloronaphthalene 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
2-Chlorophenol 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
Page 18 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 9:00
Lab ID: 11070042-003 Client Sample ID: SBA-D5-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS2-Methoxy-4-methylphenol 07/05/2011 12:300.761 mg/Kg-dry 1ND 69346
2-Methylnaphthalene 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
2-Nitroaniline 07/05/2011 12:301.17 mg/Kg-dry 1NDNELAP 69346
2-Nitrophenol 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
3,3´-Dichlorobenzidine 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
3-Nitroaniline 07/05/2011 12:301.17 mg/Kg-dry 1NDNELAP 69346
4,6-Dinitro-2-methylphenol 07/05/2011 12:301.17 mg/Kg-dry 1NDNELAP 69346
4-Bromophenyl phenyl ether 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
4-Chloro-3-methylphenol 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
4-Chloroaniline 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
4-Chlorophenyl phenyl ether 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
4-Nitroaniline 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
4-Nitrophenol 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
Aniline 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
Azobenzene 07/05/2011 12:300.410 mg/Kg-dry 1ND 69346
Benzidine 07/05/2011 12:301.24 mg/Kg-dry 1See noteNELAP 69346
Benzoic acid 07/05/2011 12:301.76 mg/Kg-dry 1NDNELAP 69346
Benzyl alcohol 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
Bis(2-chloroethoxy)methane 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
Bis(2-chloroethyl)ether 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
Bis(2-chloroisopropyl)ether 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
Butyl benzyl phthalate 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
Carbazole 07/05/2011 12:300.586 mg/Kg-dry 1ND 69346
Dibenzofuran 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
Diethyl phthalate 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
Dimethyl phthalate S 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
Di-n-butyl phthalate 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
Di-n-octyl phthalate 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
Hexachlorobenzene S 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
Hexachlorobutadiene 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
Hexachlorocyclopentadiene 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
Hexachloroethane 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
Isophorone 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
m,p-Cresol 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
Nitrobenzene S 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
N-Nitrosodimethylamine 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
N-Nitroso-di-n-propylamine 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
N-Nitrosodiphenylamine 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
o-Cresol 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
Pentachlorophenol 07/05/2011 12:302.34 mg/Kg-dry 1NDNELAP 69346
Phenol 07/05/2011 12:300.410 mg/Kg-dry 1NDNELAP 69346
Pyridine 07/05/2011 12:300.586 mg/Kg-dry 1NDNELAP 69346
1,2-Diphenylhydrazine 07/05/2011 12:300.984 mg/Kg-dry 1ND 69346
Surr: 2,4,6-Tribromophenol 07/05/2011 12:3032.7-130 %REC 1103.9 69346
Surr: 2-Fluorobiphenyl 07/05/2011 12:3034.1-116 %REC 188.0 69346
Surr: 2-Fluorophenol 07/05/2011 12:3030.5-99 %REC 182.6 69346
Surr: Nitrobenzene-d5 07/05/2011 12:3034.1-101 %REC 191.0 69346
Page 19 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 9:00
Lab ID: 11070042-003 Client Sample ID: SBA-D5-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: Phenol-d5 07/05/2011 12:3034.9-110 %REC 182.8 69346
Surr: p-Terphenyl-d14 07/05/2011 12:3041.7-124 %REC 1109.2 69346
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.Matrix spike duplicate was outside QC limits.LCS was outside upper QC limits. Sample was ND.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,1,1-Trichloroethane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,1,2,2-Tetrachloroethane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,1,2-Trichloro-1,2,2-trifluoroethane 07/05/2011 12:544.3 µg/Kg-dry 1ND 69368
1,1,2-Trichloroethane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,1-Dichloro-2-propanone 07/05/2011 12:5442.5 µg/Kg-dry 1ND 69368
1,1-Dichloroethane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,1-Dichloroethene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,1-Dichloropropene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,2,3-Trichlorobenzene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,2,3-Trichloropropane 07/05/2011 12:548.5 µg/Kg-dry 1NDNELAP 69368
1,2,3-Trimethylbenzene J 07/05/2011 12:544.3 µg/Kg-dry 11.4 69368
1,2,4-Trichlorobenzene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,2,4-Trimethylbenzene J 07/05/2011 12:544.3 µg/Kg-dry 13.3NELAP 69368
1,2-Dibromo-3-chloropropane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,2-Dibromoethane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,2-Dichlorobenzene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,2-Dichloroethane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,2-Dichloropropane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,3,5-Trimethylbenzene J 07/05/2011 12:544.3 µg/Kg-dry 10.9NELAP 69368
1,3-Dichlorobenzene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,3-Dichloropropane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1,4-Dichlorobenzene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
1-Chlorobutane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
2,2-Dichloropropane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
2-Butanone 07/05/2011 12:5442.5 µg/Kg-dry 1NDNELAP 69368
2-Chlorotoluene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
2-Hexanone 07/05/2011 12:5442.5 µg/Kg-dry 1NDNELAP 69368
2-Nitropropane 07/05/2011 12:5442.5 µg/Kg-dry 1NDNELAP 69368
4-Chlorotoluene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
4-Methyl-2-pentanone 07/05/2011 12:5442.5 µg/Kg-dry 1NDNELAP 69368
Acetone 07/05/2011 12:5442.5 µg/Kg-dry 147.8NELAP 69368
Acrolein 07/05/2011 12:5485.1 µg/Kg-dry 1NDNELAP 69368
Acrylonitrile 07/05/2011 12:548.5 µg/Kg-dry 1NDNELAP 69368
Allyl chloride 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Benzene 07/05/2011 12:540.9 µg/Kg-dry 11.7NELAP 69368
Bromobenzene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Bromochloromethane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Bromodichloromethane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Bromoform 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Bromomethane 07/05/2011 12:548.5 µg/Kg-dry 1NDNELAP 69368
Page 20 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 9:00
Lab ID: 11070042-003 Client Sample ID: SBA-D5-01 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSCarbon disulfide 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Carbon tetrachloride 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Chlorobenzene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Chloroethane 07/05/2011 12:548.5 µg/Kg-dry 1NDNELAP 69368
Chloroform 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Chloromethane 07/05/2011 12:548.5 µg/Kg-dry 1NDNELAP 69368
cis-1,2-Dichloroethene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
cis-1,3-Dichloropropene 07/05/2011 12:543.4 µg/Kg-dry 1NDNELAP 69368
Cyclohexanone 07/05/2011 12:5485.1 µg/Kg-dry 1ND 69368
Dibromochloromethane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Dibromomethane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Dichlorodifluoromethane 07/05/2011 12:548.5 µg/Kg-dry 1NDNELAP 69368
Ethyl acetate 07/05/2011 12:5442.5 µg/Kg-dry 1NDNELAP 69368
Ethyl ether 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Ethyl methacrylate 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Ethylbenzene J 07/05/2011 12:544.3 µg/Kg-dry 11.2NELAP 69368
Heptane 07/05/2011 12:5417.0 µg/Kg-dry 1ND 69368
Hexachlorobutadiene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Hexachloroethane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Iodomethane 07/05/2011 12:548.5 µg/Kg-dry 1NDNELAP 69368
Isopropylbenzene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
m,p-Xylenes J 07/05/2011 12:544.3 µg/Kg-dry 12.5NELAP 69368
Methacrylonitrile 07/05/2011 12:5442.5 µg/Kg-dry 1NDNELAP 69368
Methyl Methacrylate 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Methyl tert-butyl ether 07/05/2011 12:541.7 µg/Kg-dry 1NDNELAP 69368
Methylacrylate 07/05/2011 12:548.5 µg/Kg-dry 1ND 69368
Methylene chloride 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Naphthalene J 07/05/2011 12:548.5 µg/Kg-dry 12.3NELAP 69368
n-Butylbenzene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
n-Hexane J 07/05/2011 12:5417.0 µg/Kg-dry 14.8 69368
Nitrobenzene 07/05/2011 12:5485.1 µg/Kg-dry 1NDNELAP 69368
n-Propylbenzene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
o-Xylene J 07/05/2011 12:544.3 µg/Kg-dry 11.0NELAP 69368
Pentachloroethane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
p-Isopropyltoluene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Propionitrile 07/05/2011 12:5442.5 µg/Kg-dry 1NDNELAP 69368
sec-Butylbenzene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Styrene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
tert-Butylbenzene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Tetrachloroethene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Tetrahydrofuran 07/05/2011 12:5442.5 µg/Kg-dry 1NDNELAP 69368
Toluene J 07/05/2011 12:544.3 µg/Kg-dry 13.7NELAP 69368
trans-1,2-Dichloroethene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
trans-1,3-Dichloropropene 07/05/2011 12:543.4 µg/Kg-dry 1NDNELAP 69368
Trichloroethene 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Trichlorofluoromethane 07/05/2011 12:544.3 µg/Kg-dry 1NDNELAP 69368
Vinyl acetate 07/05/2011 12:5442.5 µg/Kg-dry 1NDNELAP 69368
Page 21 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 9:00
Lab ID: 11070042-003 Client Sample ID: SBA-D5-01 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSVinyl chloride 07/05/2011 12:541.7 µg/Kg-dry 1NDNELAP 69368
Surr: 1,2-Dichloroethane-d4 07/05/2011 12:5472.2-131 %REC 1104.9 69368
Surr: 4-Bromofluorobenzene 07/05/2011 12:5482.1-116 %REC 190.9 69368
Surr: Dibromofluoromethane 07/05/2011 12:5477.7-120 %REC 1100.4 69368
Surr: Toluene-d8 07/05/2011 12:5486-116 %REC 1106.0 69368
Marginal Exceedance for trichloroethene in LCS is verified per Volume 1 Module 4 section 1.7.4.2 of the 2009 TNI standard.
SW-846 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875
2,4,5-TP (Silvex) 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875
2,4-D R 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875
2,4-DB 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875
3,5-Dichlorobenzoic Acid 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875
Acifluorfen 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875
Bentazon 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875
Chloramben 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875
Dalapon 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875
DCPA 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875
Dicamba 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875
Dichlorprop 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875
Dinoseb R 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875
Pentachlorophenol 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875
Picloram 07/11/2011 18:300.05 mg/Kg-dry 1NDNELAP R151875
Surr: DCAA 07/11/2011 19:1724-140 %REC 149.6 R151875
The MS/MSD RPD result exceeded the QC control limits for 2,4-D and Dinoseb; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data.The blank spike recovery and/or blank spike duplicate recovery were outside the established acceptance limits for 3,5-Dichlorobenzoic Acid and 2,4,5-T. Batch was accepted based on acceptable MS/MSD/RPD results.
Page 22 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 10:00
Lab ID: 11070042-004 Client Sample ID: SBA-A3-01 (5-6)
Matrix: SOLID
Batch
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 07/01/2011 16:000.1 % 112.6 R151546
STANDARD METHODS 18TH ED. 2540 GTotal Solids 07/01/2011 16:000.1 % 187.4 R151526
SW-846 9012A (TOTAL)Cyanide 07/02/2011 12:170.64 mg/Kg-dry 1< 0.64NELAP R151533
SW-846 3050B, 6010B, METALS BY ICPArsenic 07/05/2011 12:542.27 mg/Kg-dry 14.15NELAP 69348
Barium 07/05/2011 12:540.45 mg/Kg-dry 123.7NELAP 69348
Cadmium J 07/05/2011 12:540.18 mg/Kg-dry 10.09NELAP 69348
Chromium 07/05/2011 12:540.91 mg/Kg-dry 115.7NELAP 69348
Lead 07/05/2011 12:543.64 mg/Kg-dry 110.6NELAP 69348
Silver 07/05/2011 12:540.50 mg/Kg-dry 1< 0.50NELAP 69348
SW-846 3050B, METALS BY GFAASelenium 7740 07/05/2011 12:050.588 mg/Kg-dry 1< 0.588NELAP 69349
SW-846 7471AMercury J 07/05/2011 12:220.011 mg/Kg-dry 10.003NELAP 69355
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel 07/04/2011 13:355.69 mg/Kg-dry 1NDNELAP 69330
Kerosene 07/04/2011 13:355.69 mg/Kg-dry 1NDNELAP 69330
Mineral Spirits 07/04/2011 13:355.69 mg/Kg-dry 1NDNELAP 69330
Motor Oil 07/04/2011 13:355.69 mg/Kg-dry 1NDNELAP 69330
Surr: n-Tetracontane 07/04/2011 13:3550.6-140 %REC 179.8 69330
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
4,4´-DDE 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
4,4´-DDT 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
Alachlor 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
Aldrin 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
alpha-BHC 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
alpha-Chlordane 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
beta-BHC 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
Chlordane 07/06/2011 1:083.82 µg/Kg-dry 1NDNELAP 69344
delta-BHC 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
Dieldrin 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
Endosulfan I 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
Endosulfan II 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
Endosulfan sulfate 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
Endrin 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
Endrin aldehyde 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
Endrin ketone 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
gamma-BHC 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
gamma-Chlordane 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
Heptachlor 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
Heptachlor epoxide 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
Methoxychlor 07/06/2011 1:081.91 µg/Kg-dry 1NDNELAP 69344
Toxaphene 07/06/2011 1:0834.3 µg/Kg-dry 1NDNELAP 69344
Page 23 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 10:00
Lab ID: 11070042-004 Client Sample ID: SBA-A3-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD Surr: Decachlorobiphenyl 07/06/2011 1:0848-149 %REC 1101.6 69344
Surr: Tetrachloro-m-xylene 07/06/2011 1:0819-145 %REC 171.9 69344
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/05/2011 12:0142.9 µg/Kg-dry 1NDNELAP 69344
Aroclor 1221 07/05/2011 12:0142.9 µg/Kg-dry 1NDNELAP 69344
Aroclor 1232 07/05/2011 12:0142.9 µg/Kg-dry 1NDNELAP 69344
Aroclor 1242 07/05/2011 12:0142.9 µg/Kg-dry 1NDNELAP 69344
Aroclor 1248 07/05/2011 12:0142.9 µg/Kg-dry 1NDNELAP 69344
Aroclor 1254 07/05/2011 12:0142.9 µg/Kg-dry 1NDNELAP 69344
Aroclor 1260 07/05/2011 12:0142.9 µg/Kg-dry 1NDNELAP 69344
Surr: Decachlorobiphenyl 07/05/2011 12:015-156 %REC 199.8 69344
Surr: Tetrachloro-meta-xylene 07/05/2011 12:017.35-123 %REC 173.0 69344
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/05/2011 11:150.004 mg/Kg-dry 1NDNELAP 69347
Acenaphthylene 07/05/2011 11:150.004 mg/Kg-dry 1NDNELAP 69347
Anthracene 07/05/2011 11:150.004 mg/Kg-dry 1NDNELAP 69347
Benzo(a)anthracene 07/05/2011 11:150.004 mg/Kg-dry 10.004NELAP 69347
Benzo(a)pyrene 07/05/2011 11:150.004 mg/Kg-dry 1NDNELAP 69347
Benzo(b)fluoranthene 07/05/2011 11:150.004 mg/Kg-dry 1NDNELAP 69347
Benzo(g,h,i)perylene J 07/05/2011 11:150.004 mg/Kg-dry 10.004NELAP 69347
Benzo(k)fluoranthene 07/05/2011 11:150.004 mg/Kg-dry 1NDNELAP 69347
Bis(2-ethylhexyl)phthalate 07/05/2011 11:150.076 mg/Kg-dry 1NDNELAP 69347
Chrysene 07/05/2011 11:150.004 mg/Kg-dry 1NDNELAP 69347
Dibenzo(a,h)anthracene 07/05/2011 11:150.004 mg/Kg-dry 1NDNELAP 69347
Fluoranthene 07/05/2011 11:150.004 mg/Kg-dry 1NDNELAP 69347
Fluorene 07/05/2011 11:150.004 mg/Kg-dry 1NDNELAP 69347
Indeno(1,2,3-cd)pyrene 07/05/2011 11:150.004 mg/Kg-dry 1NDNELAP 69347
Naphthalene 07/05/2011 11:150.004 mg/Kg-dry 1NDNELAP 69347
Phenanthrene 07/05/2011 11:150.004 mg/Kg-dry 1NDNELAP 69347
Pyrene 07/05/2011 11:150.004 mg/Kg-dry 1NDNELAP 69347
Surr: 2-Fluorobiphenyl 07/05/2011 11:1510-131 %REC 181.3 69347
Surr: Nitrobenzene-d5 07/05/2011 11:1510-132 %REC 173.5 69347
Surr: p-Terphenyl-d14 07/05/2011 11:1580.2-138 %REC 1121.6 69347
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
1,2-Dichlorobenzene 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
1,3-Dichlorobenzene 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
1,4-Dichlorobenzene 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
2,4,5-Trichlorophenol 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
2,4,6-Trichlorophenol 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
2,4-Dichlorophenol 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
2,4-Dimethylphenol 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
2,4-Dinitrophenol 07/05/2011 12:541.14 mg/Kg-dry 1NDNELAP 69346
2,4-Dinitrotoluene 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
2,6-Dinitrotoluene 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
2-Chloronaphthalene 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
2-Chlorophenol 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
Page 24 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 10:00
Lab ID: 11070042-004 Client Sample ID: SBA-A3-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS2-Methoxy-4-methylphenol 07/05/2011 12:540.740 mg/Kg-dry 1ND 69346
2-Methylnaphthalene 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
2-Nitroaniline 07/05/2011 12:541.14 mg/Kg-dry 1NDNELAP 69346
2-Nitrophenol 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
3,3´-Dichlorobenzidine 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
3-Nitroaniline 07/05/2011 12:541.14 mg/Kg-dry 1NDNELAP 69346
4,6-Dinitro-2-methylphenol 07/05/2011 12:541.14 mg/Kg-dry 1NDNELAP 69346
4-Bromophenyl phenyl ether 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
4-Chloro-3-methylphenol 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
4-Chloroaniline 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
4-Chlorophenyl phenyl ether 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
4-Nitroaniline 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
4-Nitrophenol 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
Aniline 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
Azobenzene 07/05/2011 12:540.398 mg/Kg-dry 1ND 69346
Benzidine 07/05/2011 12:541.20 mg/Kg-dry 1See noteNELAP 69346
Benzoic acid 07/05/2011 12:541.71 mg/Kg-dry 1NDNELAP 69346
Benzyl alcohol 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
Bis(2-chloroethoxy)methane 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
Bis(2-chloroethyl)ether 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
Bis(2-chloroisopropyl)ether 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
Butyl benzyl phthalate 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
Carbazole 07/05/2011 12:540.569 mg/Kg-dry 1ND 69346
Dibenzofuran 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
Diethyl phthalate 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
Dimethyl phthalate 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
Di-n-butyl phthalate 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
Di-n-octyl phthalate 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
Hexachlorobenzene 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
Hexachlorobutadiene 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
Hexachlorocyclopentadiene 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
Hexachloroethane 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
Isophorone 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
m,p-Cresol 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
Nitrobenzene 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
N-Nitrosodimethylamine 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
N-Nitroso-di-n-propylamine 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
N-Nitrosodiphenylamine 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
o-Cresol 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
Pentachlorophenol 07/05/2011 12:542.28 mg/Kg-dry 1NDNELAP 69346
Phenol 07/05/2011 12:540.398 mg/Kg-dry 1NDNELAP 69346
Pyridine 07/05/2011 12:540.569 mg/Kg-dry 1NDNELAP 69346
1,2-Diphenylhydrazine 07/05/2011 12:540.956 mg/Kg-dry 1ND 69346
Surr: 2,4,6-Tribromophenol 07/05/2011 12:5432.7-130 %REC 179.9 69346
Surr: 2-Fluorobiphenyl 07/05/2011 12:5434.1-116 %REC 172.3 69346
Surr: 2-Fluorophenol 07/05/2011 12:5430.5-99 %REC 173.3 69346
Surr: Nitrobenzene-d5 07/05/2011 12:5434.1-101 %REC 177.1 69346
Page 25 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 10:00
Lab ID: 11070042-004 Client Sample ID: SBA-A3-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: Phenol-d5 07/05/2011 12:5434.9-110 %REC 176.9 69346
Surr: p-Terphenyl-d14 07/05/2011 12:5441.7-124 %REC 191.3 69346
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.LCS was outside upper QC limits. Sample was ND.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,1,1-Trichloroethane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,1,2,2-Tetrachloroethane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,1,2-Trichloro-1,2,2-trifluoroethane 07/05/2011 13:224.0 µg/Kg-dry 1ND 69368
1,1,2-Trichloroethane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,1-Dichloro-2-propanone 07/05/2011 13:2239.7 µg/Kg-dry 1ND 69368
1,1-Dichloroethane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,1-Dichloroethene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,1-Dichloropropene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,2,3-Trichlorobenzene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,2,3-Trichloropropane 07/05/2011 13:227.9 µg/Kg-dry 1NDNELAP 69368
1,2,3-Trimethylbenzene 07/05/2011 13:224.0 µg/Kg-dry 1ND 69368
1,2,4-Trichlorobenzene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,2,4-Trimethylbenzene J 07/05/2011 13:224.0 µg/Kg-dry 11.8NELAP 69368
1,2-Dibromo-3-chloropropane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,2-Dibromoethane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,2-Dichlorobenzene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,2-Dichloroethane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,2-Dichloropropane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,3,5-Trimethylbenzene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,3-Dichlorobenzene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,3-Dichloropropane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1,4-Dichlorobenzene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
1-Chlorobutane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
2,2-Dichloropropane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
2-Butanone 07/05/2011 13:2239.7 µg/Kg-dry 1NDNELAP 69368
2-Chlorotoluene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
2-Hexanone 07/05/2011 13:2239.7 µg/Kg-dry 1NDNELAP 69368
2-Nitropropane 07/05/2011 13:2239.7 µg/Kg-dry 1NDNELAP 69368
4-Chlorotoluene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
4-Methyl-2-pentanone 07/05/2011 13:2239.7 µg/Kg-dry 1NDNELAP 69368
Acetone J 07/05/2011 13:2239.7 µg/Kg-dry 128NELAP 69368
Acrolein 07/05/2011 13:2279.3 µg/Kg-dry 1NDNELAP 69368
Acrylonitrile 07/05/2011 13:227.9 µg/Kg-dry 1NDNELAP 69368
Allyl chloride 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Benzene 07/05/2011 13:220.8 µg/Kg-dry 10.9NELAP 69368
Bromobenzene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Bromochloromethane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Bromodichloromethane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Bromoform 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Bromomethane 07/05/2011 13:227.9 µg/Kg-dry 1NDNELAP 69368
Carbon disulfide 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Page 26 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 10:00
Lab ID: 11070042-004 Client Sample ID: SBA-A3-01 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSCarbon tetrachloride 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Chlorobenzene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Chloroethane 07/05/2011 13:227.9 µg/Kg-dry 1NDNELAP 69368
Chloroform 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Chloromethane J 07/05/2011 13:227.9 µg/Kg-dry 14.1NELAP 69368
cis-1,2-Dichloroethene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
cis-1,3-Dichloropropene 07/05/2011 13:223.2 µg/Kg-dry 1NDNELAP 69368
Cyclohexanone 07/05/2011 13:2279.3 µg/Kg-dry 1ND 69368
Dibromochloromethane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Dibromomethane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Dichlorodifluoromethane 07/05/2011 13:227.9 µg/Kg-dry 1NDNELAP 69368
Ethyl acetate 07/05/2011 13:2239.7 µg/Kg-dry 1NDNELAP 69368
Ethyl ether 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Ethyl methacrylate 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Ethylbenzene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Heptane 07/05/2011 13:2215.9 µg/Kg-dry 1ND 69368
Hexachlorobutadiene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Hexachloroethane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Iodomethane 07/05/2011 13:227.9 µg/Kg-dry 1NDNELAP 69368
Isopropylbenzene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
m,p-Xylenes J 07/05/2011 13:224.0 µg/Kg-dry 11.0NELAP 69368
Methacrylonitrile 07/05/2011 13:2239.7 µg/Kg-dry 1NDNELAP 69368
Methyl Methacrylate 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Methyl tert-butyl ether 07/05/2011 13:221.6 µg/Kg-dry 1NDNELAP 69368
Methylacrylate 07/05/2011 13:227.9 µg/Kg-dry 1ND 69368
Methylene chloride 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Naphthalene J 07/05/2011 13:227.9 µg/Kg-dry 11.6NELAP 69368
n-Butylbenzene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
n-Hexane J 07/05/2011 13:2215.9 µg/Kg-dry 13.2 69368
Nitrobenzene 07/05/2011 13:2279.3 µg/Kg-dry 1NDNELAP 69368
n-Propylbenzene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
o-Xylene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Pentachloroethane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
p-Isopropyltoluene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Propionitrile 07/05/2011 13:2239.7 µg/Kg-dry 1NDNELAP 69368
sec-Butylbenzene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Styrene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
tert-Butylbenzene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Tetrachloroethene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Tetrahydrofuran 07/05/2011 13:2239.7 µg/Kg-dry 1NDNELAP 69368
Toluene J 07/05/2011 13:224.0 µg/Kg-dry 11.4NELAP 69368
trans-1,2-Dichloroethene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
trans-1,3-Dichloropropene 07/05/2011 13:223.2 µg/Kg-dry 1NDNELAP 69368
Trichloroethene 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Trichlorofluoromethane 07/05/2011 13:224.0 µg/Kg-dry 1NDNELAP 69368
Vinyl acetate 07/05/2011 13:2239.7 µg/Kg-dry 1NDNELAP 69368
Vinyl chloride 07/05/2011 13:221.6 µg/Kg-dry 1NDNELAP 69368
Page 27 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 10:00
Lab ID: 11070042-004 Client Sample ID: SBA-A3-01 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: 1,2-Dichloroethane-d4 07/05/2011 13:2272.2-131 %REC 1108.8 69368
Surr: 4-Bromofluorobenzene 07/05/2011 13:2282.1-116 %REC 193.0 69368
Surr: Dibromofluoromethane 07/05/2011 13:2277.7-120 %REC 1102.0 69368
Surr: Toluene-d8 07/05/2011 13:2286-116 %REC 1106.8 69368
Marginal Exceedance for trichloroethene in LCS is verified per Volume 1 Module 4 section 1.7.4.2 of the 2009 TNI standard.
SW-846 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 07/11/2011 20:050.05 mg/Kg-dry 1NDNELAP R151875
2,4,5-TP (Silvex) 07/11/2011 20:050.05 mg/Kg-dry 1NDNELAP R151875
2,4-D 07/11/2011 20:050.05 mg/Kg-dry 1NDNELAP R151875
2,4-DB 07/11/2011 20:050.05 mg/Kg-dry 1NDNELAP R151875
3,5-Dichlorobenzoic Acid 07/11/2011 20:050.05 mg/Kg-dry 1NDNELAP R151875
Acifluorfen 07/11/2011 20:050.05 mg/Kg-dry 1NDNELAP R151875
Bentazon 07/11/2011 20:050.05 mg/Kg-dry 1NDNELAP R151875
Chloramben 07/11/2011 20:050.05 mg/Kg-dry 1NDNELAP R151875
Dalapon 07/11/2011 20:050.05 mg/Kg-dry 1NDNELAP R151875
DCPA 07/11/2011 20:050.05 mg/Kg-dry 1NDNELAP R151875
Dicamba 07/11/2011 20:050.05 mg/Kg-dry 1NDNELAP R151875
Dichlorprop 07/11/2011 20:050.05 mg/Kg-dry 1NDNELAP R151875
Dinoseb 07/11/2011 20:050.05 mg/Kg-dry 1NDNELAP R151875
Pentachlorophenol 07/11/2011 20:050.05 mg/Kg-dry 1NDNELAP R151875
Picloram 07/11/2011 19:170.05 mg/Kg-dry 1NDNELAP R151875
Surr: DCAA 07/11/2011 20:0524-140 %REC 148.7 R151875
The blank spike recovery and/or blank spike duplicate recovery were outside the established acceptance limits for 3,5-Dichlorobenzoic Acid and 2,4,5-T. Batch was accepted based on acceptable MS/MSD/RPD results.
Page 28 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 11:00
Lab ID: 11070042-005 Client Sample ID: SBA-A5-01 (5-6)
Matrix: SOLID
Batch
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 07/01/2011 16:000.1 % 114.5 R151546
STANDARD METHODS 18TH ED. 2540 GTotal Solids 07/01/2011 16:000.1 % 185.5 R151526
SW-846 9012A (TOTAL)Cyanide R 07/02/2011 12:170.58 mg/Kg-dry 1< 0.58NELAP R151533
RPD for MS/MSD was outside of QC limit due to sample composition.
SW-846 3050B, 6010B, METALS BY ICPArsenic 07/05/2011 13:002.36 mg/Kg-dry 16.63NELAP 69348
Barium 07/05/2011 13:000.47 mg/Kg-dry 142.6NELAP 69348
Cadmium 07/05/2011 13:000.19 mg/Kg-dry 1< 0.19NELAP 69348
Chromium 07/05/2011 13:000.94 mg/Kg-dry 118.1NELAP 69348
Lead 07/05/2011 13:003.77 mg/Kg-dry 112.7NELAP 69348
Silver 07/05/2011 13:000.52 mg/Kg-dry 1< 0.52NELAP 69348
SW-846 3050B, METALS BY GFAASelenium 7740 07/05/2011 12:150.577 mg/Kg-dry 1< 0.577NELAP 69349
SW-846 7471AMercury 07/05/2011 12:220.011 mg/Kg-dry 10.015NELAP 69355
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel 07/04/2011 13:525.80 mg/Kg-dry 1NDNELAP 69330
Kerosene 07/04/2011 13:525.80 mg/Kg-dry 1NDNELAP 69330
Mineral Spirits 07/04/2011 13:525.80 mg/Kg-dry 1NDNELAP 69330
Motor Oil 07/04/2011 13:525.80 mg/Kg-dry 1NDNELAP 69330
Surr: n-Tetracontane 07/04/2011 13:5250.6-140 %REC 178.2 69330
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
4,4´-DDE 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
4,4´-DDT 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
Alachlor 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
Aldrin 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
alpha-BHC 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
alpha-Chlordane 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
beta-BHC 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
Chlordane 07/06/2011 1:333.88 µg/Kg-dry 1NDNELAP 69344
delta-BHC 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
Dieldrin 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
Endosulfan I 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
Endosulfan II 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
Endosulfan sulfate 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
Endrin 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
Endrin aldehyde 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
Endrin ketone 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
gamma-BHC 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
gamma-Chlordane 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
Heptachlor 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
Heptachlor epoxide 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
Methoxychlor 07/06/2011 1:331.94 µg/Kg-dry 1NDNELAP 69344
Toxaphene 07/06/2011 1:3334.8 µg/Kg-dry 1NDNELAP 69344
Page 29 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 11:00
Lab ID: 11070042-005 Client Sample ID: SBA-A5-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD Surr: Decachlorobiphenyl 07/06/2011 1:3348-149 %REC 197.6 69344
Surr: Tetrachloro-m-xylene 07/06/2011 1:3319-145 %REC 167.4 69344
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/05/2011 12:2143.6 µg/Kg-dry 1NDNELAP 69344
Aroclor 1221 07/05/2011 12:2143.6 µg/Kg-dry 1NDNELAP 69344
Aroclor 1232 07/05/2011 12:2143.6 µg/Kg-dry 1NDNELAP 69344
Aroclor 1242 07/05/2011 12:2143.6 µg/Kg-dry 1NDNELAP 69344
Aroclor 1248 07/05/2011 12:2143.6 µg/Kg-dry 1NDNELAP 69344
Aroclor 1254 07/05/2011 12:2143.6 µg/Kg-dry 1NDNELAP 69344
Aroclor 1260 07/05/2011 12:2143.6 µg/Kg-dry 1NDNELAP 69344
Surr: Decachlorobiphenyl 07/05/2011 12:215-156 %REC 197.7 69344
Surr: Tetrachloro-meta-xylene 07/05/2011 12:217.35-123 %REC 166.7 69344
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/05/2011 13:030.004 mg/Kg-dry 1NDNELAP 69347
Acenaphthylene 07/05/2011 13:030.004 mg/Kg-dry 1NDNELAP 69347
Anthracene 07/05/2011 13:030.004 mg/Kg-dry 1NDNELAP 69347
Benzo(a)anthracene 07/05/2011 13:030.004 mg/Kg-dry 10.004NELAP 69347
Benzo(a)pyrene 07/05/2011 13:030.004 mg/Kg-dry 1NDNELAP 69347
Benzo(b)fluoranthene 07/05/2011 13:030.004 mg/Kg-dry 1NDNELAP 69347
Benzo(g,h,i)perylene J 07/05/2011 13:030.004 mg/Kg-dry 10.004NELAP 69347
Benzo(k)fluoranthene 07/05/2011 13:030.004 mg/Kg-dry 1NDNELAP 69347
Bis(2-ethylhexyl)phthalate 07/05/2011 13:030.078 mg/Kg-dry 1NDNELAP 69347
Chrysene 07/05/2011 13:030.004 mg/Kg-dry 1NDNELAP 69347
Dibenzo(a,h)anthracene 07/05/2011 13:030.004 mg/Kg-dry 1NDNELAP 69347
Fluoranthene J 07/05/2011 13:030.004 mg/Kg-dry 10.004NELAP 69347
Fluorene 07/05/2011 13:030.004 mg/Kg-dry 1NDNELAP 69347
Indeno(1,2,3-cd)pyrene 07/05/2011 13:030.004 mg/Kg-dry 1NDNELAP 69347
Naphthalene 07/05/2011 13:030.004 mg/Kg-dry 1NDNELAP 69347
Phenanthrene J 07/05/2011 13:030.004 mg/Kg-dry 10.004NELAP 69347
Pyrene 07/05/2011 13:030.004 mg/Kg-dry 10.005NELAP 69347
Surr: 2-Fluorobiphenyl 07/05/2011 13:0310-131 %REC 178.2 69347
Surr: Nitrobenzene-d5 07/05/2011 13:0310-132 %REC 172.7 69347
Surr: p-Terphenyl-d14 07/05/2011 13:0380.2-138 %REC 1116.9 69347
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
1,2-Dichlorobenzene 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
1,3-Dichlorobenzene 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
1,4-Dichlorobenzene 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
2,4,5-Trichlorophenol 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
2,4,6-Trichlorophenol 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
2,4-Dichlorophenol 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
2,4-Dimethylphenol 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
2,4-Dinitrophenol 07/05/2011 11:581.16 mg/Kg-dry 1NDNELAP 69346
2,4-Dinitrotoluene 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
2,6-Dinitrotoluene 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
2-Chloronaphthalene 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
2-Chlorophenol 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
Page 30 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 11:00
Lab ID: 11070042-005 Client Sample ID: SBA-A5-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS2-Methoxy-4-methylphenol 07/05/2011 11:580.754 mg/Kg-dry 1ND 69346
2-Methylnaphthalene 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
2-Nitroaniline 07/05/2011 11:581.16 mg/Kg-dry 1NDNELAP 69346
2-Nitrophenol 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
3,3´-Dichlorobenzidine 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
3-Nitroaniline 07/05/2011 11:581.16 mg/Kg-dry 1NDNELAP 69346
4,6-Dinitro-2-methylphenol 07/05/2011 11:581.16 mg/Kg-dry 1NDNELAP 69346
4-Bromophenyl phenyl ether 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
4-Chloro-3-methylphenol 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
4-Chloroaniline 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
4-Chlorophenyl phenyl ether 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
4-Nitroaniline 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
4-Nitrophenol 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
Aniline 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
Azobenzene 07/05/2011 11:580.406 mg/Kg-dry 1ND 69346
Benzidine 07/05/2011 11:581.23 mg/Kg-dry 1See noteNELAP 69346
Benzoic acid 07/05/2011 11:581.74 mg/Kg-dry 1NDNELAP 69346
Benzyl alcohol 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
Bis(2-chloroethoxy)methane 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
Bis(2-chloroethyl)ether 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
Bis(2-chloroisopropyl)ether 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
Butyl benzyl phthalate 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
Carbazole 07/05/2011 11:580.580 mg/Kg-dry 1ND 69346
Dibenzofuran 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
Diethyl phthalate 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
Dimethyl phthalate 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
Di-n-butyl phthalate 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
Di-n-octyl phthalate 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
Hexachlorobenzene 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
Hexachlorobutadiene 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
Hexachlorocyclopentadiene 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
Hexachloroethane 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
Isophorone 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
m,p-Cresol 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
Nitrobenzene 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
N-Nitrosodimethylamine 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
N-Nitroso-di-n-propylamine 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
N-Nitrosodiphenylamine 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
o-Cresol 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
Pentachlorophenol 07/05/2011 11:582.32 mg/Kg-dry 1NDNELAP 69346
Phenol 07/05/2011 11:580.406 mg/Kg-dry 1NDNELAP 69346
Pyridine 07/05/2011 11:580.580 mg/Kg-dry 1NDNELAP 69346
1,2-Diphenylhydrazine 07/05/2011 11:580.975 mg/Kg-dry 1ND 69346
Surr: 2,4,6-Tribromophenol 07/05/2011 11:5832.7-130 %REC 186.4 69346
Surr: 2-Fluorobiphenyl 07/05/2011 11:5834.1-116 %REC 180.5 69346
Surr: 2-Fluorophenol 07/05/2011 11:5830.5-99 %REC 175.3 69346
Surr: Nitrobenzene-d5 07/05/2011 11:5834.1-101 %REC 183.9 69346
Page 31 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 11:00
Lab ID: 11070042-005 Client Sample ID: SBA-A5-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: Phenol-d5 07/05/2011 11:5834.9-110 %REC 175.2 69346
Surr: p-Terphenyl-d14 07/05/2011 11:5841.7-124 %REC 199.2 69346
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.LCS was outside upper QC limits. Sample was ND.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,1,1-Trichloroethane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,1,2,2-Tetrachloroethane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,1,2-Trichloro-1,2,2-trifluoroethane 07/05/2011 14:254.3 µg/Kg-dry 1ND 69368
1,1,2-Trichloroethane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,1-Dichloro-2-propanone 07/05/2011 14:2543.0 µg/Kg-dry 1ND 69368
1,1-Dichloroethane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,1-Dichloroethene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,1-Dichloropropene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,2,3-Trichlorobenzene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,2,3-Trichloropropane 07/05/2011 14:258.6 µg/Kg-dry 1NDNELAP 69368
1,2,3-Trimethylbenzene 07/05/2011 14:254.3 µg/Kg-dry 1ND 69368
1,2,4-Trichlorobenzene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,2,4-Trimethylbenzene J 07/05/2011 14:254.3 µg/Kg-dry 14.0NELAP 69368
1,2-Dibromo-3-chloropropane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,2-Dibromoethane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,2-Dichlorobenzene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,2-Dichloroethane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,2-Dichloropropane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,3,5-Trimethylbenzene J 07/05/2011 14:254.3 µg/Kg-dry 11.1NELAP 69368
1,3-Dichlorobenzene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,3-Dichloropropane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1,4-Dichlorobenzene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
1-Chlorobutane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
2,2-Dichloropropane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
2-Butanone 07/05/2011 14:2543.0 µg/Kg-dry 1NDNELAP 69368
2-Chlorotoluene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
2-Hexanone 07/05/2011 14:2543.0 µg/Kg-dry 1NDNELAP 69368
2-Nitropropane 07/05/2011 14:2543.0 µg/Kg-dry 1NDNELAP 69368
4-Chlorotoluene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
4-Methyl-2-pentanone 07/05/2011 14:2543.0 µg/Kg-dry 1NDNELAP 69368
Acetone J 07/05/2011 14:2543.0 µg/Kg-dry 113NELAP 69368
Acrolein 07/05/2011 14:2586.0 µg/Kg-dry 1NDNELAP 69368
Acrylonitrile 07/05/2011 14:258.6 µg/Kg-dry 1NDNELAP 69368
Allyl chloride 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Benzene 07/05/2011 14:250.9 µg/Kg-dry 11.2NELAP 69368
Bromobenzene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Bromochloromethane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Bromodichloromethane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Bromoform 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Bromomethane 07/05/2011 14:258.6 µg/Kg-dry 1NDNELAP 69368
Carbon disulfide 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Page 32 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 11:00
Lab ID: 11070042-005 Client Sample ID: SBA-A5-01 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSCarbon tetrachloride 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Chlorobenzene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Chloroethane 07/05/2011 14:258.6 µg/Kg-dry 1NDNELAP 69368
Chloroform 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Chloromethane 07/05/2011 14:258.6 µg/Kg-dry 1NDNELAP 69368
cis-1,2-Dichloroethene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
cis-1,3-Dichloropropene 07/05/2011 14:253.4 µg/Kg-dry 1NDNELAP 69368
Cyclohexanone 07/05/2011 14:2586.0 µg/Kg-dry 1ND 69368
Dibromochloromethane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Dibromomethane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Dichlorodifluoromethane 07/05/2011 14:258.6 µg/Kg-dry 1NDNELAP 69368
Ethyl acetate 07/05/2011 14:2543.0 µg/Kg-dry 1NDNELAP 69368
Ethyl ether 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Ethyl methacrylate 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Ethylbenzene J 07/05/2011 14:254.3 µg/Kg-dry 10.9NELAP 69368
Heptane 07/05/2011 14:2517.2 µg/Kg-dry 1ND 69368
Hexachlorobutadiene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Hexachloroethane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Iodomethane 07/05/2011 14:258.6 µg/Kg-dry 1NDNELAP 69368
Isopropylbenzene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
m,p-Xylenes J 07/05/2011 14:254.3 µg/Kg-dry 11.8NELAP 69368
Methacrylonitrile 07/05/2011 14:2543.0 µg/Kg-dry 1NDNELAP 69368
Methyl Methacrylate 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Methyl tert-butyl ether 07/05/2011 14:251.7 µg/Kg-dry 1NDNELAP 69368
Methylacrylate 07/05/2011 14:258.6 µg/Kg-dry 1ND 69368
Methylene chloride J 07/05/2011 14:254.3 µg/Kg-dry 11.2NELAP 69368
Naphthalene J 07/05/2011 14:258.6 µg/Kg-dry 13.6NELAP 69368
n-Butylbenzene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
n-Hexane 07/05/2011 14:2517.2 µg/Kg-dry 1ND 69368
Nitrobenzene 07/05/2011 14:2586.0 µg/Kg-dry 1NDNELAP 69368
n-Propylbenzene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
o-Xylene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Pentachloroethane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
p-Isopropyltoluene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Propionitrile 07/05/2011 14:2543.0 µg/Kg-dry 1NDNELAP 69368
sec-Butylbenzene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Styrene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
tert-Butylbenzene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Tetrachloroethene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Tetrahydrofuran 07/05/2011 14:2543.0 µg/Kg-dry 1NDNELAP 69368
Toluene J 07/05/2011 14:254.3 µg/Kg-dry 12.6NELAP 69368
trans-1,2-Dichloroethene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
trans-1,3-Dichloropropene 07/05/2011 14:253.4 µg/Kg-dry 1NDNELAP 69368
Trichloroethene 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Trichlorofluoromethane 07/05/2011 14:254.3 µg/Kg-dry 1NDNELAP 69368
Vinyl acetate 07/05/2011 14:2543.0 µg/Kg-dry 1NDNELAP 69368
Vinyl chloride 07/05/2011 14:251.7 µg/Kg-dry 1NDNELAP 69368
Page 33 of 58
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 11:00
Lab ID: 11070042-005 Client Sample ID: SBA-A5-01 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: 1,2-Dichloroethane-d4 07/05/2011 14:2572.2-131 %REC 1110.5 69368
Surr: 4-Bromofluorobenzene 07/05/2011 14:2582.1-116 %REC 184.3 69368
Surr: Dibromofluoromethane 07/05/2011 14:2577.7-120 %REC 1101.1 69368
Surr: Toluene-d8 07/05/2011 14:2586-116 %REC 1112.3 69368
Surrogate and/or internal standard recovery was outside QC limits due to matrix interference.Marginal Exceedance for trichloroethene in LCS is verified per Volume 1 Module 4 section 1.7.4.2 of the 2009 TNI standard.
SW-846 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 07/11/2011 20:520.05 mg/Kg-dry 1NDNELAP R151875
2,4,5-TP (Silvex) 07/11/2011 20:520.05 mg/Kg-dry 1NDNELAP R151875
2,4-D 07/11/2011 20:520.05 mg/Kg-dry 1NDNELAP R151875
2,4-DB 07/11/2011 20:520.05 mg/Kg-dry 1NDNELAP R151875
3,5-Dichlorobenzoic Acid 07/11/2011 20:520.05 mg/Kg-dry 1NDNELAP R151875
Acifluorfen 07/11/2011 20:520.05 mg/Kg-dry 1NDNELAP R151875
Bentazon 07/11/2011 20:520.05 mg/Kg-dry 1NDNELAP R151875
Chloramben 07/11/2011 20:520.05 mg/Kg-dry 1NDNELAP R151875
Dalapon 07/11/2011 20:520.05 mg/Kg-dry 1NDNELAP R151875
DCPA 07/11/2011 20:520.05 mg/Kg-dry 1NDNELAP R151875
Dicamba 07/11/2011 20:520.05 mg/Kg-dry 1NDNELAP R151875
Dichlorprop 07/11/2011 20:520.05 mg/Kg-dry 1NDNELAP R151875
Dinoseb 07/11/2011 20:520.05 mg/Kg-dry 1NDNELAP R151875
Pentachlorophenol 07/11/2011 20:520.05 mg/Kg-dry 1NDNELAP R151875
Picloram 07/11/2011 20:050.05 mg/Kg-dry 1NDNELAP R151875
Surr: DCAA 07/11/2011 20:5224-140 %REC 141.9 R151875
The blank spike recovery and/or blank spike duplicate recovery were outside the established acceptance limits for 3,5-Dichlorobenzoic Acid and 2,4,5-T. Batch was accepted based on acceptable MS/MSD/RPD results.
Page 34 of 58
Lab Sample ID Client Sample ID Collection DateFractions
TeklabHdrP
Matrix
Sample Summary
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
11070042-001 SBA-C3-01 (5-6) 06/29/2011 16:006Solid
11070042-002 SBA-B4-01 (5-6) 06/30/2011 8:006Solid
11070042-003 SBA-D5-01 (5-6) 06/30/2011 9:006Solid
11070042-004 SBA-A3-01 (5-6) 06/30/2011 10:006Solid
11070042-005 SBA-A5-01 (5-6) 06/30/2011 11:006Solid
Page 35 of 58
Analysis Date/TimeTest Name Prep Date/Time
____TeklabHdrP
Sample ID Client Sample ID Collection Date Received Date
Dates Report
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
11070042-001A SBA-C3-01 (5-6) 06/29/2011 16:00 7/1/2011 3:50:00 PM
EPA SW846 3550C, 5035A, ASTM D2974 07/01/2011 16:00
Standard Methods 18th Ed. 2540 G 07/01/2011 16:00
SW-846 3050B, 6010B, Metals by ICP 07/05/2011 12:2507/01/2011 20:08
SW-846 3050B, Metals by GFAA 07/05/2011 11:5507/01/2011 19:57
SW-846 7471A 07/05/2011 12:2207/05/2011 8:45
SW-846 9012A (Total) 07/02/2011 12:17
11070042-001B SBA-C3-01 (5-6) 06/29/2011 16:00 7/1/2011 3:50:00 PM
SW-846 3550B, 8015B, Total Petroleum Hydrocarbons (OA-2) by GC/FID 07/04/2011 12:4207/01/2011 17:42
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/05/2011 23:0607/01/2011 18:31
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD 07/05/2011 10:2507/01/2011 18:31
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS 07/05/2011 9:2807/01/2011 19:51
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS 07/05/2011 15:1007/01/2011 19:47
11070042-001C SBA-C3-01 (5-6) 06/29/2011 16:00 7/1/2011 3:50:00 PM
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/11/2011 16:55
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/11/2011 17:42
11070042-001F SBA-C3-01 (5-6) 06/29/2011 16:00 7/1/2011 3:50:00 PM
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS 07/05/2011 11:51
11070042-002A SBA-B4-01 (5-6) 06/30/2011 8:00 7/1/2011 3:50:00 PM
EPA SW846 3550C, 5035A, ASTM D2974 07/01/2011 16:00
Standard Methods 18th Ed. 2540 G 07/01/2011 16:00
SW-846 3050B, 6010B, Metals by ICP 07/05/2011 12:4207/01/2011 19:54
SW-846 3050B, Metals by GFAA 07/05/2011 11:5807/01/2011 19:57
SW-846 7471A 07/05/2011 12:2207/05/2011 8:45
SW-846 9012A (Total) 07/02/2011 12:17
11070042-002B SBA-B4-01 (5-6) 06/30/2011 8:00 7/1/2011 3:50:00 PM
SW-846 3550B, 8015B, Total Petroleum Hydrocarbons (OA-2) by GC/FID 07/04/2011 13:0007/01/2011 17:42
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/05/2011 23:3007/01/2011 18:31
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD 07/05/2011 11:2307/01/2011 18:31
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS 07/05/2011 10:0307/01/2011 19:51
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS 07/05/2011 13:2707/01/2011 19:47
11070042-002C SBA-B4-01 (5-6) 06/30/2011 8:00 7/1/2011 3:50:00 PM
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/11/2011 17:42
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/11/2011 18:30
11070042-002F SBA-B4-01 (5-6) 06/30/2011 8:00 7/1/2011 3:50:00 PM
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS 07/05/2011 12:24
Page 36 of 58
Analysis Date/TimeTest Name Prep Date/Time
____TeklabHdrP
Sample ID Client Sample ID Collection Date Received Date
Dates Report
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
11070042-003A SBA-D5-01 (5-6) 06/30/2011 9:00 7/1/2011 3:50:00 PM
EPA SW846 3550C, 5035A, ASTM D2974 07/01/2011 16:00
Standard Methods 18th Ed. 2540 G 07/01/2011 16:00
SW-846 3050B, 6010B, Metals by ICP 07/05/2011 12:4807/01/2011 19:54
SW-846 3050B, Metals by GFAA 07/05/2011 12:0107/01/2011 19:57
SW-846 7471A 07/05/2011 12:2207/05/2011 8:45
SW-846 9012A (Total) 07/02/2011 12:17
11070042-003B SBA-D5-01 (5-6) 06/30/2011 9:00 7/1/2011 3:50:00 PM
SW-846 3550B, 8015B, Total Petroleum Hydrocarbons (OA-2) by GC/FID 07/04/2011 13:1707/01/2011 17:42
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/06/2011 0:4407/01/2011 18:31
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD 07/05/2011 11:4207/01/2011 18:31
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS 07/05/2011 10:3907/01/2011 19:51
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS 07/05/2011 12:3007/01/2011 19:47
11070042-003C SBA-D5-01 (5-6) 06/30/2011 9:00 7/1/2011 3:50:00 PM
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/11/2011 18:30
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/11/2011 19:17
11070042-003F SBA-D5-01 (5-6) 06/30/2011 9:00 7/1/2011 3:50:00 PM
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS 07/05/2011 12:54
11070042-004A SBA-A3-01 (5-6) 06/30/2011 10:00 7/1/2011 3:50:00 PM
EPA SW846 3550C, 5035A, ASTM D2974 07/01/2011 16:00
Standard Methods 18th Ed. 2540 G 07/01/2011 16:00
SW-846 3050B, 6010B, Metals by ICP 07/05/2011 12:5407/01/2011 19:54
SW-846 3050B, Metals by GFAA 07/05/2011 12:0507/01/2011 19:57
SW-846 7471A 07/05/2011 12:2207/05/2011 8:45
SW-846 9012A (Total) 07/02/2011 12:17
11070042-004B SBA-A3-01 (5-6) 06/30/2011 10:00 7/1/2011 3:50:00 PM
SW-846 3550B, 8015B, Total Petroleum Hydrocarbons (OA-2) by GC/FID 07/04/2011 13:3507/01/2011 17:42
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/06/2011 1:0807/01/2011 18:31
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD 07/05/2011 12:0107/01/2011 18:31
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS 07/05/2011 11:1507/01/2011 19:51
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS 07/05/2011 12:5407/01/2011 19:47
11070042-004C SBA-A3-01 (5-6) 06/30/2011 10:00 7/1/2011 3:50:00 PM
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/11/2011 19:17
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/11/2011 20:05
11070042-004F SBA-A3-01 (5-6) 06/30/2011 10:00 7/1/2011 3:50:00 PM
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS 07/05/2011 13:22
Page 37 of 58
Analysis Date/TimeTest Name Prep Date/Time
____TeklabHdrP
Sample ID Client Sample ID Collection Date Received Date
Dates Report
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
11070042-005A SBA-A5-01 (5-6) 06/30/2011 11:00 7/1/2011 3:50:00 PM
EPA SW846 3550C, 5035A, ASTM D2974 07/01/2011 16:00
Standard Methods 18th Ed. 2540 G 07/01/2011 16:00
SW-846 3050B, 6010B, Metals by ICP 07/05/2011 13:0007/01/2011 19:54
SW-846 3050B, Metals by GFAA 07/05/2011 12:1507/01/2011 19:57
SW-846 7471A 07/05/2011 12:2207/05/2011 8:45
SW-846 9012A (Total) 07/02/2011 12:17
11070042-005B SBA-A5-01 (5-6) 06/30/2011 11:00 7/1/2011 3:50:00 PM
SW-846 3550B, 8015B, Total Petroleum Hydrocarbons (OA-2) by GC/FID 07/04/2011 13:5207/01/2011 17:42
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/06/2011 1:3307/01/2011 18:31
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD 07/05/2011 12:2107/01/2011 18:31
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS 07/05/2011 13:0307/01/2011 19:51
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS 07/05/2011 11:5807/01/2011 19:47
11070042-005C SBA-A5-01 (5-6) 06/30/2011 11:00 7/1/2011 3:50:00 PM
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/11/2011 20:05
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/11/2011 20:52
11070042-005F SBA-A5-01 (5-6) 06/30/2011 11:00 7/1/2011 3:50:00 PM
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS 07/05/2011 14:25
Page 38 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
STANDARD METHODS 18TH ED. 2540 G
SampID: LCS-R151526
SampType: LCS %UnitsR151526Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Total Solids 07/01/20110.1 1.01.0 1000 90 110
SampID: LCSQC-R151526
SampType: LCSQC %UnitsR151526Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Total Solids 07/01/20110.1 1.01.0 1000 90 110
SampID: 11070042-001ADUP
SampType: DUP %UnitsR151526Batch RPD Limit 15
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Total Solids 07/01/20110.1 80.0 0.7779.38
SW-846 9012A (TOTAL)
SampID: MB-R151533
SampType: MBLK mg/KgUnitsR151533Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Cyanide 07/02/20110.01 < 0.01
SampID: LCS-R151533
SampType: LCS mg/KgUnitsR151533Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Cyanide 07/02/20110.01 0.020.02 99.20 85 115
SampID: 11070042-005AMS
SampType: MS mg/Kg-dryUnitsR151533Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Cyanide 07/02/20110.63 1.461.10 75.60 75 125
SampID: 11070042-005AMSD
SampType: MSD mg/Kg-dryUnitsR151533Batch RPD Limit 15
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Cyanide R 07/02/20110.58 1.461.39 95.4 23.140 1.105
SampID: MB-R151616
SampType: MBLK mg/KgUnitsR151616Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Cyanide 07/06/20110.01 < 0.01
SampID: LCS-R151616
SampType: LCS mg/KgUnitsR151616Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Cyanide 07/06/20110.01 0.020.02 86.40 85 115
Page 39 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 9012A (TOTAL)
SampID: LCS-R151616
SampType: LCS mg/KgUnitsR151616Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
SW-846 3050B, 6010B, METALS BY ICP
SampID: MB-69348
SampType: MBLK mg/Kg-dryUnits69348Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Arsenic 07/05/20112.50 2.50< 2.50 00 -100 100
Barium 07/05/20110.50 0.50< 0.50 00 -100 100
Cadmium 07/05/20110.20 0.20< 0.20 00 -100 100
Chromium 07/05/20111.00 1.00< 1.00 00 -100 100
Lead 07/05/20114.00 4.00< 4.00 00 -100 100
Silver 07/05/20110.55 0.55< 0.55 00 -100 100
SampID: LCS-69348
SampType: LCS mg/Kg-dryUnits69348Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Arsenic 07/05/20112.50 200195 97.60 85 115
Barium 07/05/20110.50 200194 97.00 85 115
Cadmium 07/05/20110.20 5.004.90 98.00 85 115
Chromium 07/05/20111.00 20.019.7 98.50 85 115
Lead 07/05/20114.00 50.049.4 98.70 85 115
Silver 07/05/20110.55 5.004.95 99.00 85 115
SampID: 11070042-001AMS
SampType: MS mg/Kg-dryUnits69348Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Arsenic 07/05/20112.50 200207 97.711.30 75 125
Barium 07/05/20110.50 200324 96.7130.2 75 125
Cadmium 07/05/20110.20 5.005.00 95.20.2400 75 125
Chromium 07/05/20111.00 20.045.5 111.523.20 75 125
Lead 07/05/20114.00 50.068.2 95.720.36 75 125
Silver 07/05/20110.55 5.004.79 95.80 75 125
SampID: 11070042-001AMSD
SampType: MSD mg/Kg-dryUnits69348Batch RPD Limit 20
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Arsenic 07/05/20112.50 200209 98.8 1.1511.30 206.6
Barium 07/05/20110.50 200318 94.1 1.65130.2 323.6
Cadmium 07/05/20110.20 5.005.06 96.4 1.190.2400 5.000
Chromium 07/05/20111.00 20.044.8 107.9 1.6023.20 45.50
Lead 07/05/20114.00 50.068.0 95.3 0.2620.36 68.19
Silver 07/05/20110.55 5.004.87 97.4 1.660 4.790
SW-846 3050B, METALS BY GFAA
Page 40 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 3050B, METALS BY GFAA
SampID: MB-69349
SampType: MBLK mg/Kg-dryUnits69349Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Selenium 7740 07/05/20110.600 0.600< 0.600 00 -100 100
SampID: LCS-69349
SampType: LCS mg/Kg-dryUnits69349Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Selenium 7740 07/05/20110.600 3.003.16 105.40 80 120
SampID: 11070042-004AMS
SampType: MS mg/Kg-dryUnits69349Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Selenium 7740 07/05/20110.588 2.942.86 97.10 70 130
SampID: 11070042-004AMSD
SampType: MSD mg/Kg-dryUnits69349Batch RPD Limit 20
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Selenium 7740 07/05/20110.588 2.942.72 92.5 4.820 2.856
SW-846 7471A
SampID: MB-69355
SampType: MBLK mg/KgUnits69355Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Mercury 07/05/20110.010 0.010< 0.010 00 -100 100
SampID: LCS-69355
SampType: LCS mg/KgUnits69355Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Mercury 07/05/20110.010 0.2500.272 109.00 85 115
SampID: 11070042-001AMS
SampType: MS mg/Kg-dryUnits69355Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Mercury 07/05/20110.012 0.3000.367 114.40.02400 75 125
SampID: 11070042-001AMSD
SampType: MSD mg/Kg-dryUnits69355Batch RPD Limit 15
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Mercury 07/05/20110.012 0.3000.361 112.2 1.810.02400 0.3671
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FID
Page 41 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FID
SampID: MB-69330
SampType: MBLK mg/KgUnits69330Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Diesel 07/04/20115.00 NDKerosene 07/04/20115.00 NDMineral Spirits 07/04/20115.00 NDMotor Oil 07/04/20115.00 ND Surr: n-Tetracontane 07/04/20110.670.50 74.3 54.8 128
SampID: LCS-69330
SampType: LCS mg/KgUnits69330Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Diesel 07/04/20115.00 16.714.4 86.40 40.4 121
Surr: n-Tetracontane 07/04/20110.670.53 79.0 54.8 128
SampID: 11070042-005BMS
SampType: MS mg/Kg-dryUnits69330Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Diesel 07/04/20115.82 19.418.0 92.70 20.3 167
Surr: n-Tetracontane 07/04/20110.780.59 75.2 53.9 153
SampID: 11070042-005BMSD
SampType: MSD mg/Kg-dryUnits69330Batch RPD Limit 34
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Diesel 07/04/20115.84 19.519.6 100.3 8.170 18.03
Surr: n-Tetracontane 07/04/20110.780.55 70.6
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD
SampID: MB-69344
SampType: MBLK µg/KgUnits69344Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
4,4´-DDD 07/05/20111.67 ND4,4´-DDE 07/05/20111.67 ND4,4´-DDT 07/05/20111.67 NDAlachlor 07/05/20111.67 NDAldrin 07/05/20111.67 NDalpha-BHC 07/05/20111.67 NDalpha-Chlordane 07/05/20111.67 NDbeta-BHC 07/05/20111.67 NDdelta-BHC 07/05/20111.67 NDDieldrin 07/05/20111.67 NDEndosulfan I 07/05/20111.67 NDEndosulfan II 07/05/20111.67 NDEndosulfan sulfate 07/05/20111.67 NDEndrin 07/05/20111.67 NDEndrin aldehyde 07/05/20111.67 NDEndrin ketone 07/05/20111.67 NDgamma-BHC 07/05/20111.67 ND
Page 42 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD
SampID: MB-69344
SampType: MBLK µg/KgUnits69344Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
gamma-Chlordane 07/05/20111.67 NDHeptachlor 07/05/20111.67 NDHeptachlor epoxide 07/05/20111.67 NDMethoxychlor 07/05/20111.67 ND Surr: Decachlorobiphenyl 07/05/20118.339.10 109.3 73.5 150
Surr: Tetrachloro-m-xylene 07/05/20118.335.33 64.0 14.4 113
SampID: LCSPST-69344
SampType: LCS µg/KgUnits69344Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
4,4´-DDD 07/05/20111.67 8.336.94 83.30 36 208
4,4´-DDE 07/05/20111.67 8.336.54 78.50 26 191
4,4´-DDT 07/05/20111.67 8.337.20 86.50 3 215
Alachlor 07/05/20111.67 8.339.53 114.50 30 170
Aldrin 07/05/20111.67 8.335.40 64.80 46 173
alpha-BHC 07/05/20111.67 8.335.09 61.10 37 179
alpha-Chlordane 07/05/20111.67 8.336.64 79.70 38 187
beta-BHC 07/05/20111.67 8.336.63 79.60 51 185
delta-BHC 07/05/20111.67 8.336.85 82.20 46 166
Dieldrin 07/05/20111.67 8.336.48 77.80 26 216
Endosulfan I 07/05/20111.67 8.336.37 76.50 31 205
Endosulfan II 07/05/20111.67 8.338.19 98.30 42 187
Endosulfan sulfate 07/05/20111.67 8.337.98 95.90 29 230
Endrin 07/05/20111.67 8.337.30 87.60 30 215
Endrin aldehyde 07/05/20111.67 8.337.55 90.70 42 202
Endrin ketone 07/05/20111.67 8.337.50 90.00 19 244
gamma-BHC 07/05/20111.67 8.335.26 63.20 55 166
gamma-Chlordane 07/05/20111.67 8.336.07 72.80 23 186
Heptachlor 07/05/20111.67 8.335.97 71.60 43 172
Heptachlor epoxide 07/05/20111.67 8.335.96 71.60 39 204
Methoxychlor 07/05/20111.67 8.338.76 105.10 3 221
Surr: Decachlorobiphenyl 07/05/20118.338.06 96.8 50.4 176
Surr: Tetrachloro-m-xylene 07/05/20118.334.33 51.9 10 107
SampID: 11070042-002BMS
SampType: MS µg/Kg-dryUnits69344Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
4,4´-DDD 07/05/20112.01 10.08.69 86.60 36 208
4,4´-DDE 07/05/20112.01 10.08.07 80.40 26 191
4,4´-DDT 07/05/20112.01 10.08.34 72.81.027 3 215
Alachlor 07/05/20112.01 10.010.8 107.50 30 170
Aldrin 07/05/20112.01 10.07.28 72.60 46 173
alpha-BHC 07/05/20112.01 10.07.28 72.60 37 179
alpha-Chlordane 07/05/20112.01 10.08.12 80.90 38 187
beta-BHC 07/05/20112.01 10.08.53 85.00 51 185
delta-BHC 07/05/20112.01 10.08.48 84.50 46 166
Page 43 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD
SampID: 11070042-002BMS
SampType: MS µg/Kg-dryUnits69344Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Dieldrin S 07/05/20112.01 10.019.2 -45.323.73 26 216
Endosulfan I 07/05/20112.01 10.07.06 70.30 31 205
Endosulfan II 07/05/20112.01 10.09.57 95.40 42 187
Endosulfan sulfate 07/05/20112.01 10.08.49 84.60 29 230
Endrin 07/05/20112.01 10.09.28 92.40 30 215
Endrin aldehyde 07/05/20112.01 10.09.14 91.10 42 202
Endrin ketone 07/05/20112.01 10.08.83 88.00 19 244
gamma-BHC 07/05/20112.01 10.07.36 73.30 55 166
gamma-Chlordane 07/05/20112.01 10.07.24 72.20 23 186
Heptachlor 07/05/20112.01 10.07.51 74.80 43 172
Heptachlor epoxide 07/05/20112.01 10.07.55 75.20 39 204
Methoxychlor 07/05/20112.01 10.09.71 96.70 3 221
Surr: Decachlorobiphenyl 07/05/201110.010.6 105.2 48 149
Surr: Tetrachloro-m-xylene 07/05/201110.07.28 72.5 19 145
SampID: 11070042-002BMSD
SampType: MSD µg/Kg-dryUnits69344Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
4,4´-DDD 07/06/20112.01 10.07.47 74.4 15.060 8.690
4,4´-DDE 07/06/20112.01 10.07.27 72.3 10.390 8.066
4,4´-DDT 07/06/20112.01 10.07.54 64.9 10.031.027 8.339
Alachlor 07/06/20112.01 10.09.78 97.3 9.910 10.80
Aldrin 07/06/20112.01 10.06.54 65.1 10.800 7.285
alpha-BHC 07/06/20112.01 10.06.32 62.9 14.160 7.283
alpha-Chlordane 07/06/20112.01 10.07.43 73.9 8.970 8.123
beta-BHC 07/06/20112.01 10.08.13 80.9 4.750 8.528
delta-BHC 07/06/20112.01 10.08.06 80.3 5.050 8.481
Dieldrin S 07/06/20112.01 10.026.3 25.9 31.4423.73 19.18
Endosulfan I 07/06/20112.01 10.06.83 68.0 3.260 7.057
Endosulfan II 07/06/20112.01 10.08.86 88.2 7.760 9.573
Endosulfan sulfate 07/06/20112.01 10.08.03 79.9 5.530 8.488
Endrin 07/06/20112.01 10.08.29 82.5 11.270 9.275
Endrin aldehyde 07/06/20112.01 10.08.48 84.4 7.480 9.143
Endrin ketone 07/06/20112.01 10.08.11 80.7 8.610 8.834
gamma-BHC 07/06/20112.01 10.06.39 63.6 14.100 7.356
gamma-Chlordane 07/06/20112.01 10.06.40 63.7 12.320 7.244
Heptachlor 07/06/20112.01 10.06.50 64.7 14.500 7.513
Heptachlor epoxide 07/06/20112.01 10.06.69 66.5 12.140 7.550
Methoxychlor 07/06/20112.01 10.08.81 87.7 9.740 9.711
Surr: Decachlorobiphenyl 07/06/201110.09.87 98.3
Surr: Tetrachloro-m-xylene 07/06/201110.06.29 62.6
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECD
Page 44 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECD
SampID: MB-69344
SampType: MBLK µg/KgUnits69344Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Aroclor 1016 07/05/201137.5 NDAroclor 1221 07/05/201137.5 NDAroclor 1232 07/05/201137.5 NDAroclor 1242 07/05/201137.5 NDAroclor 1248 07/05/201137.5 NDAroclor 1254 07/05/201137.5 NDAroclor 1260 07/05/201137.5 ND Surr: Decachlorobiphenyl 07/05/20118.38.4 101.6 86.4 159
Surr: Tetrachloro-meta-xylene 07/05/20118.34.7 56.2 31.6 114
SampID: LCSPCB-69344
SampType: LCS µg/KgUnits69344Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Aroclor 1016 07/05/201137.5 167118 70.70 54.9 121
Aroclor 1260 07/05/201137.5 167143 86.10 65.5 133
Surr: Decachlorobiphenyl 07/05/20118.38.3 100.2 86.4 159
Surr: Tetrachloro-meta-xylene 07/05/20118.35.8 70.4 31.6 114
SampID: 11070042-001BMS
SampType: MS µg/Kg-dryUnits69344Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Aroclor 1016 07/05/201147.1 209168 80.10 35.8 143
Aroclor 1260 07/05/201147.1 209181 86.20 22.3 152
Surr: Decachlorobiphenyl 07/05/201110.410.5 100.4 5 156
Surr: Tetrachloro-meta-xylene 07/05/201110.46.6 63.6 7.35 123
SampID: 11070042-001BMSD
SampType: MSD µg/Kg-dryUnits69344Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Aroclor 1016 07/05/201147.2 210163 77.9 2.640 167.6
Aroclor 1260 07/05/201147.2 210176 84.1 2.360 180.5
Surr: Decachlorobiphenyl 07/05/201110.410 96.3
Surr: Tetrachloro-meta-xylene 07/05/201110.46.0 57.1
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MB-69347
SampType: MBLK mg/KgUnits69347Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Acenaphthene 07/05/20110.003 NDAcenaphthylene 07/05/20110.003 NDAnthracene 07/05/20110.003 NDBenzo(a)anthracene 07/05/20110.003 NDBenzo(a)pyrene 07/05/20110.003 NDBenzo(b)fluoranthene 07/05/20110.003 NDBenzo(g,h,i)perylene 07/05/20110.003 ND
Page 45 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MB-69347
SampType: MBLK mg/KgUnits69347Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Benzo(k)fluoranthene 07/05/20110.003 NDBis(2-ethylhexyl)phthalate 07/05/20110.067 NDChrysene 07/05/20110.003 NDDibenzo(a,h)anthracene 07/05/20110.003 NDFluoranthene 07/05/20110.003 NDFluorene 07/05/20110.003 NDIndeno(1,2,3-cd)pyrene 07/05/20110.003 NDNaphthalene 07/05/20110.003 NDPhenanthrene 07/05/20110.003 NDPyrene 07/05/20110.003 ND Surr: 2-Fluorobiphenyl 07/05/20110.1670.136 81.4 45.7 89.2
Surr: Nitrobenzene-d5 07/05/20110.1670.112 66.9 31.4 100
Surr: p-Terphenyl-d14 07/05/20110.1670.207 124.0 53.3 124
SampID: LCS-69347
SampType: LCS mg/KgUnits69347Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Acenaphthene 07/05/20110.003 0.1670.161 96.40 56.3 115
Acenaphthylene 07/05/20110.003 0.1670.163 97.80 60.3 143
Anthracene 07/05/20110.003 0.1670.128 76.60 52.1 109
Benzo(a)anthracene 07/05/20110.003 0.1670.148 88.40 52.8 112
Benzo(a)pyrene 07/05/20110.003 0.1670.152 90.80 40.8 127
Benzo(b)fluoranthene 07/05/20110.003 0.1670.168 100.60 50.1 150
Benzo(g,h,i)perylene 07/05/20110.003 0.1670.167 1000 52.8 145
Benzo(k)fluoranthene 07/05/20110.003 0.1670.172 102.80 52 153
Bis(2-ethylhexyl)phthalate 07/05/20110.067 0.1670.178 106.80 50 150
Chrysene 07/05/20110.003 0.1670.158 94.80 60.8 128
Dibenzo(a,h)anthracene 07/05/20110.003 0.1670.176 105.20 54.9 150
Fluoranthene 07/05/20110.003 0.1670.152 90.80 58.7 125
Fluorene 07/05/20110.003 0.1670.169 101.00 57.8 125
Indeno(1,2,3-cd)pyrene 07/05/20110.003 0.1670.173 103.60 52 147
Naphthalene 07/05/20110.003 0.1670.142 85.00 54.8 113
Phenanthrene 07/05/20110.003 0.1670.163 97.60 60.4 121
Pyrene 07/05/20110.003 0.1670.158 94.60 57.9 129
Surr: 2-Fluorobiphenyl 07/05/20110.1670.122 73.3 45.7 89.2
Surr: Nitrobenzene-d5 07/05/20110.1670.112 66.9 31.4 100
Surr: p-Terphenyl-d14 07/05/20110.1670.201 120.4 53.3 124
SampID: 11070042-004BMS
SampType: MS mg/Kg-dryUnits69347Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Acenaphthene 07/05/20110.004 0.1900.182 95.80 36 135
Acenaphthylene 07/05/20110.004 0.1900.186 98.00 17.2 167
Anthracene 07/05/20110.004 0.1900.149 78.20 39.3 124
Benzo(a)anthracene 07/05/20110.004 0.1900.170 87.40.004173 10 183
Benzo(a)pyrene 07/05/20110.004 0.1900.186 98.00 10 204
Page 46 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: 11070042-004BMS
SampType: MS mg/Kg-dryUnits69347Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Benzo(b)fluoranthene 07/05/20110.004 0.1900.196 103.00 10.6 178
Benzo(g,h,i)perylene 07/05/20110.004 0.1900.170 87.40.003794 10 168
Benzo(k)fluoranthene 07/05/20110.004 0.1900.192 101.00 27.6 181
Bis(2-ethylhexyl)phthalate 07/05/20110.076 0.1900.218 114.60 50 150
Chrysene 07/05/20110.004 0.1900.183 96.00 10 176
Dibenzo(a,h)anthracene 07/05/20110.004 0.1900.190 99.80 12.2 156
Fluoranthene 07/05/20110.004 0.1900.174 91.40 10 227
Fluorene 07/05/20110.004 0.1900.183 96.40 35.2 148
Indeno(1,2,3-cd)pyrene 07/05/20110.004 0.1900.185 97.40 10 164
Naphthalene 07/05/20110.004 0.1900.172 90.40 14.7 128
Phenanthrene 07/05/20110.004 0.1900.188 98.80 32.8 143
Pyrene 07/05/20110.004 0.1900.183 96.00 10 180
Surr: 2-Fluorobiphenyl 07/05/20110.1900.120 62.9 10 131
Surr: Nitrobenzene-d5 07/05/20110.1900.118 62.1 10 132
Surr: p-Terphenyl-d14 07/05/20110.1900.225 118.6 30.6 131
SampID: 11070042-004BMSD
SampType: MSD mg/Kg-dryUnits69347Batch RPD Limit 49.7
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Acenaphthene 07/05/20110.004 0.1900.178 93.8 2.470 0.1822
Acenaphthylene 07/05/20110.004 0.1900.178 93.8 4.730 0.1863
Anthracene 07/05/20110.004 0.1900.138 73.1 7.220 0.1488
Benzo(a)anthracene 07/05/20110.004 0.1900.162 83.2 5.150.004173 0.1704
Benzo(a)pyrene 07/05/20110.004 0.1900.184 97.2 1.180 0.1863
Benzo(b)fluoranthene 07/05/20110.004 0.1900.189 99.6 3.710 0.1958
Benzo(g,h,i)perylene 07/05/20110.004 0.1900.164 84.4 3.770.003794 0.1700
Benzo(k)fluoranthene 07/05/20110.004 0.1900.185 97.4 3.990 0.1920
Bis(2-ethylhexyl)phthalate 07/05/20110.076 0.1900.196 103.2 10.810 0.2178
Chrysene 07/05/20110.004 0.1900.175 92.2 4.390 0.1826
Dibenzo(a,h)anthracene 07/05/20110.004 0.1900.183 96.4 3.820 0.1898
Fluoranthene 07/05/20110.004 0.1900.161 85.2 7.370 0.1738
Fluorene 07/05/20110.004 0.1900.184 97.2 0.460 0.1833
Indeno(1,2,3-cd)pyrene 07/05/20110.004 0.1900.176 92.8 5.190 0.1852
Naphthalene 07/05/20110.004 0.1900.155 81.8 10.330 0.1719
Phenanthrene 07/05/20110.004 0.1900.177 93.2 6.190 0.1879
Pyrene 07/05/20110.004 0.1900.170 89.8 7.020 0.1826
Surr: 2-Fluorobiphenyl 07/05/20110.1900.115 60.9
Surr: Nitrobenzene-d5 07/05/20110.1900.108 57.1
Surr: p-Terphenyl-d14 07/05/20110.1900.210 111.0
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MB-69346
SampType: MBLK mg/KgUnits69346Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1,2,4-Trichlorobenzene 07/05/20110.500 ND1,2-Dichlorobenzene 07/05/20110.500 ND
Page 47 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MB-69346
SampType: MBLK mg/KgUnits69346Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1,3-Dichlorobenzene 07/05/20110.500 ND1,4-Dichlorobenzene 07/05/20110.500 ND2,4,5-Trichlorophenol 07/05/20110.350 ND2,4,6-Trichlorophenol 07/05/20110.350 ND2,4-Dichlorophenol 07/05/20110.500 ND2,4-Dimethylphenol 07/05/20110.500 ND2,4-Dinitrophenol 07/05/20111.00 ND2,4-Dinitrotoluene 07/05/20110.350 ND2,6-Dinitrotoluene 07/05/20110.350 ND2-Chloronaphthalene 07/05/20110.350 ND2-Chlorophenol 07/05/20110.500 ND2-Methoxy-4-methylphenol 07/05/20110.650 ND2-Methylnaphthalene 07/05/20110.350 ND2-Nitroaniline 07/05/20111.00 ND2-Nitrophenol 07/05/20110.350 ND3,3´-Dichlorobenzidine 07/05/20110.350 ND3-Nitroaniline 07/05/20111.00 ND4,6-Dinitro-2-methylphenol 07/05/20111.00 ND4-Bromophenyl phenyl ether 07/05/20110.350 ND4-Chloro-3-methylphenol 07/05/20110.500 ND4-Chloroaniline 07/05/20110.500 ND4-Chlorophenyl phenyl ether 07/05/20110.350 ND4-Nitroaniline 07/05/20110.500 ND4-Nitrophenol 07/05/20110.350 NDAniline 07/05/20110.500 NDAzobenzene 07/05/20110.350 NDBenzidine 07/05/20111.06 NDBenzoic acid 07/05/20111.50 NDBenzyl alcohol 07/05/20110.500 NDBis(2-chloroethoxy)methane 07/05/20110.350 NDBis(2-chloroethyl)ether 07/05/20110.500 NDBis(2-chloroisopropyl)ether 07/05/20110.350 NDButyl benzyl phthalate 07/05/20110.350 NDCarbazole 07/05/20110.500 NDDibenzofuran 07/05/20110.350 NDDiethyl phthalate 07/05/20110.500 NDDimethyl phthalate 07/05/20110.350 NDDi-n-butyl phthalate 07/05/20110.350 NDDi-n-octyl phthalate 07/05/20110.350 NDHexachlorobenzene 07/05/20110.350 NDHexachlorobutadiene 07/05/20110.500 NDHexachlorocyclopentadiene 07/05/20110.350 NDHexachloroethane 07/05/20110.500 NDIsophorone 07/05/20110.350 NDm,p-Cresol 07/05/20110.500 NDNitrobenzene 07/05/20110.500 NDN-Nitrosodimethylamine 07/05/20110.500 ND
Page 48 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MB-69346
SampType: MBLK mg/KgUnits69346Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
N-Nitroso-di-n-propylamine 07/05/20110.500 NDN-Nitrosodiphenylamine 07/05/20110.500 NDo-Cresol 07/05/20110.500 NDPentachlorophenol 07/05/20112.00 NDPhenol 07/05/20110.350 NDPyridine 07/05/20110.500 ND1,2-Diphenylhydrazine 07/05/20110.840 ND Surr: 2,4,6-Tribromophenol 07/05/20111.671.64 98.3 52.1 113
Surr: 2-Fluorobiphenyl 07/05/20110.8350.701 83.9 46.3 106
Surr: 2-Fluorophenol 07/05/20111.671.31 78.3 50.6 89
Surr: Nitrobenzene-d5 07/05/20110.8350.707 84.6 42.4 99.2
Surr: Phenol-d5 07/05/20111.671.30 78.1 55.9 98.5
Surr: p-Terphenyl-d14 07/05/20110.8350.891 106.7 45.5 115
SampID: LCS-69346
SampType: LCS mg/KgUnits69346Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1,2,4-Trichlorobenzene 07/05/20110.500 1.671.42 84.80 43.9 92.2
1,4-Dichlorobenzene 07/05/20110.500 1.671.35 80.80 43.8 84.1
2,4,5-Trichlorophenol 07/05/20110.350 3.332.98 89.60 38.6 123
2,4,6-Trichlorophenol 07/05/20110.350 3.332.93 88.00 35.9 123
2,4-Dimethylphenol 07/05/20110.500 3.332.54 76.20 38.3 88
2,4-Dinitrophenol 07/05/20111.00 3.334.11 123.60 1.88 162
2,4-Dinitrotoluene S 07/05/20110.350 1.672.03 121.80 48.6 102
2-Chlorophenol 07/05/20110.500 3.332.47 74.20 46.6 84
4-Chloro-3-methylphenol 07/05/20110.500 3.333.01 90.50 51.5 94.9
4-Nitrophenol S 07/05/20110.350 3.334.05 121.60 53.2 104
Diethyl phthalate 07/05/20110.500 3.333.24 97.20 51.7 106
Dimethyl phthalate 07/05/20110.350 3.332.97 89.20 58.8 104
Di-n-butyl phthalate 07/05/20110.350 1.671.70 101.90 54.3 105
Hexachlorobenzene 07/05/20110.350 3.333.03 91.00 55.9 106
Hexachlorobutadiene 07/05/20110.500 3.332.74 82.30 35.7 100
Hexachloroethane 07/05/20110.500 3.332.65 79.50 38.9 89.9
m,p-Cresol 07/05/20110.500 1.671.40 83.60 37.6 93.7
Nitrobenzene 07/05/20110.500 3.332.65 79.70 51.8 104
N-Nitroso-di-n-propylamine 07/05/20110.500 1.671.35 80.80 49.1 94.5
o-Cresol 07/05/20110.500 1.671.36 81.40 43 101
Pentachlorophenol 07/05/20112.00 3.333.22 96.80 42.2 102
Phenol 07/05/20110.350 3.332.53 75.80 41.6 81.3
Pyridine 07/05/20110.500 3.332.19 65.80 3.61 74.3
Surr: 2,4,6-Tribromophenol 07/05/20111.671.76 105.4 52.1 113
Surr: 2-Fluorobiphenyl 07/05/20110.8350.697 83.4 46.3 106
Surr: 2-Fluorophenol 07/05/20111.671.29 77.2 50.6 89
Surr: Nitrobenzene-d5 07/05/20110.8350.666 79.7 42.4 99.2
Surr: Phenol-d5 07/05/20111.671.27 76.0 55.9 98.5
Surr: p-Terphenyl-d14 07/05/20110.8350.854 102.3 45.5 115
Page 49 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: 11070042-003BMS
SampType: MS mg/Kg-dryUnits69346Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1,2,4-Trichlorobenzene 07/05/20110.585 1.961.48 75.60 35.9 102
1,4-Dichlorobenzene 07/05/20110.585 1.961.42 72.90 29.8 95.5
2,4,5-Trichlorophenol 07/05/20110.410 3.903.27 83.80 38.6 123
2,4,6-Trichlorophenol 07/05/20110.410 3.903.21 82.30 35.9 123
2,4-Dimethylphenol 07/05/20110.585 3.902.63 67.60 38.3 88
2,4-Dinitrophenol 07/05/20111.17 3.903.65 93.70 1.88 162
2,4-Dinitrotoluene 07/05/20110.410 1.962.08 106.50 37.5 107
2-Chlorophenol 07/05/20110.585 3.902.52 64.60 22.6 108
4-Chloro-3-methylphenol 07/05/20110.585 3.903.34 85.70 19.3 131
4-Nitrophenol 07/05/20110.410 3.904.51 115.70 27.6 123
Diethyl phthalate 07/05/20110.585 3.903.41 87.60 51.7 106
Dimethyl phthalate 07/05/20110.410 3.903.11 79.90 58.8 104
Di-n-butyl phthalate 07/05/20110.410 1.961.77 90.70 54.3 105
Hexachlorobenzene 07/05/20110.410 3.903.13 80.40 55.9 106
Hexachlorobutadiene 07/05/20110.585 3.902.93 75.20 35.7 100
Hexachloroethane 07/05/20110.585 3.902.79 71.60 38.9 89.9
m,p-Cresol 07/05/20110.585 1.961.54 78.50 37.6 93.7
Nitrobenzene 07/05/20110.585 3.902.78 71.20 51.8 104
N-Nitroso-di-n-propylamine 07/05/20110.585 1.961.40 71.60 45.5 99.1
o-Cresol 07/05/20110.585 1.961.46 74.90 43 101
Pentachlorophenol 07/05/20112.34 3.903.27 84.00 18.5 113
Phenol 07/05/20110.410 3.902.78 71.20 20.8 110
Pyridine 07/05/20110.585 3.902.21 56.60 3.61 74.3
Surr: 2,4,6-Tribromophenol 07/05/20111.961.96 100.4 32.7 130
Surr: 2-Fluorobiphenyl 07/05/20110.9770.665 68.1 34.1 116
Surr: 2-Fluorophenol 07/05/20111.961.42 72.7 30.5 99
Surr: Nitrobenzene-d5 07/05/20110.9770.719 73.6 34.1 101
Surr: Phenol-d5 07/05/20111.961.41 72.3 34.9 110
Surr: p-Terphenyl-d14 07/05/20110.9770.936 95.7 41.7 124
SampID: 11070042-003BMSD
SampType: MSD mg/Kg-dryUnits69346Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
1,2,4-Trichlorobenzene 07/05/20110.586 1.961.05 53.4 34.280 1.477
1,4-Dichlorobenzene 07/05/20110.586 1.960.996 50.9 35.410 1.425
2,4,5-Trichlorophenol 07/05/20110.410 3.902.43 62.3 29.220 3.266
2,4,6-Trichlorophenol 07/05/20110.410 3.902.44 62.5 27.210 3.206
2,4-Dimethylphenol 07/05/20110.586 3.902.12 54.4 21.510 2.633
2,4-Dinitrophenol 07/05/20111.17 3.902.60 66.5 33.810 3.653
2,4-Dinitrotoluene 07/05/20110.410 1.961.46 74.7 35.050 2.082
2-Chlorophenol 07/05/20110.586 3.901.85 47.4 30.530 2.518
4-Chloro-3-methylphenol 07/05/20110.586 3.902.50 64.1 28.650 3.341
4-Nitrophenol 07/05/20110.410 3.903.38 86.5 28.740 4.510
Diethyl phthalate 07/05/20110.586 3.902.51 64.4 30.310 3.413
Dimethyl phthalate S 07/05/20110.410 3.902.21 56.6 34.080 3.115
Di-n-butyl phthalate 07/05/20110.410 1.961.23 63.0 35.930 1.772
Hexachlorobenzene S 07/05/20110.410 3.902.14 54.9 37.610 3.134
Page 50 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: 11070042-003BMSD
SampType: MSD mg/Kg-dryUnits69346Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Hexachlorobutadiene 07/05/20110.586 3.901.99 50.9 38.480 2.932
Hexachloroethane 07/05/20110.586 3.901.93 49.6 36.190 2.789
m,p-Cresol 07/05/20110.586 1.961.14 58.5 29.150 1.535
Nitrobenzene S 07/05/20110.586 3.902.01 51.4 32.240 2.776
N-Nitroso-di-n-propylamine 07/05/20110.586 1.960.976 49.9 35.570 1.399
o-Cresol 07/05/20110.586 1.961.11 56.5 27.880 1.464
Pentachlorophenol 07/05/20112.34 3.902.51 64.3 26.480 3.275
Phenol 07/05/20110.410 3.902.09 53.5 28.350 2.777
Pyridine 07/05/20110.586 3.901.62 41.5 30.730 2.205
Surr: 2,4,6-Tribromophenol 07/05/20111.961.29 65.7
Surr: 2-Fluorobiphenyl 07/05/20110.9790.466 47.7
Surr: 2-Fluorophenol 07/05/20111.960.968 49.5
Surr: Nitrobenzene-d5 07/05/20110.9790.491 50.1
Surr: Phenol-d5 07/05/20111.960.992 50.7
Surr: p-Terphenyl-d14 07/05/20110.9790.657 67.1
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MBLK-A110705-1
SampType: MBLK µg/KgUnits69368Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1,1,1,2-Tetrachloroethane 07/05/20115.0 ND1,1,1-Trichloroethane 07/05/20115.0 ND1,1,2,2-Tetrachloroethane 07/05/20115.0 ND1,1,2-Trichloro-1,2,2-trifluoroethane 07/05/20115.0 ND1,1,2-Trichloroethane 07/05/20115.0 ND1,1-Dichloro-2-propanone 07/05/201150.0 ND1,1-Dichloroethane 07/05/20115.0 ND1,1-Dichloroethene 07/05/20115.0 ND1,1-Dichloropropene 07/05/20115.0 ND1,2,3-Trichlorobenzene 07/05/20115.0 ND1,2,3-Trichloropropane 07/05/201110 ND1,2,3-Trimethylbenzene 07/05/20115.0 ND1,2,4-Trichlorobenzene 07/05/20115.0 ND1,2,4-Trimethylbenzene 07/05/20115.0 ND1,2-Dibromo-3-chloropropane 07/05/20115.0 ND1,2-Dibromoethane 07/05/20115.0 ND1,2-Dichlorobenzene 07/05/20115.0 ND1,2-Dichloroethane 07/05/20115.0 ND1,2-Dichloropropane 07/05/20115.0 ND1,3,5-Trimethylbenzene 07/05/20115.0 ND1,3-Dichlorobenzene 07/05/20115.0 ND1,3-Dichloropropane 07/05/20115.0 ND1,4-Dichlorobenzene 07/05/20115.0 ND1-Chlorobutane 07/05/20115.0 ND2,2-Dichloropropane 07/05/20115.0 ND2-Butanone 07/05/201150.0 ND
Page 51 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MBLK-A110705-1
SampType: MBLK µg/KgUnits69368Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
2-Chlorotoluene 07/05/20115.0 ND2-Hexanone 07/05/201150.0 ND2-Nitropropane 07/05/201150.0 ND4-Chlorotoluene 07/05/20115.0 ND4-Methyl-2-pentanone 07/05/201150.0 NDAcetone 07/05/201150.0 NDAcrolein 07/05/2011100 NDAcrylonitrile 07/05/201110 NDAllyl chloride 07/05/20115.0 NDBenzene 07/05/20111.0 NDBromobenzene 07/05/20115.0 NDBromochloromethane 07/05/20115.0 NDBromodichloromethane 07/05/20115.0 NDBromoform 07/05/20115.0 NDBromomethane 07/05/201110 NDCarbon disulfide 07/05/20115.0 NDCarbon tetrachloride 07/05/20115.0 NDChlorobenzene 07/05/20115.0 NDChloroethane 07/05/201110 NDChloroform 07/05/20115.0 NDChloromethane 07/05/201110 NDcis-1,2-Dichloroethene 07/05/20115.0 NDcis-1,3-Dichloropropene 07/05/20114.0 NDCyclohexanone 07/05/2011100 NDDibromochloromethane 07/05/20115.0 NDDibromomethane 07/05/20115.0 NDDichlorodifluoromethane 07/05/201110 NDEthyl acetate 07/05/201150.0 NDEthyl ether 07/05/20115.0 NDEthyl methacrylate 07/05/20115.0 NDEthylbenzene 07/05/20115.0 NDHeptane 07/05/201120.0 NDHexachlorobutadiene 07/05/20115.0 NDHexachloroethane 07/05/20115.0 NDIodomethane 07/05/201110 NDIsopropylbenzene 07/05/20115.0 NDm,p-Xylenes 07/05/20115.0 NDMethacrylonitrile 07/05/201150.0 NDMethyl Methacrylate 07/05/20115.0 NDMethyl tert-butyl ether 07/05/20112.0 NDMethylacrylate 07/05/201110 NDMethylene chloride J 07/05/20115.0 2.2Naphthalene 07/05/201110 NDn-Butylbenzene 07/05/20115.0 NDn-Hexane 07/05/201120.0 NDNitrobenzene 07/05/2011100 NDn-Propylbenzene 07/05/20115.0 ND
Page 52 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MBLK-A110705-1
SampType: MBLK µg/KgUnits69368Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
o-Xylene 07/05/20115.0 NDPentachloroethane 07/05/20115.0 NDp-Isopropyltoluene 07/05/20115.0 NDPropionitrile 07/05/201150.0 NDsec-Butylbenzene 07/05/20115.0 NDStyrene 07/05/20115.0 NDtert-Butylbenzene 07/05/20115.0 NDTetrachloroethene 07/05/20115.0 NDTetrahydrofuran 07/05/201150.0 NDToluene 07/05/20115.0 NDtrans-1,2-Dichloroethene 07/05/20115.0 NDtrans-1,3-Dichloropropene 07/05/20114.0 NDTrichloroethene 07/05/20115.0 NDTrichlorofluoromethane 07/05/20115.0 NDVinyl acetate 07/05/201150.0 NDVinyl chloride 07/05/20112.0 ND Surr: 1,2-Dichloroethane-d4 07/05/201150.053.3 106.7 72.2 131
Surr: 4-Bromofluorobenzene 07/05/201150.051.8 103.5 82.1 116
Surr: Dibromofluoromethane 07/05/201150.050.7 101.3 77.7 120
Surr: Toluene-d8 07/05/201150.048.1 96.2 86 116
SampID: LCS-A110705-1
SampType: LCS µg/KgUnits69368Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1,1,1,2-Tetrachloroethane 07/05/20115.0 50.052.7 105.40 0 200
1,1,1-Trichloroethane 07/05/20115.0 50.055.0 109.90 85.6 124
1,1,2,2-Tetrachloroethane 07/05/20115.0 50.049.6 99.10 0 200
1,1,2-Trichloro-1,2,2-trifluoroethane 07/05/20115.0 50.057.6 115.10 0 200
1,1,2-Trichloroethane 07/05/20115.0 50.051.0 102.00 0 200
1,1-Dichloro-2-propanone 07/05/201150.0 125124 99.20 0 200
1,1-Dichloroethane 07/05/20115.0 50.053.6 107.20 0 200
1,1-Dichloroethene 07/05/20115.0 50.056.5 112.90 60.1 131
1,1-Dichloropropene 07/05/20115.0 50.054.9 109.70 0 200
1,2,3-Trichlorobenzene 07/05/20115.0 50.051.8 103.70 0 200
1,2,3-Trichloropropane 07/05/201110 50.048.7 97.40 0 200
1,2,3-Trimethylbenzene 07/05/20115.0 50.051.2 102.50 0 200
1,2,4-Trichlorobenzene 07/05/20115.0 50.053.7 107.40 0 200
1,2,4-Trimethylbenzene 07/05/20115.0 50.051.5 103.00 0 200
1,2-Dibromo-3-chloropropane 07/05/20115.0 50.049.1 98.30 0 200
1,2-Dibromoethane 07/05/20115.0 50.051.4 102.70 86.9 119
1,2-Dichlorobenzene 07/05/20115.0 50.052.2 104.30 88 119
1,2-Dichloroethane 07/05/20115.0 50.052.7 105.50 73 117
1,2-Dichloropropane 07/05/20115.0 50.053.4 106.90 0 200
1,3,5-Trimethylbenzene 07/05/20115.0 50.052.5 105.00 0 200
1,3-Dichlorobenzene 07/05/20115.0 50.054.7 109.40 85.8 125
1,3-Dichloropropane 07/05/20115.0 50.050.6 101.30 0 200
1,4-Dichlorobenzene 07/05/20115.0 50.053.8 107.50 84.5 124
Page 53 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCS-A110705-1
SampType: LCS µg/KgUnits69368Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1-Chlorobutane 07/05/20115.0 50.052.0 104.10 0 200
2,2-Dichloropropane 07/05/20115.0 50.053.9 107.90 0 200
2-Butanone 07/05/201150.0 125124 99.60 45.3 136
2-Chlorotoluene 07/05/20115.0 50.051.6 103.20 0 200
2-Hexanone 07/05/201150.0 125125 100.30 0 200
2-Nitropropane 07/05/201150.0 500550 109.90 0 200
4-Chlorotoluene 07/05/20115.0 50.052.5 105.00 0 200
4-Methyl-2-pentanone 07/05/201150.0 125123 98.70 0 200
Acetone 07/05/201150.0 125159 126.90 0 200
Acrylonitrile 07/05/201110 50.049.8 99.50 0 200
Allyl chloride 07/05/20115.0 50.052.4 104.70 0 200
Benzene 07/05/20111.0 50.051.4 102.90 73.9 109
Bromobenzene 07/05/20115.0 50.051.5 103.00 0 200
Bromochloromethane 07/05/20115.0 50.051.6 103.20 0 200
Bromodichloromethane 07/05/20115.0 50.054.1 108.20 91.3 126
Bromoform 07/05/20115.0 50.056.1 112.20 0 200
Bromomethane 07/05/201110 50.046.4 92.80 0 200
Carbon disulfide 07/05/20115.0 50.057.0 114.10 0 200
Carbon tetrachloride 07/05/20115.0 50.056.9 113.70 83.3 127
Chlorobenzene 07/05/20115.0 50.052.1 104.10 85.8 116
Chloroethane 07/05/201110 50.045.9 91.90 0 200
Chloroform 07/05/20115.0 50.052.3 104.60 80 113
Chloromethane 07/05/201110 50.042.9 85.80 0 200
cis-1,2-Dichloroethene 07/05/20115.0 50.052.3 104.60 0 200
cis-1,3-Dichloropropene 07/05/20114.0 50.056.8 113.50 0 200
Cyclohexanone 07/05/2011100 250252 100.60 0 200
Dibromochloromethane 07/05/20115.0 50.055.7 111.40 89.1 119
Dibromomethane 07/05/20115.0 50.052.6 105.20 0 200
Dichlorodifluoromethane 07/05/201110 50.080.1 160.20 0 200
Ethyl acetate J 07/05/201150.0 50.050 99.00 0 200
Ethyl ether 07/05/20115.0 50.054.2 108.50 0 200
Ethyl methacrylate 07/05/20115.0 50.051.2 102.40 0 200
Ethylbenzene 07/05/20115.0 50.050.9 101.90 84.1 115
Heptane 07/05/201120.0 50.053.8 107.50 0 200
Hexachlorobutadiene 07/05/20115.0 50.050.4 100.80 0 200
Hexachloroethane 07/05/20115.0 50.054.5 108.90 0 200
Iodomethane 07/05/201110 50.056.9 113.90 0 200
Isopropylbenzene 07/05/20115.0 50.052.1 104.20 0 200
m,p-Xylenes 07/05/20115.0 100102 101.80 79.1 111
Methacrylonitrile 07/05/201150.0 50.050.5 101.00 0 200
Methyl Methacrylate 07/05/20115.0 50.051.8 103.60 0 200
Methyl tert-butyl ether 07/05/20112.0 50.054.2 108.30 80 128
Methylacrylate 07/05/201110 50.050.4 100.70 0 200
Methylene chloride 07/05/20115.0 50.055.4 110.90 73.9 116
Naphthalene 07/05/201110 50.045.6 91.20 73.1 135
n-Butylbenzene 07/05/20115.0 50.059.3 118.60 0 200
n-Hexane 07/05/201120.0 50.055.8 111.60 0 200
Page 54 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCS-A110705-1
SampType: LCS µg/KgUnits69368Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Nitrobenzene 07/05/2011100 500451 90.30 0 200
n-Propylbenzene 07/05/20115.0 50.052.6 105.20 0 200
o-Xylene 07/05/20115.0 50.050.7 101.30 82 117
Pentachloroethane 07/05/20115.0 50.057.3 114.70 0 200
p-Isopropyltoluene 07/05/20115.0 50.055.3 110.50 0 200
Propionitrile 07/05/201150.0 500493 98.70 0 200
sec-Butylbenzene 07/05/20115.0 50.052.2 104.50 0 200
Styrene 07/05/20115.0 50.052.5 104.90 0 200
tert-Butylbenzene 07/05/20115.0 50.050.8 101.60 0 200
Tetrachloroethene 07/05/20115.0 50.052.2 104.40 74.6 115
Tetrahydrofuran J 07/05/201150.0 50.046 91.00 0 200
Toluene 07/05/20115.0 50.049.3 98.60 79.1 112
trans-1,2-Dichloroethene 07/05/20115.0 50.055.1 110.10 0 200
trans-1,3-Dichloropropene 07/05/20114.0 50.053.8 107.50 0 200
Trichloroethene S 07/05/20115.0 50.055.9 111.80 81 111
Trichlorofluoromethane 07/05/20115.0 50.055.1 110.20 0 200
Vinyl acetate 07/05/201150.0 50.054.5 109.10 0 200
Vinyl chloride 07/05/20112.0 50.049.2 98.30 0 200
Surr: 1,2-Dichloroethane-d4 07/05/201150.049.8 99.7 72.2 131
Surr: 4-Bromofluorobenzene 07/05/201150.050.4 100.8 82.1 116
Surr: Dibromofluoromethane 07/05/201150.050.9 101.8 77.7 120
Surr: Toluene-d8 07/05/201150.048.5 97.0 86 116
SampID: LCSD-A110705-1
SampType: LCSD µg/KgUnits69368Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
1,1,1,2-Tetrachloroethane 07/05/20115.0 50.050.1 100.2 5.080 52.72
1,1,1-Trichloroethane 07/05/20115.0 50.052.6 105.2 4.410 54.97
1,1,2,2-Tetrachloroethane 07/05/20115.0 50.049.0 97.9 1.180 49.55
1,1,2-Trichloro-1,2,2-trifluoroethane 07/05/20115.0 50.054.4 108.9 5.590 57.57
1,1,2-Trichloroethane 07/05/20115.0 50.049.7 99.5 2.540 51.02
1,1-Dichloro-2-propanone 07/05/201150.0 125128 102.7 3.420 124.1
1,1-Dichloroethane 07/05/20115.0 50.052.1 104.1 2.900 53.59
1,1-Dichloroethene 07/05/20115.0 50.054.3 108.6 3.880 56.47
1,1-Dichloropropene 07/05/20115.0 50.053.3 106.7 2.830 54.87
1,2,3-Trichlorobenzene 07/05/20115.0 50.057.8 115.6 10.820 51.85
1,2,3-Trichloropropane 07/05/201110 50.047.6 95.3 2.200 48.70
1,2,3-Trimethylbenzene 07/05/20115.0 50.049.9 99.8 2.650 51.25
1,2,4-Trichlorobenzene 07/05/20115.0 50.061.8 123.7 14.050 53.72
1,2,4-Trimethylbenzene 07/05/20115.0 50.050.3 100.6 2.400 51.50
1,2-Dibromo-3-chloropropane 07/05/20115.0 50.053.3 106.6 8.100 49.13
1,2-Dibromoethane 07/05/20115.0 50.050.2 100.5 2.240 51.37
1,2-Dichlorobenzene 07/05/20115.0 50.051.3 102.6 1.620 52.15
1,2-Dichloroethane 07/05/20115.0 50.051.2 102.5 2.870 52.73
1,2-Dichloropropane 07/05/20115.0 50.052.1 104.2 2.520 53.44
1,3,5-Trimethylbenzene 07/05/20115.0 50.051.9 103.7 1.190 52.48
1,3-Dichlorobenzene 07/05/20115.0 50.052.8 105.5 3.590 54.70
Page 55 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCSD-A110705-1
SampType: LCSD µg/KgUnits69368Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
1,3-Dichloropropane 07/05/20115.0 50.048.4 96.9 4.440 50.64
1,4-Dichlorobenzene 07/05/20115.0 50.052.3 104.7 2.700 53.76
1-Chlorobutane 07/05/20115.0 50.048.8 97.6 6.400 52.05
2,2-Dichloropropane 07/05/20115.0 50.051.4 102.9 4.740 53.94
2-Butanone 07/05/201150.0 125123 98.6 1.040 124.5
2-Chlorotoluene 07/05/20115.0 50.050.6 101.3 1.840 51.58
2-Hexanone 07/05/201150.0 125124 99.3 0.990 125.4
2-Nitropropane 07/05/201150.0 500550 109.9 0.010 549.6
4-Chlorotoluene 07/05/20115.0 50.051.0 102.1 2.820 52.50
4-Methyl-2-pentanone 07/05/201150.0 125125 100 1.360 123.3
Acetone 07/05/201150.0 125153 122.8 3.290 158.6
Acrylonitrile 07/05/201110 50.048.6 97.3 2.260 49.75
Allyl chloride 07/05/20115.0 50.050.8 101.5 3.100 52.35
Benzene 07/05/20111.0 50.050.6 101.2 1.650 51.43
Bromobenzene 07/05/20115.0 50.049.9 99.8 3.100 51.49
Bromochloromethane 07/05/20115.0 50.051.3 102.6 0.640 51.62
Bromodichloromethane 07/05/20115.0 50.053.2 106.3 1.730 54.08
Bromoform 07/05/20115.0 50.054.3 108.5 3.330 56.10
Bromomethane 07/05/201110 50.051.0 102.0 9.400 46.41
Carbon disulfide 07/05/20115.0 50.054.8 109.6 3.970 57.04
Carbon tetrachloride 07/05/20115.0 50.054.7 109.5 3.820 56.86
Chlorobenzene 07/05/20115.0 50.051.1 102.2 1.880 52.07
Chloroethane 07/05/201110 50.048.7 97.4 5.830 45.93
Chloroform 07/05/20115.0 50.050.8 101.5 3.010 52.31
Chloromethane 07/05/201110 50.038.3 76.6 11.340 42.88
cis-1,2-Dichloroethene 07/05/20115.0 50.051.1 102.2 2.300 52.28
cis-1,3-Dichloropropene 07/05/20114.0 50.055.4 110.8 2.440 56.77
Cyclohexanone 07/05/2011100 250248 99.1 1.490 251.5
Dibromochloromethane 07/05/20115.0 50.053.7 107.4 3.660 55.71
Dibromomethane 07/05/20115.0 50.052.5 105.1 0.150 52.61
Dichlorodifluoromethane 07/05/201110 50.076.2 152.4 4.980 80.08
Ethyl acetate J 07/05/201150.0 50.048 97.0 0.000 49.48
Ethyl ether 07/05/20115.0 50.051.6 103.2 5.010 54.24
Ethyl methacrylate 07/05/20115.0 50.049.9 99.9 2.470 51.19
Ethylbenzene 07/05/20115.0 50.050.5 100.9 0.910 50.93
Heptane 07/05/201120.0 50.052.7 105.4 2.010 53.76
Hexachlorobutadiene 07/05/20115.0 50.056.0 112.0 10.600 50.38
Hexachloroethane 07/05/20115.0 50.053.1 106.2 2.530 54.47
Iodomethane 07/05/201110 50.057.0 114.0 0.110 56.94
Isopropylbenzene 07/05/20115.0 50.051.0 102.1 2.070 52.12
m,p-Xylenes 07/05/20115.0 100101 100.9 0.920 101.8
Methacrylonitrile 07/05/201150.0 50.050.7 101.4 0.430 50.49
Methyl Methacrylate 07/05/20115.0 50.051.5 103.0 0.500 51.78
Methyl tert-butyl ether 07/05/20112.0 50.051.9 103.8 4.240 54.17
Methylacrylate 07/05/201110 50.050.3 100.6 0.180 50.37
Methylene chloride 07/05/20115.0 50.053.3 106.7 3.860 55.43
Naphthalene 07/05/201110 50.053.9 107.7 16.630 45.59
Page 56 of 58
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCSD-A110705-1
SampType: LCSD µg/KgUnits69368Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
n-Butylbenzene 07/05/20115.0 50.056.7 113.4 4.430 59.28
n-Hexane 07/05/201120.0 50.054.0 108.1 3.220 55.80
Nitrobenzene 07/05/2011100 500518 103.7 13.840 451.3
n-Propylbenzene 07/05/20115.0 50.051.4 102.8 2.270 52.60
o-Xylene 07/05/20115.0 50.050.4 100.7 0.630 50.67
Pentachloroethane 07/05/20115.0 50.055.7 111.3 2.960 57.33
p-Isopropyltoluene 07/05/20115.0 50.053.8 107.6 2.680 55.26
Propionitrile 07/05/201150.0 500508 101.7 2.990 493.4
sec-Butylbenzene 07/05/20115.0 50.051.0 102.0 2.400 52.23
Styrene 07/05/20115.0 50.052.0 103.9 0.980 52.46
tert-Butylbenzene 07/05/20115.0 50.049.6 99.2 2.390 50.79
Tetrachloroethene 07/05/20115.0 50.051.5 103.0 1.410 52.21
Tetrahydrofuran J 07/05/201150.0 50.047 94.3 0.000 45.48
Toluene 07/05/20115.0 50.047.9 95.8 2.840 49.28
trans-1,2-Dichloroethene 07/05/20115.0 50.052.8 105.6 4.230 55.07
trans-1,3-Dichloropropene 07/05/20114.0 50.052.0 104.0 3.330 53.77
Trichloroethene 07/05/20115.0 50.054.3 108.6 2.940 55.90
Trichlorofluoromethane 07/05/20115.0 50.057.9 115.8 4.940 55.10
Vinyl acetate 07/05/201150.0 50.053.4 106.8 2.110 54.53
Vinyl chloride 07/05/20112.0 50.047.8 95.6 2.760 49.16
Surr: 1,2-Dichloroethane-d4 07/05/201150.050.3 100.6
Surr: 4-Bromofluorobenzene 07/05/201150.051.4 102.9
Surr: Dibromofluoromethane 07/05/201150.050.4 100.8
Surr: Toluene-d8 07/05/201150.048.5 97.0
Page 57 of 58
Receiving Check List
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 14-Jul-11
Work Order: 11070042
http://www.teklabinc.com/
Received By: BSJCarrier: Michael Flora
Completed by: Reviewed by:
On:
01-Jul-11
On:
01-Jul-11
Shipping container/cooler in good condition? Yes No Not Present
Chain of custody present? Yes No
Chain of custody signed when relinquished and received? Yes No
Chain of custody agrees with sample labels? Yes No
Samples in proper container/bottle? Yes No
Sample containers intact? Yes No
Sufficient sample volume for indicated test? Yes No
All samples received within holding time? Yes No
Container/Temp Blank temperature in compliance? Yes No
Temp °C 5.4
When thermal preservation is required, samples are compliant with a temperature between 0.1°C - 6.0°C, or when samples are received on ice the same day as collected.
Any No responses must be detailed below or on the COC.
Water - vials have zero headspace? Yes No No VOA vials
Water - pH acceptable upon receipt? Yes No
Type of thermal preservation? None Ice Blue Ice Dry Ice
Chain of custody 1 Extra pages included 9
Reported field parameters measured: Field Lab NA
Pages to follow:
Water - TOX containers have zero headspace? Yes No No TOX containers
Timothy W. Mathis Elizabeth A. Hurley
Page 58 of 58
ANALYTICAL REPORT
July 13, 2011
Page 1 of 9Work Order: 11G0118
Project :
Project Number:
Subcontract - HW Project
11070042
Report To
Heather White
Teklab, Inc.
Collinsville, IL 62234
5445 Horseshoe Lake Road
Work Order Information
Date Received: 07/06/2011 10:15AM
Collector:
Phone: (618) 344-1004
PO Number: 16845
Analyte Result MRL Batch Method Analyst Analyzed Qualifier
11070042-001 06/29/11 16:00Collected: 11G0118-01 Matrix:Soil
Dalapon mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638
3,5-Dichlorobenzoic acid mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638
Dicamba mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638
Dichlorprop mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638
2,4-D mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638
Pentachlorophenol mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638
2,4,5-TP (Silvex) mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638
Chloramben mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638
2,4,5-T mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638
2,4-DB mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638
Bentazon mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638
Picloram mg/kg dry EPPEPA 8151A0.05 07/11/11 16:55<0.05 1G10638
Dinoseb mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638
DCPA mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638
Acifluorfen mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638
Surrogate: 2,5-Dichlorobenzoic Acid 71.7 % 24-140 07/11/11 17:42EPP
0.1%% Solids SM 2540 G MAV 07/11/11 11:5578.5 1G10803
11070042-002 06/30/11 08:00Collected: 11G0118-02 Matrix:Soil
Dalapon mg/kg dry EPPEPA 8151A0.05 07/11/11 18:30<0.05 1G10638
3,5-Dichlorobenzoic acid mg/kg dry EPPEPA 8151A0.05 07/11/11 18:30<0.05 1G10638
Dicamba mg/kg dry EPPEPA 8151A0.05 07/11/11 18:30<0.05 1G10638
Dichlorprop mg/kg dry EPPEPA 8151A0.05 07/11/11 18:30<0.05 1G10638
2,4-D mg/kg dry EPPEPA 8151A0.05 07/11/11 18:30<0.05 1G10638
Pentachlorophenol mg/kg dry EPPEPA 8151A0.05 07/11/11 18:30<0.05 1G10638
2,4,5-TP (Silvex) mg/kg dry EPPEPA 8151A0.05 07/11/11 18:30<0.05 1G10638
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0118
July 13, 2011
Page 2 of 9
Analyte Result MRL Batch Method Analyst Analyzed Qualifier
11070042-002 06/30/11 08:00Collected: 11G0118-02 Matrix:Soil
Chloramben mg/kg dry EPPEPA 8151A0.05 07/11/11 18:30<0.05 1G10638
2,4,5-T mg/kg dry EPPEPA 8151A0.05 07/11/11 18:30<0.05 1G10638
2,4-DB mg/kg dry EPPEPA 8151A0.05 07/11/11 18:30<0.05 1G10638
Bentazon mg/kg dry EPPEPA 8151A0.05 07/11/11 18:30<0.05 1G10638
Picloram mg/kg dry EPPEPA 8151A0.05 07/11/11 17:42<0.05 1G10638
Dinoseb mg/kg dry EPPEPA 8151A0.05 07/11/11 18:30<0.05 1G10638
DCPA mg/kg dry EPPEPA 8151A0.05 07/11/11 18:30<0.05 1G10638
Acifluorfen mg/kg dry EPPEPA 8151A0.05 07/11/11 18:30<0.05 1G10638
Surrogate: 2,5-Dichlorobenzoic Acid 64.0 % 24-140 07/11/11 18:30EPP
0.1%% Solids SM 2540 G MAV 07/11/11 11:5581.4 1G10803
11070042-003 06/30/11 09:00Collected: 11G0118-03 Matrix:Soil
Dalapon mg/kg dry EPPEPA 8151A0.05 07/11/11 19:17<0.05 1G10638
3,5-Dichlorobenzoic acid mg/kg dry EPPEPA 8151A0.05 07/11/11 19:17<0.05 1G10638
Dicamba mg/kg dry EPPEPA 8151A0.05 07/11/11 19:17<0.05 1G10638
Dichlorprop mg/kg dry EPPEPA 8151A0.05 07/11/11 19:17<0.05 1G10638
2,4-D mg/kg dry EPPEPA 8151A0.05 07/11/11 19:17<0.05 1G10638
Pentachlorophenol mg/kg dry EPPEPA 8151A0.05 07/11/11 19:17<0.05 1G10638
2,4,5-TP (Silvex) mg/kg dry EPPEPA 8151A0.05 07/11/11 19:17<0.05 1G10638
Chloramben mg/kg dry EPPEPA 8151A0.05 07/11/11 19:17<0.05 1G10638
2,4,5-T mg/kg dry EPPEPA 8151A0.05 07/11/11 19:17<0.05 1G10638
2,4-DB mg/kg dry EPPEPA 8151A0.05 07/11/11 19:17<0.05 1G10638
Bentazon mg/kg dry EPPEPA 8151A0.05 07/11/11 19:17<0.05 1G10638
Picloram mg/kg dry EPPEPA 8151A0.05 07/11/11 18:30<0.05 1G10638
Dinoseb mg/kg dry EPPEPA 8151A0.05 07/11/11 19:17<0.05 1G10638
DCPA mg/kg dry EPPEPA 8151A0.05 07/11/11 19:17<0.05 1G10638
Acifluorfen mg/kg dry EPPEPA 8151A0.05 07/11/11 19:17<0.05 1G10638
Surrogate: 2,5-Dichlorobenzoic Acid 49.6 % 24-140 07/11/11 19:17EPP
0.1%% Solids SM 2540 G MAV 07/11/11 11:5583.1 1G10803
11070042-004 06/30/11 10:00Collected: 11G0118-04 Matrix:Soil
Dalapon mg/kg dry EPPEPA 8151A0.05 07/11/11 20:05<0.05 1G10638
3,5-Dichlorobenzoic acid mg/kg dry EPPEPA 8151A0.05 07/11/11 20:05<0.05 1G10638
Dicamba mg/kg dry EPPEPA 8151A0.05 07/11/11 20:05<0.05 1G10638
Dichlorprop mg/kg dry EPPEPA 8151A0.05 07/11/11 20:05<0.05 1G10638
2,4-D mg/kg dry EPPEPA 8151A0.05 07/11/11 20:05<0.05 1G10638
Pentachlorophenol mg/kg dry EPPEPA 8151A0.05 07/11/11 20:05<0.05 1G10638
2,4,5-TP (Silvex) mg/kg dry EPPEPA 8151A0.05 07/11/11 20:05<0.05 1G10638
Chloramben mg/kg dry EPPEPA 8151A0.05 07/11/11 20:05<0.05 1G10638
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0118
July 13, 2011
Page 3 of 9
Analyte Result MRL Batch Method Analyst Analyzed Qualifier
11070042-004 06/30/11 10:00Collected: 11G0118-04 Matrix:Soil
2,4,5-T mg/kg dry EPPEPA 8151A0.05 07/11/11 20:05<0.05 1G10638
2,4-DB mg/kg dry EPPEPA 8151A0.05 07/11/11 20:05<0.05 1G10638
Bentazon mg/kg dry EPPEPA 8151A0.05 07/11/11 20:05<0.05 1G10638
Picloram mg/kg dry EPPEPA 8151A0.05 07/11/11 19:17<0.05 1G10638
Dinoseb mg/kg dry EPPEPA 8151A0.05 07/11/11 20:05<0.05 1G10638
DCPA mg/kg dry EPPEPA 8151A0.05 07/11/11 20:05<0.05 1G10638
Acifluorfen mg/kg dry EPPEPA 8151A0.05 07/11/11 20:05<0.05 1G10638
Surrogate: 2,5-Dichlorobenzoic Acid 48.7 % 24-140 07/11/11 20:05EPP
0.1%% Solids SM 2540 G MAV 07/11/11 11:5586.4 1G10803
11070042-005 06/30/11 11:00Collected: 11G0118-05 Matrix:Soil
Dalapon mg/kg dry EPPEPA 8151A0.05 07/11/11 20:52<0.05 1G10638
3,5-Dichlorobenzoic acid mg/kg dry EPPEPA 8151A0.05 07/11/11 20:52<0.05 1G10638
Dicamba mg/kg dry EPPEPA 8151A0.05 07/11/11 20:52<0.05 1G10638
Dichlorprop mg/kg dry EPPEPA 8151A0.05 07/11/11 20:52<0.05 1G10638
2,4-D mg/kg dry EPPEPA 8151A0.05 07/11/11 20:52<0.05 1G10638
Pentachlorophenol mg/kg dry EPPEPA 8151A0.05 07/11/11 20:52<0.05 1G10638
2,4,5-TP (Silvex) mg/kg dry EPPEPA 8151A0.05 07/11/11 20:52<0.05 1G10638
Chloramben mg/kg dry EPPEPA 8151A0.05 07/11/11 20:52<0.05 1G10638
2,4,5-T mg/kg dry EPPEPA 8151A0.05 07/11/11 20:52<0.05 1G10638
2,4-DB mg/kg dry EPPEPA 8151A0.05 07/11/11 20:52<0.05 1G10638
Bentazon mg/kg dry EPPEPA 8151A0.05 07/11/11 20:52<0.05 1G10638
Picloram mg/kg dry EPPEPA 8151A0.05 07/11/11 20:05<0.05 1G10638
Dinoseb mg/kg dry EPPEPA 8151A0.05 07/11/11 20:52<0.05 1G10638
DCPA mg/kg dry EPPEPA 8151A0.05 07/11/11 20:52<0.05 1G10638
Acifluorfen mg/kg dry EPPEPA 8151A0.05 07/11/11 20:52<0.05 1G10638
Surrogate: 2,5-Dichlorobenzoic Acid 41.9 % 24-140 07/11/11 20:52EPP
0.1%% Solids SM 2540 G MAV 07/11/11 11:5587.7 1G10803
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0118
July 13, 2011
Page 4 of 9
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Determination of Chlorinated Phenoxy Herbicides - Quality Control
Keystone Laboratories, Inc. - Newton
Batch 1G10638 - EPA 3550B
Blank (1G10638-BLK1) Prepared: 07/06/11 Analyzed: 07/11/11
mg/kg wet 0.0760000 24-140Surrogate: 2,5-Dichlorobenzoic Acid 43.60.0332
Dalapon "ND 0.05
3,5-Dichlorobenzoic acid "ND 0.05
Dicamba "ND 0.05
Dichlorprop "ND 0.05
2,4-D "ND 0.05
Pentachlorophenol "ND 0.05
2,4,5-TP (Silvex) "ND 0.05
Chloramben "ND 0.05
2,4,5-T "ND 0.05
2,4-DB "ND 0.05
Bentazon "ND 0.05
Picloram "ND 0.05
Dinoseb "ND 0.05
DCPA "ND 0.05
Acifluorfen "ND 0.05
LCS (1G10638-BS1) Prepared: 07/06/11 Analyzed: 07/11/11
mg/kg wet 0.0760000 24-140Surrogate: 2,5-Dichlorobenzoic Acid 48.90.0372
Dalapon "0.088 0.05 0.208000 10-9342.3
3,5-Dichlorobenzoic acid "0.008 0.05 0.0160000 QS-0153-12952.1
Dicamba "0.013 0.05 0.0160000 38-12382.3
Dichlorprop "0.022 0.05 0.0480000 31-12744.8
2,4-D "0.019 0.05 0.0320000 23-12759.4
Pentachlorophenol "0.009 0.05 0.0160000 10-9357.3
2,4,5-TP (Silvex) "0.008 0.05 0.0160000 35-11647.9
Chloramben "0.011 0.05 0.0160000 10-9468.8
2,4,5-T "0.003 0.05 0.0160000 QS-0126-10416.7
2,4-DB "0.100 0.05 0.128000 42-12277.9
Bentazon "0.024 0.05 0.0320000 42-13374.5
Picloram "0.011 0.05 0.0160000 19-15766.7
Dinoseb "0.004 0.05 0.0320000 10-9011.5
DCPA "0.016 0.05 0.0160000 10-11796.9
Acifluorfen "0.008 0.05 0.0160000 24-11353.1
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0118
July 13, 2011
Page 5 of 9
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Determination of Chlorinated Phenoxy Herbicides - Quality Control
Keystone Laboratories, Inc. - Newton
Batch 1G10638 - EPA 3550B
Matrix Spike (1G10638-MS1) Prepared: 07/06/11 Analyzed: 07/11/11 Source: 11G0118-03
mg/kg dry 0.0905046 24-140Surrogate: 2,5-Dichlorobenzoic Acid 62.10.0562
Dalapon "0.186 0.05 0.247697 ND 19-15675.0
3,5-Dichlorobenzoic acid "0.017 0.05 0.0190536 ND 38.9-18191.7
Dicamba "0.019 0.05 0.0190536 ND 40-15399.0
Dichlorprop "0.034 0.05 0.0571608 ND 19.6-13859.7
2,4-D "0.021 0.05 0.0381072 ND 10-14654.7
Pentachlorophenol "0.013 0.05 0.0190536 ND 16-12770.8
2,4,5-TP (Silvex) "0.013 0.05 0.0190536 ND 31.2-15970.8
Chloramben "0.015 0.05 0.0190536 ND 10-13380.2
2,4,5-T "0.005 0.05 0.0190536 ND 16.4-15228.1
2,4-DB "0.174 0.05 0.152429 ND 35.3-156114
Bentazon "0.031 0.05 0.0381072 ND 10-15082.3
Picloram "0.015 0.05 0.0190536 ND 45-14679.2
Dinoseb "0.011 0.05 0.0381072 ND 10-9027.6
DCPA "0.019 0.05 0.0190536 ND 10-15197.9
Acifluorfen "0.013 0.05 0.0190536 ND 10-16166.7
Matrix Spike Dup (1G10638-MSD1) Prepared: 07/06/11 Analyzed: 07/11/11 Source: 11G0118-03
mg/kg dry 0.0910147 24-140Surrogate: 2,5-Dichlorobenzoic Acid 65.40.0595
Dalapon "0.221 0.05 0.249093 ND 3019-15688.6 17.2
3,5-Dichlorobenzoic acid "0.017 0.05 0.0191610 ND 3038.9-18186.5 5.29
Dicamba "0.020 0.05 0.0191610 ND 3040-153106 7.67
Dichlorprop "0.038 0.05 0.0574830 ND 3019.6-13866.0 10.5
2,4-D "0.040 0.05 0.0383220 ND 30 QR-0210-146104 62.8
Pentachlorophenol "0.015 0.05 0.0191610 ND 3016-12780.2 13.0
2,4,5-TP (Silvex) "0.017 0.05 0.0191610 ND 3031.2-15986.5 20.4
Chloramben "0.017 0.05 0.0191610 ND 3010-13389.6 11.6
2,4,5-T "0.007 0.05 0.0191610 ND 3016.4-15234.4 20.6
2,4-DB "0.160 0.05 0.153288 ND 3035.3-156104 8.85
Bentazon "0.033 0.05 0.0383220 ND 3010-15084.9 3.68
Picloram "0.015 0.05 0.0191610 ND 3045-14680.2 1.87
Dinoseb "0.016 0.05 0.0383220 ND 30 QR-0210-9041.7 41.1
DCPA "0.025 0.05 0.0191610 ND 3010-151130 28.9
Acifluorfen "0.015 0.05 0.0191610 ND 3010-16180.2 19.0
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0118
July 13, 2011
Page 6 of 9
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Determination of Chlorinated Phenoxy Herbicides - Quality Control
Keystone Laboratories, Inc. - Newton
Batch 1G10638 - EPA 3550B
Reference (1G10638-SRM1) Prepared: 07/06/11 Analyzed: 07/12/11
mg/kg wet 0.0760000 24-140Surrogate: 2,5-Dichlorobenzoic Acid 99.10.0753
Dalapon "0.208 0.05 0.208000 70-13099.8
3,5-Dichlorobenzoic acid "0.015 0.05 0.0160000 70-13092.7
Dicamba "0.018 0.05 0.0160000 70-130109
Dichlorprop "0.049 0.05 0.0480000 70-130101
2,4-D "0.032 0.05 0.0320000 70-130100
Pentachlorophenol "0.014 0.05 0.0160000 70-13090.6
2,4,5-TP (Silvex) "0.016 0.05 0.0160000 70-13097.9
Chloramben "0.022 0.05 0.0160000 QR-0570-130134
2,4,5-T "0.012 0.05 0.0160000 70-13076.0
2,4-DB "0.138 0.05 0.128000 70-130108
Bentazon "0.035 0.05 0.0320000 70-130108
Picloram "0.018 0.05 0.0160000 70-130111
Dinoseb "0.043 0.05 0.0320000 QR-0570-130134
DCPA "0.020 0.05 0.0160000 70-130123
Acifluorfen "0.013 0.05 0.0160000 70-13079.2
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0118
July 13, 2011
Page 7 of 9
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Determination of Conventional Chemistry Parameters - Quality Control
Keystone Laboratories, Inc. - Newton
Batch 1G10803 - Wet Chem Preparation
Duplicate (1G10803-DUP1) Prepared: 07/08/11 Analyzed: 07/11/11 Source: 11G0118-05
% Solids %86.7 0.1 87.7 201.11
ND = Non Detect; REC= Recovery; RPD= Relative Percent Difference
Certified Analyses included in this Report
CertificationsAnalyteMethod/Matrix
EPA 8151A in Soil
KS-NT,NELACDalapon
KS-NT,NELAC,SIA1XDicamba
NELACDichlorprop
KS-NT,NELAC,SIA1X2,4-D
KS-NT,NELAC,SIA1X2,4,5-TP (Silvex)
KS-NT,NELAC2,4,5-T
NELAC2,4-DB
KS-NT,NELACPicloram
KS-NT,NELACDinoseb
SIA1XAcifluorfen
SM 2540 G in Soil
SIA1X% Solids
Description Number ExpiresCode
E-10110Kansas Department of Health and Environment-KC 04/30/2012KS-KC
E-10287Kansas Department of Health and Environment 10/30/2011KS-NT
140Missouri Department of Natural Resources 04/30/2012MO-KC
IA001New Jersey Department of Environmental Protection 06/30/2011NELAC
95Iowa Department of Natural Resources 02/01/2012SIA1X
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0118
July 13, 2011
Page 8 of 9
Notes and Definitions
QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC
batch were accepted based on percent recoveries and completeness of QC data.
QR-05 The reference standard was outside of established control limits. The batch was accepted based on acceptable LCS, MS/MSD
and RPD results.
QS-01 The blank spike recovery and/or blank spike duplicate recovery were outside the established acceptance limits. Batch was
accepted based on acceptable MS/MSD/RPD results.
End of Report
Christine Dawson
Project Manager
Keystone Laboratories, Inc.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0118
July 13, 2011
Page 9 of 9
COC Goes Here
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
http://www.teklabinc.com/
July 29, 2011
WorkOrder: 11070610A831-735002-012901-225Ameren Champaign 62409080120
RE:
Dear Pete Sazama:
TEKLAB, INC received 9 samples on 7/15/2011 5:03:00 PM for the analysis presented in the following report.
Samples are analyzed on an as received basis unless otherwise requested and documented. The sample results contained in this report relate only to the requested analytes of interest as directed on the chain of custody. NELAP accredited fields of testing are indicated by the letters NELAP under the Certification column.
All tests are performed in the Collinsville, IL laboratory unless otherwise noted in the Case Narrative.
All quality control criteria applicable to the test methods employed for this project have been satisfactorily met and are in accordance with NELAP except where noted. The following report shall not be reproduced, except in full, without the written approval of Teklab, Inc.
If you have any questions regarding these tests results, please feel free to call.
Sincerely,
210 West Sand Bank RoadColumbia, IL 62236-0230
(618) 281-7173(618) 281-5120
TEL:FAX:
Pete SazamaPSC Industrial Outsourcing, LP
Heather A. WhiteProject Manager(618)344-1004 ex [email protected]
Page 1 of 104
This reporting package includes the following:
Report Contents
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Cover Letter 1
Report Contents 2
Definitions 3
Case Narrative 4
Laboratory Results 5
Sample Summary 59
Dates Report 60
Quality Control Results 66
Receiving Check List 104
Chain of Custody Appended
Page 2 of 104
____TeklabHdrP
Definitions
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Abbr DefinitionCCV Continuing calibration verification is a check of a standard to determine the state of calibration of an instrument between recalibration.
DF Dilution factor is the dilution performed during analysis only and does not take into account any dilutions made during sample preparation. The reported result is final and includes all dilutions factors.
DNI Did not ignite
DUP Laboratory duplicate is an aliquot of a sample taken from the same container under laboratory conditions for independent processing and analysis independently of the original aliquot.
ICV Initial calibration verification is a check of a standard to determine the state of calibration of an instrument before sample analysis is initiated.
IDPH IL Dept. of Public Health
LCS Laboratory control sample, spiked with verified known amounts of analytes, is analyzed exactly like a sample to establish intra-laboratory or analyst specific precision and bias or to assess the performance of all or a portion of the measurement system. The acceptable recovery range is in the QC Package (provided upon request).
LCSD Laboratory control sample duplicate is a replicate laboratory control sample that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in the QC Package (provided upon request).
MB Method blank is a sample of a matrix similar to the batch of associated sample (when available) that is free from the analytes of interest and is processed simultaneously with and under the same conditions as samples through all steps of the analytical procedures, and in which no target analytes or interferences should present at concentrations that impact the analytical results for sample analyses.
MDL Method detection limit means the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type containing the analyte.
MS Matrix spike is an aliquot of matrix fortified (spiked) with known quantities of specific analytes that is subjected to the entire analytical procedures in order to determine the effect of the matrix on an approved test method’s recovery system. The acceptable recovery range is listed in the QC Package (provided upon request).
MSD Matrix spike duplicate means a replicate matrix spike that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in the QC Package (provided upon request).
MW Molecular weight
ND Not Detected at the Reporting Limit
NELAP NELAP Accredited
PQL Practical quantitation limit means the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine laboratory operation conditions. The acceptable recovery range is listed in the QC Package (provided upon request).
RL The reporting limit the lowest level that the data is displayed in the final report. The reporting limit may vary according to customer request or sample dilution. The reporting limit may not be less than the MDL.
RPD Relative percent difference is a calculated difference between two recoveries (ie. MS/MSD). The acceptable recovery limit is listed in the QC Package (provided upon request).
SPK The spike is a known mass of target analyte added to a blank sample or sub-sample; used to determine recovery deficiency or for other quality control purposes.
Surr Surrogates are compounds which are similar to the analytes of interest in chemical composition and behavior in the analytical process, but which are not normally found in environmental samples.
TNTC Too numerous to count ( > 200 CFU )
Qualifiers# - Unknown hydrocarbon B - Analyte detected in associated Method Blank
E - Value above quantitation range H - Holding times exceeded
J - Analyte detected below quantitation limits M - Manual Integration used to determine area response
ND - Not Detected at the Reporting Limit R - RPD outside accepted recovery limits
S - Spike Recovery outside recovery limits X - Value exceeds Maximum Contaminant Level
Page 3 of 104
Case Narrative
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Cooler Receipt Temp: 8.8 °C
Herbicide analysis performed by Keystone Laboratories, Inc. See attached report for QC data.
NELAPState Cert # Exp Date LabDept
Locations and Accreditations
____________________________________Collinsville
Address 5445 Horseshoe Lake Road
Collinsville, IL 62234-7425
Phone (618) 344-1004
Fax (618) 344-1005
Email [email protected]
____________________________________Springfield
Address 3920 Pintail Dr
Springfield, IL 62711-9415
Phone (217) 698-1004
Fax (217) 698-1005
Email [email protected]
____________________________________Kansas City
Address 8421 Nieman Road
Lenexa, KS 66214
Phone (913) 541-1998
Fax (913) 541-1998
Email [email protected]
Illinois 100226 1/31/2012 CollinsvilleNELAPIEPA
Kansas E-10374 1/31/2012 CollinsvilleNELAPKDHE
Louisiana 166493 6/30/2012 CollinsvilleNELAPLDEQ
Louisiana 166578 6/30/2012 SpringfieldNELAPLDEQ
Arkansas 88-0966 3/14/2012 CollinsvilleADEQ
Illinois 17584 4/30/2012 CollinsvilleIDPH
Kentucky 0073 5/26/2012 CollinsvilleUST
Missouri 00930 4/13/2013 CollinsvilleMDNR
Oklahoma 9978 8/31/2011 CollinsvilleODEQ
Page 4 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 10:00
Lab ID: 11070610-001 Client Sample ID: SBA-N4 (5-6)
Matrix: SOLID
Batch
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 07/18/2011 10:000.1 % 123.8 R152055
STANDARD METHODS 18TH ED. 2540 GTotal Solids 07/18/2011 8:300.1 % 176.2 R152054
SW-846 9012A (TOTAL)Cyanide 07/19/2011 10:260.34 mg/Kg-dry 1< 0.34NELAP 69687
SW-846 3050B, 6010B, METALS BY ICPAluminum S 07/19/2011 12:214.90 mg/Kg-dry 118100NELAP 69636
Antimony 07/27/2011 11:534.72 mg/Kg-dry 1< 4.72NELAP 69908
Arsenic 07/19/2011 12:212.45 mg/Kg-dry 19.26NELAP 69636
Barium 07/20/2011 15:010.49 mg/Kg-dry 1139NELAP 69636
Beryllium 07/19/2011 12:210.10 mg/Kg-dry 10.69NELAP 69636
Cadmium 07/19/2011 12:210.20 mg/Kg-dry 10.42NELAP 69636
Calcium S 07/28/2011 12:544.72 mg/Kg-dry 142300NELAP 69954
Chromium 07/20/2011 15:010.98 mg/Kg-dry 124.2NELAP 69636
Cobalt 07/19/2011 12:210.98 mg/Kg-dry 110.2NELAP 69636
Copper 07/28/2011 12:540.94 mg/Kg-dry 115.4NELAP 69954
Iron S 07/19/2011 12:211.96 mg/Kg-dry 126800NELAP 69636
Lead 07/19/2011 12:213.92 mg/Kg-dry 118.7NELAP 69636
Magnesium S 07/19/2011 12:210.98 mg/Kg-dry 113600NELAP 69636
Manganese S 07/19/2011 12:210.49 mg/Kg-dry 1760NELAP 69636
Nickel 07/20/2011 15:010.98 mg/Kg-dry 119.2NELAP 69636
Potassium S 07/20/2011 15:019.80 mg/Kg-dry 12230NELAP 69636
Silver 07/20/2011 15:010.54 mg/Kg-dry 1< 0.54NELAP 69636
Sodium 07/20/2011 15:014.90 mg/Kg-dry 1256NELAP 69636
Vanadium 07/20/2011 15:010.98 mg/Kg-dry 132.1NELAP 69636
Zinc 07/27/2011 10:450.98 mg/Kg-dry 175.0NELAP 69636
Ca - Sample concentration was greater than 5 times the spike concentration.K - Sample concentration was greater than 5 times the spike concentration.Al, Fe, Mg, Mn - Sample concentration was greater than 5 times the spike concentration.
SW-846 3050B, METALS BY GFAASelenium 7740 07/20/2011 8:290.566 mg/Kg-dry 1< 0.566NELAP 69639
Thallium 7841 JS 07/28/2011 9:090.189 mg/Kg-dry 10.17NELAP 69639
Tl-Matrix interference present in sample. Verified by Bench Spike
SW-846 7471AMercury 07/19/2011 12:250.012 mg/Kg-dry 10.041NELAP 69631
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel 07/19/2011 17:00164 mg/Kg-dry 25NDNELAP 69637
Kerosene 07/19/2011 17:00164 mg/Kg-dry 25NDNELAP 69637
Mineral Spirits 07/19/2011 17:00164 mg/Kg-dry 25NDNELAP 69637
Motor Oil 07/19/2011 17:00164 mg/Kg-dry 25NDNELAP 69637
Surr: n-Tetracontane 07/19/2011 17:0050.6-140 %REC 2589.2 69637
Elevated reporting limit(s) due to sample extract composition.
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/25/2011 21:56219 µg/Kg-dry 100NDNELAP 69671
4,4´-DDE 07/25/2011 21:56219 µg/Kg-dry 100NDNELAP 69671
4,4´-DDT 07/25/2011 21:56219 µg/Kg-dry 100NDNELAP 69671
Alachlor 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
Page 5 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 10:00
Lab ID: 11070610-001 Client Sample ID: SBA-N4 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECDAldrin 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
alpha-BHC 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
alpha-Chlordane 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
beta-BHC 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
Chlordane 07/22/2011 12:5721.9 µg/Kg-dry 5NDNELAP 69671
delta-BHC 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
Dieldrin 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
Endosulfan I 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
Endosulfan II 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
Endosulfan sulfate 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
Endrin 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
Endrin aldehyde 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
Endrin ketone 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
gamma-BHC 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
gamma-Chlordane 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
Heptachlor 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
Heptachlor epoxide 07/22/2011 12:5711.0 µg/Kg-dry 5NDNELAP 69671
Methoxychlor 07/25/2011 21:56219 µg/Kg-dry 100NDNELAP 69671
Toxaphene 07/22/2011 12:57197 µg/Kg-dry 5NDNELAP 69671
Surr: Decachlorobiphenyl 07/22/2011 12:5748-149 %REC 5118.4 69671
Surr: Tetrachloro-m-xylene 07/22/2011 12:5719-145 %REC 591.9 69671
Elevated reporting limit(s) due to sample extract composition.
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/20/2011 18:1949.2 µg/Kg-dry 1NDNELAP 69671
Aroclor 1221 07/20/2011 18:1949.2 µg/Kg-dry 1NDNELAP 69671
Aroclor 1232 07/20/2011 18:1949.2 µg/Kg-dry 1NDNELAP 69671
Aroclor 1242 07/20/2011 18:1949.2 µg/Kg-dry 1NDNELAP 69671
Aroclor 1248 07/20/2011 18:1949.2 µg/Kg-dry 1NDNELAP 69671
Aroclor 1254 07/20/2011 18:1949.2 µg/Kg-dry 1NDNELAP 69671
Aroclor 1260 07/20/2011 18:1949.2 µg/Kg-dry 1NDNELAP 69671
Surr: Decachlorobiphenyl 07/20/2011 18:195-156 %REC 185.3 69671
Surr: Tetrachloro-meta-xylene 07/20/2011 18:197.35-123 %REC 186.9 69671
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/20/2011 3:050.222 mg/Kg-dry 50NDNELAP 69628
Acenaphthylene 07/20/2011 3:050.222 mg/Kg-dry 50NDNELAP 69628
Anthracene 07/20/2011 3:050.222 mg/Kg-dry 50NDNELAP 69628
Benzo(a)anthracene 07/20/2011 3:050.222 mg/Kg-dry 500.567NELAP 69628
Benzo(a)pyrene 07/20/2011 3:050.222 mg/Kg-dry 500.458NELAP 69628
Benzo(b)fluoranthene 07/20/2011 3:050.222 mg/Kg-dry 500.720NELAP 69628
Benzo(g,h,i)perylene 07/20/2011 3:050.222 mg/Kg-dry 500.240NELAP 69628
Benzo(k)fluoranthene 07/20/2011 3:050.222 mg/Kg-dry 500.262NELAP 69628
Bis(2-ethylhexyl)phthalate 07/20/2011 3:054.38 mg/Kg-dry 50NDNELAP 69628
Chrysene 07/20/2011 3:050.222 mg/Kg-dry 500.567NELAP 69628
Dibenzo(a,h)anthracene 07/20/2011 3:050.222 mg/Kg-dry 50NDNELAP 69628
Fluoranthene 07/20/2011 3:050.222 mg/Kg-dry 501.22NELAP 69628
Fluorene 07/20/2011 3:050.222 mg/Kg-dry 50NDNELAP 69628
Indeno(1,2,3-cd)pyrene J 07/20/2011 3:050.222 mg/Kg-dry 500.22NELAP 69628
Page 6 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 10:00
Lab ID: 11070610-001 Client Sample ID: SBA-N4 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSNaphthalene 07/20/2011 3:050.222 mg/Kg-dry 50NDNELAP 69628
Phenanthrene 07/20/2011 3:050.222 mg/Kg-dry 500.676NELAP 69628
Pyrene 07/20/2011 3:050.222 mg/Kg-dry 501.07NELAP 69628
Surr: 2-Fluorobiphenyl 07/20/2011 3:0510-131 %REC 5070.0 69628
Surr: Nitrobenzene-d5 07/20/2011 3:0510-132 %REC 5074.0 69628
Surr: p-Terphenyl-d14 S 07/20/2011 3:0580.2-138 %REC 5080.0 69628
Surrogate recovery was outside QC limits due to matrix interference.Elevated reporting limit(s) due to sample extract composition.
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
1,2-Dichlorobenzene 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
1,3-Dichlorobenzene 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
1,4-Dichlorobenzene 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
2,4,5-Trichlorophenol 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
2,4,6-Trichlorophenol 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
2,4-Dichlorophenol 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
2,4-Dimethylphenol 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
2,4-Dinitrophenol 07/19/2011 17:5832.7 mg/Kg-dry 25NDNELAP 69627
2,4-Dinitrotoluene 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
2,6-Dinitrotoluene 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
2-Chloronaphthalene 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
2-Chlorophenol 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
2-Methoxy-4-methylphenol 07/19/2011 17:5821.3 mg/Kg-dry 25ND 69627
2-Methylnaphthalene 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
2-Nitroaniline 07/19/2011 17:5832.7 mg/Kg-dry 25NDNELAP 69627
2-Nitrophenol 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
3,3´-Dichlorobenzidine 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
3-Nitroaniline 07/19/2011 17:5832.7 mg/Kg-dry 25NDNELAP 69627
4,6-Dinitro-2-methylphenol 07/19/2011 17:5832.7 mg/Kg-dry 25NDNELAP 69627
4-Bromophenyl phenyl ether 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
4-Chloro-3-methylphenol 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
4-Chloroaniline 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
4-Chlorophenyl phenyl ether 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
4-Nitroaniline 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
4-Nitrophenol 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
Aniline 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
Azobenzene 07/19/2011 17:5811.5 mg/Kg-dry 25ND 69627
Benzidine 07/19/2011 17:5834.5 mg/Kg-dry 25see noteNELAP 69627
Benzoic acid 07/19/2011 17:5849.1 mg/Kg-dry 25NDNELAP 69627
Benzyl alcohol 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
Bis(2-chloroethoxy)methane 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
Bis(2-chloroethyl)ether 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
Bis(2-chloroisopropyl)ether 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
Butyl benzyl phthalate 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
Carbazole 07/19/2011 17:5816.4 mg/Kg-dry 25ND 69627
Dibenzofuran 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
Diethyl phthalate 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
Page 7 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 10:00
Lab ID: 11070610-001 Client Sample ID: SBA-N4 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSDimethyl phthalate 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
Di-n-butyl phthalate 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
Di-n-octyl phthalate 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
Hexachlorobenzene 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
Hexachlorobutadiene 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
Hexachlorocyclopentadiene 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
Hexachloroethane 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
Isophorone 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
m,p-Cresol 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
Nitrobenzene 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
N-Nitrosodimethylamine 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
N-Nitroso-di-n-propylamine 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
N-Nitrosodiphenylamine 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
o-Cresol 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
Pentachlorophenol 07/19/2011 17:5865.4 mg/Kg-dry 25NDNELAP 69627
Phenol 07/19/2011 17:5811.5 mg/Kg-dry 25NDNELAP 69627
Pyridine 07/19/2011 17:5816.4 mg/Kg-dry 25NDNELAP 69627
1,2-Diphenylhydrazine 07/19/2011 17:5827.5 mg/Kg-dry 25ND 69627
Surr: 2,4,6-Tribromophenol 07/19/2011 17:5832.7-130 %REC 2572.1 69627
Surr: 2-Fluorobiphenyl 07/19/2011 17:5834.1-116 %REC 2578.7 69627
Surr: 2-Fluorophenol 07/19/2011 17:5830.5-99 %REC 2575.8 69627
Surr: Nitrobenzene-d5 07/19/2011 17:5834.1-101 %REC 2584.9 69627
Surr: Phenol-d5 07/19/2011 17:5834.9-110 %REC 2575.6 69627
Surr: p-Terphenyl-d14 07/19/2011 17:5841.7-124 %REC 2588.3 69627
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.Elevated reporting limit(s) due to sample extract composition.4-Nitrophenol was outside upper QC limits in the LCS. Sample was ND.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,1,1-Trichloroethane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,1,2,2-Tetrachloroethane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,1,2-Trichloro-1,2,2-trifluoroethane 07/20/2011 16:464.9 µg/Kg-dry 1ND 69726
1,1,2-Trichloroethane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,1-Dichloro-2-propanone 07/20/2011 16:4648.9 µg/Kg-dry 1ND 69726
1,1-Dichloroethane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,1-Dichloroethene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,1-Dichloropropene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,2,3-Trichlorobenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,2,3-Trichloropropane 07/20/2011 16:469.8 µg/Kg-dry 1NDNELAP 69726
1,2,3-Trimethylbenzene 07/20/2011 16:464.9 µg/Kg-dry 1ND 69726
1,2,4-Trichlorobenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,2,4-Trimethylbenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,2-Dibromo-3-chloropropane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,2-Dibromoethane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,2-Dichlorobenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,2-Dichloroethane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,2-Dichloropropane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Page 8 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 10:00
Lab ID: 11070610-001 Client Sample ID: SBA-N4 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,3,5-Trimethylbenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,3-Dichlorobenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,3-Dichloropropane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1,4-Dichlorobenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
1-Chlorobutane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
2,2-Dichloropropane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
2-Butanone 07/20/2011 16:4648.9 µg/Kg-dry 1NDNELAP 69726
2-Chlorotoluene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
2-Hexanone 07/20/2011 16:4648.9 µg/Kg-dry 1NDNELAP 69726
2-Nitropropane 07/20/2011 16:4648.9 µg/Kg-dry 1NDNELAP 69726
4-Chlorotoluene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
4-Methyl-2-pentanone 07/20/2011 16:4648.9 µg/Kg-dry 1NDNELAP 69726
Acetone J 07/20/2011 16:4648.9 µg/Kg-dry 124NELAP 69726
Acrolein 07/20/2011 16:4697.8 µg/Kg-dry 1NDNELAP 69726
Acrylonitrile 07/20/2011 16:469.8 µg/Kg-dry 1NDNELAP 69726
Allyl chloride 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Benzene 07/20/2011 16:461.0 µg/Kg-dry 11.1NELAP 69726
Bromobenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Bromochloromethane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Bromodichloromethane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Bromoform 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Bromomethane 07/20/2011 16:469.8 µg/Kg-dry 1NDNELAP 69726
Carbon disulfide 07/20/2011 16:464.9 µg/Kg-dry 115.8NELAP 69726
Carbon tetrachloride 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Chlorobenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Chloroethane 07/20/2011 16:469.8 µg/Kg-dry 1NDNELAP 69726
Chloroform 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Chloromethane 07/20/2011 16:469.8 µg/Kg-dry 1151NELAP 69726
cis-1,2-Dichloroethene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
cis-1,3-Dichloropropene 07/20/2011 16:463.9 µg/Kg-dry 1NDNELAP 69726
Cyclohexanone 07/20/2011 16:4697.8 µg/Kg-dry 1ND 69726
Dibromochloromethane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Dibromomethane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Dichlorodifluoromethane 07/20/2011 16:469.8 µg/Kg-dry 1NDNELAP 69726
Ethyl acetate 07/20/2011 16:4648.9 µg/Kg-dry 1NDNELAP 69726
Ethyl ether 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Ethyl methacrylate 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Ethylbenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Heptane 07/20/2011 16:4619.6 µg/Kg-dry 1ND 69726
Hexachlorobutadiene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Hexachloroethane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Iodomethane 07/20/2011 16:469.8 µg/Kg-dry 1NDNELAP 69726
Isopropylbenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
m,p-Xylenes 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Methacrylonitrile 07/20/2011 16:4648.9 µg/Kg-dry 1NDNELAP 69726
Methyl Methacrylate 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Methyl tert-butyl ether 07/20/2011 16:462.0 µg/Kg-dry 1NDNELAP 69726
Page 9 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 10:00
Lab ID: 11070610-001 Client Sample ID: SBA-N4 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSMethylacrylate 07/20/2011 16:469.8 µg/Kg-dry 1ND 69726
Methylene chloride J 07/20/2011 16:464.9 µg/Kg-dry 11.5NELAP 69726
Naphthalene J 07/20/2011 16:469.8 µg/Kg-dry 14.4NELAP 69726
n-Butylbenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
n-Hexane J 07/20/2011 16:4619.6 µg/Kg-dry 13.1 69726
Nitrobenzene 07/20/2011 16:4697.8 µg/Kg-dry 1NDNELAP 69726
n-Propylbenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
o-Xylene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Pentachloroethane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
p-Isopropyltoluene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Propionitrile 07/20/2011 16:4648.9 µg/Kg-dry 1NDNELAP 69726
sec-Butylbenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Styrene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
tert-Butylbenzene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Tetrachloroethene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Tetrahydrofuran J 07/20/2011 16:4648.9 µg/Kg-dry 17.5NELAP 69726
Toluene J 07/20/2011 16:464.9 µg/Kg-dry 11.9NELAP 69726
trans-1,2-Dichloroethene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
trans-1,3-Dichloropropene 07/20/2011 16:463.9 µg/Kg-dry 1NDNELAP 69726
Trichloroethene 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Trichlorofluoromethane 07/20/2011 16:464.9 µg/Kg-dry 1NDNELAP 69726
Vinyl acetate 07/20/2011 16:4648.9 µg/Kg-dry 1NDNELAP 69726
Vinyl chloride 07/20/2011 16:462.0 µg/Kg-dry 1NDNELAP 69726
Surr: 1,2-Dichloroethane-d4 07/20/2011 16:4672.2-131 %REC 1121.6 69726
Surr: 4-Bromofluorobenzene 07/20/2011 16:4682.1-116 %REC 1107.4 69726
Surr: Dibromofluoromethane 07/20/2011 16:4677.7-120 %REC 1104.6 69726
Surr: Toluene-d8 07/20/2011 16:4686-116 %REC 1105.1 69726
SW-846 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 07/22/2011 21:060.05 mg/Kg-dry 1NDNELAP R152491
2,4,5-TP (Silvex) 07/22/2011 21:060.05 mg/Kg-dry 1NDNELAP R152491
2,4-D 07/22/2011 21:060.05 mg/Kg-dry 1NDNELAP R152491
2,4-DB 07/22/2011 21:060.05 mg/Kg-dry 1NDNELAP R152491
3,5-Dichlorobenzoic Acid 07/22/2011 21:060.05 mg/Kg-dry 1NDNELAP R152491
Acifluorfen 07/22/2011 21:060.05 mg/Kg-dry 1NDNELAP R152491
Bentazon 07/22/2011 21:060.05 mg/Kg-dry 1NDNELAP R152491
Chloramben 07/22/2011 21:060.05 mg/Kg-dry 1NDNELAP R152491
Dalapon 07/22/2011 21:060.05 mg/Kg-dry 1NDNELAP R152491
DCPA 07/22/2011 21:060.05 mg/Kg-dry 1NDNELAP R152491
Dicamba 07/22/2011 21:060.05 mg/Kg-dry 1NDNELAP R152491
Dichlorprop 07/22/2011 21:060.05 mg/Kg-dry 1NDNELAP R152491
Dinoseb 07/22/2011 21:060.05 mg/Kg-dry 1NDNELAP R152491
Pentachlorophenol 07/22/2011 21:060.05 mg/Kg-dry 1NDNELAP R152491
Picloram 07/22/2011 21:060.05 mg/Kg-dry 1NDNELAP R152491
Surr: DCAA 07/22/2011 21:0624-140 %REC 1105.0 R152491
The LCS/LCSD RPD result exceeded the QC control limits for Dinoseb; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data.
Page 10 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 11:30
Lab ID: 11070610-002 Client Sample ID: SBA-K2 (4-5)
Matrix: SOLID
Batch
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 07/18/2011 10:000.1 % 116.1 R152055
STANDARD METHODS 18TH ED. 2540 GTotal Solids 07/18/2011 8:300.1 % 183.9 R152054
SW-846 9012A (TOTAL)Cyanide 07/19/2011 10:260.32 mg/Kg-dry 1< 0.32NELAP 69687
SW-846 3050B, 6010B, METALS BY ICPAluminum 07/19/2011 12:384.90 mg/Kg-dry 114800NELAP 69636
Antimony 07/27/2011 11:585.00 mg/Kg-dry 1< 5.00NELAP 69908
Arsenic 07/19/2011 12:382.45 mg/Kg-dry 113.4NELAP 69636
Barium 07/20/2011 15:180.49 mg/Kg-dry 176.1NELAP 69636
Beryllium 07/19/2011 12:380.10 mg/Kg-dry 10.60NELAP 69636
Cadmium 07/19/2011 12:380.20 mg/Kg-dry 10.33NELAP 69636
Calcium 07/19/2011 12:384.90 mg/Kg-dry 143700NELAP 69636
Chromium 07/19/2011 12:380.98 mg/Kg-dry 119.2NELAP 69636
Cobalt 07/19/2011 12:380.98 mg/Kg-dry 19.51NELAP 69636
Copper 07/19/2011 12:380.98 mg/Kg-dry 118.0NELAP 69636
Iron 07/19/2011 12:381.96 mg/Kg-dry 124300NELAP 69636
Lead 07/19/2011 12:383.92 mg/Kg-dry 117.3NELAP 69636
Magnesium 07/19/2011 12:380.98 mg/Kg-dry 115300NELAP 69636
Manganese 07/19/2011 12:380.49 mg/Kg-dry 1584NELAP 69636
Nickel 07/19/2011 12:380.98 mg/Kg-dry 121.0NELAP 69636
Potassium 07/20/2011 15:189.80 mg/Kg-dry 12520NELAP 69636
Silver 07/20/2011 15:180.54 mg/Kg-dry 1< 0.54NELAP 69636
Sodium 07/20/2011 15:184.90 mg/Kg-dry 1177NELAP 69636
Vanadium 07/19/2011 12:380.98 mg/Kg-dry 125.0NELAP 69636
Zinc 07/19/2011 12:380.98 mg/Kg-dry 164.6NELAP 69636
SW-846 3050B, METALS BY GFAASelenium 7740 07/19/2011 9:470.600 mg/Kg-dry 1< 0.600NELAP 69639
Thallium 7841 07/28/2011 9:190.200 mg/Kg-dry 10.358NELAP 69639
SW-846 7471AMercury 07/19/2011 12:250.012 mg/Kg-dry 10.123NELAP 69631
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel 07/19/2011 16:065.96 mg/Kg-dry 1NDNELAP 69637
Kerosene 07/19/2011 16:065.96 mg/Kg-dry 1NDNELAP 69637
Mineral Spirits 07/19/2011 16:065.96 mg/Kg-dry 1NDNELAP 69637
Motor Oil 07/19/2011 16:065.96 mg/Kg-dry 1NDNELAP 69637
Surr: n-Tetracontane 07/19/2011 16:0650.6-140 %REC 1116.8 69637
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/25/2011 22:2219.9 µg/Kg-dry 10NDNELAP 69671
4,4´-DDE 07/25/2011 22:2219.9 µg/Kg-dry 10NDNELAP 69671
4,4´-DDT 07/25/2011 22:2219.9 µg/Kg-dry 10NDNELAP 69671
Alachlor 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
Aldrin 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
alpha-BHC 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
alpha-Chlordane 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
beta-BHC 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
Page 11 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 11:30
Lab ID: 11070610-002 Client Sample ID: SBA-K2 (4-5)
Matrix: SOLID
Batch
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECDChlordane 07/21/2011 21:453.97 µg/Kg-dry 1NDNELAP 69671
delta-BHC 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
Dieldrin 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
Endosulfan I 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
Endosulfan II 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
Endosulfan sulfate 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
Endrin 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
Endrin aldehyde 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
Endrin ketone 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
gamma-BHC 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
gamma-Chlordane 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
Heptachlor 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
Heptachlor epoxide 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
Methoxychlor 07/21/2011 21:451.99 µg/Kg-dry 1NDNELAP 69671
Toxaphene 07/21/2011 21:4535.7 µg/Kg-dry 1NDNELAP 69671
Surr: Decachlorobiphenyl 07/21/2011 21:4548-149 %REC 198.4 69671
Surr: Tetrachloro-m-xylene 07/21/2011 21:4519-145 %REC 170.6 69671
Elevated reporting limit(s) due to sample extract composition.
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/20/2011 18:3644.6 µg/Kg-dry 1NDNELAP 69671
Aroclor 1221 07/20/2011 18:3644.6 µg/Kg-dry 1NDNELAP 69671
Aroclor 1232 07/20/2011 18:3644.6 µg/Kg-dry 1NDNELAP 69671
Aroclor 1242 07/20/2011 18:3644.6 µg/Kg-dry 1NDNELAP 69671
Aroclor 1248 07/20/2011 18:3644.6 µg/Kg-dry 1NDNELAP 69671
Aroclor 1254 07/20/2011 18:3644.6 µg/Kg-dry 1NDNELAP 69671
Aroclor 1260 07/20/2011 18:3644.6 µg/Kg-dry 1NDNELAP 69671
Surr: Decachlorobiphenyl 07/20/2011 18:365-156 %REC 197.5 69671
Surr: Tetrachloro-meta-xylene 07/20/2011 18:367.35-123 %REC 170.1 69671
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/20/2011 3:410.004 mg/Kg-dry 1NDNELAP 69628
Acenaphthylene 07/20/2011 3:410.004 mg/Kg-dry 1NDNELAP 69628
Anthracene 07/20/2011 3:410.004 mg/Kg-dry 1NDNELAP 69628
Benzo(a)anthracene 07/20/2011 3:410.004 mg/Kg-dry 10.017NELAP 69628
Benzo(a)pyrene 07/20/2011 3:410.004 mg/Kg-dry 10.014NELAP 69628
Benzo(b)fluoranthene 07/20/2011 3:410.004 mg/Kg-dry 10.022NELAP 69628
Benzo(g,h,i)perylene R 07/20/2011 3:410.004 mg/Kg-dry 10.007NELAP 69628
Benzo(k)fluoranthene 07/20/2011 3:410.004 mg/Kg-dry 10.009NELAP 69628
Bis(2-ethylhexyl)phthalate J 07/20/2011 3:410.080 mg/Kg-dry 10.046NELAP 69628
Chrysene 07/20/2011 3:410.004 mg/Kg-dry 10.017NELAP 69628
Dibenzo(a,h)anthracene 07/20/2011 3:410.004 mg/Kg-dry 1NDNELAP 69628
Fluoranthene 07/20/2011 3:410.004 mg/Kg-dry 10.033NELAP 69628
Fluorene 07/20/2011 3:410.004 mg/Kg-dry 1NDNELAP 69628
Indeno(1,2,3-cd)pyrene 07/20/2011 3:410.004 mg/Kg-dry 10.006NELAP 69628
Naphthalene 07/20/2011 3:410.004 mg/Kg-dry 1NDNELAP 69628
Phenanthrene 07/20/2011 3:410.004 mg/Kg-dry 10.015NELAP 69628
Pyrene 07/20/2011 3:410.004 mg/Kg-dry 10.027NELAP 69628
Surr: 2-Fluorobiphenyl 07/20/2011 3:4110-131 %REC 159.1 69628
Page 12 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 11:30
Lab ID: 11070610-002 Client Sample ID: SBA-K2 (4-5)
Matrix: SOLID
Batch
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: Nitrobenzene-d5 07/20/2011 3:4110-132 %REC 176.3 69628
Surr: p-Terphenyl-d14 S 07/20/2011 3:4180.2-138 %REC 176.7 69628
Surrogate recovery was outside QC limits due to matrix interference.Benzo(g,h,i)perylene RPD for MS/MSD was outside of QC limit due to sample composition.
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
1,2-Dichlorobenzene 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
1,3-Dichlorobenzene 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
1,4-Dichlorobenzene 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
2,4,5-Trichlorophenol 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
2,4,6-Trichlorophenol 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
2,4-Dichlorophenol 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
2,4-Dimethylphenol 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
2,4-Dinitrophenol 07/19/2011 10:251.19 mg/Kg-dry 1NDNELAP 69627
2,4-Dinitrotoluene 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
2,6-Dinitrotoluene 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
2-Chloronaphthalene 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
2-Chlorophenol 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
2-Methoxy-4-methylphenol 07/19/2011 10:250.774 mg/Kg-dry 1ND 69627
2-Methylnaphthalene 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
2-Nitroaniline 07/19/2011 10:251.19 mg/Kg-dry 1NDNELAP 69627
2-Nitrophenol 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
3,3´-Dichlorobenzidine 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
3-Nitroaniline 07/19/2011 10:251.19 mg/Kg-dry 1NDNELAP 69627
4,6-Dinitro-2-methylphenol 07/19/2011 10:251.19 mg/Kg-dry 1NDNELAP 69627
4-Bromophenyl phenyl ether 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
4-Chloro-3-methylphenol 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
4-Chloroaniline 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
4-Chlorophenyl phenyl ether 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
4-Nitroaniline 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
4-Nitrophenol 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
Aniline 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
Azobenzene 07/19/2011 10:250.417 mg/Kg-dry 1ND 69627
Benzidine 07/19/2011 10:251.26 mg/Kg-dry 1see noteNELAP 69627
Benzoic acid 07/19/2011 10:251.79 mg/Kg-dry 1NDNELAP 69627
Benzyl alcohol 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroethoxy)methane 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroethyl)ether 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroisopropyl)ether 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
Butyl benzyl phthalate 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
Carbazole 07/19/2011 10:250.595 mg/Kg-dry 1ND 69627
Dibenzofuran 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
Diethyl phthalate 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
Dimethyl phthalate 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
Di-n-butyl phthalate 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
Di-n-octyl phthalate 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
Hexachlorobenzene 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
Page 13 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 11:30
Lab ID: 11070610-002 Client Sample ID: SBA-K2 (4-5)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachlorobutadiene 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
Hexachlorocyclopentadiene 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
Hexachloroethane 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
Isophorone 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
m,p-Cresol 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
Nitrobenzene 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
N-Nitrosodimethylamine 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
N-Nitroso-di-n-propylamine 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
N-Nitrosodiphenylamine 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
o-Cresol 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
Pentachlorophenol 07/19/2011 10:252.38 mg/Kg-dry 1NDNELAP 69627
Phenol 07/19/2011 10:250.417 mg/Kg-dry 1NDNELAP 69627
Pyridine 07/19/2011 10:250.595 mg/Kg-dry 1NDNELAP 69627
1,2-Diphenylhydrazine 07/19/2011 10:251.00 mg/Kg-dry 1ND 69627
Surr: 2,4,6-Tribromophenol 07/19/2011 10:2532.7-130 %REC 177.1 69627
Surr: 2-Fluorobiphenyl 07/19/2011 10:2534.1-116 %REC 164.5 69627
Surr: 2-Fluorophenol 07/19/2011 10:2530.5-99 %REC 171.9 69627
Surr: Nitrobenzene-d5 07/19/2011 10:2534.1-101 %REC 178.0 69627
Surr: Phenol-d5 07/19/2011 10:2534.9-110 %REC 171.8 69627
Surr: p-Terphenyl-d14 07/19/2011 10:2541.7-124 %REC 186.3 69627
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.4-Nitrophenol was outside upper QC limits in the LCS. Sample was ND.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,1,1-Trichloroethane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,1,2,2-Tetrachloroethane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,1,2-Trichloro-1,2,2-trifluoroethane 07/20/2011 17:164.5 µg/Kg-dry 1ND 69726
1,1,2-Trichloroethane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,1-Dichloro-2-propanone 07/20/2011 17:1644.7 µg/Kg-dry 1ND 69726
1,1-Dichloroethane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,1-Dichloroethene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,1-Dichloropropene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,2,3-Trichlorobenzene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,2,3-Trichloropropane 07/20/2011 17:168.9 µg/Kg-dry 1NDNELAP 69726
1,2,3-Trimethylbenzene 07/20/2011 17:164.5 µg/Kg-dry 1ND 69726
1,2,4-Trichlorobenzene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,2,4-Trimethylbenzene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,2-Dibromo-3-chloropropane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,2-Dibromoethane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,2-Dichlorobenzene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,2-Dichloroethane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,2-Dichloropropane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,3,5-Trimethylbenzene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,3-Dichlorobenzene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,3-Dichloropropane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1,4-Dichlorobenzene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
1-Chlorobutane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Page 14 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 11:30
Lab ID: 11070610-002 Client Sample ID: SBA-K2 (4-5)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS2,2-Dichloropropane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
2-Butanone 07/20/2011 17:1644.7 µg/Kg-dry 1NDNELAP 69726
2-Chlorotoluene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
2-Hexanone 07/20/2011 17:1644.7 µg/Kg-dry 1NDNELAP 69726
2-Nitropropane 07/20/2011 17:1644.7 µg/Kg-dry 1NDNELAP 69726
4-Chlorotoluene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
4-Methyl-2-pentanone 07/20/2011 17:1644.7 µg/Kg-dry 1NDNELAP 69726
Acetone J 07/20/2011 17:1644.7 µg/Kg-dry 126NELAP 69726
Acrolein 07/20/2011 17:1689.3 µg/Kg-dry 1NDNELAP 69726
Acrylonitrile 07/20/2011 17:168.9 µg/Kg-dry 1NDNELAP 69726
Allyl chloride 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Benzene 07/20/2011 17:160.9 µg/Kg-dry 11.9NELAP 69726
Bromobenzene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Bromochloromethane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Bromodichloromethane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Bromoform 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Bromomethane 07/20/2011 17:168.9 µg/Kg-dry 1NDNELAP 69726
Carbon disulfide J 07/20/2011 17:164.5 µg/Kg-dry 14.1NELAP 69726
Carbon tetrachloride 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Chlorobenzene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Chloroethane 07/20/2011 17:168.9 µg/Kg-dry 1NDNELAP 69726
Chloroform 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Chloromethane 07/20/2011 17:168.9 µg/Kg-dry 1NDNELAP 69726
cis-1,2-Dichloroethene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
cis-1,3-Dichloropropene 07/20/2011 17:163.6 µg/Kg-dry 1NDNELAP 69726
Cyclohexanone 07/20/2011 17:1689.3 µg/Kg-dry 1ND 69726
Dibromochloromethane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Dibromomethane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Dichlorodifluoromethane 07/20/2011 17:168.9 µg/Kg-dry 1NDNELAP 69726
Ethyl acetate 07/20/2011 17:1644.7 µg/Kg-dry 1NDNELAP 69726
Ethyl ether 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Ethyl methacrylate 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Ethylbenzene J 07/20/2011 17:164.5 µg/Kg-dry 11.3NELAP 69726
Heptane J 07/20/2011 17:1617.9 µg/Kg-dry 13.1 69726
Hexachlorobutadiene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Hexachloroethane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Iodomethane 07/20/2011 17:168.9 µg/Kg-dry 1NDNELAP 69726
Isopropylbenzene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
m,p-Xylenes J 07/20/2011 17:164.5 µg/Kg-dry 12.0NELAP 69726
Methacrylonitrile 07/20/2011 17:1644.7 µg/Kg-dry 1NDNELAP 69726
Methyl Methacrylate 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Methyl tert-butyl ether 07/20/2011 17:161.8 µg/Kg-dry 1NDNELAP 69726
Methylacrylate 07/20/2011 17:168.9 µg/Kg-dry 1ND 69726
Methylene chloride J 07/20/2011 17:164.5 µg/Kg-dry 12.1NELAP 69726
Naphthalene 07/20/2011 17:168.9 µg/Kg-dry 1NDNELAP 69726
n-Butylbenzene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
n-Hexane J 07/20/2011 17:1617.9 µg/Kg-dry 14.9 69726
Page 15 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 11:30
Lab ID: 11070610-002 Client Sample ID: SBA-K2 (4-5)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSNitrobenzene 07/20/2011 17:1689.3 µg/Kg-dry 1NDNELAP 69726
n-Propylbenzene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
o-Xylene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Pentachloroethane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
p-Isopropyltoluene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Propionitrile 07/20/2011 17:1644.7 µg/Kg-dry 1NDNELAP 69726
sec-Butylbenzene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Styrene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
tert-Butylbenzene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Tetrachloroethene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Tetrahydrofuran J 07/20/2011 17:1644.7 µg/Kg-dry 114NELAP 69726
Toluene 07/20/2011 17:164.5 µg/Kg-dry 14.6NELAP 69726
trans-1,2-Dichloroethene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
trans-1,3-Dichloropropene 07/20/2011 17:163.6 µg/Kg-dry 1NDNELAP 69726
Trichloroethene 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Trichlorofluoromethane 07/20/2011 17:164.5 µg/Kg-dry 1NDNELAP 69726
Vinyl acetate 07/20/2011 17:1644.7 µg/Kg-dry 1NDNELAP 69726
Vinyl chloride 07/20/2011 17:161.8 µg/Kg-dry 1NDNELAP 69726
Surr: 1,2-Dichloroethane-d4 07/20/2011 17:1672.2-131 %REC 1119.9 69726
Surr: 4-Bromofluorobenzene 07/20/2011 17:1682.1-116 %REC 1105.1 69726
Surr: Dibromofluoromethane 07/20/2011 17:1677.7-120 %REC 1107.1 69726
Surr: Toluene-d8 07/20/2011 17:1686-116 %REC 1107.3 69726
SW-846 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 07/22/2011 21:530.05 mg/Kg-dry 1NDNELAP R152491
2,4,5-TP (Silvex) 07/22/2011 21:530.05 mg/Kg-dry 1NDNELAP R152491
2,4-D 07/22/2011 21:530.05 mg/Kg-dry 1NDNELAP R152491
2,4-DB 07/22/2011 21:530.05 mg/Kg-dry 1NDNELAP R152491
3,5-Dichlorobenzoic Acid 07/22/2011 21:530.05 mg/Kg-dry 1NDNELAP R152491
Acifluorfen 07/22/2011 21:530.05 mg/Kg-dry 1NDNELAP R152491
Bentazon 07/22/2011 21:530.05 mg/Kg-dry 1NDNELAP R152491
Chloramben 07/22/2011 21:530.05 mg/Kg-dry 1NDNELAP R152491
Dalapon 07/22/2011 21:530.05 mg/Kg-dry 1NDNELAP R152491
DCPA 07/22/2011 21:530.05 mg/Kg-dry 1NDNELAP R152491
Dicamba 07/22/2011 21:530.05 mg/Kg-dry 1NDNELAP R152491
Dichlorprop 07/22/2011 21:530.05 mg/Kg-dry 1NDNELAP R152491
Dinoseb 07/22/2011 21:530.05 mg/Kg-dry 1NDNELAP R152491
Pentachlorophenol 07/22/2011 21:530.05 mg/Kg-dry 1NDNELAP R152491
Picloram 07/22/2011 21:530.05 mg/Kg-dry 1NDNELAP R152491
Surr: DCAA 07/22/2011 21:5324-140 %REC 176.5 R152491
The LCS/LCSD RPD result exceeded the QC control limits for Dinoseb; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data.
Page 16 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 13:15
Lab ID: 11070610-003 Client Sample ID: SBA-J5 (5-6)
Matrix: SOLID
Batch
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 07/18/2011 10:000.1 % 123.6 R152055
STANDARD METHODS 18TH ED. 2540 GTotal Solids 07/18/2011 8:300.1 % 176.4 R152054
SW-846 9012A (TOTAL)Cyanide 07/19/2011 10:260.34 mg/Kg-dry 1< 0.34NELAP 69687
SW-846 3050B, 6010B, METALS BY ICPAluminum 07/19/2011 12:444.90 mg/Kg-dry 115500NELAP 69636
Antimony 07/27/2011 12:165.00 mg/Kg-dry 1< 5.00NELAP 69908
Arsenic 07/19/2011 12:442.45 mg/Kg-dry 114.8NELAP 69636
Barium 07/20/2011 15:340.49 mg/Kg-dry 1117NELAP 69636
Beryllium 07/19/2011 12:440.10 mg/Kg-dry 10.68NELAP 69636
Cadmium 07/19/2011 12:440.20 mg/Kg-dry 10.62NELAP 69636
Calcium 07/19/2011 12:444.90 mg/Kg-dry 138800NELAP 69636
Chromium 07/19/2011 12:440.98 mg/Kg-dry 119.9NELAP 69636
Cobalt 07/19/2011 12:440.98 mg/Kg-dry 110.7NELAP 69636
Copper 07/19/2011 12:440.98 mg/Kg-dry 121.3NELAP 69636
Iron 07/19/2011 12:441.96 mg/Kg-dry 127200NELAP 69636
Lead 07/19/2011 12:443.92 mg/Kg-dry 119.6NELAP 69636
Magnesium 07/19/2011 12:440.98 mg/Kg-dry 114800NELAP 69636
Manganese 07/19/2011 12:440.49 mg/Kg-dry 11440NELAP 69636
Nickel 07/19/2011 12:440.98 mg/Kg-dry 128.9NELAP 69636
Potassium 07/20/2011 15:349.80 mg/Kg-dry 12670NELAP 69636
Silver 07/20/2011 15:340.54 mg/Kg-dry 1< 0.54NELAP 69636
Sodium 07/20/2011 15:344.90 mg/Kg-dry 1297NELAP 69636
Vanadium 07/19/2011 12:440.98 mg/Kg-dry 127.9NELAP 69636
Zinc 07/19/2011 12:440.98 mg/Kg-dry 170.9NELAP 69636
SW-846 3050B, METALS BY GFAASelenium 7740 07/19/2011 9:500.556 mg/Kg-dry 1< 0.556NELAP 69639
Thallium 7841 07/28/2011 9:220.185 mg/Kg-dry 10.349NELAP 69639
SW-846 7471AMercury 07/19/2011 12:250.013 mg/Kg-dry 10.032NELAP 69631
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel 07/19/2011 16:426.52 mg/Kg-dry 1NDNELAP 69637
Kerosene 07/19/2011 16:426.52 mg/Kg-dry 1NDNELAP 69637
Mineral Spirits 07/19/2011 16:426.52 mg/Kg-dry 1NDNELAP 69637
Motor Oil 07/19/2011 16:426.52 mg/Kg-dry 1NDNELAP 69637
Surr: n-Tetracontane 07/19/2011 16:4250.6-140 %REC 1110.4 69637
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/25/2011 22:4821.9 µg/Kg-dry 10NDNELAP 69671
4,4´-DDE 07/25/2011 22:4821.9 µg/Kg-dry 10NDNELAP 69671
4,4´-DDT 07/25/2011 22:4821.9 µg/Kg-dry 10NDNELAP 69671
Alachlor 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
Aldrin 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
alpha-BHC 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
alpha-Chlordane 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
beta-BHC 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
Page 17 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 13:15
Lab ID: 11070610-003 Client Sample ID: SBA-J5 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECDChlordane 07/21/2011 22:114.37 µg/Kg-dry 1NDNELAP 69671
delta-BHC 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
Dieldrin 07/21/2011 22:112.19 µg/Kg-dry 15.39NELAP 69671
Endosulfan I 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
Endosulfan II 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
Endosulfan sulfate 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
Endrin 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
Endrin aldehyde 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
Endrin ketone 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
gamma-BHC 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
gamma-Chlordane 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
Heptachlor 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
Heptachlor epoxide 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
Methoxychlor 07/21/2011 22:112.19 µg/Kg-dry 1NDNELAP 69671
Toxaphene 07/21/2011 22:1139.3 µg/Kg-dry 1NDNELAP 69671
Surr: Decachlorobiphenyl 07/21/2011 22:1148-149 %REC 162.3 69671
Surr: Tetrachloro-m-xylene 07/21/2011 22:1119-145 %REC 148.9 69671
Elevated reporting limit(s) due to sample extract composition.
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/20/2011 18:5449.1 µg/Kg-dry 1NDNELAP 69671
Aroclor 1221 07/20/2011 18:5449.1 µg/Kg-dry 1NDNELAP 69671
Aroclor 1232 07/20/2011 18:5449.1 µg/Kg-dry 1NDNELAP 69671
Aroclor 1242 07/20/2011 18:5449.1 µg/Kg-dry 1NDNELAP 69671
Aroclor 1248 07/20/2011 18:5449.1 µg/Kg-dry 1NDNELAP 69671
Aroclor 1254 07/20/2011 18:5449.1 µg/Kg-dry 1NDNELAP 69671
Aroclor 1260 07/20/2011 18:5449.1 µg/Kg-dry 1NDNELAP 69671
Surr: Decachlorobiphenyl 07/20/2011 18:545-156 %REC 161.1 69671
Surr: Tetrachloro-meta-xylene 07/20/2011 18:547.35-123 %REC 145.6 69671
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/21/2011 6:020.004 mg/Kg-dry 1NDNELAP 69628
Acenaphthylene 07/21/2011 6:020.004 mg/Kg-dry 1NDNELAP 69628
Anthracene 07/21/2011 6:020.004 mg/Kg-dry 1NDNELAP 69628
Benzo(a)anthracene 07/21/2011 6:020.004 mg/Kg-dry 10.006NELAP 69628
Benzo(a)pyrene 07/21/2011 6:020.004 mg/Kg-dry 1NDNELAP 69628
Benzo(b)fluoranthene 07/21/2011 6:020.004 mg/Kg-dry 10.007NELAP 69628
Benzo(g,h,i)perylene 07/21/2011 6:020.004 mg/Kg-dry 1NDNELAP 69628
Benzo(k)fluoranthene 07/21/2011 6:020.004 mg/Kg-dry 1NDNELAP 69628
Bis(2-ethylhexyl)phthalate 07/21/2011 6:020.088 mg/Kg-dry 1NDNELAP 69628
Chrysene 07/21/2011 6:020.004 mg/Kg-dry 1NDNELAP 69628
Dibenzo(a,h)anthracene 07/21/2011 6:020.004 mg/Kg-dry 1NDNELAP 69628
Fluoranthene 07/21/2011 6:020.004 mg/Kg-dry 10.008NELAP 69628
Fluorene 07/21/2011 6:020.004 mg/Kg-dry 1NDNELAP 69628
Indeno(1,2,3-cd)pyrene 07/21/2011 6:020.004 mg/Kg-dry 1NDNELAP 69628
Naphthalene 07/21/2011 6:020.004 mg/Kg-dry 1NDNELAP 69628
Phenanthrene 07/21/2011 6:020.004 mg/Kg-dry 1NDNELAP 69628
Pyrene 07/21/2011 6:020.004 mg/Kg-dry 10.007NELAP 69628
Surr: 2-Fluorobiphenyl 07/21/2011 6:0210-131 %REC 163.9 69628
Page 18 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 13:15
Lab ID: 11070610-003 Client Sample ID: SBA-J5 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: Nitrobenzene-d5 07/21/2011 6:0210-132 %REC 172.9 69628
Surr: p-Terphenyl-d14 07/21/2011 6:0280.2-138 %REC 187.2 69628
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
1,2-Dichlorobenzene 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
1,3-Dichlorobenzene 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
1,4-Dichlorobenzene 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
2,4,5-Trichlorophenol 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
2,4,6-Trichlorophenol 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
2,4-Dichlorophenol 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
2,4-Dimethylphenol 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
2,4-Dinitrophenol 07/19/2011 10:571.31 mg/Kg-dry 1NDNELAP 69627
2,4-Dinitrotoluene 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
2,6-Dinitrotoluene 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
2-Chloronaphthalene 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
2-Chlorophenol 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
2-Methoxy-4-methylphenol 07/19/2011 10:570.851 mg/Kg-dry 1ND 69627
2-Methylnaphthalene 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
2-Nitroaniline 07/19/2011 10:571.31 mg/Kg-dry 1NDNELAP 69627
2-Nitrophenol 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
3,3´-Dichlorobenzidine 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
3-Nitroaniline 07/19/2011 10:571.31 mg/Kg-dry 1NDNELAP 69627
4,6-Dinitro-2-methylphenol 07/19/2011 10:571.31 mg/Kg-dry 1NDNELAP 69627
4-Bromophenyl phenyl ether 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
4-Chloro-3-methylphenol 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
4-Chloroaniline 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
4-Chlorophenyl phenyl ether 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
4-Nitroaniline 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
4-Nitrophenol 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
Aniline 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
Azobenzene 07/19/2011 10:570.458 mg/Kg-dry 1ND 69627
Benzidine 07/19/2011 10:571.38 mg/Kg-dry 1see noteNELAP 69627
Benzoic acid 07/19/2011 10:571.96 mg/Kg-dry 1NDNELAP 69627
Benzyl alcohol 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroethoxy)methane 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroethyl)ether 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroisopropyl)ether 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
Butyl benzyl phthalate 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
Carbazole 07/19/2011 10:570.655 mg/Kg-dry 1ND 69627
Dibenzofuran 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
Diethyl phthalate 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
Dimethyl phthalate 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
Di-n-butyl phthalate 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
Di-n-octyl phthalate 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
Hexachlorobenzene 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
Hexachlorobutadiene 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
Hexachlorocyclopentadiene 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
Page 19 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 13:15
Lab ID: 11070610-003 Client Sample ID: SBA-J5 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachloroethane 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
Isophorone 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
m,p-Cresol 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
Nitrobenzene 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
N-Nitrosodimethylamine 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
N-Nitroso-di-n-propylamine 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
N-Nitrosodiphenylamine 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
o-Cresol 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
Pentachlorophenol 07/19/2011 10:572.62 mg/Kg-dry 1NDNELAP 69627
Phenol 07/19/2011 10:570.458 mg/Kg-dry 1NDNELAP 69627
Pyridine 07/19/2011 10:570.655 mg/Kg-dry 1NDNELAP 69627
1,2-Diphenylhydrazine 07/19/2011 10:571.10 mg/Kg-dry 1ND 69627
Surr: 2,4,6-Tribromophenol 07/19/2011 10:5732.7-130 %REC 177.6 69627
Surr: 2-Fluorobiphenyl 07/19/2011 10:5734.1-116 %REC 165.3 69627
Surr: 2-Fluorophenol 07/19/2011 10:5730.5-99 %REC 169.8 69627
Surr: Nitrobenzene-d5 07/19/2011 10:5734.1-101 %REC 177.9 69627
Surr: Phenol-d5 07/19/2011 10:5734.9-110 %REC 170.6 69627
Surr: p-Terphenyl-d14 07/19/2011 10:5741.7-124 %REC 190.0 69627
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.4-Nitrophenol was outside upper QC limits in the LCS. Sample was ND.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,1,1-Trichloroethane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,1,2,2-Tetrachloroethane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,1,2-Trichloro-1,2,2-trifluoroethane 07/20/2011 17:465.0 µg/Kg-dry 1ND 69726
1,1,2-Trichloroethane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,1-Dichloro-2-propanone 07/20/2011 17:4650.2 µg/Kg-dry 1ND 69726
1,1-Dichloroethane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,1-Dichloroethene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,1-Dichloropropene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,2,3-Trichlorobenzene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,2,3-Trichloropropane 07/20/2011 17:4610.0 µg/Kg-dry 1NDNELAP 69726
1,2,3-Trimethylbenzene 07/20/2011 17:465.0 µg/Kg-dry 1ND 69726
1,2,4-Trichlorobenzene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,2,4-Trimethylbenzene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,2-Dibromo-3-chloropropane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,2-Dibromoethane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,2-Dichlorobenzene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,2-Dichloroethane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,2-Dichloropropane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,3,5-Trimethylbenzene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,3-Dichlorobenzene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,3-Dichloropropane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1,4-Dichlorobenzene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
1-Chlorobutane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
2,2-Dichloropropane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
2-Butanone 07/20/2011 17:4650.2 µg/Kg-dry 1NDNELAP 69726
Page 20 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 13:15
Lab ID: 11070610-003 Client Sample ID: SBA-J5 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS2-Chlorotoluene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
2-Hexanone 07/20/2011 17:4650.2 µg/Kg-dry 1NDNELAP 69726
2-Nitropropane 07/20/2011 17:4650.2 µg/Kg-dry 1NDNELAP 69726
4-Chlorotoluene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
4-Methyl-2-pentanone 07/20/2011 17:4650.2 µg/Kg-dry 1NDNELAP 69726
Acetone J 07/20/2011 17:4650.2 µg/Kg-dry 129NELAP 69726
Acrolein 07/20/2011 17:46100 µg/Kg-dry 1NDNELAP 69726
Acrylonitrile 07/20/2011 17:4610.0 µg/Kg-dry 1NDNELAP 69726
Allyl chloride 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Benzene 07/20/2011 17:461.0 µg/Kg-dry 11.7NELAP 69726
Bromobenzene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Bromochloromethane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Bromodichloromethane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Bromoform 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Bromomethane 07/20/2011 17:4610.0 µg/Kg-dry 1NDNELAP 69726
Carbon disulfide 07/20/2011 17:465.0 µg/Kg-dry 113.3NELAP 69726
Carbon tetrachloride 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Chlorobenzene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Chloroethane 07/20/2011 17:4610.0 µg/Kg-dry 1NDNELAP 69726
Chloroform 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Chloromethane 07/20/2011 17:4610.0 µg/Kg-dry 1NDNELAP 69726
cis-1,2-Dichloroethene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
cis-1,3-Dichloropropene 07/20/2011 17:464.0 µg/Kg-dry 1NDNELAP 69726
Cyclohexanone 07/20/2011 17:46100 µg/Kg-dry 1ND 69726
Dibromochloromethane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Dibromomethane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Dichlorodifluoromethane 07/20/2011 17:4610.0 µg/Kg-dry 1NDNELAP 69726
Ethyl acetate 07/20/2011 17:4650.2 µg/Kg-dry 1NDNELAP 69726
Ethyl ether 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Ethyl methacrylate 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Ethylbenzene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Heptane J 07/20/2011 17:4620.1 µg/Kg-dry 12.8 69726
Hexachlorobutadiene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Hexachloroethane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Iodomethane 07/20/2011 17:4610.0 µg/Kg-dry 1NDNELAP 69726
Isopropylbenzene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
m,p-Xylenes J 07/20/2011 17:465.0 µg/Kg-dry 11.3NELAP 69726
Methacrylonitrile 07/20/2011 17:4650.2 µg/Kg-dry 1NDNELAP 69726
Methyl Methacrylate 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Methyl tert-butyl ether 07/20/2011 17:462.0 µg/Kg-dry 1NDNELAP 69726
Methylacrylate 07/20/2011 17:4610.0 µg/Kg-dry 1ND 69726
Methylene chloride J 07/20/2011 17:465.0 µg/Kg-dry 11.9NELAP 69726
Naphthalene 07/20/2011 17:4610.0 µg/Kg-dry 1NDNELAP 69726
n-Butylbenzene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
n-Hexane J 07/20/2011 17:4620.1 µg/Kg-dry 14.7 69726
Nitrobenzene 07/20/2011 17:46100 µg/Kg-dry 1NDNELAP 69726
n-Propylbenzene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Page 21 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 13:15
Lab ID: 11070610-003 Client Sample ID: SBA-J5 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSo-Xylene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Pentachloroethane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
p-Isopropyltoluene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Propionitrile 07/20/2011 17:4650.2 µg/Kg-dry 1NDNELAP 69726
sec-Butylbenzene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Styrene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
tert-Butylbenzene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Tetrachloroethene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Tetrahydrofuran J 07/20/2011 17:4650.2 µg/Kg-dry 113NELAP 69726
Toluene J 07/20/2011 17:465.0 µg/Kg-dry 13.5NELAP 69726
trans-1,2-Dichloroethene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
trans-1,3-Dichloropropene 07/20/2011 17:464.0 µg/Kg-dry 1NDNELAP 69726
Trichloroethene 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Trichlorofluoromethane 07/20/2011 17:465.0 µg/Kg-dry 1NDNELAP 69726
Vinyl acetate 07/20/2011 17:4650.2 µg/Kg-dry 1NDNELAP 69726
Vinyl chloride 07/20/2011 17:462.0 µg/Kg-dry 1NDNELAP 69726
Surr: 1,2-Dichloroethane-d4 07/20/2011 17:4672.2-131 %REC 1118.6 69726
Surr: 4-Bromofluorobenzene 07/20/2011 17:4682.1-116 %REC 199.2 69726
Surr: Dibromofluoromethane 07/20/2011 17:4677.7-120 %REC 1106.0 69726
Surr: Toluene-d8 07/20/2011 17:4686-116 %REC 1112.8 69726
SW-846 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 07/22/2011 22:410.05 mg/Kg-dry 1NDNELAP R152491
2,4,5-TP (Silvex) 07/22/2011 22:410.05 mg/Kg-dry 1NDNELAP R152491
2,4-D 07/22/2011 22:410.05 mg/Kg-dry 1NDNELAP R152491
2,4-DB 07/22/2011 22:410.05 mg/Kg-dry 1NDNELAP R152491
3,5-Dichlorobenzoic Acid 07/22/2011 22:410.05 mg/Kg-dry 1NDNELAP R152491
Acifluorfen 07/22/2011 22:410.05 mg/Kg-dry 1NDNELAP R152491
Bentazon 07/22/2011 22:410.05 mg/Kg-dry 1NDNELAP R152491
Chloramben 07/22/2011 22:410.05 mg/Kg-dry 1NDNELAP R152491
Dalapon 07/22/2011 22:410.05 mg/Kg-dry 1NDNELAP R152491
DCPA 07/22/2011 22:410.05 mg/Kg-dry 1NDNELAP R152491
Dicamba 07/22/2011 22:410.05 mg/Kg-dry 1NDNELAP R152491
Dichlorprop 07/22/2011 22:410.05 mg/Kg-dry 1NDNELAP R152491
Dinoseb 07/22/2011 22:410.05 mg/Kg-dry 1NDNELAP R152491
Pentachlorophenol 07/22/2011 22:410.05 mg/Kg-dry 1NDNELAP R152491
Picloram 07/22/2011 22:410.05 mg/Kg-dry 1NDNELAP R152491
Surr: DCAA 07/22/2011 22:4124-140 %REC 184.2 R152491
The LCS/LCSD RPD result exceeded the QC control limits for Dinoseb; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data.
Page 22 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 14:30
Lab ID: 11070610-004 Client Sample ID: SBA-H3 (5-6)
Matrix: SOLID
Batch
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 07/18/2011 10:000.1 % 117.3 R152055
STANDARD METHODS 18TH ED. 2540 GTotal Solids 07/18/2011 8:300.1 % 182.7 R152054
SW-846 9012A (TOTAL)Cyanide J 07/19/2011 10:260.30 mg/Kg-dry 10.14NELAP 69687
SW-846 3050B, 6010B, METALS BY ICPAluminum 07/19/2011 13:004.81 mg/Kg-dry 111500NELAP 69636
Antimony J 07/27/2011 12:224.46 mg/Kg-dry 12.8NELAP 69908
Arsenic 07/19/2011 13:002.40 mg/Kg-dry 115.8NELAP 69636
Barium 07/20/2011 15:400.48 mg/Kg-dry 1134NELAP 69636
Beryllium 07/19/2011 13:000.10 mg/Kg-dry 10.66NELAP 69636
Cadmium 07/19/2011 13:000.19 mg/Kg-dry 11.34NELAP 69636
Calcium 07/19/2011 13:004.81 mg/Kg-dry 170900NELAP 69636
Chromium 07/19/2011 13:000.96 mg/Kg-dry 114.1NELAP 69636
Cobalt 07/19/2011 13:000.96 mg/Kg-dry 18.60NELAP 69636
Copper 07/19/2011 13:000.96 mg/Kg-dry 1155NELAP 69636
Iron 07/19/2011 13:001.92 mg/Kg-dry 127200NELAP 69636
Lead 07/19/2011 13:003.85 mg/Kg-dry 166.5NELAP 69636
Magnesium 07/19/2011 13:000.96 mg/Kg-dry 113500NELAP 69636
Manganese 07/19/2011 13:000.48 mg/Kg-dry 1717NELAP 69636
Nickel 07/19/2011 13:000.96 mg/Kg-dry 121.5NELAP 69636
Potassium 07/20/2011 15:409.62 mg/Kg-dry 11400NELAP 69636
Silver 07/20/2011 15:400.53 mg/Kg-dry 1< 0.53NELAP 69636
Sodium 07/20/2011 15:404.81 mg/Kg-dry 1262NELAP 69636
Vanadium 07/20/2011 15:400.96 mg/Kg-dry 125.6NELAP 69636
Zinc 07/19/2011 13:000.96 mg/Kg-dry 1132NELAP 69636
SW-846 3050B, METALS BY GFAASelenium 7740 07/19/2011 9:540.577 mg/Kg-dry 1< 0.577NELAP 69639
Thallium 7841 07/28/2011 9:260.192 mg/Kg-dry 10.263NELAP 69639
SW-846 7471AMercury 07/19/2011 12:250.012 mg/Kg-dry 10.136NELAP 69631
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel 07/19/2011 17:19301 mg/Kg-dry 50NDNELAP 69637
Kerosene 07/19/2011 17:19301 mg/Kg-dry 50NDNELAP 69637
Mineral Spirits 07/19/2011 17:19301 mg/Kg-dry 50NDNELAP 69637
Motor Oil 07/19/2011 17:19301 mg/Kg-dry 50NDNELAP 69637
Surr: n-Tetracontane S 07/19/2011 17:1950.6-140 %REC 500 69637
Surrogate recovery was outside QC limits due to matrix interference.Elevated reporting limit(s) due to sample extract composition.
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/25/2011 23:141010 µg/Kg-dry 500NDNELAP 69671
4,4´-DDE 07/25/2011 23:141010 µg/Kg-dry 500NDNELAP 69671
4,4´-DDT 07/25/2011 23:141010 µg/Kg-dry 500NDNELAP 69671
Alachlor 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
Aldrin 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
alpha-BHC 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
alpha-Chlordane 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
Page 23 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 14:30
Lab ID: 11070610-004 Client Sample ID: SBA-H3 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECDbeta-BHC 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
Chlordane 07/22/2011 14:1520.1 µg/Kg-dry 5NDNELAP 69671
delta-BHC 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
Dieldrin 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
Endosulfan I 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
Endosulfan II 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
Endosulfan sulfate 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
Endrin 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
Endrin aldehyde 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
Endrin ketone 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
gamma-BHC 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
gamma-Chlordane 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
Heptachlor 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
Heptachlor epoxide 07/22/2011 14:1510.1 µg/Kg-dry 5NDNELAP 69671
Methoxychlor 07/25/2011 23:141010 µg/Kg-dry 500NDNELAP 69671
Toxaphene 07/22/2011 14:15181 µg/Kg-dry 5NDNELAP 69671
Surr: Decachlorobiphenyl 07/22/2011 14:1548-149 %REC 598.0 69671
Surr: Tetrachloro-m-xylene 07/22/2011 14:1519-145 %REC 587.0 69671
Elevated reporting limit(s) due to sample extract composition.
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/20/2011 19:11452 µg/Kg-dry 10NDNELAP 69671
Aroclor 1221 07/20/2011 19:11452 µg/Kg-dry 10NDNELAP 69671
Aroclor 1232 07/20/2011 19:11452 µg/Kg-dry 10NDNELAP 69671
Aroclor 1242 07/20/2011 19:11452 µg/Kg-dry 10NDNELAP 69671
Aroclor 1248 07/20/2011 19:11452 µg/Kg-dry 10NDNELAP 69671
Aroclor 1254 07/20/2011 19:11452 µg/Kg-dry 10NDNELAP 69671
Aroclor 1260 07/20/2011 19:11452 µg/Kg-dry 10NDNELAP 69671
Surr: Decachlorobiphenyl 07/20/2011 19:115-156 %REC 1079.0 69671
Surr: Tetrachloro-meta-xylene 07/20/2011 19:117.35-123 %REC 1078.0 69671
Elevated reporting limit due to sample composition.
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/20/2011 6:420.411 mg/Kg-dry 100NDNELAP 69628
Acenaphthylene 07/20/2011 6:420.411 mg/Kg-dry 100NDNELAP 69628
Anthracene 07/20/2011 6:420.411 mg/Kg-dry 100NDNELAP 69628
Benzo(a)anthracene 07/20/2011 6:420.411 mg/Kg-dry 1001.09NELAP 69628
Benzo(a)pyrene 07/20/2011 6:420.411 mg/Kg-dry 1001.09NELAP 69628
Benzo(b)fluoranthene 07/20/2011 6:420.411 mg/Kg-dry 1001.61NELAP 69628
Benzo(g,h,i)perylene 07/20/2011 6:420.411 mg/Kg-dry 1000.443NELAP 69628
Benzo(k)fluoranthene 07/20/2011 6:420.411 mg/Kg-dry 1000.604NELAP 69628
Bis(2-ethylhexyl)phthalate 07/20/2011 6:428.10 mg/Kg-dry 100NDNELAP 69628
Chrysene 07/20/2011 6:420.411 mg/Kg-dry 1001.17NELAP 69628
Dibenzo(a,h)anthracene 07/20/2011 6:420.411 mg/Kg-dry 100NDNELAP 69628
Fluoranthene 07/20/2011 6:420.411 mg/Kg-dry 1001.77NELAP 69628
Fluorene 07/20/2011 6:420.411 mg/Kg-dry 100NDNELAP 69628
Indeno(1,2,3-cd)pyrene 07/20/2011 6:420.411 mg/Kg-dry 1000.443NELAP 69628
Naphthalene 07/20/2011 6:420.411 mg/Kg-dry 100NDNELAP 69628
Phenanthrene 07/20/2011 6:420.411 mg/Kg-dry 1000.725NELAP 69628
Page 24 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 14:30
Lab ID: 11070610-004 Client Sample ID: SBA-H3 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSPyrene 07/20/2011 6:420.411 mg/Kg-dry 1001.65NELAP 69628
Surr: 2-Fluorobiphenyl 07/20/2011 6:4210-131 %REC 10060.0 69628
Surr: Nitrobenzene-d5 07/20/2011 6:4210-132 %REC 10060.0 69628
Surr: p-Terphenyl-d14 S 07/20/2011 6:4280.2-138 %REC 10064.0 69628
Surrogate recovery was outside QC limits due to matrix interference.Elevated reporting limit(s) due to sample extract composition.
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
1,2-Dichlorobenzene 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
1,3-Dichlorobenzene 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
1,4-Dichlorobenzene 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
2,4,5-Trichlorophenol 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
2,4,6-Trichlorophenol 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
2,4-Dichlorophenol 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
2,4-Dimethylphenol 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
2,4-Dinitrophenol 07/20/2011 11:1460.4 mg/Kg-dry 50NDNELAP 69627
2,4-Dinitrotoluene 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
2,6-Dinitrotoluene 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
2-Chloronaphthalene 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
2-Chlorophenol 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
2-Methoxy-4-methylphenol 07/20/2011 11:1439.3 mg/Kg-dry 50ND 69627
2-Methylnaphthalene 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
2-Nitroaniline 07/20/2011 11:1460.4 mg/Kg-dry 50NDNELAP 69627
2-Nitrophenol 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
3,3´-Dichlorobenzidine 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
3-Nitroaniline 07/20/2011 11:1460.4 mg/Kg-dry 50NDNELAP 69627
4,6-Dinitro-2-methylphenol 07/20/2011 11:1460.4 mg/Kg-dry 50NDNELAP 69627
4-Bromophenyl phenyl ether 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
4-Chloro-3-methylphenol 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
4-Chloroaniline 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
4-Chlorophenyl phenyl ether 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
4-Nitroaniline 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
4-Nitrophenol 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
Aniline 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
Azobenzene 07/20/2011 11:1421.1 mg/Kg-dry 50ND 69627
Benzidine 07/20/2011 11:1463.8 mg/Kg-dry 50see noteNELAP 69627
Benzoic acid 07/20/2011 11:1490.6 mg/Kg-dry 50NDNELAP 69627
Benzyl alcohol 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
Bis(2-chloroethoxy)methane 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
Bis(2-chloroethyl)ether 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
Bis(2-chloroisopropyl)ether 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
Butyl benzyl phthalate 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
Carbazole 07/20/2011 11:1430.2 mg/Kg-dry 50ND 69627
Dibenzofuran 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
Diethyl phthalate 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
Dimethyl phthalate 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
Di-n-butyl phthalate 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
Page 25 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 14:30
Lab ID: 11070610-004 Client Sample ID: SBA-H3 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSDi-n-octyl phthalate 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
Hexachlorobenzene 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
Hexachlorobutadiene 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
Hexachlorocyclopentadiene 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
Hexachloroethane 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
Isophorone 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
m,p-Cresol 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
Nitrobenzene 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
N-Nitrosodimethylamine 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
N-Nitroso-di-n-propylamine 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
N-Nitrosodiphenylamine 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
o-Cresol 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
Pentachlorophenol 07/20/2011 11:14121 mg/Kg-dry 50NDNELAP 69627
Phenol 07/20/2011 11:1421.1 mg/Kg-dry 50NDNELAP 69627
Pyridine 07/20/2011 11:1430.2 mg/Kg-dry 50NDNELAP 69627
1,2-Diphenylhydrazine 07/20/2011 11:1450.7 mg/Kg-dry 50ND 69627
Surr: 2,4,6-Tribromophenol 07/20/2011 11:1432.7-130 %REC 5057.8 69627
Surr: 2-Fluorobiphenyl 07/20/2011 11:1434.1-116 %REC 5072.5 69627
Surr: 2-Fluorophenol 07/20/2011 11:1430.5-99 %REC 5058.8 69627
Surr: Nitrobenzene-d5 07/20/2011 11:1434.1-101 %REC 5074.5 69627
Surr: Phenol-d5 07/20/2011 11:1434.9-110 %REC 5064.6 69627
Surr: p-Terphenyl-d14 07/20/2011 11:1441.7-124 %REC 5077.0 69627
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.Elevated reporting limit(s) due to sample extract composition.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,1,1-Trichloroethane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,1,2,2-Tetrachloroethane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,1,2-Trichloro-1,2,2-trifluoroethane 07/21/2011 12:214.7 µg/Kg-dry 1ND 69790
1,1,2-Trichloroethane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,1-Dichloro-2-propanone 07/21/2011 12:2147.1 µg/Kg-dry 1ND 69790
1,1-Dichloroethane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,1-Dichloroethene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,1-Dichloropropene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,2,3-Trichlorobenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,2,3-Trichloropropane 07/21/2011 12:219.4 µg/Kg-dry 1NDNELAP 69790
1,2,3-Trimethylbenzene 07/21/2011 12:214.7 µg/Kg-dry 1ND 69790
1,2,4-Trichlorobenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,2,4-Trimethylbenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,2-Dibromo-3-chloropropane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,2-Dibromoethane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,2-Dichlorobenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,2-Dichloroethane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,2-Dichloropropane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,3,5-Trimethylbenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,3-Dichlorobenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1,3-Dichloropropane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Page 26 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 14:30
Lab ID: 11070610-004 Client Sample ID: SBA-H3 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,4-Dichlorobenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
1-Chlorobutane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
2,2-Dichloropropane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
2-Butanone 07/21/2011 12:2147.1 µg/Kg-dry 1NDNELAP 69790
2-Chlorotoluene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
2-Hexanone 07/21/2011 12:2147.1 µg/Kg-dry 1NDNELAP 69790
2-Nitropropane 07/21/2011 12:2147.1 µg/Kg-dry 1NDNELAP 69790
4-Chlorotoluene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
4-Methyl-2-pentanone 07/21/2011 12:2147.1 µg/Kg-dry 1NDNELAP 69790
Acetone 07/21/2011 12:2147.1 µg/Kg-dry 166.6NELAP 69790
Acrolein 07/21/2011 12:2194.2 µg/Kg-dry 1NDNELAP 69790
Acrylonitrile 07/21/2011 12:219.4 µg/Kg-dry 1NDNELAP 69790
Allyl chloride 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Benzene 07/21/2011 12:210.9 µg/Kg-dry 11.0NELAP 69790
Bromobenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Bromochloromethane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Bromodichloromethane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Bromoform 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Bromomethane 07/21/2011 12:219.4 µg/Kg-dry 1NDNELAP 69790
Carbon disulfide 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Carbon tetrachloride 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Chlorobenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Chloroethane 07/21/2011 12:219.4 µg/Kg-dry 1NDNELAP 69790
Chloroform 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Chloromethane 07/21/2011 12:219.4 µg/Kg-dry 1NDNELAP 69790
cis-1,2-Dichloroethene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
cis-1,3-Dichloropropene 07/21/2011 12:213.8 µg/Kg-dry 1NDNELAP 69790
Cyclohexanone 07/21/2011 12:2194.2 µg/Kg-dry 1ND 69790
Dibromochloromethane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Dibromomethane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Dichlorodifluoromethane 07/21/2011 12:219.4 µg/Kg-dry 1NDNELAP 69790
Ethyl acetate 07/21/2011 12:2147.1 µg/Kg-dry 1NDNELAP 69790
Ethyl ether 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Ethyl methacrylate 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Ethylbenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Heptane 07/21/2011 12:2118.8 µg/Kg-dry 1ND 69790
Hexachlorobutadiene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Hexachloroethane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Iodomethane 07/21/2011 12:219.4 µg/Kg-dry 1NDNELAP 69790
Isopropylbenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
m,p-Xylenes 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Methacrylonitrile 07/21/2011 12:2147.1 µg/Kg-dry 1NDNELAP 69790
Methyl Methacrylate 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Methyl tert-butyl ether 07/21/2011 12:211.9 µg/Kg-dry 1NDNELAP 69790
Methylacrylate 07/21/2011 12:219.4 µg/Kg-dry 1ND 69790
Methylene chloride J 07/21/2011 12:214.7 µg/Kg-dry 11.9NELAP 69790
Naphthalene 07/21/2011 12:219.4 µg/Kg-dry 1NDNELAP 69790
Page 27 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 14:30
Lab ID: 11070610-004 Client Sample ID: SBA-H3 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSn-Butylbenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
n-Hexane J 07/21/2011 12:2118.8 µg/Kg-dry 11.9 69790
Nitrobenzene 07/21/2011 12:2194.2 µg/Kg-dry 1NDNELAP 69790
n-Propylbenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
o-Xylene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Pentachloroethane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
p-Isopropyltoluene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Propionitrile 07/21/2011 12:2147.1 µg/Kg-dry 1NDNELAP 69790
sec-Butylbenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Styrene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
tert-Butylbenzene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Tetrachloroethene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Tetrahydrofuran J 07/21/2011 12:2147.1 µg/Kg-dry 112NELAP 69790
Toluene J 07/21/2011 12:214.7 µg/Kg-dry 11.5NELAP 69790
trans-1,2-Dichloroethene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
trans-1,3-Dichloropropene 07/21/2011 12:213.8 µg/Kg-dry 1NDNELAP 69790
Trichloroethene 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Trichlorofluoromethane 07/21/2011 12:214.7 µg/Kg-dry 1NDNELAP 69790
Vinyl acetate 07/21/2011 12:2147.1 µg/Kg-dry 1NDNELAP 69790
Vinyl chloride 07/21/2011 12:211.9 µg/Kg-dry 1NDNELAP 69790
Surr: 1,2-Dichloroethane-d4 07/21/2011 12:2172.2-131 %REC 1119.0 69790
Surr: 4-Bromofluorobenzene 07/21/2011 12:2182.1-116 %REC 193.8 69790
Surr: Dibromofluoromethane 07/21/2011 12:2177.7-120 %REC 1105.4 69790
Surr: Toluene-d8 S 07/21/2011 12:2186-116 %REC 1117.4 69790
Surrogate recovery and/or internal standard area was outside QC limits due to matrix interference.
SW-846 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 07/22/2011 23:280.05 mg/Kg-dry 1NDNELAP R152491
2,4,5-TP (Silvex) 07/22/2011 23:280.05 mg/Kg-dry 1NDNELAP R152491
2,4-D 07/22/2011 23:280.05 mg/Kg-dry 1NDNELAP R152491
2,4-DB 07/22/2011 23:280.05 mg/Kg-dry 1NDNELAP R152491
3,5-Dichlorobenzoic Acid 07/22/2011 23:280.05 mg/Kg-dry 1NDNELAP R152491
Acifluorfen 07/22/2011 23:280.05 mg/Kg-dry 1NDNELAP R152491
Bentazon 07/22/2011 23:280.05 mg/Kg-dry 1NDNELAP R152491
Chloramben 07/22/2011 23:280.05 mg/Kg-dry 1NDNELAP R152491
Dalapon 07/22/2011 23:280.05 mg/Kg-dry 1NDNELAP R152491
DCPA 07/22/2011 23:280.05 mg/Kg-dry 1NDNELAP R152491
Dicamba 07/22/2011 23:280.05 mg/Kg-dry 1NDNELAP R152491
Dichlorprop 07/22/2011 23:280.05 mg/Kg-dry 1NDNELAP R152491
Dinoseb 07/22/2011 23:280.05 mg/Kg-dry 1NDNELAP R152491
Pentachlorophenol 07/22/2011 23:280.05 mg/Kg-dry 1NDNELAP R152491
Picloram 07/22/2011 23:280.05 mg/Kg-dry 1NDNELAP R152491
Surr: DCAA 07/22/2011 23:2824-140 %REC 189.3 R152491
The LCS/LCSD RPD result exceeded the QC control limits for Dinoseb; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data.
Page 28 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 15:30
Lab ID: 11070610-005 Client Sample ID: SBA-F2 (4-5)
Matrix: SOLID
Batch
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 07/18/2011 10:000.1 % 122.6 R152055
STANDARD METHODS 18TH ED. 2540 GTotal Solids 07/18/2011 8:300.1 % 177.4 R152054
SW-846 9012A (TOTAL)Cyanide J 07/19/2011 10:260.34 mg/Kg-dry 10.15NELAP 69687
SW-846 3050B, 6010B, METALS BY ICPAluminum 07/19/2011 13:064.63 mg/Kg-dry 119400NELAP 69636
Antimony 07/27/2011 12:284.90 mg/Kg-dry 1< 4.90NELAP 69908
Arsenic 07/19/2011 13:062.31 mg/Kg-dry 110.8NELAP 69636
Barium 07/20/2011 15:460.46 mg/Kg-dry 1129NELAP 69636
Beryllium 07/19/2011 13:060.09 mg/Kg-dry 10.83NELAP 69636
Cadmium 07/19/2011 13:060.19 mg/Kg-dry 10.42NELAP 69636
Calcium 07/19/2011 13:064.63 mg/Kg-dry 131800NELAP 69636
Chromium 07/19/2011 13:060.93 mg/Kg-dry 119.9NELAP 69636
Cobalt 07/19/2011 13:060.93 mg/Kg-dry 19.89NELAP 69636
Copper 07/19/2011 13:060.93 mg/Kg-dry 121.5NELAP 69636
Iron 07/19/2011 13:061.85 mg/Kg-dry 124100NELAP 69636
Lead 07/19/2011 13:063.70 mg/Kg-dry 137.5NELAP 69636
Magnesium 07/19/2011 13:060.93 mg/Kg-dry 113200NELAP 69636
Manganese 07/19/2011 13:060.46 mg/Kg-dry 1568NELAP 69636
Nickel 07/19/2011 13:060.93 mg/Kg-dry 119.6NELAP 69636
Potassium 07/20/2011 15:469.26 mg/Kg-dry 12540NELAP 69636
Silver 07/20/2011 15:460.51 mg/Kg-dry 1< 0.51NELAP 69636
Sodium 07/20/2011 15:464.63 mg/Kg-dry 1233NELAP 69636
Vanadium 07/20/2011 15:460.93 mg/Kg-dry 133.8NELAP 69636
Zinc 07/19/2011 13:060.93 mg/Kg-dry 187.6NELAP 69636
SW-846 3050B, METALS BY GFAASelenium 7740 07/19/2011 9:570.566 mg/Kg-dry 1< 0.566NELAP 69639
Thallium 7841 07/28/2011 9:290.189 mg/Kg-dry 10.434NELAP 69639
SW-846 7471AMercury 07/19/2011 12:250.012 mg/Kg-dry 10.054NELAP 69631
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel 07/19/2011 17:37161 mg/Kg-dry 25NDNELAP 69637
Kerosene 07/19/2011 17:37161 mg/Kg-dry 25NDNELAP 69637
Mineral Spirits 07/19/2011 17:37161 mg/Kg-dry 25NDNELAP 69637
Motor Oil 07/19/2011 17:37161 mg/Kg-dry 25NDNELAP 69637
Surr: n-Tetracontane S 07/19/2011 17:3750.6-140 %REC 250 69637
Surrogate recovery was outside QC limits due to sample dilution.Elevated reporting limit(s) due to sample extract composition.
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/25/2011 23:40216 µg/Kg-dry 100NDNELAP 69671
4,4´-DDE 07/25/2011 23:40216 µg/Kg-dry 100NDNELAP 69671
4,4´-DDT 07/25/2011 23:40216 µg/Kg-dry 100NDNELAP 69671
Alachlor 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
Aldrin 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
alpha-BHC 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
alpha-Chlordane 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
Page 29 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 15:30
Lab ID: 11070610-005 Client Sample ID: SBA-F2 (4-5)
Matrix: SOLID
Batch
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECDbeta-BHC 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
Chlordane 07/22/2011 14:4121.6 µg/Kg-dry 5NDNELAP 69671
delta-BHC 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
Dieldrin 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
Endosulfan I 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
Endosulfan II 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
Endosulfan sulfate 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
Endrin 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
Endrin aldehyde 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
Endrin ketone 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
gamma-BHC 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
gamma-Chlordane 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
Heptachlor 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
Heptachlor epoxide 07/22/2011 14:4110.8 µg/Kg-dry 5NDNELAP 69671
Methoxychlor 07/25/2011 23:40216 µg/Kg-dry 100NDNELAP 69671
Toxaphene 07/22/2011 14:41194 µg/Kg-dry 5NDNELAP 69671
Surr: Decachlorobiphenyl 07/22/2011 14:4148-149 %REC 5131.9 69671
Surr: Tetrachloro-m-xylene 07/22/2011 14:4119-145 %REC 588.2 69671
Elevated reporting limit(s) due to sample extract composition.
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/20/2011 19:2848.4 µg/Kg-dry 1NDNELAP 69671
Aroclor 1221 07/20/2011 19:2848.4 µg/Kg-dry 1NDNELAP 69671
Aroclor 1232 07/20/2011 19:2848.4 µg/Kg-dry 1NDNELAP 69671
Aroclor 1242 07/20/2011 19:2848.4 µg/Kg-dry 1NDNELAP 69671
Aroclor 1248 07/20/2011 19:2848.4 µg/Kg-dry 1NDNELAP 69671
Aroclor 1254 07/20/2011 19:2848.4 µg/Kg-dry 1NDNELAP 69671
Aroclor 1260 07/20/2011 19:2848.4 µg/Kg-dry 1NDNELAP 69671
Surr: Decachlorobiphenyl 07/20/2011 19:285-156 %REC 188.9 69671
Surr: Tetrachloro-meta-xylene 07/20/2011 19:287.35-123 %REC 187.0 69671
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/20/2011 7:190.004 mg/Kg-dry 10.022NELAP 69628
Acenaphthylene 07/20/2011 7:190.004 mg/Kg-dry 10.085NELAP 69628
Anthracene 07/20/2011 7:190.004 mg/Kg-dry 10.232NELAP 69628
Benzo(a)anthracene 07/20/2011 7:190.004 mg/Kg-dry 10.500NELAP 69628
Benzo(a)pyrene 07/20/2011 7:190.004 mg/Kg-dry 10.449NELAP 69628
Benzo(b)fluoranthene 07/20/2011 7:190.004 mg/Kg-dry 10.660NELAP 69628
Benzo(g,h,i)perylene 07/20/2011 7:190.004 mg/Kg-dry 10.141NELAP 69628
Benzo(k)fluoranthene 07/20/2011 7:190.004 mg/Kg-dry 10.241NELAP 69628
Bis(2-ethylhexyl)phthalate J 07/20/2011 7:190.087 mg/Kg-dry 10.051NELAP 69628
Chrysene 07/20/2011 7:190.004 mg/Kg-dry 10.491NELAP 69628
Dibenzo(a,h)anthracene 07/20/2011 7:190.004 mg/Kg-dry 10.047NELAP 69628
Fluoranthene 07/20/2011 7:190.004 mg/Kg-dry 11.37NELAP 69628
Fluorene 07/20/2011 7:190.004 mg/Kg-dry 10.135NELAP 69628
Indeno(1,2,3-cd)pyrene 07/20/2011 7:190.004 mg/Kg-dry 10.163NELAP 69628
Naphthalene 07/20/2011 7:190.004 mg/Kg-dry 10.028NELAP 69628
Phenanthrene 07/20/2011 7:190.004 mg/Kg-dry 11.25NELAP 69628
Pyrene 07/20/2011 7:190.004 mg/Kg-dry 11.06NELAP 69628
Page 30 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 15:30
Lab ID: 11070610-005 Client Sample ID: SBA-F2 (4-5)
Matrix: SOLID
Batch
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: 2-Fluorobiphenyl 07/20/2011 7:1910-131 %REC 164.6 69628
Surr: Nitrobenzene-d5 07/20/2011 7:1910-132 %REC 180.3 69628
Surr: p-Terphenyl-d14 S 07/20/2011 7:1980.2-138 %REC 175.0 69628
Surrogate recovery was outside QC limits due to matrix interference.
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
1,2-Dichlorobenzene 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
1,3-Dichlorobenzene 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
1,4-Dichlorobenzene 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
2,4,5-Trichlorophenol 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
2,4,6-Trichlorophenol 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
2,4-Dichlorophenol 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
2,4-Dimethylphenol 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
2,4-Dinitrophenol 07/19/2011 17:261.29 mg/Kg-dry 1NDNELAP 69627
2,4-Dinitrotoluene 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
2,6-Dinitrotoluene 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
2-Chloronaphthalene 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
2-Chlorophenol 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
2-Methoxy-4-methylphenol 07/19/2011 17:260.841 mg/Kg-dry 1ND 69627
2-Methylnaphthalene 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
2-Nitroaniline 07/19/2011 17:261.29 mg/Kg-dry 1NDNELAP 69627
2-Nitrophenol 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
3,3´-Dichlorobenzidine 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
3-Nitroaniline 07/19/2011 17:261.29 mg/Kg-dry 1NDNELAP 69627
4,6-Dinitro-2-methylphenol 07/19/2011 17:261.29 mg/Kg-dry 1NDNELAP 69627
4-Bromophenyl phenyl ether 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
4-Chloro-3-methylphenol 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
4-Chloroaniline 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
4-Chlorophenyl phenyl ether 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
4-Nitroaniline 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
4-Nitrophenol 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
Aniline 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
Azobenzene 07/19/2011 17:260.453 mg/Kg-dry 1ND 69627
Benzidine 07/19/2011 17:261.37 mg/Kg-dry 1see noteNELAP 69627
Benzoic acid 07/19/2011 17:261.94 mg/Kg-dry 1NDNELAP 69627
Benzyl alcohol 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroethoxy)methane 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroethyl)ether 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroisopropyl)ether 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
Butyl benzyl phthalate 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
Carbazole J 07/19/2011 17:260.647 mg/Kg-dry 10.26 69627
Dibenzofuran 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
Diethyl phthalate 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
Dimethyl phthalate 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
Di-n-butyl phthalate 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
Di-n-octyl phthalate 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
Hexachlorobenzene 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
Page 31 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 15:30
Lab ID: 11070610-005 Client Sample ID: SBA-F2 (4-5)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachlorobutadiene 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
Hexachlorocyclopentadiene 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
Hexachloroethane 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
Isophorone 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
m,p-Cresol 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
Nitrobenzene 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
N-Nitrosodimethylamine 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
N-Nitroso-di-n-propylamine 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
N-Nitrosodiphenylamine 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
o-Cresol 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
Pentachlorophenol 07/19/2011 17:262.59 mg/Kg-dry 1NDNELAP 69627
Phenol 07/19/2011 17:260.453 mg/Kg-dry 1NDNELAP 69627
Pyridine 07/19/2011 17:260.647 mg/Kg-dry 1NDNELAP 69627
1,2-Diphenylhydrazine 07/19/2011 17:261.09 mg/Kg-dry 1ND 69627
Surr: 2,4,6-Tribromophenol 07/19/2011 17:2632.7-130 %REC 183.6 69627
Surr: 2-Fluorobiphenyl 07/19/2011 17:2634.1-116 %REC 171.1 69627
Surr: 2-Fluorophenol 07/19/2011 17:2630.5-99 %REC 172.7 69627
Surr: Nitrobenzene-d5 07/19/2011 17:2634.1-101 %REC 181.0 69627
Surr: Phenol-d5 07/19/2011 17:2634.9-110 %REC 173.0 69627
Surr: p-Terphenyl-d14 07/19/2011 17:2641.7-124 %REC 191.2 69627
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.4-Nitrophenol was outside upper QC limits in the LCS. Sample was ND.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,1,1-Trichloroethane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,1,2,2-Tetrachloroethane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,1,2-Trichloro-1,2,2-trifluoroethane 07/21/2011 13:204.8 µg/Kg-dry 1ND 69790
1,1,2-Trichloroethane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,1-Dichloro-2-propanone 07/21/2011 13:2047.8 µg/Kg-dry 1ND 69790
1,1-Dichloroethane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,1-Dichloroethene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,1-Dichloropropene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,2,3-Trichlorobenzene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,2,3-Trichloropropane 07/21/2011 13:209.6 µg/Kg-dry 1NDNELAP 69790
1,2,3-Trimethylbenzene 07/21/2011 13:204.8 µg/Kg-dry 1ND 69790
1,2,4-Trichlorobenzene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,2,4-Trimethylbenzene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,2-Dibromo-3-chloropropane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,2-Dibromoethane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,2-Dichlorobenzene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,2-Dichloroethane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,2-Dichloropropane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,3,5-Trimethylbenzene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,3-Dichlorobenzene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,3-Dichloropropane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1,4-Dichlorobenzene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
1-Chlorobutane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Page 32 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 15:30
Lab ID: 11070610-005 Client Sample ID: SBA-F2 (4-5)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS2,2-Dichloropropane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
2-Butanone J 07/21/2011 13:2047.8 µg/Kg-dry 111NELAP 69790
2-Chlorotoluene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
2-Hexanone 07/21/2011 13:2047.8 µg/Kg-dry 1NDNELAP 69790
2-Nitropropane 07/21/2011 13:2047.8 µg/Kg-dry 1NDNELAP 69790
4-Chlorotoluene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
4-Methyl-2-pentanone 07/21/2011 13:2047.8 µg/Kg-dry 1NDNELAP 69790
Acetone 07/21/2011 13:2047.8 µg/Kg-dry 168.3NELAP 69790
Acrolein 07/21/2011 13:2095.6 µg/Kg-dry 1NDNELAP 69790
Acrylonitrile 07/21/2011 13:209.6 µg/Kg-dry 1NDNELAP 69790
Allyl chloride 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Benzene 07/21/2011 13:201.0 µg/Kg-dry 11.3NELAP 69790
Bromobenzene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Bromochloromethane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Bromodichloromethane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Bromoform 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Bromomethane 07/21/2011 13:209.6 µg/Kg-dry 1NDNELAP 69790
Carbon disulfide 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Carbon tetrachloride 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Chlorobenzene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Chloroethane 07/21/2011 13:209.6 µg/Kg-dry 1NDNELAP 69790
Chloroform 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Chloromethane 07/21/2011 13:209.6 µg/Kg-dry 1NDNELAP 69790
cis-1,2-Dichloroethene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
cis-1,3-Dichloropropene 07/21/2011 13:203.8 µg/Kg-dry 1NDNELAP 69790
Cyclohexanone 07/21/2011 13:2095.6 µg/Kg-dry 1ND 69790
Dibromochloromethane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Dibromomethane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Dichlorodifluoromethane 07/21/2011 13:209.6 µg/Kg-dry 1NDNELAP 69790
Ethyl acetate 07/21/2011 13:2047.8 µg/Kg-dry 1NDNELAP 69790
Ethyl ether 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Ethyl methacrylate 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Ethylbenzene J 07/21/2011 13:204.8 µg/Kg-dry 11.0NELAP 69790
Heptane J 07/21/2011 13:2019.1 µg/Kg-dry 12.0 69790
Hexachlorobutadiene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Hexachloroethane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Iodomethane 07/21/2011 13:209.6 µg/Kg-dry 1NDNELAP 69790
Isopropylbenzene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
m,p-Xylenes J 07/21/2011 13:204.8 µg/Kg-dry 11.6NELAP 69790
Methacrylonitrile 07/21/2011 13:2047.8 µg/Kg-dry 1NDNELAP 69790
Methyl Methacrylate 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Methyl tert-butyl ether 07/21/2011 13:201.9 µg/Kg-dry 1NDNELAP 69790
Methylacrylate 07/21/2011 13:209.6 µg/Kg-dry 1ND 69790
Methylene chloride J 07/21/2011 13:204.8 µg/Kg-dry 12.3NELAP 69790
Naphthalene 07/21/2011 13:209.6 µg/Kg-dry 1NDNELAP 69790
n-Butylbenzene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
n-Hexane J 07/21/2011 13:2019.1 µg/Kg-dry 13.5 69790
Page 33 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/13/2011 15:30
Lab ID: 11070610-005 Client Sample ID: SBA-F2 (4-5)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSNitrobenzene 07/21/2011 13:2095.6 µg/Kg-dry 1NDNELAP 69790
n-Propylbenzene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
o-Xylene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Pentachloroethane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
p-Isopropyltoluene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Propionitrile 07/21/2011 13:2047.8 µg/Kg-dry 1NDNELAP 69790
sec-Butylbenzene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Styrene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
tert-Butylbenzene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Tetrachloroethene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Tetrahydrofuran 07/21/2011 13:2047.8 µg/Kg-dry 1NDNELAP 69790
Toluene J 07/21/2011 13:204.8 µg/Kg-dry 13.1NELAP 69790
trans-1,2-Dichloroethene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
trans-1,3-Dichloropropene 07/21/2011 13:203.8 µg/Kg-dry 1NDNELAP 69790
Trichloroethene 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Trichlorofluoromethane 07/21/2011 13:204.8 µg/Kg-dry 1NDNELAP 69790
Vinyl acetate 07/21/2011 13:2047.8 µg/Kg-dry 1NDNELAP 69790
Vinyl chloride 07/21/2011 13:201.9 µg/Kg-dry 1NDNELAP 69790
Surr: 1,2-Dichloroethane-d4 07/21/2011 13:2072.2-131 %REC 1121.9 69790
Surr: 4-Bromofluorobenzene 07/21/2011 13:2082.1-116 %REC 186.3 69790
Surr: Dibromofluoromethane 07/21/2011 13:2077.7-120 %REC 1111.8 69790
Surr: Toluene-d8 S 07/21/2011 13:2086-116 %REC 1120.3 69790
Surrogate recovery and/or internal standard area was outside QC limits due to matrix interference.
SW-846 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 07/23/2011 0:150.05 mg/Kg-dry 1NDNELAP R152491
2,4,5-TP (Silvex) 07/23/2011 0:150.05 mg/Kg-dry 1NDNELAP R152491
2,4-D 07/23/2011 0:150.05 mg/Kg-dry 1NDNELAP R152491
2,4-DB 07/23/2011 0:150.05 mg/Kg-dry 1NDNELAP R152491
3,5-Dichlorobenzoic Acid 07/23/2011 0:150.05 mg/Kg-dry 1NDNELAP R152491
Acifluorfen 07/23/2011 0:150.05 mg/Kg-dry 1NDNELAP R152491
Bentazon 07/23/2011 0:150.05 mg/Kg-dry 1NDNELAP R152491
Chloramben 07/23/2011 0:150.05 mg/Kg-dry 1NDNELAP R152491
Dalapon 07/23/2011 0:150.05 mg/Kg-dry 1NDNELAP R152491
DCPA 07/23/2011 0:150.05 mg/Kg-dry 1NDNELAP R152491
Dicamba 07/23/2011 0:150.05 mg/Kg-dry 1NDNELAP R152491
Dichlorprop 07/23/2011 0:150.05 mg/Kg-dry 1NDNELAP R152491
Dinoseb 07/23/2011 0:150.05 mg/Kg-dry 1NDNELAP R152491
Pentachlorophenol 07/23/2011 0:150.05 mg/Kg-dry 1NDNELAP R152491
Picloram 07/23/2011 0:150.05 mg/Kg-dry 1NDNELAP R152491
Surr: DCAA 07/23/2011 0:1524-140 %REC 189.3 R152491
The LCS/LCSD RPD result exceeded the QC control limits for Dinoseb; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data.
Page 34 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 9:45
Lab ID: 11070610-006 Client Sample ID: TSA-02 (8-9)
Matrix: SOLID
Batch
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 07/18/2011 10:000.1 % 118.5 R152055
STANDARD METHODS 18TH ED. 2540 GTotal Solids 07/18/2011 8:300.1 % 181.5 R152054
SW-846 9012A (TOTAL)Cyanide J 07/19/2011 10:260.31 mg/Kg-dry 10.13NELAP 69687
SW-846 3050B, 6010B, METALS BY ICPAluminum 07/19/2011 13:124.72 mg/Kg-dry 120600NELAP 69636
Antimony 07/27/2011 12:334.90 mg/Kg-dry 1< 4.90NELAP 69908
Arsenic 07/19/2011 13:122.36 mg/Kg-dry 16.75NELAP 69636
Barium 07/20/2011 15:520.47 mg/Kg-dry 1150NELAP 69636
Beryllium 07/19/2011 13:120.09 mg/Kg-dry 10.76NELAP 69636
Cadmium 07/19/2011 13:120.19 mg/Kg-dry 10.26NELAP 69636
Calcium 07/19/2011 13:124.72 mg/Kg-dry 15140NELAP 69636
Chromium 07/19/2011 13:120.94 mg/Kg-dry 120.4NELAP 69636
Cobalt 07/19/2011 13:120.94 mg/Kg-dry 19.22NELAP 69636
Copper 07/19/2011 13:120.94 mg/Kg-dry 115.7NELAP 69636
Iron 07/19/2011 13:121.89 mg/Kg-dry 122700NELAP 69636
Lead 07/19/2011 13:123.77 mg/Kg-dry 116.3NELAP 69636
Magnesium 07/19/2011 13:120.94 mg/Kg-dry 13760NELAP 69636
Manganese 07/19/2011 13:120.47 mg/Kg-dry 1578NELAP 69636
Nickel 07/19/2011 13:120.94 mg/Kg-dry 115.9NELAP 69636
Potassium 07/20/2011 15:529.43 mg/Kg-dry 12520NELAP 69636
Silver 07/20/2011 15:520.52 mg/Kg-dry 1< 0.52NELAP 69636
Sodium 07/20/2011 15:524.72 mg/Kg-dry 155.4NELAP 69636
Vanadium 07/20/2011 15:520.94 mg/Kg-dry 136.9NELAP 69636
Zinc 07/19/2011 13:120.94 mg/Kg-dry 161.7NELAP 69636
SW-846 3050B, METALS BY GFAASelenium 7740 J 07/19/2011 10:010.577 mg/Kg-dry 10.52NELAP 69639
Thallium 7841 07/28/2011 9:330.192 mg/Kg-dry 10.375NELAP 69639
SW-846 7471AMercury 07/19/2011 12:250.012 mg/Kg-dry 10.021NELAP 69631
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel 07/19/2011 14:176.12 mg/Kg-dry 1NDNELAP 69637
Kerosene 07/19/2011 14:176.12 mg/Kg-dry 1NDNELAP 69637
Mineral Spirits 07/19/2011 14:176.12 mg/Kg-dry 1NDNELAP 69637
Motor Oil 07/19/2011 14:176.12 mg/Kg-dry 1NDNELAP 69637
Surr: n-Tetracontane 07/19/2011 14:1750.6-140 %REC 194.2 69637
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/26/2011 0:0620.4 µg/Kg-dry 10NDNELAP 69671
4,4´-DDE 07/26/2011 0:0620.4 µg/Kg-dry 10NDNELAP 69671
4,4´-DDT 07/26/2011 0:0620.4 µg/Kg-dry 10NDNELAP 69671
Alachlor 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
Aldrin 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
alpha-BHC 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
alpha-Chlordane 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
beta-BHC 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
Page 35 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 9:45
Lab ID: 11070610-006 Client Sample ID: TSA-02 (8-9)
Matrix: SOLID
Batch
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECDChlordane 07/21/2011 23:294.09 µg/Kg-dry 1NDNELAP 69671
delta-BHC 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
Dieldrin 07/21/2011 23:292.04 µg/Kg-dry 12.76NELAP 69671
Endosulfan I 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
Endosulfan II 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
Endosulfan sulfate 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
Endrin 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
Endrin aldehyde 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
Endrin ketone 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
gamma-BHC 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
gamma-Chlordane 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
Heptachlor 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
Heptachlor epoxide 07/21/2011 23:292.04 µg/Kg-dry 12.29NELAP 69671
Methoxychlor 07/21/2011 23:292.04 µg/Kg-dry 1NDNELAP 69671
Toxaphene 07/21/2011 23:2936.7 µg/Kg-dry 1NDNELAP 69671
Surr: Decachlorobiphenyl 07/21/2011 23:2948-149 %REC 1101.8 69671
Surr: Tetrachloro-m-xylene 07/21/2011 23:2919-145 %REC 169.9 69671
Elevated reporting limit(s) due to sample extract composition.
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/20/2011 19:4545.9 µg/Kg-dry 1NDNELAP 69671
Aroclor 1221 07/20/2011 19:4545.9 µg/Kg-dry 1NDNELAP 69671
Aroclor 1232 07/20/2011 19:4545.9 µg/Kg-dry 1NDNELAP 69671
Aroclor 1242 07/20/2011 19:4545.9 µg/Kg-dry 1NDNELAP 69671
Aroclor 1248 07/20/2011 19:4545.9 µg/Kg-dry 1NDNELAP 69671
Aroclor 1254 07/20/2011 19:4545.9 µg/Kg-dry 1NDNELAP 69671
Aroclor 1260 07/20/2011 19:4545.9 µg/Kg-dry 1NDNELAP 69671
Surr: Decachlorobiphenyl 07/20/2011 19:455-156 %REC 198.8 69671
Surr: Tetrachloro-meta-xylene 07/20/2011 19:457.35-123 %REC 170.0 69671
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Acenaphthylene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Anthracene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Benzo(a)anthracene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Benzo(a)pyrene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Benzo(b)fluoranthene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Benzo(g,h,i)perylene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Benzo(k)fluoranthene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Bis(2-ethylhexyl)phthalate 07/20/2011 6:060.082 mg/Kg-dry 1NDNELAP 69628
Chrysene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Dibenzo(a,h)anthracene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Fluoranthene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Fluorene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Indeno(1,2,3-cd)pyrene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Naphthalene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Phenanthrene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Pyrene 07/20/2011 6:060.004 mg/Kg-dry 1NDNELAP 69628
Surr: 2-Fluorobiphenyl 07/20/2011 6:0610-131 %REC 150.1 69628
Page 36 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 9:45
Lab ID: 11070610-006 Client Sample ID: TSA-02 (8-9)
Matrix: SOLID
Batch
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: Nitrobenzene-d5 07/20/2011 6:0610-132 %REC 172.5 69628
Surr: p-Terphenyl-d14 S 07/20/2011 6:0680.2-138 %REC 175.2 69628
Surrogate recovery was outside QC limits due to matrix interference.
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
1,2-Dichlorobenzene 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
1,3-Dichlorobenzene 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
1,4-Dichlorobenzene 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
2,4,5-Trichlorophenol 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
2,4,6-Trichlorophenol 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
2,4-Dichlorophenol 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
2,4-Dimethylphenol 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
2,4-Dinitrophenol 07/19/2011 14:101.22 mg/Kg-dry 1NDNELAP 69627
2,4-Dinitrotoluene 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
2,6-Dinitrotoluene 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
2-Chloronaphthalene 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
2-Chlorophenol 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
2-Methoxy-4-methylphenol 07/19/2011 14:100.795 mg/Kg-dry 1ND 69627
2-Methylnaphthalene 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
2-Nitroaniline 07/19/2011 14:101.22 mg/Kg-dry 1NDNELAP 69627
2-Nitrophenol 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
3,3´-Dichlorobenzidine 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
3-Nitroaniline 07/19/2011 14:101.22 mg/Kg-dry 1NDNELAP 69627
4,6-Dinitro-2-methylphenol 07/19/2011 14:101.22 mg/Kg-dry 1NDNELAP 69627
4-Bromophenyl phenyl ether 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
4-Chloro-3-methylphenol 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
4-Chloroaniline 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
4-Chlorophenyl phenyl ether 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
4-Nitroaniline 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
4-Nitrophenol 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
Aniline 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
Azobenzene 07/19/2011 14:100.428 mg/Kg-dry 1ND 69627
Benzidine 07/19/2011 14:101.29 mg/Kg-dry 1see noteNELAP 69627
Benzoic acid 07/19/2011 14:101.84 mg/Kg-dry 1NDNELAP 69627
Benzyl alcohol 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroethoxy)methane 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroethyl)ether 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroisopropyl)ether 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
Butyl benzyl phthalate 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
Carbazole 07/19/2011 14:100.612 mg/Kg-dry 1ND 69627
Dibenzofuran 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
Diethyl phthalate 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
Dimethyl phthalate 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
Di-n-butyl phthalate 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
Di-n-octyl phthalate 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
Hexachlorobenzene 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
Hexachlorobutadiene 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
Page 37 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 9:45
Lab ID: 11070610-006 Client Sample ID: TSA-02 (8-9)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachlorocyclopentadiene 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
Hexachloroethane 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
Isophorone 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
m,p-Cresol 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
Nitrobenzene 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
N-Nitrosodimethylamine 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
N-Nitroso-di-n-propylamine 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
N-Nitrosodiphenylamine 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
o-Cresol 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
Pentachlorophenol 07/19/2011 14:102.45 mg/Kg-dry 1NDNELAP 69627
Phenol 07/19/2011 14:100.428 mg/Kg-dry 1NDNELAP 69627
Pyridine 07/19/2011 14:100.612 mg/Kg-dry 1NDNELAP 69627
1,2-Diphenylhydrazine 07/19/2011 14:101.03 mg/Kg-dry 1ND 69627
Surr: 2,4,6-Tribromophenol 07/19/2011 14:1032.7-130 %REC 177.0 69627
Surr: 2-Fluorobiphenyl 07/19/2011 14:1034.1-116 %REC 153.5 69627
Surr: 2-Fluorophenol 07/19/2011 14:1030.5-99 %REC 168.5 69627
Surr: Nitrobenzene-d5 07/19/2011 14:1034.1-101 %REC 172.3 69627
Surr: Phenol-d5 07/19/2011 14:1034.9-110 %REC 170.5 69627
Surr: p-Terphenyl-d14 07/19/2011 14:1041.7-124 %REC 186.5 69627
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.4-Nitrophenol was outside upper QC limits in the LCS. Sample was ND.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,1,1-Trichloroethane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,1,2,2-Tetrachloroethane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,1,2-Trichloro-1,2,2-trifluoroethane 07/21/2011 13:495.1 µg/Kg-dry 1ND 69790
1,1,2-Trichloroethane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,1-Dichloro-2-propanone 07/21/2011 13:4950.8 µg/Kg-dry 1ND 69790
1,1-Dichloroethane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,1-Dichloroethene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,1-Dichloropropene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,2,3-Trichlorobenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,2,3-Trichloropropane 07/21/2011 13:4910.2 µg/Kg-dry 1NDNELAP 69790
1,2,3-Trimethylbenzene 07/21/2011 13:495.1 µg/Kg-dry 1ND 69790
1,2,4-Trichlorobenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,2,4-Trimethylbenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,2-Dibromo-3-chloropropane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,2-Dibromoethane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,2-Dichlorobenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,2-Dichloroethane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,2-Dichloropropane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,3,5-Trimethylbenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,3-Dichlorobenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,3-Dichloropropane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1,4-Dichlorobenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
1-Chlorobutane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
2,2-Dichloropropane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Page 38 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 9:45
Lab ID: 11070610-006 Client Sample ID: TSA-02 (8-9)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS2-Butanone 07/21/2011 13:4950.8 µg/Kg-dry 1NDNELAP 69790
2-Chlorotoluene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
2-Hexanone 07/21/2011 13:4950.8 µg/Kg-dry 1NDNELAP 69790
2-Nitropropane 07/21/2011 13:4950.8 µg/Kg-dry 1NDNELAP 69790
4-Chlorotoluene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
4-Methyl-2-pentanone 07/21/2011 13:4950.8 µg/Kg-dry 1NDNELAP 69790
Acetone J 07/21/2011 13:4950.8 µg/Kg-dry 133NELAP 69790
Acrolein 07/21/2011 13:49102 µg/Kg-dry 1NDNELAP 69790
Acrylonitrile 07/21/2011 13:4910.2 µg/Kg-dry 1NDNELAP 69790
Allyl chloride 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Benzene 07/21/2011 13:491.0 µg/Kg-dry 1NDNELAP 69790
Bromobenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Bromochloromethane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Bromodichloromethane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Bromoform 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Bromomethane 07/21/2011 13:4910.2 µg/Kg-dry 1NDNELAP 69790
Carbon disulfide 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Carbon tetrachloride 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Chlorobenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Chloroethane 07/21/2011 13:4910.2 µg/Kg-dry 1NDNELAP 69790
Chloroform 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Chloromethane 07/21/2011 13:4910.2 µg/Kg-dry 1NDNELAP 69790
cis-1,2-Dichloroethene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
cis-1,3-Dichloropropene 07/21/2011 13:494.1 µg/Kg-dry 1NDNELAP 69790
Cyclohexanone 07/21/2011 13:49102 µg/Kg-dry 1ND 69790
Dibromochloromethane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Dibromomethane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Dichlorodifluoromethane 07/21/2011 13:4910.2 µg/Kg-dry 1NDNELAP 69790
Ethyl acetate 07/21/2011 13:4950.8 µg/Kg-dry 1NDNELAP 69790
Ethyl ether 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Ethyl methacrylate 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Ethylbenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Heptane 07/21/2011 13:4920.3 µg/Kg-dry 1ND 69790
Hexachlorobutadiene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Hexachloroethane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Iodomethane 07/21/2011 13:4910.2 µg/Kg-dry 1NDNELAP 69790
Isopropylbenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
m,p-Xylenes 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Methacrylonitrile 07/21/2011 13:4950.8 µg/Kg-dry 1NDNELAP 69790
Methyl Methacrylate 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Methyl tert-butyl ether 07/21/2011 13:492.0 µg/Kg-dry 1NDNELAP 69790
Methylacrylate 07/21/2011 13:4910.2 µg/Kg-dry 1ND 69790
Methylene chloride J 07/21/2011 13:495.1 µg/Kg-dry 11.5NELAP 69790
Naphthalene 07/21/2011 13:4910.2 µg/Kg-dry 1NDNELAP 69790
n-Butylbenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
n-Hexane 07/21/2011 13:4920.3 µg/Kg-dry 1ND 69790
Nitrobenzene 07/21/2011 13:49102 µg/Kg-dry 1NDNELAP 69790
Page 39 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 9:45
Lab ID: 11070610-006 Client Sample ID: TSA-02 (8-9)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSn-Propylbenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
o-Xylene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Pentachloroethane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
p-Isopropyltoluene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Propionitrile 07/21/2011 13:4950.8 µg/Kg-dry 1NDNELAP 69790
sec-Butylbenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Styrene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
tert-Butylbenzene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Tetrachloroethene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Tetrahydrofuran 07/21/2011 13:4950.8 µg/Kg-dry 1NDNELAP 69790
Toluene J 07/21/2011 13:495.1 µg/Kg-dry 11.2NELAP 69790
trans-1,2-Dichloroethene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
trans-1,3-Dichloropropene 07/21/2011 13:494.1 µg/Kg-dry 1NDNELAP 69790
Trichloroethene 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Trichlorofluoromethane 07/21/2011 13:495.1 µg/Kg-dry 1NDNELAP 69790
Vinyl acetate 07/21/2011 13:4950.8 µg/Kg-dry 1NDNELAP 69790
Vinyl chloride 07/21/2011 13:492.0 µg/Kg-dry 1NDNELAP 69790
Surr: 1,2-Dichloroethane-d4 07/21/2011 13:4972.2-131 %REC 1128.7 69790
Surr: 4-Bromofluorobenzene 07/21/2011 13:4982.1-116 %REC 1103.1 69790
Surr: Dibromofluoromethane 07/21/2011 13:4977.7-120 %REC 1104.9 69790
Surr: Toluene-d8 07/21/2011 13:4986-116 %REC 1107.9 69790
SW-846 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 07/23/2011 1:020.05 mg/Kg-dry 1NDNELAP R152491
2,4,5-TP (Silvex) 07/23/2011 1:020.05 mg/Kg-dry 1NDNELAP R152491
2,4-D 07/23/2011 1:020.05 mg/Kg-dry 1NDNELAP R152491
2,4-DB 07/23/2011 1:020.05 mg/Kg-dry 1NDNELAP R152491
3,5-Dichlorobenzoic Acid 07/23/2011 1:020.05 mg/Kg-dry 1NDNELAP R152491
Acifluorfen 07/23/2011 1:020.05 mg/Kg-dry 1NDNELAP R152491
Bentazon 07/23/2011 1:020.05 mg/Kg-dry 1NDNELAP R152491
Chloramben 07/23/2011 1:020.05 mg/Kg-dry 1NDNELAP R152491
Dalapon 07/23/2011 1:020.05 mg/Kg-dry 1NDNELAP R152491
DCPA 07/23/2011 1:020.05 mg/Kg-dry 1NDNELAP R152491
Dicamba 07/23/2011 1:020.05 mg/Kg-dry 1NDNELAP R152491
Dichlorprop 07/23/2011 1:020.05 mg/Kg-dry 1NDNELAP R152491
Dinoseb 07/23/2011 1:020.05 mg/Kg-dry 1NDNELAP R152491
Pentachlorophenol 07/23/2011 1:020.05 mg/Kg-dry 1NDNELAP R152491
Picloram 07/23/2011 1:020.05 mg/Kg-dry 1NDNELAP R152491
Surr: DCAA 07/23/2011 1:0224-140 %REC 163.4 R152491
The LCS/LCSD RPD result exceeded the QC control limits for Dinoseb; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data.
Page 40 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 10:30
Lab ID: 11070610-007 Client Sample ID: TSA-01 (5-6)
Matrix: SOLID
Batch
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 07/18/2011 10:000.1 % 117.6 R152055
STANDARD METHODS 18TH ED. 2540 GTotal Solids 07/18/2011 8:300.1 % 182.4 R152054
SW-846 9012A (TOTAL)Cyanide J 07/19/2011 10:260.30 mg/Kg-dry 10.18NELAP 69687
SW-846 3050B, 6010B, METALS BY ICPAluminum 07/19/2011 13:184.81 mg/Kg-dry 120700NELAP 69636
Antimony 07/27/2011 12:394.81 mg/Kg-dry 1< 4.81NELAP 69908
Arsenic 07/19/2011 13:182.40 mg/Kg-dry 16.87NELAP 69636
Barium 07/20/2011 15:570.48 mg/Kg-dry 1148NELAP 69636
Beryllium 07/19/2011 13:180.10 mg/Kg-dry 10.80NELAP 69636
Cadmium 07/19/2011 13:180.19 mg/Kg-dry 10.32NELAP 69636
Calcium 07/19/2011 13:184.81 mg/Kg-dry 16000NELAP 69636
Chromium 07/19/2011 13:180.96 mg/Kg-dry 121.8NELAP 69636
Cobalt 07/19/2011 13:180.96 mg/Kg-dry 18.99NELAP 69636
Copper 07/19/2011 13:180.96 mg/Kg-dry 116.5NELAP 69636
Iron 07/19/2011 13:181.92 mg/Kg-dry 123700NELAP 69636
Lead 07/19/2011 13:183.85 mg/Kg-dry 117.0NELAP 69636
Magnesium 07/19/2011 13:180.96 mg/Kg-dry 13870NELAP 69636
Manganese 07/19/2011 13:180.48 mg/Kg-dry 1620NELAP 69636
Nickel 07/19/2011 13:180.96 mg/Kg-dry 117.4NELAP 69636
Potassium 07/20/2011 15:579.62 mg/Kg-dry 12520NELAP 69636
Silver 07/21/2011 13:120.53 mg/Kg-dry 1< 0.53NELAP 69636
Sodium 07/20/2011 15:574.81 mg/Kg-dry 156.9NELAP 69636
Vanadium 07/20/2011 15:570.96 mg/Kg-dry 137.4NELAP 69636
Zinc 07/19/2011 13:180.96 mg/Kg-dry 163.1NELAP 69636
SW-846 3050B, METALS BY GFAASelenium 7740 J 07/19/2011 10:040.556 mg/Kg-dry 10.45NELAP 69639
Thallium 7841 07/28/2011 9:570.185 mg/Kg-dry 10.303NELAP 69639
SW-846 7471AMercury 07/19/2011 12:250.011 mg/Kg-dry 10.022NELAP 69631
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel 07/19/2011 15:116.07 mg/Kg-dry 1NDNELAP 69637
Kerosene 07/19/2011 15:116.07 mg/Kg-dry 1NDNELAP 69637
Mineral Spirits 07/19/2011 15:116.07 mg/Kg-dry 1NDNELAP 69637
Motor Oil 07/19/2011 15:116.07 mg/Kg-dry 1NDNELAP 69637
Surr: n-Tetracontane 07/19/2011 15:1150.6-140 %REC 1101.3 69637
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/26/2011 0:3120.2 µg/Kg-dry 10NDNELAP 69671
4,4´-DDE 07/26/2011 0:3120.2 µg/Kg-dry 10NDNELAP 69671
4,4´-DDT 07/26/2011 0:3120.2 µg/Kg-dry 10NDNELAP 69671
Alachlor 07/21/2011 23:552.02 µg/Kg-dry 1NDNELAP 69671
Aldrin 07/21/2011 23:552.02 µg/Kg-dry 1NDNELAP 69671
alpha-BHC 07/21/2011 23:552.02 µg/Kg-dry 1NDNELAP 69671
alpha-Chlordane 07/21/2011 23:552.02 µg/Kg-dry 1NDNELAP 69671
beta-BHC 07/21/2011 23:552.02 µg/Kg-dry 1NDNELAP 69671
Page 41 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 10:30
Lab ID: 11070610-007 Client Sample ID: TSA-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECDChlordane J 07/21/2011 23:554.05 µg/Kg-dry 13.9NELAP 69671
delta-BHC 07/21/2011 23:552.02 µg/Kg-dry 1NDNELAP 69671
Dieldrin 07/21/2011 23:552.02 µg/Kg-dry 16.02NELAP 69671
Endosulfan I 07/21/2011 23:552.02 µg/Kg-dry 1NDNELAP 69671
Endosulfan II 07/21/2011 23:552.02 µg/Kg-dry 1NDNELAP 69671
Endosulfan sulfate 07/21/2011 23:552.02 µg/Kg-dry 1NDNELAP 69671
Endrin 07/21/2011 23:552.02 µg/Kg-dry 1NDNELAP 69671
Endrin aldehyde 07/21/2011 23:552.02 µg/Kg-dry 1NDNELAP 69671
Endrin ketone 07/21/2011 23:552.02 µg/Kg-dry 1NDNELAP 69671
gamma-BHC 07/21/2011 23:552.02 µg/Kg-dry 1NDNELAP 69671
gamma-Chlordane 07/21/2011 23:552.02 µg/Kg-dry 13.89NELAP 69671
Heptachlor 07/21/2011 23:552.02 µg/Kg-dry 1NDNELAP 69671
Heptachlor epoxide 07/21/2011 23:552.02 µg/Kg-dry 19.14NELAP 69671
Methoxychlor 07/21/2011 23:552.02 µg/Kg-dry 1NDNELAP 69671
Toxaphene 07/21/2011 23:5536.4 µg/Kg-dry 1NDNELAP 69671
Surr: Decachlorobiphenyl 07/21/2011 23:5548-149 %REC 1105.1 69671
Surr: Tetrachloro-m-xylene 07/21/2011 23:5519-145 %REC 174.8 69671
Elevated reporting limit(s) due to sample extract composition.
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/20/2011 10:3445.5 µg/Kg-dry 1NDNELAP 69671
Aroclor 1221 07/20/2011 10:3445.5 µg/Kg-dry 1NDNELAP 69671
Aroclor 1232 07/20/2011 10:3445.5 µg/Kg-dry 1NDNELAP 69671
Aroclor 1242 07/20/2011 10:3445.5 µg/Kg-dry 1NDNELAP 69671
Aroclor 1248 07/20/2011 10:3445.5 µg/Kg-dry 1NDNELAP 69671
Aroclor 1254 07/20/2011 10:3445.5 µg/Kg-dry 1NDNELAP 69671
Aroclor 1260 07/20/2011 10:3445.5 µg/Kg-dry 1NDNELAP 69671
Surr: Decachlorobiphenyl 07/20/2011 10:345-156 %REC 194.9 69671
Surr: Tetrachloro-meta-xylene 07/20/2011 10:347.35-123 %REC 175.6 69671
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/21/2011 4:470.004 mg/Kg-dry 1NDNELAP 69628
Acenaphthylene 07/21/2011 4:470.004 mg/Kg-dry 1NDNELAP 69628
Anthracene 07/21/2011 4:470.004 mg/Kg-dry 1NDNELAP 69628
Benzo(a)anthracene J 07/21/2011 4:470.004 mg/Kg-dry 10.004NELAP 69628
Benzo(a)pyrene 07/21/2011 4:470.004 mg/Kg-dry 1NDNELAP 69628
Benzo(b)fluoranthene J 07/21/2011 4:470.004 mg/Kg-dry 10.004NELAP 69628
Benzo(g,h,i)perylene 07/21/2011 4:470.004 mg/Kg-dry 1NDNELAP 69628
Benzo(k)fluoranthene 07/21/2011 4:470.004 mg/Kg-dry 1NDNELAP 69628
Bis(2-ethylhexyl)phthalate J 07/21/2011 4:470.081 mg/Kg-dry 10.053NELAP 69628
Chrysene 07/21/2011 4:470.004 mg/Kg-dry 1NDNELAP 69628
Dibenzo(a,h)anthracene 07/21/2011 4:470.004 mg/Kg-dry 1NDNELAP 69628
Fluoranthene 07/21/2011 4:470.004 mg/Kg-dry 10.008NELAP 69628
Fluorene 07/21/2011 4:470.004 mg/Kg-dry 1NDNELAP 69628
Indeno(1,2,3-cd)pyrene 07/21/2011 4:470.004 mg/Kg-dry 1NDNELAP 69628
Naphthalene 07/21/2011 4:470.004 mg/Kg-dry 1NDNELAP 69628
Phenanthrene 07/21/2011 4:470.004 mg/Kg-dry 10.007NELAP 69628
Pyrene 07/21/2011 4:470.004 mg/Kg-dry 10.006NELAP 69628
Surr: 2-Fluorobiphenyl 07/21/2011 4:4710-131 %REC 175.5 69628
Page 42 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 10:30
Lab ID: 11070610-007 Client Sample ID: TSA-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: Nitrobenzene-d5 07/21/2011 4:4710-132 %REC 179.3 69628
Surr: p-Terphenyl-d14 07/21/2011 4:4780.2-138 %REC 190.4 69628
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
1,2-Dichlorobenzene 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
1,3-Dichlorobenzene 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
1,4-Dichlorobenzene 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
2,4,5-Trichlorophenol 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
2,4,6-Trichlorophenol 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
2,4-Dichlorophenol 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
2,4-Dimethylphenol 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
2,4-Dinitrophenol 07/19/2011 14:431.21 mg/Kg-dry 1NDNELAP 69627
2,4-Dinitrotoluene 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
2,6-Dinitrotoluene 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
2-Chloronaphthalene 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
2-Chlorophenol 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
2-Methoxy-4-methylphenol 07/19/2011 14:430.786 mg/Kg-dry 1ND 69627
2-Methylnaphthalene 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
2-Nitroaniline 07/19/2011 14:431.21 mg/Kg-dry 1NDNELAP 69627
2-Nitrophenol 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
3,3´-Dichlorobenzidine 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
3-Nitroaniline 07/19/2011 14:431.21 mg/Kg-dry 1NDNELAP 69627
4,6-Dinitro-2-methylphenol 07/19/2011 14:431.21 mg/Kg-dry 1NDNELAP 69627
4-Bromophenyl phenyl ether 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
4-Chloro-3-methylphenol 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
4-Chloroaniline 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
4-Chlorophenyl phenyl ether 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
4-Nitroaniline 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
4-Nitrophenol 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
Aniline 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
Azobenzene 07/19/2011 14:430.423 mg/Kg-dry 1ND 69627
Benzidine 07/19/2011 14:431.28 mg/Kg-dry 1see noteNELAP 69627
Benzoic acid 07/19/2011 14:431.81 mg/Kg-dry 1NDNELAP 69627
Benzyl alcohol 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroethoxy)methane 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroethyl)ether 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroisopropyl)ether 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
Butyl benzyl phthalate 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
Carbazole 07/19/2011 14:430.604 mg/Kg-dry 1ND 69627
Dibenzofuran 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
Diethyl phthalate 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
Dimethyl phthalate 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
Di-n-butyl phthalate 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
Di-n-octyl phthalate 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
Hexachlorobenzene 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
Hexachlorobutadiene 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
Hexachlorocyclopentadiene 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
Page 43 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 10:30
Lab ID: 11070610-007 Client Sample ID: TSA-01 (5-6)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachloroethane 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
Isophorone 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
m,p-Cresol 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
Nitrobenzene 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
N-Nitrosodimethylamine 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
N-Nitroso-di-n-propylamine 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
N-Nitrosodiphenylamine 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
o-Cresol 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
Pentachlorophenol 07/19/2011 14:432.42 mg/Kg-dry 1NDNELAP 69627
Phenol 07/19/2011 14:430.423 mg/Kg-dry 1NDNELAP 69627
Pyridine 07/19/2011 14:430.604 mg/Kg-dry 1NDNELAP 69627
1,2-Diphenylhydrazine 07/19/2011 14:431.02 mg/Kg-dry 1ND 69627
Surr: 2,4,6-Tribromophenol 07/19/2011 14:4332.7-130 %REC 177.5 69627
Surr: 2-Fluorobiphenyl 07/19/2011 14:4334.1-116 %REC 176.1 69627
Surr: 2-Fluorophenol 07/19/2011 14:4330.5-99 %REC 170.1 69627
Surr: Nitrobenzene-d5 07/19/2011 14:4334.1-101 %REC 182.7 69627
Surr: Phenol-d5 07/19/2011 14:4334.9-110 %REC 173.2 69627
Surr: p-Terphenyl-d14 07/19/2011 14:4341.7-124 %REC 190.5 69627
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.4-Nitrophenol was outside upper QC limits in the LCS. Sample was ND.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,1,1-Trichloroethane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,1,2,2-Tetrachloroethane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,1,2-Trichloro-1,2,2-trifluoroethane 07/21/2011 14:195.2 µg/Kg-dry 1ND 69790
1,1,2-Trichloroethane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,1-Dichloro-2-propanone 07/21/2011 14:1952.0 µg/Kg-dry 1ND 69790
1,1-Dichloroethane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,1-Dichloroethene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,1-Dichloropropene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,2,3-Trichlorobenzene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,2,3-Trichloropropane 07/21/2011 14:1910.4 µg/Kg-dry 1NDNELAP 69790
1,2,3-Trimethylbenzene 07/21/2011 14:195.2 µg/Kg-dry 1ND 69790
1,2,4-Trichlorobenzene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,2,4-Trimethylbenzene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,2-Dibromo-3-chloropropane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,2-Dibromoethane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,2-Dichlorobenzene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,2-Dichloroethane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,2-Dichloropropane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,3,5-Trimethylbenzene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,3-Dichlorobenzene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,3-Dichloropropane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1,4-Dichlorobenzene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
1-Chlorobutane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
2,2-Dichloropropane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
2-Butanone 07/21/2011 14:1952.0 µg/Kg-dry 1NDNELAP 69790
Page 44 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 10:30
Lab ID: 11070610-007 Client Sample ID: TSA-01 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS2-Chlorotoluene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
2-Hexanone 07/21/2011 14:1952.0 µg/Kg-dry 1NDNELAP 69790
2-Nitropropane 07/21/2011 14:1952.0 µg/Kg-dry 1NDNELAP 69790
4-Chlorotoluene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
4-Methyl-2-pentanone 07/21/2011 14:1952.0 µg/Kg-dry 1NDNELAP 69790
Acetone 07/21/2011 14:1952.0 µg/Kg-dry 195.4NELAP 69790
Acrolein 07/21/2011 14:19104 µg/Kg-dry 1NDNELAP 69790
Acrylonitrile 07/21/2011 14:1910.4 µg/Kg-dry 1NDNELAP 69790
Allyl chloride 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Benzene 07/21/2011 14:191.0 µg/Kg-dry 1NDNELAP 69790
Bromobenzene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Bromochloromethane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Bromodichloromethane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Bromoform 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Bromomethane 07/21/2011 14:1910.4 µg/Kg-dry 1NDNELAP 69790
Carbon disulfide 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Carbon tetrachloride 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Chlorobenzene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Chloroethane 07/21/2011 14:1910.4 µg/Kg-dry 1NDNELAP 69790
Chloroform 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Chloromethane 07/21/2011 14:1910.4 µg/Kg-dry 1NDNELAP 69790
cis-1,2-Dichloroethene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
cis-1,3-Dichloropropene 07/21/2011 14:194.2 µg/Kg-dry 1NDNELAP 69790
Cyclohexanone 07/21/2011 14:19104 µg/Kg-dry 1ND 69790
Dibromochloromethane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Dibromomethane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Dichlorodifluoromethane 07/21/2011 14:1910.4 µg/Kg-dry 1NDNELAP 69790
Ethyl acetate 07/21/2011 14:1952.0 µg/Kg-dry 1NDNELAP 69790
Ethyl ether 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Ethyl methacrylate 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Ethylbenzene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Heptane 07/21/2011 14:1920.8 µg/Kg-dry 1ND 69790
Hexachlorobutadiene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Hexachloroethane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Iodomethane 07/21/2011 14:1910.4 µg/Kg-dry 1NDNELAP 69790
Isopropylbenzene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
m,p-Xylenes 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Methacrylonitrile 07/21/2011 14:1952.0 µg/Kg-dry 1NDNELAP 69790
Methyl Methacrylate 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Methyl tert-butyl ether 07/21/2011 14:192.1 µg/Kg-dry 1NDNELAP 69790
Methylacrylate 07/21/2011 14:1910.4 µg/Kg-dry 1ND 69790
Methylene chloride J 07/21/2011 14:195.2 µg/Kg-dry 11.9NELAP 69790
Naphthalene 07/21/2011 14:1910.4 µg/Kg-dry 1NDNELAP 69790
n-Butylbenzene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
n-Hexane 07/21/2011 14:1920.8 µg/Kg-dry 1ND 69790
Nitrobenzene 07/21/2011 14:19104 µg/Kg-dry 1NDNELAP 69790
n-Propylbenzene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Page 45 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 10:30
Lab ID: 11070610-007 Client Sample ID: TSA-01 (5-6)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSo-Xylene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Pentachloroethane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
p-Isopropyltoluene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Propionitrile 07/21/2011 14:1952.0 µg/Kg-dry 1NDNELAP 69790
sec-Butylbenzene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Styrene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
tert-Butylbenzene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Tetrachloroethene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Tetrahydrofuran 07/21/2011 14:1952.0 µg/Kg-dry 1NDNELAP 69790
Toluene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
trans-1,2-Dichloroethene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
trans-1,3-Dichloropropene 07/21/2011 14:194.2 µg/Kg-dry 1NDNELAP 69790
Trichloroethene 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Trichlorofluoromethane 07/21/2011 14:195.2 µg/Kg-dry 1NDNELAP 69790
Vinyl acetate 07/21/2011 14:1952.0 µg/Kg-dry 1NDNELAP 69790
Vinyl chloride 07/21/2011 14:192.1 µg/Kg-dry 1NDNELAP 69790
Surr: 1,2-Dichloroethane-d4 07/21/2011 14:1972.2-131 %REC 1129.2 69790
Surr: 4-Bromofluorobenzene 07/21/2011 14:1982.1-116 %REC 1103.0 69790
Surr: Dibromofluoromethane 07/21/2011 14:1977.7-120 %REC 1110.0 69790
Surr: Toluene-d8 07/21/2011 14:1986-116 %REC 1107.2 69790
SW-846 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 07/23/2011 1:500.05 mg/Kg-dry 1NDNELAP R152491
2,4,5-TP (Silvex) 07/23/2011 1:500.05 mg/Kg-dry 1NDNELAP R152491
2,4-D 07/23/2011 1:500.05 mg/Kg-dry 1NDNELAP R152491
2,4-DB 07/23/2011 1:500.05 mg/Kg-dry 1NDNELAP R152491
3,5-Dichlorobenzoic Acid 07/23/2011 1:500.05 mg/Kg-dry 1NDNELAP R152491
Acifluorfen 07/23/2011 1:500.05 mg/Kg-dry 1NDNELAP R152491
Bentazon 07/23/2011 1:500.05 mg/Kg-dry 1NDNELAP R152491
Chloramben 07/23/2011 1:500.05 mg/Kg-dry 1NDNELAP R152491
Dalapon 07/23/2011 1:500.05 mg/Kg-dry 1NDNELAP R152491
DCPA 07/23/2011 1:500.05 mg/Kg-dry 1NDNELAP R152491
Dicamba 07/23/2011 1:500.05 mg/Kg-dry 1NDNELAP R152491
Dichlorprop 07/23/2011 1:500.05 mg/Kg-dry 1NDNELAP R152491
Dinoseb 07/23/2011 1:500.05 mg/Kg-dry 1NDNELAP R152491
Pentachlorophenol 07/23/2011 1:500.05 mg/Kg-dry 1NDNELAP R152491
Picloram 07/23/2011 1:500.05 mg/Kg-dry 1NDNELAP R152491
Surr: DCAA 07/23/2011 1:5024-140 %REC 176.1 R152491
The LCS/LCSD RPD result exceeded the QC control limits for Dinoseb; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data.
Page 46 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 11:15
Lab ID: 11070610-008 Client Sample ID: TSA-03 (3-4)
Matrix: SOLID
Batch
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 07/18/2011 10:000.1 % 118.7 R152055
STANDARD METHODS 18TH ED. 2540 GTotal Solids 07/18/2011 8:300.1 % 181.3 R152054
SW-846 9012A (TOTAL)Cyanide J 07/20/2011 7:240.31 mg/Kg-dry 10.16NELAP 69730
SW-846 3050B, 6010B, METALS BY ICPAluminum 07/19/2011 13:234.72 mg/Kg-dry 118400NELAP 69636
Antimony 07/27/2011 12:454.81 mg/Kg-dry 1< 4.81NELAP 69908
Arsenic 07/19/2011 13:232.36 mg/Kg-dry 19.84NELAP 69636
Barium 07/20/2011 16:030.47 mg/Kg-dry 1124NELAP 69636
Beryllium 07/19/2011 13:230.09 mg/Kg-dry 10.69NELAP 69636
Cadmium 07/19/2011 13:230.19 mg/Kg-dry 10.24NELAP 69636
Calcium 07/19/2011 13:234.72 mg/Kg-dry 118800NELAP 69636
Chromium 07/19/2011 13:230.94 mg/Kg-dry 118.1NELAP 69636
Cobalt 07/19/2011 13:230.94 mg/Kg-dry 19.55NELAP 69636
Copper 07/19/2011 13:230.94 mg/Kg-dry 115.9NELAP 69636
Iron 07/19/2011 13:231.89 mg/Kg-dry 122300NELAP 69636
Lead 07/19/2011 13:233.77 mg/Kg-dry 116.3NELAP 69636
Magnesium 07/19/2011 13:230.94 mg/Kg-dry 17660NELAP 69636
Manganese 07/19/2011 13:230.47 mg/Kg-dry 1701NELAP 69636
Nickel 07/19/2011 13:230.94 mg/Kg-dry 115.8NELAP 69636
Potassium 07/20/2011 16:039.43 mg/Kg-dry 12220NELAP 69636
Silver 07/21/2011 10:450.52 mg/Kg-dry 1< 0.52NELAP 69636
Sodium 07/20/2011 16:034.72 mg/Kg-dry 162.2NELAP 69636
Vanadium 07/20/2011 16:030.94 mg/Kg-dry 134.6NELAP 69636
Zinc 07/19/2011 13:230.94 mg/Kg-dry 155.8NELAP 69636
SW-846 3050B, METALS BY GFAASelenium 7740 J 07/20/2011 9:400.588 mg/Kg-dry 10.46NELAP 69639
Thallium 7841 07/28/2011 9:460.196 mg/Kg-dry 10.274NELAP 69639
SW-846 7471AMercury 07/19/2011 12:250.012 mg/Kg-dry 10.022NELAP 69631
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel 07/19/2011 15:296.13 mg/Kg-dry 1NDNELAP 69637
Kerosene 07/19/2011 15:296.13 mg/Kg-dry 1NDNELAP 69637
Mineral Spirits 07/19/2011 15:296.13 mg/Kg-dry 1NDNELAP 69637
Motor Oil # 07/19/2011 15:296.13 mg/Kg-dry 17.37NELAP 69637
Surr: n-Tetracontane 07/19/2011 15:2950.6-140 %REC 196.4 69637
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/26/2011 0:5720.5 µg/Kg-dry 10NDNELAP 69671
4,4´-DDE 07/26/2011 0:5720.5 µg/Kg-dry 10NDNELAP 69671
4,4´-DDT 07/26/2011 0:5720.5 µg/Kg-dry 10NDNELAP 69671
Alachlor 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
Aldrin 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
alpha-BHC 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
alpha-Chlordane 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
beta-BHC 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
Page 47 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 11:15
Lab ID: 11070610-008 Client Sample ID: TSA-03 (3-4)
Matrix: SOLID
Batch
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECDChlordane 07/22/2011 0:214.11 µg/Kg-dry 1NDNELAP 69671
delta-BHC 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
Dieldrin 07/22/2011 0:212.05 µg/Kg-dry 12.09NELAP 69671
Endosulfan I 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
Endosulfan II 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
Endosulfan sulfate 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
Endrin 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
Endrin aldehyde 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
Endrin ketone 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
gamma-BHC 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
gamma-Chlordane 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
Heptachlor 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
Heptachlor epoxide 07/22/2011 0:212.05 µg/Kg-dry 12.85NELAP 69671
Methoxychlor 07/22/2011 0:212.05 µg/Kg-dry 1NDNELAP 69671
Toxaphene 07/22/2011 0:2136.9 µg/Kg-dry 1NDNELAP 69671
Surr: Decachlorobiphenyl 07/22/2011 0:2148-149 %REC 1103.8 69671
Surr: Tetrachloro-m-xylene 07/22/2011 0:2119-145 %REC 174.9 69671
Elevated reporting limit(s) due to sample extract composition.
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/20/2011 20:0246.1 µg/Kg-dry 1NDNELAP 69671
Aroclor 1221 07/20/2011 20:0246.1 µg/Kg-dry 1NDNELAP 69671
Aroclor 1232 07/20/2011 20:0246.1 µg/Kg-dry 1NDNELAP 69671
Aroclor 1242 07/20/2011 20:0246.1 µg/Kg-dry 1NDNELAP 69671
Aroclor 1248 07/20/2011 20:0246.1 µg/Kg-dry 1NDNELAP 69671
Aroclor 1254 07/20/2011 20:0246.1 µg/Kg-dry 1NDNELAP 69671
Aroclor 1260 07/20/2011 20:0246.1 µg/Kg-dry 1NDNELAP 69671
Surr: Decachlorobiphenyl 07/20/2011 20:025-156 %REC 1100.7 69671
Surr: Tetrachloro-meta-xylene 07/20/2011 20:027.35-123 %REC 177.5 69671
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Acenaphthylene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Anthracene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Benzo(a)anthracene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Benzo(a)pyrene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Benzo(b)fluoranthene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Benzo(g,h,i)perylene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Benzo(k)fluoranthene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Bis(2-ethylhexyl)phthalate 07/21/2011 5:250.082 mg/Kg-dry 1NDNELAP 69628
Chrysene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Dibenzo(a,h)anthracene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Fluoranthene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Fluorene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Indeno(1,2,3-cd)pyrene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Naphthalene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Phenanthrene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Pyrene 07/21/2011 5:250.004 mg/Kg-dry 1NDNELAP 69628
Surr: 2-Fluorobiphenyl 07/21/2011 5:2510-131 %REC 169.6 69628
Page 48 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 11:15
Lab ID: 11070610-008 Client Sample ID: TSA-03 (3-4)
Matrix: SOLID
Batch
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: Nitrobenzene-d5 07/21/2011 5:2510-132 %REC 176.1 69628
Surr: p-Terphenyl-d14 07/21/2011 5:2580.2-138 %REC 193.4 69628
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
1,2-Dichlorobenzene 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
1,3-Dichlorobenzene 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
1,4-Dichlorobenzene 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
2,4,5-Trichlorophenol 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
2,4,6-Trichlorophenol 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
2,4-Dichlorophenol 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
2,4-Dimethylphenol 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
2,4-Dinitrophenol 07/19/2011 15:151.23 mg/Kg-dry 1NDNELAP 69627
2,4-Dinitrotoluene 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
2,6-Dinitrotoluene 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
2-Chloronaphthalene 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
2-Chlorophenol 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
2-Methoxy-4-methylphenol 07/19/2011 15:150.799 mg/Kg-dry 1ND 69627
2-Methylnaphthalene 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
2-Nitroaniline 07/19/2011 15:151.23 mg/Kg-dry 1NDNELAP 69627
2-Nitrophenol 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
3,3´-Dichlorobenzidine 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
3-Nitroaniline 07/19/2011 15:151.23 mg/Kg-dry 1NDNELAP 69627
4,6-Dinitro-2-methylphenol 07/19/2011 15:151.23 mg/Kg-dry 1NDNELAP 69627
4-Bromophenyl phenyl ether 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
4-Chloro-3-methylphenol 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
4-Chloroaniline 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
4-Chlorophenyl phenyl ether 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
4-Nitroaniline 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
4-Nitrophenol 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
Aniline 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
Azobenzene 07/19/2011 15:150.430 mg/Kg-dry 1ND 69627
Benzidine 07/19/2011 15:151.30 mg/Kg-dry 1see noteNELAP 69627
Benzoic acid 07/19/2011 15:151.84 mg/Kg-dry 1NDNELAP 69627
Benzyl alcohol 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroethoxy)methane 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroethyl)ether 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroisopropyl)ether 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
Butyl benzyl phthalate 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
Carbazole 07/19/2011 15:150.615 mg/Kg-dry 1ND 69627
Dibenzofuran 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
Diethyl phthalate 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
Dimethyl phthalate 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
Di-n-butyl phthalate 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
Di-n-octyl phthalate 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
Hexachlorobenzene 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
Hexachlorobutadiene 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
Hexachlorocyclopentadiene 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
Page 49 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 11:15
Lab ID: 11070610-008 Client Sample ID: TSA-03 (3-4)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachloroethane 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
Isophorone 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
m,p-Cresol 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
Nitrobenzene 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
N-Nitrosodimethylamine 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
N-Nitroso-di-n-propylamine 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
N-Nitrosodiphenylamine 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
o-Cresol 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
Pentachlorophenol 07/19/2011 15:152.46 mg/Kg-dry 1NDNELAP 69627
Phenol 07/19/2011 15:150.430 mg/Kg-dry 1NDNELAP 69627
Pyridine 07/19/2011 15:150.615 mg/Kg-dry 1NDNELAP 69627
1,2-Diphenylhydrazine 07/19/2011 15:151.03 mg/Kg-dry 1ND 69627
Surr: 2,4,6-Tribromophenol 07/19/2011 15:1532.7-130 %REC 181.6 69627
Surr: 2-Fluorobiphenyl 07/19/2011 15:1534.1-116 %REC 167.5 69627
Surr: 2-Fluorophenol 07/19/2011 15:1530.5-99 %REC 170.7 69627
Surr: Nitrobenzene-d5 07/19/2011 15:1534.1-101 %REC 178.2 69627
Surr: Phenol-d5 07/19/2011 15:1534.9-110 %REC 171.2 69627
Surr: p-Terphenyl-d14 07/19/2011 15:1541.7-124 %REC 191.2 69627
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.4-Nitrophenol was outside upper QC limits in the LCS. Sample was ND.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,1,1-Trichloroethane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,1,2,2-Tetrachloroethane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,1,2-Trichloro-1,2,2-trifluoroethane 07/21/2011 0:304.7 µg/Kg-dry 1ND 69754
1,1,2-Trichloroethane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,1-Dichloro-2-propanone 07/21/2011 0:3047.1 µg/Kg-dry 1ND 69754
1,1-Dichloroethane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,1-Dichloroethene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,1-Dichloropropene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,2,3-Trichlorobenzene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,2,3-Trichloropropane 07/21/2011 0:309.4 µg/Kg-dry 1NDNELAP 69754
1,2,3-Trimethylbenzene 07/21/2011 0:304.7 µg/Kg-dry 1ND 69754
1,2,4-Trichlorobenzene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,2,4-Trimethylbenzene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,2-Dibromo-3-chloropropane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,2-Dibromoethane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,2-Dichlorobenzene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,2-Dichloroethane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,2-Dichloropropane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,3,5-Trimethylbenzene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,3-Dichlorobenzene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,3-Dichloropropane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1,4-Dichlorobenzene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
1-Chlorobutane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
2,2-Dichloropropane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
2-Butanone 07/21/2011 0:3047.1 µg/Kg-dry 1NDNELAP 69754
Page 50 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 11:15
Lab ID: 11070610-008 Client Sample ID: TSA-03 (3-4)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS2-Chlorotoluene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
2-Hexanone 07/21/2011 0:3047.1 µg/Kg-dry 1NDNELAP 69754
2-Nitropropane 07/21/2011 0:3047.1 µg/Kg-dry 1NDNELAP 69754
4-Chlorotoluene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
4-Methyl-2-pentanone 07/21/2011 0:3047.1 µg/Kg-dry 1NDNELAP 69754
Acetone 07/21/2011 0:3047.1 µg/Kg-dry 150.5NELAP 69754
Acrolein 07/21/2011 0:3094.2 µg/Kg-dry 1NDNELAP 69754
Acrylonitrile 07/21/2011 0:309.4 µg/Kg-dry 1NDNELAP 69754
Allyl chloride 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Benzene 07/21/2011 0:300.9 µg/Kg-dry 11.0NELAP 69754
Bromobenzene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Bromochloromethane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Bromodichloromethane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Bromoform 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Bromomethane 07/21/2011 0:309.4 µg/Kg-dry 1NDNELAP 69754
Carbon disulfide 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Carbon tetrachloride 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Chlorobenzene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Chloroethane 07/21/2011 0:309.4 µg/Kg-dry 1NDNELAP 69754
Chloroform 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Chloromethane 07/21/2011 0:309.4 µg/Kg-dry 1NDNELAP 69754
cis-1,2-Dichloroethene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
cis-1,3-Dichloropropene 07/21/2011 0:303.8 µg/Kg-dry 1NDNELAP 69754
Cyclohexanone 07/21/2011 0:3094.2 µg/Kg-dry 1ND 69754
Dibromochloromethane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Dibromomethane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Dichlorodifluoromethane 07/21/2011 0:309.4 µg/Kg-dry 1NDNELAP 69754
Ethyl acetate 07/21/2011 0:3047.1 µg/Kg-dry 1NDNELAP 69754
Ethyl ether 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Ethyl methacrylate 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Ethylbenzene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Heptane 07/21/2011 0:3018.8 µg/Kg-dry 1ND 69754
Hexachlorobutadiene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Hexachloroethane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Iodomethane 07/21/2011 0:309.4 µg/Kg-dry 1NDNELAP 69754
Isopropylbenzene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
m,p-Xylenes 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Methacrylonitrile 07/21/2011 0:3047.1 µg/Kg-dry 1NDNELAP 69754
Methyl Methacrylate 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Methyl tert-butyl ether 07/21/2011 0:301.9 µg/Kg-dry 1NDNELAP 69754
Methylacrylate 07/21/2011 0:309.4 µg/Kg-dry 1ND 69754
Methylene chloride J 07/21/2011 0:304.7 µg/Kg-dry 12.4NELAP 69754
Naphthalene 07/21/2011 0:309.4 µg/Kg-dry 1NDNELAP 69754
n-Butylbenzene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
n-Hexane 07/21/2011 0:3018.8 µg/Kg-dry 1ND 69754
Nitrobenzene 07/21/2011 0:3094.2 µg/Kg-dry 1NDNELAP 69754
n-Propylbenzene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Page 51 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 11:15
Lab ID: 11070610-008 Client Sample ID: TSA-03 (3-4)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSo-Xylene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Pentachloroethane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
p-Isopropyltoluene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Propionitrile 07/21/2011 0:3047.1 µg/Kg-dry 1NDNELAP 69754
sec-Butylbenzene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Styrene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
tert-Butylbenzene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Tetrachloroethene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Tetrahydrofuran 07/21/2011 0:3047.1 µg/Kg-dry 1NDNELAP 69754
Toluene J 07/21/2011 0:304.7 µg/Kg-dry 12.3NELAP 69754
trans-1,2-Dichloroethene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
trans-1,3-Dichloropropene 07/21/2011 0:303.8 µg/Kg-dry 1NDNELAP 69754
Trichloroethene 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Trichlorofluoromethane 07/21/2011 0:304.7 µg/Kg-dry 1NDNELAP 69754
Vinyl acetate 07/21/2011 0:3047.1 µg/Kg-dry 1NDNELAP 69754
Vinyl chloride 07/21/2011 0:301.9 µg/Kg-dry 1NDNELAP 69754
Surr: 1,2-Dichloroethane-d4 07/21/2011 0:3072.2-131 %REC 1118.5 69754
Surr: 4-Bromofluorobenzene 07/21/2011 0:3082.1-116 %REC 193.7 69754
Surr: Dibromofluoromethane 07/21/2011 0:3077.7-120 %REC 1102.0 69754
Surr: Toluene-d8 07/21/2011 0:3086-116 %REC 1114.0 69754
SW-846 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 07/23/2011 2:370.08 mg/Kg-dry 1NDNELAP R152491
2,4,5-TP (Silvex) 07/23/2011 2:370.08 mg/Kg-dry 1NDNELAP R152491
2,4-D 07/23/2011 2:370.08 mg/Kg-dry 1NDNELAP R152491
2,4-DB 07/23/2011 2:370.08 mg/Kg-dry 1NDNELAP R152491
3,5-Dichlorobenzoic Acid 07/23/2011 2:370.08 mg/Kg-dry 1NDNELAP R152491
Acifluorfen 07/23/2011 2:370.08 mg/Kg-dry 1NDNELAP R152491
Bentazon 07/23/2011 2:370.08 mg/Kg-dry 1NDNELAP R152491
Chloramben 07/23/2011 2:370.08 mg/Kg-dry 1NDNELAP R152491
Dalapon 07/23/2011 2:370.08 mg/Kg-dry 1NDNELAP R152491
DCPA 07/23/2011 2:370.08 mg/Kg-dry 1NDNELAP R152491
Dicamba 07/23/2011 2:370.08 mg/Kg-dry 1NDNELAP R152491
Dichlorprop 07/23/2011 2:370.08 mg/Kg-dry 1NDNELAP R152491
Dinoseb 07/23/2011 2:370.08 mg/Kg-dry 1NDNELAP R152491
Pentachlorophenol 07/23/2011 2:370.08 mg/Kg-dry 1NDNELAP R152491
Picloram 07/23/2011 2:370.08 mg/Kg-dry 1NDNELAP R152491
Surr: DCAA 07/23/2011 2:3724-140 %REC 153.9 R152491
The LCS/LCSD RPD result exceeded the QC control limits for Dinoseb; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data.
Page 52 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 12:00
Lab ID: 11070610-009 Client Sample ID: TSA-04 (4-5)
Matrix: SOLID
Batch
EPA SW846 3550C, 5035A, ASTM D2974Percent Moisture 07/18/2011 10:000.1 % 118.6 R152055
STANDARD METHODS 18TH ED. 2540 GTotal Solids 07/18/2011 8:300.1 % 181.4 R152054
SW-846 9012A (TOTAL)Cyanide 07/20/2011 7:240.31 mg/Kg-dry 1< 0.31NELAP 69730
SW-846 3050B, 6010B, METALS BY ICPAluminum S 07/19/2011 13:294.63 mg/Kg-dry 120800NELAP 69636
Antimony 07/27/2011 23:534.72 mg/Kg-dry 1< 4.72NELAP 69908
Arsenic 07/19/2011 13:292.31 mg/Kg-dry 18.70NELAP 69636
Barium 07/20/2011 16:090.46 mg/Kg-dry 1148NELAP 69636
Beryllium 07/19/2011 13:290.09 mg/Kg-dry 10.81NELAP 69636
Cadmium 07/19/2011 13:290.19 mg/Kg-dry 10.36NELAP 69636
Calcium S 07/19/2011 13:294.63 mg/Kg-dry 16500NELAP 69636
Chromium 07/19/2011 13:290.93 mg/Kg-dry 121.3NELAP 69636
Cobalt 07/19/2011 13:290.93 mg/Kg-dry 111.7NELAP 69636
Copper 07/19/2011 13:290.93 mg/Kg-dry 116.6NELAP 69636
Iron S 07/19/2011 13:291.85 mg/Kg-dry 124400NELAP 69636
Lead 07/19/2011 13:293.70 mg/Kg-dry 117.8NELAP 69636
Magnesium S 07/19/2011 13:290.93 mg/Kg-dry 14020NELAP 69636
Manganese S 07/19/2011 13:290.46 mg/Kg-dry 1849NELAP 69636
Nickel 07/19/2011 13:290.93 mg/Kg-dry 118.1NELAP 69636
Potassium S 07/20/2011 16:099.26 mg/Kg-dry 12640NELAP 69636
Silver 07/21/2011 10:510.51 mg/Kg-dry 1< 0.51NELAP 69636
Sodium 07/20/2011 16:094.63 mg/Kg-dry 160.8NELAP 69636
Vanadium 07/20/2011 16:090.93 mg/Kg-dry 139.0NELAP 69636
Zinc 07/19/2011 13:290.93 mg/Kg-dry 167.4NELAP 69636
K - Sample concentration was greater than 5 times the spike concentration.Al, Ca, Fe, Mg, Mn - Sample concentration was greater than 5 times the spike concentration.
SW-846 3050B, METALS BY GFAASelenium 7740 J 07/20/2011 8:430.545 mg/Kg-dry 10.35NELAP 69639
Thallium 7841 07/28/2011 9:500.182 mg/Kg-dry 10.342NELAP 69639
SW-846 7471AMercury 07/19/2011 12:250.012 mg/Kg-dry 10.028NELAP 69631
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FIDDiesel # 07/19/2011 16:246.15 mg/Kg-dry 16.19NELAP 69637
Kerosene 07/19/2011 16:246.15 mg/Kg-dry 1NDNELAP 69637
Mineral Spirits 07/19/2011 16:246.15 mg/Kg-dry 1NDNELAP 69637
Motor Oil 07/19/2011 16:246.15 mg/Kg-dry 1NDNELAP 69637
Surr: n-Tetracontane 07/19/2011 16:2450.6-140 %REC 194.4 69637
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD4,4´-DDD 07/26/2011 2:1520.5 µg/Kg-dry 10NDNELAP 69671
4,4´-DDE 07/26/2011 2:1520.5 µg/Kg-dry 10NDNELAP 69671
4,4´-DDT 07/26/2011 2:1520.5 µg/Kg-dry 10NDNELAP 69671
Alachlor 07/22/2011 1:392.05 µg/Kg-dry 1NDNELAP 69671
Aldrin 07/22/2011 1:392.05 µg/Kg-dry 1NDNELAP 69671
alpha-BHC 07/22/2011 1:392.05 µg/Kg-dry 1NDNELAP 69671
alpha-Chlordane 07/22/2011 1:392.05 µg/Kg-dry 1NDNELAP 69671
Page 53 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 12:00
Lab ID: 11070610-009 Client Sample ID: TSA-04 (4-5)
Matrix: SOLID
Batch
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECDbeta-BHC 07/22/2011 1:392.05 µg/Kg-dry 1NDNELAP 69671
Chlordane J 07/22/2011 1:394.10 µg/Kg-dry 13.7NELAP 69671
delta-BHC 07/22/2011 1:392.05 µg/Kg-dry 1NDNELAP 69671
Dieldrin 07/22/2011 1:392.05 µg/Kg-dry 13.00NELAP 69671
Endosulfan I 07/22/2011 1:392.05 µg/Kg-dry 1NDNELAP 69671
Endosulfan II 07/22/2011 1:392.05 µg/Kg-dry 1NDNELAP 69671
Endosulfan sulfate 07/22/2011 1:392.05 µg/Kg-dry 1NDNELAP 69671
Endrin 07/22/2011 1:392.05 µg/Kg-dry 1NDNELAP 69671
Endrin aldehyde 07/22/2011 1:392.05 µg/Kg-dry 1NDNELAP 69671
Endrin ketone 07/22/2011 1:392.05 µg/Kg-dry 1NDNELAP 69671
gamma-BHC 07/22/2011 1:392.05 µg/Kg-dry 1NDNELAP 69671
gamma-Chlordane 07/22/2011 1:392.05 µg/Kg-dry 13.68NELAP 69671
Heptachlor 07/22/2011 1:392.05 µg/Kg-dry 1NDNELAP 69671
Heptachlor epoxide 07/22/2011 1:392.05 µg/Kg-dry 17.45NELAP 69671
Methoxychlor 07/22/2011 1:392.05 µg/Kg-dry 1NDNELAP 69671
Toxaphene 07/22/2011 1:3936.8 µg/Kg-dry 1NDNELAP 69671
Surr: Decachlorobiphenyl 07/22/2011 1:3948-149 %REC 1109.5 69671
Surr: Tetrachloro-m-xylene 07/22/2011 1:3919-145 %REC 177.5 69671
Elevated reporting limit(s) due to sample extract composition.
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECDAroclor 1016 07/20/2011 20:2046.0 µg/Kg-dry 1NDNELAP 69671
Aroclor 1221 07/20/2011 20:2046.0 µg/Kg-dry 1NDNELAP 69671
Aroclor 1232 07/20/2011 20:2046.0 µg/Kg-dry 1NDNELAP 69671
Aroclor 1242 07/20/2011 20:2046.0 µg/Kg-dry 1NDNELAP 69671
Aroclor 1248 07/20/2011 20:2046.0 µg/Kg-dry 1NDNELAP 69671
Aroclor 1254 07/20/2011 20:2046.0 µg/Kg-dry 1NDNELAP 69671
Aroclor 1260 07/20/2011 20:2046.0 µg/Kg-dry 1NDNELAP 69671
Surr: Decachlorobiphenyl 07/20/2011 20:205-156 %REC 1105.7 69671
Surr: Tetrachloro-meta-xylene 07/20/2011 20:207.35-123 %REC 181.5 69671
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSAcenaphthene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Acenaphthylene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Anthracene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Benzo(a)anthracene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Benzo(a)pyrene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Benzo(b)fluoranthene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Benzo(g,h,i)perylene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Benzo(k)fluoranthene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Bis(2-ethylhexyl)phthalate 07/21/2011 1:520.082 mg/Kg-dry 1NDNELAP 69628
Chrysene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Dibenzo(a,h)anthracene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Fluoranthene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Fluorene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Indeno(1,2,3-cd)pyrene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Naphthalene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Phenanthrene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Pyrene 07/21/2011 1:520.004 mg/Kg-dry 1NDNELAP 69628
Page 54 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 12:00
Lab ID: 11070610-009 Client Sample ID: TSA-04 (4-5)
Matrix: SOLID
Batch
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS Surr: 2-Fluorobiphenyl 07/21/2011 1:5210-131 %REC 168.1 69628
Surr: Nitrobenzene-d5 07/21/2011 1:5210-132 %REC 174.9 69628
Surr: p-Terphenyl-d14 07/21/2011 1:5280.2-138 %REC 187.7 69628
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS1,2,4-Trichlorobenzene 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
1,2-Dichlorobenzene 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
1,3-Dichlorobenzene 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
1,4-Dichlorobenzene 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
2,4,5-Trichlorophenol 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
2,4,6-Trichlorophenol 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
2,4-Dichlorophenol 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
2,4-Dimethylphenol 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
2,4-Dinitrophenol 07/19/2011 15:481.22 mg/Kg-dry 1NDNELAP 69627
2,4-Dinitrotoluene 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
2,6-Dinitrotoluene 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
2-Chloronaphthalene 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
2-Chlorophenol 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
2-Methoxy-4-methylphenol 07/19/2011 15:480.796 mg/Kg-dry 1ND 69627
2-Methylnaphthalene 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
2-Nitroaniline 07/19/2011 15:481.22 mg/Kg-dry 1NDNELAP 69627
2-Nitrophenol 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
3,3´-Dichlorobenzidine 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
3-Nitroaniline 07/19/2011 15:481.22 mg/Kg-dry 1NDNELAP 69627
4,6-Dinitro-2-methylphenol 07/19/2011 15:481.22 mg/Kg-dry 1NDNELAP 69627
4-Bromophenyl phenyl ether 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
4-Chloro-3-methylphenol 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
4-Chloroaniline 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
4-Chlorophenyl phenyl ether 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
4-Nitroaniline 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
4-Nitrophenol 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
Aniline 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
Azobenzene 07/19/2011 15:480.429 mg/Kg-dry 1ND 69627
Benzidine 07/19/2011 15:481.29 mg/Kg-dry 1see noteNELAP 69627
Benzoic acid 07/19/2011 15:481.84 mg/Kg-dry 1NDNELAP 69627
Benzyl alcohol 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroethoxy)methane 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroethyl)ether 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
Bis(2-chloroisopropyl)ether 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
Butyl benzyl phthalate 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
Carbazole 07/19/2011 15:480.612 mg/Kg-dry 1ND 69627
Dibenzofuran 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
Diethyl phthalate 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
Dimethyl phthalate 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
Di-n-butyl phthalate 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
Di-n-octyl phthalate 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
Hexachlorobenzene 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
Hexachlorobutadiene 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
Page 55 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 12:00
Lab ID: 11070610-009 Client Sample ID: TSA-04 (4-5)
Matrix: SOLID
Batch
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MSHexachlorocyclopentadiene 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
Hexachloroethane 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
Isophorone 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
m,p-Cresol 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
Nitrobenzene 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
N-Nitrosodimethylamine 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
N-Nitroso-di-n-propylamine 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
N-Nitrosodiphenylamine 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
o-Cresol 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
Pentachlorophenol 07/19/2011 15:482.45 mg/Kg-dry 1NDNELAP 69627
Phenol 07/19/2011 15:480.429 mg/Kg-dry 1NDNELAP 69627
Pyridine 07/19/2011 15:480.612 mg/Kg-dry 1NDNELAP 69627
1,2-Diphenylhydrazine 07/19/2011 15:481.03 mg/Kg-dry 1ND 69627
Surr: 2,4,6-Tribromophenol 07/19/2011 15:4832.7-130 %REC 180.7 69627
Surr: 2-Fluorobiphenyl 07/19/2011 15:4834.1-116 %REC 170.8 69627
Surr: 2-Fluorophenol 07/19/2011 15:4830.5-99 %REC 170.0 69627
Surr: Nitrobenzene-d5 07/19/2011 15:4834.1-101 %REC 178.5 69627
Surr: Phenol-d5 07/19/2011 15:4834.9-110 %REC 171.5 69627
Surr: p-Terphenyl-d14 07/19/2011 15:4841.7-124 %REC 189.1 69627
Note: Benzidine is currently not reportable while extraction efficiency and recovery are investigated.4-Nitrophenol was outside upper QC limits in the LCS. Sample was ND.
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS1,1,1,2-Tetrachloroethane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,1,1-Trichloroethane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,1,2,2-Tetrachloroethane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,1,2-Trichloro-1,2,2-trifluoroethane 07/21/2011 14:495.9 µg/Kg-dry 1ND 69790
1,1,2-Trichloroethane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,1-Dichloro-2-propanone 07/21/2011 14:4958.6 µg/Kg-dry 1ND 69790
1,1-Dichloroethane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,1-Dichloroethene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,1-Dichloropropene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,2,3-Trichlorobenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,2,3-Trichloropropane 07/21/2011 14:4911.7 µg/Kg-dry 1NDNELAP 69790
1,2,3-Trimethylbenzene 07/21/2011 14:495.9 µg/Kg-dry 1ND 69790
1,2,4-Trichlorobenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,2,4-Trimethylbenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,2-Dibromo-3-chloropropane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,2-Dibromoethane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,2-Dichlorobenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,2-Dichloroethane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,2-Dichloropropane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,3,5-Trimethylbenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,3-Dichlorobenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,3-Dichloropropane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1,4-Dichlorobenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
1-Chlorobutane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
2,2-Dichloropropane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Page 56 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 12:00
Lab ID: 11070610-009 Client Sample ID: TSA-04 (4-5)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS2-Butanone 07/21/2011 14:4958.6 µg/Kg-dry 1NDNELAP 69790
2-Chlorotoluene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
2-Hexanone 07/21/2011 14:4958.6 µg/Kg-dry 1NDNELAP 69790
2-Nitropropane 07/21/2011 14:4958.6 µg/Kg-dry 1NDNELAP 69790
4-Chlorotoluene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
4-Methyl-2-pentanone 07/21/2011 14:4958.6 µg/Kg-dry 1NDNELAP 69790
Acetone 07/21/2011 14:4958.6 µg/Kg-dry 1NDNELAP 69790
Acrolein 07/21/2011 14:49117 µg/Kg-dry 1NDNELAP 69790
Acrylonitrile 07/21/2011 14:4911.7 µg/Kg-dry 1NDNELAP 69790
Allyl chloride 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Benzene 07/21/2011 14:491.2 µg/Kg-dry 1NDNELAP 69790
Bromobenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Bromochloromethane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Bromodichloromethane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Bromoform 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Bromomethane 07/21/2011 14:4911.7 µg/Kg-dry 1NDNELAP 69790
Carbon disulfide 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Carbon tetrachloride 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Chlorobenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Chloroethane 07/21/2011 14:4911.7 µg/Kg-dry 1NDNELAP 69790
Chloroform 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Chloromethane 07/21/2011 14:4911.7 µg/Kg-dry 1NDNELAP 69790
cis-1,2-Dichloroethene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
cis-1,3-Dichloropropene 07/21/2011 14:494.7 µg/Kg-dry 1NDNELAP 69790
Cyclohexanone 07/21/2011 14:49117 µg/Kg-dry 1ND 69790
Dibromochloromethane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Dibromomethane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Dichlorodifluoromethane 07/21/2011 14:4911.7 µg/Kg-dry 1NDNELAP 69790
Ethyl acetate 07/21/2011 14:4958.6 µg/Kg-dry 1NDNELAP 69790
Ethyl ether 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Ethyl methacrylate 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Ethylbenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Heptane 07/21/2011 14:4923.4 µg/Kg-dry 1ND 69790
Hexachlorobutadiene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Hexachloroethane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Iodomethane 07/21/2011 14:4911.7 µg/Kg-dry 1NDNELAP 69790
Isopropylbenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
m,p-Xylenes 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Methacrylonitrile 07/21/2011 14:4958.6 µg/Kg-dry 1NDNELAP 69790
Methyl Methacrylate 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Methyl tert-butyl ether 07/21/2011 14:492.3 µg/Kg-dry 1NDNELAP 69790
Methylacrylate 07/21/2011 14:4911.7 µg/Kg-dry 1ND 69790
Methylene chloride 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Naphthalene 07/21/2011 14:4911.7 µg/Kg-dry 1NDNELAP 69790
n-Butylbenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
n-Hexane 07/21/2011 14:4923.4 µg/Kg-dry 1ND 69790
Nitrobenzene 07/21/2011 14:49117 µg/Kg-dry 1NDNELAP 69790
Page 57 of 104
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 07/14/2011 12:00
Lab ID: 11070610-009 Client Sample ID: TSA-04 (4-5)
Matrix: SOLID
Batch
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MSn-Propylbenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
o-Xylene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Pentachloroethane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
p-Isopropyltoluene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Propionitrile 07/21/2011 14:4958.6 µg/Kg-dry 1NDNELAP 69790
sec-Butylbenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Styrene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
tert-Butylbenzene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Tetrachloroethene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Tetrahydrofuran 07/21/2011 14:4958.6 µg/Kg-dry 1NDNELAP 69790
Toluene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
trans-1,2-Dichloroethene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
trans-1,3-Dichloropropene 07/21/2011 14:494.7 µg/Kg-dry 1NDNELAP 69790
Trichloroethene 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Trichlorofluoromethane 07/21/2011 14:495.9 µg/Kg-dry 1NDNELAP 69790
Vinyl acetate 07/21/2011 14:4958.6 µg/Kg-dry 1NDNELAP 69790
Vinyl chloride 07/21/2011 14:492.3 µg/Kg-dry 1NDNELAP 69790
Surr: 1,2-Dichloroethane-d4 07/21/2011 14:4972.2-131 %REC 1115.3 69790
Surr: 4-Bromofluorobenzene 07/21/2011 14:4982.1-116 %REC 197.9 69790
Surr: Dibromofluoromethane 07/21/2011 14:4977.7-120 %REC 1103.9 69790
Surr: Toluene-d8 07/21/2011 14:4986-116 %REC 1109.4 69790
SW-846 8151A, CHLORINATED HERBICIDES BY GC/ECD2,4,5-T 07/23/2011 3:240.05 mg/Kg-dry 1NDNELAP R152491
2,4,5-TP (Silvex) 07/23/2011 3:240.05 mg/Kg-dry 1NDNELAP R152491
2,4-D 07/23/2011 3:240.05 mg/Kg-dry 1NDNELAP R152491
2,4-DB 07/23/2011 3:240.05 mg/Kg-dry 1NDNELAP R152491
3,5-Dichlorobenzoic Acid 07/23/2011 3:240.05 mg/Kg-dry 1NDNELAP R152491
Acifluorfen 07/23/2011 3:240.05 mg/Kg-dry 1NDNELAP R152491
Bentazon 07/23/2011 3:240.05 mg/Kg-dry 1NDNELAP R152491
Chloramben 07/23/2011 3:240.05 mg/Kg-dry 1NDNELAP R152491
Dalapon 07/23/2011 3:240.05 mg/Kg-dry 1NDNELAP R152491
DCPA 07/23/2011 3:240.05 mg/Kg-dry 1NDNELAP R152491
Dicamba 07/23/2011 3:240.05 mg/Kg-dry 1NDNELAP R152491
Dichlorprop 07/23/2011 3:240.05 mg/Kg-dry 1NDNELAP R152491
Dinoseb 07/23/2011 3:240.05 mg/Kg-dry 1NDNELAP R152491
Pentachlorophenol 07/23/2011 3:240.05 mg/Kg-dry 1NDNELAP R152491
Picloram 07/23/2011 3:240.05 mg/Kg-dry 1NDNELAP R152491
Surr: DCAA 07/23/2011 3:2424-140 %REC 195.0 R152491
The LCS/LCSD RPD result exceeded the QC control limits for Dinoseb; however, both percent recoveries were acceptable. Sample results for the QC batch were accepted based on percent recoveries and completeness of QC data.
Page 58 of 104
Lab Sample ID Client Sample ID Collection DateFractions
TeklabHdrP
Matrix
Sample Summary
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
11070610-001 SBA-N4 (5-6) 07/13/2011 10:006Solid
11070610-002 SBA-K2 (4-5) 07/13/2011 11:306Solid
11070610-003 SBA-J5 (5-6) 07/13/2011 13:156Solid
11070610-004 SBA-H3 (5-6) 07/13/2011 14:306Solid
11070610-005 SBA-F2 (4-5) 07/13/2011 15:306Solid
11070610-006 TSA-02 (8-9) 07/14/2011 9:456Solid
11070610-007 TSA-01 (5-6) 07/14/2011 10:306Solid
11070610-008 TSA-03 (3-4) 07/14/2011 11:156Solid
11070610-009 TSA-04 (4-5) 07/14/2011 12:006Solid
Page 59 of 104
Analysis Date/TimeTest Name Prep Date/Time
____TeklabHdrP
Sample ID Client Sample ID Collection Date Received Date
Dates Report
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
11070610-001A SBA-N4 (5-6) 07/13/2011 10:00 7/15/2011 5:03:00 PM
SW-846 3550B, 8015B, Total Petroleum Hydrocarbons (OA-2) by GC/FID 07/19/2011 17:0007/19/2011 7:53
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/22/2011 12:5707/19/2011 12:30
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/25/2011 21:5607/19/2011 12:30
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD 07/20/2011 18:1907/19/2011 12:30
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS 07/20/2011 3:0507/18/2011 10:39
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS 07/19/2011 17:5807/18/2011 10:37
11070610-001B SBA-N4 (5-6) 07/13/2011 10:00 7/15/2011 5:03:00 PM
EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00
Standard Methods 18th Ed. 2540 G 07/18/2011 8:30
SW-846 3050B, 6010B, Metals by ICP 07/19/2011 12:2107/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/20/2011 15:0107/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 10:4507/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 11:5307/26/2011 15:38
SW-846 3050B, 6010B, Metals by ICP 07/28/2011 12:5407/27/2011 15:52
SW-846 3050B, Metals by GFAA 07/20/2011 8:2907/18/2011 15:07
SW-846 3050B, Metals by GFAA 07/28/2011 9:0907/18/2011 15:07
SW-846 7471A 07/19/2011 12:2507/18/2011 11:31
SW-846 9012A (Total) 07/19/2011 10:2607/18/2011 19:10
11070610-001C SBA-N4 (5-6) 07/13/2011 10:00 7/15/2011 5:03:00 PM
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/22/2011 21:06
11070610-001F SBA-N4 (5-6) 07/13/2011 10:00 7/15/2011 5:03:00 PM
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS 07/20/2011 16:46
11070610-002A SBA-K2 (4-5) 07/13/2011 11:30 7/15/2011 5:03:00 PM
SW-846 3550B, 8015B, Total Petroleum Hydrocarbons (OA-2) by GC/FID 07/19/2011 16:0607/19/2011 7:53
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/21/2011 21:4507/19/2011 12:30
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/25/2011 22:2207/19/2011 12:30
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD 07/20/2011 18:3607/19/2011 12:30
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS 07/20/2011 3:4107/18/2011 10:39
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS 07/19/2011 10:2507/18/2011 10:37
11070610-002B SBA-K2 (4-5) 07/13/2011 11:30 7/15/2011 5:03:00 PM
EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00
Standard Methods 18th Ed. 2540 G 07/18/2011 8:30
SW-846 3050B, 6010B, Metals by ICP 07/19/2011 12:3807/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/20/2011 15:1807/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 11:5807/26/2011 15:38
SW-846 3050B, Metals by GFAA 07/19/2011 9:4707/18/2011 15:07
Page 60 of 104
Analysis Date/TimeTest Name Prep Date/Time
____TeklabHdrP
Sample ID Client Sample ID Collection Date Received Date
Dates Report
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3050B, Metals by GFAA 07/28/2011 9:1907/18/2011 15:07
SW-846 7471A 07/19/2011 12:2507/18/2011 11:31
SW-846 9012A (Total) 07/19/2011 10:2607/18/2011 19:10
11070610-002C SBA-K2 (4-5) 07/13/2011 11:30 7/15/2011 5:03:00 PM
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/22/2011 21:53
11070610-002F SBA-K2 (4-5) 07/13/2011 11:30 7/15/2011 5:03:00 PM
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS 07/20/2011 17:16
11070610-003A SBA-J5 (5-6) 07/13/2011 13:15 7/15/2011 5:03:00 PM
SW-846 3550B, 8015B, Total Petroleum Hydrocarbons (OA-2) by GC/FID 07/19/2011 16:4207/19/2011 7:53
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/21/2011 22:1107/19/2011 12:30
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/25/2011 22:4807/19/2011 12:30
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD 07/20/2011 18:5407/19/2011 12:30
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS 07/21/2011 6:0207/18/2011 10:39
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS 07/19/2011 10:5707/18/2011 10:37
11070610-003B SBA-J5 (5-6) 07/13/2011 13:15 7/15/2011 5:03:00 PM
EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00
Standard Methods 18th Ed. 2540 G 07/18/2011 8:30
SW-846 3050B, 6010B, Metals by ICP 07/19/2011 12:4407/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/20/2011 15:3407/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 12:1607/26/2011 15:38
SW-846 3050B, Metals by GFAA 07/19/2011 9:5007/18/2011 15:07
SW-846 3050B, Metals by GFAA 07/28/2011 9:2207/18/2011 15:07
SW-846 7471A 07/19/2011 12:2507/18/2011 11:31
SW-846 9012A (Total) 07/19/2011 10:2607/18/2011 19:10
11070610-003C SBA-J5 (5-6) 07/13/2011 13:15 7/15/2011 5:03:00 PM
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/22/2011 22:41
11070610-003F SBA-J5 (5-6) 07/13/2011 13:15 7/15/2011 5:03:00 PM
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS 07/20/2011 17:46
11070610-004A SBA-H3 (5-6) 07/13/2011 14:30 7/15/2011 5:03:00 PM
SW-846 3550B, 8015B, Total Petroleum Hydrocarbons (OA-2) by GC/FID 07/19/2011 17:1907/19/2011 7:53
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/22/2011 14:1507/19/2011 12:30
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/25/2011 23:1407/19/2011 12:30
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD 07/20/2011 19:1107/19/2011 12:30
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS 07/20/2011 6:4207/18/2011 10:39
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS 07/20/2011 11:1407/18/2011 10:37
11070610-004B SBA-H3 (5-6) 07/13/2011 14:30 7/15/2011 5:03:00 PM
EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00
Page 61 of 104
Analysis Date/TimeTest Name Prep Date/Time
____TeklabHdrP
Sample ID Client Sample ID Collection Date Received Date
Dates Report
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Standard Methods 18th Ed. 2540 G 07/18/2011 8:30
SW-846 3050B, 6010B, Metals by ICP 07/19/2011 13:0007/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/20/2011 15:4007/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 12:2207/26/2011 15:38
SW-846 3050B, Metals by GFAA 07/19/2011 9:5407/18/2011 15:07
SW-846 3050B, Metals by GFAA 07/28/2011 9:2607/18/2011 15:07
SW-846 7471A 07/19/2011 12:2507/18/2011 11:31
SW-846 9012A (Total) 07/19/2011 10:2607/18/2011 19:10
11070610-004C SBA-H3 (5-6) 07/13/2011 14:30 7/15/2011 5:03:00 PM
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/22/2011 23:28
11070610-004F SBA-H3 (5-6) 07/13/2011 14:30 7/15/2011 5:03:00 PM
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS 07/21/2011 12:21
11070610-005A SBA-F2 (4-5) 07/13/2011 15:30 7/15/2011 5:03:00 PM
SW-846 3550B, 8015B, Total Petroleum Hydrocarbons (OA-2) by GC/FID 07/19/2011 17:3707/19/2011 7:53
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/22/2011 14:4107/19/2011 12:30
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/25/2011 23:4007/19/2011 12:30
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD 07/20/2011 19:2807/19/2011 12:30
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS 07/20/2011 7:1907/18/2011 10:39
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS 07/19/2011 17:2607/18/2011 10:37
11070610-005B SBA-F2 (4-5) 07/13/2011 15:30 7/15/2011 5:03:00 PM
EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00
Standard Methods 18th Ed. 2540 G 07/18/2011 8:30
SW-846 3050B, 6010B, Metals by ICP 07/19/2011 13:0607/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/20/2011 15:4607/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 12:2807/26/2011 15:38
SW-846 3050B, Metals by GFAA 07/19/2011 9:5707/18/2011 15:07
SW-846 3050B, Metals by GFAA 07/28/2011 9:2907/18/2011 15:07
SW-846 7471A 07/19/2011 12:2507/18/2011 11:31
SW-846 9012A (Total) 07/19/2011 10:2607/18/2011 19:10
11070610-005C SBA-F2 (4-5) 07/13/2011 15:30 7/15/2011 5:03:00 PM
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/23/2011 0:15
11070610-005F SBA-F2 (4-5) 07/13/2011 15:30 7/15/2011 5:03:00 PM
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS 07/21/2011 13:20
11070610-006A TSA-02 (8-9) 07/14/2011 9:45 7/15/2011 5:03:00 PM
SW-846 3550B, 8015B, Total Petroleum Hydrocarbons (OA-2) by GC/FID 07/19/2011 14:1707/19/2011 7:53
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/21/2011 23:2907/19/2011 12:30
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/26/2011 0:0607/19/2011 12:30
Page 62 of 104
Analysis Date/TimeTest Name Prep Date/Time
____TeklabHdrP
Sample ID Client Sample ID Collection Date Received Date
Dates Report
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD 07/20/2011 19:4507/19/2011 12:30
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS 07/20/2011 6:0607/18/2011 10:39
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS 07/19/2011 14:1007/18/2011 10:37
11070610-006B TSA-02 (8-9) 07/14/2011 9:45 7/15/2011 5:03:00 PM
EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00
Standard Methods 18th Ed. 2540 G 07/18/2011 8:30
SW-846 3050B, 6010B, Metals by ICP 07/19/2011 13:1207/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/20/2011 15:5207/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 12:3307/26/2011 15:38
SW-846 3050B, Metals by GFAA 07/19/2011 10:0107/18/2011 15:07
SW-846 3050B, Metals by GFAA 07/28/2011 9:3307/18/2011 15:07
SW-846 7471A 07/19/2011 12:2507/18/2011 11:31
SW-846 9012A (Total) 07/19/2011 10:2607/18/2011 19:10
11070610-006C TSA-02 (8-9) 07/14/2011 9:45 7/15/2011 5:03:00 PM
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/23/2011 1:02
11070610-006F TSA-02 (8-9) 07/14/2011 9:45 7/15/2011 5:03:00 PM
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS 07/21/2011 13:49
11070610-007A TSA-01 (5-6) 07/14/2011 10:30 7/15/2011 5:03:00 PM
SW-846 3550B, 8015B, Total Petroleum Hydrocarbons (OA-2) by GC/FID 07/19/2011 15:1107/19/2011 7:53
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/21/2011 23:5507/19/2011 12:30
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/26/2011 0:3107/19/2011 12:30
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD 07/20/2011 10:3407/19/2011 12:30
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS 07/21/2011 4:4707/18/2011 10:39
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS 07/19/2011 14:4307/18/2011 10:37
11070610-007B TSA-01 (5-6) 07/14/2011 10:30 7/15/2011 5:03:00 PM
EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00
Standard Methods 18th Ed. 2540 G 07/18/2011 8:30
SW-846 3050B, 6010B, Metals by ICP 07/19/2011 13:1807/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/20/2011 15:5707/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/21/2011 13:1207/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 12:3907/26/2011 15:38
SW-846 3050B, Metals by GFAA 07/19/2011 10:0407/18/2011 15:07
SW-846 3050B, Metals by GFAA 07/28/2011 9:5707/18/2011 15:07
SW-846 7471A 07/19/2011 12:2507/18/2011 11:31
SW-846 9012A (Total) 07/19/2011 10:2607/18/2011 19:10
11070610-007C TSA-01 (5-6) 07/14/2011 10:30 7/15/2011 5:03:00 PM
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/23/2011 1:50
Page 63 of 104
Analysis Date/TimeTest Name Prep Date/Time
____TeklabHdrP
Sample ID Client Sample ID Collection Date Received Date
Dates Report
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
11070610-007F TSA-01 (5-6) 07/14/2011 10:30 7/15/2011 5:03:00 PM
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS 07/21/2011 14:19
11070610-008A TSA-03 (3-4) 07/14/2011 11:15 7/15/2011 5:03:00 PM
SW-846 3550B, 8015B, Total Petroleum Hydrocarbons (OA-2) by GC/FID 07/19/2011 15:2907/19/2011 7:53
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/22/2011 0:2107/19/2011 12:30
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/26/2011 0:5707/19/2011 12:30
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD 07/20/2011 20:0207/19/2011 12:30
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS 07/21/2011 5:2507/18/2011 10:39
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS 07/19/2011 15:1507/18/2011 10:37
11070610-008B TSA-03 (3-4) 07/14/2011 11:15 7/15/2011 5:03:00 PM
EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00
Standard Methods 18th Ed. 2540 G 07/18/2011 8:30
SW-846 3050B, 6010B, Metals by ICP 07/19/2011 13:2307/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/20/2011 16:0307/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/21/2011 10:4507/18/2011 14:17
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 12:4507/26/2011 15:38
SW-846 3050B, Metals by GFAA 07/20/2011 9:4007/18/2011 15:07
SW-846 3050B, Metals by GFAA 07/28/2011 9:4607/18/2011 15:07
SW-846 7471A 07/19/2011 12:2507/18/2011 11:31
SW-846 9012A (Total) 07/20/2011 7:2407/19/2011 14:00
11070610-008C TSA-03 (3-4) 07/14/2011 11:15 7/15/2011 5:03:00 PM
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/23/2011 2:37
11070610-008F TSA-03 (3-4) 07/14/2011 11:15 7/15/2011 5:03:00 PM
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS 07/21/2011 0:30
11070610-009A TSA-04 (4-5) 07/14/2011 12:00 7/15/2011 5:03:00 PM
SW-846 3550B, 8015B, Total Petroleum Hydrocarbons (OA-2) by GC/FID 07/19/2011 16:2407/19/2011 7:53
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/22/2011 1:3907/19/2011 12:30
SW-846 3550B, 8081B, Chlorinated Pesticides by GC/ECD 07/26/2011 2:1507/19/2011 12:30
SW-846 3550B, 8082, PolyChlorinated Biphenyls (PCBs) by GC/ECD 07/20/2011 20:2007/19/2011 12:30
SW-846 3550B, 8270C SIMS, Semi-Volatile Organic Compounds by GC/MS 07/21/2011 1:5207/18/2011 10:39
SW-846 3550B, 8270C, Semi-Volatile Organic Compounds by GC/MS 07/19/2011 15:4807/18/2011 10:37
11070610-009B TSA-04 (4-5) 07/14/2011 12:00 7/15/2011 5:03:00 PM
EPA SW846 3550C, 5035A, ASTM D2974 07/18/2011 10:00
Standard Methods 18th Ed. 2540 G 07/18/2011 8:30
SW-846 3050B, 6010B, Metals by ICP 07/19/2011 13:2907/18/2011 14:22
SW-846 3050B, 6010B, Metals by ICP 07/20/2011 16:0907/18/2011 14:22
SW-846 3050B, 6010B, Metals by ICP 07/21/2011 10:5107/18/2011 14:22
Page 64 of 104
Analysis Date/TimeTest Name Prep Date/Time
____TeklabHdrP
Sample ID Client Sample ID Collection Date Received Date
Dates Report
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 23:5307/26/2011 15:38
SW-846 3050B, Metals by GFAA 07/20/2011 8:4307/18/2011 15:07
SW-846 3050B, Metals by GFAA 07/28/2011 9:5007/18/2011 15:07
SW-846 7471A 07/19/2011 12:2507/18/2011 11:31
SW-846 9012A (Total) 07/20/2011 7:2407/19/2011 14:00
11070610-009C TSA-04 (4-5) 07/14/2011 12:00 7/15/2011 5:03:00 PM
SW-846 8151A, Chlorinated Herbicides by GC/ECD 07/23/2011 3:24
11070610-009F TSA-04 (4-5) 07/14/2011 12:00 7/15/2011 5:03:00 PM
SW-846 5035, 8260B, Volatile Organic Compounds by GC/MS 07/21/2011 14:49
Page 65 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
STANDARD METHODS 18TH ED. 2540 G
SampID: LCS-R152054
SampType: LCS %UnitsR152054Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Total Solids 07/18/20110.1 1.01.0 99.00 90 110
SampID: LCSQC-R152054
SampType: LCSQC %UnitsR152054Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Total Solids 07/18/20110.1 1.01.0 99.00 90 110
SampID: 11070610-004BDUP
SampType: DUP %UnitsR152054Batch RPD Limit 15
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Total Solids 07/18/20110.1 82.6 0.0882.71
SW-846 9012A (TOTAL)
SampID: MB-69687
SampType: MBLK mg/KgUnits69687Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Cyanide 07/20/20110.25 < 0.25
SampID: LCS-69687
SampType: LCS mg/KgUnits69687Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Cyanide 07/20/20110.25 1.251.20 96.30 85 115
SampID: 11070610-001BMS
SampType: MS mg/Kg-dryUnits69687Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Cyanide 07/19/20110.33 1.641.71 104.40 75 125
SampID: 11070610-001BMSD
SampType: MSD mg/Kg-dryUnits69687Batch RPD Limit 15
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Cyanide 07/19/20110.33 1.641.52 92.7 11.870 1.712
SampID: MB-R152186
SampType: MBLK mg/KgUnits69730Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Cyanide J 07/20/20110.25 0.11
Page 66 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 9012A (TOTAL)
SampID: LCS-R152186
SampType: LCS mg/KgUnits69730Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Cyanide 07/20/20110.25 1.251.33 106.70 85 115
SW-846 3050B, 6010B, METALS BY ICP
SampID: MB-69636
SampType: MBLK mg/Kg-dryUnits69636Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Aluminum 07/19/20115.00 5.00< 5.00 00 -100 100
Arsenic 07/19/20112.50 2.50< 2.50 00 -100 100
Barium 07/20/20110.50 0.50< 0.50 00 -100 100
Beryllium 07/19/20110.10 0.10< 0.10 00 -100 100
Cadmium 07/19/20110.20 0.20< 0.20 00 -100 100
Calcium 07/19/20115.00 5.00< 5.00 00 -100 100
Chromium 07/19/20111.00 1.00< 1.00 00 -100 100
Cobalt 07/19/20111.00 1.00< 1.00 00 -100 100
Copper 07/19/20111.00 1.00< 1.00 00 -100 100
Iron 07/19/20112.00 2.00< 2.00 00 -100 100
Lead 07/19/20114.00 4.00< 4.00 00 -100 100
Magnesium 07/19/20111.00 1.00< 1.00 00 -100 100
Manganese 07/19/20110.50 0.50< 0.50 00 -100 100
Nickel 07/19/20111.00 1.00< 1.00 00 -100 100
Potassium 07/20/201110.0 10.0< 10.0 00 -100 100
Silver 07/21/20110.55 0.55< 0.55 00 -100 100
Silver 07/20/20110.55 0.55< 0.55 00 -100 100
Sodium 07/20/20115.00 5.00< 5.00 00 -100 100
Vanadium 07/19/20111.00 1.00< 1.00 00 -100 100
Zinc J 07/19/20111.00 1.000.51 51.00 -100 100
Page 67 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3050B, 6010B, METALS BY ICP
SampID: LCS-69636
SampType: LCS mg/Kg-dryUnits69636Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Aluminum 07/19/20115.00 200197 98.60 85 115
Arsenic 07/19/20112.50 200208 103.80 85 115
Barium 07/20/20110.50 200212 106.10 85 115
Beryllium 07/19/20110.10 5.005.08 101.60 85 115
Cadmium 07/19/20110.20 5.005.12 102.40 85 115
Calcium 07/19/20115.00 120121 101.10 85 115
Chromium 07/19/20111.00 20.019.7 98.60 85 115
Cobalt 07/19/20111.00 50.049.7 99.40 85 115
Copper 07/19/20111.00 25.024.5 98.00 85 115
Iron 07/19/20112.00 100102 102.10 85 115
Lead 07/19/20114.00 50.051.6 103.10 85 115
Magnesium 07/19/20111.00 75.079.2 105.60 85 115
Manganese 07/19/20110.50 50.053.5 107.00 85 115
Nickel 07/19/20111.00 50.051.6 103.10 85 115
Potassium 07/20/201110.0 120133 110.80 85 115
Silver 07/21/20110.55 5.004.83 96.60 85 115
Silver 07/20/20110.55 5.005.37 107.40 85 115
Sodium 07/20/20115.00 120131 109.00 85 115
Vanadium 07/19/20111.00 50.045.8 91.70 85 115
Zinc 07/19/20111.00 50.053.0 106.00 85 115
SampID: 11070610-001BMS
SampType: MS mg/Kg-dryUnits69636Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Aluminum S 07/19/20114.90 19618900 425.018100 75 125
Arsenic 07/19/20112.45 196194 94.19.265 75 125
Barium 07/20/20110.49 196296 80.1138.8 75 125
Beryllium 07/19/20110.10 4.905.18 91.60.6863 75 125
Cadmium 07/19/20110.20 4.904.53 83.80.4216 75 125
Chromium 07/20/20110.98 19.639.0 75.624.19 75 125
Cobalt 07/19/20110.98 49.047.9 77.010.21 75 125
Iron S 07/19/20111.96 98.020400 -655026780 75 125
Lead 07/19/20113.92 49.058.8 81.818.72 75 125
Magnesium S 07/19/20110.98 73.514700 149313630 75 125
Manganese S 07/19/20110.49 49.0734 -53.2760.5 75 125
Nickel 07/20/20110.98 49.060.0 83.219.25 75 125
Potassium S 07/20/20119.80 1182550 272.52229 75 125
Silver 07/20/20110.54 4.904.27 87.20 75 125
Sodium 07/20/20114.90 118361 89.2256.1 75 125
Vanadium 07/20/20110.98 49.077.2 91.932.15 75 125
Zinc 07/27/20110.98 49.0120 91.175.05 75 125
Page 68 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3050B, 6010B, METALS BY ICP
SampID: 11070610-001BMSD
SampType: MSD mg/Kg-dryUnits69636Batch RPD Limit 20
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Aluminum S 07/19/20114.90 19619900 920.0 5.0018100 18930
Arsenic 07/19/20112.45 196204 99.3 5.139.265 193.8
Barium 07/20/20110.49 196298 81.4 0.86138.8 295.9
Beryllium 07/19/20110.10 4.905.45 97.2 5.170.6863 5.176
Cadmium 07/19/20110.20 4.904.79 89.2 5.680.4216 4.529
Chromium 07/20/20110.98 19.643.3 97.7 10.5524.19 39.00
Cobalt 07/19/20110.98 49.051.2 83.6 6.5910.21 47.94
Iron S 07/19/20111.96 98.021900 -4940 7.4626780 20360
Lead 07/19/20113.92 49.061.7 87.7 4.8018.72 58.80
Magnesium S 07/19/20110.98 73.516100 3320 8.7213630 14730
Manganese S 07/19/20110.49 49.0652 -220.6 11.83760.5 734.4
Nickel 07/20/20110.98 49.062.9 89.0 4.6419.25 60.04
Potassium S 07/20/20119.80 1182580 295.8 1.072229 2550
Silver 07/20/20110.54 4.904.01 81.8 6.390 4.275
Sodium 07/20/20114.90 118387 111.2 6.92256.1 361.0
Vanadium 07/20/20110.98 49.084.7 107.1 9.1932.15 77.22
Zinc 07/27/20110.98 49.0114 79.3 4.9575.05 119.7
SampID: 11070610-009BMS
SampType: MS mg/Kg-dryUnits69636Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Barium 07/20/20110.46 185319 92.5147.8 75 125
Potassium S 07/20/20119.26 1113010 332.52638 75 125
Silver 07/21/20110.51 4.634.31 93.00 75 125
Sodium 07/20/20114.63 111195 120.660.81 75 125
Vanadium 07/20/20110.93 46.385.8 101.038.99 75 125
SampID: 11070610-009BMSD
SampType: MSD mg/Kg-dryUnits69636Batch RPD Limit 20
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Barium 07/20/20110.46 185326 96.0 2.04147.8 319.1
Potassium S 07/20/20119.26 1113040 365.0 1.192638 3007
Silver 07/21/20110.51 4.634.33 93.6 0.640 4.306
Sodium 07/20/20114.63 111198 123.8 1.8460.81 194.8
Vanadium 07/20/20110.93 46.387.2 104.1 1.6238.99 85.77
SampID: MB-69908
SampType: MBLK mg/Kg-dryUnits69908Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Antimony 07/27/20115.00 5.00< 5.00 00 -100 100
Page 69 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3050B, 6010B, METALS BY ICP
SampID: LCS-69908
SampType: LCS mg/Kg-dryUnits69908Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Antimony 07/27/20115.00 50.051.8 103.70 85 115
SampID: 11070610-002BMS
SampType: MS mg/Kg-dryUnits69908Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Antimony 07/27/20115.00 50.047.8 95.60 75 125
SampID: 11070610-002BMSD
SampType: MSD mg/Kg-dryUnits69908Batch RPD Limit 20
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Antimony 07/27/20115.00 50.048.8 97.5 1.970 47.82
SampID: MB-69954
SampType: MBLK mg/Kg-dryUnits69954Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Aluminum 07/28/20115.00 5.00< 5.00 00 -100 100
Calcium 07/28/20115.00 5.00< 5.00 00 -100 100
Chromium 07/28/20111.00 1.00< 1.00 00 -100 100
Copper 07/28/20111.00 1.00< 1.00 00 -100 100
Iron 07/28/20112.00 2.00< 2.00 00 -100 100
Manganese 07/28/20110.50 0.50< 0.50 00 -100 100
Potassium 07/28/201110.0 10.0< 10.0 00 -100 100
SampID: LCS-69954
SampType: LCS mg/Kg-dryUnits69954Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Aluminum 07/28/20115.00 200191 95.30 85 115
Calcium 07/28/20115.00 120117 97.60 85 115
Chromium 07/28/20111.00 20.019.6 98.00 85 115
Copper 07/28/20111.00 25.024.0 95.80 85 115
Iron 07/28/20112.00 10095.5 95.50 85 115
Manganese 07/28/20110.50 50.047.8 95.50 85 115
Potassium 07/28/201110.0 120117 97.60 85 115
SampID: 11070610-001BMS
SampType: MS mg/Kg-dryUnits69954Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Calcium S 07/28/20114.72 11344200 165842280 75 125
Copper 07/28/20110.94 23.638.0 95.615.41 75 125
Page 70 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3050B, 6010B, METALS BY ICP
SampID: 11070610-001BMSD
SampType: MSD mg/Kg-dryUnits69954Batch RPD Limit 20
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Calcium S 07/28/20114.72 11338300 -3550 14.3142280 44160
Copper 07/28/20110.94 23.636.7 90.2 3.4415.41 37.95
SampID: 11070610-009BMS
SampType: MS mg/Kg-dryUnitsR152096Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Aluminum S 07/19/20114.63 18523400 144520750 75 125
Arsenic 07/19/20112.31 185189 97.68.704 75 125
Beryllium 07/19/20110.09 4.635.37 98.40.8148 75 125
Cadmium 07/19/20110.19 4.634.60 91.60.3611 75 125
Calcium S 07/19/20114.63 1116580 74.26495 75 125
Chromium 07/19/20110.93 18.538.7 94.221.28 75 125
Cobalt 07/19/20110.93 46.350.8 84.411.69 75 125
Copper 07/19/20110.93 23.237.3 89.416.63 75 125
Iron S 07/19/20111.85 92.624600 190.024440 75 125
Lead 07/19/20113.70 46.358.6 88.117.81 75 125
Magnesium S 07/19/20110.93 69.44250 328.04024 75 125
Manganese S 07/19/20110.46 46.3805 -94.4849.1 75 125
Nickel 07/19/20110.93 46.360.8 92.118.12 75 125
Zinc 07/19/20110.93 46.3115 102.267.40 75 125
SampID: 11070610-009BMSD
SampType: MSD mg/Kg-dryUnitsR152096Batch RPD Limit 20
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Aluminum S 07/19/20114.63 18523900 1690 1.9220750 23430
Arsenic 07/19/20112.31 185194 100.0 2.328.704 189.4
Beryllium 07/19/20110.09 4.635.46 100.4 1.710.8148 5.370
Cadmium 07/19/20110.19 4.634.80 95.8 4.140.3611 4.602
Calcium 07/19/20114.63 1116590 87.5 0.226495 6578
Chromium 07/19/20110.93 18.542.0 112.0 8.1721.28 38.72
Cobalt 07/19/20110.93 46.353.3 89.8 4.8411.69 50.75
Copper 07/19/20110.93 23.238.5 94.3 2.9816.63 37.32
Iron S 07/19/20111.85 92.625400 1040 3.1524440 24610
Lead 07/19/20113.70 46.362.5 96.6 6.4517.81 58.62
Magnesium S 07/19/20110.93 69.44330 436.0 1.754024 4252
Manganese S 07/19/20110.46 46.3856 16.0 6.15849.1 805.4
Nickel 07/19/20110.93 46.363.8 98.7 4.9018.12 60.78
Zinc 07/19/20110.93 46.3115 102.4 0.0867.40 114.7
Page 71 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3050B, METALS BY GFAA
SampID: MB-69639
SampType: MBLK mg/Kg-dryUnits69639Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Selenium 7740 07/19/20110.600 0.600< 0.600 00 -100 100
Thallium 7841 07/28/20110.200 0.200< 0.200 00 -100 100
SampID: LCS-69639
SampType: LCS mg/Kg-dryUnits69639Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Selenium 7740 07/19/20110.600 3.002.81 93.60 80 120
Thallium 7841 07/28/20110.200 1.501.45 96.40 80 120
SampID: 11070610-001BMS
SampType: MS mg/Kg-dryUnits69639Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Selenium 7740 07/20/20111.13 2.832.79 98.60 70 130
Thallium 7841 S 07/28/20110.189 1.422.12 137.90.1661 70 130
SampID: 11070610-001BMSD
SampType: MSD mg/Kg-dryUnits69639Batch RPD Limit 20
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Selenium 7740 07/20/20111.13 2.833.26 115.3 15.580 2.792
Thallium 7841 S 07/28/20110.189 1.422.08 135.2 1.830.1661 2.117
SW-846 7471A
SampID: MB-69631
SampType: MBLK mg/KgUnits69631Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Mercury 07/19/20110.010 0.010< 0.010 00 -100 100
SampID: LCS-69631
SampType: LCS mg/KgUnits69631Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Mercury 07/19/20110.010 0.2500.254 101.40 85 115
SampID: 11070610-002BMS
SampType: MS mg/Kg-dryUnits69631Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Mercury 07/19/20110.012 0.2940.396 92.80.1230 75 125
SampID: 11070610-002BMSD
SampType: MSD mg/Kg-dryUnits69631Batch RPD Limit 15
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Mercury 07/19/20110.012 0.2940.391 91.2 1.200.1230 0.3960
Page 72 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3550B, 8015B, TOTAL PETROLEUM HYDROCARBONS (OA-2) BY GC/FID
SampID: MB-69637
SampType: MBLK mg/KgUnits69637Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Diesel 07/19/20115.00 NDKerosene 07/19/20115.00 NDMineral Spirits 07/19/20115.00 NDMotor Oil 07/19/20115.00 ND Surr: n-Tetracontane 07/19/20110.670.52 77.9 54.8 128
SampID: LCS-69637
SampType: LCS mg/KgUnits69637Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Diesel 07/19/20115.00 16.717.7 105.90 40.4 121
Surr: n-Tetracontane 07/19/20110.670.58 87.0 54.8 128
SampID: 11070610-006AMS
SampType: MS mg/Kg-dryUnits69637Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Diesel 07/19/20116.13 20.523.0 112.40 20.3 167
Surr: n-Tetracontane 07/19/20110.820.85 103.3 53.9 153
SampID: 11070610-006AMSD
SampType: MSD mg/Kg-dryUnits69637Batch RPD Limit 34
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Diesel 07/19/20116.13 20.524.5 119.7 6.380 23.01
Surr: n-Tetracontane 07/19/20110.820.84 102.3
Page 73 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD
SampID: MB-69671
SampType: MBLK µg/KgUnits69671Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
4,4´-DDD 07/21/20111.67 ND4,4´-DDE 07/21/20111.67 ND4,4´-DDT 07/21/20111.67 NDAlachlor 07/21/20111.67 NDAldrin 07/21/20111.67 NDalpha-BHC 07/21/20111.67 NDalpha-Chlordane 07/21/20111.67 NDbeta-BHC 07/21/20111.67 NDChlordane 07/21/20113.34 NDdelta-BHC 07/21/20111.67 NDDieldrin 07/21/20111.67 NDEndosulfan I 07/21/20111.67 NDEndosulfan II 07/21/20111.67 NDEndosulfan sulfate 07/21/20111.67 NDEndrin 07/21/20111.67 NDEndrin aldehyde 07/21/20111.67 NDEndrin ketone 07/21/20111.67 NDgamma-BHC 07/21/20111.67 NDgamma-Chlordane 07/21/20111.67 NDHeptachlor 07/21/20111.67 NDHeptachlor epoxide 07/21/20111.67 NDMethoxychlor 07/21/20111.67 NDToxaphene 07/21/201130.0 ND Surr: Decachlorobiphenyl 07/21/20118.337.79 93.6 73.5 150
Surr: Tetrachloro-m-xylene 07/21/20118.335.12 61.5 14.4 113
Page 74 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD
SampID: LCSPST-69671
SampType: LCS µg/KgUnits69671Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
4,4´-DDD 07/21/20111.67 8.337.96 95.50 36 208
4,4´-DDE 07/21/20111.67 8.337.70 92.40 26 191
4,4´-DDT 07/21/20111.67 8.338.48 101.90 3 215
Alachlor 07/21/20111.67 8.335.23 62.80 30 170
Aldrin 07/21/20111.67 8.335.94 71.30 46 173
alpha-BHC 07/21/20111.67 8.336.46 77.50 37 179
alpha-Chlordane 07/21/20111.67 8.337.44 89.30 38 187
beta-BHC 07/21/20111.67 8.336.85 82.20 51 185
delta-BHC 07/21/20111.67 8.337.88 94.60 46 166
Dieldrin 07/21/20111.67 8.337.35 88.30 26 216
Endosulfan I 07/21/20111.67 8.337.35 88.30 31 205
Endosulfan II 07/21/20111.67 8.337.96 95.50 42 187
Endosulfan sulfate 07/21/20111.67 8.338.22 98.70 29 230
Endrin 07/21/20111.67 8.337.63 91.60 30 215
Endrin aldehyde 07/21/20111.67 8.338.03 96.40 42 202
Endrin ketone 07/21/20111.67 8.339.00 108.00 19 244
gamma-BHC 07/21/20111.67 8.336.02 72.20 55 166
gamma-Chlordane 07/21/20111.67 8.337.21 86.50 23 186
Heptachlor 07/21/20111.67 8.336.15 73.80 43 172
Heptachlor epoxide 07/21/20111.67 8.336.85 82.30 39 204
Methoxychlor 07/21/20111.67 8.338.79 105.50 3 221
Surr: Decachlorobiphenyl 07/21/20118.338.53 102.4 50.4 176
Surr: Tetrachloro-m-xylene 07/21/20118.334.53 54.3 10 107
Page 75 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD
SampID: 11070610-008AMS
SampType: MS µg/Kg-dryUnits69671Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
4,4´-DDD J 07/26/201120.5 10.28.6 84.00 36 208
4,4´-DDE J 07/26/201120.5 10.29.3 91.10 26 191
4,4´-DDT J 07/26/201120.5 10.29.4 92.10 3 215
Alachlor 07/22/20112.05 10.27.15 70.00 30 170
Aldrin 07/22/20112.05 10.27.95 77.80 46 173
alpha-BHC 07/22/20112.05 10.28.44 82.60 37 179
alpha-Chlordane 07/22/20112.05 10.29.38 91.80 38 187
beta-BHC 07/22/20112.05 10.28.70 85.20 51 185
delta-BHC 07/22/20112.05 10.210.1 99.00 46 166
Dieldrin 07/22/20112.05 10.211.2 89.62.090 26 216
Endosulfan I 07/22/20112.05 10.29.10 89.00 31 205
Endosulfan II 07/22/20112.05 10.29.17 89.80 42 187
Endosulfan sulfate 07/22/20112.05 10.29.04 88.50 29 230
Endrin 07/22/20112.05 10.29.26 90.60 30 215
Endrin aldehyde 07/22/20112.05 10.29.43 92.30 42 202
Endrin ketone 07/22/20112.05 10.210.6 104.20 19 244
gamma-BHC 07/22/20112.05 10.28.07 79.00 55 166
gamma-Chlordane 07/22/20112.05 10.210.1 99.30 23 186
Heptachlor 07/22/20112.05 10.28.43 82.60 43 172
Heptachlor epoxide 07/22/20112.05 10.212.3 92.92.853 39 204
Methoxychlor 07/22/20112.05 10.29.61 94.10 3 221
Surr: Decachlorobiphenyl 07/22/201110.210.2 99.7 48 149
Surr: Tetrachloro-m-xylene 07/22/201110.26.06 59.3 19 145
Page 76 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3550B, 8081B, CHLORINATED PESTICIDES BY GC/ECD
SampID: 11070610-008AMSD
SampType: MSD µg/Kg-dryUnits69671Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
4,4´-DDD J 07/26/201120.5 10.29.0 87.9 0.000 8.586
4,4´-DDE J 07/26/201120.5 10.210 97.7 0.000 9.310
4,4´-DDT J 07/26/201120.5 10.29.9 96.7 0.000 9.412
Alachlor 07/22/20112.05 10.27.03 68.8 1.720 7.150
Aldrin 07/22/20112.05 10.28.02 78.5 0.940 7.949
alpha-BHC 07/22/20112.05 10.28.31 81.3 1.660 8.445
alpha-Chlordane 07/22/20112.05 10.29.60 94.0 2.380 9.378
beta-BHC 07/22/20112.05 10.28.97 87.8 3.050 8.704
delta-BHC 07/22/20112.05 10.210.5 102.5 3.540 10.11
Dieldrin 07/22/20112.05 10.211.5 91.7 1.932.090 11.24
Endosulfan I 07/22/20112.05 10.29.08 88.8 0.240 9.097
Endosulfan II 07/22/20112.05 10.29.52 93.2 3.720 9.175
Endosulfan sulfate 07/22/20112.05 10.29.49 92.9 4.790 9.044
Endrin 07/22/20112.05 10.29.52 93.2 2.770 9.262
Endrin aldehyde 07/22/20112.05 10.29.70 94.9 2.830 9.428
Endrin ketone 07/22/20112.05 10.211.0 107.2 2.930 10.64
gamma-BHC 07/22/20112.05 10.28.11 79.3 0.480 8.067
gamma-Chlordane 07/22/20112.05 10.210.6 103.5 4.180 10.14
Heptachlor 07/22/20112.05 10.28.60 84.2 1.940 8.435
Heptachlor epoxide 07/22/20112.05 10.212.7 96.0 2.532.853 12.34
Methoxychlor 07/22/20112.05 10.29.88 96.7 2.750 9.610
Surr: Decachlorobiphenyl 07/22/201110.210.0 98.1
Surr: Tetrachloro-m-xylene 07/22/201110.25.44 53.2
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECD
SampID: MB-69671
SampType: MBLK µg/KgUnits69671Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Aroclor 1016 07/20/201137.5 NDAroclor 1221 07/20/201137.5 NDAroclor 1232 07/20/201137.5 NDAroclor 1242 07/20/201137.5 NDAroclor 1248 07/20/201137.5 NDAroclor 1254 07/20/201137.5 NDAroclor 1260 07/20/201137.5 ND Surr: Decachlorobiphenyl 07/20/20118.37.3 88.5 86.4 159
Surr: Tetrachloro-meta-xylene 07/20/20118.35.0 59.8 31.6 114
SampID: LCSPCB-69671
SampType: LCS µg/KgUnits69671Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Aroclor 1016 07/20/201137.5 167133 80.00 54.9 121
Aroclor 1260 07/20/201137.5 167156 93.50 65.5 133
Surr: Decachlorobiphenyl 07/20/20118.38.1 97.8 86.4 159
Surr: Tetrachloro-meta-xylene 07/20/20118.34.9 58.6 31.6 114
Page 77 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3550B, 8082, POLYCHLORINATED BIPHENYLS (PCBS) BY GC/ECD
SampID: 11070610-007AMS
SampType: MS µg/Kg-dryUnits69671Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Aroclor 1016 07/20/201145.5 202160 79.30 35.8 143
Aroclor 1260 07/20/201145.5 202180 88.90 22.3 152
Surr: Decachlorobiphenyl 07/20/201110.19.1 90.0 5 156
Surr: Tetrachloro-meta-xylene 07/20/201110.15.9 58.4 7.35 123
SampID: 11070610-007AMSD
SampType: MSD µg/Kg-dryUnits69671Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Aroclor 1016 07/20/201145.5 202167 82.6 4.120 160.4
Aroclor 1260 07/20/201145.5 202187 92.7 4.080 180.0
Surr: Decachlorobiphenyl 07/20/201110.19.0 89.0
Surr: Tetrachloro-meta-xylene 07/20/201110.15.8 57.9
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MB-69628
SampType: MBLK mg/KgUnits69628Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Acenaphthene 07/18/20110.003 NDAcenaphthylene 07/18/20110.003 NDAnthracene 07/18/20110.003 NDBenzo(a)anthracene 07/18/20110.003 NDBenzo(a)pyrene 07/18/20110.003 NDBenzo(b)fluoranthene 07/18/20110.003 NDBenzo(g,h,i)perylene 07/18/20110.003 NDBenzo(k)fluoranthene 07/18/20110.003 NDChrysene 07/18/20110.003 NDDibenzo(a,h)anthracene 07/18/20110.003 NDFluoranthene 07/18/20110.003 NDFluorene 07/18/20110.003 NDIndeno(1,2,3-cd)pyrene 07/18/20110.003 NDNaphthalene 07/18/20110.003 NDPhenanthrene 07/18/20110.003 NDPyrene 07/18/20110.003 ND Surr: 2-Fluorobiphenyl 07/18/20110.1670.132 78.8 45.7 89.2
Surr: Nitrobenzene-d5 07/18/20110.1670.091 54.7 31.4 100
Surr: p-Terphenyl-d14 07/18/20110.1670.132 78.8 53.3 124
Page 78 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCS-69628
SampType: LCS mg/KgUnits69628Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Acenaphthene 07/18/20110.003 0.1670.143 85.40 56.3 115
Acenaphthylene 07/18/20110.003 0.1670.148 88.40 60.3 143
Anthracene 07/18/20110.003 0.1670.139 83.40 52.1 109
Benzo(a)anthracene 07/18/20110.003 0.1670.143 85.60 52.8 112
Benzo(a)pyrene 07/18/20110.003 0.1670.124 74.10 40.8 127
Benzo(b)fluoranthene 07/18/20110.003 0.1670.163 97.40 50.1 150
Benzo(g,h,i)perylene 07/18/20110.003 0.1670.166 99.40 52.8 145
Benzo(k)fluoranthene 07/18/20110.003 0.1670.157 93.80 52 153
Chrysene 07/18/20110.003 0.1670.149 89.20 60.8 128
Dibenzo(a,h)anthracene 07/18/20110.003 0.1670.171 102.60 54.9 150
Fluoranthene 07/18/20110.003 0.1670.153 91.80 58.7 125
Fluorene 07/18/20110.003 0.1670.164 98.40 57.8 125
Indeno(1,2,3-cd)pyrene 07/18/20110.003 0.1670.170 102.00 52 147
Naphthalene 07/18/20110.003 0.1670.134 80.00 54.8 113
Phenanthrene 07/18/20110.003 0.1670.145 86.80 60.4 121
Pyrene 07/18/20110.003 0.1670.153 91.60 57.9 129
Surr: 2-Fluorobiphenyl 07/18/20110.1670.115 68.9 45.7 89.2
Surr: Nitrobenzene-d5 07/18/20110.1670.086 51.7 31.4 100
Surr: p-Terphenyl-d14 07/18/20110.1670.136 81.4 53.3 124
SampID: 11070610-002AMS
SampType: MS mg/Kg-dryUnits69628Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Acenaphthene 07/20/20110.004 0.1990.174 87.40 36 135
Acenaphthylene 07/20/20110.004 0.1990.175 88.20 17.2 167
Anthracene 07/20/20110.004 0.1990.169 85.20 39.3 124
Benzo(a)anthracene 07/20/20110.004 0.1990.177 80.80.01667 10 183
Benzo(a)pyrene 07/20/20110.004 0.1990.166 76.60.01429 10 204
Benzo(b)fluoranthene 07/20/20110.004 0.1990.207 92.80.02223 10.6 178
Benzo(g,h,i)perylene 07/20/20110.004 0.1990.126 60.10.006748 10 168
Benzo(k)fluoranthene 07/20/20110.004 0.1990.206 99.40.008733 27.6 181
Bis(2-ethylhexyl)phthalate 07/20/20110.080 0.1990.220 88.00.04565 50 150
Chrysene 07/20/20110.004 0.1990.190 87.00.01707 10 176
Dibenzo(a,h)anthracene 07/20/20110.004 0.1990.148 74.50 12.2 156
Fluoranthene 07/20/20110.004 0.1990.197 82.60.03255 10 227
Fluorene 07/20/20110.004 0.1990.174 87.40 35.2 148
Indeno(1,2,3-cd)pyrene 07/20/20110.004 0.1990.146 70.50.006351 10 164
Naphthalene 07/20/20110.004 0.1990.155 78.20 14.7 128
Phenanthrene 07/20/20110.004 0.1990.178 82.00.01469 32.8 143
Pyrene 07/20/20110.004 0.1990.190 82.00.02739 10 180
Surr: 2-Fluorobiphenyl 07/20/20110.1990.053 26.5 10 131
Surr: Nitrobenzene-d5 07/20/20110.1990.103 51.7 10 132
Surr: p-Terphenyl-d14 07/20/20110.1990.142 71.3 30.6 131
Page 79 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3550B, 8270C SIMS, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: 11070610-002AMSD
SampType: MSD mg/Kg-dryUnits69628Batch RPD Limit 49.7
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Acenaphthene 07/21/20110.004 0.1990.163 81.8 6.570 0.1736
Acenaphthylene 07/21/20110.004 0.1990.166 83.6 5.310 0.1752
Anthracene 07/21/20110.004 0.1990.152 76.4 10.830 0.1693
Benzo(a)anthracene 07/21/20110.004 0.1990.165 74.4 7.390.01667 0.1772
Benzo(a)pyrene 07/21/20110.004 0.1990.166 76.2 0.440.01429 0.1665
Benzo(b)fluoranthene 07/21/20110.004 0.1990.189 83.8 8.990.02223 0.2065
Benzo(g,h,i)perylene R 07/21/20110.004 0.1990.185 89.8 37.990.006748 0.1261
Benzo(k)fluoranthene 07/21/20110.004 0.1990.183 87.6 12.000.008733 0.2061
Bis(2-ethylhexyl)phthalate 07/21/20110.080 0.1990.224 89.6 1.460.04565 0.2204
Chrysene 07/21/20110.004 0.1990.172 78.2 9.590.01707 0.1899
Dibenzo(a,h)anthracene 07/21/20110.004 0.1990.178 89.6 18.520 0.1479
Fluoranthene 07/21/20110.004 0.1990.188 78.4 4.290.03255 0.1966
Fluorene 07/21/20110.004 0.1990.166 83.6 4.400 0.1736
Indeno(1,2,3-cd)pyrene 07/21/20110.004 0.1990.184 89.4 22.840.006351 0.1463
Naphthalene 07/21/20110.004 0.1990.149 74.9 4.400 0.1554
Phenanthrene 07/21/20110.004 0.1990.167 76.4 6.420.01469 0.1776
Pyrene 07/21/20110.004 0.1990.188 80.6 1.440.02739 0.1903
Surr: 2-Fluorobiphenyl 07/21/20110.1990.058 29.1
Surr: Nitrobenzene-d5 07/21/20110.1990.101 50.7
Surr: p-Terphenyl-d14 07/21/20110.1990.142 71.7
Page 80 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MB-69627
SampType: MBLK mg/KgUnits69627Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1,2,4-Trichlorobenzene 07/19/20110.500 ND1,2-Dichlorobenzene 07/19/20110.500 ND1,3-Dichlorobenzene 07/19/20110.500 ND1,4-Dichlorobenzene 07/19/20110.500 ND2,4,5-Trichlorophenol 07/19/20110.350 ND2,4,6-Trichlorophenol 07/19/20110.350 ND2,4-Dichlorophenol 07/19/20110.500 ND2,4-Dimethylphenol 07/19/20110.500 ND2,4-Dinitrophenol 07/19/20111.00 ND2,4-Dinitrotoluene 07/19/20110.350 ND2,6-Dinitrotoluene 07/19/20110.350 ND2-Chloronaphthalene 07/19/20110.350 ND2-Chlorophenol 07/19/20110.500 ND2-Methoxy-4-methylphenol 07/19/20110.650 ND2-Methylnaphthalene 07/19/20110.350 ND2-Nitroaniline 07/19/20111.00 ND2-Nitrophenol 07/19/20110.350 ND3,3´-Dichlorobenzidine 07/19/20110.350 ND3-Nitroaniline 07/19/20111.00 ND4,6-Dinitro-2-methylphenol 07/19/20111.00 ND4-Bromophenyl phenyl ether 07/19/20110.350 ND4-Chloro-3-methylphenol 07/19/20110.500 ND4-Chloroaniline 07/19/20110.500 ND4-Chlorophenyl phenyl ether 07/19/20110.350 ND4-Nitroaniline 07/19/20110.500 ND4-Nitrophenol 07/19/20110.350 NDAniline 07/19/20110.500 NDAzobenzene 07/19/20110.350 NDBenzidine 07/19/20111.06 NDBenzoic acid 07/19/20111.50 NDBenzyl alcohol 07/19/20110.500 NDBis(2-chloroethoxy)methane 07/19/20110.350 NDBis(2-chloroethyl)ether 07/19/20110.500 NDBis(2-chloroisopropyl)ether 07/19/20110.350 NDButyl benzyl phthalate 07/19/20110.350 NDCarbazole 07/19/20110.500 NDDibenzofuran 07/19/20110.350 NDDiethyl phthalate 07/19/20110.500 NDDimethyl phthalate 07/19/20110.350 NDDi-n-butyl phthalate 07/19/20110.350 NDDi-n-octyl phthalate 07/19/20110.350 NDHexachlorobenzene 07/19/20110.350 NDHexachlorobutadiene 07/19/20110.500 NDHexachlorocyclopentadiene 07/19/20110.350 NDHexachloroethane 07/19/20110.500 NDIsophorone 07/19/20110.350 NDm,p-Cresol 07/19/20110.500 ND
Page 81 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MB-69627
SampType: MBLK mg/KgUnits69627Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Nitrobenzene 07/19/20110.500 NDN-Nitrosodimethylamine 07/19/20110.500 NDN-Nitroso-di-n-propylamine 07/19/20110.500 NDN-Nitrosodiphenylamine 07/19/20110.500 NDo-Cresol 07/19/20110.500 NDPentachlorophenol 07/19/20112.00 NDPhenol 07/19/20110.350 NDPyridine 07/19/20110.500 ND1,2-Diphenylhydrazine 07/19/20110.840 ND Surr: 2,4,6-Tribromophenol 07/19/20111.671.34 80.3 52.1 113
Surr: 2-Fluorobiphenyl 07/19/20110.8350.656 78.6 46.3 106
Surr: 2-Fluorophenol 07/19/20111.671.23 73.4 50.6 89
Surr: Nitrobenzene-d5 07/19/20110.8350.686 82.1 42.4 99.2
Surr: Phenol-d5 07/19/20111.671.24 74.5 55.9 98.5
Surr: p-Terphenyl-d14 07/19/20110.8350.831 99.5 45.5 115
Page 82 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCS-69627
SampType: LCS mg/KgUnits69627Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1,2,4-Trichlorobenzene 07/19/20110.500 1.671.19 71.00 43.9 92.2
1,4-Dichlorobenzene 07/19/20110.500 1.671.20 71.70 43.8 84.1
2,4,5-Trichlorophenol 07/19/20110.350 3.332.55 76.70 38.6 123
2,4,6-Trichlorophenol 07/19/20110.350 3.332.58 77.60 35.9 123
2,4-Dimethylphenol 07/19/20110.500 3.332.33 70.00 38.3 88
2,4-Dinitrophenol 07/19/20111.00 3.334.25 127.50 1.88 162
2,4-Dinitrotoluene 07/19/20110.350 1.671.64 98.30 48.6 102
2-Chlorophenol 07/19/20110.500 3.332.31 69.50 46.6 84
4-Chloro-3-methylphenol 07/19/20110.500 3.332.78 83.50 51.5 94.9
4-Nitrophenol S 07/19/20110.350 3.334.00 120.00 53.2 104
Diethyl phthalate 07/19/20110.500 3.332.84 85.40 51.7 106
Dimethyl phthalate 07/19/20110.350 3.332.58 77.40 58.8 104
Di-n-butyl phthalate 07/19/20110.350 1.671.64 98.20 54.3 105
Hexachlorobenzene 07/19/20110.350 3.332.59 77.80 55.9 106
Hexachlorobutadiene 07/19/20110.500 3.332.34 70.30 35.7 100
Hexachloroethane 07/19/20110.500 3.332.49 74.80 38.9 89.9
m,p-Cresol 07/19/20110.500 1.671.30 78.00 37.6 93.7
Nitrobenzene 07/19/20110.500 3.332.47 74.20 51.8 104
N-Nitroso-di-n-propylamine 07/19/20110.500 1.671.28 76.80 49.1 94.5
o-Cresol 07/19/20110.500 1.671.29 77.20 43 101
Pentachlorophenol 07/19/20112.00 3.332.90 87.00 42.2 102
Phenol 07/19/20110.350 3.332.37 71.20 41.6 81.3
Pyridine 07/19/20110.500 3.331.89 56.90 3.61 74.3
Surr: 2,4,6-Tribromophenol 07/19/20111.671.44 86.1 52.1 113
Surr: 2-Fluorobiphenyl 07/19/20110.8350.645 77.2 46.3 106
Surr: 2-Fluorophenol 07/19/20111.671.21 72.2 50.6 89
Surr: Nitrobenzene-d5 07/19/20110.8350.623 74.6 42.4 99.2
Surr: Phenol-d5 07/19/20111.671.24 74.0 55.9 98.5
Surr: p-Terphenyl-d14 07/19/20110.8350.809 96.9 45.5 115
Page 83 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: 11070610-003AMS
SampType: MS mg/Kg-dryUnits69627Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1,2,4-Trichlorobenzene 07/19/20110.655 2.191.49 67.90 35.9 102
1,4-Dichlorobenzene 07/19/20110.655 2.191.44 65.80 29.8 95.5
2,4,5-Trichlorophenol 07/19/20110.458 4.363.12 71.60 38.6 123
2,4,6-Trichlorophenol 07/19/20110.458 4.363.16 72.60 35.9 123
2,4-Dimethylphenol 07/19/20110.655 4.362.71 62.20 38.3 88
2,4-Dinitrophenol 07/19/20111.31 4.364.10 94.10 1.88 162
2,4-Dinitrotoluene 07/19/20110.458 2.192.07 94.50 37.5 107
2-Chlorophenol 07/19/20110.655 4.362.82 64.60 22.6 108
4-Chloro-3-methylphenol 07/19/20110.655 4.363.43 78.60 19.3 131
4-Nitrophenol 07/19/20110.458 4.364.86 111.40 27.6 123
Diethyl phthalate 07/19/20110.655 4.363.64 83.40 51.7 106
Dimethyl phthalate 07/19/20110.458 4.363.33 76.20 58.8 104
Di-n-butyl phthalate 07/19/20110.458 2.192.07 94.50 54.3 105
Hexachlorobenzene 07/19/20110.458 4.363.29 75.50 55.9 106
Hexachlorobutadiene 07/19/20110.655 4.362.88 66.10 35.7 100
Hexachloroethane 07/19/20110.655 4.362.96 67.80 38.9 89.9
m,p-Cresol 07/19/20110.655 2.191.62 73.90 37.6 93.7
Nitrobenzene 07/19/20110.655 4.363.08 70.50 51.8 104
N-Nitroso-di-n-propylamine 07/19/20110.655 2.191.63 74.70 45.5 99.1
o-Cresol 07/19/20110.655 2.191.55 70.80 43 101
Pentachlorophenol 07/19/20112.62 4.363.49 80.00 18.5 113
Phenol 07/19/20110.458 4.362.92 67.10 20.8 110
Pyridine 07/19/20110.655 4.362.27 52.10 3.61 74.3
Surr: 2,4,6-Tribromophenol 07/19/20112.191.61 73.6 32.7 130
Surr: 2-Fluorobiphenyl 07/19/20111.090.524 47.9 34.1 116
Surr: 2-Fluorophenol 07/19/20112.191.40 64.1 30.5 99
Surr: Nitrobenzene-d5 07/19/20111.090.699 63.9 34.1 101
Surr: Phenol-d5 07/19/20112.191.50 68.5 34.9 110
Surr: p-Terphenyl-d14 07/19/20111.090.971 88.8 41.7 124
Page 84 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 3550B, 8270C, SEMI-VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: 11070610-003AMSD
SampType: MSD mg/Kg-dryUnits69627Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
1,2,4-Trichlorobenzene 07/19/20110.654 2.181.61 73.7 8.050 1.486
1,4-Dichlorobenzene 07/19/20110.654 2.181.62 74.3 12.010 1.439
2,4,5-Trichlorophenol 07/19/20110.458 4.363.43 78.7 9.290 3.122
2,4,6-Trichlorophenol 07/19/20110.458 4.363.47 79.6 9.180 3.165
2,4-Dimethylphenol 07/19/20110.654 4.363.07 70.5 12.410 2.712
2,4-Dinitrophenol 07/19/20111.31 4.364.31 98.9 4.920 4.102
2,4-Dinitrotoluene 07/19/20110.458 2.182.22 101.7 7.180 2.068
2-Chlorophenol 07/19/20110.654 4.363.02 69.4 7.070 2.818
4-Chloro-3-methylphenol 07/19/20110.654 4.363.63 83.4 5.880 3.426
4-Nitrophenol 07/19/20110.458 4.365.21 119.6 6.960 4.858
Diethyl phthalate 07/19/20110.654 4.363.81 87.4 4.560 3.636
Dimethyl phthalate 07/19/20110.458 4.363.50 80.4 5.120 3.325
Di-n-butyl phthalate 07/19/20110.458 2.182.15 98.4 3.880 2.068
Hexachlorobenzene 07/19/20110.458 4.363.48 80.0 5.660 3.292
Hexachlorobutadiene 07/19/20110.654 4.363.23 74.2 11.520 2.881
Hexachloroethane 07/19/20110.654 4.363.23 74.1 8.760 2.958
m,p-Cresol 07/19/20110.654 2.181.75 80.1 8.000 1.616
Nitrobenzene 07/19/20110.654 4.363.36 77.1 8.820 3.076
N-Nitroso-di-n-propylamine 07/19/20110.654 2.181.74 79.8 6.420 1.635
o-Cresol 07/19/20110.654 2.181.70 78.0 9.600 1.548
Pentachlorophenol 07/19/20112.62 4.363.77 86.6 7.800 3.487
Phenol 07/19/20110.458 4.363.14 72.1 7.070 2.925
Pyridine 07/19/20110.654 4.362.39 55.0 5.250 2.272
Surr: 2,4,6-Tribromophenol 07/19/20112.181.73 79.1
Surr: 2-Fluorobiphenyl 07/19/20111.090.503 46.0
Surr: 2-Fluorophenol 07/19/20112.181.42 64.9
Surr: Nitrobenzene-d5 07/19/20111.090.677 62.0
Surr: Phenol-d5 07/19/20112.181.56 71.6
Surr: p-Terphenyl-d14 07/19/20111.090.989 90.6
Page 85 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MBLK-G110720-1
SampType: MBLK µg/KgUnits69726Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1,1,1,2-Tetrachloroethane 07/20/20115.0 ND1,1,1-Trichloroethane 07/20/20115.0 ND1,1,2,2-Tetrachloroethane 07/20/20115.0 ND1,1,2-Trichloro-1,2,2-trifluoroethane 07/20/20115.0 ND1,1,2-Trichloroethane 07/20/20115.0 ND1,1-Dichloro-2-propanone 07/20/201150.0 ND1,1-Dichloroethane 07/20/20115.0 ND1,1-Dichloroethene 07/20/20115.0 ND1,1-Dichloropropene 07/20/20115.0 ND1,2,3-Trichlorobenzene 07/20/20115.0 ND1,2,3-Trichloropropane 07/20/201110.0 ND1,2,3-Trimethylbenzene 07/20/20115.0 ND1,2,4-Trichlorobenzene 07/20/20115.0 ND1,2,4-Trimethylbenzene 07/20/20115.0 ND1,2-Dibromo-3-chloropropane 07/20/20115.0 ND1,2-Dibromoethane 07/20/20115.0 ND1,2-Dichlorobenzene 07/20/20115.0 ND1,2-Dichloroethane 07/20/20115.0 ND1,2-Dichloropropane 07/20/20115.0 ND1,3,5-Trimethylbenzene 07/20/20115.0 ND1,3-Dichlorobenzene 07/20/20115.0 ND1,3-Dichloropropane 07/20/20115.0 ND1,4-Dichlorobenzene 07/20/20115.0 ND1-Chlorobutane 07/20/20115.0 ND2,2-Dichloropropane 07/20/20115.0 ND2-Butanone 07/20/201150.0 ND2-Chlorotoluene 07/20/20115.0 ND2-Hexanone 07/20/201150.0 ND2-Nitropropane 07/20/201150.0 ND4-Chlorotoluene 07/20/20115.0 ND4-Methyl-2-pentanone 07/20/201150.0 NDAcetone 07/20/201150.0 NDAcrolein 07/20/2011100 NDAcrylonitrile 07/20/201110.0 NDAllyl chloride 07/20/20115.0 NDBenzene 07/20/20111.0 NDBromobenzene 07/20/20115.0 NDBromochloromethane 07/20/20115.0 NDBromodichloromethane 07/20/20115.0 NDBromoform 07/20/20115.0 NDBromomethane 07/20/201110.0 NDCarbon disulfide 07/20/20115.0 NDCarbon tetrachloride 07/20/20115.0 NDChlorobenzene 07/20/20115.0 NDChloroethane 07/20/201110.0 NDChloroform 07/20/20115.0 NDChloromethane 07/20/201110.0 ND
Page 86 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MBLK-G110720-1
SampType: MBLK µg/KgUnits69726Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
cis-1,2-Dichloroethene 07/20/20115.0 NDcis-1,3-Dichloropropene 07/20/20114.0 NDCyclohexanone 07/20/2011100 NDDibromochloromethane 07/20/20115.0 NDDibromomethane 07/20/20115.0 NDDichlorodifluoromethane 07/20/201110.0 NDEthyl acetate 07/20/201150.0 NDEthyl ether 07/20/20115.0 NDEthyl methacrylate 07/20/20115.0 NDEthylbenzene 07/20/20115.0 NDHeptane 07/20/201120.0 NDHexachlorobutadiene 07/20/20115.0 NDHexachloroethane 07/20/20115.0 NDIodomethane 07/20/201110.0 NDIsopropylbenzene 07/20/20115.0 NDm,p-Xylenes 07/20/20115.0 NDMethacrylonitrile 07/20/201150.0 NDMethyl Methacrylate 07/20/20115.0 NDMethyl tert-butyl ether 07/20/20112.0 NDMethylacrylate 07/20/201110.0 NDMethylene chloride J 07/20/20115.0 1.8Naphthalene 07/20/201110.0 NDn-Butylbenzene 07/20/20115.0 NDn-Hexane 07/20/201120.0 NDNitrobenzene 07/20/2011100 NDn-Propylbenzene 07/20/20115.0 NDo-Xylene 07/20/20115.0 NDPentachloroethane 07/20/20115.0 NDp-Isopropyltoluene 07/20/20115.0 NDPropionitrile 07/20/201150.0 NDsec-Butylbenzene 07/20/20115.0 NDStyrene 07/20/20115.0 NDtert-Butylbenzene 07/20/20115.0 NDTetrachloroethene 07/20/20115.0 NDTetrahydrofuran 07/20/201150.0 NDToluene 07/20/20115.0 NDtrans-1,2-Dichloroethene 07/20/20115.0 NDtrans-1,3-Dichloropropene 07/20/20114.0 NDTrichloroethene 07/20/20115.0 NDTrichlorofluoromethane 07/20/20115.0 NDVinyl acetate 07/20/201150.0 NDVinyl chloride 07/20/20112.0 ND Surr: 1,2-Dichloroethane-d4 07/20/201150.050.2 100.3 72.2 131
Surr: 4-Bromofluorobenzene 07/20/201150.051.3 102.5 82.1 116
Surr: Dibromofluoromethane 07/20/201150.048.3 96.6 77.7 120
Surr: Toluene-d8 07/20/201150.053.1 106.2 86 116
Page 87 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCSD-G110720-1
SampType: LCSD µg/KgUnits69726Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
1,1,1,2-Tetrachloroethane 07/20/20115.0 50.054.5 109.0 1.740 53.57
1,1,1-Trichloroethane 07/20/20115.0 50.054.3 108.7 1.280 53.64
1,1,2,2-Tetrachloroethane 07/20/20115.0 50.052.5 105.1 4.540 50.20
1,1,2-Trichloro-1,2,2-trifluoroethane 07/20/20115.0 50.055.3 110.5 0.860 55.74
1,1,2-Trichloroethane 07/20/20115.0 50.054.1 108.2 4.690 51.61
1,1-Dichloro-2-propanone 07/20/201150.0 125121 96.8 8.780 110.9
1,1-Dichloroethane 07/20/20115.0 50.050.8 101.6 2.490 49.53
1,1-Dichloroethene 07/20/20115.0 50.054.0 108.0 2.080 52.89
1,1-Dichloropropene 07/20/20115.0 50.051.8 103.5 0.690 52.11
1,2,3-Trichlorobenzene 07/20/20115.0 50.050.8 101.6 9.040 55.61
1,2,3-Trichloropropane 07/20/201110.0 50.054.0 108.0 3.970 51.90
1,2,3-Trimethylbenzene 07/20/20115.0 50.053.4 106.7 1.210 54.01
1,2,4-Trichlorobenzene 07/20/20115.0 50.054.0 107.9 8.810 58.92
1,2,4-Trimethylbenzene 07/20/20115.0 50.054.8 109.7 2.800 56.40
1,2-Dibromo-3-chloropropane 07/20/20115.0 50.051.7 103.5 1.990 50.72
1,2-Dibromoethane 07/20/20115.0 50.054.6 109.3 3.140 52.96
1,2-Dichlorobenzene 07/20/20115.0 50.053.2 106.5 0.790 52.83
1,2-Dichloroethane 07/20/20115.0 50.054.4 108.8 1.040 53.82
1,2-Dichloropropane 07/20/20115.0 50.048.4 96.7 3.990 46.48
1,3,5-Trimethylbenzene 07/20/20115.0 50.054.4 108.8 2.490 55.79
1,3-Dichlorobenzene 07/20/20115.0 50.054.7 109.5 0.200 54.63
1,3-Dichloropropane 07/20/20115.0 50.052.7 105.5 0.910 52.26
1,4-Dichlorobenzene 07/20/20115.0 50.053.6 107.3 1.570 54.48
1-Chlorobutane 07/20/20115.0 50.054.9 109.9 0.530 55.22
2,2-Dichloropropane 07/20/20115.0 50.053.8 107.6 1.220 53.14
2-Butanone 07/20/201150.0 125124 99.1 1.320 122.3
2-Chlorotoluene 07/20/20115.0 50.054.4 108.8 1.370 55.17
2-Hexanone 07/20/201150.0 125130 104.0 3.570 125.5
2-Nitropropane 07/20/201150.0 500505 101.1 7.740 467.7
4-Chlorotoluene 07/20/20115.0 50.055.1 110.2 2.080 56.24
4-Methyl-2-pentanone 07/20/201150.0 125123 98.6 9.180 112.4
Acetone 07/20/201150.0 125163 130.4 3.180 168.3
Acrylonitrile 07/20/201110.0 50.045.9 91.9 10.760 41.25
Allyl chloride 07/20/20115.0 50.053.9 107.9 1.360 54.68
Benzene 07/20/20111.0 50.050.5 101.1 2.360 49.35
Bromobenzene 07/20/20115.0 50.055.4 110.9 0.910 54.93
Bromochloromethane 07/20/20115.0 50.049.7 99.3 3.170 48.11
Bromodichloromethane 07/20/20115.0 50.053.7 107.5 0.090 53.68
Bromoform 07/20/20115.0 50.056.0 112.0 4.890 53.32
Bromomethane 07/20/201110.0 50.053.9 107.7 2.880 52.34
Carbon disulfide 07/20/20115.0 50.053.1 106.3 1.190 52.51
Carbon tetrachloride 07/20/20115.0 50.054.2 108.3 0.790 54.59
Chlorobenzene 07/20/20115.0 50.054.0 108.0 1.460 53.20
Chloroethane 07/20/201110.0 50.054.8 109.5 3.850 52.70
Chloroform 07/20/20115.0 50.051.6 103.2 0.760 51.22
Chloromethane 07/20/201110.0 50.056.4 112.8 6.190 53.03
cis-1,2-Dichloroethene 07/20/20115.0 50.050.0 100.0 1.780 49.13
Page 88 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCSD-G110720-1
SampType: LCSD µg/KgUnits69726Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
cis-1,3-Dichloropropene 07/20/20114.0 50.051.4 102.9 1.710 50.56
Cyclohexanone 07/20/2011100 250217 86.8 3.430 224.6
Dibromochloromethane 07/20/20115.0 50.055.8 111.6 2.910 54.21
Dibromomethane 07/20/20115.0 50.051.4 102.8 1.450 50.65
Dichlorodifluoromethane 07/20/201110.0 50.070.1 140.2 0.720 69.61
Ethyl acetate 07/20/201150.0 50.050.4 100.8 11.800 44.80
Ethyl ether 07/20/20115.0 50.048.0 96.1 2.640 46.80
Ethyl methacrylate 07/20/20115.0 50.053.6 107.3 5.260 50.89
Ethylbenzene 07/20/20115.0 50.054.2 108.4 1.510 53.38
Heptane 07/20/201120.0 50.051.4 102.8 3.620 49.59
Hexachlorobutadiene 07/20/20115.0 50.053.1 106.3 5.190 55.96
Hexachloroethane 07/20/20115.0 50.050.5 100.9 2.770 49.08
Iodomethane 07/20/201110.0 50.048.1 96.3 4.050 46.22
Isopropylbenzene 07/20/20115.0 50.054.8 109.7 2.030 53.73
m,p-Xylenes 07/20/20115.0 100110 110.2 1.440 108.6
Methacrylonitrile J 07/20/201150.0 50.048 95.9 0.000 43.81
Methyl Methacrylate 07/20/20115.0 50.048.2 96.4 6.930 44.98
Methyl tert-butyl ether 07/20/20112.0 50.051.4 102.9 3.180 49.83
Methylacrylate 07/20/201110.0 50.048.5 96.9 8.990 44.30
Methylene chloride 07/20/20115.0 50.049.5 99.0 2.410 48.33
Naphthalene 07/20/201110.0 50.046.7 93.4 3.390 48.31
n-Butylbenzene 07/20/20115.0 50.055.1 110.2 2.460 56.46
n-Hexane 07/20/201120.0 50.052.0 104.0 1.390 51.27
Nitrobenzene 07/20/2011100 500231 46.2 1.640 234.8
n-Propylbenzene 07/20/20115.0 50.055.2 110.3 1.030 55.72
o-Xylene 07/20/20115.0 50.054.7 109.4 2.270 53.49
Pentachloroethane 07/20/20115.0 50.056.9 113.7 3.250 55.05
p-Isopropyltoluene 07/20/20115.0 50.053.8 107.7 0.330 54.02
Propionitrile 07/20/201150.0 500460 92.1 10.190 415.6
sec-Butylbenzene 07/20/20115.0 50.054.6 109.1 0.260 54.70
Styrene 07/20/20115.0 50.053.6 107.2 3.530 51.75
tert-Butylbenzene 07/20/20115.0 50.054.4 108.7 3.030 56.04
Tetrachloroethene 07/20/20115.0 50.056.9 113.8 0.020 56.92
Tetrahydrofuran J 07/20/201150.0 50.040 79.8 0.000 37.04
Toluene 07/20/20115.0 50.053.3 106.5 1.340 52.55
trans-1,2-Dichloroethene 07/20/20115.0 50.051.7 103.4 0.120 51.66
trans-1,3-Dichloropropene 07/20/20114.0 50.054.6 109.3 0.490 54.90
Trichloroethene 07/20/20115.0 50.051.6 103.2 0.900 51.16
Trichlorofluoromethane 07/20/20115.0 50.062.1 124.1 0.510 62.38
Vinyl acetate 07/20/201150.0 50.052.5 105.0 4.600 50.12
Vinyl chloride 07/20/20112.0 50.059.2 118.3 1.960 58.02
Surr: 1,2-Dichloroethane-d4 07/20/201150.052.2 104.4
Surr: 4-Bromofluorobenzene 07/20/201150.052.1 104.1
Surr: Dibromofluoromethane 07/20/201150.049.2 98.4
Surr: Toluene-d8 07/20/201150.052.9 105.7
Page 89 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCS-G110720-1
SampType: LCS µg/KgUnits69726Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1,1,1,2-Tetrachloroethane 07/20/20115.0 50.053.6 107.10 0 200
1,1,1-Trichloroethane 07/20/20115.0 50.053.6 107.30 85.6 124
1,1,2,2-Tetrachloroethane 07/20/20115.0 50.050.2 100.40 0 200
1,1,2-Trichloro-1,2,2-trifluoroethane 07/20/20115.0 50.055.7 111.50 0 200
1,1,2-Trichloroethane 07/20/20115.0 50.051.6 103.20 0 200
1,1-Dichloro-2-propanone 07/20/201150.0 125111 88.70 0 200
1,1-Dichloroethane 07/20/20115.0 50.049.5 99.10 0 200
1,1-Dichloroethene 07/20/20115.0 50.052.9 105.80 60.1 131
1,1-Dichloropropene 07/20/20115.0 50.052.1 104.20 0 200
1,2,3-Trichlorobenzene 07/20/20115.0 50.055.6 111.20 0 200
1,2,3-Trichloropropane 07/20/201110.0 50.051.9 103.80 0 200
1,2,3-Trimethylbenzene 07/20/20115.0 50.054.0 108.00 0 200
1,2,4-Trichlorobenzene 07/20/20115.0 50.058.9 117.80 0 200
1,2,4-Trimethylbenzene 07/20/20115.0 50.056.4 112.80 0 200
1,2-Dibromo-3-chloropropane 07/20/20115.0 50.050.7 101.40 0 200
1,2-Dibromoethane 07/20/20115.0 50.053.0 105.90 86.9 119
1,2-Dichlorobenzene 07/20/20115.0 50.052.8 105.70 88 119
1,2-Dichloroethane 07/20/20115.0 50.053.8 107.60 73 117
1,2-Dichloropropane 07/20/20115.0 50.046.5 93.00 0 200
1,3,5-Trimethylbenzene 07/20/20115.0 50.055.8 111.60 0 200
1,3-Dichlorobenzene 07/20/20115.0 50.054.6 109.30 85.8 125
1,3-Dichloropropane 07/20/20115.0 50.052.3 104.50 0 200
1,4-Dichlorobenzene 07/20/20115.0 50.054.5 109.00 84.5 124
1-Chlorobutane 07/20/20115.0 50.055.2 110.40 0 200
2,2-Dichloropropane 07/20/20115.0 50.053.1 106.30 0 200
2-Butanone 07/20/201150.0 125122 97.80 45.3 136
2-Chlorotoluene 07/20/20115.0 50.055.2 110.30 0 200
2-Hexanone 07/20/201150.0 125126 100.40 0 200
2-Nitropropane 07/20/201150.0 500468 93.50 0 200
4-Chlorotoluene 07/20/20115.0 50.056.2 112.50 0 200
4-Methyl-2-pentanone 07/20/201150.0 125112 89.90 0 200
Acetone 07/20/201150.0 125168 134.60 0 200
Acrylonitrile 07/20/201110.0 50.041.2 82.50 0 200
Allyl chloride 07/20/20115.0 50.054.7 109.40 0 200
Benzene 07/20/20111.0 50.049.4 98.70 73.9 109
Bromobenzene 07/20/20115.0 50.054.9 109.90 0 200
Bromochloromethane 07/20/20115.0 50.048.1 96.20 0 200
Bromodichloromethane 07/20/20115.0 50.053.7 107.40 91.3 126
Bromoform 07/20/20115.0 50.053.3 106.60 0 200
Bromomethane 07/20/201110.0 50.052.3 104.70 0 200
Carbon disulfide 07/20/20115.0 50.052.5 105.00 0 200
Carbon tetrachloride 07/20/20115.0 50.054.6 109.20 83.3 127
Chlorobenzene 07/20/20115.0 50.053.2 106.40 85.8 116
Chloroethane 07/20/201110.0 50.052.7 105.40 0 200
Chloroform 07/20/20115.0 50.051.2 102.40 80 113
Chloromethane 07/20/201110.0 50.053.0 106.10 0 200
cis-1,2-Dichloroethene 07/20/20115.0 50.049.1 98.30 0 200
Page 90 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCS-G110720-1
SampType: LCS µg/KgUnits69726Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
cis-1,3-Dichloropropene 07/20/20114.0 50.050.6 101.10 0 200
Cyclohexanone 07/20/2011100 250225 89.80 0 200
Dibromochloromethane 07/20/20115.0 50.054.2 108.40 89.1 119
Dibromomethane 07/20/20115.0 50.050.6 101.30 0 200
Dichlorodifluoromethane 07/20/201110.0 50.069.6 139.20 0 200
Ethyl acetate J 07/20/201150.0 50.045 89.60 0 200
Ethyl ether 07/20/20115.0 50.046.8 93.60 0 200
Ethyl methacrylate 07/20/20115.0 50.050.9 101.80 0 200
Ethylbenzene 07/20/20115.0 50.053.4 106.80 84.1 115
Heptane 07/20/201120.0 50.049.6 99.20 0 200
Hexachlorobutadiene 07/20/20115.0 50.056.0 111.90 0 200
Hexachloroethane 07/20/20115.0 50.049.1 98.20 0 200
Iodomethane 07/20/201110.0 50.046.2 92.40 0 200
Isopropylbenzene 07/20/20115.0 50.053.7 107.50 0 200
m,p-Xylenes 07/20/20115.0 100109 108.60 79.1 111
Methacrylonitrile J 07/20/201150.0 50.044 87.60 0 200
Methyl Methacrylate 07/20/20115.0 50.045.0 90.00 0 200
Methyl tert-butyl ether 07/20/20112.0 50.049.8 99.70 80 128
Methylacrylate 07/20/201110.0 50.044.3 88.60 0 200
Methylene chloride 07/20/20115.0 50.048.3 96.70 73.9 116
Naphthalene 07/20/201110.0 50.048.3 96.60 73.1 135
n-Butylbenzene 07/20/20115.0 50.056.5 112.90 0 200
n-Hexane 07/20/201120.0 50.051.3 102.50 0 200
Nitrobenzene 07/20/2011100 500235 47.00 0 200
n-Propylbenzene 07/20/20115.0 50.055.7 111.40 0 200
o-Xylene 07/20/20115.0 50.053.5 107.00 82 117
Pentachloroethane 07/20/20115.0 50.055.0 110.10 0 200
p-Isopropyltoluene 07/20/20115.0 50.054.0 108.00 0 200
Propionitrile 07/20/201150.0 500416 83.10 0 200
sec-Butylbenzene 07/20/20115.0 50.054.7 109.40 0 200
Styrene 07/20/20115.0 50.051.8 103.50 0 200
tert-Butylbenzene 07/20/20115.0 50.056.0 112.10 0 200
Tetrachloroethene 07/20/20115.0 50.056.9 113.80 74.6 115
Tetrahydrofuran J 07/20/201150.0 50.037 74.10 0 200
Toluene 07/20/20115.0 50.052.6 105.10 79.1 112
trans-1,2-Dichloroethene 07/20/20115.0 50.051.7 103.30 0 200
trans-1,3-Dichloropropene 07/20/20114.0 50.054.9 109.80 0 200
Trichloroethene 07/20/20115.0 50.051.2 102.30 81 111
Trichlorofluoromethane 07/20/20115.0 50.062.4 124.80 0 200
Vinyl acetate 07/20/201150.0 50.050.1 100.20 0 200
Vinyl chloride 07/20/20112.0 50.058.0 116.00 0 200
Surr: 1,2-Dichloroethane-d4 07/20/201150.052.7 105.4 72.2 131
Surr: 4-Bromofluorobenzene 07/20/201150.050.4 100.7 82.1 116
Surr: Dibromofluoromethane 07/20/201150.050.0 100.0 77.7 120
Surr: Toluene-d8 07/20/201150.053.2 106.3 86 116
Page 91 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MBLK-G110720-2
SampType: MBLK µg/KgUnits69754Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1,1,1,2-Tetrachloroethane 07/20/20115.0 ND1,1,1-Trichloroethane 07/20/20115.0 ND1,1,2,2-Tetrachloroethane 07/20/20115.0 ND1,1,2-Trichloro-1,2,2-trifluoroethane 07/20/20115.0 ND1,1,2-Trichloroethane 07/20/20115.0 ND1,1-Dichloro-2-propanone 07/20/201150.0 ND1,1-Dichloroethane 07/20/20115.0 ND1,1-Dichloroethene 07/20/20115.0 ND1,1-Dichloropropene 07/20/20115.0 ND1,2,3-Trichlorobenzene 07/20/20115.0 ND1,2,3-Trichloropropane 07/20/201110.0 ND1,2,3-Trimethylbenzene 07/20/20115.0 ND1,2,4-Trichlorobenzene 07/20/20115.0 ND1,2,4-Trimethylbenzene 07/20/20115.0 ND1,2-Dibromo-3-chloropropane 07/20/20115.0 ND1,2-Dibromoethane 07/20/20115.0 ND1,2-Dichlorobenzene 07/20/20115.0 ND1,2-Dichloroethane 07/20/20115.0 ND1,2-Dichloropropane 07/20/20115.0 ND1,3,5-Trimethylbenzene 07/20/20115.0 ND1,3-Dichlorobenzene 07/20/20115.0 ND1,3-Dichloropropane 07/20/20115.0 ND1,4-Dichlorobenzene 07/20/20115.0 ND1-Chlorobutane 07/20/20115.0 ND2,2-Dichloropropane 07/20/20115.0 ND2-Butanone 07/20/201150.0 ND2-Chlorotoluene 07/20/20115.0 ND2-Hexanone 07/20/201150.0 ND2-Nitropropane 07/20/201150.0 ND4-Chlorotoluene 07/20/20115.0 ND4-Methyl-2-pentanone 07/20/201150.0 NDAcetone 07/20/201150.0 NDAcrolein 07/20/2011100 NDAcrylonitrile 07/20/201110.0 NDAllyl chloride 07/20/20115.0 NDBenzene 07/20/20111.0 NDBromobenzene 07/20/20115.0 NDBromochloromethane 07/20/20115.0 NDBromodichloromethane 07/20/20115.0 NDBromoform 07/20/20115.0 NDBromomethane 07/20/201110.0 NDCarbon disulfide 07/20/20115.0 NDCarbon tetrachloride 07/20/20115.0 NDChlorobenzene 07/20/20115.0 NDChloroethane 07/20/201110.0 NDChloroform 07/20/20115.0 NDChloromethane 07/20/201110.0 ND
Page 92 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MBLK-G110720-2
SampType: MBLK µg/KgUnits69754Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
cis-1,2-Dichloroethene 07/20/20115.0 NDcis-1,3-Dichloropropene 07/20/20114.0 NDCyclohexanone 07/20/2011100 NDDibromochloromethane 07/20/20115.0 NDDibromomethane 07/20/20115.0 NDDichlorodifluoromethane 07/20/201110.0 NDEthyl acetate 07/20/201150.0 NDEthyl ether 07/20/20115.0 NDEthyl methacrylate 07/20/20115.0 NDEthylbenzene 07/20/20115.0 NDHeptane 07/20/201120.0 NDHexachlorobutadiene 07/20/20115.0 NDHexachloroethane 07/20/20115.0 NDIodomethane 07/20/201110.0 NDIsopropylbenzene 07/20/20115.0 NDm,p-Xylenes 07/20/20115.0 NDMethacrylonitrile 07/20/201150.0 NDMethyl Methacrylate 07/20/20115.0 NDMethyl tert-butyl ether 07/20/20112.0 NDMethylacrylate 07/20/201110.0 NDMethylene chloride J 07/20/20115.0 1.8Naphthalene 07/20/201110.0 NDn-Butylbenzene 07/20/20115.0 NDn-Hexane 07/20/201120.0 NDNitrobenzene 07/20/2011100 NDn-Propylbenzene 07/20/20115.0 NDo-Xylene 07/20/20115.0 NDPentachloroethane 07/20/20115.0 NDp-Isopropyltoluene 07/20/20115.0 NDPropionitrile 07/20/201150.0 NDsec-Butylbenzene 07/20/20115.0 NDStyrene 07/20/20115.0 NDtert-Butylbenzene 07/20/20115.0 NDTetrachloroethene 07/20/20115.0 NDTetrahydrofuran 07/20/201150.0 NDToluene 07/20/20115.0 NDtrans-1,2-Dichloroethene 07/20/20115.0 NDtrans-1,3-Dichloropropene 07/20/20114.0 NDTrichloroethene 07/20/20115.0 NDTrichlorofluoromethane 07/20/20115.0 NDVinyl acetate 07/20/201150.0 NDVinyl chloride 07/20/20112.0 ND Surr: 1,2-Dichloroethane-d4 07/20/201150.054.1 108.2 72.2 131
Surr: 4-Bromofluorobenzene 07/20/201150.051.4 102.8 82.1 116
Surr: Dibromofluoromethane 07/20/201150.049.3 98.7 77.7 120
Surr: Toluene-d8 07/20/201150.053.2 106.4 86 116
Page 93 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCSD-G110720-2
SampType: LCSD µg/KgUnits69754Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
1,1,1,2-Tetrachloroethane 07/20/20115.0 50.052.0 104.1 1.350 51.34
1,1,1-Trichloroethane 07/20/20115.0 50.050.5 101.0 1.300 51.15
1,1,2,2-Tetrachloroethane 07/20/20115.0 50.048.7 97.4 4.230 46.70
1,1,2-Trichloro-1,2,2-trifluoroethane 07/20/20115.0 50.047.5 95.1 1.730 48.36
1,1,2-Trichloroethane 07/20/20115.0 50.051.9 103.9 4.170 49.82
1,1-Dichloro-2-propanone 07/20/201150.0 125113 90.6 0.940 114.3
1,1-Dichloroethane 07/20/20115.0 50.047.0 94.0 0.530 47.23
1,1-Dichloroethene 07/20/20115.0 50.046.9 93.8 0.490 47.15
1,1-Dichloropropene 07/20/20115.0 50.046.8 93.7 2.320 47.93
1,2,3-Trichlorobenzene 07/20/20115.0 50.043.2 86.4 2.150 44.14
1,2,3-Trichloropropane 07/20/201110.0 50.050.0 100.0 2.590 48.72
1,2,3-Trimethylbenzene 07/20/20115.0 50.047.8 95.6 0.040 47.82
1,2,4-Trichlorobenzene 07/20/20115.0 50.040.8 81.5 3.660 42.28
1,2,4-Trimethylbenzene 07/20/20115.0 50.047.2 94.4 1.470 47.89
1,2-Dibromo-3-chloropropane 07/20/20115.0 50.049.8 99.6 5.640 47.07
1,2-Dibromoethane 07/20/20115.0 50.052.6 105.3 3.910 50.61
1,2-Dichlorobenzene 07/20/20115.0 50.046.1 92.2 0.300 46.26
1,2-Dichloroethane 07/20/20115.0 50.053.2 106.3 1.770 54.12
1,2-Dichloropropane 07/20/20115.0 50.044.5 89.1 1.420 43.90
1,3,5-Trimethylbenzene 07/20/20115.0 50.047.6 95.3 0.170 47.72
1,3-Dichlorobenzene 07/20/20115.0 50.045.3 90.5 1.210 45.81
1,3-Dichloropropane 07/20/20115.0 50.050.9 101.8 1.820 49.96
1,4-Dichlorobenzene 07/20/20115.0 50.044.1 88.3 2.660 45.33
1-Chlorobutane 07/20/20115.0 50.051.1 102.2 0.630 50.79
2,2-Dichloropropane 07/20/20115.0 50.047.4 94.7 1.860 48.26
2-Butanone 07/20/201150.0 125113 90.5 11.720 100.6
2-Chlorotoluene 07/20/20115.0 50.047.2 94.3 1.560 47.89
2-Hexanone 07/20/201150.0 125118 94.1 8.380 108.1
2-Nitropropane 07/20/201150.0 500505 101.0 4.660 482.2
4-Chlorotoluene 07/20/20115.0 50.046.4 92.8 0.820 46.79
4-Methyl-2-pentanone 07/20/201150.0 125119 95.3 6.410 111.7
Acetone 07/20/201150.0 125131 104.5 8.390 120.1
Acrylonitrile 07/20/201110.0 50.043.8 87.5 5.500 41.41
Allyl chloride 07/20/20115.0 50.049.5 99.0 4.330 51.71
Benzene 07/20/20111.0 50.045.6 91.1 1.110 46.08
Bromobenzene 07/20/20115.0 50.048.9 97.9 1.210 48.34
Bromochloromethane 07/20/20115.0 50.046.6 93.2 0.860 46.98
Bromodichloromethane 07/20/20115.0 50.051.2 102.5 1.740 52.14
Bromoform 07/20/20115.0 50.053.8 107.7 2.860 52.33
Bromomethane 07/20/201110.0 50.045.4 90.9 4.220 47.39
Carbon disulfide 07/20/20115.0 50.044.4 88.9 1.270 45.01
Carbon tetrachloride 07/20/20115.0 50.050.2 100.5 2.200 51.37
Chlorobenzene 07/20/20115.0 50.049.4 98.8 1.550 48.65
Chloroethane 07/20/201110.0 50.045.2 90.5 0.620 45.53
Chloroform 07/20/20115.0 50.049.8 99.7 0.140 49.76
Chloromethane 07/20/201110.0 50.041.9 83.7 3.660 43.42
cis-1,2-Dichloroethene 07/20/20115.0 50.045.1 90.2 0.440 44.91
Page 94 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCSD-G110720-2
SampType: LCSD µg/KgUnits69754Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
cis-1,3-Dichloropropene 07/20/20114.0 50.047.5 95.0 0.760 47.15
Cyclohexanone 07/20/2011100 250213 85.4 13.820 185.8
Dibromochloromethane 07/20/20115.0 50.053.3 106.6 1.320 52.60
Dibromomethane 07/20/20115.0 50.048.6 97.3 0.020 48.64
Dichlorodifluoromethane 07/20/201110.0 50.038.8 77.7 10.650 43.21
Ethyl acetate J 07/20/201150.0 50.048 95.2 0.000 46.78
Ethyl ether 07/20/20115.0 50.044.5 89.1 3.920 42.82
Ethyl methacrylate 07/20/20115.0 50.050.5 100.9 3.000 48.98
Ethylbenzene 07/20/20115.0 50.049.2 98.3 0.240 49.05
Heptane 07/20/201120.0 50.042.1 84.2 5.110 44.33
Hexachlorobutadiene 07/20/20115.0 50.044.4 88.9 3.840 46.17
Hexachloroethane 07/20/20115.0 50.046.2 92.5 1.100 46.74
Iodomethane 07/20/201110.0 50.042.2 84.5 1.140 41.75
Isopropylbenzene 07/20/20115.0 50.050.6 101.3 0.040 50.63
m,p-Xylenes 07/20/20115.0 100103 102.5 3.360 99.12
Methacrylonitrile J 07/20/201150.0 50.046 92.6 0.000 44.09
Methyl Methacrylate 07/20/20115.0 50.045.7 91.4 4.180 43.85
Methyl tert-butyl ether 07/20/20112.0 50.049.0 98.1 2.140 48.00
Methylacrylate 07/20/201110.0 50.045.3 90.6 6.280 42.56
Methylene chloride 07/20/20115.0 50.045.8 91.6 0.530 45.54
Naphthalene 07/20/201110.0 50.044.8 89.7 2.280 43.84
n-Butylbenzene 07/20/20115.0 50.044.3 88.5 3.050 45.64
n-Hexane 07/20/201120.0 50.041.4 82.8 3.770 43.01
Nitrobenzene 07/20/2011100 500221 44.2 5.130 209.7
n-Propylbenzene 07/20/20115.0 50.046.9 93.8 0.930 47.36
o-Xylene 07/20/20115.0 50.051.7 103.5 1.460 50.99
Pentachloroethane 07/20/20115.0 50.048.1 96.2 2.060 49.09
p-Isopropyltoluene 07/20/20115.0 50.047.2 94.5 2.240 48.30
Propionitrile 07/20/201150.0 500445 88.9 8.710 407.6
sec-Butylbenzene 07/20/20115.0 50.047.2 94.4 1.370 47.83
Styrene 07/20/20115.0 50.048.4 96.8 0.210 48.29
tert-Butylbenzene 07/20/20115.0 50.049.9 99.8 0.320 50.06
Tetrachloroethene 07/20/20115.0 50.052.3 104.7 0.110 52.39
Tetrahydrofuran J 07/20/201150.0 50.039 77.7 0.000 35.48
Toluene 07/20/20115.0 50.049.7 99.3 2.120 48.62
trans-1,2-Dichloroethene 07/20/20115.0 50.047.6 95.3 0.860 47.22
trans-1,3-Dichloropropene 07/20/20114.0 50.051.9 103.7 0.700 51.50
Trichloroethene 07/20/20115.0 50.046.0 92.1 0.200 45.96
Trichlorofluoromethane 07/20/20115.0 50.053.0 106.1 4.330 55.39
Vinyl acetate J 07/20/201150.0 50.048 95.4 0.000 45.98
Vinyl chloride 07/20/20112.0 50.046.1 92.1 2.320 47.14
Surr: 1,2-Dichloroethane-d4 07/20/201150.055.1 110.1
Surr: 4-Bromofluorobenzene 07/20/201150.053.2 106.4
Surr: Dibromofluoromethane 07/20/201150.049.7 99.5
Surr: Toluene-d8 07/20/201150.053.9 107.8
Page 95 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCS-G110720-2
SampType: LCS µg/KgUnits69754Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1,1,1,2-Tetrachloroethane 07/20/20115.0 50.051.3 102.70 0 200
1,1,1-Trichloroethane 07/20/20115.0 50.051.2 102.30 85.6 124
1,1,2,2-Tetrachloroethane 07/20/20115.0 50.046.7 93.40 0 200
1,1,2-Trichloro-1,2,2-trifluoroethane 07/20/20115.0 50.048.4 96.70 0 200
1,1,2-Trichloroethane 07/20/20115.0 50.049.8 99.60 0 200
1,1-Dichloro-2-propanone 07/20/201150.0 125114 91.50 0 200
1,1-Dichloroethane 07/20/20115.0 50.047.2 94.50 0 200
1,1-Dichloroethene 07/20/20115.0 50.047.2 94.30 60.1 131
1,1-Dichloropropene 07/20/20115.0 50.047.9 95.90 0 200
1,2,3-Trichlorobenzene 07/20/20115.0 50.044.1 88.30 0 200
1,2,3-Trichloropropane 07/20/201110.0 50.048.7 97.40 0 200
1,2,3-Trimethylbenzene 07/20/20115.0 50.047.8 95.60 0 200
1,2,4-Trichlorobenzene 07/20/20115.0 50.042.3 84.60 0 200
1,2,4-Trimethylbenzene 07/20/20115.0 50.047.9 95.80 0 200
1,2-Dibromo-3-chloropropane 07/20/20115.0 50.047.1 94.10 0 200
1,2-Dibromoethane 07/20/20115.0 50.050.6 101.20 86.9 119
1,2-Dichlorobenzene 07/20/20115.0 50.046.3 92.50 88 119
1,2-Dichloroethane 07/20/20115.0 50.054.1 108.20 73 117
1,2-Dichloropropane 07/20/20115.0 50.043.9 87.80 0 200
1,3,5-Trimethylbenzene 07/20/20115.0 50.047.7 95.40 0 200
1,3-Dichlorobenzene 07/20/20115.0 50.045.8 91.60 85.8 125
1,3-Dichloropropane 07/20/20115.0 50.050.0 99.90 0 200
1,4-Dichlorobenzene 07/20/20115.0 50.045.3 90.70 84.5 124
1-Chlorobutane 07/20/20115.0 50.050.8 101.60 0 200
2,2-Dichloropropane 07/20/20115.0 50.048.3 96.50 0 200
2-Butanone 07/20/201150.0 125101 80.50 45.3 136
2-Chlorotoluene 07/20/20115.0 50.047.9 95.80 0 200
2-Hexanone 07/20/201150.0 125108 86.50 0 200
2-Nitropropane 07/20/201150.0 500482 96.40 0 200
4-Chlorotoluene 07/20/20115.0 50.046.8 93.60 0 200
4-Methyl-2-pentanone 07/20/201150.0 125112 89.40 0 200
Acetone 07/20/201150.0 125120 96.00 0 200
Acrylonitrile 07/20/201110.0 50.041.4 82.80 0 200
Allyl chloride 07/20/20115.0 50.051.7 103.40 0 200
Benzene 07/20/20111.0 50.046.1 92.20 73.9 109
Bromobenzene 07/20/20115.0 50.048.3 96.70 0 200
Bromochloromethane 07/20/20115.0 50.047.0 94.00 0 200
Bromodichloromethane 07/20/20115.0 50.052.1 104.30 91.3 126
Bromoform 07/20/20115.0 50.052.3 104.70 0 200
Bromomethane 07/20/201110.0 50.047.4 94.80 0 200
Carbon disulfide 07/20/20115.0 50.045.0 90.00 0 200
Carbon tetrachloride 07/20/20115.0 50.051.4 102.70 83.3 127
Chlorobenzene 07/20/20115.0 50.048.6 97.30 85.8 116
Chloroethane 07/20/201110.0 50.045.5 91.10 0 200
Chloroform 07/20/20115.0 50.049.8 99.50 80 113
Chloromethane 07/20/201110.0 50.043.4 86.80 0 200
cis-1,2-Dichloroethene 07/20/20115.0 50.044.9 89.80 0 200
Page 96 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCS-G110720-2
SampType: LCS µg/KgUnits69754Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
cis-1,3-Dichloropropene 07/20/20114.0 50.047.2 94.30 0 200
Cyclohexanone 07/20/2011100 250186 74.30 0 200
Dibromochloromethane 07/20/20115.0 50.052.6 105.20 89.1 119
Dibromomethane 07/20/20115.0 50.048.6 97.30 0 200
Dichlorodifluoromethane 07/20/201110.0 50.043.2 86.40 0 200
Ethyl acetate J 07/20/201150.0 50.047 93.60 0 200
Ethyl ether 07/20/20115.0 50.042.8 85.60 0 200
Ethyl methacrylate 07/20/20115.0 50.049.0 98.00 0 200
Ethylbenzene 07/20/20115.0 50.049.0 98.10 84.1 115
Heptane 07/20/201120.0 50.044.3 88.70 0 200
Hexachlorobutadiene 07/20/20115.0 50.046.2 92.30 0 200
Hexachloroethane 07/20/20115.0 50.046.7 93.50 0 200
Iodomethane 07/20/201110.0 50.041.8 83.50 0 200
Isopropylbenzene 07/20/20115.0 50.050.6 101.30 0 200
m,p-Xylenes 07/20/20115.0 10099.1 99.10 79.1 111
Methacrylonitrile J 07/20/201150.0 50.044 88.20 0 200
Methyl Methacrylate 07/20/20115.0 50.043.8 87.70 0 200
Methyl tert-butyl ether 07/20/20112.0 50.048.0 96.00 80 128
Methylacrylate 07/20/201110.0 50.042.6 85.10 0 200
Methylene chloride 07/20/20115.0 50.045.5 91.10 73.9 116
Naphthalene 07/20/201110.0 50.043.8 87.70 73.1 135
n-Butylbenzene 07/20/20115.0 50.045.6 91.30 0 200
n-Hexane 07/20/201120.0 50.043.0 86.00 0 200
Nitrobenzene 07/20/2011100 500210 41.90 0 200
n-Propylbenzene 07/20/20115.0 50.047.4 94.70 0 200
o-Xylene 07/20/20115.0 50.051.0 102.00 82 117
Pentachloroethane 07/20/20115.0 50.049.1 98.20 0 200
p-Isopropyltoluene 07/20/20115.0 50.048.3 96.60 0 200
Propionitrile 07/20/201150.0 500408 81.50 0 200
sec-Butylbenzene 07/20/20115.0 50.047.8 95.70 0 200
Styrene 07/20/20115.0 50.048.3 96.60 0 200
tert-Butylbenzene 07/20/20115.0 50.050.1 100.10 0 200
Tetrachloroethene 07/20/20115.0 50.052.4 104.80 74.6 115
Tetrahydrofuran J 07/20/201150.0 50.036 71.00 0 200
Toluene 07/20/20115.0 50.048.6 97.20 79.1 112
trans-1,2-Dichloroethene 07/20/20115.0 50.047.2 94.40 0 200
trans-1,3-Dichloropropene 07/20/20114.0 50.051.5 103.00 0 200
Trichloroethene 07/20/20115.0 50.046.0 91.90 81 111
Trichlorofluoromethane 07/20/20115.0 50.055.4 110.80 0 200
Vinyl acetate J 07/20/201150.0 50.046 92.00 0 200
Vinyl chloride 07/20/20112.0 50.047.1 94.30 0 200
Surr: 1,2-Dichloroethane-d4 07/20/201150.056.0 112.1 72.2 131
Surr: 4-Bromofluorobenzene 07/20/201150.053.2 106.4 82.1 116
Surr: Dibromofluoromethane 07/20/201150.049.8 99.7 77.7 120
Surr: Toluene-d8 07/20/201150.052.8 105.6 86 116
Page 97 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MBLK-G110721-1
SampType: MBLK µg/KgUnits69790Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1,1,1,2-Tetrachloroethane 07/21/20115.0 ND1,1,1-Trichloroethane 07/21/20115.0 ND1,1,2,2-Tetrachloroethane 07/21/20115.0 ND1,1,2-Trichloro-1,2,2-trifluoroethane 07/21/20115.0 ND1,1,2-Trichloroethane 07/21/20115.0 ND1,1-Dichloro-2-propanone 07/21/201150.0 ND1,1-Dichloroethane 07/21/20115.0 ND1,1-Dichloroethene 07/21/20115.0 ND1,1-Dichloropropene 07/21/20115.0 ND1,2,3-Trichlorobenzene 07/21/20115.0 ND1,2,3-Trichloropropane 07/21/201110.0 ND1,2,3-Trimethylbenzene 07/21/20115.0 ND1,2,4-Trichlorobenzene 07/21/20115.0 ND1,2,4-Trimethylbenzene 07/21/20115.0 ND1,2-Dibromo-3-chloropropane 07/21/20115.0 ND1,2-Dibromoethane 07/21/20115.0 ND1,2-Dichlorobenzene 07/21/20115.0 ND1,2-Dichloroethane 07/21/20115.0 ND1,2-Dichloropropane 07/21/20115.0 ND1,3,5-Trimethylbenzene 07/21/20115.0 ND1,3-Dichlorobenzene 07/21/20115.0 ND1,3-Dichloropropane 07/21/20115.0 ND1,4-Dichlorobenzene 07/21/20115.0 ND1-Chlorobutane 07/21/20115.0 ND2,2-Dichloropropane 07/21/20115.0 ND2-Butanone 07/21/201150.0 ND2-Chlorotoluene 07/21/20115.0 ND2-Hexanone 07/21/201150.0 ND2-Nitropropane 07/21/201150.0 ND4-Chlorotoluene 07/21/20115.0 ND4-Methyl-2-pentanone 07/21/201150.0 NDAcetone 07/21/201150.0 NDAcrolein 07/21/2011100 NDAcrylonitrile 07/21/201110.0 NDAllyl chloride 07/21/20115.0 NDBenzene 07/21/20111.0 NDBromobenzene 07/21/20115.0 NDBromochloromethane 07/21/20115.0 NDBromodichloromethane 07/21/20115.0 NDBromoform 07/21/20115.0 NDBromomethane 07/21/201110.0 NDCarbon disulfide 07/21/20115.0 NDCarbon tetrachloride 07/21/20115.0 NDChlorobenzene 07/21/20115.0 NDChloroethane 07/21/201110.0 NDChloroform 07/21/20115.0 NDChloromethane 07/21/201110.0 ND
Page 98 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: MBLK-G110721-1
SampType: MBLK µg/KgUnits69790Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
cis-1,2-Dichloroethene 07/21/20115.0 NDcis-1,3-Dichloropropene 07/21/20114.0 NDCyclohexanone 07/21/2011100 NDDibromochloromethane 07/21/20115.0 NDDibromomethane 07/21/20115.0 NDDichlorodifluoromethane 07/21/201110.0 NDEthyl acetate 07/21/201150.0 NDEthyl ether 07/21/20115.0 NDEthyl methacrylate 07/21/20115.0 NDEthylbenzene 07/21/20115.0 NDHeptane 07/21/201120.0 NDHexachlorobutadiene 07/21/20115.0 NDHexachloroethane 07/21/20115.0 NDIodomethane 07/21/201110.0 NDIsopropylbenzene 07/21/20115.0 NDm,p-Xylenes 07/21/20115.0 NDMethacrylonitrile 07/21/201150.0 NDMethyl Methacrylate 07/21/20115.0 NDMethyl tert-butyl ether 07/21/20112.0 NDMethylacrylate 07/21/201110.0 NDMethylene chloride J 07/21/20115.0 1.7Naphthalene 07/21/201110.0 NDn-Butylbenzene 07/21/20115.0 NDn-Hexane 07/21/201120.0 NDNitrobenzene 07/21/2011100 NDn-Propylbenzene 07/21/20115.0 NDo-Xylene 07/21/20115.0 NDPentachloroethane 07/21/20115.0 NDp-Isopropyltoluene 07/21/20115.0 NDPropionitrile 07/21/201150.0 NDsec-Butylbenzene 07/21/20115.0 NDStyrene 07/21/20115.0 NDtert-Butylbenzene 07/21/20115.0 NDTetrachloroethene 07/21/20115.0 NDTetrahydrofuran 07/21/201150.0 NDToluene 07/21/20115.0 NDtrans-1,2-Dichloroethene 07/21/20115.0 NDtrans-1,3-Dichloropropene 07/21/20114.0 NDTrichloroethene 07/21/20115.0 NDTrichlorofluoromethane 07/21/20115.0 NDVinyl acetate 07/21/201150.0 NDVinyl chloride 07/21/20112.0 ND Surr: 1,2-Dichloroethane-d4 07/21/201150.054.0 108.1 72.2 131
Surr: 4-Bromofluorobenzene 07/21/201150.053.0 105.9 82.1 116
Surr: Dibromofluoromethane 07/21/201150.050.1 100.1 77.7 120
Surr: Toluene-d8 07/21/201150.052.8 105.6 86 116
Page 99 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCSD-G110721-1
SampType: LCSD µg/KgUnits69790Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
1,1,1,2-Tetrachloroethane 07/21/20115.0 50.053.5 107.0 0.870 53.96
1,1,1-Trichloroethane 07/21/20115.0 50.053.2 106.5 4.120 55.49
1,1,2,2-Tetrachloroethane 07/21/20115.0 50.050.5 101.1 3.120 48.98
1,1,2-Trichloro-1,2,2-trifluoroethane 07/21/20115.0 50.050.7 101.4 3.470 52.48
1,1,2-Trichloroethane 07/21/20115.0 50.052.4 104.7 1.080 51.79
1,1-Dichloro-2-propanone 07/21/201150.0 125117 93.6 4.370 122.2
1,1-Dichloroethane 07/21/20115.0 50.048.9 97.7 2.150 49.92
1,1-Dichloroethene 07/21/20115.0 50.048.9 97.7 2.590 50.14
1,1-Dichloropropene 07/21/20115.0 50.050.8 101.5 4.050 52.85
1,2,3-Trichlorobenzene 07/21/20115.0 50.054.8 109.5 3.500 56.72
1,2,3-Trichloropropane 07/21/201110.0 50.052.3 104.6 0.270 52.14
1,2,3-Trimethylbenzene 07/21/20115.0 50.053.2 106.5 2.450 54.57
1,2,4-Trichlorobenzene 07/21/20115.0 50.057.3 114.5 5.800 60.68
1,2,4-Trimethylbenzene 07/21/20115.0 50.054.4 108.7 1.590 55.23
1,2-Dibromo-3-chloropropane 07/21/20115.0 50.051.7 103.4 5.690 54.72
1,2-Dibromoethane 07/21/20115.0 50.053.8 107.5 1.460 52.98
1,2-Dichlorobenzene 07/21/20115.0 50.052.9 105.8 2.130 54.03
1,2-Dichloroethane 07/21/20115.0 50.055.7 111.4 2.530 57.14
1,2-Dichloropropane 07/21/20115.0 50.046.3 92.6 2.540 47.49
1,3,5-Trimethylbenzene 07/21/20115.0 50.052.2 104.5 0.900 52.70
1,3-Dichlorobenzene 07/21/20115.0 50.054.6 109.1 1.780 55.53
1,3-Dichloropropane 07/21/20115.0 50.052.3 104.6 0.950 52.80
1,4-Dichlorobenzene 07/21/20115.0 50.053.3 106.7 2.790 54.84
1-Chlorobutane 07/21/20115.0 50.053.7 107.5 1.120 53.14
2,2-Dichloropropane 07/21/20115.0 50.052.7 105.4 4.650 55.22
2-Butanone 07/21/201150.0 125135 107.7 0.640 135.5
2-Chlorotoluene 07/21/20115.0 50.054.1 108.2 0.970 54.64
2-Hexanone 07/21/201150.0 125133 106.3 0.490 132.2
2-Nitropropane 07/21/201150.0 500510 101.9 3.970 530.3
4-Chlorotoluene 07/21/20115.0 50.054.9 109.8 1.890 55.95
4-Methyl-2-pentanone 07/21/201150.0 125120 96.2 2.270 123.0
Acetone 07/21/201150.0 125185 148.1 2.840 190.5
Acrylonitrile 07/21/201110.0 50.042.7 85.5 1.580 43.41
Allyl chloride 07/21/20115.0 50.052.8 105.7 5.840 56.01
Benzene 07/21/20111.0 50.048.4 96.7 0.970 48.83
Bromobenzene 07/21/20115.0 50.053.5 107.0 0.060 53.55
Bromochloromethane 07/21/20115.0 50.049.3 98.5 2.550 50.53
Bromodichloromethane 07/21/20115.0 50.053.5 107.1 3.900 55.66
Bromoform 07/21/20115.0 50.055.3 110.7 1.490 56.17
Bromomethane 07/21/201110.0 50.046.4 92.7 12.060 52.32
Carbon disulfide 07/21/20115.0 50.047.0 94.0 3.550 48.68
Carbon tetrachloride 07/21/20115.0 50.052.9 105.8 4.980 55.62
Chlorobenzene 07/21/20115.0 50.052.4 104.7 1.270 53.03
Chloroethane 07/21/201110.0 50.047.3 94.6 5.850 50.16
Chloroform 07/21/20115.0 50.051.9 103.7 2.640 53.26
Chloromethane 07/21/201110.0 50.042.4 84.8 10.460 47.08
cis-1,2-Dichloroethene 07/21/20115.0 50.048.4 96.7 0.190 48.27
Page 100 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCSD-G110721-1
SampType: LCSD µg/KgUnits69790Batch RPD Limit 40
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
cis-1,3-Dichloropropene 07/21/20114.0 50.050.8 101.6 1.490 51.54
Cyclohexanone 07/21/2011100 250224 89.7 0.050 224.1
Dibromochloromethane 07/21/20115.0 50.055.6 111.3 2.070 54.51
Dibromomethane 07/21/20115.0 50.050.8 101.6 3.630 52.69
Dichlorodifluoromethane 07/21/201110.0 50.036.9 73.7 16.910 43.67
Ethyl acetate J 07/21/201150.0 50.047 93.6 0.000 47.41
Ethyl ether 07/21/20115.0 50.045.3 90.5 0.780 44.92
Ethyl methacrylate 07/21/20115.0 50.052.6 105.2 2.660 51.20
Ethylbenzene 07/21/20115.0 50.053.1 106.1 1.760 54.01
Heptane 07/21/201120.0 50.049.6 99.2 1.900 50.53
Hexachlorobutadiene 07/21/20115.0 50.055.1 110.2 6.020 58.51
Hexachloroethane 07/21/20115.0 50.049.7 99.4 0.640 50.04
Iodomethane 07/21/201110.0 50.045.6 91.2 4.830 47.88
Isopropylbenzene 07/21/20115.0 50.054.0 108.0 4.150 56.30
m,p-Xylenes 07/21/20115.0 100109 108.7 1.950 110.8
Methacrylonitrile J 07/21/201150.0 50.046 92.9 0.000 46.67
Methyl Methacrylate 07/21/20115.0 50.047.4 94.8 0.000 47.42
Methyl tert-butyl ether 07/21/20112.0 50.050.1 100.1 1.250 49.45
Methylacrylate 07/21/201110.0 50.046.3 92.7 2.180 45.34
Methylene chloride 07/21/20115.0 50.046.6 93.2 6.060 49.50
Naphthalene 07/21/201110.0 50.049.1 98.2 5.000 51.64
n-Butylbenzene 07/21/20115.0 50.056.2 112.5 4.980 59.12
n-Hexane 07/21/201120.0 50.047.7 95.3 0.750 48.03
Nitrobenzene 07/21/2011100 500223 44.5 9.250 244.2
n-Propylbenzene 07/21/20115.0 50.054.6 109.3 0.660 54.99
o-Xylene 07/21/20115.0 50.054.7 109.3 3.200 56.44
Pentachloroethane 07/21/20115.0 50.055.0 110.0 0.160 55.11
p-Isopropyltoluene 07/21/20115.0 50.052.4 104.8 1.230 53.04
Propionitrile 07/21/201150.0 500435 87.1 5.810 461.4
sec-Butylbenzene 07/21/20115.0 50.053.7 107.4 1.090 54.31
Styrene 07/21/20115.0 50.052.8 105.5 2.470 54.07
tert-Butylbenzene 07/21/20115.0 50.054.6 109.1 2.030 55.69
Tetrachloroethene 07/21/20115.0 50.056.0 111.9 1.050 56.55
Tetrahydrofuran J 07/21/201150.0 50.039 77.4 0.000 40.13
Toluene 07/21/20115.0 50.051.3 102.7 0.640 51.67
trans-1,2-Dichloroethene 07/21/20115.0 50.050.4 100.7 0.950 50.84
trans-1,3-Dichloropropene 07/21/20114.0 50.055.2 110.4 0.430 55.42
Trichloroethene 07/21/20115.0 50.050.2 100.5 0.240 50.37
Trichlorofluoromethane 07/21/20115.0 50.055.4 110.9 8.380 60.30
Vinyl acetate 07/21/201150.0 50.050.8 101.6 1.570 50.01
Vinyl chloride 07/21/20112.0 50.046.8 93.5 8.790 51.05
Surr: 1,2-Dichloroethane-d4 07/21/201150.054.6 109.2
Surr: 4-Bromofluorobenzene 07/21/201150.052.7 105.5
Surr: Dibromofluoromethane 07/21/201150.050.0 100.1
Surr: Toluene-d8 07/21/201150.053.2 106.4
Page 101 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCS-G110721-1
SampType: LCS µg/KgUnits69790Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
1,1,1,2-Tetrachloroethane 07/21/20115.0 50.054.0 107.90 0 200
1,1,1-Trichloroethane 07/21/20115.0 50.055.5 111.00 85.6 124
1,1,2,2-Tetrachloroethane 07/21/20115.0 50.049.0 98.00 0 200
1,1,2-Trichloro-1,2,2-trifluoroethane 07/21/20115.0 50.052.5 105.00 0 200
1,1,2-Trichloroethane 07/21/20115.0 50.051.8 103.60 0 200
1,1-Dichloro-2-propanone 07/21/201150.0 125122 97.80 0 200
1,1-Dichloroethane 07/21/20115.0 50.049.9 99.80 0 200
1,1-Dichloroethene 07/21/20115.0 50.050.1 100.30 60.1 131
1,1-Dichloropropene 07/21/20115.0 50.052.8 105.70 0 200
1,2,3-Trichlorobenzene 07/21/20115.0 50.056.7 113.40 0 200
1,2,3-Trichloropropane 07/21/201110.0 50.052.1 104.30 0 200
1,2,3-Trimethylbenzene 07/21/20115.0 50.054.6 109.10 0 200
1,2,4-Trichlorobenzene 07/21/20115.0 50.060.7 121.40 0 200
1,2,4-Trimethylbenzene 07/21/20115.0 50.055.2 110.50 0 200
1,2-Dibromo-3-chloropropane 07/21/20115.0 50.054.7 109.40 0 200
1,2-Dibromoethane 07/21/20115.0 50.053.0 106.00 86.9 119
1,2-Dichlorobenzene 07/21/20115.0 50.054.0 108.10 88 119
1,2-Dichloroethane 07/21/20115.0 50.057.1 114.30 73 117
1,2-Dichloropropane 07/21/20115.0 50.047.5 95.00 0 200
1,3,5-Trimethylbenzene 07/21/20115.0 50.052.7 105.40 0 200
1,3-Dichlorobenzene 07/21/20115.0 50.055.5 111.10 85.8 125
1,3-Dichloropropane 07/21/20115.0 50.052.8 105.60 0 200
1,4-Dichlorobenzene 07/21/20115.0 50.054.8 109.70 84.5 124
1-Chlorobutane 07/21/20115.0 50.053.1 106.30 0 200
2,2-Dichloropropane 07/21/20115.0 50.055.2 110.40 0 200
2-Butanone 07/21/201150.0 125135 108.40 45.3 136
2-Chlorotoluene 07/21/20115.0 50.054.6 109.30 0 200
2-Hexanone 07/21/201150.0 125132 105.80 0 200
2-Nitropropane 07/21/201150.0 500530 106.10 0 200
4-Chlorotoluene 07/21/20115.0 50.056.0 111.90 0 200
4-Methyl-2-pentanone 07/21/201150.0 125123 98.40 0 200
Acetone 07/21/201150.0 125190 152.40 0 200
Acrylonitrile 07/21/201110.0 50.043.4 86.80 0 200
Allyl chloride 07/21/20115.0 50.056.0 112.00 0 200
Benzene 07/21/20111.0 50.048.8 97.70 73.9 109
Bromobenzene 07/21/20115.0 50.053.6 107.10 0 200
Bromochloromethane 07/21/20115.0 50.050.5 101.10 0 200
Bromodichloromethane 07/21/20115.0 50.055.7 111.30 91.3 126
Bromoform 07/21/20115.0 50.056.2 112.30 0 200
Bromomethane 07/21/201110.0 50.052.3 104.60 0 200
Carbon disulfide 07/21/20115.0 50.048.7 97.40 0 200
Carbon tetrachloride 07/21/20115.0 50.055.6 111.20 83.3 127
Chlorobenzene 07/21/20115.0 50.053.0 106.10 85.8 116
Chloroethane 07/21/201110.0 50.050.2 100.30 0 200
Chloroform 07/21/20115.0 50.053.3 106.50 80 113
Chloromethane 07/21/201110.0 50.047.1 94.20 0 200
cis-1,2-Dichloroethene 07/21/20115.0 50.048.3 96.50 0 200
Page 102 of 104
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
SW-846 5035, 8260B, VOLATILE ORGANIC COMPOUNDS BY GC/MS
SampID: LCS-G110721-1
SampType: LCS µg/KgUnits69790Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
cis-1,3-Dichloropropene 07/21/20114.0 50.051.5 103.10 0 200
Cyclohexanone 07/21/2011100 250224 89.60 0 200
Dibromochloromethane 07/21/20115.0 50.054.5 109.00 89.1 119
Dibromomethane 07/21/20115.0 50.052.7 105.40 0 200
Dichlorodifluoromethane 07/21/201110.0 50.043.7 87.30 0 200
Ethyl acetate J 07/21/201150.0 50.047 94.80 0 200
Ethyl ether 07/21/20115.0 50.044.9 89.80 0 200
Ethyl methacrylate 07/21/20115.0 50.051.2 102.40 0 200
Ethylbenzene 07/21/20115.0 50.054.0 108.00 84.1 115
Heptane 07/21/201120.0 50.050.5 101.10 0 200
Hexachlorobutadiene 07/21/20115.0 50.058.5 117.00 0 200
Hexachloroethane 07/21/20115.0 50.050.0 100.10 0 200
Iodomethane 07/21/201110.0 50.047.9 95.80 0 200
Isopropylbenzene 07/21/20115.0 50.056.3 112.60 0 200
m,p-Xylenes 07/21/20115.0 100111 110.80 79.1 111
Methacrylonitrile J 07/21/201150.0 50.047 93.30 0 200
Methyl Methacrylate 07/21/20115.0 50.047.4 94.80 0 200
Methyl tert-butyl ether 07/21/20112.0 50.049.4 98.90 80 128
Methylacrylate 07/21/201110.0 50.045.3 90.70 0 200
Methylene chloride 07/21/20115.0 50.049.5 99.00 73.9 116
Naphthalene 07/21/201110.0 50.051.6 103.30 73.1 135
n-Butylbenzene 07/21/20115.0 50.059.1 118.20 0 200
n-Hexane 07/21/201120.0 50.048.0 96.10 0 200
Nitrobenzene 07/21/2011100 500244 48.80 0 200
n-Propylbenzene 07/21/20115.0 50.055.0 110.00 0 200
o-Xylene 07/21/20115.0 50.056.4 112.90 82 117
Pentachloroethane 07/21/20115.0 50.055.1 110.20 0 200
p-Isopropyltoluene 07/21/20115.0 50.053.0 106.10 0 200
Propionitrile 07/21/201150.0 500461 92.30 0 200
sec-Butylbenzene 07/21/20115.0 50.054.3 108.60 0 200
Styrene 07/21/20115.0 50.054.1 108.10 0 200
tert-Butylbenzene 07/21/20115.0 50.055.7 111.40 0 200
Tetrachloroethene 07/21/20115.0 50.056.6 113.10 74.6 115
Tetrahydrofuran J 07/21/201150.0 50.040 80.30 0 200
Toluene 07/21/20115.0 50.051.7 103.30 79.1 112
trans-1,2-Dichloroethene 07/21/20115.0 50.050.8 101.70 0 200
trans-1,3-Dichloropropene 07/21/20114.0 50.055.4 110.80 0 200
Trichloroethene 07/21/20115.0 50.050.4 100.70 81 111
Trichlorofluoromethane 07/21/20115.0 50.060.3 120.60 0 200
Vinyl acetate 07/21/201150.0 50.050.0 100.00 0 200
Vinyl chloride 07/21/20112.0 50.051.0 102.10 0 200
Surr: 1,2-Dichloroethane-d4 07/21/201150.057.1 114.2 72.2 131
Surr: 4-Bromofluorobenzene 07/21/201150.053.8 107.6 82.1 116
Surr: Dibromofluoromethane 07/21/201150.050.8 101.6 77.7 120
Surr: Toluene-d8 07/21/201150.052.6 105.1 86 116
Page 103 of 104
Receiving Check List
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 29-Jul-11
Work Order: 11070610
http://www.teklabinc.com/
Received By: DBCarrier: Michael Flora
Completed by: Reviewed by:
On:
15-Jul-11
On:
18-Jul-11
Shipping container/cooler in good condition? Yes No Not Present
Chain of custody present? Yes No
Chain of custody signed when relinquished and received? Yes No
Chain of custody agrees with sample labels? Yes No
Samples in proper container/bottle? Yes No
Sample containers intact? Yes No
Sufficient sample volume for indicated test? Yes No
All samples received within holding time? Yes No
Container/Temp Blank temperature in compliance? Yes No
Temp °C 8.8
When thermal preservation is required, samples are compliant with a temperature between 0.1°C - 6.0°C, or when samples are received on ice the same day as collected.
Any No responses must be detailed below or on the COC.
The samples were out of temperature compliance upon receipt. Per Michael Flora, continue with analyses out of temperature compliance. DB 7/15/11
Per Leslie Hoosier, add TCL list of metals to analysis (1 day TAT). 7/26/11 HAW
Water - vials have zero headspace? Yes No No VOA vials
Water - pH acceptable upon receipt? Yes No
Type of thermal preservation? None Ice Blue Ice Dry Ice
Chain of custody 1 Extra pages included 12
Reported field parameters measured: Field Lab NA
Pages to follow:
Water - TOX containers have zero headspace? Yes No No TOX containers
Timothy W. Mathis Elizabeth A. Hurley
Page 104 of 104
ANALYTICAL REPORT
July 25, 2011
Page 1 of 12Work Order: 11G0968
Project :
Project Number:
Subcontract - HW Project
11070610
Report To
Heather White
Teklab, Inc.
Collinsville, IL 62234
5445 Horseshoe Lake Road
Work Order Information
Date Received: 07/20/2011 10:15AM
Collector:
Phone: (618) 344-1004
PO Number: 16874
Analyte Result MRL Batch Method Analyst Analyzed Qualifier
11070610-001 07/13/11 10:00Collected: 11G0968-01 Matrix:Soil
Dalapon mg/kg dry EPPEPA 8151A0.05 07/22/11 21:06<0.05 1G12046
3,5-Dichlorobenzoic acid mg/kg dry EPPEPA 8151A0.05 07/22/11 21:06<0.05 1G12046
Dicamba mg/kg dry EPPEPA 8151A0.05 07/22/11 21:06<0.05 1G12046
Dichlorprop mg/kg dry EPPEPA 8151A0.05 07/22/11 21:06<0.05 1G12046
2,4-D mg/kg dry EPPEPA 8151A0.05 07/22/11 21:06<0.05 1G12046
Pentachlorophenol mg/kg dry EPPEPA 8151A0.05 07/22/11 21:06<0.05 1G12046
2,4,5-TP (Silvex) mg/kg dry EPPEPA 8151A0.05 07/22/11 21:06<0.05 1G12046
Chloramben mg/kg dry EPPEPA 8151A0.05 07/22/11 21:06<0.05 1G12046
2,4,5-T mg/kg dry EPPEPA 8151A0.05 07/22/11 21:06<0.05 1G12046
2,4-DB mg/kg dry EPPEPA 8151A0.05 07/22/11 21:06<0.05 1G12046
Bentazon mg/kg dry EPPEPA 8151A0.05 07/22/11 21:06<0.05 1G12046
Picloram mg/kg dry EPPEPA 8151A0.05 07/22/11 21:06<0.05 1G12046
Dinoseb mg/kg dry EPPEPA 8151A0.05 07/22/11 21:06<0.05 1G12046
DCPA mg/kg dry EPPEPA 8151A0.05 07/22/11 21:06<0.05 1G12046
Acifluorfen mg/kg dry EPPEPA 8151A0.05 07/22/11 21:06<0.05 1G12046
Surrogate: 2,5-Dichlorobenzoic Acid 105 % 24-140 07/22/11 21:06EPP
0.1%% Solids SM 2540 G MAV 07/20/11 16:4284.1 1G12048
11070610-002 07/13/11 11:30Collected: 11G0968-02 Matrix:Soil
Dalapon mg/kg dry EPPEPA 8151A0.05 07/22/11 21:53<0.05 1G12046
3,5-Dichlorobenzoic acid mg/kg dry EPPEPA 8151A0.05 07/22/11 21:53<0.05 1G12046
Dicamba mg/kg dry EPPEPA 8151A0.05 07/22/11 21:53<0.05 1G12046
Dichlorprop mg/kg dry EPPEPA 8151A0.05 07/22/11 21:53<0.05 1G12046
2,4-D mg/kg dry EPPEPA 8151A0.05 07/22/11 21:53<0.05 1G12046
Pentachlorophenol mg/kg dry EPPEPA 8151A0.05 07/22/11 21:53<0.05 1G12046
2,4,5-TP (Silvex) mg/kg dry EPPEPA 8151A0.05 07/22/11 21:53<0.05 1G12046
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0968
July 25, 2011
Page 2 of 12
Analyte Result MRL Batch Method Analyst Analyzed Qualifier
11070610-002 07/13/11 11:30Collected: 11G0968-02 Matrix:Soil
Chloramben mg/kg dry EPPEPA 8151A0.05 07/22/11 21:53<0.05 1G12046
2,4,5-T mg/kg dry EPPEPA 8151A0.05 07/22/11 21:53<0.05 1G12046
2,4-DB mg/kg dry EPPEPA 8151A0.05 07/22/11 21:53<0.05 1G12046
Bentazon mg/kg dry EPPEPA 8151A0.05 07/22/11 21:53<0.05 1G12046
Picloram mg/kg dry EPPEPA 8151A0.05 07/22/11 21:53<0.05 1G12046
Dinoseb mg/kg dry EPPEPA 8151A0.05 07/22/11 21:53<0.05 1G12046
DCPA mg/kg dry EPPEPA 8151A0.05 07/22/11 21:53<0.05 1G12046
Acifluorfen mg/kg dry EPPEPA 8151A0.05 07/22/11 21:53<0.05 1G12046
Surrogate: 2,5-Dichlorobenzoic Acid 76.5 % 24-140 07/22/11 21:53EPP
0.1%% Solids SM 2540 G MAV 07/20/11 16:4286.4 1G12048
11070610-003 07/13/11 13:15Collected: 11G0968-03 Matrix:Soil
Dalapon mg/kg dry EPPEPA 8151A0.05 07/22/11 22:41<0.05 1G12046
3,5-Dichlorobenzoic acid mg/kg dry EPPEPA 8151A0.05 07/22/11 22:41<0.05 1G12046
Dicamba mg/kg dry EPPEPA 8151A0.05 07/22/11 22:41<0.05 1G12046
Dichlorprop mg/kg dry EPPEPA 8151A0.05 07/22/11 22:41<0.05 1G12046
2,4-D mg/kg dry EPPEPA 8151A0.05 07/22/11 22:41<0.05 1G12046
Pentachlorophenol mg/kg dry EPPEPA 8151A0.05 07/22/11 22:41<0.05 1G12046
2,4,5-TP (Silvex) mg/kg dry EPPEPA 8151A0.05 07/22/11 22:41<0.05 1G12046
Chloramben mg/kg dry EPPEPA 8151A0.05 07/22/11 22:41<0.05 1G12046
2,4,5-T mg/kg dry EPPEPA 8151A0.05 07/22/11 22:41<0.05 1G12046
2,4-DB mg/kg dry EPPEPA 8151A0.05 07/22/11 22:41<0.05 1G12046
Bentazon mg/kg dry EPPEPA 8151A0.05 07/22/11 22:41<0.05 1G12046
Picloram mg/kg dry EPPEPA 8151A0.05 07/22/11 22:41<0.05 1G12046
Dinoseb mg/kg dry EPPEPA 8151A0.05 07/22/11 22:41<0.05 1G12046
DCPA mg/kg dry EPPEPA 8151A0.05 07/22/11 22:41<0.05 1G12046
Acifluorfen mg/kg dry EPPEPA 8151A0.05 07/22/11 22:41<0.05 1G12046
Surrogate: 2,5-Dichlorobenzoic Acid 84.2 % 24-140 07/22/11 22:41EPP
0.1%% Solids SM 2540 G MAV 07/20/11 16:4283.9 1G12048
11070610-004 07/13/11 14:30Collected: 11G0968-04 Matrix:Soil
Dalapon mg/kg dry EPPEPA 8151A0.05 07/22/11 23:28<0.05 1G12046
3,5-Dichlorobenzoic acid mg/kg dry EPPEPA 8151A0.05 07/22/11 23:28<0.05 1G12046
Dicamba mg/kg dry EPPEPA 8151A0.05 07/22/11 23:28<0.05 1G12046
Dichlorprop mg/kg dry EPPEPA 8151A0.05 07/22/11 23:28<0.05 1G12046
2,4-D mg/kg dry EPPEPA 8151A0.05 07/22/11 23:28<0.05 1G12046
Pentachlorophenol mg/kg dry EPPEPA 8151A0.05 07/22/11 23:28<0.05 1G12046
2,4,5-TP (Silvex) mg/kg dry EPPEPA 8151A0.05 07/22/11 23:28<0.05 1G12046
Chloramben mg/kg dry EPPEPA 8151A0.05 07/22/11 23:28<0.05 1G12046
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0968
July 25, 2011
Page 3 of 12
Analyte Result MRL Batch Method Analyst Analyzed Qualifier
11070610-004 07/13/11 14:30Collected: 11G0968-04 Matrix:Soil
2,4,5-T mg/kg dry EPPEPA 8151A0.05 07/22/11 23:28<0.05 1G12046
2,4-DB mg/kg dry EPPEPA 8151A0.05 07/22/11 23:28<0.05 1G12046
Bentazon mg/kg dry EPPEPA 8151A0.05 07/22/11 23:28<0.05 1G12046
Picloram mg/kg dry EPPEPA 8151A0.05 07/22/11 23:28<0.05 1G12046
Dinoseb mg/kg dry EPPEPA 8151A0.05 07/22/11 23:28<0.05 1G12046
DCPA mg/kg dry EPPEPA 8151A0.05 07/22/11 23:28<0.05 1G12046
Acifluorfen mg/kg dry EPPEPA 8151A0.05 07/22/11 23:28<0.05 1G12046
Surrogate: 2,5-Dichlorobenzoic Acid 89.3 % 24-140 07/22/11 23:28EPP
0.1%% Solids SM 2540 G MAV 07/20/11 16:4288.8 1G12048
11070610-005 07/13/11 15:30Collected: 11G0968-05 Matrix:Soil
Dalapon mg/kg dry EPPEPA 8151A0.05 07/23/11 0:15<0.05 1G12046
3,5-Dichlorobenzoic acid mg/kg dry EPPEPA 8151A0.05 07/23/11 0:15<0.05 1G12046
Dicamba mg/kg dry EPPEPA 8151A0.05 07/23/11 0:15<0.05 1G12046
Dichlorprop mg/kg dry EPPEPA 8151A0.05 07/23/11 0:15<0.05 1G12046
2,4-D mg/kg dry EPPEPA 8151A0.05 07/23/11 0:15<0.05 1G12046
Pentachlorophenol mg/kg dry EPPEPA 8151A0.05 07/23/11 0:15<0.05 1G12046
2,4,5-TP (Silvex) mg/kg dry EPPEPA 8151A0.05 07/23/11 0:15<0.05 1G12046
Chloramben mg/kg dry EPPEPA 8151A0.05 07/23/11 0:15<0.05 1G12046
2,4,5-T mg/kg dry EPPEPA 8151A0.05 07/23/11 0:15<0.05 1G12046
2,4-DB mg/kg dry EPPEPA 8151A0.05 07/23/11 0:15<0.05 1G12046
Bentazon mg/kg dry EPPEPA 8151A0.05 07/23/11 0:15<0.05 1G12046
Picloram mg/kg dry EPPEPA 8151A0.05 07/23/11 0:15<0.05 1G12046
Dinoseb mg/kg dry EPPEPA 8151A0.05 07/23/11 0:15<0.05 1G12046
DCPA mg/kg dry EPPEPA 8151A0.05 07/23/11 0:15<0.05 1G12046
Acifluorfen mg/kg dry EPPEPA 8151A0.05 07/23/11 0:15<0.05 1G12046
Surrogate: 2,5-Dichlorobenzoic Acid 89.3 % 24-140 07/23/11 0:15EPP
0.1%% Solids SM 2540 G MAV 07/20/11 16:4279.5 1G12048
11070610-006 07/14/11 09:45Collected: 11G0968-06 Matrix:Soil
Dalapon mg/kg dry EPPEPA 8151A0.05 07/23/11 1:02<0.05 1G12046
3,5-Dichlorobenzoic acid mg/kg dry EPPEPA 8151A0.05 07/23/11 1:02<0.05 1G12046
Dicamba mg/kg dry EPPEPA 8151A0.05 07/23/11 1:02<0.05 1G12046
Dichlorprop mg/kg dry EPPEPA 8151A0.05 07/23/11 1:02<0.05 1G12046
2,4-D mg/kg dry EPPEPA 8151A0.05 07/23/11 1:02<0.05 1G12046
Pentachlorophenol mg/kg dry EPPEPA 8151A0.05 07/23/11 1:02<0.05 1G12046
2,4,5-TP (Silvex) mg/kg dry EPPEPA 8151A0.05 07/23/11 1:02<0.05 1G12046
Chloramben mg/kg dry EPPEPA 8151A0.05 07/23/11 1:02<0.05 1G12046
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0968
July 25, 2011
Page 4 of 12
Analyte Result MRL Batch Method Analyst Analyzed Qualifier
11070610-006 07/14/11 09:45Collected: 11G0968-06 Matrix:Soil
2,4,5-T mg/kg dry EPPEPA 8151A0.05 07/23/11 1:02<0.05 1G12046
2,4-DB mg/kg dry EPPEPA 8151A0.05 07/23/11 1:02<0.05 1G12046
Bentazon mg/kg dry EPPEPA 8151A0.05 07/23/11 1:02<0.05 1G12046
Picloram mg/kg dry EPPEPA 8151A0.05 07/23/11 1:02<0.05 1G12046
Dinoseb mg/kg dry EPPEPA 8151A0.05 07/23/11 1:02<0.05 1G12046
DCPA mg/kg dry EPPEPA 8151A0.05 07/23/11 1:02<0.05 1G12046
Acifluorfen mg/kg dry EPPEPA 8151A0.05 07/23/11 1:02<0.05 1G12046
Surrogate: 2,5-Dichlorobenzoic Acid 63.4 % 24-140 07/23/11 1:02EPP
0.1%% Solids SM 2540 G MAV 07/20/11 16:4278.3 1G12048
11070610-007 07/14/11 10:30Collected: 11G0968-07 Matrix:Soil
Dalapon mg/kg dry EPPEPA 8151A0.05 07/23/11 1:50<0.05 1G12046
3,5-Dichlorobenzoic acid mg/kg dry EPPEPA 8151A0.05 07/23/11 1:50<0.05 1G12046
Dicamba mg/kg dry EPPEPA 8151A0.05 07/23/11 1:50<0.05 1G12046
Dichlorprop mg/kg dry EPPEPA 8151A0.05 07/23/11 1:50<0.05 1G12046
2,4-D mg/kg dry EPPEPA 8151A0.05 07/23/11 1:50<0.05 1G12046
Pentachlorophenol mg/kg dry EPPEPA 8151A0.05 07/23/11 1:50<0.05 1G12046
2,4,5-TP (Silvex) mg/kg dry EPPEPA 8151A0.05 07/23/11 1:50<0.05 1G12046
Chloramben mg/kg dry EPPEPA 8151A0.05 07/23/11 1:50<0.05 1G12046
2,4,5-T mg/kg dry EPPEPA 8151A0.05 07/23/11 1:50<0.05 1G12046
2,4-DB mg/kg dry EPPEPA 8151A0.05 07/23/11 1:50<0.05 1G12046
Bentazon mg/kg dry EPPEPA 8151A0.05 07/23/11 1:50<0.05 1G12046
Picloram mg/kg dry EPPEPA 8151A0.05 07/23/11 1:50<0.05 1G12046
Dinoseb mg/kg dry EPPEPA 8151A0.05 07/23/11 1:50<0.05 1G12046
DCPA mg/kg dry EPPEPA 8151A0.05 07/23/11 1:50<0.05 1G12046
Acifluorfen mg/kg dry EPPEPA 8151A0.05 07/23/11 1:50<0.05 1G12046
Surrogate: 2,5-Dichlorobenzoic Acid 76.1 % 24-140 07/23/11 1:50EPP
0.1%% Solids SM 2540 G MAV 07/20/11 16:4284.0 1G12048
11070610-008 07/14/11 11:15Collected: 11G0968-08 Matrix:Soil
Dalapon mg/kg dry EPPEPA 8151A0.08 07/23/11 2:37<0.08 1G12046
3,5-Dichlorobenzoic acid mg/kg dry EPPEPA 8151A0.08 07/23/11 2:37<0.08 1G12046
Dicamba mg/kg dry EPPEPA 8151A0.08 07/23/11 2:37<0.08 1G12046
Dichlorprop mg/kg dry EPPEPA 8151A0.08 07/23/11 2:37<0.08 1G12046
2,4-D mg/kg dry EPPEPA 8151A0.08 07/23/11 2:37<0.08 1G12046
Pentachlorophenol mg/kg dry EPPEPA 8151A0.08 07/23/11 2:37<0.08 1G12046
2,4,5-TP (Silvex) mg/kg dry EPPEPA 8151A0.08 07/23/11 2:37<0.08 1G12046
Chloramben mg/kg dry EPPEPA 8151A0.08 07/23/11 2:37<0.08 1G12046
2,4,5-T mg/kg dry EPPEPA 8151A0.08 07/23/11 2:37<0.08 1G12046
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0968
July 25, 2011
Page 5 of 12
Analyte Result MRL Batch Method Analyst Analyzed Qualifier
11070610-008 07/14/11 11:15Collected: 11G0968-08 Matrix:Soil
2,4-DB mg/kg dry EPPEPA 8151A0.08 07/23/11 2:37<0.08 1G12046
Bentazon mg/kg dry EPPEPA 8151A0.08 07/23/11 2:37<0.08 1G12046
Picloram mg/kg dry EPPEPA 8151A0.08 07/23/11 2:37<0.08 1G12046
Dinoseb mg/kg dry EPPEPA 8151A0.08 07/23/11 2:37<0.08 1G12046
DCPA mg/kg dry EPPEPA 8151A0.08 07/23/11 2:37<0.08 1G12046
Acifluorfen mg/kg dry EPPEPA 8151A0.08 07/23/11 2:37<0.08 1G12046
Surrogate: 2,5-Dichlorobenzoic Acid 53.9 % 24-140 07/23/11 2:37EPP
0.1%% Solids SM 2540 G MAV 07/20/11 16:4264.8 1G12048
11070610-009 07/14/11 12:00Collected: 11G0968-09 Matrix:Soil
Dalapon mg/kg dry EPPEPA 8151A0.05 07/23/11 3:24<0.05 1G12046
3,5-Dichlorobenzoic acid mg/kg dry EPPEPA 8151A0.05 07/23/11 3:24<0.05 1G12046
Dicamba mg/kg dry EPPEPA 8151A0.05 07/23/11 3:24<0.05 1G12046
Dichlorprop mg/kg dry EPPEPA 8151A0.05 07/23/11 3:24<0.05 1G12046
2,4-D mg/kg dry EPPEPA 8151A0.05 07/23/11 3:24<0.05 1G12046
Pentachlorophenol mg/kg dry EPPEPA 8151A0.05 07/23/11 3:24<0.05 1G12046
2,4,5-TP (Silvex) mg/kg dry EPPEPA 8151A0.05 07/23/11 3:24<0.05 1G12046
Chloramben mg/kg dry EPPEPA 8151A0.05 07/23/11 3:24<0.05 1G12046
2,4,5-T mg/kg dry EPPEPA 8151A0.05 07/23/11 3:24<0.05 1G12046
2,4-DB mg/kg dry EPPEPA 8151A0.05 07/23/11 3:24<0.05 1G12046
Bentazon mg/kg dry EPPEPA 8151A0.05 07/23/11 3:24<0.05 1G12046
Picloram mg/kg dry EPPEPA 8151A0.05 07/23/11 3:24<0.05 1G12046
Dinoseb mg/kg dry EPPEPA 8151A0.05 07/23/11 3:24<0.05 1G12046
DCPA mg/kg dry EPPEPA 8151A0.05 07/23/11 3:24<0.05 1G12046
Acifluorfen mg/kg dry EPPEPA 8151A0.05 07/23/11 3:24<0.05 1G12046
Surrogate: 2,5-Dichlorobenzoic Acid 95.0 % 24-140 07/23/11 3:24EPP
0.1%% Solids SM 2540 G MAV 07/20/11 16:4280.9 1G12048
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0968
July 25, 2011
Page 6 of 12
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Determination of Chlorinated Phenoxy Herbicides - Quality Control
Keystone Laboratories, Inc. - Newton
Batch 1G12046 - EPA 8151A
Blank (1G12046-BLK1) Prepared: 07/20/11 Analyzed: 07/22/11
mg/kg wet 0.0760000 24-140Surrogate: 2,5-Dichlorobenzoic Acid 41.70.0317
Dalapon "ND 0.05
3,5-Dichlorobenzoic acid "ND 0.05
Dicamba "ND 0.05
Dichlorprop "ND 0.05
2,4-D "ND 0.05
Pentachlorophenol "ND 0.05
2,4,5-TP (Silvex) "ND 0.05
Chloramben "ND 0.05
2,4,5-T "ND 0.05
2,4-DB "ND 0.05
Bentazon "ND 0.05
Picloram "ND 0.05
Dinoseb "ND 0.05
DCPA "ND 0.05
Acifluorfen "ND 0.05
LCS (1G12046-BS1) Prepared: 07/20/11 Analyzed: 07/22/11
mg/kg wet 0.0760000 24-140Surrogate: 2,5-Dichlorobenzoic Acid 66.40.0505
Dalapon "0.081 0.05 0.208000 10-9339.1
3,5-Dichlorobenzoic acid "0.012 0.05 0.0160000 53-12971.9
Dicamba "0.013 0.05 0.0160000 38-12383.3
Dichlorprop "0.047 0.05 0.0480000 31-12797.9
2,4-D "0.032 0.05 0.0320000 23-12799.0
Pentachlorophenol "0.012 0.05 0.0160000 10-9372.9
2,4,5-TP (Silvex) "0.011 0.05 0.0160000 35-11667.7
Chloramben "0.006 0.05 0.0160000 10-9437.5
2,4,5-T "0.008 0.05 0.0160000 26-10449.0
2,4-DB "0.101 0.05 0.128000 42-12278.8
Bentazon "0.028 0.05 0.0320000 42-13389.1
Picloram "0.013 0.05 0.0160000 19-15779.2
Dinoseb "0.011 0.05 0.0320000 10-9033.9
DCPA "0.009 0.05 0.0160000 10-11754.2
Acifluorfen "0.013 0.05 0.0160000 24-11383.3
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0968
July 25, 2011
Page 7 of 12
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Determination of Chlorinated Phenoxy Herbicides - Quality Control
Keystone Laboratories, Inc. - Newton
Batch 1G12046 - EPA 8151A
LCS Dup (1G12046-BSD1) Prepared: 07/20/11 Analyzed: 07/22/11
mg/kg wet 0.0760000 24-140Surrogate: 2,5-Dichlorobenzoic Acid 70.20.0533
Dalapon "0.082 0.05 0.208000 3010-9339.4 0.816
3,5-Dichlorobenzoic acid "0.013 0.05 0.0160000 3053-12981.2
Dicamba "0.012 0.05 0.0160000 3038-12378.1 6.45
Dichlorprop "0.048 0.05 0.0480000 3031-127101 3.14
2,4-D "0.032 0.05 0.0320000 3023-127102 2.60
Pentachlorophenol "0.011 0.05 0.0160000 3010-9367.7 7.41
2,4,5-TP (Silvex) "0.010 0.05 0.0160000 3035-11664.6 4.72
Chloramben "0.006 0.05 0.0160000 3010-9434.4 8.70
2,4,5-T "0.008 0.05 0.0160000 3026-10449.0 0.00
2,4-DB "0.111 0.05 0.128000 3042-12287.0 9.90
Bentazon "0.029 0.05 0.0320000 3042-13390.1 1.16
Picloram "0.013 0.05 0.0160000 3019-15783.3 5.13
Dinoseb "0.007 0.05 0.0320000 30 QR-0210-9022.4 40.7
DCPA "0.010 0.05 0.0160000 3010-11765.6 19.1
Acifluorfen "0.016 0.05 0.0160000 3024-113103 21.2
Matrix Spike (1G12046-MS1) Prepared: 07/20/11 Analyzed: 07/22/11 Source: 11G0968-02
mg/kg dry 0.0879935 24-140Surrogate: 2,5-Dichlorobenzoic Acid 83.10.0731
Dalapon "0.185 0.05 0.240824 ND 19-15676.9
3,5-Dichlorobenzoic acid "0.016 0.05 0.0185250 ND 38.9-18184.4
Dicamba "0.017 0.05 0.0185250 ND 40-15391.7
Dichlorprop "0.057 0.05 0.0555748 ND 19.6-138102
2,4-D "0.035 0.05 0.0370499 ND 10-14694.3
Pentachlorophenol "0.014 0.05 0.0185250 ND 16-12777.1
2,4,5-TP (Silvex) "0.014 0.05 0.0185250 ND 31.2-15974.0
Chloramben "0.008 0.05 0.0185250 ND 10-13343.8
2,4,5-T "0.012 0.05 0.0185250 ND 16.4-15263.5
2,4-DB "0.152 0.05 0.148200 ND 35.3-156103
Bentazon "0.028 0.05 0.0370499 ND 10-15076.0
Picloram "0.012 0.05 0.0185250 ND 45-14663.5
Dinoseb "0.012 0.05 0.0370499 ND 10-9032.3
DCPA "0.008 0.05 0.0185250 ND 10-15142.7
Acifluorfen "0.020 0.05 0.0185250 ND 10-161110
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0968
July 25, 2011
Page 8 of 12
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Determination of Chlorinated Phenoxy Herbicides - Quality Control
Keystone Laboratories, Inc. - Newton
Batch 1G12046 - EPA 8151A
Reference (1G12046-SRM1) Prepared: 07/20/11 Analyzed: 07/22/11
mg/kg wet 0.0760000 24-140Surrogate: 2,5-Dichlorobenzoic Acid 92.50.0703
Dalapon "0.233 0.05 0.208000 70-130112
3,5-Dichlorobenzoic acid "0.017 0.05 0.0160000 70-130106
Dicamba "0.018 0.05 0.0160000 70-130110
Dichlorprop "0.047 0.05 0.0480000 70-13097.9
2,4-D "0.033 0.05 0.0320000 70-130103
Pentachlorophenol "0.017 0.05 0.0160000 70-130107
2,4,5-TP (Silvex) "0.018 0.05 0.0160000 70-130109
Chloramben "0.013 0.05 0.0160000 70-13083.3
2,4,5-T "0.015 0.05 0.0160000 70-13095.8
2,4-DB "0.137 0.05 0.128000 70-130107
Bentazon "0.029 0.05 0.0320000 70-13089.6
Picloram "0.019 0.05 0.0160000 70-130117
Dinoseb "0.034 0.05 0.0320000 70-130107
DCPA "0.018 0.05 0.0160000 70-130110
Acifluorfen "0.012 0.05 0.0160000 70-13078.1
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0968
July 25, 2011
Page 9 of 12
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Determination of Conventional Chemistry Parameters - Quality Control
Keystone Laboratories, Inc. - Newton
Batch 1G12048 - Wet Chem Preparation
Duplicate (1G12048-DUP1) Prepared & Analyzed: 07/20/11 Source: 11G0968-09
% Solids %80.1 0.1 80.9 201.06
ND = Non Detect; REC= Recovery; RPD= Relative Percent Difference
Certified Analyses included in this Report
CertificationsAnalyteMethod/Matrix
EPA 8151A in Soil
KS-NT,NELACDalapon
KS-NT,NELAC,SIA1XDicamba
NELACDichlorprop
KS-NT,NELAC,SIA1X2,4-D
KS-NT,NELAC,SIA1X2,4,5-TP (Silvex)
KS-NT,NELAC2,4,5-T
NELAC2,4-DB
KS-NT,NELACPicloram
KS-NT,NELACDinoseb
SIA1XAcifluorfen
SM 2540 G in Soil
SIA1X% Solids
Description Number ExpiresCode
E-10110Kansas Department of Health and Environment-KC 04/30/2012KS-KC
E-10287Kansas Department of Health and Environment 10/30/2011KS-NT
140Missouri Department of Natural Resources 04/30/2012MO-KC
IA001New Jersey Department of Environmental Protection 06/30/2011NELAC
95Iowa Department of Natural Resources 02/01/2012SIA1X
Notes and Definitions
QR-02 The RPD result exceeded the QC control limits; however, both percent recoveries were acceptable. Sample results for the QC
batch were accepted based on percent recoveries and completeness of QC data.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0968
July 25, 2011
Page 10 of 12
End of Report
Christine Dawson
Project Manager
Keystone Laboratories, Inc.
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0968
July 25, 2011
Page 11 of 12
COC Goes Here
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
Teklab, Inc.5445 Horseshoe Lake RoadCollinsville, IL 62234
Work Order: 11G0968
July 25, 2011
Page 12 of 12
COC Goes Here
The results in this report apply to the samples analyzed in accordance with the chain of custody document. This analytical report must be reproduced in
its entirety. Samples were preserved in accordance with 40 CFR for pH adjustment unless otherwise noted. MRL= Method Reporting Limit.
Phone 641-792-8451 600 East 17th Street South Fax 641-792-7989
Newton, IA 50208
http://www.teklabinc.com/
July 28, 2011
WorkOrder: 11071019A831-735002-012901-225Ameren Champaign 62409080120
RE:
Dear Pete Sazama:
TEKLAB, INC received 5 samples on 7/1/2011 3:50:00 PM for the analysis presented in the following report.
Samples are analyzed on an as received basis unless otherwise requested and documented. The sample results contained in this report relate only to the requested analytes of interest as directed on the chain of custody. NELAP accredited fields of testing are indicated by the letters NELAP under the Certification column.
All tests are performed in the Collinsville, IL laboratory unless otherwise noted in the Case Narrative.
All quality control criteria applicable to the test methods employed for this project have been satisfactorily met and are in accordance with NELAP except where noted. The following report shall not be reproduced, except in full, without the written approval of Teklab, Inc.
If you have any questions regarding these tests results, please feel free to call.
Sincerely,
210 West Sand Bank RoadColumbia, IL 62236-0230
(618) 281-7173(618) 281-5120
TEL:FAX:
Pete SazamaPSC Industrial Outsourcing, LP
Heather A. WhiteProject Manager(618)344-1004 ex [email protected]
Page 1 of 14
This reporting package includes the following:
Report Contents
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 28-Jul-11
Work Order: 11071019
http://www.teklabinc.com/
Cover Letter 1
Report Contents 2
Definitions 3
Case Narrative 4
Laboratory Results 5
Sample Summary 10
Dates Report 11
Quality Control Results 12
Chain of Custody Appended
Page 2 of 14
____TeklabHdrP
Definitions
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 28-Jul-11
Work Order: 11071019
http://www.teklabinc.com/
Abbr DefinitionCCV Continuing calibration verification is a check of a standard to determine the state of calibration of an instrument between recalibration.
DF Dilution factor is the dilution performed during analysis only and does not take into account any dilutions made during sample preparation. The reported result is final and includes all dilutions factors.
DNI Did not ignite
DUP Laboratory duplicate is an aliquot of a sample taken from the same container under laboratory conditions for independent processing and analysis independently of the original aliquot.
ICV Initial calibration verification is a check of a standard to determine the state of calibration of an instrument before sample analysis is initiated.
IDPH IL Dept. of Public Health
LCS Laboratory control sample, spiked with verified known amounts of analytes, is analyzed exactly like a sample to establish intra-laboratory or analyst specific precision and bias or to assess the performance of all or a portion of the measurement system. The acceptable recovery range is in the QC Package (provided upon request).
LCSD Laboratory control sample duplicate is a replicate laboratory control sample that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in the QC Package (provided upon request).
MB Method blank is a sample of a matrix similar to the batch of associated sample (when available) that is free from the analytes of interest and is processed simultaneously with and under the same conditions as samples through all steps of the analytical procedures, and in which no target analytes or interferences should present at concentrations that impact the analytical results for sample analyses.
MDL Method detection limit means the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix type containing the analyte.
MS Matrix spike is an aliquot of matrix fortified (spiked) with known quantities of specific analytes that is subjected to the entire analytical procedures in order to determine the effect of the matrix on an approved test method’s recovery system. The acceptable recovery range is listed in the QC Package (provided upon request).
MSD Matrix spike duplicate means a replicate matrix spike that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in the QC Package (provided upon request).
MW Molecular weight
ND Not Detected at the Reporting Limit
NELAP NELAP Accredited
PQL Practical quantitation limit means the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine laboratory operation conditions. The acceptable recovery range is listed in the QC Package (provided upon request).
RL The reporting limit the lowest level that the data is displayed in the final report. The reporting limit may vary according to customer request or sample dilution. The reporting limit may not be less than the MDL.
RPD Relative percent difference is a calculated difference between two recoveries (ie. MS/MSD). The acceptable recovery limit is listed in the QC Package (provided upon request).
SPK The spike is a known mass of target analyte added to a blank sample or sub-sample; used to determine recovery deficiency or for other quality control purposes.
Surr Surrogates are compounds which are similar to the analytes of interest in chemical composition and behavior in the analytical process, but which are not normally found in environmental samples.
TNTC Too numerous to count ( > 200 CFU )
Qualifiers# - Unknown hydrocarbon B - Analyte detected in associated Method Blank
E - Value above quantitation range H - Holding times exceeded
J - Analyte detected below quantitation limits M - Manual Integration used to determine area response
ND - Not Detected at the Reporting Limit R - RPD outside accepted recovery limits
S - Spike Recovery outside recovery limits X - Value exceeds Maximum Contaminant Level
Page 3 of 14
Case Narrative
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 28-Jul-11
Work Order: 11071019
http://www.teklabinc.com/
Cooler Receipt Temp: °C
Additional analyses to WO# 11070042.
NELAPState Cert # Exp Date LabDept
Locations and Accreditations
____________________________________Collinsville
Address 5445 Horseshoe Lake Road
Collinsville, IL 62234-7425
Phone (618) 344-1004
Fax (618) 344-1005
Email [email protected]
____________________________________Springfield
Address 3920 Pintail Dr
Springfield, IL 62711-9415
Phone (217) 698-1004
Fax (217) 698-1005
Email [email protected]
____________________________________Kansas City
Address 8421 Nieman Road
Lenexa, KS 66214
Phone (913) 541-1998
Fax (913) 541-1998
Email [email protected]
Illinois 100226 1/31/2012 CollinsvilleNELAPIEPA
Kansas E-10374 1/31/2012 CollinsvilleNELAPKDHE
Louisiana 166493 6/30/2012 CollinsvilleNELAPLDEQ
Louisiana 166578 6/30/2012 SpringfieldNELAPLDEQ
Arkansas 88-0966 3/14/2012 CollinsvilleADEQ
Illinois 17584 4/30/2012 CollinsvilleIDPH
Kentucky 0073 5/26/2012 CollinsvilleUST
Missouri 00930 4/13/2013 CollinsvilleMDNR
Oklahoma 9978 8/31/2011 CollinsvilleODEQ
Page 4 of 14
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 28-Jul-11
Work Order: 11071019
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/29/2011 16:00
Lab ID: 11071019-001 Client Sample ID: SBA-C3-01 (5-6)
Matrix: SOLID
Batch
SW-846 3050B, 6010B, METALS BY ICPAluminum 07/27/2011 13:554.72 mg/Kg-dry 120600NELAP 69916
Antimony 07/27/2011 11:004.90 mg/Kg-dry 1< 4.90NELAP 69908
Beryllium 07/27/2011 13:550.09 mg/Kg-dry 10.93NELAP 69916
Calcium 07/27/2011 13:554.72 mg/Kg-dry 118500NELAP 69916
Cobalt 07/27/2011 13:550.94 mg/Kg-dry 111.0NELAP 69916
Copper 07/27/2011 13:550.94 mg/Kg-dry 123.2NELAP 69916
Iron 07/27/2011 13:551.89 mg/Kg-dry 128200NELAP 69916
Magnesium 07/27/2011 13:550.94 mg/Kg-dry 111100NELAP 69916
Manganese 07/27/2011 13:550.47 mg/Kg-dry 1684NELAP 69916
Nickel 07/27/2011 13:550.94 mg/Kg-dry 129.8NELAP 69916
Potassium 07/27/2011 13:559.43 mg/Kg-dry 12900NELAP 69916
Sodium 07/27/2011 13:554.72 mg/Kg-dry 1203NELAP 69916
Vanadium 07/27/2011 13:550.94 mg/Kg-dry 134.4NELAP 69916
Zinc 07/27/2011 13:550.94 mg/Kg-dry 181.6NELAP 69916
SW-846 3050B, METALS BY GFAAThallium 7841 07/28/2011 8:280.185 mg/Kg-dry 10.435NELAP 69917
Page 5 of 14
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 28-Jul-11
Work Order: 11071019
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 8:00
Lab ID: 11071019-002 Client Sample ID: SBA-B4-01 (5-6)
Matrix: SOLID
Batch
SW-846 3050B, 6010B, METALS BY ICPAluminum S 07/27/2011 14:014.55 mg/Kg-dry 118600NELAP 69916
Antimony 07/27/2011 11:185.00 mg/Kg-dry 1< 5.00NELAP 69908
Beryllium 07/27/2011 14:010.09 mg/Kg-dry 10.76NELAP 69916
Calcium S 07/27/2011 14:014.55 mg/Kg-dry 133600NELAP 69916
Cobalt 07/27/2011 14:010.91 mg/Kg-dry 112.1NELAP 69916
Copper 07/27/2011 14:010.91 mg/Kg-dry 121.5NELAP 69916
Iron S 07/27/2011 14:011.82 mg/Kg-dry 126600NELAP 69916
Magnesium S 07/27/2011 14:010.91 mg/Kg-dry 113100NELAP 69916
Manganese S 07/27/2011 14:010.45 mg/Kg-dry 1821NELAP 69916
Nickel 07/27/2011 14:010.91 mg/Kg-dry 127.3NELAP 69916
Potassium S 07/27/2011 14:019.09 mg/Kg-dry 12740NELAP 69916
Sodium 07/27/2011 14:014.55 mg/Kg-dry 1177NELAP 69916
Vanadium 07/27/2011 14:010.91 mg/Kg-dry 130.0NELAP 69916
Zinc 07/27/2011 14:010.91 mg/Kg-dry 169.0NELAP 69916
Al, Ca, Fe, Mg Mn, K - Sample concentration was greater than 5 times the spike concentration.
SW-846 3050B, METALS BY GFAAThallium 7841 07/28/2011 8:310.185 mg/Kg-dry 10.361NELAP 69917
Page 6 of 14
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 28-Jul-11
Work Order: 11071019
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 9:00
Lab ID: 11071019-003 Client Sample ID: SBA-D5-01 (5-6)
Matrix: SOLID
Batch
SW-846 3050B, 6010B, METALS BY ICPAluminum 07/27/2011 14:184.72 mg/Kg-dry 112500NELAP 69916
Antimony 07/27/2011 11:244.90 mg/Kg-dry 1< 4.90NELAP 69908
Beryllium 07/27/2011 14:180.09 mg/Kg-dry 10.55NELAP 69916
Calcium 07/27/2011 14:184.72 mg/Kg-dry 154000NELAP 69916
Cobalt 07/27/2011 14:180.94 mg/Kg-dry 19.08NELAP 69916
Copper 07/27/2011 14:180.94 mg/Kg-dry 115.3NELAP 69916
Iron 07/27/2011 14:181.89 mg/Kg-dry 121200NELAP 69916
Magnesium 07/27/2011 14:180.94 mg/Kg-dry 129100NELAP 69916
Manganese 07/27/2011 14:180.47 mg/Kg-dry 1425NELAP 69916
Nickel 07/27/2011 14:180.94 mg/Kg-dry 121.9NELAP 69916
Potassium 07/27/2011 14:189.43 mg/Kg-dry 13360NELAP 69916
Sodium 07/27/2011 14:184.72 mg/Kg-dry 1143NELAP 69916
Vanadium 07/27/2011 14:180.94 mg/Kg-dry 116.4NELAP 69916
Zinc 07/27/2011 14:180.94 mg/Kg-dry 153.5NELAP 69916
SW-846 3050B, METALS BY GFAAThallium 7841 07/28/2011 8:350.192 mg/Kg-dry 10.313NELAP 69917
Page 7 of 14
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 28-Jul-11
Work Order: 11071019
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 10:00
Lab ID: 11071019-004 Client Sample ID: SBA-A3-01 (5-6)
Matrix: SOLID
Batch
SW-846 3050B, 6010B, METALS BY ICPAluminum 07/27/2011 14:244.90 mg/Kg-dry 110800NELAP 69916
Antimony 07/27/2011 11:294.81 mg/Kg-dry 1< 4.81NELAP 69908
Beryllium 07/27/2011 14:240.10 mg/Kg-dry 10.47NELAP 69916
Calcium 07/27/2011 14:244.90 mg/Kg-dry 160600NELAP 69916
Cobalt 07/27/2011 14:240.98 mg/Kg-dry 17.79NELAP 69916
Copper 07/27/2011 14:240.98 mg/Kg-dry 114.7NELAP 69916
Iron 07/27/2011 14:241.96 mg/Kg-dry 119400NELAP 69916
Magnesium 07/27/2011 14:240.98 mg/Kg-dry 131500NELAP 69916
Manganese 07/27/2011 14:240.49 mg/Kg-dry 1393NELAP 69916
Nickel 07/27/2011 14:240.98 mg/Kg-dry 121.3NELAP 69916
Potassium 07/27/2011 14:249.80 mg/Kg-dry 13500NELAP 69916
Sodium 07/27/2011 14:244.90 mg/Kg-dry 1145NELAP 69916
Vanadium 07/27/2011 14:240.98 mg/Kg-dry 114.4NELAP 69916
Zinc 07/27/2011 14:240.98 mg/Kg-dry 149.5NELAP 69916
SW-846 3050B, METALS BY GFAAThallium 7841 07/28/2011 8:380.182 mg/Kg-dry 10.268NELAP 69917
Page 8 of 14
TeklabHdrP
Laboratory Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 28-Jul-11
Work Order: 11071019
http://www.teklabinc.com/
Analyses Result Units Date AnalyzedRL DFCertification Qual
Collection Date: 06/30/2011 11:00
Lab ID: 11071019-005 Client Sample ID: SBA-A5-01 (5-6)
Matrix: SOLID
Batch
SW-846 3050B, 6010B, METALS BY ICPAluminum 07/27/2011 14:294.72 mg/Kg-dry 116100NELAP 69916
Antimony 07/27/2011 11:354.72 mg/Kg-dry 1< 4.72NELAP 69908
Beryllium 07/27/2011 14:290.09 mg/Kg-dry 10.67NELAP 69916
Calcium 07/27/2011 14:294.72 mg/Kg-dry 145200NELAP 69916
Cobalt 07/27/2011 14:290.94 mg/Kg-dry 19.75NELAP 69916
Copper 07/27/2011 14:290.94 mg/Kg-dry 117.7NELAP 69916
Iron 07/27/2011 14:291.89 mg/Kg-dry 123100NELAP 69916
Magnesium 07/27/2011 14:290.94 mg/Kg-dry 122300NELAP 69916
Manganese 07/27/2011 14:290.47 mg/Kg-dry 1567NELAP 69916
Nickel 07/27/2011 14:290.94 mg/Kg-dry 123.4NELAP 69916
Potassium 07/27/2011 14:299.43 mg/Kg-dry 13750NELAP 69916
Sodium 07/27/2011 14:294.72 mg/Kg-dry 1191NELAP 69916
Vanadium 07/27/2011 14:290.94 mg/Kg-dry 123.9NELAP 69916
Zinc 07/27/2011 14:290.94 mg/Kg-dry 160.4NELAP 69916
SW-846 3050B, METALS BY GFAAThallium 7841 07/28/2011 8:520.185 mg/Kg-dry 10.341NELAP 69917
Page 9 of 14
Lab Sample ID Client Sample ID Collection DateFractions
TeklabHdrP
Matrix
Sample Summary
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 28-Jul-11
Work Order: 11071019
http://www.teklabinc.com/
11071019-001 SBA-C3-01 (5-6) 06/29/2011 16:001Solid
11071019-002 SBA-B4-01 (5-6) 06/30/2011 8:001Solid
11071019-003 SBA-D5-01 (5-6) 06/30/2011 9:001Solid
11071019-004 SBA-A3-01 (5-6) 06/30/2011 10:001Solid
11071019-005 SBA-A5-01 (5-6) 06/30/2011 11:001Solid
Page 10 of 14
Analysis Date/TimeTest Name Prep Date/Time
____TeklabHdrP
Sample ID Client Sample ID Collection Date Received Date
Dates Report
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 28-Jul-11
Work Order: 11071019
http://www.teklabinc.com/
11071019-001A SBA-C3-01 (5-6) 06/29/2011 16:00 7/1/2011 3:50:00 PM
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 11:0007/26/2011 20:14
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 13:5507/26/2011 20:32
SW-846 3050B, Metals by GFAA 07/28/2011 8:2807/26/2011 20:54
11071019-002A SBA-B4-01 (5-6) 06/30/2011 8:00 7/1/2011 3:50:00 PM
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 11:1807/26/2011 20:14
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 14:0107/26/2011 20:32
SW-846 3050B, Metals by GFAA 07/28/2011 8:3107/26/2011 20:54
11071019-003A SBA-D5-01 (5-6) 06/30/2011 9:00 7/1/2011 3:50:00 PM
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 11:2407/26/2011 20:14
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 14:1807/26/2011 20:32
SW-846 3050B, Metals by GFAA 07/28/2011 8:3507/26/2011 20:54
11071019-004A SBA-A3-01 (5-6) 06/30/2011 10:00 7/1/2011 3:50:00 PM
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 11:2907/26/2011 20:14
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 14:2407/26/2011 20:32
SW-846 3050B, Metals by GFAA 07/28/2011 8:3807/26/2011 20:54
11071019-005A SBA-A5-01 (5-6) 06/30/2011 11:00 7/1/2011 3:50:00 PM
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 11:3507/26/2011 20:14
SW-846 3050B, 6010B, Metals by ICP 07/27/2011 14:2907/26/2011 20:32
SW-846 3050B, Metals by GFAA 07/28/2011 8:5207/26/2011 20:54
Page 11 of 14
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 28-Jul-11
Work Order: 11071019
http://www.teklabinc.com/
SW-846 3050B, 6010B, METALS BY ICP
SampID: MB-69908
SampType: MBLK mg/Kg-dryUnits69908Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Antimony 07/27/20115.00 5.00< 5.00 00 -100 100
SampID: LCS-69908
SampType: LCS mg/Kg-dryUnits69908Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Antimony 07/27/20115.00 50.051.8 103.70 85 115
SampID: 11071019-001AMS
SampType: MS mg/Kg-dryUnits69908Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Antimony 07/27/20114.90 49.049.0 1000 75 125
SampID: 11071019-001AMSD
SampType: MSD mg/Kg-dryUnits69908Batch RPD Limit 20
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Antimony 07/27/20114.90 49.050.3 102.6 2.610 49.02
SampID: MB-69916
SampType: MBLK mg/Kg-dryUnits69916Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Aluminum 07/27/20115.00 5.00< 5.00 00 -100 100
Beryllium 07/27/20110.10 0.10< 0.10 00 -100 100
Calcium 07/27/20115.00 5.00< 5.00 00 -100 100
Cobalt 07/27/20111.00 1.00< 1.00 00 -100 100
Copper 07/27/20111.00 1.00< 1.00 00 -100 100
Iron 07/27/20112.00 2.00< 2.00 00 -100 100
Magnesium 07/27/20111.00 1.00< 1.00 00 -100 100
Manganese 07/27/20110.50 0.50< 0.50 00 -100 100
Nickel 07/27/20111.00 1.00< 1.00 00 -100 100
Potassium 07/27/201110.0 10.0< 10.0 00 -100 100
Sodium 07/27/20115.00 5.00< 5.00 00 -100 100
Vanadium 07/27/20111.00 1.00< 1.00 00 -100 100
Zinc 07/27/20111.00 1.00< 1.00 00 -100 100
Page 12 of 14
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 28-Jul-11
Work Order: 11071019
http://www.teklabinc.com/
SW-846 3050B, 6010B, METALS BY ICP
SampID: LCS-69916
SampType: LCS mg/Kg-dryUnits69916Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Aluminum 07/27/20115.00 200208 104.00 85 115
Beryllium 07/27/20110.10 5.005.23 104.60 85 115
Calcium 07/27/20115.00 120124 103.70 85 115
Cobalt 07/27/20111.00 50.050.0 1000 85 115
Copper 07/27/20111.00 25.025.6 102.60 85 115
Iron 07/27/20112.00 100104 103.60 85 115
Magnesium 07/27/20111.00 75.080.8 107.80 85 115
Manganese 07/27/20110.50 50.053.0 106.00 85 115
Nickel 07/27/20111.00 50.053.3 106.60 85 115
Potassium 07/27/201110.0 120126 104.80 85 115
Sodium 07/27/20115.00 120128 106.90 85 115
Vanadium 07/27/20111.00 50.050.7 101.30 85 115
Zinc 07/27/20111.00 50.050.6 101.30 85 115
SampID: 11071019-002AMS
SampType: MS mg/Kg-dryUnits69916Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Aluminum S 07/27/20114.55 18219000 225.018570 75 125
Beryllium 07/27/20110.09 4.545.41 102.20.7636 75 125
Calcium S 07/27/20114.55 10930000 -334233640 75 125
Cobalt 07/27/20110.91 45.452.6 89.012.13 75 125
Copper 07/27/20110.91 22.743.3 95.921.47 75 125
Iron S 07/27/20111.82 90.925500 -115026580 75 125
Magnesium S 07/27/20110.91 68.213300 426.713050 75 125
Manganese S 07/27/20110.45 45.4773 -106.2821.2 75 125
Nickel 07/27/20110.91 45.471.6 97.427.30 75 125
Potassium S 07/27/20119.09 1092950 184.22745 75 125
Sodium 07/27/20114.55 109295 108.0176.9 75 125
Vanadium 07/27/20110.91 45.477.6 104.630.00 75 125
Zinc 07/27/20110.91 45.4108 86.169.03 75 125
Page 13 of 14
Quality Control Results
Client Project: A831-735002-012901-225Ameren Champaign 62409080120
Client: PSC Industrial Outsourcing, LP
Report Date: 28-Jul-11
Work Order: 11071019
http://www.teklabinc.com/
SW-846 3050B, 6010B, METALS BY ICP
SampID: 11071019-002AMSD
SampType: MSD mg/Kg-dryUnits69916Batch RPD Limit 20
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Aluminum S 07/27/20114.55 18218800 135.0 0.8718570 18980
Beryllium 07/27/20110.09 4.545.37 101.4 0.670.7636 5.409
Calcium S 07/27/20114.55 10932100 -1450 6.6533640 29990
Cobalt 07/27/20110.91 45.452.1 88.0 0.9012.13 52.60
Copper 07/27/20110.91 22.743.7 97.8 1.0021.47 43.26
Iron S 07/27/20111.82 90.924900 -1800 2.3426580 25540
Magnesium S 07/27/20110.91 68.212800 -360.0 4.1013050 13350
Manganese S 07/27/20110.45 45.4725 -212.6 6.46821.2 772.9
Nickel 07/27/20110.91 45.469.3 92.3 3.2527.30 71.56
Potassium S 07/27/20119.09 1092900 146.7 1.402745 2945
Sodium 07/27/20114.55 109304 116.6 3.13176.9 294.7
Vanadium 07/27/20110.91 45.474.3 97.6 4.2430.00 77.56
Zinc 07/27/20110.91 45.4107 84.3 0.7669.03 108.2
SW-846 3050B, METALS BY GFAA
SampID: MB-69917
SampType: MBLK mg/Kg-dryUnits69917Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Thallium 7841 07/28/20110.200 0.200< 0.200 00 -100 100
SampID: LCS-69917
SampType: LCS mg/Kg-dryUnits69917Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Thallium 7841 07/28/20110.200 1.501.30 86.90 80 120
SampID: 11071019-004AMS
SampType: MS mg/Kg-dryUnits69917Batch
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC Low Limit High Limit
Thallium 7841 07/28/20110.182 1.362.02 128.30.2675 70 130
SampID: 11071019-004AMSD
SampType: MSD mg/Kg-dryUnits69917Batch RPD Limit 20
Analyses Result
Date AnalyzedRL SpikeQual SPK Ref Val %REC RPD Ref Val %RPD
Thallium 7841 07/28/20110.182 1.362.00 126.7 1.060.2675 2.017
Page 14 of 14