Technical Report for Matrix New World Engineering, Inc.09/26/12 Technical Report for Matrix New World Engineering, Inc. PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road,

09/26/12

Technical Report for

Matrix New World Engineering, Inc.

PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

12-100E-01

Accutest Job Number: C23633

Sampling Dates: 09/12/12 - 09/13/12

Report to:

Matrix New World Engineering, Inc.

[email protected]

ATTN: Jody Mack

Total number of pages in report:

Certifications: CA (08258CA) AZ (AZ0762) DoD/ISO/IEC 17025:2005 (L2242)

This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.

Test results relate only to samples analyzed.

Northern California • 2105 Lundy Ave. • San Jose, CA 95131 • tel: 408-588-0200 • fax: 408-588-0201 • http://www.accutest.com

Test results contained within this data package meet the requirements

of the National Environmental Laboratory Accreditation Conference

and/or state specific certification programs as applicable.

Client Service contact: Beth Proffitt 408-588-0200

Kesavalu M. Bagawandoss,Ph.D., J.D., Lab Director

Northern California

09/26/12

e-Hardcopy 2.0Automated Report

68

Accutest Laboratories is the sole authority for authorizing edits or modifications to thisdocument. Unauthorized modification of this report is strictly prohibited.

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SDMS DOCID# 1142989

Table of Contents-1-

Sections:

Section 1: Sample Summary ................................................................................................... 3Section 2: Case Narrative/Conformance Summary .............................................................. 5Section 3: Summary of Hits .................................................................................................... 6Section 4: Sample Results ........................................................................................................ 8

4.1: C23633-1: TB001-09122012 ........................................................................................ 94.2: C23633-2: EPAMW57A-09122012 ............................................................................. 104.3: C23633-3: EPAMW15C-09122012 ............................................................................. 124.4: C23633-4: MW21-09122012 ........................................................................................ 134.5: C23633-5: EPAMW1A-09122012 ............................................................................... 144.6: C23633-6: EPAMW1C-09122012 ............................................................................... 164.7: C23633-7: EB001-09122012 ........................................................................................ 174.8: C23633-8: MW27-09132012 ........................................................................................ 194.9: C23633-9: EPAMW5C-09132012 ............................................................................... 214.10: C23633-10: EPAMW56A-09132012 ......................................................................... 234.11: C23633-11: EPAMW48A-09132012 ......................................................................... 244.12: C23633-12: EPAMW3C-09132012 ........................................................................... 254.13: C23633-13: DUP001-09132012 ................................................................................. 274.14: C23633-14: EB001-09132012 .................................................................................... 29

Section 5: Misc. Forms ............................................................................................................ 315.1: Arizona Qualifiers .......................................................................................................... 325.2: Chain of Custody ........................................................................................................... 33

Section 6: GC/MS Volatiles - QC Data Summaries .............................................................. 366.1: Method Blank Summary ................................................................................................ 376.2: Blank Spike/Blank Spike Duplicate Summary .............................................................. 386.3: Laboratory Control Sample Summary ........................................................................... 396.4: Matrix Spike/Matrix Spike Duplicate Summary ........................................................... 406.5: Instrument Performance Checks (BFB) ......................................................................... 416.6: Internal Standard Area Summaries ................................................................................ 446.7: Surrogate Recovery Summaries ..................................................................................... 456.8: Initial and Continuing Calibration Summaries .............................................................. 46

Section 7: General Chemistry - QC Data Summaries .......................................................... 617.1: Method Blank and Spike Results Summary .................................................................. 627.2: Blank Spike Duplicate Results Summary ...................................................................... 637.3: Duplicate Results Summary .......................................................................................... 647.4: Matrix Spike Results Summary ..................................................................................... 657.5: Matrix Spike Duplicate Results Summary .................................................................... 667.6: Inst QC GN9101: Perchlorate ........................................................................................ 67

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Sample Summary

Matrix New World Engineering, Inc.Job No: C23633

PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZProject No: 12-100E-01

Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID

C23633-1 09/12/12 00:00 GLJL 09/14/12 AQ Trip Blank Water TB001-09122012

C23633-2 09/12/12 09:07 GLJL 09/14/12 AQ Ground Water EPAMW57A-09122012

C23633-2D 09/12/12 09:07 GLJL 09/14/12 AQ Water Dup/MSD EPAMW57A-09122012

C23633-2S 09/12/12 09:07 GLJL 09/14/12 AQ Water Matrix Spike EPAMW57A-09122012

C23633-3 09/12/12 10:37 GLJL 09/14/12 AQ Ground Water EPAMW15C-09122012

C23633-4 09/12/12 11:07 GLJL 09/14/12 AQ Ground Water MW21-09122012



C23633-7 09/12/12 14:00 GLJL 09/14/12 AQ Equipment Blank EB001-09122012

C23633-8 09/13/12 07:47 GLJL 09/14/12 AQ Ground Water MW27-09132012




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Sample Summary(continued)

Matrix New World Engineering, Inc.Job No: C23633

PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZProject No: 12-100E-01

Sample Collected Matrix Client Number Date Time By Received Code Type Sample ID


C23633-13 09/13/12 11:06 GLJL 09/14/12 AQ Ground Water DUP001-09132012

C23633-14 09/13/12 12:20 GLJL 09/14/12 AQ Equipment Blank EB001-09132012

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13 Sample(s), 1 Trip Blank(s) and 0 Field Blank(s) were collected between 09/12/2012 and 09/13/2012 and were received at Accutest on 09/14/2012 properly preserved, at 3.2 Deg. C and intact. These Samples received an Accutest job number of C23633. A listing of the Laboratory Sample ID, Client Sample ID and dates of collection are presented in the Results Summary Section of this report.

Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more information, please refer to QC summary pages.

Client: Matrix New World Engineering, Inc.

Site: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Ph

Job No: C23633

Report Date 9/21/2012 10:37:58 P

SAMPLE DELIVERY GROUP CASE NARRATIVE

Volatiles by GCMS By Method SW846 8260BMatrix: AQ Batch ID: VR416

Sample(s) C23633-2MS, C23633-2MSD were used as the QC samples indicated.

Wet Chemistry By Method EPA 314Matrix: AQ Batch ID: GP4141

Sample(s) C23633-2MS, C23633-2MSD were used as the QC samples for Perchlorate.

C23633-9, -12, -13 for Perchlorate: Elevated detection limit due to matrix interference.

Wet Chemistry By Method SM18 2510B/EPA 120.1Matrix: AQ Batch ID: GN9059

Sample(s) C23633-2DUP were used as the QC samples for Specific Conductivity.

Accutest Laboratories Northern California (ALNCA) certifies that this report meets the project requirements for analytical data produced for the samples as received at ALNCA and as stated on the COC. ALNCA certifies that the data meets the Data QualityObjectives for precision, accuracy and completeness as specified in the ALNCA Quality Manual except as noted above. This report is to be used in its entirety. ALNCA is not responsible for any assumptions of data quality if partial data packages are used

Friday, September 21, 2012 Page 1 of 1

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Summary of Hits Page 1 of 2 Job Number: C23633Account: Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZCollected: 09/12/12 thru 09/13/12

Lab Sample ID Client Sample ID Result/Analyte Qual RL MDL Units Method

C23633-1 TB001-09122012

Acetone a 5.2 J 20 4.0 ug/l SW846 8260B

C23633-2 EPAMW57A-09122012

Chloroform a 0.23 J 1.0 0.20 ug/l SW846 8260BTetrachloroethylene 3.7 1.0 0.30 ug/l SW846 8260BPerchlorate a 2.1 J 3.0 0.31 ug/l EPA 314Specific Conductivity 1990 1.0 1.0 umhos/cm SM18 2510B/EPA 120.1

C23633-3 EPAMW15C-09122012

No hits reported in this sample.

C23633-4 MW21-09122012

Trichloroethylene 3.0 1.0 0.20 ug/l SW846 8260B

C23633-5 EPAMW1A-09122012

Trichloroethylene 8.1 1.0 0.20 ug/l SW846 8260BPerchlorate 3.8 3.0 0.31 ug/l EPA 314Specific Conductivity 3410 1.0 1.0 umhos/cm SM18 2510B/EPA 120.1

C23633-6 EPAMW1C-09122012


C23633-7 EB001-09122012


C23633-8 MW27-09132012

Trichloroethylene 10.5 1.0 0.20 ug/l SW846 8260BPerchlorate 3.5 3.0 0.31 ug/l EPA 314Specific Conductivity 3530 1.0 1.0 umhos/cm SM18 2510B/EPA 120.1

C23633-9 EPAMW5C-09132012

1,1-Dichloroethylene 2.6 1.0 0.20 ug/l SW846 8260BTrichloroethylene 17.2 1.0 0.20 ug/l SW846 8260BPerchlorate b 8.4 6.0 0.63 ug/l EPA 314Specific Conductivity 4360 1.0 1.0 umhos/cm SM18 2510B/EPA 120.1

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Summary of Hits Page 2 of 2 Job Number: C23633Account: Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZCollected: 09/12/12 thru 09/13/12

Lab Sample ID Client Sample ID Result/Analyte Qual RL MDL Units Method

C23633-10 EPAMW56A-09132012


C23633-11 EPAMW48A-09132012

Trichloroethylene 456 10 2.0 ug/l SW846 8260B

C23633-12 EPAMW3C-09132012

Trichloroethylene 975 20 4.0 ug/l SW846 8260BPerchlorate b 22.7 6.0 0.63 ug/l EPA 314Specific Conductivity 4390 1.0 1.0 umhos/cm SM18 2510B/EPA 120.1

C23633-13 DUP001-09132012

Trichloroethylene 1080 20 4.0 ug/l SW846 8260BPerchlorate b 22.7 6.0 0.63 ug/l EPA 314Specific Conductivity 4360 1.0 1.0 umhos/cm SM18 2510B/EPA 120.1

C23633-14 EB001-09132012


(a) Estimated concentration below laboratory reporting limit. AZ:E4(b) Elevated detection limit due to matrix interference.

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Sample Results

Report of Analysis

Northern California

Section 4

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Report of Analysis Page 1 of 1

Client Sample ID: TB001-09122012 Lab Sample ID: C23633-1 Date Sampled: 09/12/12 Matrix: AQ - Trip Blank Water Date Received: 09/14/12 Method: SW846 8260B Percent Solids: n/a Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

File ID DF Analyzed By Prep Date Prep Batch Analytical BatchRun #1 R11649.D 1 09/18/12 BD n/a n/a VR416Run #2

Purge VolumeRun #1 10.0 mlRun #2

VOA Special List

CAS No. Compound Result RL MDL Units Q

67-64-1 Acetone a 5.2 20 4.0 ug/l J71-43-2 Benzene ND 1.0 0.20 ug/l67-66-3 Chloroform ND 1.0 0.20 ug/l56-23-5 Carbon tetrachloride ND 1.0 0.20 ug/l75-35-4 1,1-Dichloroethylene ND 1.0 0.20 ug/l78-87-5 1,2-Dichloropropane ND 1.0 0.20 ug/l156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.20 ug/l156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.20 ug/l100-41-4 Ethylbenzene ND 1.0 0.20 ug/l75-09-2 Methylene chloride ND 10 2.0 ug/l78-93-3 Methyl ethyl ketone ND 10 2.0 ug/l79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.20 ug/l127-18-4 Tetrachloroethylene ND 1.0 0.30 ug/l108-88-3 Toluene ND 1.0 0.20 ug/l79-01-6 Trichloroethylene ND 1.0 0.20 ug/l75-69-4 Trichlorofluoromethane ND 1.0 0.20 ug/l75-01-4 Vinyl chloride ND 1.0 0.20 ug/l

m,p-Xylene ND 1.0 0.26 ug/l95-47-6 o-Xylene ND 1.0 0.20 ug/l

CAS No. Surrogate Recoveries Run# 1 Run# 2 Limits

1868-53-7 Dibromofluoromethane 99% 60-130%2037-26-5 Toluene-D8 100% 60-130%460-00-4 4-Bromofluorobenzene 94% 60-130%

(a) Estimated concentration below laboratory reporting limit. AZ:E4

ND = Not detected MDL - Method Detection Limit J = Indicates an estimated valueRL = Reporting Limit B = Indicates analyte found in associated method blankE = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound

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Client Sample ID: EPAMW57A-09122012 Lab Sample ID: C23633-2 Date Sampled: 09/12/12 Matrix: AQ - Ground Water Date Received: 09/14/12 Method: SW846 8260B Percent Solids: n/a Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ



VOA Special List


67-64-1 Acetone ND 20 4.0 ug/l71-43-2 Benzene ND 1.0 0.20 ug/l67-66-3 Chloroform a 0.23 1.0 0.20 ug/l J56-23-5 Carbon tetrachloride ND 1.0 0.20 ug/l75-35-4 1,1-Dichloroethylene ND 1.0 0.20 ug/l78-87-5 1,2-Dichloropropane ND 1.0 0.20 ug/l156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.20 ug/l156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.20 ug/l100-41-4 Ethylbenzene ND 1.0 0.20 ug/l75-09-2 Methylene chloride ND 10 2.0 ug/l78-93-3 Methyl ethyl ketone ND 10 2.0 ug/l79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.20 ug/l127-18-4 Tetrachloroethylene 3.7 1.0 0.30 ug/l108-88-3 Toluene ND 1.0 0.20 ug/l79-01-6 Trichloroethylene ND 1.0 0.20 ug/l75-69-4 Trichlorofluoromethane ND 1.0 0.20 ug/l75-01-4 Vinyl chloride ND 1.0 0.20 ug/l






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Client Sample ID: EPAMW57A-09122012 Lab Sample ID: C23633-2 Date Sampled: 09/12/12 Matrix: AQ - Ground Water Date Received: 09/14/12

Percent Solids: n/a Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

General Chemistry

Analyte Result RL MDL Units DF Analyzed By Method

Perchlorate by ICPerchlorate a 2.1 J 3.0 0.31 ug/l 1 09/20/12 17:51 PH EPA 314

Specific Conductivity 1990 1.0 1.0 umhos/cm 1 09/14/12 AC SM18 2510B/EPA 120.1


RL = Reporting Limit U = Indicates a result < MDLMDL = Method Detection Limit J = Indicates a result >= MDL but < RL

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Client Sample ID: EPAMW15C-09122012 Lab Sample ID: C23633-3 Date Sampled: 09/12/12 Matrix: AQ - Ground Water Date Received: 09/14/12 Method: SW846 8260B Percent Solids: n/a Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ



VOA Special List


67-64-1 Acetone ND 20 4.0 ug/l71-43-2 Benzene ND 1.0 0.20 ug/l67-66-3 Chloroform ND 1.0 0.20 ug/l56-23-5 Carbon tetrachloride ND 1.0 0.20 ug/l75-35-4 1,1-Dichloroethylene ND 1.0 0.20 ug/l78-87-5 1,2-Dichloropropane ND 1.0 0.20 ug/l156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.20 ug/l156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.20 ug/l100-41-4 Ethylbenzene ND 1.0 0.20 ug/l75-09-2 Methylene chloride ND 10 2.0 ug/l78-93-3 Methyl ethyl ketone ND 10 2.0 ug/l79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.20 ug/l127-18-4 Tetrachloroethylene ND 1.0 0.30 ug/l108-88-3 Toluene ND 1.0 0.20 ug/l79-01-6 Trichloroethylene ND 1.0 0.20 ug/l75-69-4 Trichlorofluoromethane ND 1.0 0.20 ug/l75-01-4 Vinyl chloride ND 1.0 0.20 ug/l





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Client Sample ID: MW21-09122012 Lab Sample ID: C23633-4 Date Sampled: 09/12/12 Matrix: AQ - Ground Water Date Received: 09/14/12 Method: SW846 8260B Percent Solids: n/a Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ



VOA Special List


67-64-1 Acetone ND 20 4.0 ug/l71-43-2 Benzene ND 1.0 0.20 ug/l67-66-3 Chloroform ND 1.0 0.20 ug/l56-23-5 Carbon tetrachloride ND 1.0 0.20 ug/l75-35-4 1,1-Dichloroethylene ND 1.0 0.20 ug/l78-87-5 1,2-Dichloropropane ND 1.0 0.20 ug/l156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.20 ug/l156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.20 ug/l100-41-4 Ethylbenzene ND 1.0 0.20 ug/l75-09-2 Methylene chloride ND 10 2.0 ug/l78-93-3 Methyl ethyl ketone ND 10 2.0 ug/l79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.20 ug/l127-18-4 Tetrachloroethylene ND 1.0 0.30 ug/l108-88-3 Toluene ND 1.0 0.20 ug/l79-01-6 Trichloroethylene 3.0 1.0 0.20 ug/l75-69-4 Trichlorofluoromethane ND 1.0 0.20 ug/l75-01-4 Vinyl chloride ND 1.0 0.20 ug/l





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VOA Special List







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Client Sample ID: EPAMW1A-09122012 Lab Sample ID: C23633-5 Date Sampled: 09/12/12 Matrix: AQ - Ground Water Date Received: 09/14/12


General Chemistry


Perchlorate by ICPerchlorate 3.8 3.0 0.31 ug/l 1 09/20/12 18:08 PH EPA 314



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VOA Special List







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Client Sample ID: EB001-09122012 Lab Sample ID: C23633-7 Date Sampled: 09/12/12 Matrix: AQ - Equipment Blank Date Received: 09/14/12 Method: SW846 8260B Percent Solids: n/a Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ



VOA Special List







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Client Sample ID: EB001-09122012 Lab Sample ID: C23633-7 Date Sampled: 09/12/12 Matrix: AQ - Equipment Blank Date Received: 09/14/12


General Chemistry


Perchlorate by ICPerchlorate 0.31 U 3.0 0.31 ug/l 1 09/20/12 17:16 PH EPA 314

Specific Conductivity 1.0 U 1.0 1.0 umhos/cm 1 09/14/12 AC SM18 2510B/EPA 120.1


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Client Sample ID: MW27-09132012 Lab Sample ID: C23633-8 Date Sampled: 09/13/12 Matrix: AQ - Ground Water Date Received: 09/14/12 Method: SW846 8260B Percent Solids: n/a Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ



VOA Special List







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Client Sample ID: MW27-09132012 Lab Sample ID: C23633-8 Date Sampled: 09/13/12 Matrix: AQ - Ground Water Date Received: 09/14/12


General Chemistry


Perchlorate by ICPerchlorate 3.5 3.0 0.31 ug/l 1 09/20/12 18:26 PH EPA 314



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VOA Special List


67-64-1 Acetone ND 20 4.0 ug/l71-43-2 Benzene ND 1.0 0.20 ug/l67-66-3 Chloroform ND 1.0 0.20 ug/l56-23-5 Carbon tetrachloride ND 1.0 0.20 ug/l75-35-4 1,1-Dichloroethylene 2.6 1.0 0.20 ug/l78-87-5 1,2-Dichloropropane ND 1.0 0.20 ug/l156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.20 ug/l156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.20 ug/l100-41-4 Ethylbenzene ND 1.0 0.20 ug/l75-09-2 Methylene chloride ND 10 2.0 ug/l78-93-3 Methyl ethyl ketone ND 10 2.0 ug/l79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.20 ug/l127-18-4 Tetrachloroethylene ND 1.0 0.30 ug/l108-88-3 Toluene ND 1.0 0.20 ug/l79-01-6 Trichloroethylene 17.2 1.0 0.20 ug/l75-69-4 Trichlorofluoromethane ND 1.0 0.20 ug/l75-01-4 Vinyl chloride ND 1.0 0.20 ug/l





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Client Sample ID: EPAMW5C-09132012 Lab Sample ID: C23633-9 Date Sampled: 09/13/12 Matrix: AQ - Ground Water Date Received: 09/14/12


General Chemistry


Perchlorate by ICPerchlorate a 8.4 6.0 0.63 ug/l 2 09/20/12 19:53 PH EPA 314


(a) Elevated detection limit due to matrix interference.


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VOA Special List







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VOA Special List


67-64-1 Acetone ND 200 40 ug/l71-43-2 Benzene ND 10 2.0 ug/l67-66-3 Chloroform ND 10 2.0 ug/l56-23-5 Carbon tetrachloride ND 10 2.0 ug/l75-35-4 1,1-Dichloroethylene ND 10 2.0 ug/l78-87-5 1,2-Dichloropropane ND 10 2.0 ug/l156-59-2 cis-1,2-Dichloroethylene ND 10 2.0 ug/l156-60-5 trans-1,2-Dichloroethylene ND 10 2.0 ug/l100-41-4 Ethylbenzene ND 10 2.0 ug/l75-09-2 Methylene chloride ND 100 20 ug/l78-93-3 Methyl ethyl ketone ND 100 20 ug/l79-34-5 1,1,2,2-Tetrachloroethane ND 10 2.0 ug/l127-18-4 Tetrachloroethylene ND 10 3.0 ug/l108-88-3 Toluene ND 10 2.0 ug/l79-01-6 Trichloroethylene 456 10 2.0 ug/l75-69-4 Trichlorofluoromethane ND 10 2.0 ug/l75-01-4 Vinyl chloride ND 10 2.0 ug/l

m,p-Xylene ND 10 2.6 ug/l95-47-6 o-Xylene ND 10 2.0 ug/l




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VOA Special List







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Client Sample ID: EPAMW3C-09132012 Lab Sample ID: C23633-12 Date Sampled: 09/13/12 Matrix: AQ - Ground Water Date Received: 09/14/12


General Chemistry






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Client Sample ID: DUP001-09132012 Lab Sample ID: C23633-13 Date Sampled: 09/13/12 Matrix: AQ - Ground Water Date Received: 09/14/12 Method: SW846 8260B Percent Solids: n/a Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ



VOA Special List







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Client Sample ID: DUP001-09132012 Lab Sample ID: C23633-13 Date Sampled: 09/13/12 Matrix: AQ - Ground Water Date Received: 09/14/12


General Chemistry






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Client Sample ID: EB001-09132012 Lab Sample ID: C23633-14 Date Sampled: 09/13/12 Matrix: AQ - Equipment Blank Date Received: 09/14/12 Method: SW846 8260B Percent Solids: n/a Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ



VOA Special List







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Client Sample ID: EB001-09132012 Lab Sample ID: C23633-14 Date Sampled: 09/13/12 Matrix: AQ - Equipment Blank Date Received: 09/14/12


General Chemistry


Perchlorate by ICPerchlorate 0.31 U 3.0 0.31 ug/l 1 09/20/12 17:34 PH EPA 314

Specific Conductivity 1.0 U 1.0 1.0 umhos/cm 1 09/14/12 AC SM18 2510B/EPA 120.1


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Misc. Forms

Custody Documents and Other Forms

Includes the following where applicable:

• Arizona Qualifiers• Chain of Custody

Northern California

Section 5

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Arizona Qualifiers Page 1 of 1 Job Number: C23633Account: MTXFPNJ Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

The following Arizona qualifiers have been applied to data and/or QC in this report.

Qual Description

E4 Concentration estimated. Analyte was detected below laboratory minimum reporting limit (MRL).

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C23633: Chain of CustodyPage 1 of 3

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Accutest Laboratories Sample Receipt Summary

Accutest LaboratoriesV:408.588.0200

2105 Lundy AvenueF: 408.588.0201

San Jose, CA 95131www/accutest.com

Accutest Job Number: C23633 Client: MATRIX

Date / Time Received: 9/14/2012 Delivery Method: FedEx

Project: PLAN

4. No. Coolers: 1

Airbill #'s:

Cooler Security

1. Custody Seals Present:

Y or N

2. Custody Seals Intact:

3. COC Present:

4. Smpl Dates/Time OK

2. Cooler temp verification:

Cooler Temperature Y or N

1. Temp criteria achieved:

3. Cooler media:

IR Gun

Ice (Bag)

Quality Control Preservation Y or N N/A

1. Trip Blank present / cooler:

2. Trip Blank listed on COC:

3. Samples preserved properly:

4. VOCs headspace free:

Sample Integrity - Documentation Y or N

1. Sample labels present on bottles:

2. Container labeling complete:

3. Sample container label / COC agree:

Sample Integrity - Condition Y or N

1. Sample recvd within HT:

3. Condition of sample:

2. All containers accounted for:

Sample Integrity - Instructions

1. Analysis requested is clear:

2. Bottles received for unspecified tests

3. Sufficient volume recvd for analysis:

4. Compositing instructions clear:

5. Filtering instructions clear:

Intact

Y or N

Comments

Y or N N/A

Cooler Temps (Initial/Adjusted): #1: (4.2/3.2); 0


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GC/MS Volatiles

QC Data Summaries

Includes the following where applicable:

• Method Blank Summaries• Blank Spike Summaries• Matrix Spike and Duplicate Summaries• Instrument Performance Checks (BFB)• Internal Standard Area Summaries• Surrogate Recovery Summaries• Initial and Continuing Calibration Summaries

Northern California

Section 6

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C23633

6

Method Blank Summary Page 1 of 1 Job Number: C23633Account: MTXFPNJ Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchVR416-MB R11647.D 1 09/18/12 BD n/a n/a VR416

The QC reported here applies to the following samples: Method: SW846 8260B

C23633-1, C23633-2, C23633-3, C23633-4, C23633-5, C23633-6, C23633-7, C23633-8, C23633-9, C23633-10, C23633-11, C23633-12, C23633-13, C23633-14




CAS No. Surrogate Recoveries Limits


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Blank Spike/Blank Spike Duplicate Summary Page 1 of 1 Job Number: C23633Account: MTXFPNJ Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchVR416-BS R11643.D 1 09/18/12 BD n/a n/a VR416VR416-BSD R11644.D 1 09/18/12 BD n/a n/a VR416


C23633-1, C23633-2, C23633-3, C23633-4, C23633-5, C23633-6, C23633-7, C23633-8, C23633-9, C23633-10, C23633-11, C23633-12, C23633-13, C23633-14

Spike BSP BSP BSD BSD LimitsCAS No. Compound ug/l ug/l % ug/l % RPD Rec/RPD

67-64-1 Acetone 80 90.9 114 89.1 111 2 60-130/3071-43-2 Benzene 20 25.2 126 26.3 132* a 4 60-130/3067-66-3 Chloroform 20 24.9 125 25.3 127 2 60-130/3056-23-5 Carbon tetrachloride 20 22.4 112 24.0 120 7 60-130/3075-35-4 1,1-Dichloroethylene 20 21.0 105 22.6 113 7 60-130/3078-87-5 1,2-Dichloropropane 20 25.0 125 25.6 128 2 60-130/30156-59-2 cis-1,2-Dichloroethylene 20 24.4 122 24.7 124 1 60-130/30156-60-5 trans-1,2-Dichloroethylene 20 23.3 117 24.5 123 5 60-130/30100-41-4 Ethylbenzene 20 25.8 129 26.7 134* b 3 60-130/3075-09-2 Methylene chloride 20 23.9 120 24.0 120 0 60-130/3078-93-3 Methyl ethyl ketone 80 96.7 121 95.5 119 1 60-130/3079-34-5 1,1,2,2-Tetrachloroethane 20 24.8 124 25.3 127 2 60-130/30127-18-4 Tetrachloroethylene 20 23.5 118 25.4 127 8 60-130/30108-88-3 Toluene 20 25.5 128 26.3 132* b 3 60-130/3079-01-6 Trichloroethylene 20 24.4 122 25.7 129 5 60-130/3075-69-4 Trichlorofluoromethane 20 23.1 116 23.1 116 0 60-130/3075-01-4 Vinyl chloride 20 24.8 124 25.5 128 3 60-130/30

m,p-Xylene 40 51.4 129 53.0 133* b 3 60-130/3095-47-6 o-Xylene 20 25.8 129 26.4 132* b 2 60-130/30

CAS No. Surrogate Recoveries BSP BSD Limits

1868-53-7 Dibromofluoromethane 98% 98% 60-130%2037-26-5 Toluene-D8 101% 101% 60-130%460-00-4 4-Bromofluorobenzene 99% 98% 60-130%

(a) Outside control limits (high bias). Not detected in associated samples. AZ:L1(b) Outside control limits (high bias). Not detected in associated samples.

* = Outside of Control Limits.

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Laboratory Control Sample Summary Page 1 of 1 Job Number: C23633Account: MTXFPNJ Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchVR416-LCS R11646.D 1 09/18/12 BD n/a n/a VR416


C23633-1, C23633-2, C23633-3, C23633-4, C23633-5, C23633-6, C23633-7, C23633-8, C23633-9, C23633-10, C23633-11, C23633-12, C23633-13, C23633-14

Spike LCS LCSCAS No. Compound ug/l ug/l % Limits

CAS No. Surrogate Recoveries BSP Limits



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66.3.1

Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 1 Job Number: C23633Account: MTXFPNJ Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Sample File ID DF Analyzed By Prep Date Prep Batch Analytical BatchC23633-2MS R11665.D 1 09/18/12 BD n/a n/a VR416C23633-2MSD R11666.D 1 09/18/12 BD n/a n/a VR416C23633-2 R11650.D 1 09/18/12 BD n/a n/a VR416


C23633-1, C23633-2, C23633-3, C23633-4, C23633-5, C23633-6, C23633-7, C23633-8, C23633-9, C23633-10, C23633-11, C23633-12, C23633-13, C23633-14

C23633-2 Spike MS MS MSD MSD LimitsCAS No. Compound ug/l Q ug/l ug/l % ug/l % RPD Rec/RPD

67-64-1 Acetone ND 80 73.2 92 77.9 97 6 60-130/2571-43-2 Benzene ND 20 21.6 108 22.6 113 5 60-130/2567-66-3 Chloroform 0.23 J 20 21.8 108 22.6 112 4 60-130/2556-23-5 Carbon tetrachloride ND 20 19.2 96 20.0 100 4 60-130/2575-35-4 1,1-Dichloroethylene ND 20 16.9 85 18.3 92 8 60-130/2578-87-5 1,2-Dichloropropane ND 20 21.7 109 22.7 114 5 60-130/25156-59-2 cis-1,2-Dichloroethylene ND 20 20.6 103 21.7 109 5 60-130/25156-60-5 trans-1,2-Dichloroethylene ND 20 19.1 96 20.2 101 6 60-130/25100-41-4 Ethylbenzene ND 20 21.6 108 22.5 113 4 60-130/2575-09-2 Methylene chloride ND 20 19.7 99 21.1 106 7 60-130/2578-93-3 Methyl ethyl ketone ND 80 78.6 98 80.8 101 3 60-130/2579-34-5 1,1,2,2-Tetrachloroethane ND 20 20.5 103 21.7 109 6 60-130/25127-18-4 Tetrachloroethylene 3.7 20 21.5 89 22.5 94 5 60-130/25108-88-3 Toluene ND 20 21.1 106 22.3 112 6 60-130/2579-01-6 Trichloroethylene ND 20 21.2 106 22.1 111 4 60-130/2575-69-4 Trichlorofluoromethane ND 20 17.7 89 18.9 95 7 60-130/2575-01-4 Vinyl chloride ND 20 18.5 93 19.8 99 7 60-130/25

m,p-Xylene ND 40 42.5 106 44.5 111 5 60-130/2595-47-6 o-Xylene ND 20 21.5 108 22.5 113 5 60-130/25

CAS No. Surrogate Recoveries MS MSD C23633-2 Limits

1868-53-7 Dibromofluoromethane 96% 96% 96% 60-130%2037-26-5 Toluene-D8 99% 99% 102% 60-130%460-00-4 4-Bromofluorobenzene 99% 97% 96% 60-130%


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Instrument Performance Check (BFB) Page 1 of 1 Job Number: C23633Account: MTXFPNJ Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Sample: VR412-BFB Injection Date: 09/12/12Lab File ID: R11526.D Injection Time: 09:57 Instrument ID: GCMSR

Raw % Relativem/e Ion Abundance Criteria Abundance Abundance Pass/Fail

50 15.0 - 40.0% of mass 95 714292 26.2 Pass75 30.0 - 60.0% of mass 95 1613653 59.1 Pass95 Base peak, 100% relative abundance 2730325 100.0 Pass96 5.0 - 9.0% of mass 95 179541 6.58 Pass173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass174 50.0 - 100.0% of mass 95 2018816 73.9 Pass175 5.0 - 9.0% of mass 174 166037 6.08 (8.22) a Pass176 95.0 - 101.0% of mass 174 1956181 71.6 (96.9) a Pass177 5.0 - 9.0% of mass 176 129061 4.73 (6.60) b Pass

(a) Value is % of mass 174(b) Value is % of mass 176

This check applies to the following Samples, MS, MSD, Blanks, and Standards:

Lab Lab Date Time Hours ClientSample ID File ID Analyzed Analyzed Lapsed Sample ID

VR412-IC412 R11529.D 09/12/12 11:22 01:25 Initial cal 0.5VR412-IC412 R11530.D 09/12/12 11:48 01:51 Initial cal 1.0VR412-IC412 R11531.D 09/12/12 12:15 02:18 Initial cal 2.5VR412-IC412 R11532.D 09/12/12 12:41 02:44 Initial cal 5.0VR412-ICC412 R11533.D 09/12/12 13:08 03:11 Initial cal 20VR412-IC412 R11534.D 09/12/12 13:34 03:37 Initial cal 50VR412-IC412 R11535.D 09/12/12 14:01 04:04 Initial cal 75VR412-IC412 R11536.D 09/12/12 14:27 04:30 Initial cal 100VR412-ICV412 R11541.D 09/12/12 16:49 06:52 Initial cal verification 20VR412-IC412 R11543.D 09/12/12 17:41 07:44 Initial cal 25VR412-IC412 R11544.D 09/12/12 18:08 08:11 Initial cal 50VR412-IC412 R11545.D 09/12/12 18:34 08:37 Initial cal 75VR412-IC412 R11546.D 09/12/12 19:01 09:04 Initial cal 100VR412-IC412 R11547.D 09/12/12 19:27 09:30 Initial cal 125VR412-IC412 R11548.D 09/12/12 19:53 09:56 Initial cal 250VR412-IC412 R11549.D 09/12/12 20:20 10:23 Initial cal 500VR412-IC412 R11550.D 09/12/12 20:46 10:49 Initial cal 1000VR412-ICV412 R11552.D 09/12/12 21:39 11:42 Initial cal verification 125

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Raw % Relativem/e Ion Abundance Criteria Abundance Abundance Pass/Fail

50 15.0 - 40.0% of mass 95 662382 26.4 Pass75 30.0 - 60.0% of mass 95 1481045 58.9 Pass95 Base peak, 100% relative abundance 2513067 100.0 Pass96 5.0 - 9.0% of mass 95 167637 6.67 Pass173 Less than 2.0% of mass 174 0 0.00 (0.00) a Pass174 50.0 - 100.0% of mass 95 1904811 75.8 Pass175 5.0 - 9.0% of mass 174 156843 6.24 (8.23) a Pass176 95.0 - 101.0% of mass 174 1853952 73.8 (97.3) a Pass177 5.0 - 9.0% of mass 176 119712 4.76 (6.46) b Pass

(a) Value is % of mass 174(b) Value is % of mass 176

This check applies to the following Samples, MS, MSD, Blanks, and Standards:


VR416-CC412 R11641.D 09/18/12 10:22 00:19 Continuing cal 20VR416-CC412 R11642.D 09/18/12 10:53 00:50 Continuing cal 125VR416-BS R11643.D 09/18/12 11:20 01:17 Blank SpikeVR416-BSD R11644.D 09/18/12 11:46 01:43 Blank Spike DuplicateVR416-LCS R11646.D 09/18/12 12:45 02:42 Laboratory Control SampleVR416-MB R11647.D 09/18/12 13:11 03:08 Method BlankZZZZZZ R11648.D 09/18/12 13:38 03:35 (unrelated sample)C23633-1 R11649.D 09/18/12 14:04 04:01 TB001-09122012C23633-2 R11650.D 09/18/12 14:31 04:28 EPAMW57A-09122012C23633-7 R11651.D 09/18/12 14:57 04:54 EB001-09122012C23633-14 R11652.D 09/18/12 15:23 05:20 EB001-09132012C23633-3 R11653.D 09/18/12 15:50 05:47 EPAMW15C-09122012C23633-4 R11654.D 09/18/12 16:16 06:13 MW21-09122012C23633-5 R11655.D 09/18/12 16:43 06:40 EPAMW1A-09122012C23633-6 R11656.D 09/18/12 17:09 07:06 EPAMW1C-09122012C23633-8 R11657.D 09/18/12 17:36 07:33 MW27-09132012C23633-9 R11658.D 09/18/12 18:02 07:59 EPAMW5C-09132012C23633-10 R11659.D 09/18/12 18:28 08:25 EPAMW56A-09132012ZZZZZZ R11660.D 09/18/12 18:55 08:52 (unrelated sample)C23633-11 R11661.D 09/18/12 19:21 09:18 EPAMW48A-09132012C23633-12 R11662.D 09/18/12 19:48 09:45 EPAMW3C-09132012C23633-13 R11663.D 09/18/12 20:14 10:11 DUP001-09132012ZZZZZZ R11664.D 09/18/12 20:40 10:37 (unrelated sample)C23633-2MS R11665.D 09/18/12 21:07 11:04 Matrix Spike

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C23633-2MSD R11666.D 09/18/12 21:33 11:30 Matrix Spike Duplicate

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66.5.2

Volatile Internal Standard Area Summary Page 1 of 1 Job Number: C23633Account: MTXFPNJ Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Check Std: VR416-CC412 Injection Date: 09/18/12Lab File ID: R11641.D Injection Time: 10:22 Instrument ID: GCMSR Method: SW846 8260B

IS 1 IS 2 IS 3 IS 4AREA RT AREA RT AREA RT AREA RT

Check Std 6229326 11.11 9985168 12.42 9171174 16.08 4686046 19.06Upper Limit a 12458652 11.61 19970336 12.92 18342348 16.58 9372092 19.56Lower Limit b 3114663 10.61 4992584 11.92 4585587 15.58 2343023 18.56

Lab IS 1 IS 2 IS 3 IS 4Sample ID AREA RT AREA RT AREA RT AREA RT

VR416-BS 5488443 11.11 8949291 12.42 8022946 16.08 4208063 19.06VR416-BSD 5669086 11.10 9157919 12.42 8264574 16.08 4245055 19.06VR416-LCS 6769785 11.10 10925773 12.42 9775438 16.08 4980022 19.06VR416-MB 5424078 11.11 8823294 12.42 7882166 16.08 3949151 19.06ZZZZZZ 5853431 11.10 9529454 12.42 8572212 16.08 4271166 19.06C23633-1 4841541 11.10 7944440 12.41 7040755 16.08 3543317 19.06C23633-2 5570776 11.10 9022677 12.42 7972070 16.08 4033761 19.06C23633-7 6343013 11.10 10074450 12.42 9019245 16.08 4587719 19.06C23633-14 6173209 11.10 9826604 12.42 8771501 16.08 4454430 19.06C23633-3 5587827 11.10 8891377 12.42 7886254 16.08 4039596 19.06C23633-4 6134083 11.10 9833600 12.42 8727810 16.08 4459902 19.06C23633-5 4928708 11.10 7807580 12.42 7027160 16.08 3516160 19.06C23633-6 5153245 11.10 8259622 12.42 7463880 16.08 3740341 19.06C23633-8 4812626 11.10 7908610 12.42 7129836 16.08 3548669 19.06C23633-9 5363667 11.10 8621168 12.42 7799226 16.08 3930167 19.06C23633-10 4939559 11.10 7994859 12.42 7235872 16.08 3601082 19.06ZZZZZZ 6663718 11.10 10621194 12.42 9661176 16.08 4896273 19.06C23633-11 4682700 11.10 7446602 12.42 6624370 16.08 3368077 19.06C23633-12 4700351 11.10 7480407 12.42 6728569 16.08 3428664 19.06C23633-13 4698922 11.10 7568049 12.42 6828248 16.08 3442403 19.06ZZZZZZ 5572409 11.10 8806032 12.42 7985162 16.08 4082156 19.06C23633-2MS 6041687 11.10 9722341 12.42 9111059 16.08 4871622 19.06C23633-2MSD 5642618 11.10 9077596 12.42 8376291 16.08 4358831 19.06

IS 1 = PentafluorobenzeneIS 2 = 1,4-DifluorobenzeneIS 3 = Chlorobenzene-D5IS 4 = 1,4-Dichlorobenzene-d4

(a) Upper Limit = +100% of check standard area; Retention time +0.5 minutes.(b) Lower Limit = -50% of check standard area; Retention time -0.5 minutes.

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Volatile Surrogate Recovery Summary Page 1 of 1 Job Number: C23633Account: MTXFPNJ Matrix New World Engineering, Inc.Project: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Method: SW846 8260B Matrix: AQ

Samples and QC shown here apply to the above method

Lab LabSample ID File ID S1 S2 S3

C23633-1 R11649.D 99.0 100.0 94.0C23633-2 R11650.D 96.0 102.0 96.0C23633-3 R11653.D 97.0 103.0 96.0C23633-4 R11654.D 97.0 101.0 95.0C23633-5 R11655.D 97.0 101.0 94.0C23633-6 R11656.D 96.0 101.0 95.0C23633-7 R11651.D 95.0 100.0 96.0C23633-8 R11657.D 99.0 101.0 95.0C23633-9 R11658.D 98.0 101.0 96.0C23633-10 R11659.D 99.0 100.0 95.0C23633-11 R11661.D 98.0 102.0 96.0C23633-12 R11662.D 99.0 101.0 95.0C23633-13 R11663.D 100.0 100.0 94.0C23633-14 R11652.D 96.0 99.0 95.0C23633-2MS R11665.D 96.0 99.0 99.0C23633-2MSD R11666.D 96.0 99.0 97.0VR416-BS R11643.D 98.0 101.0 99.0VR416-BSD R11644.D 98.0 101.0 98.0VR416-LCS R11646.D 93.0 102.0 96.0VR416-MB R11647.D 98.0 102.0 95.0

Surrogate RecoveryCompounds Limits

S1 = Dibromofluoromethane 60-130%S2 = Toluene-D8 60-130%S3 = 4-Bromofluorobenzene 60-130%

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Initial Calibration Summary Page 1 of 3 Job Number: C23633 Sample: VR412-ICC412Account: MTXFPNJ Matrix New World Engineering, Inc. Lab FileID: R11533.DProject: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Response Factor Report MSVOA-R

Method : C:\msdchem\1\METHODS\VR412_120912.M (RTE Integrator)Title : EPA -8260BLast Update : Thu Sep 13 11:49:53 2012Response via : Initial Calibration

Calibration Files1 =R11543.D 2 =R11544.D 3 =R11545.D 4 =R11546.D 5 =R11547.D 6 =R11548.D 7 =R11549.D 8 =R11550.D

Compound 1 2 3 4 5 6 7 8 Avg %RSD---------------------------------------------------------------------------

1) I Pentafluorobenzene ----------------ISTD---------------------2) Dichlorodifl 1.278 0.739 1.128 1.075 0.970 1.059 1.142 0.985 1.047 15.09

---- Linear regression ---- Coefficient = 0.9920 Response Ratio = 0.02909 + 1.03844 *A

3) Chloromethan 1.569 1.300 1.381 1.306 1.180 1.185 1.307 1.115 1.293 10.94 4) Vinyl Chlori 1.301 0.898 1.166 1.106 0.969 1.016 1.123 0.972 1.069 12.19 5) Bromomethane 0.931 0.697 0.768 0.735 0.674 0.676 0.751 0.639 0.734 12.35 6) Chloroethane 0.822 0.586 0.680 0.642 0.586 0.601 0.668 0.568 0.644 12.83 7) Ethanol 0.008 0.006 0.006 0.007 0.006 0.007 0.007 0.007# 9.47 8) Trichloroflu 1.841 1.208 1.742 1.662 1.372 1.532 1.672 1.435 1.558 13.52 9) Acrolein 0.199 0.148 0.162 0.154 0.148 0.149 0.163 0.136 0.158 12.04 10) Acetone 0.086 0.082 0.072 0.064 0.064 0.068 0.058 0.071# 14.55 11) Freon 113 0.671 0.425 0.621 0.593 0.491 0.549 0.604 0.532 0.561 13.96 12) 1,1-Dichloro 0.890 0.613 0.756 0.723 0.625 0.674 0.754 0.644 0.710 12.94 13) tert-Butanol 0.152 0.110 0.116 0.116 0.112 0.114 0.128 0.111 0.120 11.69 14) Acetonitrile 2.396 1.747 1.985 1.917 1.772 1.800 1.990 1.666 1.909 11.96 15) Methyl Aceta 1.078 1.156 1.083 0.881 0.883 0.964 0.810 0.979 13.16 16) Allyl Chlori 0.635 0.492 0.554 0.524 0.489 0.498 0.555 0.468 0.527 10.18 17) Iodomethane 1.669 1.242 1.396 1.316 1.231 1.255 1.403 1.193 1.338 11.52 18) Diethyl ethe 0.690 0.518 0.564 0.530 0.497 0.500 0.551 0.463 0.539 12.76 19) Methylene Ch 1.270 1.179 1.021 0.891 0.886 0.974 0.819 1.006 16.42

---- Quadratic regression ---- Coefficient = 0.9921 Response Ratio = -0.05378 + 1.07114 *A + -0.02232 *A^2

20) Acrylonitril 0.381 0.310 0.326 0.321 0.295 0.295 0.324 0.272 0.316 10.17 21) Carbon Disul 3.227 2.344 2.848 2.720 2.447 2.593 2.879 2.438 2.687 10.91 22) Methyl-t-but 3.790 2.889 3.159 2.991 2.763 2.783 3.045 2.529 2.994 12.55 23) trans-1,2-Di 1.175 0.846 0.942 0.891 0.799 0.829 0.918 0.778 0.897 14.00 24) Hexane 1.159 0.718 1.098 1.059 0.899 0.995 1.100 0.942 0.996 14.27 25) Diisopropyl 4.984 3.807 4.111 3.922 3.638 3.636 3.966 3.264 3.916 12.85 26) 1,1-Dichloro 2.560 1.927 2.143 2.047 1.865 1.886 2.071 1.726 2.028 12.46 27) Vinyl Acetat 4.539 3.412 3.800 3.571 3.367 3.384 3.658 2.970 3.588 12.72 28) Chloroprene 2.031 1.438 1.811 1.805 1.597 1.724 1.896 1.593 1.737 10.93 29) Propionitril 0.159 0.120 0.140 0.131 0.122 0.124 0.135 0.113 0.131 11.00 30) tert-Butyl E 4.423 3.410 3.784 3.568 3.294 3.299 3.578 2.946 3.538 12.32 31) Tetrahydrofu 0.324 0.359 0.337 0.299 0.306 0.333 0.280 0.320 8.30 32) 2-Butanone ( 0.116 0.085 0.096 0.091 0.086 0.088 0.096 0.081 0.093# 11.89 33) 2,2-Dichloro 2.168 1.537 1.808 1.686 1.536 1.587 1.717 1.433 1.684 13.60 34) cis-1,2-Dich 1.385 0.965 1.073 1.017 0.941 0.961 1.070 0.901 1.039 14.66 35) Methacryloni 0.434 0.322 0.366 0.352 0.331 0.341 0.372 0.315 0.354 10.74 36) Isobutyl Alc 0.059 0.043 0.051 0.047 0.046 0.048 0.054 0.046 0.049# 10.38 37) Chloroform 2.491 1.946 2.161 2.041 1.889 1.890 2.070 1.718 2.026 11.43 38) Bromochlorom 0.566 0.450 0.499 0.458 0.427 0.435 0.482 0.406 0.465 10.80 39) Dibromofluor 0.683 0.668 0.674 0.666 0.655 0.655 0.649 0.646 0.662 1.95 40) 1,1,1-Trichl 2.076 1.404 1.789 1.692 1.482 1.561 1.723 1.455 1.648 13.42

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41) Cyclohexane 1.717 1.104 1.606 1.547 1.272 1.432 1.582 1.367 1.453 13.77 42) tert-Amyl Me 3.739 2.841 3.125 2.927 2.741 2.777 3.021 2.502 2.959 12.41

43) I 1,4-Difluorobenzene ----------------ISTD---------------------44) 1,1-Dichloro 1.018 0.738 0.926 0.899 0.783 0.845 0.936 0.790 0.867 10.86 45) Carbon Tetra 1.024 0.721 0.947 0.907 0.797 0.870 0.963 0.820 0.881 11.27 46) 1,2-Dichloro 1.396 1.114 1.196 1.129 1.050 1.052 1.143 0.939 1.127 11.84 47) Benzene 2.921 2.154 2.417 2.321 2.144 2.192 2.379 1.736 2.283 14.62 48) Trichloroeth 0.741 0.578 0.659 0.635 0.578 0.601 0.673 0.569 0.629 9.49 49) 1,2-Dichloro 0.824 0.652 0.697 0.661 0.621 0.633 0.701 0.588 0.672 10.71 50) Methyl Metha 0.674 0.460 0.577 0.564 0.528 0.562 0.623 0.532 0.565 11.36 51) Methylcycloh 0.909 0.601 0.879 0.844 0.717 0.796 0.873 0.748 0.796 12.97 52) 1,4-Dioxane 0.003 0.003 0.003 0.003 0.003 0.003 0.003 0.003# 5.84 53) Bromodichlor 1.209 0.918 1.031 0.996 0.954 0.973 1.075 0.892 1.006 10.02 54) Dibromometha 0.531 0.425 0.464 0.439 0.414 0.423 0.463 0.387 0.444 9.83 55) 2-Chloroethy 0.430 0.344 0.391 0.367 0.363 0.378 0.415 0.352 0.380 7.94 56) 4-Methyl-2-P 0.759 0.600 0.678 0.660 0.631 0.637 0.619 0.431 0.627 14.80 57) cis-1,3-Dich 1.231 0.971 1.077 1.043 1.006 1.032 1.141 0.950 1.057 8.75

58) I Chlorobenzene-d5 ----------------ISTD---------------------59) Toluene-d8 1.435 1.413 1.398 1.398 1.401 1.409 1.415 1.402 1.409 0.88 60) Toluene 1.834 1.428 1.551 1.496 1.391 1.430 1.605 1.339 1.509 10.39 61) trans-1,3-Di 1.358 1.059 1.165 1.132 1.093 1.107 1.223 1.016 1.144 9.35 62) Ethyl Methac 0.850 0.673 0.756 0.761 0.764 0.798 0.893 0.749 0.780 8.60 63) 1,1,2-Trichl 0.621 0.445 0.497 0.470 0.445 0.451 0.505 0.422 0.482 13.01 64) 2-Hexanone 0.612 0.478 0.533 0.517 0.495 0.500 0.533 0.387 0.507 12.46 65) 1,3-Dichloro 1.225 0.944 1.032 0.981 0.918 0.933 1.032 0.862 0.991 11.17 66) Tetrachloroe 0.572 0.441 0.516 0.499 0.434 0.471 0.547 0.484 0.495 9.81 67) Dibromochlor 0.743 0.605 0.672 0.662 0.643 0.669 0.753 0.635 0.673 7.65 68) 1,2-Dibromoe 0.653 0.501 0.551 0.535 0.504 0.517 0.576 0.484 0.540 10.07 69) Chlorobenzen 2.004 1.571 1.709 1.632 1.540 1.584 1.783 1.427 1.656 10.68 70) 1,1,1,2-Tetr 0.805 0.613 0.683 0.636 0.620 0.636 0.723 0.617 0.667 10.14 71) Ethyl Benzen 3.725 2.853 3.181 3.078 2.850 2.920 2.676 3.040 11.31 72) Xylene, m+p 1.271 0.962 1.092 1.057 1.003 1.054 1.127 1.081 9.24 73) Xylene, o 1.264 0.960 1.069 1.046 0.993 1.033 1.178 1.005 1.068 9.57 74) Styrene 1.983 1.579 1.771 1.753 1.733 1.821 2.056 1.541 1.780 9.95 75) cis-1,4-dich 0.296 0.199 0.222 0.222 0.236 0.249 0.276 0.237 0.242 12.92 76) Bromoform 0.486 0.376 0.408 0.417 0.416 0.437 0.496 0.423 0.432 9.28 77) Cyclohexanon 0.015 0.017 0.016 0.016 0.015 0.019 0.016 0.016# 7.16 78) Isopropylben 3.286 2.486 2.930 2.823 2.635 2.742 2.723 2.804 9.08 79) 4-Bromofluor 0.602 0.598 0.595 0.596 0.612 0.612 0.615 0.616 0.606 1.45 80) 1,2,3-Trichl 0.326 0.307 0.276 0.261 0.266 0.292 0.245 0.282 10.00 81) trans-1,4-Di 0.288 0.234 0.261 0.259 0.262 0.269 0.294 0.245 0.264 7.51

82) I 1,4-Dichlorobenzene-d ----------------ISTD---------------------83) 1,1,2,2-Tetr 1.667 1.240 1.372 1.320 1.221 1.252 1.386 1.167 1.328 11.78 84) n-Propylbenz 8.101 6.100 7.058 6.778 6.182 6.354 5.666 6.606 12.13 85) Bromobenzene 1.669 1.297 1.384 1.321 1.229 1.274 1.437 1.222 1.354 10.84 86) 1,3,5-Trimet 5.465 4.182 4.776 4.593 4.293 4.450 4.795 3.451 4.501 12.87 87) 2-Chlorotolu 6.204 4.601 5.048 4.869 4.321 4.576 5.050 3.855 4.815 14.28 88) 4-Chlorotolu 5.312 3.979 4.622 4.334 3.860 4.033 4.439 3.239 4.227 14.41 89) tert-Butylbe 5.092 3.773 4.483 4.285 3.947 4.202 4.713 3.629 4.266 11.50 90) Pentachloroe 1.017 0.781 0.883 0.836 0.857 0.879 0.995 0.819 0.883 9.38 91) 1,2,4-Trimet 5.683 4.441 4.973 4.828 4.511 4.635 4.767 3.362 4.650 13.93 92) sec-Butylben 6.554 4.738 5.853 5.652 5.149 5.427 5.035 5.487 11.00 93) p-Isopropylt 5.680 4.152 4.961 4.793 4.451 4.686 4.568 4.756 10.14 94) 1,3-Dichloro 3.100 2.429 2.672 2.560 2.383 2.465 2.764 2.317 2.586 9.88 95) 1,4-Dichloro 3.283 2.494 2.737 2.569 2.435 2.500 2.819 2.338 2.647 11.36 96) n-Butylbenze 6.022 4.289 5.290 5.065 4.605 4.789 4.387 4.921 12.22 97) 1,2-Dichloro 2.873 2.277 2.566 2.373 2.231 2.306 2.594 2.179 2.425 9.69

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98) 1,2-Dibromo- 0.307 0.339 0.335 0.298 0.303 0.335 0.280 0.314 7.20 99) 1,2,4-Trichl 2.411 1.737 1.886 1.799 1.717 1.813 2.080 1.772 1.902 12.39

100) Hexachlorobu 1.308 0.879 0.978 0.965 0.857 0.931 1.082 0.933 0.992 14.63 101) Naphthalene 4.570 3.435 3.810 3.626 3.460 3.601 3.860 2.796 3.645 13.64 102) 1,2,3-Trichl 1.994 1.509 1.623 1.565 1.439 1.516 1.736 1.481 1.608 11.29

103) I 1,4-Dichlorobenzene-d ----------------ISTD---------------------104) TPH-GRO (C6- 8.501 5.577 6.109 6.676 6.224 5.677 5.973 5.220 6.245 16.23

---- Quadratic regression ---- Coefficient = 0.9989 Response Ratio = -0.50540 + 6.43604 *A + -0.01200 *A^2

----------------------------------------------------------------------------(#) = Out of Range ### Number of calibration levels exceeded format ###

VR412_120912.M Thu Sep 13 14:07:19 2012

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Initial Calibration Verification Page 1 of 3 Job Number: C23633 Sample: VR412-ICV412Account: MTXFPNJ Matrix New World Engineering, Inc. Lab FileID: R11541.DProject: PGA-N Phoenix-Goodyear Airport North, 102 S. Litchfield Road, Phoenix, AZ

Evaluate Continuing Calibration Report

Data File : C:\msdchem\1\DATA\120912\R11541.D Vial: 14Acq On : 12 Sep 2012 4:49 pm Operator: beladSample : ICV412-20 Inst : MSVOA-RMisc : MS1603,VR412,50,,,,1 Multiplr: 1.00MS Integration Params: RTEINT.P

Method : C:\msdchem\1\METHODS\VR412_120912.M (RTE Integrator)Title : EPA -8260BLast Update : Thu Sep 13 11:49:53 2012Response via : Multiple Level Calibration

Min. RRF : 0.100 Min. Rel. Area : 50% Max. R.T. Dev 0.50minMax. RRF Dev : 20% Max. Rel. Area : 200%

Compound AvgRF CCRF %Dev Area% Dev(min)R.T.----------------------------------------------------------------------------1 I Pentafluorobenzene 1.000 1.000 0.0 83 0.00 11.03

----------------------- Amount Calc. %Drift -------------2 T Dichlorodifluoromethane 20.000 20.976 -4.9 94 0.00 4.21

----------------------- AvgRF CCRF %Dev --------------3 P Chloromethane 1.293 1.402 -8.4 99 0.02 4.604 C Vinyl Chloride 1.069 1.118 -4.6 96 0.02 4.875 T Bromomethane 0.734 0.797 -8.6 98 0.01 5.726 T Chloroethane 0.644 0.682 -5.9 96 0.00 5.897 T Ethanol 0.007 0.006# 14.3 78 0.01 6.008 T Trichlorofluoromethane 1.558 1.562 -0.3 94 -0.01 6.559 T Acrolein 0.158 0.167 -5.7 94 -0.02 7.1610 T Acetone 0.071 0.075# -5.6 96 0.00 7.2811 T Freon 113 0.561 0.564 -0.5 95 0.00 7.5112 M,C 1,1-Dichloroethene 0.710 0.723 -1.8 96 0.00 7.7013 T tert-Butanol (TBA) 0.120 0.121 -0.8 89 0.01 7.7814 T Acetonitrile 1.909 2.053 -7.5 96 -0.01 8.3215 T Methyl Acetate 0.979 1.039 -6.1 98 0.00 8.1916 T Allyl Chloride 0.527 0.572 -8.5 97 0.00 8.3217 T Iodomethane 1.338 1.452 -8.5 98 0.00 8.1918 T Diethyl ether 0.539 0.588 -9.1 98 0.02 7.08

----------------------- Amount Calc. %Drift -------------19 T Methylene Chloride 20.000 21.963 -9.8 102 0.00 8.48

----------------------- AvgRF CCRF %Dev --------------20 T Acrylonitrile 0.316 0.345 -9.2 97 0.00 8.5621 T Carbon Disulfide 2.687 2.819 -4.9 96 0.00 8.5922 T,M Methyl-t-butyl Ether 2.994 3.260 -8.9 98 0.00 8.8823 T trans-1,2-Dichloroethene 0.897 0.926 -3.2 96 0.00 9.0724 T Hexane 0.996 1.035 -3.9 95 0.00 9.3725 T Diisopropyl Ether 3.916 4.280 -9.3 98 0.00 9.6726 P 1,1-Dichloroethane 2.028 2.176 -7.3 97 0.00 9.7127 T Vinyl Acetate 3.588 3.963 -10.5 98 0.00 9.6728 T Chloroprene 1.737 1.827 -5.2 95 0.00 9.9129 T Propionitrile 0.131 0.143 -9.2 97 -0.01 10.2630 T tert-Butyl Ethyl Ether 3.538 3.899 -10.2 98 0.00 10.2931 T Tetrahydrofuran 0.320 0.355 -10.9 98 -0.01 11.1132 T 2-Butanone (MEK) 0.093 0.102 -9.7 98 0.00 10.2733 T 2,2-Dichloropropane 1.684 1.753 -4.1 95 0.01 10.6234 T cis-1,2-Dichloroethene 1.039 1.111 -6.9 98 0.00 10.62

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35 T Methacrylonitrile 0.354 0.391 -10.5 98 0.00 10.6336 T Isobutyl Alcohol 0.049 0.051# -4.1 92 0.00 10.7737 C Chloroform 2.026 2.211 -9.1 97 0.00 10.8538 T Bromochloromethane 0.465 0.511 -9.9 99 0.00 11.0439 S,M Dibromofluoromethane 0.662 0.664 -0.3 84 0.00 11.1340 T 1,1,1-Trichloroethane 1.648 1.689 -2.5 95 0.00 11.4841 T Cyclohexane 1.453 1.460 -0.5 95 0.00 11.6242 T tert-Amyl Methyl Ether 2.959 3.245 -9.7 98 0.00 11.88

43 I 1,4-Difluorobenzene 1.000 1.000 0.0 83 0.00 12.3544 T 1,1-Dichloropropene 0.867 0.893 -3.0 95 0.00 11.7045 T Carbon Tetrachloride 0.881 0.897 -1.8 94 0.00 11.8646 T 1,2-Dichloroethane 1.127 1.231 -9.2 97 0.00 11.9247 M Benzene 2.283 2.501 -9.5 97 0.00 12.0248 M Trichloroethene 0.629 0.673 -7.0 97 0.00 12.8349 C 1,2-Dichloropropane 0.672 0.731 -8.8 98 0.00 13.0050 T Methyl Methacrylate 0.565 0.615 -8.8 97 0.00 13.0251 T Methylcyclohexane 0.796 0.827 -3.9 96 0.00 13.0452 T 1,4-Dioxane 0.003 0.003# 0.0 78 0.00 13.2353 T Bromodichloromethane 1.006 1.132 -12.5 99 0.00 13.2654 T Dibromomethane 0.444 0.489 -10.1 98 0.00 13.3155 T 2-Chloroethyl-vinyl Ether 0.380 0.429 -12.9 98 0.00 13.5856 T 4-Methyl-2-Pentanone(MIBK 0.627 0.745 -18.8 98 0.00 13.6657 T cis-1,3-Dichloropropene 1.057 1.191 -12.7 98 0.00 13.91

58 I Chlorobenzene-d5 1.000 1.000 0.0 83 0.00 16.0259 S,M Toluene-d8 1.409 1.401 0.6 83 0.00 14.2860 M,C Toluene 1.509 1.634 -8.3 97 0.00 14.3761 T trans-1,3-Dichloropropene 1.144 1.296 -13.3 98 0.00 14.4762 T Ethyl Methacrylate 0.780 0.907 -16.3 98 0.00 14.4763 T 1,1,2-Trichloroethane 0.482 0.532 -10.4 99 0.00 14.6864 T 2-Hexanone 0.507 0.586 -15.6 98 0.00 14.6865 T 1,3-Dichloropropane 0.991 1.088 -9.8 98 0.00 14.9766 T Tetrachloroethene 0.495 0.503 -1.6 96 -0.01 15.1867 T Dibromochloromethane 0.673 0.773 -14.9 100 0.00 15.3168 T 1,2-Dibromoethane (EDB) 0.540 0.602 -11.5 99 0.00 15.5569 M,P Chlorobenzene 1.656 1.823 -10.1 98 0.00 16.0770 T 1,1,1,2-Tetrachloroethane 0.667 0.737 -10.5 99 0.00 16.1071 C, TEthyl Benzene 3.040 3.333 -9.6 97 0.00 16.1372 T Xylene, m+p 1.081 1.183 -9.4 98 0.00 16.2273 T Xylene, o 1.068 1.179 -10.4 98 0.00 16.7474 T Styrene 1.780 2.067 -16.1 99 0.00 16.7475 T cis-1,4-dichloro-2-butene 0.242 0.282 -16.5 99 0.00 17.1076 P Bromoform 0.432 0.498 -15.3 99 0.00 17.1477 T Cyclohexanone 0.016 0.015# 6.3 80 0.00 17.1678 T Isopropylbenzene 2.804 3.061 -9.2 96 0.00 17.1879 S,M 4-Bromofluorobenzene 0.606 0.606 0.0 82 0.00 17.4680 T 1,2,3-Trichloropropane 0.282 0.308 -9.2 98 0.01 17.4881 T trans-1,4-Dichloro-2-bute 0.264 0.309 -17.0 98 0.00 17.51

82 I 1,4-Dichlorobenzene-d4 1.000 1.000 0.0 82 0.00 19.0183 P 1,1,2,2-Tetrachloroethane 1.328 1.475 -11.1 99 0.00 17.2984 T n-Propylbenzene 6.606 7.269 -10.0 96 0.00 17.6985 T Bromobenzene 1.354 1.505 -11.2 100 0.00 17.7686 T 1,3,5-Trimethylbenzene 4.501 5.081 -12.9 97 0.00 17.9087 T 2-Chlorotoluene 4.815 5.336 -10.8 101 0.00 17.9588 T 4-Chlorotoluene 4.227 4.756 -12.5 101 0.00 18.0089 T tert-Butylbenzene 4.266 4.687 -9.9 97 0.00 18.4090 T Pentachloroethane 0.883 1.029 -16.5 98 0.00 18.4791 T 1,2,4-Trimethylbenzene 4.650 5.355 -15.2 97 0.00 18.44

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92 T sec-Butylbenzene 5.487 6.032 -9.9 96 0.00 18.6693 T p-Isopropyltoluene 4.756 5.231 -10.0 96 0.00 18.8194 T 1,3-Dichlorobenzene 2.586 2.864 -10.8 98 0.00 18.9495 T 1,4-Dichlorobenzene 2.647 2.935 -10.9 99 0.00 19.0596 T n-Butylbenzene 4.921 5.424 -10.2 96 0.00 19.2997 T 1,2-Dichlorobenzene 2.425 2.691 -11.0 99 0.00 19.4798 T 1,2-Dibromo-3-Chloropropa 0.314 0.352 -12.1 97 0.00 20.2499 T 1,2,4-Trichlorobenzene 1.902 2.058 -8.2 98 0.00 21.20

100 T Hexachlorobutadiene 0.992 0.995 -0.3 95 0.00 21.37101 T Naphthalene 3.645 4.148 -13.8 98 0.00 21.47102 T 1,2,3-Trichlorobenzene 1.608 1.728 -7.5 98 0.00 21.74

103 I 1,4-Dichlorobenzene-d4A 1.000 1.000 0.0 112 0.00 19.01

----------------------- Amount Calc. %Drift -------------104 H TPH-GRO (C6-C10) ----------NA--------------------------------------------------------------------------------------------------------------------------------------------------------------

(#) = Out of Range SPCC's out = 0 CCC's out = 0R11547.D VR412_120912.M Thu Sep 13 14:06:11 2012

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Evaluate Continuing Calibration Report

Data File : C:\msdchem\1\DATA\120912\R11552.D Vial: 25Acq On : 12 Sep 2012 9:39 pm Operator: beladSample : ICV412-125 Inst : MSVOA-RMisc : MS1603,VR412,50,,,,1 Multiplr: 1.00MS Integration Params: RTEINT.P

Method : C:\msdchem\1\METHODS\VR412_120912.M (RTE Integrator)Title : EPA -8260BLast Update : Thu Sep 13 11:49:53 2012Response via : Multiple Level Calibration

Min. RRF : 0.100 Min. Rel. Area : 50% Max. R.T. Dev 0.50minMax. RRF Dev : 20% Max. Rel. Area : 200%

Compound AvgRF CCRF %Dev Area% Dev(min)R.T.----------------------------------------------------------------------------1 I Pentafluorobenzene 1.000 1.000 0.0 76 0.00 11.02

----------------------- Amount Calc. %Drift -------------2 T Dichlorodifluoromethane ----------NA----------

----------------------- AvgRF CCRF %Dev --------------3 P Chloromethane ----------NA----------4 C Vinyl Chloride ----------NA----------5 T Bromomethane ----------NA----------6 T Chloroethane ----------NA----------7 T Ethanol ----------NA----------8 T Trichlorofluoromethane ----------NA----------9 T Acrolein ----------NA----------10 T Acetone ----------NA----------11 T Freon 113 ----------NA----------12 M,C 1,1-Dichloroethene ----------NA----------13 T tert-Butanol (TBA) ----------NA----------14 T Acetonitrile ----------NA----------15 T Methyl Acetate ----------NA----------16 T Allyl Chloride ----------NA----------17 T Iodomethane ----------NA----------18 T Diethyl ether ----------NA----------

----------------------- Amount Calc. %Drift -------------19 T Methylene Chloride ----------NA----------

----------------------- AvgRF CCRF %Dev --------------20 T Acrylonitrile ----------NA----------21 T Carbon Disulfide ----------NA----------22 T,M Methyl-t-butyl Ether ----------NA----------23 T trans-1,2-Dichloroethene ----------NA----------24 T Hexane ----------NA----------25 T Diisopropyl Ether ----------NA----------26 P 1,1-Dichloroethane ----------NA----------27 T Vinyl Acetate ----------NA----------28 T Chloroprene ----------NA----------29 T Propionitrile ----------NA----------30 T tert-Butyl Ethyl Ether ----------NA----------31 T Tetrahydrofuran ----------NA----------32 T 2-Butanone (MEK) ----------NA----------33 T 2,2-Dichloropropane ----------NA----------34 T cis-1,2-Dichloroethene ----------NA----------

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35 T Methacrylonitrile ----------NA----------36 T Isobutyl Alcohol ----------NA----------37 C Chloroform ----------NA----------38 T Bromochloromethane ----------NA----------39 S,M Dibromofluoromethane 0.662 0.673 -1.7 78 0.00 11.1340 T 1,1,1-Trichloroethane ----------NA----------41 T Cyclohexane ----------NA----------42 T tert-Amyl Methyl Ether ----------NA----------

43 I 1,4-Difluorobenzene 1.000 1.000 0.0 77 0.00 12.3444 T 1,1-Dichloropropene ----------NA----------45 T Carbon Tetrachloride ----------NA----------46 T 1,2-Dichloroethane ----------NA----------47 M Benzene ----------NA----------48 M Trichloroethene ----------NA----------49 C 1,2-Dichloropropane ----------NA----------50 T Methyl Methacrylate ----------NA----------51 T Methylcyclohexane ----------NA----------52 T 1,4-Dioxane ----------NA----------53 T Bromodichloromethane ----------NA----------54 T Dibromomethane ----------NA----------55 T 2-Chloroethyl-vinyl Ether ----------NA----------56 T 4-Methyl-2-Pentan