SYLLABI

B. Tech

IN

CHEMICAL ENGINEERING

2016

Department of Chemical Engineering

JAYPEE UNIVERSITY OF ENGINEERING & TECHNOLOGY

A-B ROAD, RAGHOGARH, DIST. GUNA-473226 MP, INDIA

TEACHING SCHEME

Bachelor of Technology (B.Tech.)

Branch – CHE

Year/Sem : Ist Year/Ist Sem

S. No. Code Title Core/Elective L T P Credits

1. 14B11HS111 Presentation & Communication Skills Core 1 2 0 3

2. 14B19HS199 English Audit 2 0 0

3. 14B11MA111 Mathematics-I Core 3 1 0 4

4. 14B11PH111 Physics-I Core 3 1 0 4

5. 14B11CI111 Introduction to Computers &

Programming Core 3 1 0 4

6. 1411EC111 Electrical Circuit Analysis Core 3 1 0 4

7. 14B17PH171 Physics Lab-I Core 0 0 2 1

8. 14B17CI171 Computer Programming Lab Core 0 0 4 2

9. 14B17EC171 Electrical Circuits Lab Core 0 0 2 1

Total 15 4 10 23

Year/Sem : Ist Year/IInd Sem

S. No. Code Title Core/Elective L T P Credits

1. 14B11HS211 Group & Co-operative Processes Core 3 0 0 3

2. 14B11GE211 Environmental Studies Core 3 0 0 3

3. 14B11MA201 Mathematics-II Core 3 1 0 4

4. 14B11PH212 Physics for Chemical Engineers Core 3 1 0 4

5. 14B11CL211 Physical & Inorganic Chemistry Core 3 1 0 4

6. 14B11ME211 Engineering Mechanics Core 3 1 0 4

7. 14B17PH272 Physics Lab-II Core 0 0 2 1

8. 14B17CL271 Physical & Inorganic Chemistry Lab Core 0 0 2 1

9. 14B17ME271 Workshop Practice Lab Core 0 0 2 1

Total 18 4 6 25

Year/Sem : IInd Year/IIIrd Sem

S. No. Code Title Core/Elective L T P Credits

1. 14B11HS311 Managerial Economics Core 3 0 0 3

2. 14B11CL311 Organic Chemistry Core 3 1 0 4

3. 14B11EC314 Electrical & Electronics Engineering Core 3 1 0 4

4. 14B11CL312 Fluid & Fluid-Particle Mechanics Core 3 1 0 4

5. 14B11CL313 Chemical Process Calculations Core 3 1 0 4

6. 14B17CL371 Organic Chemistry Lab Core 0 0 2 1

7. 14B17EC376 Electrical & Electronics Engineering Lab Core 0 0 2 1

8. 14B17ME374 Engineering Graphics & CAD Lab Core 0 0 4 2

9. 14B17CL372 Fluid & Fluid Particle Mechanics Lab Core 0 0 4 2

Total 15 4 12 25

Year/Sem : IInd Year/IVth Sem

S. No. Code Title Core/Elective L T P Credits

1. 14B11HS411 Financial Management Core 3 0 0 3

2. 14B11CL411 Industrial Organic Synthesis Core 3 1 0 4

3. 14B11CL412 Chemical Engineering Thermodynamics Core 3 1 0 4

4. 14B11CL413 Heat Transfer Operations Core 3 1 0 4

5. 14B11CL414 Mass Transfer Operations Core 3 1 0 4

6. 14B17CL415 Chemical Reaction Engineering Core 3 1 0 4

7. 14B17CL471 Heat Transfer Operations Lab Core 0 0 2 1

8. 14B17CL472 Mass Transfer Opns & Thermodynamics Lab

Core 0 0 2 1

9. 14B17CL473 Chemical Reaction Engineering Lab Core 0 0 2 1

Total 18 5 6 26

Year/Sem : IIIrd Year/Vth Sem

S. No. Code Title Core/Elective L T P Credits

1. HSS Electives: Elective 3 0 0 3

14B14HS541 Social & Legal Issues

14B14HS542 Human Psychology

14B14HS543 Professional Ethics

14B14HS544 Macro Economics

2. 14B11CL511 Instrumentation & Process Control Core 3 1 0 4

3. 14B11CL512 Equipment Design and Drawing Core 3 1 0 4

4. 14B11CL513 Design of Separation Processes Core 3 1 0 4

5. 14B11CL514 Chemical Processes Core 3 1 0 4

6. 14B17CL571 Instrumentation & Process Control Lab Core 0 0 2 1

7. 14B17CL572 Equipment Design and Drawing

Practical Core

0 0 2 1

8. 14B17CL573 Separation Processes Lab Core 0 0 2 1

9. 14B14CL541- CL543

DE-1 Elective 3 0 0 3

18 4 6 25

List of Electives for DE-1 Type L T P Credits 14B14CL541 Solid and Hazardous Waste Management Elective 3 0 0 3 14B14CL542 Pharmaceutical Technology Elective 3 0 0 3 14B14CL543 Pulp & Paper Technology Elective 3 0 0 3

Year/Sem : IIIrd Year/VIth Sem

S. No. Code Title Core/Elective L T P Credits

1 HSS Elective Elective 3 0 0 3 14B14HS641 Project Management 14B14HS642 Business Environment 14B14HS643 Fundamentals of Financial Market 14B14HS644 Marketing Management

2 14B11CL611 Environmental Engineering Core 3 1 0 4 3 14B11CL612 Chemical Reactor Design Core 3 1 0 4 4 14B11CL613 Process Modelling & Simulation Core 3 1 0 4 5 14B11CL614 Process Engineering & Safety Core 3 1 0 4 6 14B17CL671 Environmental Engineering Lab Core 0 0 2 1 7 14B17CL672 Process Modelling & Simulation Lab Core 0 0 2 1 8 14B17CL672 Experimental Project Core 0 0 2 1 9 14B14CE641-

CE643 Department Elective – 2 (DE-2) Elective 3 0 0 3

Total 18 4 6 25

List of Electives for DE-2 Type L T P Credits 14B14CL641 Petroleum Refining Elective 3 0 0 3 14B14CL642 Fertilizer Technology Elective 3 0 0 3 14B14CL643 Fluidization Engineering Elective 3 0 0 3

* Students have to proceed for Industrial Training after sixth semester for six weeks. Evaluation for this will be done in Semester VII.

Year/Sem : IVth Year/VIIth Sem

S. No. Code Title Core/Elective L T P Credits

1 HSS Elective Elective 3 0 0 3 14B14HS743 Entrepreneurship and Small Business 14B14HS744 Brand Management 14B14HS745 Human Resource Management 14B14HS746 Total Quality Management

2 14B14CL741- CL743

Department Elective – 3 Elective 3 0 0 3

3 14B14CL744- CL746

Department Elective – 4 Elective 3 0 0 3

4 14B14CL747- CL749

Department Elective – 5 Elective 3 0 0 3

5 14B11CL711 Project Engineering Core 3 1 0 4 6 14B19CL791 Project Part-I Core 0 0 14 7

Total 15 1 14 23

List of Electives For VII Semester Type L T P Credits DE-3

14B14CL741 Cement Technology Elective 3 0 0 3 14B14CL742 Energy Sources & Energy Conservation Elective 3 0 0 3 14B14CL743 Multiphase Reactor Design Elective 3 0 0 3

DE-4 14B14CL744 Polymer Engineering Elective 3 0 0 3 14B14CL745 Adsorptive Process Design Elective 3 0 0 3

14B14CL746 Plant Utilities & Energy Systems Elective 3 0 0 3 DE-5

14B14CL747 Membrane Process Design Elective 3 0 0 3 14B14CL748 Mixing Technology Elective 3 0 0 3 14B14CL749 Piping Engineering Elective 3 0 0 3

Year/Sem : IVth Year/VIIIth Sem

S. No. Code Title Core/Elective L T P Credits

1 HSS Elective Elective 3 0 0 3 14B14HS841 Knowledge Management 14B14HS843 Supply Chain Management 14B14HS844 Management of Technology 14B14HS845 Strategic Management

2 14B14CL841- CL843

Department Elective – 6 Elective 3 0 0 3

3 14B14CL844- CL846

Department Elective – 7 Elective 3 0 0 3

4 14B14CL847- CL850

Department Elective – 8 Elective 3 0 0 3

5 14B14***** Outside Department Elective – 9 Elective 3 0 0 3 6 14B19CL891 Project Part-II Core 0 0 16 8

Total 15 0 16 23

TOTAL CREDITS 195

List of Electives For VIII Semester Type L T P Credits DE-6

14B14CE841 Industrial Catalysis Elective 3 0 0 3 14B14CE842 Thermal Energy Generation Systems Elective 3 0 0 3 14B14CE843 Food Process Engineering Elective 3 0 0 3

DE-7 14B14CE844 Downstream Processing in Biotechnology Elective 3 0 0 3 14B14CE845 Cogeneration Elective 3 0 0 3 14B14CE846 Advanced Process Control Elective 3 0 0 3

DE-8 14B14CE847 Industrial Biotechnology Elective 3 0 0 3 14B14CE848 Fluidized Bed Combustion Elective 3 0 0 3 14B14CE849 Introduction to Computational Fluid Dynamics Elective 3 0 0 3 14B14CE850 Process Simulation and Design Elective 3 0 0 3

DE-9 (Outside Department) 14B14MA843 Optimization Methods For Engineering (Math) Elective 3 0 0 3 14B14PH731 Nanoscience & Technology (Physics) Elective 3 0 0 3 14B14CI857 Introduction to Artificial Intelligence (CSE) Elective 3 0 0 3 14B14ME744 Design of Heat Exchangers (MEC) Elective 3 0 0 3 14B14MA845 Mathematical Methods in Engineering (Math) Elective 3 0 0 3

SYLLABAI

Bachelor of Technology (B. Tech.)

Branch - CHE

Year/Sem: Ist Year/I Sem

14B11HSS111 Presentation and Communications Skills Introduction to Communication, Oral Communication skills: Stress, Rhythm, Intonation, Coherence, Phonetics etc., Listening Skills, Reading Skills: Intensive and Extensive Reading, SQ3R, Vocabulary and morphology, Writing Skills: Letter Writing, Circulars, Notices, Agenda, Minutes, Report Writing, Power point presentation. 14B11PD199 English Conversational Skills, Vocabulary and comprehension, Functional English Grammar: Noun, Pronoun, Verb, Tenses, Narration, Active and Passive voices, Clause etc., Compositions and Translations. 14B11MA111 Mathematics-I Partial differentiation, Taylor’s series, Maxima and Minima, Jacobians, Double integrals Equations to a line, plane, curve and surfaces, Line and surface integrals, Gradient, divergence and curl, Normal and tangent to a surface, Gauss and Stokes theorems, Differential Equations with constants coefficients, Laplace transforms, Algebra of matrices, Determinants, Gauss elimination method, Rank, Eigen values and vectors, Quadratic forms. 14B11PH111 Physics-I Physical Optics: Analytical treatment of interference, Intensity distribution of fringe system, Fresnel’s biprism, Newton’s rings, Diffraction (limited to Fraunhofer class) from Single slit, double slit and Diffraction grating, Polarization, Phenomenological understanding of Birefringence, Principles of use of uniaxial crystals in practical polarizers, compensators and wave plates, Production and analysis of completely polarized light. Optical activity. Relativity: Michelson-Morley experiment, Lorentz transformations, Addition of velocities, Mass variation with velocity, Mass-energy relation. Radiation: Black body radiation, Wein’s law, Rayleigh Jean’s law, Planck’s law of radiation, Compton scattering. Atomic Structure: Origin of spectral lines, spin and orbital angular momentum, Quantum numbers, Atoms in magnetic field, Zeeman Effect. Statistical Distributions: Maxwell-Boltzmann, Bose-Einstein and Fermi-Dirac distributions and their applications. Lasers: Principle and working of laser, Different types of lasers (He-Ne Laser, Ruby Laser, Semiconductor Laser), Holography. 14B17PH171 Physics Lab-I Experiments List 1. To study the variation of magnetic field along the axis of Helmholtz Galvanometer and to determine

its reduction factor. [Set-up no. 1 & 11] 2. To determine the specific rotation of cane sugar solution using Biquartz polarimeter. [Set-up no. 2 &

12] 3. To observe Newton’s rings and to determine the wavelength of sodium light [Set-up no. 3 & 13]

4. To determine the wavelengths of spectral lines Red, Green and Violet of mercury using plane transmission grating. [Set-up no. 4 & 14]

5. To study the presence of energy levels in an atom by Franck-Hertz Experiment. [Set-up no. 5 & 15] 6. To determine the resistance per unit length of a Carey Foster’s bridge and to obtain the specific

resistance of a given wire. [Set-up no. 6 & 16] 7. To determine the Planck’s constant using solar cell. [Set-up no. 7 & 17] 8. To determine the wavelength of sodium light with the help of Fresnel’s biprism. [Set-up no. 8 & 18] 9. To draw hysteresis loop of a ferromagnetic material & calculate its retentivity and coercivity. [Set-

up no. 9 & 19] 10. To study ultrasonic waves in aluminium and to obtain Young’s modulus for it. [Set-up no. 10 & 20] 14B11EC111 Electrical Circuit Analysis Introduction to circuit elements R, L, C and their characteristics, Different types of sources (like AC and DC, current and voltage, dependent and independent), KCL and KVL, Node and Loop analysis, Star and Delta conversion, Thevenin’s and Norton’s theorem, Superposition, Reciprocity, Maximum Power Transfer, Graph Theory, Tree and links, planar networks, Ideal opamp as a circuit element, AC waveform analysis frequency, phase, amplitude, peak, RMS and average value of ac waveform. Single phase ac circuit analysis containing R, L and C, and their combinations, Concepts of impedance, power, active, reactive and apparent power and power factor, Series and parallel resonance, bandwidth and quality factor, Concept of 3-phase ac circuits, star and delta connections, Frequency domain analysis – Laplace transform solution of Integral differential equations, Forced and natural responses, Transient analysis, Concept of two-port Network, Z, Y, transmission (ABCD) and Hybrid parameter, Introduction to electrical filters and transmission line. 14B17EC171 Electrical Circuit Lab List of Experiments Experiment No. 1: To familiarization with the Digital multimeter (DMM) and measurement of various

signals and circuit elements. Experiment No. 2: To familiarization with the CRO, Function generator and power supply. Experiment No. 3: (a) To study & draw the volt-ampere characteristics of the resistor. (b) To study the loading effect of a voltmeter. Experiment No. 4: To verify Thevenin’s Theorem. Experiment No. 5: To verify Tellegen’s Theorem. Experiment No. 6: To verify Superposition Theorem. Experiment No. 7: To verify Reciprocity Theorem. Experiment No. 8: To verify Maximum Power Transfer Theorem. Experiment No. 9: To determine the Z parameters of the given two port network. Experiment No. 10: To determine the Y parameters of the given two port network. Experiment No. 11: To sketch the transient response of RC Low pass filter. Experiment No. 12: To sketch the transient response of RC High pass filter. 14B11CI111 Introduction to Computer Programming Introduction to Programs, Processing programs, Types of Programming Languages, Programming Design tools (Pseudo code and Flowcharts), Program Design, Structured Programming, Problem solving and programming, Quality aspects of structured programs, Testing and Debugging Techniques, Self Learning of Pascal 14B17CI171 Computer Programming Lab Initial exercises on MS office, Familiarity with Microsoft word, Familiarity with Microsoft power point, Familiarity with Microsoft excels, Pattern generating problems, Loop Control and Case Control

Structures, Arrays and Strings, Functions and Pointers, Structures and Union, Recursion, Dynamic Memory Allocation, linked-lists, File I/O, C Library. Year/Sem: Ist Year/II Sem 14B11HS211 Group and Cooperative Process Group- Behaviour, Development, Structure and Process, Team- Types and Contemporary issues, Individual--Personality, Learning, Perception, Values, Attitudes and Job satisfaction, Assertiveness- Communication Styles, self expression, Social Boldness, Emotional intelligence, Transactional Analysis- Ego states, Life position, Transaction, Stroking, Motivation, Leadership, Conflict and Negotiation. 14B11GE211 Environmental Studies The Multidisciplinary nature of environmental studies: Definition, scope and importance, Need for public awareness, Types of Ecosystems, World Biomes, Ecosystem functioning, biogeochemical cycles. Natural resources, their consumption & Protection: Water, Land Energy (Renewable, non-renewable, wind, solar, hydro, Biomass), Mineral, Forest, & Food resources, Role of an individual in conservation of natural resources, Equitable use of resources. Pollution- a threat to environment: Air, Water & Land pollution, sources & causes, Space pollution, causes & effects, toxicity limits of pollutants. Critical issues concerning global Environment (Urbanization, population growth, global warming, climate change, acid rain, ozone depletion etc.) and the Roots in: Cultural, Social, Political, Commercial, industrial, territorial domains. Biodiversity loss: Diversity of flora and fauna, species and wild life diversity, Biodiversity hotspots, threats to biodiversity. Environmental Impact assessment: Objectives of impact assessment, Study of impact parameters, Methods for impact identification, Economics. Environmental standards & Quality: Air, Water & Soil Quality, Pollutant sampling, pollution control systems, Sustainable building, Urban planning, Disaster Management and Contingency Planning, Modern safety systems. Sustainability & Planned reversal of human destruction to environment: redevelopment of brown fields, energy plantations, social forestry, engineering aspects of Re-use & Recycling, biogas for marginal income groups, organic farming, eco-consumerism, dematerialization, green technologies, eco-tourism. Regulation of technology and innovation, Policy and law: Environmental Laws & Regulations (Different Acts – Environmental Protection Act, Air and Water Acts, Wildlife and Forest Acts), US-EPA, National Environmental Policy. Function of pollution control boards (SPCB and CPCB), their roles and responsibilities, Eco-mark Scheme, Laws relating to Urbana and Rural land use, Ethics. Case studies: Industry–Environment interface, Field Work: Explore the surrounding flora & fauna (Study of common plants, insects, birds document environmental assets), documentation of industries in local region and their possible effects, measure of water, air and land quality, Visit to a local polluted site-Urban/Rural /Industrial / Agricultural, Study of simple ecosystems-pond, river, hill slopes etc. 14B11MA211 Mathematics-II

Differential Equations: Second order linear differential equations with variable coefficients; Convergence of series, convergence tests; Solution in series; Bessel and Legendre functions; Chebyshev polynomials. Orthogonality, Second order partial differential equations and their classification; One dimensional wave and diffusion equations and their applications; Laplace and Poisson equations; Use of Green’s function, Complex Variables: Functions of a complex variable; Analytic functions and Cauchy-Riemann equations. Conformal mapping; Poles and singularities; Complex Integration; Taylor’s and Laurent’s series; Cauchy residue theorem, contour integration and their applications

14B11PH211 Physics-II Electromagnetism: Review of vector calculus, Coulomb’s law, Gauss law and its applications, boundary value, Biot-Savart law, Ampere’s law, Faraday’s law of induction, boundary conditions, Electrical and magnetic field in matter, Maxwell’s equations in free space and dielectric media. Electromagnetic waves in matter, Derivations of expressions for energy density and energy flux (Pointing vector) in an electromagnetic field, Radiation pressure. Propagation of EM waves through boundary- Reflection, Refraction, Absorption and Total Internal Reflection. Band theory of solids, carrier scattering, effective mass, Electronic conduction in metals, Intrinsic and extrinsic (n- and p-type) semiconductors and their electrical conductivity; Direct and indirect band gap semiconductors, optical and thermal properties, Hall Effect in semiconductors; Review of Maxwell-Boltzmann, Fermi Dirac and Bose Einstein distribution functions. Equilibrium carrier concentrations, equilibrium thermal generation, intrinsic carrier concentration, Fermi level, dopants, extrinsic semiconductors, Statistics of donors and acceptors, Drift current; electrical mobility. Device Processing Technology: oxidation, diffusion, ion-implantation, deposition, lithography, etching and interconnect. Integrated-Circuit Technology: understanding at the level of Muller and Kamins of integrated-circuit fabrication processes.

14B11ME212 Engineering Mechanics

INTRODUCTION: Idealization of mechanics, Concept of rigid body, External forces (body forces & surface forces), Laws of mechanics. FORRCE SYSTEMS AND EQUILIBRIUM: Introduction to vector, statically equivalent force systems (planar and spatial), free body diagram, Equations of equilibrium and their applications to various systems of forces, Variational mechanics. STRUCTURES AND MACHINES: Plane trusses, Space trusses, Method of joints, Method of section, Graphical method, Frames and machines. DISTRIBUTED FORCES AND MOMENT OF INERTIA: Centroid of composite figures, Area moment of inertia, Mass moment of inertia, Principle axes and principle moment of inertia FRICTION: Introduction of friction, Laws of friction, Wedge, Screw, Belt, and Rolling friction. BEAMS: Different support & loading conditions of Beam, Shear force diagram (SFD), Bending moment diagram (BMD).KINEMATICS AND KINETICS OF RIGID BODIES: Velocity and acceleration, Rotation of rigid bodies, Rolling motion, Plane motion of rigid bodies, Effective forces on a rigid body, D'Alembert's principle, Force, Mass and Acceleration, Work and energy, Impulse and momentum. 14B17PH272 Physics Lab- II

LIST OF EXPERIMENTS

1. To determine the value of specific charge e/m for an electron by Thomson method.

2. To study Hall effect in a P type semiconductor. To determine

(i) Hall voltage and Hall coefficient (ii) Number of charge carriers per unit volume

(iii) Hall angle and mobility.

3. Using Fiber Optic Kit, to determine

(i) Numerical aperture of the fibre.

(ii) Losses in given fibres.

(iii) The power loss in fibre due to addition of air gaps.

(iv) Loss caused by scattering due to bending.

(v) Characteristics of LED.

(vi) Characteristics of Phototransistor.

4. To determine the magnetic susceptibility of a paramagnetic, FeCl3 solution by Quinck’s tube method.

5. To study the dielectric constant and Curie temperature of Ferroelectric ceramics.

6. To study the magnetostriction in metallic rod.

7. To study the Photo-Electric effect and to determine the value of the Planck’s constant.

8. To study the acousto-optic effect and to determine the ultrasonic velocity in the given liquid.

9. To study the variation of resistivity of a semiconductor with temperature and to determine the band gap using Four-Probe method.

10. To study the presence of energy levels in an atom by Franck-Hertz Experiment. 14B11CL211 PHYSICAL & INORGANIC CHEMISTRY Coordinate bond, Werner’s theory, Isomerism, Valence bond theory, Explanation of magnetism, geometry and colour of coordination complexes, Crystal field theory, Octahedral, tetrahedral and square planar complexes, Crystal field stabilization energies, Ideal gas equation, van der Waal Gas Equation; Properties of Liquids: Intermolecular forces; Bonds weaker than covalent bonds e.g. H bond, van der Waal forces and their effects on various properties of liquids: Evaporation, Vapour pressure, Boiling point, heat of vaporization, Nernst equation, Reference electrodes, Electrochemical cells, Applications of emf measurements Chemical Kinetics, Atomic Absorption Spectrometry, NMR, IR/Raman Spectrometry, Mass Spectrometry, Phase rule, One component system (water system, CO2 system), Two component phase diagrams, Applications.

14B17CL271PHYSICAL & INORGANIC CHEMISTRY LAB

LIST OF EXPERIMENTS

1. Measurement of physical properties: Surface tension by Stalagmometer 2. Measurement of physical properties: Viscosity by Ostwald’s viscometer 3. Preparation of standard solutions: NaOH, HCl, KMnO4 4. pH metric titration of:

a. Strong acid (HCl) against strong base (NaOH) b. Weak acid (CH3COOH) against strong base (NaOH) c. Mixture of strong and weak acids against strong base

5. Determination of equivalent conductivity of a strong electrolyte (KNO3) at different concentrations and hence examine the validity of Onsager equation

6. Determination of equivalent conductivity of a weak electrolyte (CH3COOH) with the help of Kohlrausch law

7. Potentiometry: Determination of the solubility and solubility product of AgCl 8. Chemical kinetics: To study the relative strength of two acids 9. Determine the order of Saponification of ethyl acetate with NaOH 6. Determination of depression in freezing point and elevation in boiling point

14B17ME271 Workshop Practice

Unit I Carpentry Shop: Timber: Type, Qualities of timber disease, Timber seasoning, Timber preservation, Wood Working tools: Wood working machinery, joints & joinery. Jobs to cover above courses such as Name Plate, Carpentry joints such as cross halving joint mortise and Tennon joint, Dovetail joint etc.

Unit II Fitting Shop: Metal bench work Measuring instruments; Engineer steel rule, Surface gauges calliper, feeler gauges, Try square and micrometre. Use, Care and maintenance of hand tools such as hammer, Cold chisel of different type, Centre punch, Hack-saw, Dot punch, Different types of files, Use of surface plate, Surface gauges, type of drills, Taps and dies for drilling tapping and screw threads. Fitting operations: Chipping, filling, Drilling and tapping.

Two joints to cover above course such as: Preparation of job piece by making use of filling, sawing and chipping operation. Job having combined-practice for drilling and tapping; Job having combined practice for drilling and reaming.

Unit III Welding: Students are required to make three jobs related to Brazing, Soldering and welding and to know about: Equipment used for Brazing, Soldering and gas, Arc welding. Selection of material and flux used in brazing and soldering Selection of welding rods, flux and pipe for gas welding; Selection of welding machine, Electrodes and current for Arc welding; Use of tools and the equipment’s, Safety precautions. Unit IV Black Smithy Shop: Smithy forges maintenance and control of fire and fuel used in smithy shop. Use of various smithy tools such as swage block; Anvil, different types of Hammers, Tongs, Flatters, Cold set, Hot set, set hammers punches, Calipers (outside and inside). Introduction to forging and forging methods heating metals for forging; Forging operations: Upsetting, Punching and drafting. Three jobs to cover above course such as: Forging of chisel; Forging of C-Ring; Forging of Pan Hook (S-shaped); Forging of screw driver; Forging of hexagonal nut etc.

Unit V Foundry: Pattern Making: Students are required to prepare four jobs related to pattern making and moulding and know about: Pattern materials, pattern allowances and types of patterns. Core box and core print, Use and care of tools used for making wooden patterns. Moulding: Properties of good moulding and core sand, Composition of green sand, Dry sand and loam sand. Care and use of moulding tools; Attempt should be made to expose students to as many workshop practices as feasible. Year/Sem: IInd Year/III Sem

10B11PD311 Managerial Economics

Introduction to Managerial Economics & Macro-economic Concepts: Definition of Economics, Meaning & Scope of Managerial Economics, Micro & Macro Economics, Concept of economic profit, (Opportunity Cost), Concept of Present value. Demand Analysis: Law of demand, Individual & market demand, Determinants of market demand, Marginal Utility theory, Elasticity of demand– Price, Income, Cross, Advertising Theory of Consumer choice using Indifference Curve analysis, Demand forecasting techniques, Delphi, Survey, Time series analysis. Production Theory and Analysis: Production with one variable, optimal employment of a factor of production, Cobb Douglas production function, Production with two variable inputs, Production Isoquants, Production Isocosts, Optimal employment of two inputs, the expansion path, Basics of Supply, Market Equilibrium. Cost Theory and Analysis: Cost concepts – Opportunity, Explicit, Marginal, Incremental and Sunk, Relation between Production & Cost, Short run cost function, Long run cost function, Special topics -Profit contribution analysis, - Break Even analysis, Operating Leverage. Pricing under Different Market Structures: Perfect Competition - Determination of Price output relationship in short run, long run, Monopoly Determination of Price output relationship in short run & long run, Price discrimination, Monopolistic Competition- Determination of Price output

relationship in short run & long run, Product Differentiation, Oligopoly- Types, Determination of Price output relationship, Kinky demand curve {Stickiness of Price}, Price leadership model. 14B11CL311 ORGANIC CHEMISTRY

Fundamentals of organic chemistry, types of bonds in organic compounds, inductive effect, electromeric effect, mesomeric effect, hyper conjugative effect, resonance and resonance energy, substitution reactions, addition reactions, elimination reactions. Industrially important organic chemistry, organic compounds of nitrogen: nitro compounds, diazonium salts, amines. Sulphonation, chlorosulphonation, o-alkylation, acylation, halogenation, oxidation, carboxylation; Important named reactions: Aldol condensation, Cannizaro, Reformatsky, Friedel-Crafts, Diels-Alder, Ullmann, Wurtz reaction; Mechanism and industrial application of rearrangements such as Claisen, Curtius and Fries. Stereochemistry: chirality, concept of stereoisomerisms, classification of stereoisomers, enantiomers and diastereoisomers, geometrical isomerism, E-Z nomenclature. Photochemistry

14B11CL312 FLUID AND FLUID-PARTICLE MECHANICS

Fluid statics, Newtonian and non-Newtonian fluid behaviour; Turbulence, Reynolds number, Boundary layer theory; Equation of continuity; Equations of motion; Bernoulli equation; Flow of incompressible fluids, Laminar flow of Newtonian fluids. Hagen-Poiseuille equation; Turbulent flow in pipes; Von-Karman equation; Friction factor; Friction loss in non-Newtonian fluid flow; Flow through non-circular cross-section; Fluid flow through coils. Basic relationships for compressible flow, adiabatic and isothermal flow of compressible fluids through orifices and pipes; Flow past immersed bodies, fluidization, agitation and mixing of fluids, gas/liquid and liquid/liquid two phase flow; Properties of solids & screen analysis, particle size distribution, size reduction of solids, settling and sedimentation, filtration. 14B11CL313 CHEMICAL PROCESS CALCULATIONS

Concept of unit operations and unit processes; Units and dimensions, stoichiometric relations; Composition of mixtures and solutions; Material balance in systems involving physical changes, material balance in systems involving chemical reactions; Phase diagram, ideal gas law, relationships for real gases and compressibility factory charts, vapour pressure of liquids. Humidity and saturation, psychometric charts; Material balance involving condensation and vaporization; Heat capacity, calculation of enthalpy changes; The general energy balance; Energy balance for systems involving chemical reactions; Material and energy balances in unsteady state systems; Material and energy balances via computer codes. 14B11EC314 ELECTRICAL & ELECTRONICS ENGINEERING THREE PHASE SUPPLY: Star/Delta connections, line and phase voltage/current relations. MAGNETIC CIRCUITS AND TRANSFORMERS: Magnetic circuit concept; Theory and principle of working of single phase transformer. ROTATING MACHINES: Principles of energy conversion and rotating machines, DC machines- types, characteristics and their applications; Synchronous and induction machines; Single phase induction and steeper motors & applications NUMBER SYSTEM & BINARY CODES: Conversion bases, representation of –ve numbers, 1’s & 2’s complements, arithmetic using 2’s complements. Hexadecimal codes, weighted codes, BCD codes, Gray codes & alphanumeric codes, INTRODUCTION TO DIGITAL CIRCUITS: Logic gates, Gate level realization of Boolean expression, Multiplexer, DE multiplexer. Flip-flops, SR, JK, T & D flip-flop, Counters and Registers.

MICROPROCESSOR & APPLICATION (8 BIT): Use and advantage of microprocessor, Architecture and pin configuration of 8-bit microprocessor (Intel 8085), Instruction set, Arithmetic and Logical operation, Application and Interfacing. 14B17CL371ORGANIC CHEMISTRY LAB

LIST OF EXPERIMENTS

1. Preparation of organic compounds, their purification and determination of physical constant (at least 2)

2. Identification of organic compounds a. Single Organic compounds (at least 6) b. Binary mixture of solid organic compounds (at least 3)

3. Organic estimation: a. Estimation of phenol b. Estimation of aniline

4. Industrially important preparations: a. Aspirin (Drug) a. Bakelite (Polymer)

14B17EC376 ELECTRICAL & ELECTRONICS ENGINEERING LAB

LIST OF EXPERIMENTS

Four Experiments on Electrical Engineering; DC Generator (self & separately excited), Single phase Induction Motor, Single and three phase transformer; Five Experiments on Digital Electronics: Logic gates using TTL ICs, Combinational circuits using TTL IC, Multiplexor and Demultiplexure, Flip-flops, Counters and Registers; 3 Experiments on 8085 Microprocessor Programming

14B17ME374 ENGINEERING GRAPHICS & CAD LAB

Introduction: Lettering, Lines, Dimensioning, Scales, and Geometric constructions; Conic Sections: Ellipse, Parabola and Hyperbola; Orthographic Projections: Points, Straight lines, Planes, Simple solids. Isometric Projections: Simple solids: cube, cylinder, prism, cone; Orthographic projections of simple building and machine elements; Applications of AutoCAD Software: Basic terminology, Drawing commands and skills, Project Planning, 3-Dimensional drawing, Advance Tools: Template files, object snap in AutoCAD, line types, file formats, editing and modifying, Inquiry tools, X-Rays in CAD, System variables

14B17CL372FLUID AND FLUID-PARTICLE MECHANICS LAB

LIST OF EXPERIMENTS

1. Reynold’s Apparatus 2. Bernoulli’s Apparatus 3. Venturi Meter 4. Orifice Meter 5. Pitot Tube 6. Rectangular/V-notch 7. Friction Losses in Pipes 8. Minor Losses in Pipes 9. Characteristics of Centrifugal pump 10. Efflux Time of Tank 11. Size Reduction By Jaw Crusher

12. Size Reduction By Hammer Mill 13. Size Reduction By Ball Mill 14. Sieving And Particle Size Distribution 15. Effectiveness Of Screen 16. Elutriation And Particle Size Distribution 17. Batch Sedimentation 18. Plate And Frame Filter Press 19. Vacuum Filter 20. Leaf Filter 21. Cyclone Separator 22. Sigma Mixer

STUDY EXPERIMENTS

1. Newtonian – Pseudo plastic, Viscoelastic, Time-dependent materials. 2. Pumps – Centrifugal , Screw, Diaphragm 3. Fans. 4. Fittings & Valves (Constructional Features) 5. Compressors (Reciprocating, Centrifugal)

Year/Sem: IInd Year/IV Sem 14B11HS411 Financial Management

Introduction, Scope and Objectives, Basic Financial Concept, Time value of money, Capital budgeting techniques, Cash flows, Long term sources of finances; Concept and measurement of cost of capital, Leverages, EBIT-EPS analysis, Working capital management- Inventory Management, Financial Statement analysis.

14B11CL411 INDUSTRIAL ORGANIC SYNTHESIS

Process involved during organic synthesis: Nitration, halogenation, sulphonation, amination; Synthesis of natural products: carbohydrate, terpenes, alkaloids, steroids. Pigments and their synthesis; Synthesis for industrially important polymers: polyethylene, polystyrene, PVC, polyisobutylene, polyester, nylon, Bakelite, Teflon. Synthesis of important materials for industry: ceramics, glasses, zeolites. 14B11CL412 CHEMICAL ENGINEERING THERMODYNAMICS

Scope and laws of thermodynamics; Concepts of open and closed systems, state and path functions, reversible and irreversible processes, equilibrium, phase rule; PVT behaviour of pure substances; Equations of state; Standard heats of formation, reaction and combustion; Entropy; Applications of first and second laws to steady/unsteady processes in open/closed systems. Compression and expansion processes. Thermodynamic properties of fluids; Refrigeration and liquefaction; Solution thermodynamics, chemical potential and phase equilibria; Partial properties; Excess properties; Fugacity in solution; Concept of activity and activity co-efficient; Property changes of mixing. Vapour-liquid equilibrium in miscible binary and multi component systems, azeotropy, liquid-liquid equilibrium; Solubility of gases and solids in liquids, chemical reaction equilibria in homogenous and heterogeneous systems 14B11CL413 HEAT TRANSFER OPERATIONS

Mechanisms of heat flow: Conduction, natural and forced Convection, Radiation. Concept of resistance to heat transfer. Insulation & critical radius; Extended Heat transfer; Dimensional analysis and dimensionless numbers; Heat transfer by natural and forced convection; Heating and cooling of fluids in forced convection. Heat transfer in agitated vessels. Heat transfer to fluids with phase change: Heat transfer from condensing vapours, heat transfer to boiling liquids. Black body radiation; Stefan-Boltzmann law; Planck’s law; Wein’s displacement law; Kirchoff’s law; Gray body radiation;

Radiation between surfaces; View factors; Radiation from non-luminous gases and luminous flames. Combined conduction, convection and radiation; Design of furnaces; Types of heat exchange equipment; Design of shell and tube heat exchangers, Kern’s method, NTU method, Effectiveness. Types of evaporators; Design of single effect evaporator & multiple effect evaporators 14B11CL414 MASS TRANSFER OPERATIONS Mass transfer operations and their importance; Diffusion and mass transfer between phases, equipment for gas-liquid operations, distillation, vapour-liquid equilibrium. Relative volatility; Flash vaporization; Differential distillation; Continuous rectification of binary systems; Steam distillation, gas absorption; Absorption in plate columns, humidification and dehumidification; Drying, wet bulb, dry bulb and adiabatic saturation temperatures, humidity, drying mechanism, drying rate curves. Crystallization, solubility curves, population balance method. 14B11CL415 CHEMICAL REACTION ENGINEERING Examples of various types of reactions; Formulation and solution of rate equations for simple and complex reactions in batch reactor; Effect of thermodynamic equilibrium; Integral methods of analysis of data; Differential method of analysis of data; Ideal batch reactor and concept of batch time. Flow reactors and concepts of space time/space velocity and holding time/residence time. Ideal mixed flow reactor (MFR) and plug flow reactor (PFR), Irreversible reactions and Reversible reactions in series/parallel applications; Effect of temperature on thermodynamic equilibrium and heats of reaction; Optimum temperature progression. Non catalytic Heterogeneous Reactions models for controlling; Catalytic Heterogeneous reaction Langmuir-Hinshelwood model

14B17CL471 HEAT TRANSFER OPERATIONS LAB LIST OF EXPERIMENTS

1. Thermal Conductivity of Metal 2. Fin Effectiveness 3. Double Pipe Heat Exchanger 4. Shell and Tube Heat Exchanger 5. Emissivity Apparatus 6. Heat Transfer in Agitated Vessels 7. Film wise and Drop wise Condensation 8. Forced Convection Apparatus 9. Natural Convection Apparatus 10. Heat Transfer through Composite Wall 11. Thermal Conductivity of Liquid 12. Single Effect Evaporator 13. Critical Thickness of Insulation 14. Boiling Heat Transfer Apparatus

14B17CL472 MASS TRANSFER OPERATIONS AND THERMODYNAMICS LAB

LIST OF EXPERIMENTS:

1. Diffusion of CCl4 in Air 2. Diffusion of Solid in Air 3. Steam Distillation 4. Differential Distillation 5. Absorption in Packed Column 6. Forced Draft Tray Dryer 7. Rotary Dryer

STUDY EXPERIMENTS:

1. Absorption in Mechanically Agitated Contactor 2. Wetted wall column. 3. Sieve Plate Distillation Column 4. Packed Bed Distillation Column

14B17CL473 CHEMICAL REACTION ENGINEERING LAB LIST OF EXPERIMENTS

1. Performance Study of an Ideal CSTR 2. Isothermal CSTR 3. Cascade of CSTR’s 4. Performance Study of PFR 5. Performance Study of an Ideal PFR ( Coiled Tube Type) 6. Batch Reactor 7. Combined Flow Reactor 8. Isothermal Semi-Batch Reactor

Year/Sem: IIIrd Year/V Sem

14B11HS541 Social & Legal Issues Contract Act, Consumer Laws, Laws of Patent, Company Act, Business ethics and values, Codes of Ethics & Professional Conduct, The place of code of ethics for an Engineer, Ethics in Bio-Tech, Environmental Ethics, Role of Board of Directors, The role of Top Management, Executive Compensation, Legal provisions and SEBI code, Governance mechanism and ethical behaviour, Corporate governance in India, Impact of internet on corporate governance. Intellectual Property Issues (What is Intellectual Property, Copyright law, Software Copyright), Copyright in Cyberspace, Offensive Speech in Cyberspace , pornography, censorship, Bomb-making Information Harassing Speech Online), Liability of service providers. Computer Crimes(Fraud and Embezzlement, Sabotage & Information theft, Intruders, Hacking & Cracking), Computer Crime Laws, Digital Forgery, Cyber Terrorism, Wiretapping, IT Act 2000, ICE Bill. 14B14HS542 Human Psychology Understanding human experience and behaviour: Definition, schools, methods, branches and application of psychology for engineers. Measuring human abilities; Intelligence, Personnel testing; the individual working life; Personality - definition, approaches and theories, Psychological problems of everyday life; Stress and coping; Psychological disorders, human error & Reliability, Work and mental health. Human learning Theories, conflict resolutions, Leadership and management 14B14HS543 Professional Ethics

Introduction, The nature and characteristics of professions, Obligations and professional services, Obligation to clients, professions and third parties; The foundations and norms of professional ethics; The need for separate code of conduct for professionals. The relation between professional and general ethics; Moral conflict and the issue of autonomy of professional ethics; Certain specific issues pertaining to medical ethics, legal ethics, computer ethics and business ethics; Teaching from scriptures and tradition (Geeta, Ramayana, Mahabharata, Upanishads, Vedas, Bible and Quran). Ethical Issues in Capitalism and market systems, Ethics and social responsibility, Ethics and marketing, Ethics in finance, Ethics and human resource, Ethics and Information Technology, Intellectual property rights like designs, patents, trademarks, copy rights,

14B14HS544 Macro Economics

Meaning and Importance of Macro Economics; Concepts of Income, Output and employment – Gross Domestic Product (GDP), GNP, GNI and NNP – methods of measurement of GDP and limitations; monetary policy a fiscal policy, Balance of Payments: Current and Capital Accounts; Disequilibrium in balance of payments and its consequences; Balance of payments, adjustment policies in fixed and flexible exchange rate. Theories of Consumption spending: Absolute, Relative, Permanent Income and Lifecycle hypotheses. Consumption under uncertainty, Price Level at the macro level – WPI and CPI; Theories of Investment spending: Keynesian, Accelerator and Neo-classical, Determination of Money Supply: Functions and Post-war controversy on definition of Money. Theories of Demand for Money: Quantity Theory and Keynes approach. Baumol and Tobin Contributions and Friedman’s restatement of quantity theory; IS and LM curves: Derivation, their shifts and rotations. Simultaneous equilibrium of product market and money market 14B11CL511 INSTRUMENTATION AND PROCESS CONTROL

Concept of feedback and feed forward control, process dynamics in time, Laplace and frequency domains; Concept of stability and optimal control; General performance and characteristics of instruments, Errors and their types. Calibration standards; Different types of sensors; Types of valves, Valve characteristics Selection and sizing of valves; Models for first and second and higher order systems; On-off, proportional, integral, derivative and their combinations. Closed loop transfer functions for servo and regulator problems. Use of Root locus and Frequency Response analyses; Gain margin and phase margin in controller tuning; Performance criterion-IAE, ISE and IATE. Ziegler-Nichols and Cohen-Coon rules; Fundamentals of digital control; Introduction to Z-transforms; D D C and D C S. Ratio control, cascade and adaptive controls. Control strategies for common industrial operations. 14B11CL512 EQUIPMENT DESIGN AND DRAWING Nature of process equipment General design procedure; Review of stresses, temperature effects; Theories of failure; Materials of construction; Code and standards for pressure vessels (IS: 2825:1969); Materials of construction; Pressure Vessel Subjected to Pressure; Storage vessels for volatile and non volatile liquids, gases; Various types of roofs. Nozzles and mountings; various types of agitator, Power requirement, Reaction vessel classifications, materials of construction and design of vessel; Design of jackets (IS 2825) and cols. Classification of supports. Design of skirt support considering stresses due to dead weight, wind load, seismic load and period of vibration; Design of base plate, Skirt bearing plate, anchor bolts, bolting chairs and skirt shell plates; Design of Lug or bracket supports; Codes and standards for heat exchangers; Design of shell and tube heat exchangers as per IS: 4503 and TEMA standards. Basic features of distillation and absorption columns; Stress in columns. 14B11CL513 DESIGN OF SEPARATION PROCESSES Design of sieve plate columns; Design of packed columns; Fractionation of multi component mixtures; multiple feeds and withdrawals; Performance evaluation of packed and plate columns cooling tower process design; Performance evaluation of cooling towers; Process design of crystallizers; Performance evaluation of crystallizers; Process design of dryers Performance evaluation of dryers; Solvent selection for extraction; Ternary liquid equilibria and ternary diagrams; Solid – liquid equilibria Single and multi – stage leaching Staged calculations and efficiency; Performance evaluation; Supercritical fluid extraction; Adsorption and ion exchange process. Adsorption and ion exchange equilibria, various isotherms; Design of fixed bed adsorber; Types of membranes and modules for membranes; Transport through membranes. Ultra filtration; Reverse Osmosis; Electro dialysis; Liquid membranes; Equipment and operations

14B11CL514 CHEMICAL PROCESSES Salient features of manufacture of commodity chemicals. Status of chemical industry in India Nitrogen industries Phosphorus industries, Chlor-alkali industries Manufacture of soda ash. Manufacture of sulphuric acid, Oleum, and sulphur trioxide, Manufacture of lime and cement. Manufacture of oxygen, nitrogen, argon and helium. Manufacture of synthesis gas. Manufacture of acetylene. Manufacture of aluminium, and sodium and sodium chlorate. Outlines of operations and processes in petroleum refining. Engineering aspects of the manufacture with consideration for alternative routes of basic organic chemicals Outlines of synthesis of polymers. Manufacture of soaps and detergents, dyes and intermediates, agrochemicals, perfumery and specialty chemicals. 14B11CL541 SOLID AND HAZARDOUS WASTE MANAGEMENT

Environment and development, Solid, liquid and gaseous emissions, Environmental standards and legal framework, Hazardous wastes, Solid Waste Management, Hazardous Waste Management, Site Remediation: Quantitative risk assessment, Site and sub-surface characterization, Remedial Technologies, Remedial actions and corrective measures, Solid Waste Utilization Options : Concept of waste to wealth, Case studies of solid waste utilization, By-products, Land fill management, Ash management, Incineration, Biological sludge disposal 14B11CL542 PHARMACEUTICAL TECHNOLOGY Chemical properties of drugs of importance to drug formulation, and how these are characterized, Principles of drug formulation and the release of drugs from pharmaceutical dosage forms, Recipients and their properties, Important pharmaceutical unit operations, Manufacturing and packaging of pharmaceutical dosage forms, Quality assurance and quality evaluation including good manufacturing practices. 14B11CL543 PULP AND PAPER TECHNOLOGY

Introduction, raw materials for paper making: Fibrous raw materials, Wood/ Non woods, storage and preparation. Pulping: Chemical and high yield pulping; Alkaline pulping, operation of batch digesters; Modified; Kraft pulping; Processing of secondary fibres, pulp washing, screening and bleaching, stock preparation and paper making, chemical recovery, energy and environmental issues on paper making

14B17CL571 INSTRUMENTATION & PROCESS CONTROL LAB LIST OF EXPERIMENTS

1. Level Control Trainer 2. Temperature Control Trainer 3. Characteristics of PID controller with data logger 4. Water level measuring tutor 5. Temperature measuring tutor (using thermocouple) 6. Temperature measuring tutor (using RTD) 7. Two tank interacting system 8. Two tank non-interacting system 9. Time constant of thermometer 10. Pneumatic control valve Characteristics 11. Bourdon tube Pressure gauge for demonstration 12. Dead Weight Pressure Gauge

14B17CL572 EQUIOMENT DESIGN AND DRAWING PRACTICAL Design of shell and tube heat exchangers, multi pass exchangers; Kern’s method and Donohue equation to estimate shell side heat transfer coefficient. Effectiveness; NTU method Design of single effect evaporator with negligible and appreciable heat of dilution; Design of multiple effect evaporators with effect of liquid head and boiling point elevation; Vapor recompression. Home Assignments or Seminars on Design of Heat Exchange Equipment’s; Types of evaporators: Short tube vertical evaporators; Basket type vertical evaporators; Long tube vertical evaporator; Long tube recirculation evaporator; Falling film evaporator; Rising film evaporator. Plate type evaporator; Evaporator Accessories; Multiple Effect evaporator Methods of feeding; Forward feed; backward feed; mixed feed; Parallel feed. 1. Use of Computer Aided Design Software such as Mechanical Desktop & converter Series Design

Software, IDEAS, Pro Engineer, etc. 2. At least eight design and drawings as suggested by the teacher must be submitted during the term.

14B17CL573 SEPARATION PROCESSES LAB LISTS OF EXPERIMENTS

1. Packed Bed Adsorption Column 2. Liquid-Liquid Extraction in Packed Bed 3. Liquid-Liquid Extraction in Spray Column 4. Solid-Liquid Extraction Apparatus 5. Humidification De-humidification Apparatus 6. Water Cooling Tower 7. Agitated Batch Crystallizer 8. Liquid-Liquid Extraction Data 9. Fluidized Bed Dryer

Year/Sem: IIIrd Year/VI Sem

14B14HS641 Project Management

Project Management Basics, Role, attitude and skills of Project manager, Project Lifecycle, Project Environment, 7’S of Project Management., Project Model. Basics of Project Selection, Risk Management; Key Structure of Project Organization, Project Planning, Project Budgeting and cost estimation; Project Scheduling (Importance, PERT/CPM, AOA and AON charts, Probability analysis). Project Control, Project Termination.

14B14HS642 Business Environment

The concept of Business Environment, significance and nature; Environment Scanning: meaning, nature and scope, the process of environmental scanning, Interaction between internal and external environments, basic philosophies of Capitalism and Socialism with their variants. Concepts of Mixed Economy; Overview of Political, Socio-cultural, Legal, Technological and Global environment; An introduction to MRTP, FEMA, SEBI Act, Consumer Protection Act; The changing dimensions of these laws and their impact on business; Philosophy and strategy of planning in India; Industrial Policy in recent years; Policy with regard to small scale industries; the monetary policy and fiscal policy, Stock Exchange-BSE-NSE; Depository system in India (Options, Futures and Derivatives) RBI-Role and functions, banking structure reforms; Narasimha Committee Recommendations, Financial Sector reforms. E-Banking in India-objectives, trends and practical uses-Recent technological developments in Indian Banking (ATM, Debit and Credit Cards, EMI, EFT) Consumerism, Social Responsibility of business enterprises, New Economic Policy, Globalization, EXIM policy, FDI policy, Multinational Corporation (MNCs) and Transnational Corporations (TNCs), Global Competitiveness.

14B1HS643 Fundamentals of Financial Market

Financial institutions as firms & intermediaries, Financial markets, Lenders and borrowers, The financial system and the real economy, Deposit-taking institutions, Non-deposit-taking institutions, Interest rates. Money market purpose and structure, Money market segments, Money market participants, Money market instruments - Treasury bills and other government securities, Commercial papers, Certificates of deposit, Repurchase agreements, Money market interest rates and yields. Debt market instrument characteristics, Bond market: characteristics & yields, Bond valuation - Discounted models, Bond duration and risk, Bond analysis. Equity instruments - Common shares, preferred shares, Private equity, Primary equity market, Secondary equity market structure, Equity market transactions, Equity market characteristics, Stock valuation, Processes of consolidation of stock exchanges. Hedging against risk, Description of derivatives markets, forward and futures contracts: Principles, valuation, uses, Swaps, Options: definition, components, determinants, Option pricing models.

14B14HS644 Marketing Management

Defining Marketing for the 21st Century, Developing Marketing Strategies and Plans; Gathering Information and Scanning the Environment, Conducting Marketing Research and Forecasting Demand; Creating Customer Value, Satisfaction, and Loyalty, Analyzing Consumer Markets, Analyzing Business Markets, Identifying Market Segments and Targets. Dealing with Competition, Creating Brand Equity, Crafting the Brand Positioning; Setting Product Strategy, Designing and Managing Services, Developing Pricing Strategies and Programs. 14B11CL611 ENVIRONMENTAL ENGINEERING

Importance of environmental pollution control, Concept of Ecological Balance, Pollution control aspects, Environmental legislation & Regulations. Classification, sources and effect of water pollutant, Pre-treatment: Bar Racks, grit chambers, Comminutors, equalization (theory) Primary Treatment: Secondary Treatment, Tertiary treatment Air pollutants, sources & effect in man and environment, The Gaussian Plume model, Air pollution sampling and measurement, Review of equipment, system, and processes Correction Methods for air pollution control. Solid waste including plastic waste, nuclear waste; Hazardous Waste, Noise- Pollution 14B11CL612 CHEMICAL REACTOR DESIGN

Review of different type of reactors Non Ideal Flow Reactors. Concept of Residence Time Distribution (RTD); Segregation mixing in reactors; Models of non-ideal flow-Dispersion model; Effect of dispersion; Tanks in series model; Multi parameter models; Diagnostic methods of analysis of flow patterns in reactors; Applications to design of continuous solid flow reactors. Various design considerations of fluid bed reactors and their design consideration. Heat transfer effects; Phenomena observed in operation of packed, fluid bed, slurry and such reactors. Product distribution in multiple and complex reactions; Phenomenon of stability, un stability. Strategies for stable operations of reactors; Design considerations of fluid/solid catalytic reactors; Fluid bed reactors; Heterogeneous reactors; Bubble heterogeneous reactors, Co-current & Counter-Current flow packed bed reactor. 14B11CL613 PROCESS MODELING AND SIMULATION

Introduction to process modelling and simulation, Fundamental Laws, Application of principles of conservation and types of boundary conditions for various reactors; State space models, Cayley-Hamilton theorem, Sylvester’s formula, Gram Schmidt Orthogonalization procedure. Numerical solution by power method and polynomial method; Staged-process models: modelling of multiple, Numerical solution techniques for solving single and systems of non-linear algebraic equations. Dynamic and steady state model of a staged gas absorber, distillation column, and extraction column, Multiple Effect Evaporator. Population balance models, Deterministic Approach, Expected Value, Moments of Probability density function.

10B11CL614 PROCESS ENGINEERING & SAFETY

Preliminary Process Selection, Economic evaluation. Environmental footprint; Safety analysis and controlibity; Flexibility; Selection of Process steps; Identification of individual process steps Development of alternative routes; Selection criterion for modules; Determination of flow sheet based on heuristics. Development of P & ID; Estimation of capital and cost of product; Factors affecting the estimations-taxes, inflation, Concepts of break even, optimality of design, optimality of operation, cost benefit analysis, marginal rate of return; Profitability, alternative investments and replacement options; Types of Accidents; Causes and direct & indirect effects of accidents, Role of safety considerations in chemical plant Design & operations. Managerial aspects of safety; typical toxins and their biological effects; Source Models, Dispersion Models, HAZOOP, HAZAN and such methods, safety Review & other methods, Learning from accidents Methods of investigating and diagnosing. Aids for recommending case studies of well known accidents 14B11CL641 PETROLEUM REFINING Origin formation and composition of petroleum, refinery products and feed stocks, fractionation of petroleum, dehydration & desalting of crudes, treatment techniques and product specification, catalytic cracking and thermal process, asphalt technology, feed stock for petrochemicals.

14B11CL642 FERTILIZER TECHNOLOGY Need for use of fertilizers and micronutrients. Nutrient requirements of plants; Nature of chemical fertilizers, NITROGEN FERTILIZERS: Ammonia, Urea, ammonium nitrate, ammonium sulphate and other nitrogen based fertilizers. Production process with special reference to engineering aspects, Ordinary (Single) Super-phosphate, triple super-phosphate, di-ammonium phosphate and other phosphorus based fertilizers; Production process with special reference to engineering aspects, POTASH FERTILIZERS: Potassium chloride, potassium sulphate and potassium nitrate and other potassium based fertilizers. Production process 14B11CL643 FLUIDIZATION ENGINEERING Fluidization phenomena, behaviour of fluidized beds, industrial applications, Packed Beds: Flow of fluids, Darcy’s law and permeability, specific surface and voidage, general expressions for flow through packed beds; Carman-Kozeny equation, Fluidized Beds: Properties of gas fluid and liquid-solid systems, onset of fluidization, minimum fluidizing velocity, terminal velocity, slugging, channelling, bed expansion, distributors, voidage, entrainment and elutriation, Bubbles In Dense Phase Pneumatic and Hydraulic conveying: Pneumatic and hydraulic conveying of solids in horizontal and vertical pipelines, choking and saltation velocity, hydraulic conveying of solids.

14B17CL671 ENVIRONMENTAL ENGINEERING LAB

LIST OF EXPERIMENTS

1. BOD Incubator 2. COD Apparatus 3. DO Meter 4. Jar Test Apparatus 5. Nephelo(Turbidity) Meter 6. Ion exchange Column 7. pH & Conductivity Meter 8. To determine Acidity & Alkalinity of Water Sample 9. Chlorine demand and Residual Chlorine 10. Determine Chlorides in Water Sample 11. To Determine Dissolved, Suspended & Total Solids in Water Sample

12. To Determine Total Settle able Solids by Imhoff Cone

STUDY TYPE EXPERIMENTS

1. High Volume Sampler 2. Aerobic Digester Unit 3. Anaerobic Digester Unit 4. Deep Bed Filtration Set Up 5. Aeration Apparatus

14B17CL672 PROCESS SIMULATION LAB LIST OF EXPERIMENTS/TUTORIALS

1. Solving Equations of State, Vapor–Liquid Equilibrium, and Chemical Reaction Equilibrium using Excel and MATLAB.

2. Molar volume and compressibility factor from Redlich-Kwong equation. Dew point and two-phase flash in a non-ideal system

3. Mass Balances with Recycle Streams using Excel, Steady state material balances on a separation train.

4. Plug Flow Reactor, Batch Reactor and Continuous Stirred Tank Reactor. Isothermal Plug Flow Reactor, Non-isothermal Plug Flow Reactor.

5. Continuous Stirred Tank Reactors: Solution Using Excel, Solution Using MATLAB. CSTR with Multiple Solutions - Solutions to Multiple Equations Using MATLAB.

6. Three CSTRs in Series and Non-isothermal CSTR, Operation of a cooled exothermic CSTR.

7. Reversible, exothermic, gas phase reaction in a catalytic reactor. Catalyst decay in a packed bed reactor modeled by a series of CSTRs. Semi batch reactor with reversible liquid phase reaction.

8. Diffusion with chemical reaction in a one-dimensional slab.

9. Binary Distillation. Binary Batch Distillation.

10. Multi component Distillation with Shortcut Methods, Multi component Distillation with Rigorous Plate-to-Plate Methods.

11. Absorber: Packed and plate column.

12. Extraction: Packed column, plate column and stirred vessel.

13. Shell & Tube Heat Exchanger, Single and Multiple Effect Evaporators. Heat exchange in a series of tanks

14. Pipe and pump network, Gravity-Flow Tank.

15. Dynamics of a heated tank with PI temperature control.

16. Simulation of a Chemical Plant (Combination of Units)

14B17CL673 EXPERIMENTAL PROJECT

Student as individual or in groups (max. of 3 students) will be given projects in the area of subjects taught during that semester. The students will do a project based on literature review, small experiments where possible and prepare a report. There will be one midterm evaluation, a presentation at the end followed by a viva voce examination.

Year/Sem: IV Year/VII Sem

14B14HS741 Entrepreneurial Development

Concept of Entrepreneurship, Entrepreneurial Development Agencies, Business Planning, Entrepreneurial Development Programmes, Economic Development and Entrepreneurial growth, Importance of small scale industries. 14B14HS741 Managing and Marketing Technology

Understanding Marketing Management, Developing marketing strategies and capturing marketing insights, Strategic Planning and the marketing Process, Assessing opportunities in a dynamic marketing environment, The Marketing Environment, Managing and Marketing Information, Consumer and Business Buyer Behaviour, Developing marketing strategies and capturing marketing insights, Product and service strategy, Pricing products: Pricing considerations and strategies, Marketing Channels and Integrated-Marketing Communications, Managing marketing and growth. 14B14HS743 Entrepreneurship and Small Business

Entrepreneurship-Enterprise: Conceptual issues, Entrepreneurship vs. Management, Roles and functions of entrepreneur in relation to the enterprise and in relation to the economy. Entrepreneurship is an interactive process between the individual and the environment. The process of setting up a small business: Preliminary screening and aspects of the detailed study of the feasibility of the business idea and financing/non-financing support agencies to familiarize themselves with the policies/programs and procedures and the available schemes. Management roles and functions in a small business. Designing and re-designing business process, location, layout, operations planning and control. The pros and cons of alternative growth options: internal expansion, acquisitions and mergers, integration and diversification, Crisis in business growth. Brief introduction to Single-Entry system of record keeping; Sources of risk/venture capital, fixed capital, working capital and a basic awareness of financial services such as leasing and factoring; The contemporary perspectives on Infrastructure Development, Product and Procurement Reservation, Marketing Assistance, Subsidies and other Fiscal and Monetary Incentives. National state level and grass-root level financial and non-financial institutions in support of small business development. 14B14HS744 Brand Management

Customer-Based Brand Equity, Brand Positioning. Choosing Brand Elements to Build Brand Equity, Designing Marketing Programs to Build Brand Equity, Integrating Marketing Communications to Build Brand Equity, Leveraging Secondary Brand Associations to Build Brand Equity; Developing a Brand Equity Measurement and Management System, Measuring Sources of Brand Equity: Capturing Customer Mindset, Measuring Outcomes of Brand Equity: Capturing Market Performance. Designing and Implementing Branding Strategies, Introducing and Naming New Products and Brand Extensions, Managing Brands over Time, Managing Brands over Geographic, Boundaries and Market Segments. 14B14HS745 Human Resource Management

Human Resource Management: Meaning, Nature and Scope, HRM functions and objectives, evolution of HRM environment. Human resource development in India: evolution and principles of HRD Vs personnel functions, Role of HR managers. Strategic Human Resource Management: Nature of strategies and strategic management, strategic management process. Environment scanning, strategy formulation, implementation and evaluation; Human Resource Planning: Definition, purposes, processes and limiting factors. Human resources information system (HRIS): HR Accounting and audit, Job analysis- job description, job specification. Training and Development: purpose, methods and issues of training and management development programmes. Performance Appraisal: definition, purpose of appraisal, procedures and techniques including 360 degree performance appraisal. Job evaluation and Compensation administration: nature and objectives of compensation, components of

pay structure in India, Wage policy in India. Discipline and Grievance Procedures: definition, disciplinary procedure, grievance handling procedures. Industrial relations: nature, importance and approaches to industrial relations. 14B14HS746 Total Quality Management

Basics of Total Quality, Total Quality Management, TQM -Thinkers and Thoughts, Quality Awards; Cost of Quality, Team work for Quality, Total Employee Involvement Customer Satisfaction. Quality Circles, Kaizen, Six Sigma, People CMM, Benchmarking. Control of Accuracy and Precision, Process Capability, Statistical Process Control, Quality Function Deployment, Quality Management Systems, Design of Experiments (Taguchi Technique), FMEA, Total Productivity Maintenance. ISO: 9000 series, ISO: 14000 series. 14B11CL711 PROJECT ENGINEERING

Definition of project; Project Management; Constituents, Capital-Fixed, working; Estimation of capital and cost of product; Feasibility reports of various types; Project Licensing; Basic & Detailed Engineering; Various Laws & Regulations. Intellectual property rights; Patents need for clearances & its influence on project management; various forms like pure project, matrix and mixed type; Project team, WBS & responsibility charts, Contracts of various types. CPM.PERT.GANTT charts, LOB, resource allocation, material management, ABC analysis, and VED analysis; Project termination Commissioning, Start-up. Stabilization, Close out 14B11CL741 CEMENT TECHNOLOGY

Various processes of cement manufacture – dry, semi-dry and wet, overview of various unit operations, Indian cement industry, the global scenario, Phase composition of clinker minerals and cement, pozzolanic reaction, hydration of cement, Raw mix proportioning, 2-, 3- and 4-component mixes, concepts of burn ability, absorption and effect of coal ash Different zones in a cement kiln, preheaters and precalcinators, coolers, burners, fuels, waste-derived fuels, Pet coke, refractory and refractory practices, Approaches to energy conservation, energy audits, co-generation of power, Pollution control, noise abatement, concepts of LCA. EIA and EMP 14B11CL742 ENERGY SOURCES AND ENERGY CONSERVATION Introduction: Classification of energy sources and resources, present and future energy demands. Solid fuels, liquid fuels, gaseous fuels, combustion fuels, alternative energy sources, waste heat recovery, energy conservation in process industry. 14B11CL743 MULTIPHASE REACTOR DESIGN Introduction to multiphase reactions and multiphase reactors and design considerations, Catalyst deactivation and regeneration, industrial reactors: Trickle bed, bubble column, segmented bed, agitated slurry, fluidized bed and slurry reactors. Residence time distributions (RTD and macro mixing models; Review of methods for obtaining RTD, Problems in Scale-up; Models for gas liquid solid reactors, Brief description of laboratory reactors and significance of laboratory data for reactor design and scale-up. Intrinsic kinetics: Catalysis, Langmuir-Hinshelwood model, Determination of limiting steps from reaction data. Introduction to Chemical Vapour Deposition reactors 14B11CL744 POLYMER ENGINEERING Defining polymers; Basic chemistry of polymers; Classification and types, Examples of industrial and high-performance polymers, step growth (condensation) polymerization, free radical addition (chain growth) polymerization, ionic and coordination chain (addition) polymerization, copolymerization, polymerization system such as Bulk polymerization (quiescent and stirred )~ Solution polymerization; Suspension polymerization ~ Emulsion polymerization, Comparison of the various processes~

Advantages and disadvantages; Heat transfer and mixing in polymerization reactors. Characterization of molecular weight, polymer rheology and morphology, polymer processing like Blow moulding~ Injection moulding~ Compression moulding; Extrusion; Calendaring 14B11CL745ADSORPTIVE PROCESS DESIGN ADSORPTION PROCESS: Modern adsorbent such as activated carbons, molecular sieves of various types, activated alumina and their characteristics and applications. Regeneration and activation of adsorbents; Fixed bed, moving bed, simulated moving bed and other processing schemes; Design of adsorption processes for separation & purification. Industrial examples, Foam formation, coalescence, Principal of froth floatation, Properties of foam relevant to floatation operation; Design & Development of floatation equipment; Application of froth floatation to mineral processing, protein & enzyme separation, waste water treatment, Column design & filling 14B11CL746 PLANT UTILITY AND ENERGY SYSTEMS Identification of common plant utilities; Importance of utilities in India, Raw water storage and treatment, Properties of steam; Steam generation by boilers; Type of boilers and their operations, Compressed air from blowers and compressors; Air drying systems, Refrigeration systems such as compression and absorption refrigeration, Selection of vacuum system and maintenance, flaring and venting, energy audit, engineering integration in process industry, design of heat exchange networks, heat integration in process units, co generation of energy: introduction, renewable sources of energy, introduction to tidal geothermal source of energy. 14B11CL747 MEMBRANE PROCESS DESIGN Introduction to membrane processes, history, definition of membrane, importance of processes, MEMBRANES AND THEIR APPLICATIONS, Liquid membranes supported and unsupported liquid membranes, application and mathematical modelling, Materials and material properties polymers and effect of various properties of polymers such as Tg, thermal, chemical and mechanical stability, elastomers and their properties, inorganic membranes, biological membranes, CHARACTERIZATION OF MEMBRANES, PREPARATION OF SYNTHETIC MEMBRANES, spiral wound, tubular, capillary, hollow fibre modules and their comparison, system design, application of membrane reactors in biotechnology, comparison of membrane technology, scope in the future, current and existing industrial application. 14B11CL748 MIXING TECHNOLOGY Introduction to mixing, classification: Types of impellers and their characteristics. Power consumption for different impellers and correlations, mechanism of mixing, liquid, solid and gas dispersions in liquid; Three phase dispersions, heat transfer and mass transfer in mixing, Design and scale-up of mixing equipment’s. 14B11CL749 PIPING ENGINEERING Role of piping, scope of piping engineering, responsibilities of piping engineer, introduction to engineering line diagram, process flow diagram and piping and instrumentation diagram for process plant and utilities including various symbols, material of construction and fabrication for pipes, Statutory rules and regulations, Codes and standards, Introduction to various standard pipe fittings pipe flanges and gaskets their selection and specifications, valves and other piping components, piping system design, piping layout and drawing, computer aided piping design, application of piping engineering.

14B11CL791 PROJECT I Student will make a complete survey of the relevant literature and collect information from different sources. The students will do the process selection from the available alternative processes, give detailed description of the selected process with process flow diagram and P&ID. The student shall append MSDS of the hazardous chemicals. A suitable plant capacity and plant location shall be discussed. It is expected that students will spend approximately 30 working hours on the design project. The assessment for this will be done in the 8th semester. Year/Sem: IVth Year/VIII Sem 14B14HS841 Knowledge Management Introduction, Types of Knowledge, Knowledge workers, Valuing knowledge, Communities of Practice, Content management, Creativity and Innovation, Knowledge management strategies, Business process and the process oriented organization, Information and communication technologies (ICT), Management of intellectual capital, Different level of Knowledge management, Organizational culture, Developing human capital, Building and managing the knowledge repository. 14B14HS842 Industrial Psychology Definitions & Scope of Industrial Psychology, Major influences on industrial Psychology- Scientific management and human relations schools Hawthorne Experiments. Motivation : Theories of Motivation: Early and Contemporary views, Three level Work Motivation Model, Motivating a Diverse Workforce, Stress management: Understanding Stress and Its Consequences, Causes of Stress, Managing Stress, Leadership: Style and Theories of Leadership-Trait, Behavioral and Situational Theories. Fatigue, Boredom, Accidents and safety, Job Analysis, Job Satisfaction, Recruitment and Selection – Different types of recruitment and selection tests, Reliability & Validity of recruitment Tests. Group Dynamics: Definition, Stages of Group Development, Group Cohesiveness, Formal and Informal Groups, Group Processes and Decision Making, Dysfunctional Groups, Organizational culture : Organizational Culture: Concept, Characteristics, Elements of Culture, Implications of Organization culture, Process of Organizational Culture. 14B14HS843 Supply Chain Management Introduction: Basic Concept & Philosophy of Supply Chain Management; Essential features, Various flows (cash, value and information), Key Issues in SCM, benefits and case examples. Logistics as part of SCM, Logistics costs, different models, logistics sub-system, inbound and outbound logistics, and bullwhip effect in logistics, Distribution and warehousing management, Purchasing & Vendor management: Centralized and decentralized purchasing, functions of purchase, department and purchase policies; Use of mathematical model for vendor rating/evaluation, single vendor concept, management of stores, accounting for materials. Concept, various costs associated with inventory, various EOQ models, buffer stock ( tradeoff between stock out/working capital cost), lead time reduction, re-order point/re-order level fixation, exercises –numerical problem solving , ABC, SDE/VED Analysis, Just-In-Time & Kanban System of Inventory management. Role of Computer/IT in Supply Chain Management, CRM Vs SCM, Benchmarking concept, Features and Implementation, Outsourcing-basic concept, Value Addition in SCM-concept of demand chain management. 14B14HS845 Strategic Management

Introduction, Strategic Management, Business Policy, Corporate Strategy, Basic Concept of Strategic Management, Mission, Vision, Objectives, Impact of globalization, Basic Model of Strategic Management, Strategic Decision Making, Impact of Internet and E-Commerce, Role of Strategic Management in Marketing, Finance, HR and Global Competitiveness. Environmental Scanning, Industry Analysis, Competitive Intelligence ETOP Study, OCP, SAP Scanning, Corporate Analysis,

Resource based approach, Value-Chain Approach, Scanning Functional Resources, Strategic Budget and Audit. SWOT Analysis, TOWS Matrix, Various Corporate Strategies: Growth/Expansion, Diversification, Stability, Retrenchment & Combination Strategy. Process of Strategic Planning, Stages of corporate development, Corporate Restructuring, Mergers & Acquisitions, Strategic Alliances, Portfolio Analysis, Corporate Parenting, Functional Strategy, BCG Model, GE 9 Cell, Porters Model: 5 Force and Porters Diamond Model, Strategic Choice. Strategy Implementation through structure, through Human Resource Management: through values and ethics. Mc Kinsey’s 7S Model, Organization Life Cycle, Management and Control, Activity based Costing, Strategic Information System. 14B11CL841 INDUSTRIAL CATALYSIS

catalytic reactions, homogeneous catalysis, heterogeneous catalysis, analysis of external and internal transport processes, design of heterogeneous catalytic reactors: Global rates and experimental reactors; Design calculations for ideal reactors operating at isothermal, adiabatic and non-adiabatic conditions; Deviations from ideal reactor performance; Design of industrial fixed bed, fluidized bed and slurry reactors; Examples from petro-refinery, pharmaceutical and fine chemical industry; DeNOx and DeSOx technologies. 14B11CL842 THERMAL ENERGY GENERATION SYSTEMS Introduction, Energy needs in Indian scenario, Thermal energy and power. Fuels and combustion, Combustion Mechanism and Equipment’s, Steam Generators, Analysis of steam cycles, Steam turbines, Condenser, Steam and condensate handling 14B11CL843 FOOD PROCESS ENGINEERING Introduction to food industry, opportunities for the Indian Processed Food Industry, Engineering challenges in the Food Processing Industry, Basic food biochemistry and microbiology: Food Constituents, Water activity Enzymes, D & Z values Food safety. Indian laws regulating Foods and Food Processing; Raw material preparation Size reduction of solid fibrous foods and in liquid foods, Theory and Equipment, heat processing using water, air and hot oil, heat processing by direct and radiated energy, processing by removal of heat, food preservation and storage, post processing applications. 14B11CL844 DOWNSTREAM PROCESSING IN BIOTECHNOLOGY Separation process in biochemical industry, special needs, Separation process for bulk chemicals and proteins, Unit operations in biochemical industry such as filtration, centrifugation, extraction, liquid ion exchangers and adsorption; Protein purification methods: Chromatographic methods. 14B11CL845 COGENERATION Introduction, Energy sources, Available energy referred to a cycle, Maximum work in a reversible process, Useful work, Availability in chemical reactions, Concepts of co-generation, Properties of pure substances: PVT surfaces, Mollier diagram, Steam tables, Thermodynamic properties, Measurement of steam quality, Vapour power cycle, Gas power cycle, Steam generation: Boilers, Construction, Working of different types of boilers, Steam turbines: Types, Classification, Co-generation: Characteristics of cogeneration plant, Cogeneration economics. 14B11CL846 ADVANCED PROCESS CONTROL

Advanced Control Systems: Introduction to multiple loop control systems, Cascade control, Feed Forward control; Inferential control; Adaptive and Ratio control, Multivariable Process Control: Introduction, Design of controllers for Multivariable processes: Selection of manipulated and controlled variables, Pairing controlled and manipulated variables, BLT Tuning, Load rejection

performance, Decoupling Control Systems, Introduction to Model Predictive Control, Sampled Data Control Systems: Introduction; Sampling, Z Transforms and stability; Stability analysis of sampled data systems; Process Identification, State Space Methods: State Space representation of Physical Systems, Transfer function Matrix. 14B11CL847 INDUSTRIAL BIOTECHNOLOGY Introduction to biochemical engineering, introduction to microbiology, cell growth, Michaelis Menten Kinetics, Methods for determining rate parameters, Lineweaver – Burk Plot; Edie Hofstee, Hanes plot, Reversible reactions, Multiple substrates, cofactor activation, Substrate activation & inhibition, Types of Enzyme inhibition reversible & irreversible, Competitive, Non-competitive, uncompetitive and mixed, Effect of pH, Temperature and other environmental factors, Types of deactivation and deactivation kinetics, kinetics of immobilized enzyme, bioreactor engineering, special product recovery operations, genetic engineering & recombinant DNA technology . 14B11CL848 FLUIDISED BED COMBUSTION Introduction: Fuels and combustion; Limitations, Advantages of fluidized combustion of solid fuels. Fluidisation Phenomena, Fluidised bed Combustion, Fundamental Processes in Fluidised bed Combustion Boilers, Fluidised bed combustion applications. 14B11CL849 INTRODUCTION TO COMPUTATIONAL FLUID DYNAMICS History, Comparison of the three basic approaches for engineering problems in solving by analytical, experimental and computational methods, Beam advance in computational techniques, Software’s available for CFD, problem formulation, methods of discretisation, numerical solution of heat conduction problems, numerical solution of fluid flow problems Calculation of boundary layer over a flat plate, Numerical algorithm for solving complete Navier-Stokes equation-MAC method SIMPLE algorithm, Introduction to standard - model for turbulent incompressible flow, Project problem. 14B11CL850 PROCESS SIMULATION AND DESIGN Mathematical models, their classification Model Building, Solution of system of non-linear algebraic equation (Newton’s and successive substitution); Application in chemical engg., such as equilibrium flash calculation, Solution of single ODE and system of ODEs (Implicit Euler & Runge-Kutta 4th order) Application in chemical engineering problems such as homogenous well mixed reactor Approaches to simulation: (1) Sequential modular. Precedence ordering of Modules (partitioning and Tearing of flow sheets) (2) Simultaneous: Process Simulation; Simulation of batch distillation and batch reactor. 14B14MA843 OPTIMIZATION METHODS FOR ENGINEERING OPTIMIZATION: Introduction and concept of optimization, Optimization problems in chemical engineering, Heat exchanger, reactor, fluid flow, separation chain, inventory Control, Analytical methods for unconstrained single variable optimization. NUMERICAL METHODS FOR UNCONSTRAINED SINGLE AND MULTI VARIABLE OPTIMIZATION: Various Numerical methods applicable to optimization of chemical processes; OPERATION RESEARCH; LINEAR PROGRAMMING: Graphical solution, Simplex method, Duality and duel simplex, Integer programming (Branch and bound only), brief review of Transportation problem, Assignment problem; INVENTORY CONTROL: EQQ single item static model, Static model with price breaks, Static model with shortage permitted; QUEUING THEORY: Cost model, Aspiration level model; GAME THEORY: Games of pure strategy, Games of mixed strategy: Solution of 22 Games by mixed strategy

14B14PH731 NANOSCIENCE AND TECHNOLOGY

Introduction and Classification of nano-structured materials: Nanoscience and Nanotechnology, Brief History and future scope, Gleiter's classification of nano-structured materials, Classification of nanostructures by dimensionality. Fullerene, Nanotubes, Graphene; Concept of matter waves, Schrodinger wave equation, confinement, particle in a potential box, barrier penetration and tunneling effects, concept of density of states. Size effects and properties of nano-structured materials: Concept of characteristic time and length scales of physical phenomena, Definition and types of size effects, extended internal surface, increasing surface energy and tension, Grain boundaries, classical and quantum size effects, size dependent thermal, mechanical, electrical, magnetic and optical properties of nano-structured materials e.g. Reduction of lattice parameter, decrease in melting point, decreasing thermal conductivity, diffusion enhancement, increasing plastic yield strength and hardness, blue shift, broadening of energy bands, phase transitions in ferromagnetic and ferroelectric materials; Techniques for synthesis of Nanostructures: Top-down and Bottom approaches, Vapor – phase synthesis, Liquid phase synthesis, Sol-gel technique, Solid – state phase synthesis, consolidation of nano-powders; Basic characterization and microscopy of Nanostructure materials: X-ray diffraction (XRD), UV- visible, FTIR, TGA, Scanning Electron microscopy (SEM), Transmission electron Microscopy (TEM), Scanning probe microscopy, Scanning tunneling Microscopy (STM) and Atomic Force microscopy (AFM) Nanotechnology Applications: Applications of Nanostructures for diversified fields of Engineering 14B14CI857 INTRODUCTION TO ARTIFICIAL INTELLIGENCE Problems, Problem spaces, Heuristic search techniques, Parallel and distributed AI, Common sense, Expert systems Knowledge representation: issues, using predicate logic, Representing knowledge using rules, symbolic reasoning under uncertainty, Statistical reasoning Learning: functions, decision trees, reinforcement learning, learning sets of rules: explanation based learning, inductive logic programming, game plying, Planning Understanding & Natural Language processing

14B14ME744 DESIGN OF HEAT EXCHANGERS

CLASSIFICATION OF HEAT EXCHANGERS: Recuperation and regeneration, Transfer processors, Geometry of construction–tubular heat exchangers, plate heat exchangers, extended surface heat exchanges, Heat transfer mechanisms, Flow arrangements, Selection of heat exchangers. BASIC DESIGN METHODS OF HEAT EXCHANGES: Arrangement of flow path in heat exchangers , Basic equations in design, Overall heat transfer coefficient , Log mean temperature difference method for heat exchanger analysis , The -NTU method for heat exchanger analysis, Heat exchanger design calculation, Variable overall heat transfer coefficient , Heat exchanger design methodology DESIGN CORRELATIONS FOR CONDENSERS AND EVAPORATORS: Condensation, Film condensation on a single horizontal tube-laminar film condensation, forced convection, Film condensation in tube bundles-effect of condensate inundation, effect of vapor shear, combined effects of inundation and vapor shear, Condensation inside tubes-condensation in vertical tubes. SHELL AND TUBE HEAT EXCHANGERS: Basic components-shell types, tube bundle types, baffle type and geometry, Basic design procedure of a heat exchanger-preliminary estimation of unit size, rating of preliminary design, Bell-Delaware method. COMPACT HEAT EXCHANGERS: Plate-fin heat exchangers, tube-fin heat exchangers, Heat transfer and pressure drop-heat transfer, pressure drop for finned-tube exchangers, Pressure drop for plate-fin exchangers, gasketed plate type heat exchangers.

14B14MA845 MATHEMATICAL METHODS IN ENGINEERING

SYSTEMS OF LINEAR ALGEBRAIC EQUATIONS: Introduction to Linear System; Fundamental Definitions and Operations of Matrix Analysis; Solutions of Linear Algebraic Systems; Applications to

Chemical Engineering; NONLINEAR ALGEBRAIC EQUATIONS: Solution of a single equation in one unknown; Systems of Nonlinear Algebraic Equations; ORDINARY DIFFERENTIAL EQUATIONS: Review of ODE of various types. Application in velocity profile for laminar flow in circular tubes and annulus (*), Heat conduction with chemical heat source.(*), Diffusion with homogeneous chemical reaction (*), Reactions of various orders in batch reactors; Numerical Methods covering Euler, Runge-Kutta and predictor-corrector method; Shooting method for BVP; Systems of differential equations (**)PARTIAL DIFFERENTIAL EQUATIONS: Introduction to formulation and classification of PDEs, solving PDE by finite difference techniques; Applications in Heat and Mass transfer and chemical reaction NUMERICAL METHODS FOR UNCONSTRAINED SINGLE AND MULTI VARIABLE OPTIMIZATION: Newton’s, Quasi-Newton, Secant, Region elimination method: Golden section, Fibonacci, Dichotomous search. Direct method: Univariate Search, Conjugate directions Search. Indirect method: Gradient, Conjugate gradient, and Newton. TRANSFORM METHODS: Fourier transform and its application to chemical engineering.

14B11CL891 PROJECT II Student will make a complete survey of the relevant literature and collect information from different sources. The students will do the process selection, mass and energy balances, process design of all equipments and mechanical design of at least one of equipment per student and give information on instrumentation and control, plant layout, safety & environmental aspects and economic evaluation.