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Surface hardening of stainless steel in the Food Processing Industry

Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

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Page 1: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

Surface hardening of stainless steel in the Food Processing Industry

Page 2: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Agenda

Why use Stainless Steel in Food Processing Industry

Key factors

Challenges

Options

Expanite processes. This is how we do it

Expanite Introduction

Expanite Treatment in the Food Industry

Next generation surface treatment technology

Page 3: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

Why use Stainless Steel in

Food Processing Industry

Page 4: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Corrosion resistant

Migration – Approved to have Food contact

Hygienic - Clean ability

Mechanical properties

Key Factors

Page 5: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Stainless steel has good corrosion properties

- but it suffers from poor wear resistancegiving several challenges

Page 6: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Wear

Corrosion

And the increased focus on:

Lifetime cycle

Maintenance and Service

Cleaning

Production efficiency

Food safety.

What are the Challenges

Page 7: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

What are the options

Do nothing – and live with wearCoatings – and live with risk of spalling:

Hard Crome PlatingPVD/DLC

Diffusion:PlasmaSalt-bathGas

We believe the future is gas!

Expanite treatment improve the surface hardening while maintaining and/or even improving the corrosion resistance

Page 8: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

What happens with wear and corrosion after

Expanite

Page 9: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

The pain…and the solution!

0

1

2

3

4

5

6

0 20 40 60 80 100 120 140

WeightLoss[mg]

Time[min]

Materialloss-accelerated

Untreated

ExpaniteHighT

SuperExpanite

Page 10: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Improved wear resistance

Alloy: duplex 2205

Knifes used to cut enzyme powder

Accelerated wear without Expanite hardening

Unused knife

Used knife withoutExpanite

Used knife with Expanite

Page 11: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

ASTM G133 wear test performed on AISI 316 stainless steel with and without “SuperExpanite” surface hardening treatment

Lubrication: noneCeramic silicon nitride ballForce: 25NTotal sliding distance: 100m

9h June 2015 AT n° CET0111600_PV_01_a Page 13/23

Final

Friction force The friction force is measured by a piezoelectric sensor attached between the machine frame and the support of the fixed specimen.

Figure 7 : Tribometer PLINT TE-77.

Figure 8 : General overview of tribometer PLINT TE77.

Page 12: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Findings – worn surface trace profiles

Main conclusion: 125 times less wear on SuperExpanitetreated plane surface

Page 13: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

ASTM G98 galling resistance test on AISI 316 stainless Non-treated 316 vs. 316 reference SuperExpanite vs. SuperExpanite

Non-treated Expanite-treated

0.5 ksi + no

1 ksi + no

2 ksi + no

5 ksi + no

… … …

40 ksi + no

Page 14: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

“I haven’t seen such a solution to galling on 316 in my 15+ years of tribology testing”

–Steven Budinski Owner/ Bud Labs

Dont just take our words for it

Page 15: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

-500

-300

-100

100

300

500

700

900

1100

1300

1500

1E-08 0.00000010.000001 0.00001 0.0001 0.001 0.01 0.1 1 10 100

AISI316

Annealed

*AISI 316 –Pitting resistance in seawater

SuperExpaniteExpaniteHigh-T

ReferencePitting potential increase: 400mV

Improved corrosion resistance Voltage

Current

Page 16: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Improved corrosion resistance

-400

-200

0

200

400

600

800

1000

1200

1E-08 0.00000010.0000010.00001 0.0001 0.001 0.01 0.1 1 10 100

AISI316Annealed

AISI304Annealed

AISI304ExpaniteHighTV1

316 reference

304 reference

304 ExpaniteHigh-T

*AISI 316/304 –Pitting resistance in seawater

Voltage

Current

Page 17: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

EXPANITEEnhancing the properties in

the stainless steel

This is how we do it

Page 18: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

What is Expanite?

A technology =

process/recipe =

time + temperature + pressure + gas flow + surface physics & chemistry in a furnace=

a gas-based diffusion process

N+Cnotabletopenetrateoxidelayer

Expanitegasprocessremovesoxidelayer

N+Cisnowabletoentermaterial

Page 19: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

What’s unique?

150

250

350

450

550

650

750

850

950

1050

1150

0 50 100

Hardness[HV0.01]

Distancefromsurface[µm]

Micrographs & hardness profile of part in AISI316

ISO9227 168hr salt spray

Improving hardness and in the same time improving/restoring corrosion resistance beyond what the market previously has seen

Page 20: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

What’s unique?

Accurate control• Tailoring• Scalable• Clean• Fast & Cost effective

Bulk-ware treatment• Homogenous hardening• No post cleaning• Bulk treatment

. . .

Identical temperature and time – only increasing gas potential

Page 21: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

The processesTemperature in vacuum: 1000-1200CFast gas quenchAdds nitrogenDK: 400x400x600 DE: 400x400x1000

Page 22: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

The processesTemperature in atmospheric environment: 380-470CAdds nitrogen and carbon in solid solutionDK: 600x600x1000DE: 800x800x1100

Page 23: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

The processes

Page 24: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Martensitic stainless steel

ExpaniteHigh-T Hardness and corrosion resistance increase!

Duplex stainless steel

Austenite + ferrite

Expanded austenite

Carbon martensite

Nitrogen martensite

Page 25: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Martensitic stainless steel

350

400

450

500

550

600

650

700

750

0 0.4 0.8 1.2 1.6 2

Hardness[HV0.3]

Distancefromsurface[mm]

Treatment: ExpaniteHigh-TCase Depth High-T: 0.55 mmSurface hardness: 950 HV0.3

12.5Cr-0.12C-(1.5Mn+1.0Si max)

Page 26: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

Expanite Introduction

Page 27: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Established 2010 based on ongoing research since 2000HQ in Hillerød 8 furnaces doing running production R&D and production facility incl. laboratory and five experimental furnacesISO9001 certifiedLocated: DK, US and Germany

Expanite – the company

Page 28: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

Goes beyond the surface to reduce leadtime and costs

BEYOND THE SURFACE

Page 29: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

Expanite Treatment in the Food Industry

Page 30: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Typical segments in food processing industry

Beverage equipment especially capping and filling equipment Bakery machines Chocolate processing & packagingIce-cream processing & packagingDairy processingMeat processing incl. slicing machinesPumps for food incl. positive displacement pumps and screw pumps

Page 31: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Typical products in Food Processing Industry

Page 32: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Page 33: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Page 34: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Page 35: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Page 36: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Page 37: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

Next generation

Page 38: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

The future is gas

Why.?

Short process timeCleanerBulk wearCost effectiveHigher QualityImproving hardness and in the same time

improving/restoring corrosion resistance

Page 39: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

BEYOND THE SURFACE

Expanite Hardening of Titanium - Why.?

Our technology works on it

It’s a alloy in growth and use

It’s a soft material

Page 40: Surface hardening of stainless steel in the Food ... · Coatings –and live with risk of spalling: Hard Crome Plating PVD/DLC Diffusion: Plasma Salt-bath Gas We believe the future

Thank you

www.expanite.com