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General Chemistry II Laboratory Summer 2015

Summer 2015. Name:Mark Martinson Phone:786-1368 E-mail:[email protected]@uaa.alaska.edu Office:CPSB 302 N Office Hours:

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  • Summer 2015
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  • Name:Mark Martinson Phone:786-1368 E-mail:[email protected]@uaa.alaska.edu Office:CPSB 302 N Office Hours: Mondays: Tuesdays: Wednesdays: Thursdays: Fridays: (Page 1)
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  • CHEM A105 with a minimum grade of C and CHEM A105L with a minimum grade of C and CHEM A106 with a minimum grade of C or concurrent enrollment Strong background in algebra. (Page 13)
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  • A continuation of the basics of: Laboratory equipment and procedures Data collection Data analysis Reporting (Page 13)
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  • General Chemistry II Laboratory Manual, Summer 2015 edition Lab coat, 40 Safety goggles 1.5 three-ring binder (no fabric covers) Scientific or graphing calculator Any General Chemistry textbook such as the one required by your lecture instructor WolfCard (Page 14)
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  • Computer lab locations and hours Computer use and etiquette E-mail use and etiquette Blackboard Online safety (Pages 14-17)
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  • Attendance is mandatory. Dress appropriately. Submit pre-labs before lab. Be on time for lab. Arrive prepared for the procedure. Behave appropriately. Attend all skill evaluation sessions or receive an F for the course. (Pages 19-20)
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  • Excused LabsUnexcused Labs Verifiable, pre-approved reasonNon-approved reason Submit a Missed Lab Form before or after the absence (see pages 9 12) Additional documentation requiredNo additional documentation required Lab make-up during the same weekNo make-up permitted Averaged / Exempted or earned grade assigned Grade of zero assigned If extenuating circumstances exist, miss no more than 2 labs or receive an F for the course.
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  • Skill Evaluations Must attend and pass two complete sets. Pass / Fail Academic Pre-lab questions (30%) Lab and report completion (20%) Quizzes (20%) Fully graded reports (20%) Formal lab report (10%) Plagiarism Zero-tolerance policy (Pages 25 28)
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  • Lab 1 Homework: Start in lab Lab 1 Homework deadline No labs on May 25 th (Memorial Day) Lab 2 Pre-lab: Monday lab deadline: Tuesday lab deadline:
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  • Check the schedule to see which lab should be prepped for. (Page 4) Read the required reading section from the textbook. (Example, page 89) Read through the entire lab write-up. (Example, pages 89 - 106) Work through sample calculations and examples until they are understood. (Example, pages 93 - 97 ) Write a synopsis of the lab procedure or draw pictures. (Example, pages 98 - 102) Complete calculations and fill in units where possible. (Example, page 105 ) Complete and submit pre-lab questions. (Example, pages 103 104) Ask questions BEFORE lab. Ideally during office hours. (Page 28)
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  • The chemistry department SAPs are in place to minimize health and safety risks. Any person in violation of these protocols shall face administrative action as outlined in the letter from the Dean of CAS. (Page 5)
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  • Anybody who wishes to perform any course work in a chemistry lab shall first receive the proper safety training (CHP and SAPs overviewed). Pets are not allowed in the CPSB. Chemicals, equipment, cultures, specimens and other university property may not be removed from the premises without the expressed written consent of the laboratory manager. http://www.layoutcodez.net/facebook/pets/
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  • Never enter any teaching laboratory without the presence and / or permission of your lab instructor. The number of students permitted to each lab shall never exceed the number of stations available in the laboratory. Children, friends, and visitors are not allowed in laboratories without the expressed written permission of the laboratory coordinator and notification of the laboratory manager and Department Chair. Horseplay and unauthorized experiments are strictly forbidden. http://cheezburger.com/TemplateView.aspx?ciid=4902675
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  • Keep the lab clean and orderly. Wipe spills immediately. If the spill involves hazardous materials notify your instructor immediately. Inform classmates of the spill and make sure that they avoid the area. If an experiment has special safety considerations not covered in these SAPs, the instructor of the class and the lab manual shall instruct students explicitly on how to safely perform the experiment and appropriately discard waste.
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  • Deposit waste in the appropriate receptacles. If glassware is broken, the instructor should be notified immediately so that they can use a brush and dustpan to discard the broken glass in the broken glass disposal box. Students should be prevented for accessing the area containing the broken glass until after a thorough cleanup has been performed. Hazardous chemicals should be disposed of in special, labeled waste containers in the fume hood(s). Non-toxic, non-hazardous aqueous solutions with a pH between 6 and 8 should be disposed of down the drain only if permitted under all current applicable EPA, CDC, NIH, DEC, and MOA regulations and policies. Solutions with a pH below 6 and above 8 should go in a waste container. Regular trash should be disposed of in a non-hazardous waste bin only. Where available, recyclable paper only should be discarded in recycling bins.
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  • Injuries or incidents should be reported to the lab instructor immediately and to EHS/RMS within 8 hours using their online reporting system. Students who sustain minor injuries in lab may be required to visit the student health center before continuing with lab. Consultations at the Student Health Center are free for students taking 6 or more credits. 911 will be dialed for all severe injuries. http://www.eyesafety.4ursafety.com/eye-safety-articles.html
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  • Know where all safety equipment is located and how they function. These are to remain clear of obstructions at all times. Your instructor will point each of these out to you. Gloves Safety shower Eyewash basin Fire extinguisher Fire blanket Fume hoods First aid kit Glass disposal boxes (M)SDS binder Phone
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  • All exits are clearly marked and should be unobstructed at all times. Your instructor will go over the emergency escape route for this lab. In the advent of a visible fire or the sound of a building fire alarm, everybody should remain calm. Follow your instructors directions for evacuating the building. http://www.itsoftmedia.com/category/economy/page/2 http://www.securityworldnews.com/2011/02/17/the- importance-of-having-a-proper-exit-plan-in-your- workplace/
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  • In the event of an earthquake, everybody should remain calm, get under a bench or stand against an inside wall. Do not stand in a doorway or against windows. Follow the instructors verbal directions regarding any building evacuation once the shaking stops. http://www.in.gov/dhs/3729.htm
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  • During a building evacuation if time and safety permits: Shut off all electrical devices Stop any chemical procedures Collect personal belongings Calmly proceed to exit the building via the nearest and safest exit Do not use the elevators Once outside, stay at least 50 to 100 feet from any buildings Do not leave your class evacuation assembly point until your instructor has personally accounted for every one in your class. http://www.cfdsolution.com/firesafetymanagement.htm
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  • Consult with your healthcare provider if you have any special medical conditions or any other medical concerns while participating in lab exercises. Voluntarily inform your instructor of any relevant medical conditions that could pose a safety hazard to yourself or others. http://www.herc.org/news/ehp/miller.html
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  • Smoking, eating and drinking are strictly forbidden in laboratories. Any visible food / drink container shall be discarded in a garbage bin. Gum and mints are considered food items. Food and beverage containers may not be left outside laboratory doors on the floor as they pose a trip and slip hazard. Use one of the shelves instead.
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  • Appropriate attire is required in all laboratories at all times. Your instructor will elaborate. Long hair must be tied back. Keep it out of your eyes and out of your chemicals! OSHA recommends strongly against wearing contact lenses in lab. Notify your instructor at the beginning of each lab if you are wearing contact lenses. Research chemical incompatibility! Remove dangling jewelry and all ornaments (including watches and rings) worn below the elbow from your person before entering the lab. The application of any and all make-up, including lip balm and ChapStick, is strictly prohibited in laboratories. http://uncrate.com/stuff/gap-original-shorts/ http://blog.asiantown.net/-/2707/mr-t--treat-your-mother-right.aspx http://cooksafe.dumgal.gov.uk/GetReadyForCookSafe/getready_34.h tm
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  • Specific procedures must be fully read and understood prior to coming to lab. Know the properties of your chemicals. All hazardous characteristics of chemicals should be known prior to lab. These may be found in the Material Safety Data Sheet (MSDS) or Safety Data Sheet (SDS) for each chemical and / or the lab manual.
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  • The appropriate personal protective equipment (PPE) shall be worn by all persons in the laboratory. This includes indirectly vented, splash proof goggles, lab coats and non-permeable gloves. Your instructor will discuss proper lab coat handling with you. The fume hood should be used anytime hazardous chemicals are present. Wear goggles whenever glassware and / or chemicals are in use by anyone in the lab.
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  • Plan the use of appropriate glassware. Always use the smallest container feasible. Always use the smallest amount of a given chemical. Never pour directly from a very large container into a very small container. Always add acid to water, not the reverse. http://www.dermaamin.com/site/atlas-of- dermatology/3-c/256-chemical-cauterization-.html http://caretheskin.com/what-is-chemical- burn
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  • Never intentionally inhale or ingest any chemicals. If you get any chemicals on your skin, rinse the exposed areas with copious amounts of water unless otherwise indicated by your instructor / MSDS / SDS. A major spill on your person will require use of a safety shower. You should get into the shower as soon as possible, and as soon as possible begin to remove all clothing. Do not let modesty prevent you from taking the appropriate safety measures. If you get a chemical in your eye, you should flush it out for a minimum of 15 minutes at the eyewash basin. If you are wearing contacts, you should remove them as soon as possible after an initial rinsing. Follow your instructors directions. http://www.medicine.uotta wa.ca/ehss- spe/eng/accidents.html http://www.quitsmok ingsupport.com/lung photos.htm
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  • All powered equipment in the chemistry laboratory pose a risk of electrical shock. Hotplates pose a burn hazard. Individuals who pose a danger to themselves or others by being under the influence of any drug, inhibiting medication or who become violent or threatening will be removed from any laboratory by UAA University Police. http://www.wktv.com/news/crime- reports/otsego/911-conspiracy-film- producer-in-NY-drug-arrest- 114931424.html
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  • The use of cell phones, i-pods, blue tooth devices etc. while in attendance of any laboratory class is prohibited, except when placing or receiving an emergency call. All cell phones should be turned off or placed in the silent or vibration mode and be kept in a pocket, purse or backpack. Before handling a cell phone, gloves must be removed and hands washed to prevent chemical contamination. Notify the instructor before leaving the lab to take or continue an emergency call. When making an emergency call the call takers will need to know: a. Your name and location (building, room number, building address) b. The nature of your emergency c. Type and severity of injuries d. The suspect description and direction of travel (if applicable)
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  • Upon entering the chemistry laboratory: Sign the attendance sheet as soon as possible after entering the lab. Bench tops and isles should be kept free of clutter by placing personal items, coats, and non-relevant books in a cubby. Submit any work that is due. Wipe down lab benches with water and paper towels. Wash hands with soap and water. Wait until after the pre-lab presentation before starting the experiment (including removing glassware from drawers). http://foodcourtlunch.com/?p=2757
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  • Faulty or inoperative equipment should be reported to the instructor immediately. Never contaminate equipment or solutions unnecessarily. Keep all cabinets and drawers closed when not in use to avoid catching and bumping hazards. http://www.notesintoimages.com/2011/12/five-things-you-need-to-do-to-become.html
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  • Before leaving the chemistry laboratory: Clean (using soap, a brush, tap water, and then distilled water), dry (using a paper towel), and put away all glassware in the appropriate drawer (use the provided inventory sheet to verify) Clean all common-use equipment and areas (balances, etc.) Log off / Shut down the computer (where applicable) Turn off all hotplates, thermometers, and MicroLab boxes (when applicable) Push in all chairs / stools (where available) Ask your instructor to perform a station check-out and assign completion grades. Sign out from the lab. Remove all personal belongings from the bench top and cubbies. Remove coffee cups, water bottles, and food from the shelf outside the lab.
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  • If you are uncertain of any safety measures, ask your instructor for clarification. http://www.paduiblog.com/pa-dui/harrisburg-dui-lawyer-comments-on-inaccurate-blood-alcohol-content-and-bad-bac-results/
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  • http://pnergy.wikispaces.com/SM+-+Introduction+to+Lab+Safety
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  • Please print, sign and date the Laboratory Safety Agreement and Procedures Signature Form. Please sign next to your station number. Please use a pen and write legibly. If you make a mistake, ask your instructor what the proper procedure is for correcting the mistake.
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  • Open the Equipment file. Students complete the equipment check-in sheets. Submit them to the instructor when finished. These sheets will be kept on file in the lab coordinators office.