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STUDENT TRAINING PRESENTATION NAME : IZZAH SOFIAHANUN BINTI ISHAK STUDENT ID: 2011816436 PROGRAMME : BACHELOR OF ENGINEERING (HONS) OF OIL AND GAS SUPERVISOR : EN SUHAIMI BIN AHMAD DEPARTMENT : ASSET COGEN WATER (ACW) 1

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Student Training Presentation

Student Training PresentationNAME : IZZAH SOFIAHANUN BINTI ISHAKSTUDENT ID: 2011816436PROGRAMME : BACHELOR OF ENGINEERING (HONS) OF OIL AND GASSUPERVISOR : EN SUHAIMI BIN AHMADDEPARTMENT : ASSET COGEN WATER (ACW)

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Presentation OutlineIntroductionCompany BackgroundProcess Flow PlantActivitiesConclusion2

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IntroductionIndustrial training is one of compulsory courses in learning curriculum for UiTMThe objective of industrial training is : To familiarize and expose the student with the real working environment To widen skill in safety practices, work ethics, communication, management, etc3

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Company Background

Internship location: Petronas Gas ( PGB ) : Utilities KertehInternship duration : 5 Month

Utilities Kerteh (UK) is one of the division under PGB which is grouped in the Gas processing and utilities ( GPU )

Located at Kerteh Integrated Petrochemical Complexes (KIPC).

UK provide utilities to surrounding industrial customers within KIPC area. i.e: Power, Steam, industrial gas and Industrial water

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Company Background cont.VISSION A World Class Gas and Utilities Company

MISSIONWe are a business entity Gas is our core businessOur primary responsibility is to add value to this natural resource

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UK Feed and Product6

EQUIPMENT

AIR SEPARATION UNIT

COGENERATION

PACKAGED BOILER

WATER TREATMENT

DEMINERALISED WATER

CONDENSATE POLISHING

INSTRUMENT/PLANT AIR

CUSTOMERS

I

M

P

O

R

T

E

X

P

O

R

TFEEDSTOCK

NATURAL GAS

AIR

WATERPRODUCTSELECTRICITYCOOLING WATER STEAMNITROGENDEMIN WATERFIRE FIGHTING WATER

CHEMICALPOTABLE WATEROXYGENARGON

PRIMARY/ SECONDARY WASTE(SCREENED)SEMI SOLID WASTE (STORED AND READY FOR DISPOSAL)

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UK O&M Structure: Main Section

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Utilities Kerteh Section HeadA Sharifudden Abdullah

ASU & Utilities Unit HeadM Zaini M ZainCogen and Water Unit HeadAzli IsmailMaintenance Unit HeadAhmad Radzuri IsmailHSE Unit HeadAdiba Farhana Abu Bakar

Attached Department

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Department Background8Asset Cogen Water (ACW)Asset WaterAsset Cogen

Demineralized Plant (Demin)Effluent Treatment Plant (ETP)Cooling TowerCogen Plant

Process Flow Plant

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Demin Plant

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ActivitiesDaily ActivityPlant operation monitoring i.e: Field data collectionDCS data monitoringLab analysis result compilation

Project Basis i.e:OGT Produced water transfer and treatment at UKCP A & E vessel repair and commissioningRO chemical cleaningDemin Plant Overall Equipment Effectiveness ( OEE )

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Daily activities (cont)Field Data CollectionThe job scobe of this activity is to check daily process equipment data and recorded it according in daily log book sheet.The operating data is required to monitor and ensure equipment operated within control range

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The picture above show the example of daily log book sheet that need to be filled by operator

Daily activities (cont)Distributed Control System (DCS) data monitoringAll the plant and machineries are being monitored through DCS in the panel room to ensure that the condition maintained in safe range.From DCS panel, any abnormalities or defect can be detected and immediate action can be taken.

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Daily activities (cont)Lab analysis result compilation

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The figure shows the template of LODS for lab analysis use in UK

Project

14CP A & E vessel repair and commissioningRubber lining is installed on the steel wall of condensate polisher to prevent corrosion to occur by:i. Preventing acid to make contact with the wall of CP.ii. Avoid oxidation process on the metal due to H2 and O2 presence.

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15There is blister inside rubber lining on the wall of CPMid collector installed bent due to high pressure and high flow of waterProblem

Blister been markedRemoving the rubber lining and install the new2. Installation of new mid collector.

Solution

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Project (cont..)

OGT has been operating for many years ago since 1983. For the past few years, OGT has been experienced fluctuation in produced water flow and volume during the production due to aging reservoirTimeline of the project are as follows ;162. OGT Produced water transfer and treatment at UKDate Remarks10/8/2014Meeting with OGT representative to discuss on the letter agreement 20/8/2014Meeting with contractor assigned (MRSB) , discussing on the standard operating procedure (SOP) for transporting the waste water14/10/2014Meeting on the preparation for first tanker delivery on the next day15/10/2014First tanker of OGT produced water has been successfully transported to UK19/10/2014Meeting regarding the raised issue on the analysis data for both party are not tally. Discussing the solution/ action to solve the problem20/10/2014Site visit to OGT to establish the area and method to take the sample for lab analysis1/12/2014Meeting with OGT representative on correlation result of lab analysis

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Project (cont)

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The figure show the first tanker of produced water has been transported on 15 October 2014

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Project183. RO Chemical Cleaning When to clean

After a certain time where the RO membrane becomes fouled and clogged with dirt and mineral deposited on the membraneReduced the RO performanceCheck the conductivity of MRO and BROHow to clean

During the cleaning process, a flexible hose will attached from RO Cleaning Skid to Inlet of RO Filter Membrane while another flexible hose is attached at the RO reject water outlet to drain out Chemical used ie : Acid HydrochloridFormalin (caustic)Detergent

RO chemical Cleaning

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The process of RO chemical cleaning

Project

OEE is the calculation to determine the overall effectiveness of equipmentOEE quantifies how well a manufacturing unit performs relative to its designed capacity, during the periods when it is scheduled to run.

204. Demin Plant Overall Equipment Effectiveness ( OEE )

The template of Daily Log Sheet used in determining OEE of Demin Plant

Project (cont)21

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External Factor (Total running hours) = taken from the daily log sheet templateStandby Hours= 24- (total running hours+ total not available)Internal Factor = data taken from the daily log sheet templateTotal daily Prod = data taken from the daily log sheet templateTotal slowdown = (design capacity* running hours) total daily prod ie. (110*11.38 )- 1410 The template of OEE used in UK)

Conclusion PETRONAS GAS BERHAD as host company has given me a very good technical exposure and experience opportunity.Based on the on the exprience and exposure during my training period in UK, I standly believe that the objective of the training has been achieved.To familiarize and expose the student with the real working environment To widen skill in safety practices, work ethics, communication, management, etc

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Treatment of Industrial waste water and produced water using membraneFinal Year Project 123Name : Izzah Sofiahanun Binti IshakProgramme : Bachelor of Engineering (Hons) Oil and GasUniversiti : Universiti Teknologi MARA (UiTM)

outlineIntroductionProblem statementObjectiveScope of workSelected literatureMethodologyExpected result

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introductionIndustry oil and gas have become significance for developing country such as Malaysia. However, the increasing industrialization has given some impact on ecosystem and environment which human relies on.Discharging industrial waste water without being treated further can contaminate water and soil that may lead disturbances to the ecosystem. Once the organic pollutants are discharged into watercourse, biodegradation by the microorganism will take place.

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. During the biodegradation process, the microbes will consume the dissolved oxygen in the water. This can reduce the oxygen supply in water needed by the aquatic life and can kill the aquatic life.

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Problem statementWaste water from the refinery and industry has become one of major sources to water pollution. This is because in the various type of industries, a large amount of fresh water is used to be raw material, as a mean of production and also for cooling purpose.Concerning on the environment and ecosystem, the discharge of waste water need to be treated and improve its quality before being released to river, coastal or lake.The use of membrane filtration processes ie microfiltration, nanofiltration, ultra filtration and reverse osmosis has offer a lot of advantages for the treatment.26

objectiveThere are two main objectives for this research which are as follows:To characterize the parameter of industrial waste water after treatedTo treat the industrial waste water using different characteristic of membrane.

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Scope of workThe scope of this research project comprised of two approaches i.e. :Material preparationMaterials used in this research are flat membrane (polymersulfone and polyethersulfone) and industrial waste water (sample from UK)2. Characterization of sample waste water by using 7 parameter i.e : pH, BOD, COD, PO4, NH3, TSS, FCL28

Selected literature

This paper focus on treatment of oily wastewater coming out from the post-treatment unit of petroleum industries.Use polysufone with additives ie : polyvinylpyrrolidone (PVP) and polyethylene glycol (PEG)The experimental results showed oil retentions of almost all the membranes were over 90% oil concentration in the permeate was below 10 mg/L29Ghoshal, A., & Purkait, M. (n.d.). Ultrafiltration of stable oil-in-water emulsion by polysulfone membrane. Journal of Membrane Science, 325(2008), 427-437. Retrieved from Science Direct.

where finely divided oil droplets are uniformly dispersed in large volumes of water

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methodologySynthesis of membrane Raw material : polymer sulfone and polyether sulfone bead Additive: polyvinylpyrrolidone (PVP)Solvent : N-methyl-2-pyrrolidone (NMP) Measured amount of polymer (PSf) and (PES) along with PVP was dissolved in the solvent (NMP) at room temperature (25 C) and relative humidity (72%) to make the casting solution.

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Set up of experiment31

Schematic diagram of experimental set up

Expected resultParameterResultpH 5.5-9COD