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QUALITY ASSURANCE REVIEWGROUNDWATER ANALYTICAL DATA
STANDARD CHLORINE OF DELAWARE, INC. LABORATORY(SAMPLES COLLECTED FROM AUGUST 2, 1990 TO AUGUST 16, 1990)
JANUARY 1991
REMEDIAL INVESTIGATION/FEASIBILITY STUDYSTANDARD CHLORINE OF DELAWARE, INC.
DELAWARE CITY, DELAWARE
PREPARED BY:
WESTON ANALYTICAL LABORATORYA DIVISION OF
ROY F. WESTON, INC.
AR30U357
STANDARD CHLORINEGC VOLATILE
OVERVIEW
This batch totals 95 samples consisting of trip blanks and watersamples that were received at Standard Chlorine of Delaware, Inc.from August 2, 1990 until August 16, 1990. These samples wereanalyzed for GC Volatile target compounds (Method 602) andExtractable Volatile target compounds (Methods 8120/8090). Threedifferent methods were used to obtain the appropriate analyte listsand sample results on the data summary are reported in ppb.Problems have been listed under appropriate analytical method.
METHOD 602
The analytes associated with this method are: benzene, toluene,ethylbenzene, chlorobenzene, dichlorobenzene isomers, and surrogatecompound "trifluorotoluene".
The seven-day holding time was exceeded for one sample GW25-0-1TW24 analyzed by Method 602. The holding time was one day outsideof the limit established by the QAPP. All positive results andquantitation limits are considered estimated.
Method blanks were not analyzed for all of the analysis dates.However, since there were no specific requirements in the QAPP orthe method regarding blank analysis, no qualification has beenapplied.
Most of the matrix spike recoveries were within the method controllimits. No qualification has been applied on this basis alone.
Upon evaluation of the laboratory duplicate data, the overallsample results reproducibility was satisfactory. Several compoundresults were not comparable to the duplicate results. Due to thelack of established QC criteria, the data has not been qualified onthis basis.
Overall, the reported Method 602 data is considered fair. Sampleswith high levels of dilution allow for much bias concerning thesample results. It is the evaluator's opinion that these sampledata are considered estimated and flagged in the data summary.
The laboratory failed to provide QC criteria for surrogaterecoveries; however, the evaluator recommends a ± 40% QC limit forthe a,a,a-Trifluorotoluene surrogate compound. The affectedsamples positive results and quantitation limits are consideredestimated.
AR30U358
Sample Surrogate Recovery
GW27-1-MW2 192.8%GW35-0-1TW31 195.8%
The analytes associated with this method are: trichlorobenzene andtetrachlorobenzene isomers plus penta and hexachlorobenzene.
All extraction/analysis holding times were met for this analysis.
Most method blanks contained very low levels (less than the CRQL)of the target compounds; however, due to the high sample dilutions,the affect of the associated blank levels cannot be determined. Noqualification has been applied.
Several compounds had the amount detected exceed the calibrationrange. The reported results are not considered an actual amount,and are rejected "R" in the data summary.
In "Standard Methods" broad ranges are given for the spike recoverylimits in Method 8120 and 8090. Therefore, the sample has not beenqualified on this basis.
Upon evaluation of the laboratory duplicate data, the overallsample result reproducibility was good. Several compound resultswere not comparable to the duplicate results. Due to the lack ofestablished QC criteria, the data has not been qualified on thisbasis.
Overall, many samples were analyzed at high levels of dilution.The detection limits are elevated; and it is the evaluators'sopinion that these diluted sample results are considered estimated.The affected quantitation limits are flagged MUJ".
METHOD 8090
The analytes associated with this method nitrobenzene and meta-chloronitrobenzene.
Several compounds had the amount detected exceed the calibrationrange. The affected positive results are rejected "R".
GENERAL . • ~~
There were several calculation errors throughout the package. Thedata reported on the summaries have been corrected.
A four point calibration was performed for all methods rather thanthe five point standard calibration. Therefore, the calculatedresults are calculated in reference to the average response factor,instead of using the curves. Although all curves did meet therequired criteria.
The package was missing several pieces of information. Refer tothe phone conversation record and letter attached. All correctionswere resubmitted by the laboratory. (See Attachment III).
INFORMATION REGARDING DATA
All data were reviewed according to Methods 602, 8120, 8090; aswell as the criteria established in the Standard Chlorine QAPP.All data have been validated with regard to usability.
ATTACHMENTS _ ..
1. Attachment I - Glossary of Data Qualifier Codes
2. Attachment II - Data Summary by Method
A) Lab Chron
B) All positive results for the target analytes witthe gualifier codes, if applicable; and allunusable detection limits (qualified "R").
3. Attachment III - Resubmissions
ATTACHMENT IGLOSSARY OP DATA QUALIFIER CODES
GLOSSARY OF DATA QUALIFIERS
CODES RELATING TO IDENTIFICATION
(confidence concerning presence or absence of compounds)
O - NOT DETECTED, SUBSTANTIALLY ABOVE THE LEVELREPORTED IN LABORATORY OR FIELD BLANKS.
R « UNRELIABLE RESULT. ANALYTE MAY OR MAY NOT BEPRESENT IN THE SAMPLE. SUPPORTING DATANECESSARY TO CONFIRM RESULT.
N = NEGATED COMPOUND WAS CONSIDERED AS NOTPRESENT IN THE SAMPLE.
(NO CODE) = CONFIRMED IDENTIFICATION
CODES RELATING TO QUANTITATION
(can be /used for both positive results and sample guantitationlimits)t
J = ANALYTE PRESENT. REPORTED VALUE MAY NOT BEACCURATE OR PRECISE.
L = ANALYTE PRESENT. REPORTED VALUE MAY BEBIASED LOW. ACTUAL VALUE IS EXPECTED TO BEHIGHER.
UJ = THE REPORTED QUANTITATION LIMITS AREQUALIFIED ESTIMATED.
UL = NOT DETECTED. QUANTITATION LIMIT MAY BEHIGHER.
OTHER CODES __ _ .
Q = NO ANALYTICAL RESULT.
ATTACHMENT IIDATA SUMMARIES
WESTON ANALYTICSPURGEABLE AROHATICS BY GC, METHOD 602
ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
PATE RECEIVED: 08/02/90 RFU LOT #: gooscooaCLIENT ID RFW * MTX PREP I COLLECTION EXTR/PREP ANALYSIS
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
DATE RECEIVED: 08/06/90 RFW LOT #. 9008coog
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
DATE RECEIVED: 08/07/90 RFW LOT #: 9008C007
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
DATE RECEIVED: 08/08/90 RFW LOT f: 9008C008
CLIENT ID RFW I HTX PREP I COLLECTION EXTR/PREP ANALYSIS
GW-14-1-1 MW6 001 W 08/08/90 08/10/90 08/10/90GW-14-1-3 MW6 002 W 08/08/90 08/10/90 08/10/90GU-14-0-1 HW6 003 U 08/08/90 08/10/90 08/10/90GW-15-1-1 MW7 004 W 08/08/90 08/10/90 08/10/90GW-15-0-1 MW7 005 W 08/08/90 08/10/90 08/10/90GW-15-0-2 MW7 006 W 08/08/90 08/10/90 08/10/90GW-16-1-1 MW8 008 W 08/08/90 08/10/90 08/10/90GW-16-0-1 MW8 009 W 08/08/90 08/11/90 08/11/90GW-17-1-1 TW22 010 W 08/08/90 08/11/90 08/11/90GW-17-0-1 TW22 Oil W 08/08/90 08/11/90 08/11/90GW-32-1-1 RW3 012 W 08/08/90 08/10/90 08/10/90GW-32-1-2 RW3 013 W 08/08/90 08/10/90 08/10/90GW-17-1-4 TW22 015 W 08/08/90 08/11/90 08/11/90
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
(DATE RECEIVED: 08/09/90 ; RFW LOT #: 9008C009
CLIENT ID RFW I MTX PREP I COLLECTION EXTR/PREP ANALYSIS
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
ATE RECEIVED: 08/10/90 RFW LOT #: 9008C010
CLIENT ID RFW * MTX PREP # COLLECTION EXTR/PREP ANALYSIS
GW-22-0-1 TW6A 001 W 08/10/90 08/14/90 08/14/90GW-22-1-1 TW6A 002 W 08/10/90 08/14/90 08/14/90GW-22-0-3 TW6A 003 W 08/10/90 08/14/90 08/14/90GW-23-1-1 RW5 004 W 08/10/90 08/14/90 08/14/90GW-23-1-2 RW5 005 W 08/10/90 08/14/90 08/14/90GW-22-1-4 TW6A 007 W 08/10/90 08/15/90 08/15/90
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
DATE RECEIVED: 08/13/90 RFW LQT #
CLIENT ID RFW # MTX PREP i COLLECTION EXTR/PREP ANALYSIS
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WESTON ANALYTICSPURGEABLE AROMATICS BY GC, METHOD 602
ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
RECEIVED: 08/14/90 RFW LOT #.
£NT ID a™ * MTX PREP I COLLECTION EXTR/PREP ANALYSIS
•W-26-I-1 TW25 001 W 08/14/90 08/21/90 08/21/90:W-26-0-l TW25 002 W 08/14/90 08/21/90 08/21/90GW-27-1-1 MW2 003 W 08/14/90 08/17/90 08/17/90<=W-27-0-l MW2 004 W 08/14/90 08/17/90 08/17/90W-28-1-1 MW4 005 W 08/14/90 08/17/90 08/17/90
uW-28-0-1 MW4 006 W 08/14/90 08/17/90 08/17/90GW-29-1-1 MW3 007 W 08/14/90 08/17/90 08/17/90"W-29-0-1 MW3 008 W 08/14/90 08/17/90 08/17/90W-30-1-1 TW50 009 W 08/14/90 08/17/90 08/17/90
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
DATE RECEIVED: 08/15/90 RFW LOT I: 9008C015
ID RFW # MTX PREP * COLLECTION EXTR/PREP ANALYSIS
GW-33-1-1 TV49 001 W 08/15/90 08/21/90 08/21/90GW-33-0-1 TW49 002 U 08/15/90 08/21/90 08/21/90GW-34-1-1 MW1 003 U 08/15/90 08/21/90 08/21/90GW-34-0-1 MW1 004 W 08/15/90 08/20/90 08/20/90GW-34-0-2 HW1 005 W 08/15/90 08/20/90 08/20/90GW-35-1-1 TW31 007 W 08/15/90 08/21/90 08/21/90GW-3S-0-I TW31 008 W 08/15/90 08/20/90 08/20/90GW-35-0-2 TW31 009 W 08/15/90 08/20/90 08/20/90GW-36-0-1 TW5 Oil W 08/15/90 08/21/90 08/21/90GW-36-1-1 TW5 012 W 08/15/90 08/21/90 08/21/90GW-36-Q-4 TW5 013 W 08/15/90 08/21/90 08/21/90
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WESTON ANALYTICS8090
ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
'ATE RECEIVED: 08/15/90 RFW LOT #: 9008C015
'CLIENT ID RFW I MTX PREP * COLLECTION EXTR/PREP ANALYSIS
GW-33-1-1 TW49 001 W 08/15/90 08/20/90 09/22/90GW-33-0-1 TW49 002 W 08/15/90 08/20/90 09/22/90GW-34-1-1 MW1 003 W 08/15/90 08/20/90 09/22/90GW-34-0-1 MW1 004 W 08/15/90 08/18/90 08/20/90GW-34-0-2 MW1 005 W 08/15/90 08/18/90 08/20/90GW-35-1-1 TW31 007 W 08/15/90 08/20/90 09/22/90GW-35-0-1 TW31 008 W 08/15/90 08/18/90 08/20/90GW-35-0-2 TW31 009 W 08/15/90 08/18/90 08/20/90GW-36-0-1 TW5 Oil W 08/15/90 08/20/90 09/22/90GW-36-1-1 TW5 012 W 08/15/90 08/20/90 09/22/90
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WESTON ANALYTICSv??MATICS BY GC' METHOD 602ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
DATE RECEIVED: 08/16/90 RFW LQT #;
CLI£NT ID ' R« I MTX PREP » COLLECTION EXTR/PREP ANALYSIS
GW-37-1-1 TW28 001 W 08/16/90 08/21/90 08/21/90GW-37-0-1 TW28 002 W 08/16/90 08/22/90 08/22/90GW-38-M TW30 003 W 08/16/90 08/22/90 08/22/90GW-38-0-1 TW30 004 W 08/16/90 08/22/90 08/22/90GW-38-0-3 TW30 005 W 08/16/90 08/22/90 08/22/90GW-39-1-1 RW2 006 W 08/16/90 08/21/90 08/21/90GW-39-I-2 RW2 007 W 08/16/90 08/21/90 08/21/90GW-39-0-4 RW2 009 W 08/16/90 08/22/90 08/22/90
WESTON ANALYTICS8010/8020
ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
DATE RECEIVED: 08/02/90 RFW LOT #: 9008C003
CLIENT ID RFW * MTX PREP * COLLECTION EXTR/PREP ANALYSIS
GW-5-0-1 MW13 001 W 08/02/90 08/03/90 08/06/90GH-5-1-1 MW13 002 W 08/02/90 08/03/90 08/06/90GW-6-0-1 MW10 003 W 08/02/90 08/03/90 08/07/90GW-6-1-1 MW10 004 W 08/02/90 08/03/90 08/07/90GW-7-0-1 C30 005 W 08/02/90 08/06/90 08/22/90GW-7-0-2 C30 006 W 08/02/90 08/06/90 08/22/90fiW-7-0-3 C30 007 W 08/02/90 08/06/90 08/23/90GW-7-1-1 C30 008 W 08/02/90 08/06/90 08/23/90GW-7-1-3 C30 009 W 08/02/90 08/06/90 08/23/90GW-8-0-1 C31 Oil W 08/03/90 08/06/90 08/23/90GW-8-1-1 C31 012 W 08/03/90 08/06/90 08/23/90GW-9-0-1 MW9 013 W 08/03/90 08/07/90 08/23/90GW-9-1-1 MW9 014 W 08/03/90 08/07/90 09/13/90GW-9-0-3 MW9 015 W 08/03/90 08/07/90 08/23/90
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
DATE RECEIVED: 08/06/90 RFW LOT I: 9008C006
CLIENT ID RFW * MTX PREP # COLLECTION EXTR/PREP ANALYSIS
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
,DATE RECEIVED: 08/07/90 RFW LOT f. 9008COQ7
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
'ATE RECEIVED: 08/08/90 RFW LOT #: 9008C008
CLIENT ID RFW i MTX PREP I COLLECTION EXTR/PREP ANALYSIS
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
DATE RECEIVED: 08/09/90 RFW LOT #: 9008C009
CLIENT ID RFW # MTX PREP # COLLECTION EXTR/PREP ANALYSIS
GW-20-I-1 TW10 001 W 08/09/90 08/13/90 09/14/90GW-20-0-1 TW10 002 W 08/09/90 08/13/90 09/17/90GW-18-1-1 TW1 003 W 08/09/90 08/13/90 09/17/90GW-18-0-1 TW1 004 W 08/09/90 08/13/90 09/17/90GW-21-1-1 RW4 005 W 08/09/90 08/13/90 09/17/90
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
[ATE RECEIVED: 08/10/90 RFW LOT f. 90Q8C010
LIENT ID a™ » MTX PREP I COLLECTION EXTR/PREP ANALYSIS
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
DATE RECEIVED: 08/13/90 RFW LOT ,. 9008C013
CLIENT ID RFW I MTX PREP * COLLECTION EXTR/PREP ANALYSIS
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
DATE RECEIVED: 08/14/90 RFW LOT I: 9008C014CLIENT ID RFW * MTX PREP # COLLECTION EXTR/PREP ANALYSIS
GW-26-1-1 TW25 001 W 08/14/90 08/17/90 09/21/90GW-26-0-1 TW25 002 W 08/14/90 08/17/90 09/21/90GW-27-1-1 MW2 003 W 08/14/90 08/17/90 09/21/90GW-27-0-1 MW2 004 W 08/14/90 08/17/90 09/21/90GW-28-1-1 MW4 005 W 08/14/90 08/17/90 09/21/90GW-28-0-1 MW4 006 W 08/14/90 08/17/90 09/20/90GW-29-1-1 MW3 007 W 08/14/90 08/17/90 09/21/90GW-29-0-1 MW3 008 W 08/14/90 08/17/90 09/21/90GW-3Q-1-1 TW50 009 W 08/14/90 08/16/90 09/19/90GW-30-0-3 TW50 010 W 08/14/90 08/16/90 09/19/90GW-30-0-1 TW50 Oil W 08/14/90 08/16/90 09/20/90GW-31-1-1 RW1 012 W 08/14/90 08/16/90 08/17/90GW-31-1-2 RW1 013 W 08/14/90 08/16/90 08/17/90
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
DATE RECEIVED: 08/15/90 RFW LOT l: 9008C015
CLIENT ID RFH * MTX PREP I COLLECTION EXTR/PREP ANALYSIS
GW-33-1-1 TW49 001 W 08/15/90 08/20/90 09/22/90GW-33-0-1 TW49 002 W 08/15/90 08/20/90 09/22/90GW-34-1-1 MH1 003 W 08/15/90 08/20/90 09/22/90GW-34-0-1 MW1 004 W 08/15/90 08/18/90 08/20/90GW-34-0-2 HW1 005 W 08/15/90 08/18/90 08/20/90GW-35-1-1 TW31 007 W 08/15/90 08/20/90 09/22/90GW-35-0-1 TW31 008 W 08/15/90 08/18/90 08/20/90GW-35-0-2 TW31 009 W 08/15/90 08/18/90 08/20/90GW-36-0-1 TW5 Oil W 08/15/90 08/20/90 09/22/90GW-36-1-1 TW5 012 W 08/15/90 08/20/90 09/23/90
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
DATE RECEIVED: 08/16/90 " RFW LOT f. 9008CQ16
CLIENT ID «™ * MTX PREP f COLLECTION EXTR/PREP ANALYSIS
GW-37-1-1 TW28 001 W 08/16/90 08/21/90 09/24/906H-37-0-1 TW28 002 W 08/16/90 08/21/90 09/24/90GW-38-0-1 TW30 004 W 08/16/90 08/21/90 09/24/90GW-38-0-3 TW30 005 W 08/16/90 08/21/90 09/25/90GW-39-1-1 RW2 006 W 08/16/90 08/21/90 08/22/90GW-39-1-2 RW2 007 W 08/16/90 08/21/90 08/21/90
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DATE RECEIVED: 08/02/90 RFW LOT #: 9008C003
CLIENT ID RFW # MTX PREP # COLLECTION EXTR/PREP ANALYSIS
GW-5-0-1 MW13 001 W 08/02/90 08/03/90 08/06/90GW-5-1-1 MW13 002 W 08/02/90 08/03/90 08/06/90GW-6-0-1 MW10 003 W 08/02/90 08/03/90 08/06/90GW-6-1-1 MW10 004 W 08/02/90 08/03/90 08/08/90GW-7-0-1 C30 005 W 08/02/90 08/06/90 08/22/90GW-7-0-2 C30 006 W 08/02/90 08/06/90 08/22/90GW-7-0-3 C30 007 W 08/02/90 08/06/90 08/22/90GW-7-1-1 C30 008 W 08/02/90 08/06/90 08/23/90GW-7-1-3 C30 009 W 08/02/90 08/06/90 08/23/90GW-8-0-1 C31 Oil W 08/03/90 08/06/90 08/23/90GW-8-1-1 C31 012 W 08/03/90 08/06/90 08/27/90GW-9-0-1 MW9 013 W 08/03/90 08/07/90 08/23/90GU-9-1-1 MW9 014 W 08/03/90 08/07/90 08/23/90GW-9-0-3 MW9 015 W 08/03/90 08/07/90 08/23/90
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
lATE RECEIVED: 08/06/90 RFW LOT #: 9008C006
CLIENT ID RFW * MTX PREP # COLLECTION EXTR/PREP ANALYSIS
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
DATE RECEIVED: 08/07/90 RFW LOT #. 9008C£)07
CL1ENT ID RFW # MTX PREP I COLLECTION EXTR/PREP ANALYSIS
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
DATE RECEIVED: 08/08/90 RFW LOT f. 9008C008
CLIENT ID RFW I MTX PREP t COLLECTION EXTR/PREP ANALYSIS
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ANALYTICAL DATA PACKAGE FORSTANDARD CHLORINE
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' C/iginator
PHONE CONVERSATION RECORD
Conversation with: Date — L _ / — 3_Name - s Timm /Q:</o
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Originator's Initials.
W110-4-63
SENT BY:ROY F, WESTQN S12-23-9Q ; i:OOP« : 215*307401-* 21552475Q3:* 2* — 93-91 W g n i » i i - » a T n , CHLQftlH* » - • a
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208 WELSH POOL ROADPICKERtNG CREEK INDUSTRIAL PARKLIONVILLE. PA 19341-1313PHONE (215)524-7360TELEX. 83-5348
7 January 1991
Mr. Jacob GeorgeManager, Laboratory ServicesStandard Chlorine of Delaware, Inc.Governor Lea RoadP.O. Box 319Delaware City, DE 19706
Dear Mr. George:
The following is a list of missing GC chromatograms for Weston'sground water samples received at your firm during the month ofAugust, 1990.
Sample GW-14-1-3 MW6 (08080-02) - missing the GC chromatogram* -for method 602.
Calibration verification 08/01/90 Std #07319001 - missing theverification for 08/01/90 and OS/,05/90.
ICalibration verification 09/04/90 Std #07319002 - missing theverification for O9/21/90, 09/22/90, 09/23/90 and 09/24/90.
As per our phone conversation of 01/04/91, the calibrationstandards are missing for methods 8010/8020, 8090 for samplesanalyzed on 09/21,22/90 (examples: sample GW-26-1-1 [0814001] andGW-26-O-l [0814002]). What is also peculiar about this situationis that samples analyzed on 09/24,25/90 used the calibrationstandards dated on 09/04/90. Please clarify this problem.
Please respond to these deficiencies immediately. Corrections maybe faxed to (215) 524-6140. Response must be received no laterthan January 11, 1991.
Please feel free to contact me with any questions.
Sincerely,
ROY F,., WESTON, IN?.
Kllyuir SpittlerData Validation Unit LeaderAnalytics Division
CC: Jack Tuschall (Weston)Sharon Nordstrom (Weston)
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