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piperina
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450 4.92805449 5448 5447 5446 5445 5444 4.90457443 5442 4.97921441 5440 4.8216439 4.80476438 4.69324437 4.76987436 4.72093435 4.73617434 4.65301433 4.67941432 4.60458431 4.54077430 4.53099429 4.56102428 4.66481427 4.75196426 4.97921425 5424 5423 5422 5421 5420 4.46732419 4.50209418 4.53011417 4.47576416 4.44368415 4.44368414 4.42058413 4.41314412 4.38461411 4.39157410 4.38461409 4.42815408 4.42815407 4.4199406 4.43584405 4.46808404 4.49394403 4.48515
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Spectru UV-VIS al extractului de piper, obținut prin procedeul Soxhlet
Lungimea de undă, nmA
bso
rban
ța
402 4.47653401 4.43584400 4.47653399 4.43584398 4.49394397 4.51207396 4.59328395 4.59328394 4.62702393 4.62702392 4.58127391 4.58127390 4.61513389 4.72093388 4.59226387 4.70621386 4.61513385 4.75196384 4.65185383 4.61513382 4.52057381 4.58127380 4.58127379 4.72093378 4.62702377 4.59226376 4.58127375 4.62702374 4.57054373 4.61513372 4.60354371 4.63813370 4.06817369 4.17164368 4.16364367 4.21146366 4.17979365 4.26473364 4.26473363 4.27484362 4.21997361 4.2056360 4.20106359 4.24837358 4.25298357 4.26377356 4.26951355 4.33207
354 4.38399353 4.52057352 4.4199351 4.33151350 4.23305349 4.2847348 4.31892347 4.22777346 4.19534345 4.15691344 4.23261343 4.35024342 4.29632341 4.24335340 4.17357339 4.08202338 4.04632337 4.03076336 3.99915335 4.03104334 4.06545333 4.17706332 4.2567331 4.22255330 4.05918329 4.02169328 3.97626327 3.99274326 3.9897325 4.03692324 3.99606323 3.98743322 3.9358321 4.02799320 4.11853319 4.3293318 4.2269317 4.18136316 4.18136315 4.19982314 4.27827313 4.22299312 4.17744311 4.12504310 4.14881309 4.20353308 4.19049307 4.21357
306 4.19534305 4.33486304 4.2614303 4.22646302 4.1986301 4.14409300 4.18969299 4.19819298 4.39994297 4.46885296 4.54167295 4.86111294 5293 5292 5291 5290 5289 4.47653288 4.17473287 3.96848286 4.03889285 3.97235284 4.1682283 4.03635282 4.06636281 3.9338280 3.92981279 3.85643278 3.85144277 3.87234276 3.83644275 3.80825274 3.88567273 3.8708272 3.95778271 3.9153270 3.8352269 3.71971268 3.70555267 3.72724266 3.88092265 3.91894264 3.90707263 3.87895262 3.86375261 3.93916260 3.95311259 4.00724
258 3.97626257 3.89127256 3.9025255 3.92044254 4.0706253 4.08991252 4.27925251 4.2842250 4.3686249 4.47498248 5247 5246 5245 5244 5243 4.41114242 3.69426241 3.25456240 3.16398239 3.01976238 2.8643237 2.61754236 2.37643235 2.13957234 2.07348233 1.92605232 2.01228231 1.97004230 1.9144229 1.76815228 1.64705227 1.59656226 1.56309225 1.68175224 1.36829223 1.27194222 1.30467221 1.29043220 1.32502219 1.05534218 1.06492217 1.12782216 1.12086215 1.16482214 1.16576213 1.17939212 1.06522211 0.96989
210 0.93564209 1.02237208 1.01284207 1.0278206 1.02302205 1.08922204 1.18467203 1.03069202 1.00944201 0.99631200 1.11205199 1.30394198 1.22303197 0.99929196 0.9017195 1.01161194 1.08207193 1.23546192 1.14216191 1.05496190 1.10123
150 200 250 300 350 400 450 5000
1
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5
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Spectru UV-VIS al extractului de piper, obținut prin procedeul Soxhlet
Lungimea de undă, nm
Ab
sorb
anța
450 5449 5448 5447 5446 5445 5444 5443 4.95288442 5441 5440 5439 5438 5437 4.90457436 4.76835435 4.66601434 4.61619433 4.60458432 4.64039431 4.69324430 4.67941429 4.75343428 4.90666427 5426 5425 5424 5423 5422 5421 5420 4.50209419 4.59226418 4.65185417 4.60354416 4.61513415 4.60354414 4.59226413 4.60354412 4.53987411 4.57054410 4.50209409 4.50209408 4.47576407 4.52057406 4.55078405 4.65301404 4.65301403 4.80312
150 200 250 300 350 400 450 5000
1
2
3
4
5
6
Spectru UV-VIS al extractului de piper, obținut prin extracție la cald
Lungimea de undă, nm
Abso
rban
ța
402 4.78697401 4.82332400 4.67818399 4.65185398 4.69197397 4.78539396 4.8427395 4.80312394 4.76835393 4.72093392 4.8409391 4.8409390 4.97921389 4.8823388 4.8823387 4.8409386 4.8823385 4.95288384 5383 4.97921382 5381 5380 5379 5378 5377 5376 5375 5374 5373 4.90457372 4.76835371 5370 4.07766369 4.09086368 4.13552367 4.10152366 4.22996365 4.24426364 4.35784363 4.26951362 4.24335361 4.29073360 4.20106359 4.32599358 4.37715357 4.48436356 4.37041355 4.24335
354 4.2857353 4.27435352 4.33823351 4.27435350 4.3903349 4.31946348 4.3903347 4.38274346 4.34334345 4.27925344 4.54986343 4.49313342 4.67695341 4.59024340 4.09182339 4.14014338 4.04661337 4.12608336 4.0495335 4.09246334 4.04892333 4.06186332 4.05534331 4.01253330 4.02414329 4.06216328 4.11785327 4.26188326 4.27729325 4.23128324 4.08832323 4.04288322 4.07182321 4.10679320 4.11011319 4.09924318 4.06186317 4.1861316 4.28371315 4.40125314 4.35962313 4.32163312 4.34677311 4.27241310 4.25159309 4.15247308 4.07859307 4.05563
306 4.0789305 4.16478304 4.15616303 4.11346302 4.15616301 4.29377300 4.51376299 4.82505298 4.4524297 4.49475296 4.56102295 5294 5293 5292 5291 5290 5289 5288 4.58424287 4.31892286 4.08959285 4.04031284 4.02772283 3.99071282 3.95591281 3.85662280 3.81597279 3.84541278 3.80377277 3.83202276 3.77201275 3.79594274 3.71903273 3.74328272 3.76367271 3.91339270 3.88467269 3.86908268 3.82091267 3.79984266 3.8131265 3.82401264 3.81869263 3.85273262 3.84851261 3.77524260 3.92152259 3.93335
258 4.14158257 4.07643256 4.06515255 3.95802254 3.98567253 4.00514252 4.36558251 4.48673250 5249 5248 5247 5246 5245 5244 5243 3.97114242 3.51766241 3.51706240 3.21821239 2.95176238 2.97192237 2.60009236 2.53673235 2.26013234 2.14983233 1.9826232 1.76091231 1.68237230 1.70559229 1.74467228 1.56405227 1.54074226 1.53728225 1.63351224 1.62925223 1.47232222 1.46934221 1.33187220 1.28643219 1.37067218 1.15113217 1.07574216 0.97862215 1.11028214 1.2213213 1.46457212 1.48845211 1.31613
210 1.39705209 1.4414208 1.45709207 1.2196206 1.23874205 1.40163204 1.38686203 1.2363202 1.01404201 1.10102200 1.05219199 1.04347198 1.1228197 0.93938196 1.14007195 1.03249194 1.02536193 0.9855192 0.95302191 0.9655190 0.90182
150 200 250 300 350 400 450 5000
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Spectru UV-VIS al extractului de piper, obținut prin extracție la cald
Lungimea de undă, nm
Abso
rban
ța
450 2.57345449 2.60925448 2.66646447 2.72807446 2.78718445 2.84807444 2.90526443 2.96755442 3.02957441 3.08186440 3.13189439 3.17295438 3.21442437 3.2561436 3.29936435 3.35637434 3.40735433 3.46566432 3.52549431 3.59358430 3.65982429 3.73631428 3.81784427 3.91594426 3.99812425 4.07182424 4.09567423 4.09567422 4.06156421 4.00045420 3.72366419 3.70752418 3.70752417 3.69478416 3.69465415 3.68905414 3.69606413 3.71364412 3.72257411 3.72257410 3.70766409 3.70489408 3.71646407 3.72545406 3.73308405 3.74543404 3.74543403 3.75167
150 200 250 300 350 400 450 5000
1
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Spectru UV-VIS al extractului de piper, obținut prin macerare
Lungimea de undă, nmA
bso
rban
ța
402 3.75505401 3.75021400 3.75021399 3.76987398 3.76805397 3.77293396 3.74673395 3.73886394 3.72052393 3.7342392 3.73871391 3.745390 3.73406389 3.73871388 3.72339387 3.71431386 3.70991385 3.68829384 3.69401383 3.65617382 3.65758381 3.63847380 3.63723379 3.63589378 3.6321377 3.60375376 3.59572375 3.5718374 3.55914373 3.56319372 3.56633371 3.55699370 3.73322369 3.78114368 3.82992367 3.83167366 3.83715365 3.82922364 3.81394363 3.83485362 3.85886361 3.87974360 3.87138359 3.89289358 3.91829357 3.88368356 3.88786355 3.91297
354 3.92217353 3.877352 3.8436351 3.82435350 3.84162349 3.83378348 3.80147347 3.76038346 3.76382345 3.79497344 3.78951343 3.80758342 3.71849341 3.71971340 3.73985339 3.64999338 3.64368337 3.67608336 3.74443335 3.80692334 3.79255333 3.75711332 3.74789331 3.74789330 3.73999329 3.74185328 3.76593327 3.76593326 3.75756325 3.75608324 3.76744323 3.75593322 3.75431321 3.78808320 3.81142319 3.82401318 3.79111317 3.81801316 3.85126315 3.84723314 3.82418313 3.81835312 3.82177311 3.82765310 3.84906309 3.87196308 3.83733307 3.82974
306 3.79675305 3.8041304 3.81835303 3.84924302 3.85942301 3.94757300 3.96513299 3.95451298 3.94895297 3.96921296 3.99581295 4.09278294 4.22255293 4.22169292 4.56576291 4.14337290 3.85606289 3.63622288 3.60469287 3.59972286 3.69529285 3.59582284 3.57724283 3.46039282 3.4199281 3.39132280 3.38324279 3.37066278 3.40689277 3.39845276 3.39529275 3.38217274 3.34522273 3.38745272 3.41268271 3.43072270 3.4362269 3.38537268 3.41523267 3.447266 3.50755265 3.5002264 3.52601263 3.4719262 3.56939261 3.59267260 3.67498259 3.61716
258 3.62637257 3.62615256 3.61534255 3.61353254 3.59654253 3.63232252 3.67929251 3.68879250 3.68377249 3.76367248 3.7314247 3.83414246 3.76563245 3.47855244 3.2567243 3.08547242 2.95425241 2.70675240 2.59779239 2.38916238 2.21097237 2.13544236 2.03343235 1.94179234 1.72841233 1.65627232 1.48988231 1.40409230 1.31483229 1.26923228 1.26021227 1.23889226 1.09316225 0.94966224 0.87555223 0.90488222 0.89627221 0.901220 0.82065219 0.75019218 0.68959217 0.71355216 0.71138215 0.68737214 0.69592213 0.70873212 0.76175211 0.74801
210 0.71765209 0.60126208 0.57498207 0.58505206 0.69552205 0.70161204 0.71549203 0.67741202 0.69146201 0.6446200 0.64451199 0.62275198 0.57747197 0.57401196 0.57602195 0.60901194 0.60826193 0.58592192 0.5876191 0.57692190 0.54177
150 200 250 300 350 400 450 5000
1
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3
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5
Spectru UV-VIS al extractului de piper, obținut prin macerare
Lungimea de undă, nm
Ab
sorb
anța
450 1.66277449 1.69188448 1.73658447 1.78673446 1.83806445 1.8901444 1.94243443 1.99306442 2.04357441 2.09185440 2.14125439 2.18878438 2.23679437 2.28462436 2.33463435 2.39228434 2.45427433 2.52698432 2.60767431 2.706430 2.81869429 2.9464428 3.08396427 3.23341426 3.38311425 3.52793424 3.64414423 3.7271422 3.74428421 3.75255420 3.68065419 3.68615418 3.69171417 3.69031416 3.69877415 3.69465414 3.68102413 3.69209412 3.6893411 3.70032410 3.69057409 3.70332408 3.70752407 3.70032406 3.6989405 3.70607404 3.70885403 3.73744
150 200 250 300 350 400 450 5000
0.51
1.52
2.53
3.54
4.5
Spectru UV-VIS al extractului de piper, obținut prin cromatografie pe coloană
Lungimea de undă, nm
Ab
sorb
anța
402 3.74688401 3.75505400 3.7314399 3.72973398 3.739397 3.74371396 3.7549395 3.72807394 3.71297393 3.70568392 3.72339391 3.72627390 3.74486389 3.73084388 3.70542387 3.67744386 3.67327385 3.68427384 3.67339383 3.66673382 3.63836381 3.63221380 3.63466379 3.62856378 3.62626377 3.60961376 3.60825375 3.58344374 3.57695373 3.54775372 3.54167371 3.53091370 3.65046369 3.67744368 3.69388367 3.74142366 3.75211365 3.80328364 3.80642363 3.81377362 3.80279361 3.79707360 3.83609359 3.82453358 3.8384357 3.82643356 3.81142355 3.81327
354 3.75919353 3.76578352 3.77927351 3.81344350 3.80394349 3.78618348 3.74774347 3.70792346 3.70097345 3.71849344 3.7321343 3.69786342 3.661341 3.63544340 3.68766339 3.71903338 3.72366337 3.66721336 3.69709335 3.70371334 3.6478333 3.66053332 3.66613331 3.69171330 3.6767329 3.67904328 3.72311327 3.69414326 3.71565325 3.70097324 3.74313323 3.74156322 3.76412321 3.71552320 3.71257319 3.73168318 3.75036317 3.82904316 3.84705315 3.80493314 3.78068313 3.7737312 3.76896311 3.80361310 3.79675309 3.82609308 3.78776307 3.77416
306 3.77232305 3.77079304 3.82974303 3.82211302 3.81428301 3.77324300 3.76142299 3.82453298 3.84979297 3.88686296 3.93269295 4.05888294 4.02634293 3.96061292 3.85458291 3.84108290 3.75182289 3.65429288 3.56824287 3.49286 3.43918285 3.44548284 3.47498283 3.44017282 3.35216281 3.25745280 3.2509279 3.24195278 3.27363277 3.30111276 3.32217275 3.40262274 3.42448273 3.43634272 3.43289271 3.43953270 3.43911269 3.41489268 3.43592267 3.46938266 3.46717265 3.48936264 3.48483263 3.48145262 3.4763261 3.4904260 3.49048259 3.49337
258 3.5317257 3.63578256 3.71538255 3.68829254 3.60044253 3.63432252 3.6522251 3.69057250 3.64028249 3.61587248 3.53808247 3.45475246 3.39259245 3.41054244 3.15743243 2.99514242 2.89378241 2.76826240 2.59187239 2.43958238 2.28042237 2.03024236 1.82316235 1.7162234 1.57806233 1.53474232 1.39682231 1.43296230 1.34595229 1.28964228 1.12448227 1.05223226 1.01395225 1.02958224 0.91094223 0.81027222 0.74778221 0.70483220 0.66717219 0.64616218 0.60957217 0.58191216 0.62117215 0.5866214 0.57904213 0.58732212 0.59535211 0.60172
210 0.61358209 0.6015208 0.61212207 0.60889206 0.64843205 0.58929204 0.61006203 0.52908202 0.56218201 0.53916200 0.55568199 0.56629198 0.56112197 0.58604196 0.54387195 0.57533194 0.51101193 0.49472192 0.45607191 0.48084190 0.5078
150 200 250 300 350 400 450 5000
0.51
1.52
2.53
3.54
4.5
Spectru UV-VIS al extractului de piper, obținut prin cromatografie pe coloană
Lungimea de undă, nm
Ab
sorb
anța