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AP-42 Section Number: 1.8
Reference Number:
Title:
41
Source Test Report for Particulate Emissions Twin Impingement Wet Scrubbers Boiler Number 3
November 1991
i
>-
SOURCE TEST REPORT
PARTICULATE EMISSIONS for
TWIN IMPINGEMENT WET SCRUBBERS BOILER NUMBER 3
NOVEMBER 21, 1991
Prepared for:
SUGAR CANE GROWERS COOPERATIVE OF FLORIDA
AIRPORT ROAD BELLE GLADE, FLORIDA 33430-0666
Prepared by:
AIR CONSULTING AND ENGINEERING, INC. 2106 N.W. 67TH PLACE, SUITE 4 GAINESVILLE. FLORIDA 32606
(9041 335-1889
236-91-03
TABLE OF CONTENTS
SECTION - PAGE
1 . D INTRODUCTION .................................................. 1
2.0 SUHMARY AND DISCUSSION OF RESULTS ............................. 2
3 .O PROCESS DESCRIPTION AND OPERATION ............................. 4
4 . D SAHPLING POINT LOCATION ....................................... 5
5 . 0 FIELD AND ANALYTICAL PROCEDURES ............................... 7 5 . 1 PARTICULATE HATTER SAHPLING AND ANALYSIS--EPA HETHOD S . . . . . . . . 7
APPENDICES
APPENDIX A--COHPLETE EMISSION DATA
APPENDIX E--FIELD DATA SHEETS
APPENDIX C--LABORATORY ANALYSIS
APPENDIX D--PRODUCTION RATE CERTIFICATION
APPENDIX E--QUALITY ASSURANCE
APPENDIX F--PROJECT PARTICIPANTS
i
LIST OF TABLES
- PAGE
1 EMISSION SUMMARY ..................................... 3
LIST OF FIGURES
PAGE FIGURE - 1 SAMPLING POINT LOCATION .............................. 6
2 EPA METHOD 5 SAMPLING TRAIN .......................... 8
ii
AIR CONSULTING & ENGINEERING. INC.
2106 N. W. 67th Place - Suite 4 . Gainesville, Florida 32606 (904) 335-1889 FAX (904) 335-1891
REPORT CERTIFICATION
To the best of my knowledge, all applicable field and analytical
procedures comply with Florida Department of Environmental Regulation
requirements and all test data and plant operating data are true and correct.
q m w 4 e C - e Uagmg,r"eck
/do / 9 / Date
.., 111
1 .O INTRODUCTION
On November 21, 1991, Air Consulting and Engineering, Inc. (ACE), conducted
particulate emission testing on the Wet Scrubber Outlet of Boiler 3 at Sugar
Cane Growers Cooperative of Florida (Sugar Cane Growers) located in Belle
Glade, Florida.
Testing was performed to demonstrate compliance with the current Florida
Department of Environmental Regulation (FDER) operating permit.
United States Environmental Protection Agency (EPA) Method 5 was utilized for
the emission testing.
Mr. Ken Tucker and Mr. Sterling Jordan of the FDER observed a portion of the
testing.
Mr. Blas Marin of Sugar Cane Growers coordinated testing and provided
production data.
1
2.0 SUMMARY AND DISCUSSION OF RESULTS
Boiler Number 3 demonstrated compliance with the permit conditions.
Table 1 is a summary of the emission results and flue gas parameters.
Particulate emissions averaged 35.53 pounds per hour (IbslHr) and 0.181 pounds
per million BTU (IbslMMBTU) which is within the allowable emissions of 45.78
IbslHr and 0.233 Ibs/MMBTU.
Complete emission summaries, field data sheets and laboratory data are
presented in Appendices A, B, and C, respectively.
Production rate summaries are provided in Appendix D. This data was obtained
from control room recordings of steam flow, temperature, and pressure as
well as feed water temperature and pressure. Residue integrator and oil meter
readings were recorded a t the beginning and end of each particulate run.
I 2
Table 1 Emission Summary Boiler Number 3 Sugar Cane Growers Cooperative of Florida Belle Glade, Florida November 21, 1991 I
I Run Flow Rate Stack Stack Particulate Emissions Allowable Emissions
Number SCFMD Temp. Moisture lbs/Hr lbs/MMBTU lbs/Hr lbs/MMBTU I
OF %
1 58456 149 28.0 40.43 0.211 46.12 0.241
2 55686 157 27.1 30.79 0.159 44.16 0.228
3 54050 157 27.1 35.36 0.174 47.06 0.231
AVERAGE 56064 154 27.4 35.53 0.181 45.78 0.233
3
3.0 PROCESS DESCRIPTION AND OPERATION
I The Number 3 Boiler at Sugar Cane Growers is a spreader stoker design used
primarily for residue fuel firing. Supplemental oil firing was also utilized
for the emission test. The boiler averaged 102,676 IbslHr steam production
over the three run test period.
Oil meters, steam integrators, and other production monitoring devices were
rigorously calibrated prior to the production season.
i
I
4
,
4.0 SAMPLING POINT LOCATION
The sampling point location (Figure 1 ) consists of dual scrubber outlet
stacks, each 64" in diameter. Each stack has two sample ports 90 degrees
apart. The ports on the south stack are located 126 from an upstream
disturbance and 64" from the outlet.
Twenty-four test points were sampled on each stack for each test run. The
traverse were located as shown below. The stack configuration is such that
there was no reason to evaluate the presence of cyclonic flow.
5
c
E
-
- 64'- ...
A
64.
c- - SAMPLING PORTS
126.
U
gCHES INSIDE C A C K WALL
I 2 3 4
S 6
7 8 9
10
I 1
12
~~
I .4
4 .3
7.6 11.3
16.0
22.8
' 4 1 . 2
48.0
52.7
S6.4
s9.7 62.6
UPSTREAM -0 ISTUR BANCE
FIGURE I.
SAMPLING POINT LOCATION BOILER N 0 . 3 SUGARCANE GROWERS COOP OF FLORIDA I
A I R CONSULTING and
ENGINEERING
6
5.0 FIELD AND ANALYTICAL PROCEDURES
5.1 Particulate Matter Sampling and Analysis--EPA Method 5 (Glass Probe1
Particulate matter samples were collected by the particulate matter emission
measurement method specified by the United States Environmental Protection
Agency. A schematic diagram of the sampling train used is shown in Figure 2.
All particulate matter captured from the nozzle to, and including, the filter
was included in the calculation of the emission rate of particulate matter.
PREPARATION OF EQUIPMENT
1. FILTERS - Gelman type "A" filters were placed in a dr ing
a standard desiccator containing indicaring silica gel, allowed to cool for two hours, and weighed to the nearesi 0.1 mg. The filters were then re-desiccated for a minimum of six hours and weighed to a constant weight (less than 0.5 mg change from previous weighing). The average of the two constant weights was used as the tare weight.
2. NOZZLE, FILTER HOLDER, AND SAMPLING PROBE - The nozzle, filter holder, and sampling probe were washed vigorously with soapy water and brushes, rinsed with distilled water and acetone, and dried prior to the test program. All openings on the sampling equipment were sealed while in transit to the test site.
IMPlNGEilS - The Greenburg-Smith impingers were cleaned with a warm soaoy water solution and brushes, rinsed with distilled water and acetone, and dried. The impingers were sealed tightly during transit.
oven for t w o hours a t 105 degrees C. removed and p Y ' aced in
3.
'TEST PROCEDURE
Prior to performing the actual particulate matter sample runs, certain stack
and stack gas parameters were measured. These preliminary measurements
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included the average gas temperature, the stack gas velocity head, the stack
gas moisture content, and the stack dimensions a t the point where the tests
were being performed. The stack gas temperature was determined by using a
bimetallic thermocouple and calibrated pyrometer. Velocity head measurements
were made with calibrated type "S" pitor tube and an inclined manometer.
Velocity head measurements of 0.05 inches H20 or less were measured utilizing
a micromanometer.
The sampling traverse points were selected so that a representative sample
could be exrracred from the gas stream. The traverse points were located in
the center of equal areas, the number of which were dependent upon the
distance upstream and downstream from flow disturbances.
,
Each particulate matter test run consisled of sampling for a specific amount
of time a t each traverse point. The type "S" pitot tube was connected to the
sampling probe so that an instantaneous velocity head measurement could be
I
I
made at each traverse point while making the test run. The slack gas
temperature was also measured a t each traverse point. Nomographs were used to
calculate the isokinetic sampling rate a t each traverse point during each test
run.
1
The gases sampled passed through the following components: a stainless steel
nozzle and glass probe; a glass fiber filter: two impingers each with 100 ml
9
Of distilled deionized water; one impinger dry; one impinger with 200 grams of
silica gel; a flexible sample line; an air-tight pump; a dry test meter; and a
calibrated orifice. The second impinger had a standard tip, while the first,
third, and fourth impingers had modified tips with a 0.5 inch I.D. opening.
Sample recovery was accomplished by the following procedures:
1. The pre-tared filter was removed from its holder and placed in Container 1 and sealed. (This is usually performed in the lab.)
2. All sample-exposed surfaces prior to the filter were washed with acetone and placed in Container 2, sealed and the liquid level marked.
3. The volume of water from the first three impin ers was measured for the purpose of calculating the moisture in t a e stack gas and then discarded.
4. The used silica gel from the fourth impinger was transferred to the original tared container and sealed.
LAB0 RAT0 RY ANALYSIS
The three sample containers from each sample run were analyzed according to
the following procedures:
1. The filter was dried at 105 degrees C for three hours, desiccated for a minimum of one hour, and weighed to the nearest 0.1 mg. A minimum of two such weighings six hours apart was made to determine constant weight.
2. The acetone from Container 2 was transferred to a tared beaker and evaporated to dryness at ambient temperature and pressure, desiccated for 24 hours, and weighed to the nearest 0.1 mg. A minimum of two such weighings six hours apart were made to determine constant weight.
3. The used silica gel in its tared container was weighed to the nearest 0.1 gram.
10
The total sample weight included the weight of material collected on the
filter plus the weight of material collected in the nozzle, sampling probe,
and front half of the filter holder.
' DATA
The field data sheets, calculation sheets, and nomenclature definitions are
included in the appendices of this report.
11
APPENDIX A COMPLETE EMISSION DATA
FILTER iiz:. 113.1 WASH vtg. 7 1 . I:!
.-.= ., . . ~- ~- -. -. -., , >:, r!'
. ~ . -.:z. . . . . - . . . . . , . . , - . . .i ....
. , . i ,'- , .. . . ~ - ' , i , : : _ _ - . ... ._
. . . . . . . . ~ I - ., , : , . - . . ,
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.... .-.r - -. , .. . . . . ....
. . . . . . . . . , . , , ~ , . , ' , t ~ , , . ,,I,.. .......... .......... . . . . / ; , '= h , - ~ I .......
- __ ________ .. _ _ ............ .. -__ :.,..> , ; :. .;.
I
FIELD DATA SHEETS
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APPENDIX C
LABORATORY ANALYSIS
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APPENDIX D
PRODUCTION RATE CERTIFICATION
_ _ _ _ _ _ ._
E:IJILER UPERATI01\1 PARAMETERS
I
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I I I I I I I I I I
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APPENDIX E
QUALITY ASSURANCE AND
CHAIN OF CUSTODY
I
STAXDARD METER CALIBRATION Meter Xumber 1040616
Air Consulting and Engineering. Inc. (ACE1 uses a dry gas meter for the calibration standard. This meter has been calibrated against a wet test meter in triplicate. This data was used to generate a standard meter calibration curve (see next page). Field meter calibrations are corrected to this curve using the following formula:
Y X Y s = Y a
Ya = actuai ratio of field meter to standard meter
Y = ratio of standard meter to wet test meter at a given S flaw rate (from Calibration Curve)
Y = corrected ratio of field meter
The dry standard meter was calibrated on June 11. 1991. and is checked and/or recalibrated at least annually.
STANDARD METER C A L I B R A T I O N AIR CONSULTING and CURVE
JUNE I I , 1991 ENGINEERING
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4IR CONSULTING AND ENGINEERING, Inc. I S A M P L E RECOVERY AND CHAIN OF CUSTODY
R U N NO.
. I I
S A M P L E RECOVERY
CONTAINER LIQUID LEVEL COLOR C 0 M ME NTS NO. MARKED
35 12- - M d T 5- 7 J &
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WATERBLANK 5- 3 Y FILTER BLANK 3 Y 7 3 c
SILICA GEL CONTAINER FINAL WT. INIT. W T N E T WT. COLOR
RUN NO. NO. (Q) ( 0 ) ( P )
200.0
200.0
200.0
200.0
200.0
APPENDIX F
PROJECT PARTICIPANTS
PROJECT PARTICIPANTS
AIR CONSULTING AND ENGINEERING, INC.
Stephen L. Neck, P.E. Project Manager
Gerard Gauthreaux Field Testing
Early McFarland Field Testing
Christy Neck Laboratory Analysis
Dagmar Neck Report Preparation
Candace V. Taylor Document Production
SUGAR CANE GROWERS
Jose Alvarez Test Coordinator
Blas Marin Test Coordinator
Ken Tucker Test Observer
Sterlin Jordan Test 8 bserver
PALM BEACH COUNTY
Jeffrey K. Koerner Test Observer
David Brown Test Observer