1
Solvent Extractions The New and Better Way Presented Before the Twenty-first Annual Convention of The American Oil Chemists" Society, May, 103o By DAVID WESSON beans about 45 cents per pound. Cotton- seed containing 17% protein would carry 340 pounds per ton and be worth on the basis of bean protein $153.00 per ton. As a matter of fact, cottonseed protein has a higher biologic value and should be worth more, several times as much in fact. To utilize this protein is plainly the work of the chemist and the chemical engineer. We all know that by the proper appli- cation of solvents 50 to 55 pounds more crude oil per ton of seed can be made avail- able. We also know that the gossypol and gums can be removed from the meats at the same time, It is also known that with proper handling the crude oil obtained by extraction can be refined and bleached as well or better than that obtained by press- ing. With purified solvents the flavor of the extracted oil can be made equal to the pressed oil. With suitable apparatus the solvent losses should cost not far from press cloth under present methods, and the labor should be much less. In Europe, solvent extraction plants are fast superseding the press rooms for soya beans, copra, palm-kernel and other oil bearing materials. In this country they are used for taking the grease from garbage, cracklings, linseed and other substances. Solvents have not been used on cotton- seed in the past because with improper methods and lack of knowledge of the fundamental requirements of operation it has been impossible to obtain refinable oils. Recent experiments show that these diffi- culties can be overcome, and with suitable separation machinery it is possible to pre- pare a meal running from 60 to 65 per cent protein. Shall we, as chemists, bring about these results or follow the example of the Irish- man who when told to clean and open some oysters served the shells and told the boss that he had cleaned them entirely. ~ HENEVER we hear about how laws were passed keeping gin houses away from towns and villages, and how laws were passed to prevent cottonseed being thrown into the water courses, we feel like patting ourselves on the back to think how much we have done to extract valuable oil from the once despised DAWD WESSO~ cottonseed and how we obtain cattle food and rayon from what is left. Some of us remember the time when most of the oil went into the soap kettles or was burned in miners' lamps, especially in off oil years. We do not have to go back much over forty years to find that the oil used for lard compounds was used sparing- ly, and did not improve the compounds a little bit. Now thanks to the work of the chemist, our vegetable shortenings consist entirely of cottonseed oil and are, in most respects, better than the animal product. In converting the crude oil into refined, we have a process which is 96.5% efficient. Not perfection by any means but much bet- ter than the efficiency of press-room work, which obtains on the average only about 84.5% of the total crude oil in the seed and converts the balance into cattle food and fertilizer, overlooking the fact that the pro- tein of the seed, properly prepared, can be made into a valuable food for the human race. At the present time the oil in the seed is worth about 10 cents per pound, when re- fined. The cheapest vegetable protein in a concentration of 20% is that of beans, which is worth at 10 cents per pound for 258

Solvent extractions— The new and better way

Embed Size (px)

Citation preview

Page 1: Solvent extractions— The new and better way

Solvent Extractions The New and Better Way Presented Before the Twenty-first Annual Convention

of The American Oil Chemists" Society, May, 103o By DAVID WESSON

beans about 45 cents per pound. Cot ton- seed conta in ing 17% prote in would car ry 340 pounds per ton and be wor th on the basis of bean protein $153.00 per ton. As a ma t t e r of fact, cot tonseed protein has a higher biologic value and should be wor th more, several t imes as much in fact. T o utilize this protein is plainly the work of the chemis t and the chemical engineer.

W e all know that b y the proper appli- cation of solvents 50 to 55 pounds more crude oil per ton of seed can be made avail- able. W e also know tha t the gossypol and gums can be removed f rom the meats at the same time, I t is also known that wi th proper handl ing the crude oil obta ined by ext ract ion can be refined and bleached as well or be t te r than tha t obta ined b y press- ing. W i t h purified solvents the flavor of the ex t rac ted oil can be made equal to the pressed oil. Wi th suitable appara tus the solvent losses should cost not far f rom press cloth under present methods, and the labor should be much less.

In Europe , solvent ext rac t ion plants are fast supersed ing the press rooms for soya beans, copra, pa lm-kerne l and other oil bear ing materials . In this count ry they are used for t ak ing the grease from g a r b a g e , cracklings, linseed and o the r substances.

Solvents have not been used on cot ton- seed in the past because with improper methods and lack of knowledge of the fundamenta l requi rements of operat ion it has been impossible to obta in refinable oils. Recent exper iments show tha t these diffi- culties can be overcome, and with suitable separa t ion machinery it is possible to pre- pare a meal running f rom 60 to 65 per cent protein.

Shall we, as chemists , b r ing about these resul ts or follow the example of the Ir ish- man who when told to clean and open some oys ters served the shells and told the boss that he had cleaned them entirely.

~ H E N E V E R we hear about how l a w s w e r e passed keeping

gin houses away from towns and villages, and how laws were passed to prevent cottonseed being thrown into the water courses, we feel like patting ourselves on the back to think how much we have done to extract valuable oil f rom the once despised DAWD WESSO~ cottonseed and how we obtain cattle food and rayon from what is left.

Some of us r e m e m b e r the t ime when mos t of the oil went into the soap ket t les or was burned in miners ' lamps, especial ly in off oil years. W e do not have to go back much over for ty years to find tha t the oil used for lard compounds was used spar ing- ly, and did not improve the compounds a little bit. N o w thanks to the work of the chemist , our vege tab le shor tenings consist ent i rely of cot tonseed oil and are, in mos t respects , be t te r than the animal product .

In conver t ing the crude oil into refined, we have a process which is 96.5% efficient. Not perfect ion by any means but much bet- ter than the efficiency of press - room work, which obta ins on the average only abou t 84.5% of the total crude oil in the seed and conver ts the balance into catt le food and fertilizer, over looking the fact tha t the pro- tein of the seed, p roper ly prepared, can be made into a valuable food for the h u m a n race.

At the presen t t ime the oil in the seed is wor th abou t 10 cents per pound, when re- fined. The cheapes t vege tab le protein in a concentra t ion of 20% is that of beans, which is wor th at 10 cents per pound for

258