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SK-10 High Pressure Rotor
Application Book
Application Book
Application Book
INDEXApplication field: AgricultureHPR-AG-01 Pine LeavesHPR-AG-02 Dried Plant TissueHPR-AG-03 Ground VegetableHPR-AG-04 MaizeHPR-AG-05 HayHPR-AG-06 LentisHPR-AG-07 RootsHPR-AG-08 Tea Leaves
Application field: Catalyst-PigmentsHPR-CA-01 Paint ResiduesHPR-CA-02 Paint PigmentHPR-CA-03 Pd on Allumina Base partial digestionHPR-CA-04 Organo-Metallic PigmentHPR-CA-05 Cu and Mo on Allumina BaseHPR-CA-06 InkHPR-CA-07 High Added Dry PaintsHPR-CA-08 Catalyst Al-Cr-Fe-NiHPR-CA-09 V and Mo on Oxide BaseHPR-CA-10 Pt and Rh on RefractoriesHPR-CA-11 Green Organic PigmentHPR-CA-12 Red Organic PigmentHPR-CA-13 Black Tattoo InkHPR-CA-14 Red Tattoo InkHPR-CA-15 Cosmetic Components
Application field: Ceramic-RefractaryHPR-CE-01 Al2O3 and TiO2 MixtureHPR-CE-02 Al2O3 Sintered at 1800°CHPR-CE-03 Alluminous RefractaryHPR-CE-04 Alumina 90%HPR-CE-05 BCS 315 Refractory BrickHPR-CE-06 Car CatalystHPR-CE-07 Catalyst TiO2 80%, WO3 8%, V2O5 3%HPR-CE-08 CementHPR-CE-09 Enamel SiO2 55%, TiO2 10%, B2O3 10%HPR-CE-10 Frit CeramicHPR-CE-11 Gamma Allumina 90%HPR-CE-12 Glass Fiber BorosilicateHPR-CE-13 ZirconiaHPR-CE-14 Iron Oxide TreatedHPR-CE-15 PbO 68% ZrO2 22% TiO2HPR-CE-16 Primary AluminaHPR-CE-17 QuartzHPR-CE-18 Refractary BrickHPR-CE-19 Refractary Brick Al2O3 35%HPR-CE-20 TiO2 95% V2O5 5%HPR-CE-21 SiO2 Al2O3 RefractoryHPR-CE-22 SRM 1412 Glass SiO2 40-45%HPR-CE-23 Zirconium Oxide
Application field: ChemicalsHPR-CH-01 Montana waxHPR-CH-02 Acid resin
HPR-CH-03 DisterglaminHPR-CH-04 UreaHPR-CH-05 Activated carbon 90%HPR-CH-06 Gelatin vegetable baseHPR-CH-07 Commercial paperHPR-CH-08 Polaroid KM-653 modifierHPR-CH-09 Ferrous chlorideHPR-CH-10 Lithium GreaseHPR-CH-11 Adipic acidHPR-CH-12 Hand soapHPR-CH-13 Adogene 442HPR-CH-14 HEQHPR-CH-15 Paper pulpHPR-CH-16 GreaseHPR-CH-17 Stearic acidHPR-CH-18 Isophtalic acidHPR-CH-19 CaHPO4HPR-CH-20 Acetic acid
Application field: Clinical PharmaHPR-CL-01 CFX-PC ReviconHPR-CL-02 Animal TissueHPR-CL-03 BloodHPR-CL-04 Cosmetic ComponentsHPR-CL-05 DimethylagoxineHPR-CL-06 Fine CellulosHPR-CL-07 Garlic OilHPR-CL-08 Glicerine StearateHPR-CL-09 Granular SaccharoseHPR-CL-10 HairHPR-CL-12 LactoseHPR-CL-13 Lyophilized OrangeHPR-CL-14 Magnesium StearateHPR-CL-15 MannitolHPR-CL-16 Methylviolet BHPR-CL-17 NBS 1577B Bovine LiverHPR-CL-18 PD-01 IMPROVED REVICONHPR-CL-19 PectinHPR-CL-20 Red Colour For TabletsHPR-CL-21 SuppositoryHPR-CL-22 TetracyclineHPR-CL-23 UrineHPR-CL-24 Waxoline OrangeHPR-CL-25 Tooth Paste
Application field: EnvironmentalHPR-EN-01 Ashes of polluted oilHPR-EN-02 Cellulose ester filterHPR-EN-03 Dried biological sludgeHPR-EN-04 Fly ashHPR-EN-05 GrassHPR-EN-06 LeavesHPR-EN-07 Municipal sludgeHPR-EN-08 Municipal waste
Application Book
HPR-EN-09 Nist SRM 2781 dried domestic sludgeHPR-EN-10 PollenHPR-EN-11 SludgeHPR-EN-12 Soil partial digestionHPR-EN-13 Soil total digestionHPR-EN-14 US EPA Method 3015HPR-EN-15 US EPA Method 3052 for oilHPR-EN-16 US EPA Method 3052HPR-EN-17 WastewaterHPR-EN-18 Wood chipsHPR-EN-19 Industrial wastewaterHPR-EN-20 BCR CRM 146 Sewage sludge _method 1HPR-EN-21 BCR CRM 146 Sewage sludge _method 2HPR-EN-22 BCS 300 soilHPR-EN-23 US EPA 3051HPR-EN-24 Green algaeHPR-EN-25 Mud 25% of OrganicHPR-EN-26 PET _plastic_ wasteHPR-EN-27 Plastic FilterHPR-EN-28 Raw wasteHPR-EN-29 River sedimentHPR-EN-30 Saw dustHPR-EN-31 Saw dust with oilHPR-EN-32 Saw dust with sludgeHPR-EN-33 Sea sedimentHPR-EN-34 Siliceous soil with organicHPR-EN-35 Sludge with 7% of oilHPR-EN-36 Urban dustHPR-EN-37 Urban wastewaterHPR-EN-38 Wastewater _method 2HPR-EN-39 Acid slagHPR-EN-40 Iron silicate slagHPR-EN-41 Manganese silicate slagHPR-EN-42 Copper slagHPR-EN-43 Soil and crude oilHPR-EN-44 Crude and Millipore filtersHPR-EN-45 Polyethersulfone filter
Application field: Food-FeedHPR-FO-01 HamHPR-FO-02 AgaroseHPR-FO-03 Baby foodHPR-FO-04 BCR 100 Beech LeavesHPR-FO-05 BCR 185 Bovine LiverHPR-FO-06 BCR 185 Bovine Liver less 1.5HPR-FO-07 BCR464 Tuna FishHPR-FO-08 Aquatic PlantHPR-FO-09 Bovine MilkHPR-FO-10 Calcium Alginate from SEHPR-FO-11 CaseinHPR-FO-12 Cheese ashesHPR-FO-13 Chewing gumHPR-FO-14 Chocolate
HPR-FO-15 Cocoa powderHPR-FO-16 Corn StarchHPR-FO-17 Dried FishHPR-FO-18 Dry infant formulaHPR-FO-19 Feed for fishHPR-FO-20 Fish in oilHPR-FO-21 Fresh kidneyHPR-FO-22 Fresh liverHPR-FO-23 GlycerineHPR-FO-24 GrapesHPR-FO-25 LecithinHPR-FO-26 Lyophilized meatHPR-FO-27 Margarine.pdfHPR-FO-28 Milk powder _1HPR-FO-29 Milk powder _2HPR-FO-30 Mint OilHPR-FO-31 MonoglicerideHPR-FO-32 MushroomHPR-FO-33 NoodlesHPR-FO-34 OlivesHPR-FO-35 Oyster tissueHPR-FO-36 Palm OilHPR-FO-37 Pet foodHPR-FO-38 Raw sugarHPR-FO-39 Reconst infant formulaHPR-FO-40 Rice flourHPR-FO-41 SalamiHPR-FO-42 Sheep MilkHPR-FO-43 Soya FatHPR-FO-44 Soya OilHPR-FO-45 SoybeanHPR-FO-46 Sunflowe seedsHPR-FO-47 Tea LeavesHPR-FO-48 Tinned beefHPR-FO-49 Tinned Pork.HPR-FO-50 Tuna Fish in OilHPR-FO-51 Vegetable oilHPR-FO-52 Wheat flourHPR-FO-53 Tobacco leavesHPR-FO-54 FertilizerHPR-FO-55 LichenHPR-FO-56 BarleyHPR-FO-57 HopHPR-FO-58 GrassHPR-FO-59 Grape LeavesHPR-FO-60 Dried GraminaceeHPR-FO-61 Roasted PeanutsHPR-FO-62 SpinachesHPR-FO-63 TomatoesHPR-FO-64 WineHPR-FO-65 CoffeeHPR-FO-66 ButterHPR-FO-67 Fresh Meat
Application Book
HPR-FO-68 SaladHPR-FO-69 VinegardHPR-FO-70 YeastHPR-FO-71 Corn FlakesHPR-FO-72 Whole wheat grainHPR-FO-73 Honey
Application field: GeochemistryHPR-GE-01 Cement clinkerHPR-GE-02 General procedure for cement _method 1HPR-GE-03 General procedure for cement _method 2HPR-GE-04 LimestoneHPR-GE-05 Red clayHPR-GE-06 Quartz sandHPR-GE-07 Raw mix for cementHPR-GE-08 Slag from cement planHPR-GE-09 EmaniteHPR-GE-10 OliviniteHPR-GE-11 Nickel oreHPR-GE-12 Iron oreHPR-GE-13 Alluminium oxideHPR-GE-14 Alluminium silicateHPR-GE-15 Gypsum CaSO4HPR-GE-16 IlmeniteHPR-GE-17 Zinc OxideHPR-GE-18 Silicon and Tungsten oreHPR-GE-19 White pumiceHPR-GE-20 SilicaHPR-GE-21 Phosphatic rockHPR-GE-22 Feldsphatic rockHPR-GE-23 Cu2OHPR-GE-24 SnOHPR-GE-25 Aluminum hidroxideHPR-GE-26 Italian iron oreHPR-GE-27 CryoliteHPR-GE-28 Berillium oxideHPR-GE-29 Ferrous sulphatHPR-GE-30 Zn and Pb oxidesHPR-GE-31 Cobalt oxideHPR-GE-32 Hydrate magnesium silicaHPR-GE-33 Mica or biotiteHPR-GE-34 Titanium bioxideHPR-GE-35 QuartzHPR-GE-36 CorendumHPR-GE-37 SilmaniteHPR-GE-38 WC 73%, Cr2O2 20%, Ni 7%HPR-GE-39 Iron ore low silicateHPR-GE-40 Iron ore high silicatesHPR-GE-41 BauxiteHPR-GE-42 Fe2O3, SiO2, TiO2HPR-GE-43 ChromiteHPR-GE-44 Copper sulfideHPR-GE-45 Copper oreHPR-GE-46 Copper concentrate _method 1HPR-GE-47 Copper concentrate _method 2
HPR-GE-48 Calcium fluorideHPR-GE-49 Lead sulphateHPR-GE-50 Zr oreHPR-GE-51 Glass PowderHPR-GE-52 Chromite oresHPR-GE-53 SandHPR-GE-54 PyriteHPR-GE-55 Cr2O3HPR-GE-57 Molybdem oxideHPR-GE-58 GraniteHPR-GE-59 GabbroHPR-GE-60 SyeniteHPR-GE-61 DuniteHPR-GE-62 Magnesium alloyHPR-GE-63 Alumino cementHPR-GE-64 Slags Fe-MnHPR-GE-65 Fe concentrateHPR-GE-66 Cristalline Cr2O3HPR-GE-67 FeBHPR-GE-68 FePHPR-GE-69 Coke slagsHPR-GE-70 BasalteHPR-GE-71 Fly ash from cement planHPR-GE-72 Borosilicate glass fiberHPR-GE-73 Magnesium peroxideHPR-GE-74 Magnesium oxideHPR-GE-75 Mix of W, Co, Ni, Ti oxideHPR-GE-76 SilicaHPR-GE-77 Quartz _method 1HPR-GE-78 Quartz _method 2HPR-GE-79 TalcHPR-GE-80 TantaliteHPR-GE-81 HfO2HPR-GE-82 Fluorite
Application field: Metals, AlloysHPR-ME-01 Fe MnHPR-ME-02 SteelHPR-ME-03 Titanium scrapsHPR-ME-04 BrassHPR-ME-05 NBS 168 high temperatureHPR-ME-06 Si and Cr alloyHPR-ME-07 NBS 321 stainless steelHPR-ME-08 FeSiHPR-ME-09 Fe, V, Zr alloyHPR-ME-10 Ag, Au, Pd and Pt alloyHPR-ME-11 Cu and Cr alloHPR-ME-12 Ni and Cr alloyHPR-ME-13 Steel plant dustHPR-ME-14 Si, Cu, and C alloyHPR-ME-15 Steel for toolsHPR-ME-16 White cast ironHPR-ME-17 Inconel 600HPR-ME-18 Inconel 625HPR-ME-19 Inconel 718
The following application notes are suitable only for the configuration described in each notes.
Application Book
HPR-ME-20 SiliconHPR-ME-21 BCS 341 cast ironHPR-ME-22 High C, Cr alloyHPR-ME-23 Co and Ni alloyHPR-ME-24 FeCr high carbonHPR-ME-25 FeVHPR-ME-26 FeMoHPR-ME-27 Metal needlesHPR-ME-28 Cr, Co, Ni alloyHPR-ME-29 Pd and Sn alloyHPR-ME-30 Steel axlesHPR-ME-31 Noble metals residueHPR-ME-32 SeleniumHPR-ME-33 NBS 173b Titanium base alloyHPR-ME-34 NBS 134a Mo, W, Cr, V steelHPR-ME-35 Nickel-Chromium alloyHPR-ME-36 Alloy Ti 90%, Al 6%, V 4%HPR-ME-37 Cadmium tungstateHPR-ME-38 Cast ironHPR-ME-39 CopperHPR-ME-40 FerrochromHPR-ME-41 HastalloyHPR-ME-42 High alloyed steelHPR-ME-43 Lead for car batteriesHPR-ME-44 Manganese-Iridium shavingsHPR-ME-45 Nickel based alloyHPR-ME-46 TungstenHPR-ME-47 Welding alloyHPR-ME-48 MolybdenumHPR-ME-49 Al-SiHPR-ME-50 Nickel
Application field: Petrochemical - EnergyHPR-PE-01 Atmospheric dustHPR-PE-02 Boiler ashesHPR-PE-03 CoalHPR-PE-04 Coal _Partial digestionHPR-PE-05 Coke ashesHPR-PE-06 Exhaust oilHPR-PE-07 Lub and hydraulic oilHPR-PE-08 Pit coalHPR-PE-09 Silicon oilHPR-PE-10 NaphthaHPR-PE-11 Used lubrificant oilHPR-PE-12 Crude oilHPR-PE-13 Lignite ashes
HPR-PE-14 Gums in mineral oilHPR-PE-15 CokHPR-PE-16 Diesel fuelHPR-PE-17 Hard pitch from coal tarHPR-PE-18 NIST 1634b Fuel oilHPR-PE-19 Carbon black
Application field: Plastic-polymersHPR-PL-01 AcrylobushystyreneHPR-PL-02 AcrylonitrileHPR-PL-03 ButadieneHPR-PL-04 Ethylene vinyl alcoholHPR-PL-05 Polyacryl acidHPR-PL-06 Plyammide granulateHPR-PL-07 PolyesterHPR-PL-08 Polyesther granulateHPR-PL-09 Polyethylene - rubber separatorHPR-PL-10 PVC Sn stabilizedHPR-PL-11 WaxHPR-PL-12 Silicon oil
Basic Method Optimization
The following guidelines will help the operator to adapt and optimize (if required) the basic methods to the specific problems:
POOR DIGESTION QUALITY
� Increase T1 of the two last program Steps in 10°C increments.
� Extend Time of the last step.
� Reduce weight and / or increase quantity of chemicals / concentration of acids.
� Optimize acid mixtures particularly with inorganic samples.
� Use stirrer.
� With good quality of digestion, the last program step can be reduced
Q/P-SENSOR ACTIVE EARLIER THAN EXPECTED
� Replace possible defective parts (vessel / cover, etc.).
� Reduce sample weights to generate smaller quantities of gas.
� Extend heating steps 1 and 2 (Temperature increase / flatter gradients).
� Reduce the Temperatures.
� Addo one, two ml of water in the acid mixture.
� Reduce HCl portion for digestions with HNO3 / HCl.
� With good quality of digestion, the last step can be reduced.
� If very high temperatures are reached, add high boiling acids.
� Check this cookbook before run a new sample.
T1-WISHED TEMPERATURE IS NOT REACHED
� Extend the heating steps accordingly.
� Increase the microwave power emissions.
� Total solvent quantity is too small – Caution with power increase.
� Use vessels for small sample quantities.
For additional application information, please contact the Milestone Customer
Support at +39 035 57 38 57, e-mail:
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-AG-01
Pine Leaves
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-AG-02
Dried Plant Tissue
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-AG-03
Ground Vegetable
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-AG-04
Maize
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-AG-05
Hay
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-AG-06
Lentis
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-AG-07
Roots
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-AG-08
Tea Leaves
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-01
Paint Residues
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-01
Paint Residues
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-02
Paint Pigment
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-03
Pd on Allumina Base (partial digestion)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-04
Organo - Metallic Pigment
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-05
Cu and Mo on Allumina Base
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-06
Ink
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-07
High Added Dry Paints
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-08
Catalyst Al-Cr-Fe-Ni
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-09
V and Mo on Oxide Base
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-10
Pt and Rh on Refractories (partial digestion)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-11
Green Organic Pigment
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-12
Red Organic Pigment
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-13
Black Tattoo Ink
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-14
Red Tattoo Ink
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CA-15
Cosmetic Components
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-01
Al203 and TiO2 Mixture
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-02
Al2O3 Sintered at 1800°C
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-03
Alluminous Refractary
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-03
Alluminous Refractary
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-04
Alumina 90%
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-05
BCS 315 Refractory Brick
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-06
Car Catalyst Al2O3 60%, Ce 20%, Zr 10%
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-06
Car Catalyst Al2O3 60%, Ce 20%, Zr 10%
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-07
Catalyst TiO2 80%, WO3 8%, V2O5 3%
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-08
Cement
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-09
ENAMEL SiO2 55-60%,TiO2 5-10%,B2O3 5-10%
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-10
FRIT CERAMIC
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-11
GAMMA ALLUMINA 90%
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-12
GLASS FIBER BOROSILICATE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-13
Zirconia
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-14
IRON OXIDE TREATED
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-15
PbO 68% ZrO2 22% TiO2 10%
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-16
PRIMARY ALUMINA
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-17
QUARTZ
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-18
REFRACTORY BRICK
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-19
REFRACTORY BRICK Al2O3 35%
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-20
TiO2 95% V2O5 5%
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-20
TiO2 95% V2O5 5%
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-21
SiO2/Al2O3 REFRACTORY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-22
SRM 1412 GLASS SiO2 40-45%,Al2O3 5-10%
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CE-23
Zirconium Oxide
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-01
MONTANA WAX
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-02
ACID RESIN
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-03
DISTERGLAMIN
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-04
UREA
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-05
ACTIVATED CARBON 90%
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-06
GELATIN VEGETABLE BASE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-07
COMMERCIAL PAPER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-08
POLAROID KM-653 MODIFIER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-08
POLAROID KM-653 MODIFIER
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-09
FERROUS CHLORIDE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-10
LITHIUM GREASE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-10
LITHIUM GREASE
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-11
ADIPIC ACID
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-12
HAND SOAP
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-13
ADOGENE-442
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-14
HEQ
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-15
PAPER PULP
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-16
GREASE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-17
STEARIC ACID
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-18
ISOPHTALIC ACID
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-19
CaHPO4
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CH-20
ACETIC ACID
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-01
CFX-PC REVICON
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-02
ANIMAL TISSUE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-03
BLOOD
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-04
COSMETIC COMPONENTS
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-05
DIMETHYLAGOXINE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-06
FINE CELLULOSE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-07
GARLIC OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-08
GLICERINE STEARATE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-09
GRANULAR SACCHAROSE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-10
HAIR
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-11
ICING SACCHAROSE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-12
LACTOSE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-13
LYOPHILIZED ORANGE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-14
MAGNESIUM STEARATE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-15
MANNITOL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-16
METHYLVIOLET B
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-17
NBS 1577B BOVINE LIVER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-18
PD-01 IMPROVED REVICON
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-19
PECTIN
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-20
RED COLOUR FOR TABLETS
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-21
SUPPOSITORY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-22
TETRACYCLINE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-23
URINE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-24
WAXOLINE ORANGE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-CL-25
TOOTH PASTE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-01
ASHES OF POLLUTED OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-02
CELLULOSE ESTER FILTER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-03
DRIED BIOLOGICAL SLUDGE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-04
FLY ASH
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-05
GRASS
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-06
LEAVES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-07
MUNICIPAL SLUDGE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-08
MUNICIPAL WASTE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-09
NIST SRM 2781 DRIED DOMESTIC SLUDGE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-10
POLLEN
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-11
SLUDGE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-12
SOIL PARTIAL DIGESTION
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-13
SOIL TOTAL DIGESTION
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-14
US EPA METHOD 3015
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-15
US EPA METHOD 3051 for OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-16
US EPA METHOD 3052
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-17
WASTEWATER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-18
WOOD CHIPS
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-19
INDUSTRIAL WASTEWATER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
-Rev 05_11-
Application Note HPR-EN-20
BCR CRM 146 Sewage Sludge BCR CRM 146 Sewage Sludge BCR CRM 146 Sewage Sludge BCR CRM 146 Sewage Sludge ((((Method Method Method Method 1)1)1)1)
SummarySummarySummarySummary
This method provides the acid digestion of the
sample in a closed vessel device using
temperature control microwave heating for the
metal determination by spectroscopic methods.
InstrumentationInstrumentationInstrumentationInstrumentation
Microwave acid digestion apparatus
Milestone Ethos or Start labstation with internal
temperature sensor, 640-260 terminal with
easyCONTROL software installed and
HPR1000/10S high pressure segmented rotor.
Sample weightSample weightSample weightSample weight
Up to 0.25 g
ReagentsReagentsReagentsReagents
7 ml of HNO3 65%, 1 ml of HClO4 65%.
ProcedureProcedureProcedureProcedure
1. Place a TFM vessel on the balance plate, tare
it and weigh of the sample.
2. Introduce the TFM vessel into the HTC safety
shield.
3. Add the acids; if part of the sample stays on
the inner wall of the TFM vessel, wet it by
adding acids drop by drop, then gently swirl
the solution to homogenize the sample with
the acids.
4. Close the vessel and introduce it into the rotor
segment, then tighten by using the torque
wrench.
5. Insert the segment into the microwave cavity
and connect the temperature sensor.
6. Run the microwave program to completion.
7. Cool the rotor by air or by water until the
solution reaches room temperature.
8. Open the vessel and transfer the solution to a
marked flask.
Microwave programMicrowave programMicrowave programMicrowave program
Step Time T1 T2 (1)
P (2)
Power
1 00:15:00 200°C 110°C 45 bar Max power*
2 00:15:00 200°C 110°C 45 bar Max power*
(1), (2) Optional sensors
Temperature profileTemperature profileTemperature profileTemperature profile
NoteNoteNoteNote
*Max power: 1500W for Ethos and 1200W for Start units.
Use up to 500 Watt for operations with 3 or less vessels
simultaneously.
This procedure is only a guideline and it may need to be
modified or changed to obtain the required results on your
sample.
Milestone suggest to use pressure sensor (P) only for
method developments or unknown samples. See the
pressure sensor user manual for more information.
Always use hand, eye and body protection when operating
with the microwave system.
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-20
BCR CRM 146 Sewage Sludge (Method 1)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
-Rev 05_11-
Application Note HPR-EN-21
BCR CRM 146 Sewage Sludge BCR CRM 146 Sewage Sludge BCR CRM 146 Sewage Sludge BCR CRM 146 Sewage Sludge ((((Method 2Method 2Method 2Method 2))))
SummarySummarySummarySummary
This method provides the acid digestion of the
sample in a closed vessel device using
temperature control microwave heating for the
metal determination by spectroscopic methods.
InstrumentationInstrumentationInstrumentationInstrumentation
Microwave acid digestion apparatus
Milestone Ethos or Start labstation with internal
temperature sensor, 640-260 terminal with
easyCONTROL software installed and
HPR1000/10S high pressure segmented rotor.
Sample weightSample weightSample weightSample weight
Up to 0.25 g
ReagentsReagentsReagentsReagents
7 ml of HNO3 65%, 1 ml of HClO4 65%.
ProcedureProcedureProcedureProcedure
1. Place a TFM vessel on the balance plate, tare
it and weigh of the sample.
2. Introduce the TFM vessel into the HTC safety
shield.
3. Add the acids; if part of the sample stays on
the inner wall of the TFM vessel, wet it by
adding acids drop by drop, then gently swirl
the solution to homogenize the sample with
the acids.
4. Close the vessel and introduce it into the rotor
segment, then tighten by using the torque
wrench.
5. Insert the segment into the microwave cavity
and connect the temperature sensor.
6. Run the microwave program to completion.
7. Cool the rotor by air or by water until the
solution reaches room temperature.
8. Open the vessel and transfer the solution to a
marked flask.
Microwave programMicrowave programMicrowave programMicrowave program
Step Time T1 T2 (1)
P (2)
Power
1 00:20:00 220°C 120°C 45 bar Max power*
2 00:15:00 220°C 120°C 45 bar Max power*
(1), (2) Optional sensors
Temperature profileTemperature profileTemperature profileTemperature profile
NoteNoteNoteNote
*Max power: 1500W for Ethos and 1200W for Start units.
Use up to 500 Watt for operations with 3 or less vessels
simultaneously.
This procedure is only a guideline and it may need to be
modified or changed to obtain the required results on your
sample.
Milestone suggest to use pressure sensor (P) only for
method developments or unknown samples. See the
pressure sensor user manual for more information.
Always use hand, eye and body protection when operating
with the microwave system.
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-21
BCR CRM 146 Sewage Sludge (Method 2)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-22
BCS 300 SOIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-23
US EPA 3051
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-24
GREEN ALGAE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-25
MUD 25% OF ORGANIC
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
-Rev 05_11-
Application Note HPR-EN-26
PET (Plastic) WPET (Plastic) WPET (Plastic) WPET (Plastic) WASTEASTEASTEASTE
SummarySummarySummarySummary
This method provides the acid digestion of the
sample in a closed vessel device using
temperature control microwave heating for the
metal determination by spectroscopic methods.
InstrumentationInstrumentationInstrumentationInstrumentation
Microwave acid digestion apparatus
Milestone Ethos or Start labstation with internal
temperature sensor, 640-260 terminal with
easyCONTROL software installed and
HPR1000/10S high pressure segmented rotor.
Sample weightSample weightSample weightSample weight
Up to 0.25 g
ReagentsReagentsReagentsReagents
4 ml of H2SO4 98%, 5 ml of HNO3 65%,
3 ml of HBF4 40%.
ProcedureProcedureProcedureProcedure
1. Place a TFM vessel on the balance plate, tare
it and weigh of the sample.
2. Introduce the TFM vessel into the HTC safety
shield.
3. Add the acids; if part of the sample stays on
the inner wall of the TFM vessel, wet it by
adding acids drop by drop, then gently swirl
the solution to homogenize the sample with
the acids.
4. Close the vessel and introduce it into the rotor
segment, then tighten by using the torque
wrench.
5. Insert the segment into the microwave cavity
and connect the temperature sensor.
6. Run the microwave program to completion.
7. Cool the rotor by air or by water until the
solution reaches room temperature.
8. Open the vessel and transfer the solution to a
marked flask.
Microwave programMicrowave programMicrowave programMicrowave program
Step Time T1 T2 (1)
P (2)
Power
1 00:20:00 220°C 120°C 45 bar Max power*
2 00:15:00 220°C 120°C 45 bar Max power*
(1), (2) Optional sensors
Temperature profileTemperature profileTemperature profileTemperature profile
NoteNoteNoteNote
*Max power: 1500W for Ethos and 1200W for Start units.
Use up to 500 Watt for operations with 3 or less vessels
simultaneously.
This procedure is only a guideline and it may need to be
modified or changed to obtain the required results on your
sample.
Milestone suggest to use pressure sensor (P) only for
method developments or unknown samples. See the
pressure sensor user manual for more information.
Always use hand, eye and body protection when operating
with the microwave system.
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-26
PET (Plastic) WASTE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-27
PLASTIC FILTER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-28
RAW WASTE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-29
RIVER SEDIMENT
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-29
RIVER SEDIMENT
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-30
SAW DUST
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-31
SAW DUST WITH OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-32
SAW DUST WITH SLUDGE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-33
SEA SEDIMENT
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-34
SILICEOUS SOIL ORGANIC
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-35
SLUDGE WITH 7% OF OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-36
URBAN DUST
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-37
URBAN WASTEWATER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
-Rev 05_10-
Application Note HPR-EN-38
WWWWASTEWATERASTEWATERASTEWATERASTEWATER (Method(Method(Method(Method 2) 2) 2) 2)
SummarySummarySummarySummary
This method provides the acid digestion of the
sample in a closed vessel device using
temperature control microwave heating for the
metal determination by spectroscopic methods.
InstrumentationInstrumentationInstrumentationInstrumentation
Microwave acid digestion apparatus
Milestone Ethos or Start labstation with internal
temperature sensor, 640-260 terminal with
easyCONTROL software installed and
HPR1000/10S high pressure segmented rotor.
Sample weightSample weightSample weightSample weight
Up to 5 g
ReagentsReagentsReagentsReagents
8 ml of HNO3 65%, 3 ml of HCl 37%,
0.25 ml of H2O2 30%.
ProcedureProcedureProcedureProcedure
1. Place a TFM vessel on the balance plate, tare
it and weigh of the sample.
2. Introduce the TFM vessel into the HTC safety
shield.
3. Add the acids; if part of the sample stays on
the inner wall of the TFM vessel, wet it by
adding acids drop by drop, then gently swirl
the solution to homogenize the sample with
the acids.
4. Close the vessel and introduce it into the rotor
segment, then tighten by using the torque
wrench.
5. Insert the segment into the microwave cavity
and connect the temperature sensor.
6. Run the microwave program to completion.
7. Cool the rotor by air or by water until the
solution reaches room temperature.
8. Open the vessel and transfer the solution to a
marked flask.
Microwave programMicrowave programMicrowave programMicrowave program
Step Time T1 T2 (1)
P (2)
Power
1 00:15:00 200°C 110°C 45 bar Max power*
2 00:15:00 200°C 110°C 45 bar Max power*
(1), (2) Optional sensors
Temperature profileTemperature profileTemperature profileTemperature profile
NoteNoteNoteNote
*Max power: 1500W for Ethos and 1200W for Start units.
Use up to 500 Watt for operations with 3 or less vessels
simultaneously.
This procedure is only a guideline and it may need to be
modified or changed to obtain the required results on your
sample.
Milestone suggest to use pressure sensor (P) only for
method developments or unknown samples. See the
pressure sensor user manual for more information.
Always use hand, eye and body protection when operating
with the microwave system.
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-38
WASTEWATER (Method 2)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-39
ACID SLAG
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-40
IRON SILICATE SLAG
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-41
MANGANESE SILICATE SLAG
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-42
COPPER SLAG
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-43
SOIL AND CRUDE OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-44
Filter CRUDE or Millipore (47mm)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-45
POLYETHERSULFONE FILTER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-EN-45
POLYETHERSULFONE FILTER
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-01
HAM
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-02
AGAROSE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-03
BABY FOOD
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-04
BCR 100 BEECH LEAVES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-05
BCR 185 BOVINE LIVER (< 1 g)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
-Rev 05_11-
Application Note HPR-FO-06
BCR 185 BOVINE LIVER (< 0.5 g)BCR 185 BOVINE LIVER (< 0.5 g)BCR 185 BOVINE LIVER (< 0.5 g)BCR 185 BOVINE LIVER (< 0.5 g)
SummarySummarySummarySummary
This method provides the acid digestion of the
sample in a closed vessel device using
temperature control microwave heating for the
metal determination by spectroscopic methods.
InstrumentationInstrumentationInstrumentationInstrumentation
Microwave acid digestion apparatus
Milestone Ethos or Start labstation with internal
temperature sensor, 640-260 terminal with
easyCONTROL software installed and
HPR1000/10S high pressure segmented rotor.
Sample weightSample weightSample weightSample weight
Up to 0.5 g
ReagentsReagentsReagentsReagents
10 ml of HNO3 65%.
ProcedureProcedureProcedureProcedure
1. Place a TFM vessel on the balance plate, tare
it and weigh of the sample.
2. Introduce the TFM vessel into the HTC safety
shield.
3. Add the acids; if part of the sample stays on
the inner wall of the TFM vessel, wet it by
adding acids drop by drop, then gently swirl
the solution to homogenize the sample with
the acids.
4. Close the vessel and introduce it into the rotor
segment, then tighten by using the torque
wrench.
5. Insert the segment into the microwave cavity
and connect the temperature sensor.
6. Run the microwave program to completion.
7. Cool the rotor by air or by water until the
solution reaches room temperature.
8. Open the vessel and transfer the solution to a
marked flask.
Microwave programMicrowave programMicrowave programMicrowave program
Step Time T1 T2 (1)
P (2)
Power
1 00:10:00 180°C 100°C 45 bar Max power*
2 00:15:00 180°C 100°C 45 bar Max power*
(1), (2) Optional sensors
Temperature profileTemperature profileTemperature profileTemperature profile
NoteNoteNoteNote
*Max power: 1500W for Ethos and 1200W for Start units.
Use up to 500 Watt for operations with 3 or less vessels
simultaneously.
This procedure is only a guideline and it may need to be
modified or changed to obtain the required results on your
sample.
Milestone suggest to use pressure sensor (P) only for
method developments or unknown samples. See the
pressure sensor user manual for more information.
Always use hand, eye and body protection when operating
with the microwave system.
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-06
BCR 185 BOVINE LIVER (< 0.5 g)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-07
BCR 464 TUNA FISH
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-08
AQUATIC PLANT
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-09
BOVINE MILK
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-10
CALCIUM ALGINATE FROM SE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-11
CASEIN
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-12
CHEESE ASHES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-13
CHEWING GUM
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-14
CHOCOLATE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-15
COCOA POWDER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-16
CORN STARCH
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-17
DRIED FISH
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-18
DRY INFANT FORMULA
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-19
FEED FOR FISH
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-20
FISH IN OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-21
FRESH KIDNEY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-22
FRESH LIVER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-23
GLICERINE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-23
GLICERINE
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-24
GRAPES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-25
LECITHIN
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-26
LYOPHILIZED MEAT
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-27
MARGARINE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
-Rev 05_11-
Application Note HPR-FO-28
MILK POWDERMILK POWDERMILK POWDERMILK POWDER
SummarySummarySummarySummary
This method provides the acid digestion of the
sample in a closed vessel device using
temperature control microwave heating for the
metal determination by spectroscopic methods.
InstrumentationInstrumentationInstrumentationInstrumentation
Microwave acid digestion apparatus
Milestone Ethos or Start labstation with internal
temperature sensor, 640-260 terminal with
easyCONTROL software installed and
HPR1000/10S high pressure segmented rotor.
Sample weightSample weightSample weightSample weight
Up to 1.5 g
ReagentsReagentsReagentsReagents
12 ml of HNO3 65%.
ProcedureProcedureProcedureProcedure
1. Place a TFM vessel on the balance plate, tare
it and weigh of the sample.
2. Introduce the TFM vessel into the HTC safety
shield.
3. Add the acids; if part of the sample stays on
the inner wall of the TFM vessel, wet it by
adding acids drop by drop, then gently swirl
the solution to homogenize the sample with
the acids.
4. Close the vessel and introduce it into the rotor
segment, then tighten by using the torque
wrench.
5. Insert the segment into the microwave cavity
and connect the temperature sensor.
6. Run the microwave program to completion.
7. Cool the rotor by air or by water until the
solution reaches room temperature.
8. Open the vessel and transfer the solution to a
marked flask.
Microwave programMicrowave programMicrowave programMicrowave program
Step Time T1 T2 (1)
P (2)
Power
1 00:10:00 180°C 100°C 45 bar Max power*
2 00:15:00 180°C 100°C 45 bar Max power*
(1), (2) Optional sensors
Temperature profileTemperature profileTemperature profileTemperature profile
NoteNoteNoteNote
*Max power: 1500W for Ethos and 1200W for Start units.
Use up to 500 Watt for operations with 3 or less vessels
simultaneously.
This procedure is only a guideline and it may need to be
modified or changed to obtain the required results on your
sample.
Milestone suggest to use pressure sensor (P) only for
method developments or unknown samples. See the
pressure sensor user manual for more information.
Always use hand, eye and body protection when operating
with the microwave system.
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-28
MILK POWDER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
-Rev 05_11-
Application Note HPR-FO-29
MILK POWDERMILK POWDERMILK POWDERMILK POWDER
SummarySummarySummarySummary
This method provides the acid digestion of the
sample in a closed vessel device using
temperature control microwave heating for the
metal determination by spectroscopic methods.
InstrumentationInstrumentationInstrumentationInstrumentation
Microwave acid digestion apparatus
Milestone Ethos or Start labstation with internal
temperature sensor, 640-260 terminal with
easyCONTROL software installed and
HPR1000/10S high pressure segmented rotor.
Sample weightSample weightSample weightSample weight
Up to 0.5 g
ReagentsReagentsReagentsReagents
7 ml of HNO3 65%, 1 ml of H2O2 30%.
ProcedureProcedureProcedureProcedure
1. Place a TFM vessel on the balance plate, tare
it and weigh of the sample.
2. Introduce the TFM vessel into the HTC safety
shield.
3. Add the acids; if part of the sample stays on
the inner wall of the TFM vessel, wet it by
adding acids drop by drop, then gently swirl
the solution to homogenize the sample with
the acids.
4. Close the vessel and introduce it into the rotor
segment, then tighten by using the torque
wrench.
5. Insert the segment into the microwave cavity
and connect the temperature sensor.
6. Run the microwave program to completion.
7. Cool the rotor by air or by water until the
solution reaches room temperature.
8. Open the vessel and transfer the solution to a
marked flask.
Microwave programMicrowave programMicrowave programMicrowave program
Step Time T1 T2 (1)
P (2)
Power
1 00:10:00 180°C 100°C 45 bar Max power*
2 00:15:00 180°C 100°C 45 bar Max power*
(1), (2) Optional sensors
Temperature profileTemperature profileTemperature profileTemperature profile
NoteNoteNoteNote
*Max power: 1500W for Ethos and 1200W for Start units.
Use up to 500 Watt for operations with 3 or less vessels
simultaneously.
This procedure is only a guideline and it may need to be
modified or changed to obtain the required results on your
sample.
Milestone suggest to use pressure sensor (P) only for
method developments or unknown samples. See the
pressure sensor user manual for more information.
Always use hand, eye and body protection when operating
with the microwave system.
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-29
MILK POWDER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-30
MINT OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-31
MONOGLICERIDE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-32
MUSHROOM
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-33
NOODLES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-34
OLIVES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-35
OYSTER TISSUE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-36
PALM OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-37
PET FOOD
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-38
RAW SUGAR
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-39
RECONSTITUED INFANT FORMULA
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-40
RICE FLOUR
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-41
SALAMI
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-42
SHEEP MILK
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-43
SOYA FAT
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-44
SOYA OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-45
SOYBEAN
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-46
SUNFLOWER SEEDS
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-47
TEA LEAVES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-48
TINNED BEEF
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-49
TINNED PORK
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-50
TUNA FISH IN OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-51
VEGETABLE OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-52
WHEAT FLOUR
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-53
TOBACCO LEAVES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-54
FERTILIZER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-55
LICHEN
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-56
BARLEY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-57
HOP
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-58
GRASS
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-59
GRAPE LEAVES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-60
DRIED GRAMINACEE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-61
ROASTED PEANUTS
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-62
SINACHES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-63
TOMATOES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-64
WINE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-65
COFFEE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-66
BUTTER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-67
FRESH MEAT
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-68
SALAD
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-69
VINEGARD
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-70
YEAST
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-71
CORN FLAKES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-72
WHOLE WHEAT GRAIN
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-FO-73
HONEY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
CEMENT CLINKER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
-Rev 05_11-
Application Note HPR-GE-02
METHOD FORMETHOD FORMETHOD FORMETHOD FOR CEMENT 1 CEMENT 1 CEMENT 1 CEMENT 1
SummarySummarySummarySummary
This method provides the acid digestion of the
sample in a closed vessel device using
temperature control microwave heating for the
metal determination by spectroscopic methods.
InstrumentationInstrumentationInstrumentationInstrumentation
Microwave acid digestion apparatus
Milestone Ethos or Start labstation with internal
temperature sensor, 640-260 terminal with
easyCONTROL software installed and
HPR1000/10S high pressure segmented rotor.
Sample weightSample weightSample weightSample weight
Up to 0.1 g
ReagentsReagentsReagentsReagents
2ml of HNO3 65%, 6ml of HCl 37%,
1ml of H3PO4 85%, 1.5ml HBF4 50%
ProcedureProcedureProcedureProcedure
1. Place a TFM vessel on the balance plate, tare
it and weigh of the sample.
2. Introduce the TFM vessel into the HTC safety
shield.
3. Add the acids; if part of the sample stays on
the inner wall of the TFM vessel, wet it by
adding acids drop by drop, then gently swirl
the solution to homogenize the sample with
the acids.
4. Close the vessel and introduce it into the rotor
segment, then tighten by using the torque
wrench.
5. Insert the segment into the microwave cavity
and connect the temperature sensor.
6. Run the microwave program to completion.
7. Cool the rotor by air or by water until the
solution reaches room temperature.
8. Open the vessel and transfer the solution to a
marked flask.
Microwave programMicrowave programMicrowave programMicrowave program
Step Time T1 T2 (1)
P (2)
Power
1 00:20:00 230°C 125°C 45 bar Max power*
2 00:15:00 230°C 125°C 45 bar Max power*
(1), (2) Optional sensors
Temperature profileTemperature profileTemperature profileTemperature profile
NoteNoteNoteNote
*Max power: 1500W for Ethos and 1200W for Start units.
Use up to 500 Watt for operations with 3 or less vessels
simultaneously.
This procedure is only a guideline and it may need to be
modified or changed to obtain the required results on your
sample.
Milestone suggest to use pressure sensor (P) only for
method developments or unknown samples. See the
pressure sensor user manual for more information.
Always use hand, eye and body protection when operating
with the microwave system.
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-02
METHOD FOR CEMENT 1
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
-Rev 05_11-
Application Note HPR-GE-03
METHODMETHODMETHODMETHOD FOR C FOR C FOR C FOR CEMENT 2EMENT 2EMENT 2EMENT 2
SummarySummarySummarySummary
This method provides the acid digestion of the
sample in a closed vessel device using
temperature control microwave heating for the
metal determination by spectroscopic methods.
InstrumentationInstrumentationInstrumentationInstrumentation
Microwave acid digestion apparatus
Milestone Ethos or Start labstation with internal
temperature sensor, 640-260 terminal with
easyCONTROL software installed and
HPR1000/10S high pressure segmented rotor.
Sample weightSample weightSample weightSample weight
Up to 0.1 g
ReagentsReagentsReagentsReagents
2ml of HNO3 65%, 2ml of HCl 37%,
3ml of H3PO4 85%, 3ml HBF4 50%
ProcedureProcedureProcedureProcedure
1. Place a TFM vessel on the balance plate, tare
it and weigh of the sample.
2. Introduce the TFM vessel into the HTC safety
shield.
3. Add the acids; if part of the sample stays on
the inner wall of the TFM vessel, wet it by
adding acids drop by drop, then gently swirl
the solution to homogenize the sample with
the acids.
4. Close the vessel and introduce it into the rotor
segment, then tighten by using the torque
wrench.
5. Insert the segment into the microwave cavity
and connect the temperature sensor.
6. Run the microwave program to completion.
7. Cool the rotor by air or by water until the
solution reaches room temperature.
8. Open the vessel and transfer the solution to a
marked flask.
Microwave programMicrowave programMicrowave programMicrowave program
Step Time T1 T2 (1)
P (2)
Power
1 00:20:00 230°C 125°C 45 bar Max power*
2 00:10:00 230°C 125°C 45 bar Max power*
(1), (2) Optional sensors
Temperature profileTemperature profileTemperature profileTemperature profile
NoteNoteNoteNote
*Max power: 1500W for Ethos and 1200W for Start units.
Use up to 500 Watt for operations with 3 or less vessels
simultaneously.
This procedure is only a guideline and it may need to be
modified or changed to obtain the required results on your
sample.
Milestone suggest to use pressure sensor (P) only for
method developments or unknown samples. See the
pressure sensor user manual for more information.
Always use hand, eye and body protection when operating
with the microwave system.
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-03
METHOD FOR CEMENT 2
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-04
LIMESTONE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-05
RED CLAY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-06
QUARTZ SAND
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-07
RAW MIX FOR CEMENT
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-08
SLAG FROM CEMENT PLAN
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-09
EMANITE (Fe Oxide)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-10
OLIVINITE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-11
NICKEL ORE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-12
IRON ORE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-13
ALLUMINIUM OXIDE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-14
ALLUMINIUM SILICATE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-15
GYPSUM CaSO4
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-16
ILMENITE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-17
ZINC OXIDE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-18
SILICON AND TUNGSTEN ORE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-19
WITHE PUMICE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-20
SILICA
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-21
PHOSPHATIC ROCK
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-22
FELDSPHATIC ROCK
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-23
Cu2O
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-24
SnO
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-25
ALUMINUM HIDROXIDE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-26
ITALIAN IRON ORE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-27
CRYOLITE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-28
BERYLLIUM OXIDE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-29
FERROUS SULPHATE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-30
Zn AND Pb OXIDES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-31
COBALT OXIDE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-32
HYDRATE MAGNESIUM SILICA
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-33
MICA OR BIOTITE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-34
TITANIUM BIOXIDE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-35
QUARTZ
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-36
CORENDUM
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-37
SILMANITE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-38
WC 73%, Cr2O3 20%, Ni 7%
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-39
IRON ORE LOW SILICATES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-40
IRON ORE HIGH SILICATES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-41
BAUXITE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-42
Fe2O3, SiO2, TiO2
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-43
CHROMITE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-44
COPPER SULFIDE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-45
COPPER ORE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
-Rev 05_11-
Application Note HPR-GE-46
COPPER COPPER COPPER COPPER CONCENTRATE CONCENTRATE CONCENTRATE CONCENTRATE (Metho(Metho(Metho(Method 1)d 1)d 1)d 1)
SummarySummarySummarySummary
This method provides the acid digestion of the
sample in a closed vessel device using
temperature control microwave heating for the
metal determination by spectroscopic methods.
InstrumentationInstrumentationInstrumentationInstrumentation
Microwave acid digestion apparatus
Milestone Ethos or Start labstation with internal
temperature sensor, 640-260 terminal with
easyCONTROL software installed and
HPR1000/10S high pressure segmented rotor.
Sample weightSample weightSample weightSample weight
Up to 0.25 g
ReagentsReagentsReagentsReagents
5 ml of HCl 37%, 2 ml of HNO3 65%,
2 ml of HF 40%
ProcedureProcedureProcedureProcedure
1. Place a TFM vessel on the balance plate, tare
it and weigh of the sample.
2. Introduce the TFM vessel into the HTC safety
shield.
3. Add the acids; if part of the sample stays on
the inner wall of the TFM vessel, wet it by
adding acids drop by drop, then gently swirl
the solution to homogenize the sample with
the acids.
4. Close the vessel and introduce it into the rotor
segment, then tighten by using the torque
wrench.
5. Insert the segment into the microwave cavity
and connect the temperature sensor.
6. Run the microwave program to completion.
7. Cool the rotor by air or by water until the
solution reaches room temperature.
8. Open the vessel and transfer the solution to a
marked flask.
Microwave programMicrowave programMicrowave programMicrowave program
Step Time T1 T2 (1)
P (2)
Power
1 00:20:00 220°C 120°C 45 bar Max power*
2 00:15:00 220°C 120°C 45 bar Max power*
(1), (2) Optional sensors
Temperature profileTemperature profileTemperature profileTemperature profile
NoteNoteNoteNote
*Max power: 1500W for Ethos and 1200W for Start units.
Use up to 500 Watt for operations with 3 or less vessels
simultaneously.
This procedure is only a guideline and it may need to be
modified or changed to obtain the required results on your
sample.
Milestone suggest to use pressure sensor (P) only for
method developments or unknown samples. See the
pressure sensor user manual for more information.
Always use hand, eye and body protection when operating
with the microwave system.
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-46
COPPER CONCENTRATE (Method 1)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
-Rev 05_11-
Application Note HPR-GE-47
COPPER COPPER COPPER COPPER CONCENTRATE CONCENTRATE CONCENTRATE CONCENTRATE (Me(Me(Me(Method 2thod 2thod 2thod 2))))
SummarySummarySummarySummary
This method provides the acid digestion of the
sample in a closed vessel device using
temperature control microwave heating for the
metal determination by spectroscopic methods.
InstrumentationInstrumentationInstrumentationInstrumentation
Microwave acid digestion apparatus
Milestone Ethos or Start labstation with internal
temperature sensor, 640-260 terminal with
easyCONTROL software installed and
HPR1000/10S high pressure segmented rotor.
Sample weightSample weightSample weightSample weight
Up to 0.1 g
ReagentsReagentsReagentsReagents
4 ml of HNO3 65%, 4 ml of HF 40%
ProcedureProcedureProcedureProcedure
1. Place a TFM vessel on the balance plate, tare
it and weigh of the sample.
2. Introduce the TFM vessel into the HTC safety
shield.
3. Add the acids; if part of the sample stays on
the inner wall of the TFM vessel, wet it by
adding acids drop by drop, then gently swirl
the solution to homogenize the sample with
the acids.
4. Close the vessel and introduce it into the rotor
segment, then tighten by using the torque
wrench.
5. Insert the segment into the microwave cavity
and connect the temperature sensor.
6. Run the microwave program to completion.
7. Cool the rotor by air or by water until the
solution reaches room temperature.
8. Open the vessel and transfer the solution to a
marked flask.
Microwave programMicrowave programMicrowave programMicrowave program
Step Time T1 T2 (1)
P (2)
Power
1 00:20:00 220°C 120°C 45 bar Max power*
2 00:15:00 220°C 120°C 45 bar Max power*
(1), (2) Optional sensors
Temperature profileTemperature profileTemperature profileTemperature profile
NoteNoteNoteNote
*Max power: 1500W for Ethos and 1200W for Start units.
Use up to 500 Watt for operations with 3 or less vessels
simultaneously.
This procedure is only a guideline and it may need to be
modified or changed to obtain the required results on your
sample.
Milestone suggest to use pressure sensor (P) only for
method developments or unknown samples. See the
pressure sensor user manual for more information.
Always use hand, eye and body protection when operating
with the microwave system.
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-47
COPPER CONCENTRATE (Method 2)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-48
CALCIUM FLUORITE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-49
LEAD SULPHATE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-49
LEAD SULPHATE
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-50
Zr ORE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-50
Zr ORE
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-51
GLASS POWDER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-52
CHROMITE ORES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-53
SAND
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-54
PYRITE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-55
Cr2O3
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-56
Fe2O3 AND Cr2O3 MIXTURE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-57
MOLYBDEM OXIDE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-58
GRANITE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-59
GABBRO
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-60
SYENITE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-61
DUNITE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-62
MAGNESIUM ALLOY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-63
ALUMINO CEMENT
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-64
SLAGS Fe-Mn
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-65
Fe concentrate (Fe 68%, FeO 27%, Si 5%, CaO, MgO, Al2O3
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-66
CRISTALLINE Cr2O3
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-67
FeB
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-68
FeP
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-69
COKE SLAGS (Fe>50%, 25<C<30%)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-70
BASALTE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-71
FLY ASH FROM CEMENT PLAN
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-72
BOROSILICATE GLASS FIBER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-73
MAGNESIUM PEROXIDE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-74
MAGNESIUM OXIDE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-75
MIXTURE OF W, Co, Ni, Ti OXIDE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-76
SILICA
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
-Rev 05_11-
Application Note HPR-GE-77
QUARTZ QUARTZ QUARTZ QUARTZ (Method 1(Method 1(Method 1(Method 1))))
SummarySummarySummarySummary
This method provides the acid digestion of the
sample in a closed vessel device using
temperature control microwave heating for the
metal determination by spectroscopic methods.
InstrumentationInstrumentationInstrumentationInstrumentation
Microwave acid digestion apparatus
Milestone Ethos or Start labstation with internal
temperature sensor, 640-260 terminal with
easyCONTROL software installed and
HPR1000/10S high pressure segmented rotor.
Sample weightSample weightSample weightSample weight
Up to 0.25 g
ReagentsReagentsReagentsReagents
6 ml of HF 40%, 2 ml of HNO3 67%
ProcedureProcedureProcedureProcedure
1. Place a TFM vessel on the balance plate, tare
it and weigh of the sample.
2. Introduce the TFM vessel into the HTC safety
shield.
3. Add the acids; if part of the sample stays on
the inner wall of the TFM vessel, wet it by
adding acids drop by drop, then gently swirl
the solution to homogenize the sample with
the acids.
4. Close the vessel and introduce it into the rotor
segment, then tighten by using the torque
wrench.
5. Insert the segment into the microwave cavity
and connect the temperature sensor.
6. Run the microwave program to completion.
7. Cool the rotor by air or by water until the
solution reaches room temperature.
8. Open the vessel and transfer the solution to a
marked flask.
Microwave programMicrowave programMicrowave programMicrowave program
Step Time T1 T2 (1)
P (2)
Power
1 00:20:00 220°C 120°C 45 bar Max power*
2 00:15:00 220°C 120°C 45 bar Max power*
(1), (2) Optional sensors
Temperature profileTemperature profileTemperature profileTemperature profile
NoteNoteNoteNote
*Max power: 1500W for Ethos and 1200W for Start units.
Use up to 500 Watt for operations with 3 or less vessels
simultaneously.
This procedure is only a guideline and it may need to be
modified or changed to obtain the required results on your
sample.
Milestone suggest to use pressure sensor (P) only for
method developments or unknown samples. See the
pressure sensor user manual for more information.
Always use hand, eye and body protection when operating
with the microwave system.
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-77
QUARTZ (Method 1)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
-Rev 05_11-
Application Note HPR-GE-78
QUARTZ QUARTZ QUARTZ QUARTZ (Method 1)(Method 1)(Method 1)(Method 1)
SummarySummarySummarySummary
This method provides the acid digestion of the
sample in a closed vessel device using
temperature control microwave heating for the
metal determination by spectroscopic methods.
InstrumentationInstrumentationInstrumentationInstrumentation
Microwave acid digestion apparatus
Milestone Ethos or Start labstation with internal
temperature sensor, 640-260 terminal with
easyCONTROL software installed and
HPR1000/10S high pressure segmented rotor.
Sample weightSample weightSample weightSample weight
Up to 0.25 g
ReagentsReagentsReagentsReagents
2ml of HNO3 65%, 2ml of HCl 37%,
6ml HBF 50%.
ProcedureProcedureProcedureProcedure
1. Place a TFM vessel on the balance plate, tare
it and weigh of the sample.
2. Introduce the TFM vessel into the HTC safety
shield.
3. Add the acids; if part of the sample stays on
the inner wall of the TFM vessel, wet it by
adding acids drop by drop, then gently swirl
the solution to homogenize the sample with
the acids.
4. Close the vessel and introduce it into the rotor
segment, then tighten by using the torque
wrench.
5. Insert the segment into the microwave cavity
and connect the temperature sensor.
6. Run the microwave program to completion.
7. Cool the rotor by air or by water until the
solution reaches room temperature.
8. Open the vessel and transfer the solution to a
marked flask.
Microwave programMicrowave programMicrowave programMicrowave program
Step Time T1 T2 (1)
P (2)
Power
1 00:20:00 220°C 120°C 45 bar Max power*
2 00:15:00 220°C 120°C 45 bar Max power*
(1), (2) Optional sensors
Temperature profileTemperature profileTemperature profileTemperature profile
NoteNoteNoteNote
*Max power: 1500W for Ethos and 1200W for Start units.
Use up to 500 Watt for operations with 3 or less vessels
simultaneously.
This procedure is only a guideline and it may need to be
modified or changed to obtain the required results on your
sample.
Milestone suggest to use pressure sensor (P) only for
method developments or unknown samples. See the
pressure sensor user manual for more information.
Always use hand, eye and body protection when operating
with the microwave system.
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-78
QUARTZ (Method 1)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-79
TALC
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-80
TANTALITE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-81
HfO2
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-GE-82
FLUORITE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-01
Fe - Mn
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-02
STEEL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-03
TITANIUM SCRAPS
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-04
BRASS
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-05
NBS 168 HIGH TEMPERATURE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-06
Si AND Cr ALLOY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-07
NBS 321 STAINLESS STEEL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-08
FeSi
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-09
Fe, V, Zr ALLOY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-10
Ag, Au, Pd and Pt alloy
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-11
Cu AND Cr ALLOY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-12
Ni AND Cr ALLOY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-13
STEEL PLANT DUST
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-14
Si, Cu, AND C ALLOY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-14
Si, Cu, AND C ALLOY
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-15
STEEL FOR TOOLS
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-16
WHITE CAST IRON
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-17
INCONEL 600
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-18
INCONEL 625
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-19
INCONEL 718
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-20
SILICON
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-21
BCS 341 CAST IRON
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-22
HIGH C, Cr ALLOY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-23
Co AND Ni ALLOY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-24
FeCr HIGH CARBON
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-25
FeV
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-26
FeMo
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-27
METAL NEEDLES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-28
Cr, Co, Ni ALLOY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-29
Pd AND Sn ALLOY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-30
STEEL AXLES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-31
NOBLE METALS RESIDUE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-31
NOBLE METALS RESIDUE
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-32
SELENIUM
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-33
NBS 173b TITANIUM BASE ALLOY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-34
NBS 134a Mo, W, Cr, V STEEL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-35
NICKEL - CHROMIUM ALLOY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-36
ALLOY Ti 90%, Al 6%, V 4%
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-37
CADMIUM TUNGSTATE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-38
CAST IRON
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-39
COPPER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-40
FERROCHROM
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-41
HASTALLOY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-42
HIGH ALLOYED STEEL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-43
LEAD FOR CAR BATTERIES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-44
MANGANESE – IRIDIUM SHAVINGS
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-45
NICKEL BASED ALLOY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-46
TUNGSTEN
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-47
WELDING ALLOY
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-48
MOLYBDENUM
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-49
Al-Si
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-ME-50
NICKEL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-01
ATMOSPHERIC DUST
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-02
BOILER DUST
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-03
COAL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-03
COAL
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
-Rev 05_11-
Application Note HPR-PE-04
COAL (Partial digCOAL (Partial digCOAL (Partial digCOAL (Partial digestion)estion)estion)estion)
SummarySummarySummarySummary
This method provides the acid digestion of the
sample in a closed vessel device using
temperature control microwave heating for the
metal determination by spectroscopic methods.
InstrumentationInstrumentationInstrumentationInstrumentation
Microwave acid digestion apparatus
Milestone Ethos or Start labstation with internal
temperature sensor, 640-260 terminal with
easyCONTROL software installed and
HPR1000/10S high pressure segmented rotor.
Sample weightSample weightSample weightSample weight
Up to 0.25 g
ReagentsReagentsReagentsReagents
3 ml oof HCl 37%, 3 ml of HF 40%,
9 ml of HNO3 65%.
ProcedureProcedureProcedureProcedure
1. Place a TFM vessel on the balance plate, tare
it and weigh of the sample.
2. Introduce the TFM vessel into the HTC safety
shield.
3. Add the acids; if part of the sample stays on
the inner wall of the TFM vessel, wet it by
adding acids drop by drop, then gently swirl
the solution to homogenize the sample with
the acids.
4. Close the vessel and introduce it into the rotor
segment, then tighten by using the torque
wrench.
5. Insert the segment into the microwave cavity
and connect the temperature sensor.
6. Run the microwave program to completion.
7. Cool the rotor by air or by water until the
solution reaches room temperature.
8. Open the vessel and transfer the solution to a
marked flask.
Microwave programMicrowave programMicrowave programMicrowave program
Step Time T1 T2 (1)
P (2)
Power
1 00:10:00 180°C 100°C 45 bar Max power*
2 00:15:00 180°C 100°C 45 bar Max power*
(1), (2) Optional sensors
Temperature profileTemperature profileTemperature profileTemperature profile
NoteNoteNoteNote
*Max power: 1500W for Ethos and 1200W for Start units.
Use up to 500 Watt for operations with 3 or less vessels
simultaneously.
This procedure is only a guideline and it may need to be
modified or changed to obtain the required results on your
sample.
Milestone suggest to use pressure sensor (P) only for
method developments or unknown samples. See the
pressure sensor user manual for more information.
Always use hand, eye and body protection when operating
with the microwave system.
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-04
COAL (Partial digestion)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-05
COKE ASHES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-06
EXHAUST OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-07
LUB AND HYDRAULIC OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-08
PIT COAL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-09
SILICON OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-10
NAPHTHA
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-11
USED LUBRIFICANT OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-12
CRUDE OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-13
LIGNITE ASHES
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-14
GUMS IN MINERAL OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-15
COKE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-16
DIESEL FUEL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-16
DIESEL FUEL
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-17
HARD PITCH FROM COAL TAR
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-17
HARD PITCH FROM COAL TAR
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-18
NIST 1634b FUEL OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PE-19
CARBON BLACK
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-01
ACRYLOBUSHYSTYRENE (ABS)
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-01
ACRYLOBUSHYSTYRENE (ABS)
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-02
ACRYLONITRILE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-03
BUTADIENE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-04
ETHYLENE VINYL ALCOHOL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-05
POLYACRYL ACID
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-06
POLYAMMIDE GRANULATE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-06
POLYAMMIDE GRANULATE
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-07
POLYESTER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-08
POLYESTHER GRANULATE
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-08
POLYESTHER GRANULATE
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-09
POLYESTER
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-10
PVC Sn STABILIZED
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-10
PVC Sn STABILIZED
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-11
WAX
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note
Milestone Srl – Helping Chemists www.milestonesrl.com [email protected]
Application Note HPR-PL-12
SILICON OIL
Summary
Instrumentation
Sample weight
Reagents
Procedure
Microwave program
Temperature profile
Note