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Sensible Solutions for Pesticide Extraction QuEChERS Products SPEX CertiPrep provides a complete solution to all your QuEChERS needs with a comprehensive set of Internal Standards for the QuEChERS analytical techniques (GC, GC/MS, LC/MS). QuEChERS Standards Meeting all your QuEChERS needs with general purpose kits suitable for removal of polar organic acids, some low to moderate levels of sugars and lipids. General purpose kits are available for US (AOAC Method 2007.01) and European Methods (EN Method 15662). QuEChERS Kits Part # Compound Solvent Conc (μg/mL) QuECR-PCB-18 PCB 18 Acetonitrile 50 QuECR-PCB-28 PCB 28 Acetonitrile 50 QuECR-PCB-52 PCB 52 Acetonitrile 50 QuECR-PCB-138 PCB 138 Acetonitrile 50 QuECR-PCB-153 PCB 153 Acetonitrile 50 QuECR-5190 triphenylmethane Acetonitrile 10 QuECR-3765 triphenylphosphate Acetonitrile 20 QuECR-AOAC-TTP triphenylphosphate Acetonitrile 2 QuECR-4381 tris-(dichloroisopropyl)phosphate Acetonitrile 50 Single Component Reference Standards Volume: 5 mL Method Part # Product Name Material Qty Centrifuge Tube Volume EN 15662 EN-CIT-50ML Citrate Buffered Extraction Tubes 4 g MgSO 4 ,1 g NaCl, 0.5 g sodium citric dibasic sesquihydrate, 1 g sodium citrate tribasic dihydrate 50 pk 15 mL w/50 mL Centrifuge tube EN-PSA-2ML PSA Dispersive SPE Clean-Up Tubes 25 mg PSA, 150 mg MgSO 4 100 pk 2 mL EN-PSA-15ML PSA Dispersive SPE Clean-Up Tubes 150 mg PSA, 900 mg MgSO 4 50 pk 15 mL AOAC 2007.01 AOAC-ACE-50ML Acetate Buffered Extraction Tubes 6 g MgSO 4 , 1.5 g sodium acetate 50 pk 15 mL w/50 mL Centrifuge tube AOAC-PSA-2ML PSA Dispersive SPE Clean-Up Tubes 50 mg PSA, 150 mg MgSO 4 100 pk 2 mL AOAC-PSA-15ML PSA Dispersive SPE Clean-Up Tubes 400 mg PSA, 1200 mg MgSO 4 50 pk 15 mL SPEXQ uE TM

Sensible Solutions for Pesticide Extraction...GC/NPD & LC/MS Internal Standard Mix Solvent: Acetonitrile Volume: 5 mL Part # QuECR-NPD-MS-IS Compound Conc (μg/mL) triphenylphosphate

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Page 1: Sensible Solutions for Pesticide Extraction...GC/NPD & LC/MS Internal Standard Mix Solvent: Acetonitrile Volume: 5 mL Part # QuECR-NPD-MS-IS Compound Conc (μg/mL) triphenylphosphate

Sensible Solutions for Pesticide ExtractionQuEChERS Products

SPEX CertiPrep provides a complete solution to all your QuEChERS needs with a comprehensive set of Internal Standards for the QuEChERS analytical techniques (GC, GC/MS, LC/MS).

QuEChERS Standards

Meeting all your QuEChERS needs with general purpose kits suitable for removal of polar organic acids, some low to moderate levels of sugars and lipids. General purpose kits are available for US (AOAC Method 2007.01) and European Methods (EN Method 15662).

QuEChERS Kits

Part # Compound Solvent Conc (μg/mL)

QuECR-PCB-18 PCB 18 Acetonitrile 50

QuECR-PCB-28 PCB 28 Acetonitrile 50

QuECR-PCB-52 PCB 52 Acetonitrile 50

QuECR-PCB-138 PCB 138 Acetonitrile 50

QuECR-PCB-153 PCB 153 Acetonitrile 50

QuECR-5190 triphenylmethane Acetonitrile 10

QuECR-3765 triphenylphosphate Acetonitrile 20

QuECR-AOAC-TTP triphenylphosphate Acetonitrile 2

QuECR-4381 tris-(dichloroisopropyl)phosphate Acetonitrile 50

Single Component Reference StandardsVolume: 5 mL

Method Part # Product Name Material Qty Centrifuge Tube Volume

EN 15662

EN-CIT-50ML Citrate Buffered Extraction Tubes4 g MgSO4,1 g NaCl, 0.5 g sodium citric dibasic

sesquihydrate, 1 g sodium citrate tribasic dihydrate50 pk 15 mL w/50 mL

Centrifuge tube

EN-PSA-2ML PSA Dispersive SPE Clean-Up Tubes 25 mg PSA, 150 mg MgSO4 100 pk 2 mL

EN-PSA-15ML PSA Dispersive SPE Clean-Up Tubes 150 mg PSA, 900 mg MgSO4 50 pk 15 mL

AOAC 2007.01

AOAC-ACE-50ML Acetate Buffered Extraction Tubes 6 g MgSO4, 1.5 g sodium acetate 50 pk 15 mL w/50 mL Centrifuge tube

AOAC-PSA-2ML PSA Dispersive SPE Clean-Up Tubes 50 mg PSA, 150 mg MgSO4 100 pk 2 mL

AOAC-PSA-15ML PSA Dispersive SPE Clean-Up Tubes 400 mg PSA, 1200 mg MgSO4 50 pk 15 mL

SPEXQuETM

Page 2: Sensible Solutions for Pesticide Extraction...GC/NPD & LC/MS Internal Standard Mix Solvent: Acetonitrile Volume: 5 mL Part # QuECR-NPD-MS-IS Compound Conc (μg/mL) triphenylphosphate

SPEX CertiPrep203 Norcross AvenueMetuchen, NJ 08840

Tel: 732-549-7144Fax: [email protected]

European DivisionSPEX CertiPrep Ltd2 Dalston GardensStanmore, Middlesex HA7 1BQ

Tel: +44(0)208-204-6656Fax: +44(0)[email protected]

Corporate Headquarters

BEFORE

AFTER

Safety interlock prevents unit from operating when lid is open. Window allows analyst to view samples during operation.

Vertical shaking motion ensures thorough mixing and analyte extraction.

Clamp holds six 50 mL vials or six 15 mL vials. Alternate clamp for six 50 mL vials or six 2 mL vials.

Spill tray for easy cleanup.

Digital timer display with adjustable operating time.

Compact, powerful motor agitates samples at 1500 rpm.

ShaQe Up Your QuEChERS Method!A Simple, Safe & Effective solution for QuEChERS

Compound Conc (μg/mL)

PCB 18 50

PCB 28 50

PCB 52 50

triphenylmethane 10

triphenylphosphate 20

tris-(1,3-dicholorisopropyl)phosphate

50

GC/ECD Internal Standard Mix50 μg/mL each in AcetonitrileVolume: 5 mLPart # QuECR-ECD-IS

PCB 18

PCB 28

PCB 52

tris-(1,3-dicholorisopropyl)phosphate

LC/MS Internal Standard Mix10 μg/mL each in AcetonitrileVolume: 5 mLPart # QuECR-LC-MS-IS

nicarbazin

GC/NPD & LC/MS Internal Standard MixSolvent: AcetonitrileVolume: 5 mLPart # QuECR-NPD-MS-IS

Compound Conc (μg/mL)

triphenylphosphate 20

tris-(1,3-dicholorisopropyl)phosphate 50

GC/MS QC StandardsSolvent: AcetonitrileVolume: 5 mL

Part # Compound Conc (μg/mL)

QuECR-MS-QC-1 PCB138 50

PCB 153 50

QuECR-MS-QC-2 anthracene 100

GC/MS Internal Standard MixSolvent: AcetonitrileVolume: 5 mLPart # QuECR-MS-IS

AOAC Internal Standard Mix40 μg/mL each in AcetonitrileVolume: 5 mLPart # QuECR-AOAC-IS

α-BHC-d6 (α-HCH-d6)

parathion-d10

AOAC QC Spike Mix40 μg/mL each in AcetonitrileVolume: 5 mLPart # QuECR-AOAC-QC

atrazine

azoxystrobin

bifenthrin

carbaryl (Sevin)

chlorothalonil

chlorpyrifos (Dursban)

chlorpyrifos methly

lambda-cyhalothrin

cyprodinil

2,4'-DDD

dichlorvos (DDVP)

endosulfan sulfate

ethion

imidacloprid

kresoxim methyl

linuron

methamidophos

methomyl

cis-permethrin

trans-permethrin

procymidone

pymetrozine

tebuconazole (Folicur)

thiabendazole

tolylfluanid

trifluralin

ShaQer1500

BEFORE

Your Science is our Passion®