SCREENING SITE INSEPCTION ANALYTICAL RESULTS · Ncrtn cncogo R«rtn«ni I SnVUre:LC 067371583 SAMPLING POINT VCLA TILES SSI SEDUgCNT SAMPLE ANALYTICAL RESULTS 1 .2-C'cnk»asth«r»

10971250007 - l»k. CountyN. Chicago Refiner* & Smclten

!LD 097271563

Superiund/HRS

CERCLAScreening Site

InspectionAnalytical Results

Illinois EnvironmentalProtection AgencyP.O. Box 19276Springfield, IL 62794-9276

EPA Region 5 Records Ctr

229807

Confidential Material May be Enclosed

Printed on Recycled Paper

Appendix H

Target Compound List Analytical Results

H-l

CERCLA SSI: North Chicago Refiner* and Smelten - ILD 097271563

U:OB7Z715«I

iAMPUNG POUT

VCCAT'LES

i - O

FESTiClOES/PCB**x:rtn« -DOEEn dm4 41 -DOT

vcclor-icn»VOCKX-1254

S6VHVOLW1LES

ncurxa 1 i3-c<*0>nn4>

1NOROAMC*MXTM jm

Annmony

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HI SON. 3AUPLE AWSLrDOi. RESULTS

X119

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1300 a8.X l>aoou6.00U

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22.00U4100U42.00 U1100 J

220 00 U220. 00 U210.00 U42000 U(B*)

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— ...._

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NOTES:U -8 - indUM confound * iJ - ndc«M compound • •

Ncrtn cncogo R«rtn«ni I SnVUre:LC 067371583

SAMPLING POINT

VCLA TILES

SSI SEDUgCNT SAMPLE ANALYTICAL RESULTS

1 .2-C'cnk»asth«r» (total)5-3a«non«1 . 1 . t - TncMara«r<ano

E:ryEir»f

4.4'-OC€Enorin44 ' -OOr

gamma-Chioraan*Afaciof-1018Aroctaf- 1 254

SeWIVOLATlLES

P>r»Bjy1

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3enz(a)anthr«c«n»

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1 -m«<nry1

INORGANICS .AluminumA/ximonyAnwicSan urnB«rybiumCadmium

CobaKCopp«fIronUnaMagrmun

M«rcuryNek*

SsicnuinSilv«rSodiumVaradiunZ.ncCyvnd*

NOTCS:U - indiutMconxxxnl wai t«M tor but not d*«ttdS - indicAM compound * an Ktimoled valueJ - indwM«« compocnd » an MiimatM vilu*

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Il l inois Envi ronmenta l Protection Agency P.O. Box 19276, Springfield. IL 52794-3273

MEMORANDUM

DATE: February 11,1992

TO: Greg Dunn

FROM: Ron Turpin <Sc Jim Shaw

SUBJECT: Review of Data PackageNorth Chicago Refiners and Smelters

The Division of Laboratories Quality Assurance Section has reviewed theabove referenced data package. The package was for 18 soil samplestaken on November 15,1991, for the target compound list. The sampleswere analyzed at the IEPA laboratories in Springfield (organics) and inChampaign (inorganics). The results are valid as qualified on theattached Forms 1.

attachments

cc John HurleyKarl ReedTom Crause

RECEIVED

FEB131992

Illinois Environmental Protection Agency • P.O. Box 19276, Springfield, IL 62T94-9276

MEMORANDUM

DATE: September 1, 1992

TO: Greg Dunn

FROM: Ron Turpin <W f U<V^1

SUBJECT: Erroneous Mercury results reported on N. Chicago Refiners & SmeltersSDG 59.

Attached are corrected Form 1's to replace the original forms for the above referencedsite. Due to a calculation error made by the laboratory, the Mercury results wereincorrect.

SAMPLE DATA SUMMARY PACKAGE

J

ILLINOIS ENVIRONMENTAL PROTECTION AGENCYSpringfield Organicg Laboratory

825 N. Rut ledgeSpringfield, Illinois S27Q2

217-732-9730

CASE NARRATTVT^

N. Chicago Refiners i Smelters

X101 D199S73X102 D199679X103 D199680X104 D199681X105 D199S66X106 D199667X107 D1996S3X103 D199669X109 D199S7QXliO 1-199571Xlll D199S&2X112 3199623

X114 D199685Xllo ~199636X.11S ^199537X117 Il99f^2'{' • ?.

Flucr-ce.-oene is used as an additional ir.terr.al standard to oalo\

vela- 1_= 3'andard.

•Zair.p'.-Ti wi-h laboratory file ident if ica~ ir.-.s cegir.r.ir.g with ar. A warerun on instrument 5 100 A. Those beginning with a 2 war? run on instru-sr.t

X101 w=.s rerun as X101RE. In XlOl 5urr:gatr3 573 and toluene-dS as wea3 two ~z the three internal standard- were outside acceptable iimit=In X1:J2?_Z both surrogates were still rut cf control as well as ailthree internal standards. This reanalysis ot-plies with the Volatilerequire-ents, feotion III. paragraphs 4.2.2.1.4 and 6.1.1.2 of the2/85 itatenent of Woric.

The Wi.ey Mass Spectral Database in the Chemical Information System.on-line service was searched as an ado it ic.Tal oheok to try tt identisome tf the more signif ioant TICs. N-: r.atrhes were found.

The baseline rise in the 12/02/31 standard had no effect on ouant 1 tat :-.-.

î-i". "i----~i"T. - — ^_~ r. 'S r. r. c CT. ir.u ir. & ~i*icrit«cr. c r ' " 5 r' a.

Although all samples were extracted on 11/15/91, the samples received cr.11/14/91 were extracted by the day shift and those received on 11/15/9:were extracted by the evening shift. Hence- there are two blanks and-wo sets of matrix spikes.

XilS matrix spike FORM III SV-2 ;Pyrene was detected in the original sample at a concentration higherthan that in the matrix spiked samples. This resulted in a net negativerecovery in the matrix spikes on FORM III. This may be due to an unevendistribution of the analyte in the sample container.

X1C2 ; The spectral disagreement of fluoranthene is more than the 2C°Sallowed when compared with the standard spectrum because of a co-elutingTIC in the sample.

X103 ; The spectral disagreement of di-n-butylphthalate is more thar. tr.e2Crs allowed when compared with the standard spectrum because of aoo-eluting TIC in the sample.

X106 ; The spectral disagreement of fluoranthene is more than the 20%allowed when compared with the standard spectrum because of backgroundnoise in the sample.

X10S : The spectral disagreement of ber.zc cb ; fluoranthene , ir.deno( 1, 2 , 2- : d -pyrer.e and ber.ro •;. ghi )pery ler.e is more than the 20Ji all-wed when ccmparec,with the standard spectrum because of background noise in the sample.

XI10 ; The spectral disagreement of n-nitrosodiphenylamine is more th-zr.the 20^ allowed when compared with the standard spectrum because ofbackground noise in the sarr.ple.

X.lll ; The spectral disagreement cf ir.der.c ; 1, 2. 3-od ; pyrer.e ar.o rrr.~o i/.. -p-rryle.-.e is r.:r? Than the 20% allowed when ocr.pared with the £tandardspectrum because of background noise in the sample.

X112 ; The stertral disagreement of fluorene is more thar. the 2'.'"i allcveowhen ccmpared with the standard spectrum brcause 4-ohloropher.yl phenylet.-.er c:-elute* in the standard.The spectra, disagreement of naphthalene, butylbenrylphthslate. benrc =. -pyrer.e. -.n-der.: : 1, 2 . 3-od ; pyrer.e and bsr.zc-'. gr.i . pery ler.e is mere thar. the 21 •.allcwed when compared with the standard spectrum because of a cc-eluf.r.aTIC in the sample.

XI13 : The spectral disagreement of bsr.o:; b : f luorar.thene and ber.o-.'.-: -flu:r*nthene is more than the 2G£ allowed when compared with the standirdspectrum because of background no is? ir. the simple.

XI15 : The spectral disagreement of flucrene is more than the 20% ail eweuwren ccmpared with the standard spectrum because 4-ohlcropher.yl pher.ylether cr-elutes in the standard.The spectr=l disagreement c-f bisi 2-ethylhe>:yl'phthalate is more than tr.s20ti al_:wed when compared with the standard =p»otrur. because ber.scio =.cidco-elutes in the standard.The spectral disagreement of indenc ( 1. 2. 3-cd pyrer.e and bensc'. ghi :?ery ler.is more thar. the 20"4 allowed when compared with the standard speotru:"hecauze cf cackground noise in the sample.

X115 : The spectral disagreement of flucrer.e is more than the 20 - all-ewe:

-» — •»-*— —* -• .a * • • .a a * o **W A • ** a *^ '^ a v*^5 - i. 5 r »w~"r--*'-(33 ^ n -**e 3.a.*â.^.

XI 13 ; There is insufficient space on FORM III EV-TIC for the naj.es ofthe components detected. Most are PCS isomers. See the Library searcheswith the seoivolatiie data or the pesticide results for identification.

Surrogate recoveries on samples X112. Xil5, X115 and XllSMS (Fern 25)were high due to matrix interference in the samples.

Surrogate was not detected (Form SE ; in samples X115, XllSMS and X112MSL1

due to the high amount of PCS causing masking, so recovery was calculate:from the alternative confirmation column.

Matrix spike analytes Aldrin. Dieldrin and DLT were net detected 'Form 2:due to masking by the PCS concentration.

The %r> for 4,4'-DDT was high ;?orT. 9} due to the improper integrationof the peaks in the late runs caused by the rise in the baseline fromthe temperature program". 4,4'-DDT was not detected frr quant itat ion zzno corrective action was taken.

The alpha and gamma-Chlordane found in X1C5 (Fcrm 10; was confirmedby GC/M2 but the specific isomers were not determined.

Celeste Crowley (/ DatePesticide Supervisor

ar/jermannC-'Mi Supervisor

- ^ - , . + ^ i —arf..-. :-:--rley 7aboratory Manager

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1AVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: ILLINOIS EPA

EPA SAMPLE NO

X101

Lab Code: SPFLD

Matrix: (soil/water) SOIL

Sample wt/vol: 5.Q (g/mL)

Level: (low/ned) LOW

% Moisture: not dec. 46

Column: (pack/cap) CAP

Contract: 097l25nnn7

Case No.: REFINE SAS No.: SDG No.: D1996R

Lab Sample ID: D19967H

Lab File ID: Blll9LCMn

Date Received: 11/15/91

Date Analyzed: 11/19/91

Dilution Factor: 1. 0

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

74-87-3 Chlorome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride.67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1,1-Dichloroethene.75-34-3 1, 1-D ichloroethane.

67-66-3 Chloroform107-06-2 1, 2-Dichloroethane73-93-3 2-Butanone71-55-6 1,1,1-Tr ichloroethane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1, 2-Dichloropropane10061-01-5 cis-l,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochlorome thane79-00-5 1,1, 2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene.75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene.79-34-5 1,1,2,2108-88-3 Toluene108-90-7 Chlorobenzene_100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total).

19191919142399999919991999999999919199999999

Q

;u;u:u

: u;u:u;u:u;u!U10IU:u:u;o:u:o!u:u:u!U;u:u;u: u10:u:o:u;u

FORM I VGA 000004

IEVOLATILE ORGANICS ANALYSIS DATA SHEET

TENTATIVELY IDENTIFIED COMPOUNDS


EPA SAMPLE NC

X101

Lab Code: SPFLD



Level: (low/Bed) LOW


Column (pack/cap) CAP

Contract: Q97125QQ07

Case No.: REFINE SAS No.: SDG No.: D19966

Lab Sample ID: D199678

Lab File ID: B1119LC10



Dilution Factor: 1.0

Number TICs found; Q.CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. Q

FORM I VOA-TIC OOOCOS 1/37



EPA SAMPLE SC

X102

Lab Code: SPFLD


Sample wt/vol: 5.0 (g/mL)








Date Received: 11/15/9!


Dilution Factor: 1.Q


74-87-3 Chlorome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulf ide75-35-4 1,1-Dichloroethene75-34-3 1, 1-Dichloroe thane540-59-0 1,2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1, 2-Dichloroethane73-93-3 2-Butanone71-55-6 1,1, 1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-l,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochlorome thane79-00-5 1,1,2-Trichloroe thane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1, 1,2, 2-Tetrachloroethane_108-83-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)

17171717Jf2499999917991799999999917179999999

Q

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: u: u;u

:u10;u:u:o!U: u:u;u1U

: u!U:u:u;u1 U:u;u;u

FORM I VOA oooccs

IBVOLATILE ORGANICS ANALYSIS DATA SHEET



EPA SAMPLE SO

X102

Lab Code: SPFLD

Matrix: (soil/water) SJUL.

Sample wt/vol:

Level: (low/med)

Contract: Q97125QOQ7 |

Case No.: BJLLLNJL SAS No.: SDG No.: D19966

(g/mL)




Lab File ID: Blll9LC!3




Number TICs found: Q.CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG


FOPM I V O A - T I Cnnnnrvi

1/3"



EPA SAMPLE NO

X103

Lab Code: SPFLD



Level: (low/med) LOW

% Moisture: not dec. 4Q


Contract: Q97i?snnn7


Lab Sample ID: D19968Q




Dilution Factor: 1. Q


74-87-3 Chlorome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulf ide75-35-4 1, 1-Dichloroethene75-34-3 1, 1-Dichlo roe thane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1, 2-Dichloroethane73-93-3 2-Butanone71-55-6 1 ,1 , 1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-l,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochlorome thane79-00-5 1,1,2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1,2,2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)

17171717

88838817881788888888817178883388

Q

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! U!D!DIDIUIDID!DIU!UID:o:uIDID:uID:uIDIDIDIDIDIDIUIUIU,'D

FORM I VGA 1/37 ?-



Lab Name: ILLINOIS EPA Contract: 0971250QQ7

EPA SAMPLE S:

X103

Lab Code: SPFLD Case No.: REFINE SAS No.: SDG No.: D19966






Lab Sample ID: 0199680



Date Analyzed: 11/19/9!




FQBM I V O A - T I C 000011 1 /Q 'i / J

LAVOLATILE ORGANICS ANALYSIS DATA SHEET

Name: ILLINOIS EPA Contract: 0971250007

a?A SAMPLE NC

X104

Lab Code: SPFLD

Matrix: (soil/water)

Sample wt/vol:

Level: (low/Bed) LOW

Case No.: REFINE SAS No.: SDG No.:

(g/mL)





Date Received: . 11/15/91



CAS NO. COMPOUNDCONCENTRATION DNITS:(ug/L or ug/Rg) UG/KG

74-37-3 Chlorome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chlo roe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulf ide75-35-4 1, 1-Dichloroethene75-34-3 1, 1-Dichloroethane540-59-0 1,2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1,2-Dichloroethane78-93-3 2-Butanone71-55-6- ---1,1,1-Trichloroethane56-23-5 Carbon Tetrachloride103-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochloromethane79-00-5 1,1,2-Trichloroe thane71-43-2 Benzene10061-02-6 trane-1,3-Dichloropropene_75-25-2 Bromoform1 OS-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-13-4 Tetrachloroethene79-34-5 1,1, 2,2-Tetrachloroethane_108-83-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)

121212127

6666612661266666666612126666666

Q

!U

uuuuuuuu:u:u;u!U', u;u

UUuu:u:uiu:u

FORM i VOAQOQG12

1/8'

12VOLATILE OBGANICS ANALYSIS DATA SHEET


Lab Name: Tr.LTNOIS EPAX104

Lab Code: SPFLD






Contract: 0971250007

Case No.: REFINE SAS No.: £DG No.: D19966


Lab File ID: B1119LCM




Number TICs found: Q_CONCENTRATION UNITS:(ug/L or ug/Kg) UG/RG


FORM I V G A - T I C000013


Lab Nam«: ILLINOIS EPA

EPA SAMPLE NO

X105

Lab Code: SPFLD




% Moisture: not dec. .. 14



Case No.: REFINE SAS No.: SDG No.: D199SS

Lab Sample ID: D199fififi

Lab File ID: All2f)Ryn4




CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Rg) DG•KG

74-37-3 ChJ ore. me thane74-33-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulf ide75-35-4 1, 1-Dichloroethene75-34-3 1,1-Dichloroethane540-59-0 1,2-Dichloroethene (total),67-66-3 Chloroform107-06-2 1,2-Dichloroe thane78-93-3 2-Butanone71-55-6 1,1,1-Trichloroethane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cia-l,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochloromethane79-00-5 1,1, 2-Trichloroethane71-43-2 Benzene10061-02-6 trans-l,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 l,l,2,2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)

12121212666666

12661266666666612126666666

Uu

UuuuU

uU

i U;u!U:u;u:u:u:u

Uuuu

i uiu:u:u:u

FORM I VOA OOG014


TENTATIVELY IDENTIFIED COMPOUNDSLab Name: ILLINOIS EPA Contract: Q97125QOQ7

EPA SAMPLE NO

X105

Lab Code: SEILJL Case No.: REFINE SAS No.: SDG No.: D19966






Number TICs found: L


Lab File ID: A112QBK04




CONCENTRATION UNITS:(ug/L or ug/Kg) OG/KG

CAS NUMBER

1. 60-29-3

COMPOUND NAME

ETHYL ETHER

! RT

1 1.65l'

E3T. CONC. ^

9.8 J

FOPM I VOA-TIC 000015



EPA SAMPLE NO

X106

Lab Code: SPFLD


Sample wt/vol: 5 .


Contract: Q97l25pflfl7


(g/mL)


Lab File ID: A112QRKOfi

% Moisture: not dec. 2^






.7^-87-3 ChloromethaneT4-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1, 1-Dichloroethene75-34-3 1, 1-Dichloroe thane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1, 2-Dichloroethane78-93-3 2- Bu t anone71-55-6 1,1,1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1, 2-Dichloropropane10061-01-5 cis-l,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochloromethane79-00-5 1,1,2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1, 2,2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)

1313131371377777713771377777777713137777777

:u;u10i ui

i u!U:ui ri

iu:u:u

;u;u;ui ui ui u:u:u;u:u!Ui u;u:oiui u:u;u

FORM I VOA OOOOlo

ISVOLATILE ORGANICS ANALYSIS DATA SHEET



EPA SAMPLE N:

X106

Lab Code: SPFLD


Sample wt/vol: 5 .

Level: (low/aed) LOW

Contract: 09712500Q7


(g/mL)

Lab Sample ID: Dl99fifi7

Lab File ID: A112nBKns



Date Received: 11 /I


Dilution Factor: l.Q

Number TICs found:CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

CAS NUMBER

1. 60-29-3

COMPOUND NAME

ETHYL ETHER

RT

1.65

EST. CONC. !

5.4! J1

Q

FORM T VOA-TTH


EPA SAMPLE SO

Lab Nam«: T T . T . T N Q T S EPAX107

Lab Code: SPFLD




X Moisture: not dec. . 16


Contract: Q97i25nnn7 _

Case No.: REFINE SAS No.: SDG No.: D1996S

Lab Sample ID: D1996B3

Lab File ID: A112QBKnfi


Date Analyzed: 11/2Q/91


CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Rg) UG/RG

74-87-3 Chlororae thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Kethylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1, 1-Dichloroethene75-34-3 1,1-Dichloroe thane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1, 2-Dichloroethane78-93-3 2-Butanone71-55-6 1,1, 1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-43-1 Dibromochlorome thane79-00-5 1,1, 2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1, l,2,2-Tetrachloroethane_108-38-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)

12121212612666666

12661266666666612126666666

Q

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;u

uuU

: u;U;uI U!U:u!Ui U:u!U!U!U:o:u!U

FORM I VOA 00001S

IBVOLATILE ORGANICS ANALYSIS DATA SHEET



EPA SAMPLE SC

X107

Lab Code: SPFLD






Contract: Q9712SQQQ7



Lab File ID: A112Q3K06




Number TICs found:CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

CAS NUMBER

1. 60-29-3

COMPOUND NAME

ETHYL ETHER

l

! RT

1 1.67I

EST. CONC.

6.5

'•*

J

FORM



EPA SAMPLE NO

X108

Lab Code: SPFLD


Sample wt/vol: S.Q (g/mL)




Contract: Q97i?.snon7_



Lab File ID: A1120BK07




CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/RG

74-87-3 Chloromethane74-83-9 Bromomethane75-01-4 Vinyl Chloride75-00-3 Chloroethane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1,1-Dichloroethene75-34-3 1, 1-Dichloroe thane540-59-0 1,2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1, 2-Dichloroethane78-93-3 2-Butanone71-55-6 1,1,1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-43-1 Dibromochloromethane79-00-5 1,1, 2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1,2, 2-Tetrachlorc-:-r.ane_108-88-3 Toluene108-90-7 Chlorobenzenel"00-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)

1212121261266666612661266666666612126666666

Q

'J;uo:u; uUuu10

uo

au:o;u1U10;u:u

;ui u;u!U10:u

FOPM I VOA 000020 I/




EPA SAMPLE MO

X108

Lab Code: SPFLD


Sample wt/vol: 5. Q (g/mL)



Column (pads/cap) CAP

Contract: 097125QDQ7


Lab Sample ID: D1996p3

Lab File ID: All20Ryn7




Number TICs found: Q.CONCENTRATION DNITS:(ug/L or ug/Kg) DG/KG


FORM I V O A - T I C 000021 1 / 5'


L-b Name: n.MNOlS EPAX109

Lab Code: SPFLD






Contract: 097125DQQ7

Case No.: REFINE SAS No.: SDG No.;

Lab Sample ID: Dl996?n

Lab File ID: A1121HK04




CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG.

74-87-3 Chlorome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chlo roe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1, 1-Dichloroethene75-34-3 1,1-Dichloroethane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-C6-2 1, 2-Dichloroethane73-93-3 2-Butanone71-55-6 1,1, 1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate7 5 - 2 7 - 4 Bromodichlorome thane76-37-5 1, 2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochloromethane79-00-5 1,1,2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1 , 1 , 2 , 2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)

1212121261266666612661266666666612126666666

Q

UUuIU

IU!U:o!U!U!U

!U:u;o10i u:u;u;u;u!U!U10IUIU

uuiuiu

FORM I VOA000022

ISVOLATILE ORGANICS ANALYSIS DATA SH2ST


EPA 3A:l?"_Z S"

Lab Name: n.T.TNQTS EPAX109

Lab Code: SPFLD

Matrix: (soil/water) S_C_1L

Sample wt/vol:



Case No.: REFINE SAS No.: SDG No.: 019955

D1996TO

(g/mL)

% Moisture: not dec. Lfi.


Lab Sample ID:

Lab File ID: A11215KQ4

Date Received: 11/14/9:



Number TICs found: Q_CONCENTRATION UNITS:(ug/L or ug/Kg) DG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. ; £ -

FORM I V O A - T I C

000023


Name: ILLINOIS EPA Contract: Q97i25nnn?

SPA SAMPLE NO

X110

Lab Code: S_P_£LD Case No.: REFINE SAS No.: SDG No.: D19966







Lab File ID: A112QBKn9




CAS NO. COMPOUNDCONCENTRATION Ur-ITS:(ug/L or ug/Kg) UG/RG

74-87-3 Chlorome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1,1-Dichloroethene75-34-3 1,1-Dichloroethane540-59-0 1,2-Dichloroethcne (total).67-66-3 Chloroform107-06-2 1,2-Dichloroethane78-93-3 2-Butanone71-55-6 1,1,1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichloromethane78-87-5 1,2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloro«T.-.ene124-48-1 Dibromochlorome thane79-00-5 1,1,2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1,2,2-Tetrachloroethane.108-38-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)

1313131361366666613661366666666613136666666

1 UU•J:u:u:u:u

u

UU

uu:u:u;u:u!U

U

u:o:u

FORM I VOA000024

1/8'




EPA SAMPLE N'

X110

Lab Code: SPFLD

Matrix: (soil/water) S_Q_LL

Sample wt/vol: 5,_


, Contract: Q97125QQQ7

Case No.: REFINE SAS No.: SDG No.: 019966

(g/nL)

% Moisture: not dec. 22.


Number TICs found: Q.


Lab File ID: A112CER09




CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG


FORM I VOA-TIC OOC02-?



EPA SAMPLE Si

Xlll

Lab Code: SPFLD Case No.: REFINE SAS No.: SDG No.: Dl996n






Lab Sample ID: D1996R7

Lab File ID: B1119r.r!' A




CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

74-87-374-83-975-01-475-00-375-09-267-64-175_15_075-35-475-34-3KdO-^Q-O

67-66-3107-06-278-93-371-55-656-23-5108-05-475-27-473-37-510061-01-579-01-6124-48-179-00-571-43-21 nnfii -.n9-fi---75-25-2108-10-1591-78-6127-18-47Q_-ax_K

108-88-3108-90-7100-41-4100-42-51330-20-7

Chlorome thaneBromome thaneVinyl ChlorideChlo roe thaneMethylene ChlorideAcetoneCarbon Disulf ide1 1-Dichloroe thene1, 1-D ichloroethaneI O — rii/^Kl^^y^rtA^K^n^ / t" n "t* .a 1 i £i/icn.i.OiO*Jiinene v. total iChloroform1 . 2-Dichloroethane2-Butanone1 1 1-TrichloroethaneCarbon TetrachlorideVinyl AcetateBromodichlorome thane

- — 1 2 — Dichloropropane— -— cis-1, 3— Dichloropropene

Trichlo roe thene— — Dibromochloromethane

1 1 2-TrichloroethaneBenzenetrans i , *3 .ui.cn loropropeneBromof orm4-Methy 1-2-Pentanone2-HexanoneTetrachloroethene

i l)£|£ie&racn J-oroeunaneTolueneChlorobenzeneEthyl benzeneStyreneXvlene (total}

1212121225126664661219612666

106666612122666666

:u! U!U:u&U 4\ u!U;u;ui j!U;UI Ut

:u!U:u:u:u\

i ui U!U:u;u!U:uuiu!U:u:u:u', Ui

FORM I VOA

LEVOLATILE ORGANICS ANALYSIS DATA SHEET


Lab Name: ILLTMQIS EPA Contract: Q9712500Q7

EPA SAMPLE

Xlll

Lab Code: S££LD_ Case No.: R£F_1N£ SAS No. : SDG No.: D19955


Sample wt/vol:


(g/aL)








Number TICs found: Q.CONCENTRATION UNITS:(ug/L or ug/Rg) UG/RG

CAS NUMBER COMPOUND NAME PT EST. CONC. Q

FORM I VOA-TIC000027

1 /' 3 ?

1AVOLATILE CRGANICS ANALYSIS DATA SHEET

L«o Name: ILLINOIS EPA

EPA SAMPLE NO

X112

Lab Code: SPFLD




% Moisture: not dec.


Case No.: REFINE SAS No.: SDG No.: D199SQ


Lab File ID: B112QLC:J4


CAS NO. COMPOUND




CONCENTRATION UNITS:(ug/L or ug/Xg) DG/KG

74-87-3 Chlorome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroethane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1,1-Dichloroethene75-34-3 1,1-Dichloroe thane540-59-0 1,2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1,2-Dichloroethane78-93-3 2-3utanone71-55-6 1,1,1-Trichloroethane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochlorome thane79-00-5 1,1,2-Trichloroe thane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1,2, 2-Tetrachloroethane_108-33-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)

13131313111366666613661366676666613136666666

Q

;o:o!U;ut

io; o

U000o00ua:ui

iu;u:o

;o!0;u:u!D

FORM I VOA 000028

ISVOLATILE CRGANICS ANALYSIS DATA SHEET


Lab Nan«: ILLINOIS EPA

EPA SAKF1S $

X112

Lab Code: SPFLD


Sample wt/ypl: 5.Q (g/mL)






Number TICs found:


Lab File ID: B1120LCC4




CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KQ

CAS NUMBER

1. 60-29-32.3.4.5.

f

i COMPOUND NAME

1 ETHYL ETHER! UNKNOWN! UNKNOWN1 UNKNOWN! UNKNOWNi

RT

1.8315.4216.1216.6917.92

EST. CONC.

6.7147.2

116. 1

Q

JJJJJ

FOPM I V O A - T I C000029

1/3'


o Name: ILLINOIS EPA

Lab Code: SPFLD Case No.: REFINE


Sample wt/vol: 510 Cg/mL) G_


% Moisture: not dec. I5



SAS No.:

EPA SAMPLE N(

X113

SDG No,:


Lab File ID: Bli2QLr:n

Date Received: 11/15/9"!



CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG-

74-87-3 Chloromethane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroethane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1, 1-Dichloroethene75-34-3 1,1-Dichloroethane540-59-0 1, 2-Dichloroethene (total)_67-66-3 Chloroform107-06-2 1,2-Dichloroethane78-93-3 2- Bu t anone71-55-6 1,1,1-Trichloroethane56-23-5 Carbon Tetrachloride103-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-37-5 1, 2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene .124-43-1 Dibromochloromethane79-00-5 1, l, 2-Trichloroethan*71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene__75-2^-2 Bromoform108-10-1 4-Me thy 1-2-Pent anone591-73-6 2-Hexanone127-13-4 Tetrachloroethene79-34-5 1,1, 2,2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene-100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)

121212121612666666

12661266hi

6

68612126666666

Q

UUUU

UU

.11UUUUUU

!U:u1 u:u

1 T;

;U

!UI ri

iuIU

:u:u

FORM I VOA OOO0301/3"




EPA SAMPLE !>'(

X113

Lab Code: SPFLD






Number TICs found:


Case No.: REFINE SAS No.: SDG No.: D1996S

D199684

3112CLC03

Lab Sample ID:

Lab File ID:






FORM I VOA-TIC 000031 1 / :


EPA SAMPLE SO

I Name: ILLINOIS EPA

Lab Code: SPFLD




% Moisture; not dec. 20


_ Contract: 0971250007

Case No.: REFTNE SAS No.:

X114

No.:


Lab File ID: B112QL(?ns


Date Analyzed: 11/20/9!


CAS NO. COMPOUNDCONCENTRATION DNITS:(ug/L or ug/Kg) OG/KG

74-87-3 Chloromethane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroethane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1,1-Dichloroethene75-34-3 1, 1-Dichloroe thane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1,2-Dichloroe thane75-9 3-3 2-Butanone71-55-6 1,1,1-Trichloroethane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichloromethane78-87-5 1, 2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-43-1 Dibromochlorome thane79-00-5 1,1,2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-13-4 Tetrachloroethene79-34-5 1, l,2,2-Tetrachloroethane_103-88-3 Toluene108-90-7 Chlorobenzene100-41-4- Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)

121212121012666666126612666666665121 i-L —6666666

Q

oo

Uu

;u:u;u;u:u:u;u:u:u;u;u

;u:u

uuUouu:u

FOPM I VOA000032

1/8




EPA SAMPLE

X114

Lab Code: 3PFLD

Matrix: (soil/water) S_Q_LL

Sample wt/vol:

Level: (low/med) LQJi


Case No.'- REFINE SAS No.: SDG No.: D19??6

D199635

(g/mL) B112QLC05


Column (pack/cap) CAE—

Lab Sample ID:

Lab File ID:



Dilution Factor-- 1. 0

Number TICs found: Q_CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG

CAS NUMBER COMPOUND NAME RT EST. CONC. i~i.<* i

(

FORM I VGA-TIC



Lab Code: SPFLD Case No.: REFTN5


Sample wt/vol: 5.Q (g/mL) G_



EPA SAMPLE NC

X115

SAS No. : SDG No.: D19956

Lab Sample ID: D

Lab File ID: B112QLCD6

% Moisture: not dec.




Dilution Factor: L. 0

CAS NO. COMPOUNDCONCENTRATION DNITS:(ug/L or ug/Kg) DG/KG

74-87-3 Chloromethane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroethane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1,1-Dichloroethene75-34-3 1,1-Dichloroethane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1,2-Dichloroethane78-93-3 2-Butanone71-55-6 1,1,1-Trichloroethane56-23-5 Carbon Tetrachloride103-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-l,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochloromethane79-00-5 1,1, 2-Trichloroethane71-43-2 Benzene10061-02-6 trans-l,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Fentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1,2, 2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenrene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (totalj

13131313161366656613861366676666613139666666

Q

ID!UIDIDI

ID! DIDi:J: J: o!D:Dii

:D:o;u:D:DID;D:DIDIDID!0iIDiDIDIDIDID

FOPM I VOA 0000341/87 Fe



-O Name: ILLINOIS EPA

EPA SAMPLE NO

X115

Lab Code: SPFLD





Column (pack/cap) CAE

Contract: 097125QQQ7

Case No.: REFINE SAS No.: SDG No.: HL3_2££


Lab File ID: B112QLCQ6





CAS NUMBER COMPOUND NAME RT EST. CONC. ,— i<*

FOPM I VOA-TIC 000035



EPA SAMPLE :;r

X116

Lab Code: SPFLD

Mat r ix : ( soi l /water) SJ1LL

Sample wt/vol :

Level: ( low/med)

. Contract: Q971250Q07

Case No.: B££IH2. SAS No.: SDG No.: D19956

(g/mL)

% Moisture: not dec. Lfi.








74-87-3 Chlorome thane74-83-9 Bromomethane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1, 1-Dichloroethene75-34-3 1, 1-Dichloroe thane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1, 2-Dichloroethane78-93-3 2-Butanone71-55-6 1 , 1 , 1-Trichloroethane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1, 2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-43-1 Dibromochlorome thane79-00-5 1,1, 2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoforo108-10-1 4-Methyl-2-Pentanone591-73-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1,2, 2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene100-41-4--- Ethylbenzene100-42-5 Styrene1330-20-7 Xylene ( to ta l )

12121212

666666

1266

12665.666666

1212

6666666

Q

! U: u: U! Ui

: u: u

: u;":a; u; u; u! U; u;u! U;u:u; u:u:ui ri

i u! U! U! U: u;u:u; u! U

FORM I VOA OOC036




EPA SAMPLE SO

X116

Lab Code: SPFLD



Level: (low/aed) LOW



Contract: 097125Qnn7

Case No.: REFINE SAS No.: SDG No.: DI9966


Lab File ID: B112QLCQ3



Dilution Factor; 1.0


CAS NUMBER COMPOUND NAME RT EST. CONC. 3

FOPM I VGA-TIC 000037



EPA SAMPLE

X117

Lab Code: SPFLD




X Moisture: not dec. 24


Contract: Q971250Q07



Lab File ID: A112QBK1G





74-87-3 Ch lor ome thane74-83-9 Bromome thane75-01-4 Vinyl Chloride75-00-3 Chloroe thane75-09-2 Methylene Chloride67-64-1 Acetone75-15-0 Carbon Disulfide75-35-4 1, 1-Dichloroethene75-34-3 1, 1-Dichloroethane540-59-0 1, 2-Dichloroethene (total).67-66-3 Chloroform107-06-2 1, 2-Dichloroethane78-93-3 2-Butanone71-55-6 1,1, 1-Trichloroe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1, 2-Dichloropropane10061-01-5 cie-1,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochlorome thane79-00-5 1, 1, 2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1,1,2,2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene100-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)

13131313IS247777771377

1377777777713137777777

Q

! U;u!U:ui

ITi U!U;u;u; u

:u!U:uIU;ui u!U:u;uiu;u:u:u!U:ui u:u;u!U;u!U

FORM I VOA



1 > Name: ILLINOIS EPA

EPA SAMPLE NC

X117

Lab Code: SPFLD









Lab File ID: Al12QBE 10


Date Analyzed: 11/2Q/91

Dilution Factor: LJ1



FORM I V G A - T I C 1,nnnmo

1AVOLATILE OHGANICS ANALYSIS DATA SHEET

EPA SAMPLE NC

Lab Name: ILLINOIS FPA

Lab Code: SPFLD



Level: (low/med) LOH




Case No.: BEJLLHi SAS No.: SDG No.

X118

Lab Sample ID:

Lab File ID:

Date Received:

Date Analyzed:

A112DRK1

11/14/91

11/20/91

Dilution Factor-- 1. Q

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) OG/KG

74-87-3 Chlorome thane74-83-9 Bromo me thane75-01-4 Vinyl Chloride75-00-3 Chlo roe thane75-09-2 Kethylene Chloride67-64- 1 Acetone75- 15-0 Carbon Disulfide75-35-4 1, 1-Dichloroethene75-34-3 1, 1-Dichloroe thane540-59-0 1,2-Dichloroethene (total).67-66- 3 Chloroform107-06-2 1, 2-DichloroethaneT 3-93-3 2-3utanone71-55-6 1,1, 1-Trichlo roe thane56-23-5 Carbon Tetrachloride108-05-4 Vinyl Acetate75-27-4 Bromodichlorome thane78-87-5 1,2-Dichloropropane10061-01-5 cis-1,3-Dichloropropene79-01-6 Trichloroethene124-48-1 Dibromochlorome thane79-00-5 1,1,2-Trichloroethane71-43-2 Benzene10061-02-6 trans-1,3-Dichloropropene_75-25-2 Bromoform108-10-1 4-Methyl-2-Pentanone591-78-6 2-Hexanone127-18-4 Tetrachloroethene79-34-5 1, l,2,2-Tetrachloroethane_108-88-3 Toluene108-90-7 Chlorobenzene10 0-41-4 Ethylbenzene100-42-5 Styrene1330-20-7 Xylene (total)

1212121214126666661266126661066666121259666666

uou

u

;ui

i u:u:ui u;uiu:ui

iu;u; u:u;u;u

FORM i VOA



3 Name: ILLINOIS EPA

SPA SAMPLE SO

X118

Lab Code: SPFLD


Sample wt/vol:

Level: (low/rned; LOW


Contract: Q97i?5pnn7


(g/mL)

Lab Sample ID- D199571

Lab File ID: All COBS'

Column pack/cap) CAP

Date Received: 11 -• 14 / 9 1

Date Analyzed: 11/20/9 1

Dilution Factor: 1 . 'J

Nur.ber TICs found:CONCENTRATION UNITS:(ug/L or ug/Rg) UG/KG

CAS NUMBER

1. 60-29-3

COMPOUND NAME

ETHYL ETHER

RT

1.67

EST. CCNC.

8.2

Q

J

FORM I VOA-TIC 000041

3IMI VOLATILE ORGAN ICS ANALYSIS 3ATA SHEET

Lab Name: TT.LTNQIS EPAX101

Lab Code: SPFLD




X Moisture: not dec. 46 dec.

Extraction: (SepF/Cont/Sonc)

GPC Cleanup: (Y/N) I pH:

Contract: Q9712500Q7 ;

Case No.: EE£ULB SAS No.: SDG No.: D19966


Lab File ID: C12Q3W10

7.9


Date Extracted: 11/15/91



CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UQ/XG Q

n i A A A^ qq q _

Q j- c 7 p

541-73-1X >J W T O '

100-51-6xJ w) W v .L

S5-4S-7i AQ CA i1UO DO _

106-44-5* O 1 r .4 7Oil i — On '

67-72-1QO _QR t1

70 =.q i _1 O O3 1a Q ~7 ~ c.Bo- ,'O-0105 57 9 -65-85-0i i 1 qi i120-33-2120-82-191-20-3106-47-887-68-359-50 7-91-57-677 47_4_88-06-295-95 4-

88-74 4 — -131-11-3208-96-8606-20-2 --

— — fneno i.i • / o f*, 1 , i INfftV.— — — Disi . — nj-oroeLnyi j n tnero r < v t v i— z umoropneno± _1 r 3— Dichlorobenzene

— — — 1 T 4— DichlorobenzeneBenzyl Alcohol

- — 1 . 2— Dichlorobenzene ..2 -Methyl phenol

— _ Xi^fO.. r*l^T/-NT»/^-l— T-N'»^/-\T-,»*''iIr*-U^»%— o i s i.~ L/n J, o ro . oopropy - j iT-ner4-Methvlohenol

- — N— Ni t rosw— D i n-Prcp/ . mi neHe xachloro ethaneLl X Li X LJ R 1 1 C 1 1 c

T U— — i sopnorone _. _ _-witrophenol ,

2 t 4 — Dimethyl phenolBenzoic Acid

2 , 4— Dichloropheno 1

Naphthalene

Hexachlorobutadiene

2— Me thy 1 naphthalene

2 4 T 6— Trichlorophenol

2 -N it roan i 1 ineDime thy IphfchalateAc en a ph thy lene2 6— Din i, t ro to luene

1 r\r\lîUU5 o r\ r\lÛU1 O/ÂlÛU12001 OAA1-iUU12001 OPiAlÛU120C1 OA/*"^1^ JU

12001 O/"l AlÛU1 200T or\r\IÛU1 OAP)UUUx200120057001 90O1200120031012001200120012001 ?0012005700i onolÛU

5700120012001200

li r Ti *Ji r Ti Ui r T, U1 ni r T) 1Ui r ii U• r Ti r i

1 T I

( 1 Ui r T, Ui r •)i U

i U' U1 U1 ni >J1 U1 U; J!U;u1 U!U1 U1 VJ

;u', U1 n;u!U!U:u

FORM I SV-1

000042

1CSEMIVOLATILE ORGANICSÂNALYSIS DATA SHEET

I? A SAJ1PL3 NO

L,ab Name: T T . r . T N Q T S RPA Contract: 0971250007X101

Code: SPFT.D Case No.: REFINE SAS No.: SDG No.: D1S566

Matrix: (soil/water) SQTL

Sample wt/vol: 31.Q (g/mL) G


% Moisture: not dec. 46 dec.

Extraction: (SepF/Cont/Sonc) SQNC

GPC Cleanup: (Y/N) £_ pH: 7.9



Date Received: 11/15/9T_





99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene34-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol.35-30-6 N-Nitrosodiphenylamine (1).101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol35-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b)Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(1.2,3-cd)Pyrene53-70-3 Dibenz( a, h) Anthracene191-24-2 Benzo(g,h,i)Perylene

57001200570057001200120012001200120057005700120012001200570054012001200630500120024001200120012001200120012001200120012001200

Q

:u;u:u;u;u;u;u;u

;u:uI T TI ^

!J:u;u!J!J:u!U;u!U:u:uiu:u!U;u;u:u

(1) - Cannot be separated from Diphenylamine

FORM I SV-2000043

IFSEMIVOLATILE ORGAN ICS ANALYSIS DATA SHZZT


,ah NAm«: ILLINOIS EPA

.a_ Coda: SPFLD Case No. :

Matrix: f Boil/water 1 SOIL

Sample wt/vol: 31.0 (g

Level: (

S Moisture:

Extraction:

3PC Cleanup

Dumber TICs

low/me d) LOW

not dec. 46

(SepF/Cont/Sonc)

: (Y/N) I

found: 20

t

CAS NUMBER I

1.2.3.4.c.

e!•7a

9.10.11.12.13.14.15.16.17.18.19.20.

! UN KNOWN1 UNKNOWN! UN KNOWN1 UNKNOWN; UNKNOWN; UNKNOWN; UN KNOWN: UNKNOWN! UNKNOWN; UNKNOWN; UN KNOWNi UNKNOWNi UNKNOWN; UN KNOWN! UNKNOWNi UNKNOWNi UNKNOWN! UN KNOWN1 UN KNOWN[UNKNOWNl

X101Contract: 0971250007

REFINE SAS No.: SDG No.! m996fi

Lab Samcle ID: D1996^3

/mL) G Lab File ID: C1203W10


dec. Date Extracted: 11/15/91

SOJiC Date Analyzed: 12/03/91

pH: 7.9 Dilution Factor: 1.0


COMPOUND NAME

ALIP

ALIP

ALIP

ALIPALIPALIPALIP

ALIPALIP

. HYDROCARBON

. HYDROCARBON

. HYDROCARBON

. HYDROCARBON

. HYDROCARBON

. HYDROCARBON

. HYDROCARBON

. HYDROCARBON

. HYDROCARBON

RT

27.5627.7727.8423.0123.0223.0728.1428.3128.5428.5928.8128.8929.0129.0429.6630.8231.0931.4231.7131.84

EST. CCNC.

1900740960120044024001200180013001100200075016004102200130010005201500780

3 :

jJ ;T

T

J

J

"

**

.J

J

T

u7

JT

7

JJJT

FORM I SV-TIC

000044

13SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAKPLZ SC.

Lab Name: TLLINQTS EPAX102

Lau Code: SPFLD

Matrix: (3oil/water) SOIL

Sample wt/vol: 30.6 (g/nxL) G




GPC Cleanup: (Y/N) Y pH:

Contract: Q9712SQQQ7

Case No.: REPINE SAS No.: SDG No. : D19966








108-95-2 Phenol111-44-4 b is (2-Chloroe thy 1) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1, 2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 Ms(2-Chloroisopropyl) Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bi s (2-Chloroethoxy) Methane120-83-2 2, 4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene___:88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2, 6-Dinitrotoluene

110011001100110011001100110011001100110011001100110011001100110054001100110011001100110011001100110011001100540011005400110011001100

FORM I SV-1

Q

;u:u!U!U!U:u;u:u;u;u;u;ui u;u!U:uiu;u;u:u!U:u!U:u;u!U:u!U:u:u:u:u;u

1/87 Re-

000045

SEMIVOLATILE ORGANIC3 ANALYSIS DATA SHEET2?A SAM?12 SC

Lab Name: ILLINOIS EPA Contract: 09712SQQO7X102

Lab Code: SPFLD Case No. : REFINE SAS No. :

Matrix: (soil/water) SOIL _

Sample wt/vol: 30-6 (g/mL) G



Extraction: (SepF/Cont/Sonc) SQH£

GPC Cleanup: (Y/N) Y. pH:

SDG No.: 019966







CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) US/KG

99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dini tro toluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4 ,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene8'-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b)Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz( a, h) Anthracene191-24-2 BenzoCg.h , i )Perylene

5400110054005400110011001100110011005400540011001100110054001100110011002601100110022001100110011001100110011001100110011001100

Q

u;u;u;u;u;u:u

:u;u!U:u!U:u:u!U:u!J!U:u;u:u;u;u!U!U:u!U;u:u;u


FORM I SV-2 000046

IFSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET


SPA SAM?L& NO

Lab Name: TLLINQTS EPA Contract: 0971950007X102

Code: SPFLD Case No.: REFTNE SAS No.: SDG No.: D19966

Matrix: (ooil/water) SOIL

Sample wt/vol: 30.6 (g/mL) Q


% Moisture: not dec. 42. dec.

Extraction: (SepF/Cont/Sonc) SONG

GPC Cleanup: (Y/N) Y. pH: 7.3

Number TICs found: 2Q


Lab File ID: C12Q3WT1






CAS NUMBER

1.2.3. 100-52-74.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.

l

! COMPOUND NAME

; UNKNOWN; UNKNOWNi BENZALDEHYDE; UNKNOWN; UN KNOWN PHTHALATEI UNKNOWN ALIP. HYDROCARBONI UNKNOWN'.UNKNOWN[UNKNOWN ALIP. HYDROCARBON; UNKNOWN! UNKNOWN! UNKNOWN1 UNKNOWN! UNKNOWN! UNKNOWN1 UNKNOWN! UNKNOWN! UNKNOWN! UN KNOWN[UNKNOWNI

RT

9.5410.2010.5511.0923.7526.7127.1927.5629.6631.4131.5932.9633.6933.7134.6634.7635.3635.8438.2740.17

EST. CONC.

3800440022001400730660530800120012006208900210011006801000270064016001100

; a!BAJ:AJ!J!AJ; j: Jp Ti '-'

;JI T1 •-<

;j;jp Ti w

:J; J!Ju;ji TI u

IJ

!J!

FORM I SV-TIC

000047


EPA £AM?LZ NC

Lab Name: Tr.r.TNQIS EPA Contract: Q97125QQQ7X103

Lab Code: SPFLD Case No. : EEJEIM SAS No . : SDG No.: D19966


Sample wt/vol: 3.Q.3 (g/mL) G




GPC Cleanup: (Y/N) Y pH: 7.8


Lab File ID: C1204W03






108-95-2 Phenol111-44-4 bis (2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1, 4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis (2-Chloroisopropyl) Ether.106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine_67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2 , 4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane_120-33-2 2,4-Dichlorophenol120-32-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2, 4 , 6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dime thy Iphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitrotoluene

11001100110011001100110011001100110011001100110011001100110011005300110011001100650110011001100180011001100530011005300110011001100

FORM I SV-1

Q

;u:u;u;u!U;u;ui M, w

!U;u!U:u!U;u:u;u:u;u:u;uu:u;u:ut

:u;uIU;u;uiu;u;u

000048

1CSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

SrA SAM? 12

Lab Name: ILLINOIS EPA Contract: Q97125QQQ7X103

Lao Code: SPFLD Case No.: REFTNB SAS No.: SDG No.:




X Moisture: not dec. 4p dec.


GPC Cleanup: (Y/N) £ pH: 7.B


Lab File ID: C1204WQ3





CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg)

99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitro toluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether_118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3*-Dichlorobenzidine56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Be nzo(b) Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo(a)Pyrene193-33-5 Indeno(l,2,3-cd)Pyrene53-70-3 DibenzC a, h) Anthracene191-24-2 Benzo(g,h,i)Perylene

530011005300530011001100110011001100530053001100110011005300880liOO11001000710110022001100110011001100110011001100110011001100

Q

:u!U1U:u!U!U!U:uI TlI ^<

:u;u:u;u;u;u!J;u:uu;j:u:u;u;u:u:u:u!Uiu:u;uiu


FORM I SV-2 OC0049

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS


ErA 3AM?12 N.

X103

Lab Code: SPFLD


Sample wt/vol: 30.3 (g/mL) G





Number TICs found: ,19




Lab File ID: C12Q4WQ3






CAS NUMBER

1.2.3.4.5.6.7.3.9.10.11.12.13.14.15.IS.17.18.19.

(

[ COMPOUND NAME

1 UNKNOWN ALIP.J UNKNOWN! UNKNOWN1 UN KNOWN; UNKNOWN ALIP.1 UNKNOWNi UNKNOWN; UN KNOWN ALIP.; UN KNOWN1 UNKNOWN ALIP.[UNKNOWN; UNKNOWN! UNKNOWN ALIP.! UN KNOWN! UNKNOWN[UNKNOWN ALIP.[UNKNOWN! UNKNOWN[UNKNOWN ALIP.I

HYDROCARBON

HYDROCARBON

HYDROCARBON

HYDROCARBON

HYDROCARBON

HYDROCARBON

HYDROCARBON

RT

27.8628.0928.1728.4928.7628.9729.3929.6129.9130.4730.7730.9631.4231.6631.7932.5432.9133.5133.74

EST. CONC.

3300100012001800440095080050002200290017001700260080023001300410023003700

i •— .j

; Q

!J!J: Ji Ti tJ

i Ti »-'

, u

: J: j; J: j!J;j;J;j;J!J;j[J;j

FORM I SV-TIC

000050

/o 7 ~ =.- •/ w ' . .2 -

SEMIVOLATILE ORGANiCS ARAL*513 DATA SHE2T

Lab Name: Jt.T.TNnrs EPA Contract: Q97125QQQ7X104

Code: SPFLD Case No.: REFINE SAS No.: SDG No.: D19956


Sample vrt/vol: 30.2 (g/mL)

Level: ( low/med) LOW


Extraction: ( SepF/Cont/Sonc )

GfJ Cleanup: ( Y / N ) Y. _ pH:

CAS NO. COMPOUND



8.6





CONCENTRATION UNITS:(ug/L or ug/Kg)

108-95-2 Phenol111-44-4 bis (2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-I'ichlorobenzene95-48-7 2-Methylphenol

60-1 bis(2-Chloroisopropyl)Ethei44-5 4-Methylphenol

621-64-7 N-Nitroso-Di-n-Propylamine_67-72-1 Hexachloroethane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane.120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene.106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene_88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitrotoluene

820820820820820820820820820820820820820820820820400082082082082082082082082082082040008204000820820820

Q

!U!UiU;u;u:u;u:u:u:u!U:u!U:u;u;u!U;u:uIU:u;u:u!UiU;u:u:u•!U!U;u!U

FORM I SV-1 1/87 ?. = •

000051

SEMIVOLATILZ ORGANICS ANALYSIS DATA SHZZTS?A SAM?12 .r

Lab Name: ILLINOIS EPAX104

Lab Code: SPFLD


Sample wt/vol: 30.2 (g/mL) £


% Moisture: not dec. 2Q dec.

Extraction: (SepF/Cont/Sonc) S_QUC

GPC Cleanup: (Y/N) X pH: 8.6


Case No.: EEEIHE SAS No.: SDG No.: D19266

Lab Sample ID: D1996S1






CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) US/KG

99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol.100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-284-66-27005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene

•2,4-Dinitrotoluene.-Diethylphthalate

•Pentachlorophenol.-Phenanthrene-Anthracene

100-10-6 4-Nitroaniline534-52-1 4, 6-Dinitro-2-Methy 1 phenol.86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether_118-74-1 Hexachlorobenzene87-86-585-01-8120-12-784-74-2 Di-n-Butylphthalate.206-44-0 Fluoranthene129-00-085-68-791-94-156-55-3218-01-9117-81-7117-84-0

-Pyrene-Butylbenzylphthalate-3,3'-Dichlorobenzidine.-Benzo(a)Anthracene-Chrysene.bis(2-Ethylhexyl)Phthalate_Di-n-Octyl Phthalate

205-99-2 Benzo(b)Fluoranthene .207-08-9 Benzo (k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno( 1,2,3-cd)Pyrene53-70-3 Dibenzt a, h) Anthracene191-24-2 Benzo( g,h, i )Perylene

4000820400040008208208208208204000400082082082040008208208208201808201600820820820820820820820820820820

Q

;u;u:u;u;u:u;u;u;u;u;u;u!UIU:u:u:uIU!U;j!Uiu!U:u!U!U:u:u:uiu:u:u

(I) - Cannot be separated from Diphenylamine

FORM I SV-2 000052



T 5 Code: SPFLD Case No.:






GPC Cleanup: (Y/N) Y_ pH: 8.6

Number TICs found: I


SAS No. : SDG No. : D19966

Lab Sample ID: D1996fll







CAS NUMBER

1.2.3.4.5. 100-52-76.7.

1

i COMPOUND NAME

[UNKNOWN ALIP.; UNKNOWN ALIP..UNKNOWN1 UN KNOWN; BENZALDEHYDE; UN KNOWN[UNKNOWN ALIP.i

HYDROCARBONHYDROCARBON

HYDROCARBON

RT

8.428,599.5710.2210.5511.1021.77

EST. CONC.

810710310013001800690570

t

i Q

!JU! BAJ! AJ:J;AJ! J

FORM I SV-TIC

000053

1/87 p.e

IBSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: Tf.r.TNQTS EPA Contract: 097125QQQ7X105


Matrix: (soil/water) SOIL.

Sample wt/vol: 30.J



(g/mL)

dec.





Extraction: (SepF/Cont/Sonc) SO.UC





108-95-2 Phenol111-44-4 bis (2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis(2-Chloroisopropyl)Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis (2-Chloroethoxy) Me thane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dime thy Iphthalate208-96-8 Acenaphthylene606-20-2 2, 6-Dinitrotoluene

760760760760760760760760760760760760760760760760370076076076076076076076076076076037007603700760760760

FORM I SV-1

;u;u;u;u!U:u:u;u:u!U; u:u:u:u;u:u;u;u;u;u!U:u;u:u!U:ui u!U!U;u;u:u;u

0000541/5'

SEMI VOLATILE ORGAN ICS ANALYSIS DATA SHZST

Lab Name: ILLINOIS EPA Contract: 0971250QQ7X105

> Code: SPFLT) Case No.: REFINE SAS No.: SDG No.: D19966

Matrix: (eoil/water) SQTL






Lab Sample ID: D19966K






CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) Q

99-09-283-32-951-28 5100-02-7132-64-9121-14-284-66-27005 72 3 - -86-73-7100-10-6R04_CO_ 1JO^l lj£ 1PC QA (S_

i ni -c.R-'s _.iw i. — sJO — O1 1 R 7d- 11 1O / n — I87 86-5-QC A 1 _fl _.acjui — a —120-12-734-74-2206-44-0129-00-085-68 7 —91-94-1 -56-55-3218-01-9i i 7 — a i 7 .

117-84-0205-99-2207-08 950-32-8193-39-553-70-3 — —191-24-2

3-Ni troanilineAcenaphthene

4-NitrophenolDibenzofuran2 , 4-Dinitro tolueneDiethylphthalate

Fluorene4 -Ni troaniline, D— JJinj.ur'o— £.— ne iny xpneno ±M i. LruBuu ipricny io-uunc ^ j. i

— oromopneny j. — pnen v j.e uner— — Hexach 1 orobenzene __

Pentachlorophenol— r'nenancnrene ... ......AnthraceneDi-n-ButylphthalateFluoranthenePyrene

Benzo( a ) AnthraceneChryaeneV>1a/C> tTi-V<w1 Viavtrl ^PVit-V>a 1 a+-o

Di-n-Octyl Phthalate

Ben2O( k )FluorantheneBenzo( a )PyreneTndeno(l 2 3-cd)Pyrene

— Dibenzfa h)AnthraceneRen2:o(g,h i)Perylene

3700760370037007607607607607603700-3700o / uu7fiO7 er\/ ou7AOf o\l37007fin/ Dv

76076019019076015007607607 (3 AI DVJ

760760760760760760760

i

1 U;U'U;Um!U:u1 ni ^:u;U1 ni Ui n1 n( Ui rii u!UP MI U

!U'U! J! J!U!U:u:ui ni u;U:u;u:u;U!U;Ut

m |


FORM I SV-2 000055 1/87 He-

IFSEMIVCLATILE ORGANICS ANALYSIS DATA SHEET


i?A 5AMP1Z

Lab Name: Tr.LINQIS EPAX105

Lab Code: SPFLD







Number TICs found: Q.


Case No. : REFINE SAS No. : SDG No. : D-19_9_£fi


Lab File ID: C12Q2WG4





CONCENTRATION UNITS(ug/L or ug/Kg)

CAS NUMBER

1.2.3.4.5.6.7.8.

l

i COMPOUND NAME

; UNKNOWNi UNKNOWN! UNKNOWN1 UNKNOWN PHTHALATE1CHLORDANE ISOMERICHLORDANE ISOMER;CHLORDANE ISOMER; UNKNOWN ALIP. HYDROCARBON

RT

9.5410.1911.0723.7526.6927.0127.0933.87

EST. CONC.

14004806105609201000410590

Q

BAJBAJBAJTuJuT

rJ

FORM I SV-TIC

0000561/5-

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: ILLINOIS EPA Contract: 0971250007X106

Code: SJPFLD Case No.: REPINE SAS No.: SDG No.: D19966





Lab File ID: C12Q2WQR

Moisture: not dec. 24 dec.



Date Received: 11/14/9 ]_

Date Extracted: 11/15/9]




108-95-2 Phenol111-44-4 bis (2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1, 3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-43-7 2-Methylphenol108-60-1 bis(2-Chloroisopropyl)Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroethane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Me thane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol ,__91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene ,606-20-2 2,6-Dinitrotoluene

870870870870870870870870870870870870870870870870420087087087087087087087087087087042008704200870870870

FORM I SV-1

Q

!U!U:u!U!U!U:u;u;u:u!U1U!U!UI U!U:u:u;u:ui u!U;u:u:u!U;u:u:u:u;u;u;u

0000571/87 Re


EPA SAMPLE

Lab Name: ILLINOIS EPA Contract: 097125QQQ7X106



Sample wt/vol: 30 -Q (g/mL) Q



Extraction: (SepF/Cont/Sonc) SONC

GPC Cleanup: (Y/N) £ pH: 6.7








99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2, 4-Dini trophenol100-02-7 4-Ni trophenol132-64-9 Dibenzofuran121-14-2 2, 4-Dinitrotoluene

70C5-72-3 4-Chlorophenyl-phenyletner_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4, 6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene

206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo( a) Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate.117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b) Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz(a,h

24-2 Benzo(g,h,:

4200870420042008708708708708704200420087087087042001000870870120011008701700870510870870470410430870870870

Q

u:u:u;u;u:u

;u;ui r Ti ^:u;u!U!Ui

iu;u

:u!U!U!J!UiUiJ!J;j!U:u!U


FORM I SV-2 000058

IrSEMI VOLATILE ORGANICS" ANALYSIS DATA SHEET



L Code: SPFLD Case No.: REFINE

X106Contract: 0971250007

SAS No. : SDG No. : D19966




% Mois*«ure: not dec. 24 dec.



Number TICs found: Z


Lab File ID: C12Q2WQfi





CONCENTRATION UNITS:(ug/L or ug/Kg) US/KG

CAS NUMBER

1.2.3.4.cw .

6.7. 205-82-3

l

! COMPOUND NAME

! UN KNOWN ALIP. HYDROCARBON; UNKNOWN! UNKNOWN! UN KNOWN[UNKNOWN PHTHALATE1 UNKNOWN ALIP. HYDROCARBON! BEN ZO [ J ] FLUORANTHENE

RT

8.599.5510.2011.0923.7733.8934.81

EST. CONC.

52020004906706201300530

l

! Q

: j!BAJ!BAJ: BAJ; J;BJ;j

FORM I SV-TIC 1/87 p.e

000059


EPA 3AT.PL2 NC

Lab Name: T T . T . T N O T S EPA Contract: Q97125QQO7X107






Extraction: (SepF/Cont/Sonc) SQ_t!£


Lab Sample ID: D19966S

Lab File ID: C1202WOfi






108-95-2 Phenol111-44-4 bis (2-Chloroe thy 1) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1, 4-Bichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis(2-Chloroisopropyl)Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis (2-Chloroethoxy) Me thane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dime thy Iphthalate208-96-8 Acenaphthylene606-20-2 ' 2,6-Dinitrotoluene

790790790790790790790790790790790790790790790790380079079079079079079079079079079038007903800790790790

Q

:u!U;u!U:u!U;u;u;u;u:u!U:u:u1U;u:u;u!U:u:u;u;u:u;u;u;u;u;u:u;u:u;u

FORM I SV-1 1/67

OOC060

SEMIVOLATILE ORGAN ICS ANALYSIS DATA 5HZ2T

Lab Name: TT.LINQIS EPA

I C.-de: SPFLD Case No.: REPINE

X107Contract: 0971250007

SAS No.: SDG No.: D199fifi





Extraction: (SepF/Cont/Sonc) SQJI£


CAS NO. COMPOUND








99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitro toluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenyl ether.86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol.86-30-6 N-Nitrosodiphenylamine (1).101-55-3 4-Bromophenyl-phenyiether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3*-Dichlorobenzidine56-55-3 Benzo( a) Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate.117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b)Fluoranthene207-08-9 Benzo(k) Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indenod, 2,3-cd) Pyrene53-70-3 Dibenz( a, h) Anthracene191-24-2 Benzo(g,h,i)Perylene

3800790380038007907907907907903800380079079079038007907907907907907901600790790790790790790790790790790

Q

!U!U,'U;u;u;u;u:u:u;u:u:u;u:u;u!U;u:u:u!U:u;u:u;u:u!U;u!U!U:u!U!U

(1)"- Cannot be separated from Diphenylamine

FORM I SV-: 000061 1/S7 ?.e

=ah!VOLATILE ORGAN ICS ANALYSIS DATA S"ri2ETTENTATIVELY IDENTIFIED COMPOUNDS

X107Lab Name: TT.LINQTS EPA Contract: Q97125QQQ7

Lab Code: 5PFLD Case No.: REFINE SAS No.: SDG No.: D19966




% Moisture: not dec. Ifi dec.



Number TICs found:








CAS NUMBER

1.2.3.4.5.

t

,' COMPOUND NAME

i UNKNOWN ALIP. HYDROCARBON1 UNKNOWN ALIP. HYDROCARBON; UNKNOWN! UNKNOWN[UNKNOWN PHTHALATE

RT

8.428.609.5711.1023.79

EST. CONC. i Q

570 iJ470 ! J2000 ;J610 : j520 ; J

FORM I SV-TIC 1/S7 Rev.

000062

SEMIVOLATIL2 ORGANICS ANALYSIS DATA SHEET

Lab Name: TT.LINQIS EPAX108

I Code: SPFLD


Sample wt/vol: 30.Q (g/mL) Q





Contract: Q97125QQQ7 ;

Case No.: REPINE SAS No.: SDG No.: D199fifi







CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/~ or ug/Kg) UG/KG

108-95-2 Phenol111-44-4 bis(2-Chloroethyl)Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis (2-Chloroisopropyl) Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitrotoluene

810810810810810810810810810810810810810810810810400081081081081081081081081081081040008104000810810810

Q

!U;u!U;u;u;u;u:u;u!U;u!UIU:u;u!U;u;u:u:uIU:u:u!U:u:u:u!U:u:uI U:u:u

FORM I SV-1

000063l/S'

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET£rA NO.


Lab Code: SPFLD







Contract: Q97125QQQ7

Case No. : REFINE SAS No. : SDG No. :







CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) DG/KQ

99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran

84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate.117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo (b)Fluoranthene207-08-9 Benzo (k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz( a, h) Anthracene

24-2 BensoCg.h, i )Perylene

400081040004000810810810810810400040008108108104000930810810120012008101600810600810810500510540430810500

Q

:uIU;u;u;u;u:u:u!U;u:u;u!U!U!Ui

;u!UI

iT!U:u!U!J:u;u

!J:u


FORM I SV-2 O00064 1/3" =ev.



SAMPLE SO.


. o Code: SPFLD




3» Moisture: not dec. 19 dec.



Number TICs found: a


Case No.: REFINq SAS No.: SDG No.: D19966








CAS NUMBER

1.2.3.4.5.6.7. 205-82-38.

l

i COMPOUND NAME

; UNKNOWN ALIP. HYDROCARBON! UNKNOWN! UN KNOWN1 UNKNOWN[UNKNOWN PHTHALATE! UNKNOWN ALIP. HYDROCARBONi BENZO [ J ] FLUORANTHENEI UNKNOWN ALIP. HYDROCARBONi

RT

8.609.5710.2211.1023.7933.9134.8437.36

EST. CONG.

4401800570620530

1400730850

l

: Q;j!BAJ!BAJ!BAJ!J;j!J!J<

FORM I SV-TIC 1/87

000065

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEETir A iAXr _£.


. a Code: SPFLD






GPC Cleanup: (Y/N) X pH:




Lab File ID: C1202WOft

7.3






108-95-2 Phenol111-44-4 bis(2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis (2-Chloroisopropyl) Ether.106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine_67-72-1 Hexachloroethane^98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane_120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene •106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitro toluene

790790790790790790790790790790790790790790790790380079079079079079079079079079079038007903800790790790

Q

!U;u;u;u:u!U;u:u!U:u!U;u;u!U:u:uIU;u:u:u:u!U:u;u:u

!U;u:u;u;u!U

FORM I SV-1 1/87 Re-

000066

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEETirA SArtrLS SO



Matrix: (aoil/water) SOIL

Sample wt/vcl: 30.0 (g/mL) fi


% Moisture: not dec. Lfi dec.




Lab File ID: C1202WQR






99-09-2 3-Nitroaniline '83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether_118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate.117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b)Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo (a) Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz(a,h)Anthracene191-24-2 Benso(g,h,i)Perylene

3800790380038007907907907907903800380079079079038007907907907907907901600790790790790790790790790790790

Q

;u:uiu;u!U!U;uiu;u:u;uiUIU:u:u!U:uiU;u:u!U!U:u:u!U:u!U:u!U:u;u!U


FORM I SV-2 000067 i//p-7

SZHIVOLATILE ORGANICS ANALYSIS DATA STENTATIVELY IDENTIFIED COMPOUNDS

Lab Name: TLLINQIS EPAX109

T i Code: SPFLD




% Moisture: not dec. 16, dec.


GPC Cleanup: ( Y / N ) I pH:

Number TICs found:

Contract: Q97125QOO7

Case No. : REFINE SAS No. : SDG No. : D19966








1

CAS NUMBER

1.2.3.4.5.

11

l

! UNKNOWN! UNKNOWN! UNKNOWN! UN KNOWN! UNKNOWN

COMPOUND NAME

ALIP. HYDROCARBON

PHTHALATE

RT

8.609.5710.2211.1023.79

EST. CONC.

5902100870690510

; Q

!JIBAJiBAJ;BAJ;j

FORM I SV-TIC 1/87 P.ev

000068

IBIIVOLATILE ORGAfllCS ANALYSIS DATA SHEET

EPA SAMPLE SO,

Lab Name: Tr r .TMQTS EPA Contract: 0971250007X110















108-95-2 Phenol111-44-4 bis(2-Chloroethyl)Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1, 4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis(2-Chloroisopropyl)Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol

65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichiorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitro toluene

850850850850850850850850850850850850850850850850410085085085085085085085085085085041008504100850850850

FORM I SV-1

Q

:u:u;u;u;u!U:u!U:u:u;u;u:u:u!U;u:u:u;u!U!U;u:u:u:u:u:u!U:u:u!U!U:u

1/37 Rev,

000069


SPA SAHFL3 NO,

Lab Name: ILLINOIS RPAX110

o Code: SPFLD



Leve1: (low/med) LOW


extraction: (SepF/Cont/Sonc) SQNC

GPC Cleanup: (Y/N) Y__ pH: 7.Q


Case No.: REFIMg SAS No.: SDG No.: £19966







CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) Q

-3-Nitroaniline.-Acenaphthene

99-09-283-32-951-28-5 2,4-Dini trophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-284-66-2

2,4-Dinitrotoluene.Diethylphthalate

72-3 4-Chl or ophenyl-phenyl ether.86-73-7 Fluorene100-10-6

2-1L-Nitroaniline.

-Anthracene-Di-n-Butylphthalate.-Fluoranthene-Pyrene

4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1).101-55-3 4-Bromophenyl-phenylether_118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-784-74-2206-44-0129-00-085-68-791-94-156-55-3218-01-9117-81-7117-84-0205-99-2207-08-950-32-8193-39-5

•Butylbenzylphthalate-3,3*-Dichlorobenzidine_- Benzo(a)Anthracene-Chrysene-bie(2-]-Di-n-Octyl Phthalate.-Benzo(b)Fluoranthene.-Benzo(k)Fluoranthene.-Benzo(a)Pyrene

53-70-3-191-24-2-

-Indeno(1,2,3-cd)Pyrene.-Dibenz(a,h)Anthracene-Benzo(g,h,i)Perylene

410085041004100850850850850

41004100

85041008508508502101808501700850850850850850850850850850850

!U!U:u:u;u;u:u:u

iu!U;u:u;u!J

iu:u:uiuI M

:u:u:u:u:u:u!U


FORM I SV-2000070

1/87 Re-



EPA SAMPLE SO

Lab Name: T T.LI NO IS EPAX110

Lab Code: SPFLD





Extraction: (SepF/Cont/Sonc) SQHC

GPC Cleanup: (Y/N) Y__ pH: 7.Q



Case No.: REFtN% SAS No. : SDG No. : D199S6

Lab Sample ID: D19967]







CAS NUMBER

1.2.3.4.5.6.7.

i COMPOUND NAME

1 UNKNOWN ALIP. HYDROCARBON! UNKNOWN! UNKNOWN[UNKNOWN PHTHALATE1 UN KNOWN! UNKNOWN ALIP. HYDROCARBON.UNKNOWN ALIP. HYDROCARBON

RT

8.609.5910.2423.8033.1933.9437.39

EST. CONC.

4901800670520940800950

rI

! Q

!J!BAJ!BAJ; j!J; j; J

FORM I SV-TIC000071

1/87 Re-


EPA SAhPLS MO.

Lab Name: TT.TJNQIS SPA Contract: Q97125QQQ7Xlll

SDG No.: D19_966. b Code: SPFLD Case No.: REPINff SAS No.:

Matrix: (soil/water) SOIL Lab Sample ID: D199682

Sample wt/vol: 30-7 (g/mL) Q Lab File ID: C1203W14

Level: (low/med) LOW Date Received: 11/15/91

% Moisture: not dec. 15. dec. Date Extracted: 11/15/91


GPC Cleanup: (Y/N)

SQNC

7.2




108-95-2 Phenol111-44-4 bis(2-Chloroethyl)Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis(2-Chloroisopropyl )Ether106---? f 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroethane_98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenc;65-85-0 Benzoic Acid111-91-1 bia(2-Chloroethoxy)Me thane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol '95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitro toluene

760760760760760760760760760760760760760760760760370076076076076076076076076076076037007603700760760760

FORM I SV-1

Q

:u!U!U!U;u!U!U!U:u:u:u:u;u!U!U:uiu:u:u:uiu:u!U:u!U:uiu:u!U!U!U!U!U

000072

SSMIVOLATILE ORGANICS ANALYSIS DATA SHZST

Lab Name: TLLINQIS EPA Contract: Q97125QQQ7Xlll

Lab Code: SPFLD Case No.: REPINE SAS No.:


Sample wt/vol: 30.7 (g/nxL) G



SDG No.: D19966










99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo( a) Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b) Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo(a)Pyrene___193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibens(a,h) Anthracene191-24-2 Benzo(g,h, i)Perylene

3700760370037007607607607607603700370076076076037001300300760140012007601500760540760320480450500450760460

Q

:u;u!U:u!U;u;u!U:u;u;u!U!U:u!U

!UiU;u!J:u!J!J!J!J!J!U!J


FORM I SV-2 000073 1/87 ?.-•

SEMIVOLATILS ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

Lab Name: ILLINQIg EPA Contract: Q97125QQQ7Xlll

f b Code: SPFLD Case No.: REFINE SAS No.: SDG No.:


Sample wt/vol: 30.7 (g/mL) fi





Number TICs found:







CONCENTRATION UNITS:(ug/L or ug/Kg) UQ/KG

CAS NUMBER

1.2.3.4. 100-52-75.6.7.8. 56-55-39. 192-97-2

l

! COMPOUND NAME

! UNKNOWN ALIP. HYDROCARBONi UNKNOWN! UNKNOWN! BEN Z ALDEHYDE! UNKNOWN! UNKNOWN PHTHALATE; UNKNOWN PHTHALATEiBENZC A] ANTHRACENE!BENZO[E]PYRENE1i

RT

8.429.5510.2210.5511.1023.7730.1730.2134.79

EST. CONC.

420150013004805103807501000580

l

i Q!J:BAJiAJ!J!AJ; J!J: j;j!

FORM I SV-TIC

0000741/87 F.e

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEETS?A SAJlr

Lab Name: ILLINOIS EPA Contract: 097125QQQ7X112

Case No.: REFINE SAS No.:Lab Code: SPFLD

Matrix: (soil/water) S


Level: (low/mod) LOW




SDG No . : P19966








108-95-2 Phenol111-44-4 bis(2-Chloroethyl)Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis (2-Chloroisopropyl) Ether,106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane_120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitro toluene

830830830830830830830830830830830830830830830830400083083083063083083083029083083040008304000830830830

Q

;u!U:u;u:u:u;u:u:ui u:u:u!U;u;u!U;u:u:u:uu:u:u:uuiu;u!U:u:u;u;u:u

FORM I SV-1 1/37 Re-

000075

SEMIVOLATILE ORGANICS ANALYSIS DATA 3KZSTSArtrLS NO,


Code: SPFLD Case No.: REFINE SAS No.: SDG No.: D199fifi


Sample wt/vol: 30.2 (g/mL) G _


% Moisture: not dec. 21 dec. _


GPC Cleanup: (Y/N) Y. _ pH:

CAS NO. COMPOUND


Lab File ID: C12Q3Wlfi

Date Received: 11/15/qi






FORM I SV-2

000076

Q

83-32-9C -1 _OO R3 i. 4,0 3 — —

100-02-7

121-14-2

j* k _fpc 70 7 _

100 10 6 -

PC Of) C_

101-55-3--118-74-1P7 PC_K,

85-01-8120-12-784-74-2-206-44-0129-00-085-68 7 — —9i_94_i56-55-3O 1 p A 1 _Q ___

m pi _7

m-84-0205-99-29H7 OP. Q*_u i uo y50-32-8- —193-39-553-70 3 -191-24-2

— N i troan i .L ine _Acenaphthene

T *i — uini tropneno -L .4-Nitrophenol

— — — jjinenzoiuraii2 T 4-Dinitro toluene

— — — T^^+-Vnr1 i**Vs V^ a 1 A +• a— — — ijie tny -LpriLnaxa iie_ .

— r j.uorene4-Ni troani line

Hexachlorobenzene— Pentachlorophenol. ... .

PhenanthreneAnthraceneDi-n-ButylphthalateFluor an thenePyrene

Benzo ( a ) Anthracene

hi s( 9-Ft-hvl hf»w1 tPhthal at-pDi-n-Octvl Phthalate

— — nenzo K ) p luaraniLnerieBenzo ( a ) PyreneIndeno (1,2, 3-cd ) PyreneDibenz(a h)AnthraceneBenzo ( g , h t i )Pery lene

40001500400040009608308308301400400040008308308304000100002000830

1100067002101700830470083083048003500440036008303400

iu

iu;uiu:u;uiu!U;u;u:u!U

IT:u

!J!U!U

iu!U1

iu111

1/87 Rev.



EPA SA*?L3 NC.

Lab Name: TT.T .TNOTS EPAX112

Lab Code: SPFLD


Sample wt/vol: 30.2 (g/mL) fi




GPC Cleanup: (Y/N) Y_ PH:

Number TICa found: _12


Case No.: REFINE SAS No.: SDG No.: TM9966








CAS NUMBER

1.2.3.4.5. 613-12-76.7. 84-65-18. 243-42-59.10.11.12.13.14.15.16.17.18.19.

1

! COMPOUND NAME

! UNKNOWN ALIP. HYDROCARBON'.UNKNOWN ALIP. HYDROCARBON,' UNKNOWN ALIP. HYDROCARBONI UNKNOWN; ANTHRACENE, 2-METHYL-; UNKNOWN ALIP. HYDROCARBON1 9 , 10-ANTHRACENEDIONE;BENZO[B]NAPHTHO[2,3-D]FURAN1 UNKNOWN PNA; UNKNOWN PNAI UNKNOWN PNA[UNKNOWN PNA[UNKNOWN PNA! UNKNOWN PNA[UNKNOWN PNA[UNKNOWN PNA[UNKNOWN PNA! UNKNOWN! UNKNOWN11 ___—_^_— _ _^__^____^_^_^__

RT

11.3211.7513.1523.7924.5925.0225.3627.2927.5927.8728.0228.1428.4629.2229.5129.5929.6429.6429.76

EST. CONC.

140004000110002200150011001900110094027001100110064012001800160015008001500

iItI

I —I —

!J!J!Ju;j;Ji 7, o

;J; J:J;j:J!J!J!J[JU!J;j1

Q

FORM I SV-TIC

0000771/87 Rev.


SPA SAMP12 HC

Lab Name: TLLINQTS EPA Contract: Q97125QQQ7X113

L j Code: SPFLD Case No.: REFINE SAS No.: SDG No.: E19966






GPC Cleanup: (Y/N) Y, pH: 7.6


Lab File ID: C12Q3Wifi






108-95-2 Phenol111-44-4 bis(2-Chloroethyl)Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis(2-Chloroisopropyl) Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzole Acid111-91-1 bis(2-Chloroethoxy)Me thane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitrotoluene

770770770770770770770770770770770770770770770770370077077077077077077077077077077037007703700770770770

Q

!U!U;u!U;u;u!U!U;u;u:u;u;u:u:u:u:u:u:u:u!U!U:u!U!U:u!U:u!U:u:u:u:u

FORM I SV-1 1/87

00007R

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEETEFA SAMPLE NC .

Lab Name: TT.LTNQTS EPA Contract: Q97125QOQ7X113

Lab Code: SPFLD Case No. : REZLNE SAS No. : SDG No.: D19966


Sample wt/vol: 30-2 (g/mL)












99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Die thy Iphtha late7005-72-3 4-Chlorophenyl-phenylether86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol86-30-6 N-Nitrosodiphenylamine (1)101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo( a )Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b)Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo( a )Pyrene •193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz( a, h) Anthracene191-24-2 Benzo(g,h,i)Perylene

I_ _ - . _ __ - — i


3700770370037007707707707707703700370077077077037003107707703704107701500770190770770210170190770770770

Q

;u!U:u;u!U:u:u:u:u;u;u!U:u!U!U!J:u!U!J!J:u!U:u!J:u:uu!J!J:u;u:u

FORM I SV-2 000079 1/87 Rev.

IrSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET


£PA SO.

Lab Name: TLLINQTS SPA

1

X113

Code: SPFLD






GPC Cleanup: (Y/N) Y_ pH:

Number TICs found: S










CAS NUMBER

1.2.3.4. 100-52-75.6.

1

i COMPOUND NAME. _ i _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ ____

! UNKNOWN ALIP. HYDROCARBON! UNKNOWN[UNKNOWN! BENZALDEHYDEi UN KNOWN! UNKNOWN ALIP. HYDROCARBONi

RT___ — ___

8.599.5510.2010.5511.1021.75

EST. CONC.

42019001100420710610

i1

: Q!J:BAJ!AJ!J:AJ;Ji

FORM I SV-TIC 1/87 Rev

000080

SEKIVOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: EPAX114

Lab Code: SPFLD







Lab Sample ID: D1996fl5


Extraction:

GPC Cleanup:

CAS NO.

(SepF/Cont/Sonc) SQKC

(Y/N) Y__ pH: 7.5

COMPOUND






108-95-2 Phenol111-44-4 bis (2-Chloroe thy 1) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis (2-Chloroisopropyl) Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylajnine67-72-1 Hexachlo roe thane98-95-3 Nitrobenzene73-59-1 Isophorone38-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene83-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitrotoluene

800800800800800800800800800800800800800800800800390080080080080080080080080080080039008003900800300800

Q

!U:u:u:u:u:u!U:u:u;u;u:u!U;u!U:u;u;u:u;u:u:u!U:u;u!U:u!U:u:u:u;u;u

FORM I SV-1 i/e?

OQ0081


Lab Name: ILLINOIS EPA Contract: Q97i9finnn7X114

; . Code: SPFLD Case No.: REFINE SAS No.:







SDG No.:

Lab Sample ID:

Lab Pile ID: C12Q3WT7






99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 ButylbenzylDhthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo( a) Anthracene218-01-9 Chryeene117-81-7 biB(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b) Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz( a,h) Anthracene191-24-2 Benzo(g,h,i)Perylene

3900800390039008008008008008003900390080080080039001908008002802808001600800800800800800800800800800800

Q

:u:u:u!U:u:u;u:u;u:u;u!U!U!U!J:u:u!J!J

iu!U:u:u;u;u:u;u!U:u!U


FORM I SV-2

000082

SEMTVOLATILE ORGANICS ANALYSIS DATA SHZETTENTATIVELY IDENTIFIED COMPOUNDS

Lab Name: TLLTNQTS EPAX114

Lab Code: SPFLD







Number TICs found: 18










CAS NUMBER

1.2.3. 100-52-74.5.6.7.8.9.10.11.12.13.14.15.16.17.18.

i

i COMPOUND NAME

! UNKNOWN! UNKNOWN; BENZALDEHYDE! UNKNOWN ALIP.1 UNKNOWN ALIP.; UNKNOWN ALIP.; UNKNOWN ALIP.; UNKNOWN ALIP.; UNKNOWN ALIP.! UNKNOWN ALIP.; UNKNOWN ALIP.; UNKNOWN ALIP.[UNKNOWN ALIP.! UNKNOWN ALIP.1 UNKNOWN ALIP.[UNKNOWN ALIP.', UN KNOWN ALIP.[UNKNOWN ALIP.1

HYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBONHYDROCARBON

RT

9.5210.1910.5211.2513.1015.0016.3417.4517.7919.1420.4421.0421.6521.7222.8222.9423.9226.94

EST. CONC.

15006804804907304808003006207105904306401200510550470530

ll

! Q

!BAJ!AJ! Ju: J;ji 7i '-*

i J! J; J: J!J;j;ju;j!Ji -ri wi

FORM I SV-TIC

OOGC831/2"



I . Code: SPFLD Case No.: REPINE


Sample wt/vol: 30.2 (g/mL) G_



SAS No.:

X115

SDG No.: D19966





GPC Cleanup: (Y/N) Y__ pH:

CAS NO. COMPOUND






108-95-2 Phenol111-44-4 bis(2-Chloroethyl)Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol103-60-1 bis (2-Chloroisopropyl) Ether10S-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroethane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline .131-11-3 Diznethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitro toluene

830830830830830830830830630830330830830830830830400083083083055083083083032083083040008304000830830830

FORM I SV-1

Q

!U:u!U!U:u!U;u;u:u,u:ui u:u;u!U!U!U:u:u;u;j;u;u:u;J;u;u:u:u:u:u;u;u

1/87 p.e-

000084

SZMIVOLATILE ORGAN!CS ANALYSIS DATA SHEET

Lab Name: TLLINQTS KPAX115

Lab Code: SPFLD


Sample vrt/vol: 30.2 (g/mL) G


% Moiature: not dec. 21 dec.


GPC Cleanup: (Y/N) I pH: 7.5










99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether.86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4 , 6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-j118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene__85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine.56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhe117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo (b) Fluoranthene207-08-9 Benzo (k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene.53-70-3 Dibenz(a,h)Anthracene_191-24-2 Benzo(g,h, i)Perylene

4000100040004000660830830830100040004000830830830400084001700830930068008301700830390072083040002800370031008303000

Q

u

:u;j!U:u;uii:u:u!U!U:u!U

:ui

\J:u!U:uIT!J!U\J:J

u


FORM I SV-2

0000851/8"


Lab Name: ILLINOIS RPAX115

7 b Code: SPFLD



Leve1: (low/med) LOW





Contract: Q97125Q007

Case No. : REFTNE SAS No.: SDG No. : D19966

Lab Sample ID: Dl9968fi

Lab File ID: C1203Wifl

Date Received: ll/15/Q^

Date Extracted: 11/15/Q1




CAS NUMBER

1.2.3.4. 613-12-75.6. 612-94-27.8.9.10.11.12.13.14.15.16.17.18.19.20.

! COMPOUND NAME

1 UNKNOWN ALIP. HYDROCARBON1 UNKNOWN[UNKNOWN ALIP. HYDROCARBON; ANTHRACENE, 2-METHYL-; UNKNOWN ALIP. HYDROCARBON; NAPHTHALENE, 2-PHENYL-! UN KNOWN1 UNKNOWN PNA; UN KNOWN ALIP. HYDROCARBON! UNKNOWN; UNKNOWN PNA'.UNKNOWN PNA! UNKNOWN PNA1 UN KNOWN PNAi UNKNOWN PNA'.UNKNOWN PNA! UN KNOWN; UNKNOWN PNA! UN KNOWN! UNKNOWNi

RT

21.7423.7423.9224.5424.9925.2425.3125.9625.9927.2427.5427.8227.9728.1128.3628.4229.4629.5429.6229.71

EST. CONC.

23001500140012001000780120032072098079026001200990650620130013004001100_______^__^__

i Q

!J!J;j!J: J!J, <J1 . j

:J;j, T

. <J; J;J!J!J!J!J;j;j!Ji>

FORM I SV-TIC000086

1/3-

IDSEMIVOLATILE ORGANICS ANALYSIS DATA SHEET

fir A

Lab Name: TLf.TNQIS EPA Contract: Q97125QQQ7X116



Sample wt/vol: 30-8 (g/mL) G





CAS NO. COMPOUND

Lab Sample ID: D1996B7







108-95-2 Phenol111-44-4 bis(2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 b is (2-Chloroisopropyl) Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dime thy Iphthalate208-96-8 Acenaphthylene606-20-2 : 2,6-Dinitrotoluene

780780780780780780780780780780780780780780780780380078078078078078078078078078078038007803800780780780

Q

!U!U;u:uJ U!U:u;u!U:u:u:u:u!U;u;u!U!U!U;u!U:u!U:u!U;u:u!U:u;u:u!U:u

FORM I SV-1

000087

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEZT

Lab Name: TLLTNQIS EPAX116

' ) Code: SPFLD




% Moisture: not dec. Lfl dec.



Contract: Q971253QQ7 ;____

Case No.: REFTNB SAS No. : SDG No. : D19966



7.4






99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol_100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitro toluene.84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-]86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo( a) Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b)Fluoranthene207-08-9 BenzoCk) Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz( a, h) Anthracene191-24-2 Benzo(g,h, i)Perylene

38002003800380018078078076033038003800780780780380028001000780430040007801600780210078078014001300160012007801300

Q

uU;u;u;jIUc,u:u; j:u;u;u:u:u:u

!U

\S;u:u:u:SJU!Ufu

- Cannot be separated from Diphenylamine

FORM I SV-2 00008S 1/3-7 ? • = • - •

SIMIVOLATILE OMAN US ANALYSIS 2AIA SHUTTENTATIVELY IDENTIFIED COMPOUNDS

X116Lab Name: TTLTNOTS gPA

Lab Code: SPFLD


Sample wt/voi: 30.8 (g/mL) fi






Contract: 097125QQQ7 ;

Case No. : REFINE SAS No.: SDG No. :








CAS NUMBER

1.2.3. 100-52-74.5.6. 613-12-77. 610-48-08. 243-42-59.10. 238-84-611.12.13.14.15.16. 2C5-82-3

I

i COMPOUND NAME

! UNKNOWN; UNKNOWN! BENZALDEHYDE! UNKNOWN ALIP. HYDROCARBON! UNKNOWN ALIP. HYDROCARBON! ANTHRACENE , 2-METHYL-; ANTHRACENE, 1-METHYL-;BENZO[B]NAPHTHO[2,3-D]FURANI UNKNOWN PNA! 11H-BENZO[A]FLUORENE! UN KNOWN PNAi UN KNOWN PNA; UN KNOWN PNA! UN KNOWN PNA! UNKNOWN PNA1 BENZO [ J ] FLUORANTHENEtI _____^—^^— — — — — — — — _

RT

9.5010.1710.5221.6521.7224.4524.5427.2227.5227.8127.9728.0729.4429.5230.4134.74

EST. CONG.

93061043046078055070055057017008907005406806501700

ii Q -

; EAJ;AJ!J,'Ji Tt w

, u. T• ««

. TI <-*

; J!JiJ;ji TI •->

IJ

u!J

FORM I SV-TIC

0000891/57 ?.e-


EPA SAMPLE MO,

Lab Name: ILLINOIS SPA Contract: 097125QQQ7X117

L^J Code: SPFLD Case No.: R5FTNE SAS No.:





Extr'ttion: (SepF/Cont/Sonc) SONG

GPC Cleanup: (Y/N) Y. pH: B.2

SDG No.: D19966


Lab File ID: C12Q2W1Q





CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Kg) UG/KQ Q

108-95-2 Phenol111-44-4 bis (2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis (2-Chloroiscpropyl) Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroethane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis(2-Chloroethoxy)Methane120-83-2 2,4-Dichlorophenol '__120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chlorc-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene.88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate •208-96-8 Acenaphthylene606-20-2 '• 2,6-Dinitro toluene

870870870870870870870870870870870870870870£70F. 70420087087087087087087087087087087042008704200870870870

!U!U!U!U!U!U!U:u:ui •

;u:u;u!U:u:u:u!U:u:u:u!U:u:u:u;u;u;u;u:u;u:u

FORM I SV-11/87 Rev.

000090

SSMIVOLATILE ORGANI Co ANALYSIS DATA SHEET

Lab Name: TLLINQIS EPA Contract: Q97125QQQ7X117

Lab Code: SPFLD Case No.: REPINE SAS No.: SDG No.: D19966


Sample wt/vol: 30. Q (g/mL)



Extraction: ( SepF/Cont/Sonc )

GPC Cleanup: (Y/N) X _ pH:

Lab Sample ID: D19967?


S.2





CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or ug/Xg) UG/KG

99-09-2 3-Nitroaniline83-32-9 Acenaphthene51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_36-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenylether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene ;120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene_129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-99-2 Benzo(b)Fluoranthene207-08-9 Benzo(k)Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz( a, h) Anthracene191-24-2 Benzo(g,h, i)Perylene

1t - _- . - - - - —


4200870420042008708708708708704200420087087087042001908703702502508701700870870870870870870870870870870

Q

i U;ui U;u:u!U:u;u;u;u;ui u:u:u!U!J!U:u!JU!U!U:u:u!U:u;u!U:u!U:u!U

FORM I SV-2000091

SSMIVOLATILE ORGANICS ANALYSIS DATA SHEETTENTATIVELY IDENTIFIED COMPOUNDS

Lab Name: TLT.TMQTS EPAX117

J > Code: SPFLD


Sairple wt/vol: 30.Q (g/mL)




GPC Cleanup: (Y/N) X pH: B.2



Case No.: REZIHE SAS No. : SDG No. : D19966


Lab File ID: C12Q2WJQ






CAS NUMBER

1.2.3.4. 100-52-75.6.7.

I

i COMPOUND NAME

1 UNKNOWN ALIP. HYDROCARBON[UNKNOWN[UNKNOWN[BENZALDEHYDE1 UNKNOWN[UNKNOWN ALIP. HYDROCARBON[UNKNOWN PHTRALATE

RT

8.579.5410.2010.5511.0921.6723.75

EST. CONC.

53018001000580860570610

; Q

: J[BAJ[BAJ[J[BAJ: J:Ji

FORM I SV-TIC 1/87 Re

000092



Lab Code: SPFLD






GPC Cleanup: (Y/N) X pH: B.I

Contract: 09712SOOO7

Case No. : REFINE SAS No. : SDG No.: D19966








108-95-2 Phenol111-44-4 bis (2-Chloroethyl) Ether95-57-8 2-Chlorophenol541-73-1 1,3-Dichlorobenzene106-46-7 1,4-Dichlorobenzene100-51-6 Benzyl Alcohol95-50-1 1,2-Dichlorobenzene95-48-7 2-Methylphenol108-60-1 bis (2-Chloroiscpropyl) Ether106-44-5 4-Methylphenol621-64-7 N-Nitroso-Di-n-Propylamine67-72-1 Hexachloroe thane98-95-3 Nitrobenzene78-59-1 Isophorone88-75-5 2-Nitrophenol105-67-9 2,4-Dimethylphenol65-85-0 Benzoic Acid111-91-1 bis (2-Chloroethoxy) Me thane120-83-2 2,4-Dichlorophenol120-82-1 1,2,4-Trichlorobenzene91-20-3 Naphthalene106-47-8 4-Chloroaniline87-68-3 Hexachlorobutadiene59-50-7 4-Chloro-3-Methylphenol91-57-6 2-Methylnaphthalene77-47-4 Hexachlorocyclopentadiene88-06-2 2,4,6-Trichlorophenol95-95-4 2,4,5-Trichlorophenol91-58-7 2-Chloronaphthalene88-74-4 2-Nitroaniline131-11-3 Dimethylphthalate208-96-8 Acenaphthylene606-20-2 2,6-Dinitrotoluene

800800800800800800410800800800sooSCO800800800800390080080080080080080080080080080039008003900800800800

Q

!U;u1U:u!U:uu:u:u:ui r Ti i~:u:u:u:u:u;u;u;u;u!U!U:u:u;u;u:u!U:u;u!U:u!U

FORM I SV-1 1/87 R.ev.

000093

SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET* ^ A *^ *k ** ' •**•*•*• •» X«A* *i *»

Lab Name: ILLINOIS EPA Contract: Q9712SQQn7xiia

L j Code: SPFLIL Case No.: REFINE SAS No.: SDG No.: D19966




% Moisture: not dec. LZ dec.



Lab Sample ID: D1996?a







99-09-2 3-Nitroaniline83-32-9 Acenaphthene__51-28-5 2,4-Dinitrophenol100-02-7 4-Nitrophenol ,132-64-9 Dibenzofuran121-14-2 2,4-Dinitrotoluene84-66-2 Diethylphthalate7005-72-3 4-Chlorophenyl-phenylether_86-73-7 Fluorene100-10-6 4-Nitroaniline534-52-1 4,6-Dinitro-2-Methylphenol_86-30-6 N-Nitrosodiphenylamine (1)_101-55-3 4-Bromophenyl-phenyl ether118-74-1 Hexachlorobenzene87-86-5 Pentachlorophenol85-01-8 Phenanthrene120-12-7 Anthracene84-74-2 Di-n-Butylphthalate206-44-0 Fluoranthene129-00-0 Pyrene85-68-7 Butylbenzylphthalate91-94-1 3,3'-Dichlorobenzidine56-55-3 Benzo(a)Anthracene218-01-9 Chrysene117-81-7 bis(2-Ethylhexyl)Phthalate_117-84-0 Di-n-Octyl Phthalate205-39-2 Benzo(b) Fluoranthene207-08-9 Benzo(k) Fluoranthene50-32-8 Benzo(a)Pyrene193-39-5 Indeno(l,2,3-cd)Pyrene53-70-3 Dibenz( a,h)Anthracene191-24-2 Benzo(g,h, i)Perylene

3900800390039008008008008008003900390080080080039008201608009508708001600800410800800340340330300800800

Q

1U;u!U;u:u:u;u;u!U:u;u;u:u;u:uit!J:u\S:u:u:u!J:u;u!Ju!J!J!U:u


FORM I SV-2000094

1/8'


Lab Name: TT.MNQIS KPAxiia

Lab Code: SPFLD Case No. :








Contract: Q97125QOQ7

SAS No.: SDG No.: D1996S


Lab File ID: C12Q2WH

JLJ.






CAS

1.2.3.4.5.6.7.8.9.10.11.12.13.14.15.16.17.18.19.20.

NUMBER

26914-33-0

38380-02-841464-51-137680-73-273575-56-125429-29-251908-16-825429-29-256030-56-951908-16-825429-29-2

26601-64-9

-

COMPOUND NAME

UNKNOWNUNKNOWN ALIP. HYDROCARBONUNKNOWN PHTHALATEUNKNOWN ALIP. HYDROCARBON1,1 '-BIPHENYL, TETRACHLORO-UNKNOWN ALIP. HYDROCARBONUNKNOWN ALIP. HYDROCARBON1,1 '-BIPHENYL, 2, 2', 3, 4, 5' -P1,1 '-BIPHENYL, 2, 2', 3' ,4,5-P1,1'-BIPHENYL, 2,2',4,5,5'-P1,1'-BIPHENYL, 2,2',3,5,6-PEl.l'-BIPHENYL, PENTACHLORO-l.l'-BIPHENYL, 2, 2', 3, 4', 5, 5l.l'-BIPHENYL, PENTACHLORO-l.l'-BIPHENYL, 2, 2', 3, 4, 4', 61,1'-BIPHENYL, 2, 2', 3, 4', 5, 51 , 1 '-BIPHENYL, PENTACHLORO-UNKNOWN ALIP. HYDROCARBON1,1 '-BIPHENYL, HEXACHLORO-UNKNOWN ALIP. HYDROCARBON

RT

9.5521.7523.7723.9524.8725.0026.0126.2926.7426.8627.2127.5228.0128.0428.4628.5928.5928.7929.0429.66

- -

EST. CONC.

150015006107005705705207801700700540190084012008705106205501100600

n "*"

!BAJ! <JiJu; J; J, JT

J

!J;Ju; J!J!J Û;JU!J;Jj

FORM I SV-TIC

000095

1 /PTL/ w '

FESTICILE Ir.jANICS ANALYSIS DATA SHEET

V ' iA — o *

L=b Name: ILLINOI a EPA Contract: 0971250007

Lab Code: SPFLB. Case No.: BEEiHE SAS No.: SDG No . : Dl

Matrix: fsoil/water) SOIL






Lab Sample ID: Dl9967a

Lab File ID:






319-84-6 alpha-BHC319-65-7 beta-BHC319-86-8 delta-BHC58-89-9 gamma-BHC76-44-6 Heptachlcr309-00-2 Aldrin1024-57-3 Hept. epoxide959-93-8 Endcsulfan I6C -£7- 1 Dieldrin72-55-9 4, 4'-DDE72-20-8 Endr in33212-65-9 Sndosulfan II72-04-6 4,4'-DDI>1031-O^-? Endcsulfan sulfate.50-29-3 4, 4'-DDT72-43-5 Methoxychlor53494-70-5 Endrin ketone5103-71-9 a Ipha-Ch lordane5103-74-2 gamma-Chlordane8001-35-2 Toxaphene12674-11-2 Aroc lor-101611104-28-2 Aroclor-122111141-16-5 Aroclor-123253469-21-9 Aroclor-124212672-29-6 Aroc lor-124811097-69-1 Aroc lor-125411096-82-5 Aroc lor-1260

31313131313131316161-> ^C j.

61616161310•313103106303103103103103101700610

Q

:u:u:u:U:u:u•r

:U:U:u.u:U:'J!U;u!U:u:u:u:ui

:u

FORM I PEST 1/87 Rev

000096

IDPESTICIDE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE

X102Lab Name: ILLINOIS EPA Contract: 0971250007

Lab Code: SPFLD Case N o . : REELilE 3AS N o . : SE*j No.: 1-1 j






GPC Cleanup: (Y/N) Y__ pH: 7.3

CAS NO. COMPOUND


Lab File ID:






*^ « •— - .— , 4 {-*J la-is - b319 65 7-q i o fl C PO 1 .3 O C O

5g_cp_97 r-: ' A-O1 O t *i D

i-~>'">,; P."? "i Ji. t ~— ' ' • -•

959-93-360-57-17 c c Q _1 . -^-j y72-20-833213-65-9-7^-54-Si • j i ,i" ^x O 1 U ' oC ,'\ O Q -j^ J ^3 •;'7'" _ <1 •- P• — H-- •->

53-43:4 -''f-.? -£103-71-- --P 1 /I •! 7/'w i ' J O / H ô on 1 ^c; oCUU 1 JO £:

12674-11-2-11104-28-2-11141-16-5-CO^CQ_O1 _Q_OO1D3<il;3

12672-29-6-11097-69-1-11096-82-5-

alpha-BHCbeta-BHC

ffamma-BHC

Aldrin

Endosulfan IDie Idr inA A* .nnp"

Endr inEndosulfan II4.4'-DDD

< A* _rir1'T** . 4 L/L'l

"ndîn kp-t-orâ 1 p h a - C '•-. 1 c r T % n e

_,, . ,gamiTia Lnior'aaneT U— — i oxapneneAro'clor-1016Aroc lor- 1221Aroc lor- 1232

Aroc lor- 1248Aroc lor- 1254Aroc lor- 1260

29

:.9'__'->!

L". 929292957575757C.'JO 1

e -7

c;7

290290580280290280280280380570

T 'W

T)

;u1 1.1' rJ:U' r ;

:uTJ:u. r Ti_;

:U. ' T

r •

• : i

1 T.j

:u!U:u:u:u:u:u:u: j:u

FORM I PEST 1/37 Rev.

000097


L-o Name: ILLINOIS EPA

E?A SAMPLE NO

X103

Lab Code: SPFLD







. Contract: 0971 50007 ;

Case No.: BEZlNJa SAS No.: SDG No.:

Lab Sample ID: D1996BQ

Lab File ID:





CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/'L or ug/Kg) U_£ Q

1

319-84-631S-85-7319-86-8fâ AQ QOO Oi? C7

76-44-8-o f \ q n O - 9 -^ C\/~, A c; 7 -3 _iUi-H G / v-< —QCQ QR AJ533 C7~ Q" ' \ p. 7 1C-U 3 ' 17 *•< _ c. K Q _

7 •-, _ O f) M -' _ £. ' J ~ ~

33213-65-9-72-54-81 031-07-8 —50-29-372 43 553494-70-5-cipvo 71 Q_

5103-74-2 —Ann 1 TC. oOUU 1 O!j 4i

12674-11-2-11104-28-2-11141-16-5-53469-21-9-12672 29 611 A 07 J;Q •)IX'ôi— C3 1

1 1 j36-cll-.t, -

aloha-BHCbeta-EHCdelta-BHC

— samma— BH^Heptachlor

— Aldr inHept . epcxideT-< j -i f -r~ tnaosu LL an ir\ • i — Jjieiurin4 A ' nT'C1• 1JL/E. , . , , . , .

— ~EndrinEndosulfan II4.4'-DDDEndosulfan sulfate4.4'-DDTMethoxvchlorEndrin ketone

— alpha— Cnl ordanegairuna— Chlordane

— — ToxapneneAroclor-1016Aroc lor- 1221Aroc lor- 1232Aroc lor- 124TAroclor-12-a

_A *-,/-,/-, 1 /-.v»— 1 ***£ A— — t\L oc ior— L^^t^tAroc lor- 1260

'"' i

2823'"* Q

28232828555555555555552805523028057027028027027017 (,240550

i

:u:u', U:u:u: rj' F T

'U:u:u:u:u:u'U!U:U:u'U!U:U•U:u:u:u

:.]:ui

FOR-X I PEST000098

1/37 Rev.


Lab Name: ILLINOIS EPA Contract: 0971250007

v • ^ <A . -< t

Lab Code: £££LIL Case N o . : BJEZLNJi 3A3 N c . : 2LG No . : Hii-iE

(g/mL)


Sample wt/vol:






Lab File ID:

CAS NO. COMPOUND

Date Received: 11/15/9J.


Date Analysed: 11/30/91


CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Q

1

319 84 6- - -0 1 Q O C, "7oj.y oo iO 1 Q Or? Qj iy oo o58-89-97fi ^1/1 fl - -/ D t t t t~O

303-00-2•> /-i--. -1 c,7 •?J. \J <£ -i -J 1 O —n c o QR Qy 3 y y C O

60-57-1~ •-' c. e; q< _ .J.J y72-20-8^ QO 1 -3 CC, Qooi. 10 DO y7^ = " QI — o -» Oi n "5 1 n7 P _lU>-/ i U( Oc,f- 9Q QOv_/ â O — — —

72-43-5cq,jQ.i 7n cOo'ty'n » U O5103-71 9- --c-i 0^ — 7/1 — 9O X U o — / *t — <i —Rnrn ^c._9OUUJ. OO <i

12674-11-211104-28-211141-16-553469-21-912672-29-61 1 DQ7 £Q 1i .Luy / oy i1 1 ("iQrt R9 Cij. iuyo oî D

alpha-BHC_U04- _ RHP— De L.a Dfiv_ _ .

do 1 +• a PUPe 1 w3 cri^gamma-BHC

Aldr in

— n.nao&uiân iE ' ie ldr in

— ii d ' _nnr— H , t — L>L>L.

Endrin—Endosul fan I I— A A ' -nnr^— — *i . *4 — UUL

T-t , -| _£ 1 - 4 .

— 4 4 * PlFlT

Methoxvchlor"Endrin ketone

alpha— Chi ordane

xoxapneneAroc lor- 10 16Aroc lor- 1221Aroc lor- 1232Aroc lor- 1242Aroclor-1248

""HTOC -LOr~ 1^3*4

— Av»*-i/-»T/-iv» lOf in— r t r o c ± o i r J.^DU , , . , , .

2121O 1

2121

212141414141414141

21041

210210420210210210210210410410

; U:u:u1 n' U: U' U

:u:u! U:u:u:u:u

:u:u!U:uI U:u:u:u:ui

FORM I PE.-3T 1/87

000099


.Ô Name: ILLINOIS EPA

[FA SAMPLE NO.

X105

Lab Code: SPFLD


Sample wt/vol: 30.5 (g/mL) G.








Lab File ID:

Date Received: 11/14/9;\±c*f>

Date Extracted: l l /Lfc/91~f ~ ~




T 1 Q o A CLo 1 3 OS DQ i Q OC, 7

"3 1 L AS fiwj-J OC OJ- p pQ Q

'"'» y 1 a

309-00-2

C, C. Q Q D Q _3 o3 3O a£.•"* R7— •" -D u D ' i70 cc Q( ^. 3D 3

72-20-833213-65 9-T~- ^(A R/ 4. OS — oi f \ o i H7 — A —1 U o 1 wio —

50-29-372 43 5-

5103-71-95103-74-28001-35-212674-11-2111C4-28-211141-16-5

12672-29-611 r~lQ7 AQ 1iuy i oy— i—i i n Q R _ P O _ f ^ _1 1U3D — o£ <J~

a i i-,Ka nwr*aipna r>n\^V\a-(- a — RUfD e t a — on orê. 1 t- a -TaUPa e i u a — on

Pjjp• r , •,neptacmorAldrinHept . epoxideT-, i i f Ttnuosuiran i . ._r\ • i Jijie lar in. . > nriTT

EndrinEndosulfan II

T-. , -I f 1 JT 4.— tLnaosu 1 1 an suiraL,e4.4 '-DDTMethoxychlor

—Endrin ketonealpha-Chlordaneflamma-ChlordaneToxapheneAroclor-1016Aroc lor- 1221Aroc lor- 1232

•~ ™AlT*OC ior*" J. 4tf£

Aroc lor- 12 48~ f\ \j c i o r ^ -i. ^t o

A 1 1 OC/t— Arocior— IZDU

1 QLJ1 Qlj1 Qi y1 Q1C71 Q13

191 Q

1 QL3•30OOOQOO

3333COOOOflOO

3 '^190

•JOOO130012003901901901901 r\Aiyu190VjO \J

•3Qn

11 f 1, u1 f T, u1 T T

i r i. UI M

:U1 " 1. O. r.

1 M

i r i. U' U:ui ri. U-. r T

' U1 ; T; r ;, Uit

:U:u;u;u\ r T, U

!Ui CTi Ui r T

:

FORM I PEST 1/87 R*-,

000100

::;:z ORGANics ANALYSIS DATA SHEET

Lab Name: ILLINOIS £PA

Lab Code: SPFLD


Sample wt/vol: 30.6 fg/mL) Q


% Moisture: not dec. 2A dec.




Case No.: REJLL&E 3A.5 No.: SDG No.: Llai


Lab File ID:

CAS NO. COMPOUND


Date Extracted: 11/4- /91


Dilution Factor: 1. C'."-

CONCENTRATION UNITS:fug/L or ue/Kgl UG/KG £

-213 Q/i £_ _>i^.d 0*1 O —313 35 7--o • Q pc a•J is OO C

58-89-5-7c 44 3"5''*C 1O ""o >-• cr u u _i A - - / 1 _ C , 7 _ Q _tU.in O ' O —Q C, a Q O Q

£(-. c.7 iDU O ' 170 cc, q _' ^ o-j y7^ "/(•• P' ._ ^v o-aoo i o crc, QoO<i. 1 0 DD ir"? P A P

1 r> "3 1 — D 7 3 _I v O i U / O=, r> ^ Q "3DO ^.y ^.- -T~> A~* R' t- T'-' vJ

53494-70-5-5103-71 9-5103-74 28001-35-2 —1 fJR'7 A 11 OliCO ' H 1 J. «i1 1 1 C\A OR — O —l i lwl Ô ~ £,~1 1 1 4 1 — 1 f t R —111H1 — JLO «J~

53469-21-9-12672-29-6-1 1 AQ7_f f Q_ 11 lUj ' — D i 7 i

11096-82-5-

a 1 -.U -j nU("— aipna cnv^beta-BHC

_ j _, i r - _OUp

ear^na-BHCHeota^hlor

— n icir in

— . , f -r— C.P.CIOSU ir an i

4 A ' rifiP— .— — Unarm"C*— -J -. e;* » "T f — —. T Tr,nuoouiia.n 11

- d. A ' TlTlTlj-, . , ,- , .— incJosuiian sullate4 4 • _rir)T. i — uu i.

eurioxYcnj.01Endrin ketonea Ipha-Chlordanegamma -ChlordaneToxaphene

— — — A»**-v/^1^\»«— 1A1 ft— — — rtroc j.or— J.VJ ID^. Av%îs*1^v 1*?T^1— — HrOCJ.Or L££.±.

— — ___ A »>/->/-» 1 /-»» 1OQO— — rtrocj.or izjzAroc lor- 1242Aroclor-1248flv.^l/^1 /-1T»_1 OC</1— — ttroc io r— LÔH . .,Aroc lor- 1260

•~1 •"

.-j /-,

'". O

O *"•

O'"1

* •' VOO

431643434343

110220

43220220440210220210210210180430

: U: C >I T T

:u1 ' J! rJ• -JT.i1 ' 1

: J! U:u:u:ui

;u: U:U:u:u:u:u!U!U!U: J:u


000101


EPA SAMPLE NO.

i. _> Name: ILLINOIS EPAX107

Lab Code: SPFLD




% Moisture: not dec. IS dec.


GPC Cleanup: CY/N) Y_ pH: 7.3


Case N o . : REEIiiE. SAS N o . : SDG N o . :


Lab File ID:

Received: 11/14/91fil C 6

Date Extracted: ll/ier/91




3 1 Q ft A K-.1-3 Ol O

319-85-7•7 1 O PA fl3 1.3 OD O

58-89-97G-44-8309-00-21C24-57-3

'- - - 7 i

72-20-3o '-_•-•• o O C. O•-'K-'ii-i.O — DO 3 —

72-54-81031-07-850-29-370 y l Q _ C . _

53494-70-5--5103-71-9f\ 1 m 7/1 _o _DJ-VJo I <i~ £ —

8001-35-212674-11-2 —11104-28-2 —11141-16-5 —53469-21-9 —12672-29-6 —11097-69-1 —11096-82-5 —

beta-BHC— ae 1 La— nriL.

garrjTJct-S'-'CHpptachlorAldr in

Er<rjc£ul£&-i I

4 A * — rîtr. «t LJJJE.

Endrin

4.4 ' -DDDEndosulfan svilfate4. 4 '-DDT

— ne unoxycn j-or .. ,Endrin ketonealpha-Chlordane

— — ganuna— Cnlordane ., _,„ToxapheneAroc lor- 10 16Aroc lor- 1221Aroc lor- 1232Aroc lor- 1242Aroclor-1248Aroc lor- 1254Aroc lor- 12 60

2020202020

20390.753939393939

20039

200200400200200200200200

20390

i:u:U•u

• L I

:u:u:u •:u:u:u

:u:u:u!U:u:u!U

! J!U1


000102


EPA SAMPLE

Lab Name: ILLINOIS EPA Contract: 0971250007

Lab Code: SPFLD Case N o . : REFINE SAS N o . : SDG No.:

( g/mL )

Matr ix : (soi l /water)

Sample wt/vol:

Level: ( low/med) LOW


Extraction: (SepF/Cont/Sonc) SOHC .


Lab Sample ID:. D199669

Lab File ID:

Date Received: 11/14/91i4s<^>

Date Extracted: Il/:fc5/9l


Dilution Factor: l.QO

CAS NO. COMPOUNDCONCENTRATION UNITS:fug/L or ug/Kg) UG/KG

319-84-6 alpha-BHC319-85-7 beta-EHC319-86-8 delta-BHC58-89-9 gamma-BHC76-44 -3 Heptachlor309-00-2 Aldrin1024-57-3 Kept, epoxide959-98-8 Endosulfan I60-57-1 Dieldrin72-55-9 4, 4'-DDE72-20-8 Endrin33213-65-9 Endosulfan II72-54-8 4,4'-DDD1031-07-8 Endosulfan sulfate50-29-3 4, 4'-DDT72-43-5 Methoxychlor53494-70-5 Endrin ketone5103-71-9 alpha-Chlordane5103-74-2 gamma-Chlordane8001-35-2 Toxaphene12674-11-2 Aroclor-101611104-28-2 Aroclor-122111141-16-5 Aroclor-123253469-21-9 Aroclor-124212672-29-6 Aroclor-124811097-69-1 Aroc lor-125411096-82-5 Aroc lor-1260

2121212121

3.212140404040404040

21040

210210410200200200200200190400

!U;U'U:u:u

7; j

:u:u:u:u!U;u!U:u:u:u:u:u:u!U:u:u!U: j:u

Q

FORM I FE3T 1/87 Rev.

000103



EPA SAMPLE S'C.

XI03

Lab Code: SPFLD Case No.: REFIME SAS No.: SDG No. : D199r:n





Extraction: fSepF/Cont/Sonc) SONC



Lab File ID:

Date Received: 11/14/91ft £<&

Date Extracted: 11/Mr/91



CAS NO. COMPOUNDCONCENTRATION ONITS:(ug/L or ug/Kg) UG/KG Q

319-84-6 alpha-BHC319-85-7 beta-EHC319-86-8 delta-BHC58-89-9 gamma-BHC76-44-8 Heptachlor309-00-2 Aldrin1024-57-3 Hept. epoxide959-98-3 Endosulfan I60-57-1 Dieldrin72-55-9 4, 4'-DDE72-20-8 Endrin33213-65-9 Endosulfan II72-54-8 4,4'-DDD1031-07-8 Endosulfan sulfate.50-19-3 4, 4'-DDT72-43-5 Me t hoxy c h lor534-94-70-5 Endrin ketone5103-71-9 alpha-Chlordane5103-74-2 gamma-Chlordane8001-35-2 Toxaphene12674-11-2 Aroclor-101611104-28-2 Aroclor-122111141-16-5 Aroc lor-123253469-21-9 Aroclor-124212672-29-6 Aroclor-124811097-69-1 Aroc lor-125411096-82-5 Aroclor-1260

20 :u20 ; u20 in2020

202039393939393939

20039

200200400190200190190190110390

:u:u

5' J:u:uu

:u• u

:u:u;u:u!U!U:u:u:u:u:u!J:u

FORM I- PES

O00104Rev.


X11CLab Name: ILLINOIS EPA Contract: 0971250007

Lab Code: £££LP_ Case No.: BEEIHE SAS No.: SDG No. : Llâc-i:

Matrix: (soil/water) SOIL.






Lab File ID:

Cleanup:

CAS NO.

(Y/N) PH: 7.Q

COMPOUND


Date Extracted: ll/Jrg/91



CONCENTRATION UNITS:fug/L or ug/Ks) UG. 'KG Q

319-84-60 i Q QC 7J ^ C 7 O O ~ '

319-86-3K O PQ Q"._> OC> 3

76-44-8•3r'd '• , (•• . ••••J U. v w ~1 n^^d ^7 "^- -J. U .i. M Q' o — —QCQ QQ Qy^/cr yo o60-57-17O K C Q _I ^. --/O ^ — ~

7 o _ C1 n A-' «_ -iU OO •; •". 1 "3 (if SvjO^. 1 o Do 3

72-54-81031-07-8e.r\ oq o

72 43-553494-70-55103-71-9c-iA'i 74_9_O .LvJo— / t~ ii—8001-35-212674-11-211104-28-21 1 1 4 1 — 1 f t — c i —J. i XM i — iO~ sJ~ ~ ~

53469-21-919R79-°C1 Ci j d D ' ^ . i . C ' D — — —1 1 fSQ7 (iQ 1X J . U i # / DC? i11096-82-5

--alpha-BHCKof-a RWi"DeT..a — tiri^

--dplta-BHCgciinnici nnVx

— Heritachl cr—A Idr in

— , . . T— i,ndosu i r an i--Dieldrin

4 A ' TiT^t?. 1. — UUC.

— I7*ri/^ /-\ c»i i 1 -f a »-» T T— rLnaosLi .LI an 11- -4 .4 ' -DDD— Endosulfan sulfate

4 A ' _r\r\'r. ** — LiLtL

— Methoxychlor--Endrin ketone— alpha-Chlordane

— gamma — i_>n j. o r aa.ne- -Toxaphene--Aroclor-1016— Aroclor-1221_ — At*r\s\ 1 **•**_ , 1 OQO— — HrOC ± O r — l<iOii--Aroclor-1242, __A*^ /»>^1 r-.vt_1 O.4Q— — n r O C l O r — J.^.îo

A v^— v^v 1 ^VV*—1 OÂnrOC J.or— 1 iDt

--Aroclor-1260

22/-• .->t,

j"*) «*.^_ 4_

22

22222242424242

* O»-t<i.4212

22042

220220440210210210210210420420

:u:u: u' • j' r!

:u:u:u:TJ:u! LT

:u:u:u:J' U!U:u:u:u:u:u:u:u:u:u:uii

FORM I PEST 000105


Name: ILLINOIS

EPA SAMPLE SO.

Xlll

Lab Code: SPFLD


Sample wt/vol: 30.1 (g/mL


% Moisture: not dec. JLS dec.



Contract: Q971250Q07 I



Lab File ID:



Date Analysed: 11/30/9;

Dilution Factor: 1.QQ

CAS NO. COMPOUNDCONCENTRATION UNITS:fug/L or ug/Kg) UG/KG Q

•3 1 Q a A C _>_/ j. y OH o319-85-7319-86-8RR OQ Q_DO OJ i? —

76 44 83C9 00 2- -t n^4 ^7 ^ -L<J t.'i 3 f O

959-98-360 57 172-55-970 ^ n - R/ <i ^.U — OQ T O 1 O CC QOOi.lO DO a —7° ^4 fli ^. CJT O" i"i '^ 1 ("17 P-Ô^l U ' Oc f •-> Q T

7"? 43-5-- -c- j , iQ, i 7(-i cDOn3M 1 U O51 r\ o 71 Q _luo / i a —5103-74-28001-35-212674-11-211104-28-211141-16-553469-21-912672-29-611097-69-111096-82-5

a 1 T-iVia — RPPaipna — Dfio .beta-BHCdelta-BHCff/inuTia BflL-

HeptachlorAldr inHept . epoxideEndosulfan IDie ldr in4 . 4 ' - D D EEndr in

— c.naosu±ran LL4 A ' T\T\T\. i \j\j\jTT -J 1 * 1 * 4.— iinaosunan suirats4 /1 * HTiT

T ** JJLJl

MethoxychlorEndrin Ice tone

i.pna— L^n lorQane _ .gamma— Chi ordaneToxapheneAroc lor -10 16Aroc lor- 1221Aroclor-1232Aroclor-1242Aroc lor- 1248Aroclor-1254Aroc lor- 12 60

202020202020202039393939393939

20039

200200400190200190190190240390

i

:u:u:u;u:u:u:u

:u1U:u:u!U:u!U:u:u:u:u!U!U!U:u:u:u!J!U1


OOOlOfi


E?A = A«?'_;

X112Lab Name: ILLINOIS EPA Contract: 0971250007

Lab Code: SPFLD Case No.: EEEIUE. SAS No.: SDG No.: ri9sgg

Matrix: (soil/water) 20J_L_


Level: flow/med) LOW





Lab File ID:

CAS NO. COMPOUND






319 84-6T 1 Q_P Ci_7•J±3 CO- /010 PC flO 1 i7 — OO O

58-89-97 C ilJ R —i D *t*t O

309-00-2^ f~;n A Pi 7 "5iU^l'i U ' OQC.Q QA -PI- -333 jo O ~CA R7 1Du O ' 17 •-, c c Qi .i. 33 370 on O' i. — £. U O•;• 0 O 1 1 C R Q^^•J*O DO !3

72-54-31 f. •? 1 c\ 7 -^ — _lUO^. wl o — -c,"s ^Q -^_^ l J i. 3 O70 /iq c.r {. to Oc-3^C|.i 7fi C

5103-71-9C.1 A'5_7/l_'7__O1UO / H ônn i — ^ 9 —DUU1 — JO 4. —1 OC7/1 1 1 _OX<cD ' 4 1 1. £.

11104-28-211141-16-553469-21-912672-29-611097-69-11 1 D Q f i — fl9 R1J.UC3O — Oî O

-alpha BHC— Viot- a _nup— oe ua — Dno

j_ 1 4. -,_nur— uei ta — DfiL/gamma -BHCHsptacnlorAldr in

— nepu . epoxxCieEndosulfan ITi ' 1 Juie icir ind 4 ' _ r>r>F'i . 4 — UUE,T? Jtncir in

— TT»-i^^ôT»l'^ 'a»-i TT— n.nuosuiran 114 . 4 ' - D D D

4 A ' _nriT. *i ~ L>L> iM 4- U U Tne LnoxvcniorT-. , . .£.no.rin xetonealDha-Chlordane

— gamma— Cnlordane _.rp >— — — loxapneneA-»>«/^1 ^»«_ 1 f"M C— — Kroc J.OT*— lu J.DAroc lor- 1221Aroc lor- 1232Aroclor-1242Aroclor-1248Aroclor-1254

— — — Av^r f - t r^ l^ iv* lOAPl— — — rtrocior _L^-DU, _._

2222

222242424242424242

22042

220220430210210210210210

1500420

i

:u• u!U

! U

;u\ \ i:u'. U:u' U:u:u:u:u!U!U:u:u:u:u!U:ui ut

FORM I PEST 000107 1/S7 Rev.

PESTICIDE ORGANICS ANALYSIS DATA SHEETCm o.-„ .r _z.

Name: ILLINOIS EPAX113

Lab Code: £?FLD

Matrix: (soil/water) £.






Contract: 0971250007 ;

Case No.: BEEIME SAS No.: SDG No.:

CAS NO. COMPOUND

Lab Sample ID: D

Lab File ID:


Date Extracted: 11/15.'91



CONCENTRATION UNITS:(ug/L or ug/Kg) UG/KG Jj

312-54-6 alpha-BHC319-85-7 beta-BHC319-e6-5 deita-BHC55-39-9 gamma-BHC75-44-3 Kept ach lor3CS-00-2 Aldrin1024-57-3 Kept, epoxide95.^-^3-3 Endosulfan I60-57-1 Dieldrin^2-55-9 4, 4'-DDE72-20-6 Endrin33213-65-9 Endosulfan II72-54-3 4.4'-DDD1031-07-8 Endcsulfan sulfate.5C-29-3 4. 4'-DDT72-43-5 Methoxychlor53494-70-5 Endrin ketone5103-71-3 alpha-Chlordane5103-74-2 gamma-Chlordane8001-35-2 Toxaphene12674-11-2 Aroclor-101611104-28-2 Aroc lor-122111141-16-5 Aroc lor-123253469-21-9 Aroc lor-124212672-29-6 Aroc lor-124811097-69-1 Aroclor-125411096-82-5 Aroc lor-1260

202020202020203939393939393920039200200400190200190190190390390

!U:u:u

u: u:u;u:u:u:u'U:u•u:u:U:u:u:u;u!U:u!U:u:u

FORM I PEST 1/3

00010S


| — , T v -

Lab Name: ILLINOIS EPA Ccr.tract: 0971250007

Lab Code: 3RFLD Case No.: REFINE SAS No.: SDG No.:


Sample wt/voi: 30.1 (g/mL^ Q

Level: (low/tned) LOW




CAS NO. COMPOUND


Lab File ID:






319-34-6 alpha-BHC_319-85-7 beta319-36-8 delta-]58-39-9 g a mm a - B K C76-44-3 Heptachlor309-00-2 Aldrin1024-57-3 Hept. epoxide959-98-6 Endcsulfan I60-57- 1 Jieldrin

72-20-6 Endrin33213-65-9 Endosulfan II72-54-8 4.4'- DDD1031-07-8 Endosulfan sulfate.50-29-3 4,4 '-DDT72-43-5 Methoxychlor53494-7C-5 Endrin ketone5103-71-9 alpha-Chlordane5103-74-2 gamma-Chlordane8001-35-2 Toxaphene12674-11-2 Aroc lor—101611104-28-2 Aroc lor-:11141-16-5 Aroc53469-21-9 Aroc lor-!12672-29-6 Aroclor-1248.

11096-82-5 Aroc lor-:

21212121212121r*i i~ 1

41414141414141

2lL>

41210210420210210210210210410410

:u: u'U:u•u:u:IT;u:u:u:U!'J' U:U:U:U:n;U:u:u!U!U:u:u:u:u:u

FORM I PEST 1/87 Rev

000109

IDPESTICIDE ORGAN ICS ANALYSIS DATA SHEET

_?A SAMPLE SO

X115Name: ILLINOIS EPA Contract:

Lab Code: SPFLD Case N o . : R££IiiE £AS N o . : SDG No. : I-lrri-

Matrix: (scii/water) SOIL

Sample wt/vol: 3Q.0 ig/mL) Q

Level: flow/med) LOW


Extraction: fSepF/Cont/Sonc) SQNC



Lab File lli:


Date Extracted: 11/15/9:


Dilution Factor: 1. 0(J

CAS NO. COMPOUNDCONCENTRATION UNITS:(ug/L or us/Kg) UG/KG Q

319-84-6319-35-7•j 1 a a £ po iy — oo c58-89-97 p ,1 ." Qi !D ^l O'ViG r><~> 9•J'Jlr L'U Z1 rv~) ^ c, 7 Q1 L _. 4 - 3 / O —359-33-5---6 -~i c "> 1 _•J O ' i

72 c 5 9T~ '->c ATOO '. 1 CC, Q

•-7 *~- [^ 4 /j

T3--C7-3--50-29-372-43-553494-70-5-5103-71-9--5 1 /-> — 74 •-.

8001-35-2--

11104-28-2-11141-16-5-53469-21-9-12672-29-6-11097-69-1-11096-82-5-

%loha_BHcbeta-BHCd *. 1 4- -, _ TDLJê 1 1 a — cn*^samma— BHC

•i i •.i i. >3 r i nr.ez-t. epox. :•?Endcsu l fan Ir- . 1 jL' i. e lar in4 4 ' D*^^"C1 Jtncir inT— - i r* j -r— £.naosu i. j. an 11A A ' riPiFl

"ndosu It" an sul^'ate4 . 4 ' - D D TM^-thoxvchlorEndrin ketonea I'&ha-Ch lordane

— sainina—Cn lordane ,Tox* phene

— Aroc lo r— lOlbAroclor-1221Arcclor- 1232Aroc lor- 12 42Aroc lor- 1248Aroclor- 1254Aroc lor -1260

: 22' O'".

1 •', r>*

.

i .-,,-.

i

f .~> /-\

i ' j •",

4242

: 42! 42

42' 4°1 4 -~j

•1 -

: 42

! 220! 430

! 210: 210! 210: 210

1400! 420I

:u1 U1 rjt r •

(.'.

' f ;

:ui n

:u!U

:u:u

:u; u

FORM I PS.-.'

000110l'.:<7 Rev.


EPA £AM?LZ SO

Lab N

Lab C

Matri.

Sanpl

Level

% Moi

Extra<

GPC C

ame: ILLINOIS

sde: SPFLD

x: (soil /water

= wt/vol:

: ( low/med )

sture : not dec

EPA

Case No. : REFINE

^ SOIL

30.0 fg/mL) G

LOW

. 18 dec.


SAS No. : SCO No

Lab S<

Lab F

Date

Date ]

rtion: (SepF/Cont/Sonc) SQNC Date I

leanup: (Y/N) Y. pH: 7.4 Dilut

CONCENTRATECAS NO. COMPOUND fug/L or ug,

319-84-6319-85-7T 1 Q O C QO j. o OO O

7fi 44 R^ |7 n

i no A c,7 "3L\J 4 O ( o

, c- i

•""" =, S. Q. _ O -J J"-? /• O '"V Qi — ; > — O

3? O * "3 C - O._>_.,. O C-_ ir7 •"• r .- o

• O 1 _' ' CC •) OQ J

^"JQJ, 7'" -

5103-71-95103-74-2RAA1 T^ O

12674-11 2 —11104-28-2 —11141-16-5 —C •0,1 CQ O1 Q _•JOHDO < -L CJ

• t • Q-^ SQ i"

11C33-32-5--

alpha-BHrbeta-BHC

T ' U n&ptacn ior— rtiarin— riept . epoxide

T-i , •) ,- Ttnuosuiian i- - r' • e 1 -^ »•• i "•

, . , p." ^^ndr inEnacsultan I j.

T7 1 • •" JT- E.ndos'Li i rar sj-t/ _1 * ""ifiT"- 4 . -i r'L'l

Methoxychlor— Endrin Ketone

alpha-Chlordanegamma-Chlordane

Aroc lor- 10 16Aroc lor- 1221Aroc lor- 1232

A 1 1 " JR

* -^1 1 ° P J

Aroclor-1260

ate

XI 16

£} • QO •- *-,

ample ID: D199687

ile ID:

Received: i.

Extracted : .L

Analyzed: ±.

ion Factor:

3N UNITS:'Kg) UG/'KG

21212121212121

404'J

40

4040

21040210210410200200200200200400400

1/15/91

1/15/91

1/30/91

1.00

Q

i '

;u:u ::u ;;u:u ::u:u• ry

!U"J:un

:u:u:u : ^:u:u :!U ::u ::u:u:u:u:u:u :!Ui i

FORM I FE3TO00111

IDRGANIC3 ANALYSIS DATA SHEET

Name: ILLINOIS EPAXI 17

Lab Code: SPFLD

Matrix: fsoil/water) SOIL

Sample wt/vol: 30. 3 (g./mL) Q




GPC Cleanup: CY/N) Y_ pH: 8.2

Contract: 0971250007 ;

Case No.: EEZLNE 3AS No.: SDG No.:

Lab Sample ID:

Lab File ID:

CAS NO. COMPOUND

Date Received: 11/14/51i 4 t*

Date Extracted: 11/3-6-/91



CONCENTRATION UNITS:.'ug/L or ug/Kg) UG/KG Q

319-34-6 alpha-BHC31S-85-7 beta-BHC319-36-3 delta-BHC58-39-9 gamma-BHC76-44-8 Heptachlor3C9-CO-2 Aldrir.1024-57-3 Kept, epoxide959-93-8 Er.dosulfar. I60-57-1 Dieldrin72-55-9 4, 4'-DDE72-20-8 Endrin33213-65-9 Endosulfan II72-54-8 4,4'-DDD1051-07-8 Endosulfan sulfate.50-29-3 4. 4'-DDT72-43-5 Methoxychlor53494-70-5 Endrin ketone5103-71-9 alpha-Chlordane5103-74-2 gamma-Chlordane8001-35-2 Toxaphene12674-11-2 Aroclor-101611104-28-2 Aroc lor-122111141-16-5 Aroc lor-123253469-21-9 Aroc lor-124212672-29-6 Aroclor-124811097-69-1 Aroc lor-125411096-82-5 Aroclor-1260

22 ' 'J22 : U22 !U22 !U22 IU22 | H22 : U22 ' U43 !U43 'U43434343432204322022044083220210210210480430

!U•n'U

•_i:U:U'U:u!U:u1 j!U:u:u:ui

:u

FORM I PEST000112

IDPESTICIDE ORGAN ICS ANALYSIS DATA SHEET

Lab Name: I L L I N O I S

Lab Code: SPFLD

: X116EPA Contract: 0971250007 :

HARP N o . : REFINE SAS N o . : ' SDG Nn • D'SS**.

Matrix: ( soi l /water) S.OIL Lab S<

Sample wt/vol: 30 . 1 ( g / m L ) Q Lab F

Level: ( low/med) LOW Date I

% Moisture: not dec. 17. dec. Date I

Extraction: (SepF/Cont/Sonc ) SONC Date t

GPC Cleanup: ( Y / N ) Y pH: 8.1 Dilut:

CONCENTRATKCAS NO. COMPOUND (ug/L or ug,

i•313 C A fioiy-o^ o -•5 1 Q DC, 7o iy 0.3 '3 1 Q Q A fliy 3D Oc c pa QT ••* * * Q

•3 r\ Q ri f\ oo u y i j u i. —1 o _ 4 57 3C P C ^ £3 Qy v^ y ^ o o

7 o c, c ot-l f- /~l ,*. Q/ ^. ^.Vj O ~

- O R 3,'t;0 A750-29-37? 43-5^ Q ^ O X _-7O — 'SP i n ^ 71 Q — —ClUo t L J

5103-74-2

1007^4 11 o _

1 1 1 / 1 1 1A *^ .

12672-29-6 —i 1 n<37 — AO 1i ivjy / oy i11096-82-5--

- Ko1-n RWP

H o T -h a RWr*

Hept achlcr— MI ur in

— h e p t . epcxide— • J i -r T— ii,ncsosuii&n in « i ^, ,, , n^tr

— ,— fc.nur in— Endosulfari il

. . , r\nr>C1 J T •£ 1 JT i.c.nuosuiian suiiaê4 . 4 ' - D D TMethoxychlorEndrin ketone.

— — a l p h a — Cnl or danegamma-Chlordane

~Toxapnsne— — — rtroc ior— lu ID

A l t O O 1

A 1 1 T3O

A 1 1 O X O— — — — Hrocior— IZHZAroc lor- 1248

Aroc lor- 1260

ample ID: D199S73

Received: 11/14/91I1* C*6

Extracted: 11/J^v'Sl

^nalvzed: 11/30/91

ton Factor: 1.00

JN UNITS:' 'Kg) UG/KG Q

20 : u J" •20 : 'J J"20 : rJj ;20 ^J20 : Uj20 : "J"20 ' UJ"20 ' US40 ' Uj-

260 ! T40 ! UJ-40 ! UJ i40 ;UJ40 'UJ~

200 ! UT40 : ur

200 !UJ200 : UT410 ;uj~200 : ur i200 !UT :200 : ur200 : ur i200 :uJ

12000 : j"400 : ui

t

FORM I

000113

U.S. EPA - CLP

COVER PAGE - INORGANIC ANALYSES DATA PACKAGE

Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. Chicago Refiners & Smelters

Lab Code: Case No.: SAS No.: SDG No.: —59—

SOW No.: ILM01.0

EPA Sample No. Lab Sample ID

-X102—-X102S-

-B115908-B115908S—-B115908D—-B115909-B115910-B115911-B115912-B115913-B115914-B115975-B115976-B115977-B115978-B115979-B115980

Vere ICP interelement corrections applied?

Were ICP background corrections applied?If yes, were raw data generated beforeapplication of background corrections?

Yes

Yes

No

Comments: -1.0 ML OF 1:1 HCL ADDED TO MICROWAVE DIGESTION PROCEDURE TOIMPROVE ANTIMONY RECOVERY. FIELD SAMPLE 1X111 AMD #X113 WERE INITIALLY-RECEIVED IN BROKEN BOTTLES AND THEN RESAMPLED.-

I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness, for otherfrât the conditions detailed above. Release of the data contained in this. .rdcopy data package has been authorized by the Laboratory Manager or theManager's des(S nee7Ss<* vesX.ified by the following signature.

Signature:Date:

Name:Title:

-ROY FRAZIE1-LAB MGR-

BOOOOOi

U.S. EPA - CLP

COVER PAGE - INORGANIC ANALYSES DATA PACKAGE

Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERS

Lab Code: Case No, SAS No.:

SOW No.: ILM01.0

SDG No.: —59—

EPA Sample No,

-XI10--XI17--XI18--XI11--XI13-

Lab Sample ID

B115981B115982B115983B116417B116418

Were ICP interelement corrections applied?

Were ICP background corrections applied?If yes, were raw data generated beforeapplication of background corrections?

Yes

Yes

No

Comments: -1.0 ML OF 1:1 HCL ADDED TO MICROWAVE DIGESTION PROCEDURE TOIMPROVE ANTIMONY RECOVERY. FIELD SAMPLE fXlll AND 1X113 WERE INITIALLYRECEIVED IN BROKEN BOTTLES AND THEN RESAMPLED

I certify that this data package is in compliance with the terms andconditions of the contract, both technically and for completeness, for otherthat the conditions detailed above. Release of the data contained in thishardcopy data pacfakge has been authorized by the Laboratory Manager or theManager's deslgnee, Jas^ve^rif ied by the following signature.

Signature:Date:

Name:Title:

-ROY FRAZIER--LAB MGR

Rnnnnn-

U.S. EPA - CLP1

INORGANIC ANALYSIS DATA SHEET

EPA SAMPLE NO

X101

Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERY

Matrix ( S<Level ( LoiX Solids:

Color Bef(Color Aft<Comments:

ail ) •j j. i. i .

âac 11 u.. —

Lab

-56.5-Concentration Units (mg/kg dry weigl

CAS No.

7429-90-57440-36-0

7440-39 3

7440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-1743Q-Q5-4

7439-96-57439-97-67440-09-2

7440-09-77782-49-27440-22-47440-73— 57440-7ft-O

7440-62-27440-fifi-fi

-

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZincCyanide

Concentration i C;i

14300 !

45 5 ' '\

°se '5 3 '

56 5 !

57800 •76 fi '1 ° 7 ' E '

R1 fiO '

31500 !fiflfiQ '

0 4 5 0 0 ij

/t7' q« |

t

255051 '

1 i?1 0 ' '

1039 ' B35 ! u!-

27 *5

4970Q ' i -

1 5 U1

1

O1JVJ 11 U . . J3

Qqmnl i~ TT>- nil^Q?^


Q ; M •

PM _:

E PM "T

E * , pu T"PM

- - . PM

E , ., .. . PM... 7

PM ,1 PMPM

PM

. , OM

•t, „ ,. pM

PM

t PM

E AS JT

-,_ . . PMii PM - -

S F , , . FM Ji

1 mE ! FM T

PM ,

AS1

1 '

! i

_ /^ 1 a T* 1 V A 4* t" T" • _-_ - f* 1 A ft T* - — Artifacts •

FORM I - INSOIL BOOOO i u 3 /X

U.S. EPA - CLP1


EPA SAMPLE SO,

XI 0/2

Lab Name: ILLINOIS EPA CHAMPAIGN LABLab Code: Case No.:Matrix (Soil):Level (Low/Med):X Solids: -62.2-

Contract: N. CHICAGO REFINERS t SMELTERSSAS No.: SDG No.: —59—

Lab Sample ID: —B115908—Date Received: 11/14/91

Concentration Units (mg/kg dry weight):

CAS No. Analyte Concentration

Clarity Before: —Opaque-Clarity After: Clear—

Q

Artifacts:

M

7 4 * ? < } c i O » c ? Aluminum ' 1 fl?^rt ' nu

7440^-^f i -O Ant -i ntrtnv . 1 o n ; rr : p nu Ti '

7 4 4 0 - ? Q - - ^ RAPT urn

7 4 4 O 41 7 : ROT-V! 1 i um

74 4 O — 4 *3 — 9 PoHmiiim

17 fi F * FM

°°Q PM

-1 ^ PM

oa c ' TT nu

7 4 4 0 7 O ? r«.1 r* i um 1^2 00 i ! PM _.

sJ

T

7440 47 -T Phi-omi lira TC n ' nu

7440 4ft 4 fnhn.1 f l -

7 4 4 O — SO — ft PnrmoT*

j°0 0 : PM

ci nn i : DL<

74 TO ftQ fi Tr-nn T ft 000 , PM

7^9q_qo 1 T r-Ad .- - T T f i Q t FM

74*^Q«Q^ — 4. Mocfnooium - - - 1 fi 7 HO......... ' ^M

7400 qc c Montf an*»*>*» i OTrt * nu

7439-97-6 ' Morrurv •

7440 — 0? — ? i Ni r*1r*» 1

744O O1 — 7 ' Pni*««ainm

77f t?— r A Q ^ O ôloniim - _— _- _-

744O ?? 4 îl V^T-

74dO-2fl-0 ThAl 1 iu»

1 7/i4n-fiR-f5 7inr \

i

"'"dîf^' E \si en PM

1

3 500 PM

5 0 + p PM

9 0 , , , , : , , , , ' P M .

070 ' P PM

2 -t i ^ E ! FM

Tft O ' PM

>R400 ' i PM ,

1 *? i II ' \SI

I it !

J

J

J

Texture: -PintColor Before: -GrayColor After: -YellowComments: ICP RESULTS TAKEN FROM 5X DILUTION ZINC CHANNEL SATURATION.

FORM I - INSOIL BOOOOO: 3/90

U.S. EPA - CLP1


EPA SAMPLE NO,

X103

Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS i SMELTERSLab Code:Matrix (Soil): —Level (Low/Med):X Solids: -72.3-

Case No.: SAS No.: SDG No.: —59—Lab Sample ID: —B115909—



CAS No. Analyte Concentration C-

Color Before: —BrowiColor After: —YellovComments:


Q M

7429-90-5

7440-^fi-O

7440-Tf t -?

7440-^Q — **

7440-4 1-7

7440-43-9

7440-70-?

7440—47-^

7440-48-4

i 7440-50-fi

7419-89-fi

. 741Q-Q2-1

74TQ-Q5-4

74qq Qf i_S

• 7440-02-2

7440-09-7

77R9-4Q-2

, 7440-22-4

i 744O — 2^-51 744O-28-O

i 7440-fi?-?

• 744O-fif i— fi!

1

i

R^r*vl 1 i urn

C* A rim i nm

Cobalt

r^ntiri^ T*

T *>aH

Ni rlr^l

c \ 1 V*»T*

Tî A Ili iim

7 1 T\f*

. - . - 1 2*50O PM .,07 O ' F PM T1 0 ^ ' \ F * . FM -T

IOC pM j

138 . . PM ;1° ft F ' PM T

i i15800 ' ! PM •'

fl° 0 - •' i PM i

15 0 i ' PM !1°700 PM i31100 i ' PM '-

1000 ! + * FM -T*i ;

1 0000 i PM ,1100 i + PM i

""fr'Sll *** F A^ TOt50 i PM !

150Q PM i

5 7. .- . J_, . + F FM, ^

6 0 PM Io .u inft 1 Q Ft PM

2 fi TI P FM ,301 O ' PM \

** "" *iOO i PM !

1 ° U ' AS--!

i ! i

i i i— Texture:Artifacts:

—Fine-

FORM I - INSOIL B000004 3/90

U.S. EPA - CLP1


EPA SAMPLE NC

X104

Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERS

Matrix (ScLevel ( LovX Solids:

Color BefcColor Af t<Comments:

^___ ^•> i "M •j / M ^ H } *

-80.2-Concentration Units (mg /k

CAS No.

74297440-^fi-O

7440-38-27440-39-37440-4 1 -7

7440-43-97440-70-27440-47-3 '7440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-27440-09-77782-49-2

7440-22-47440-23-57440-28-07440-62-27440-66-6

Tab ^/imnlf* TD- ^ R 1 1 "5 Q 1 0


Analyte ; Concentration C; Q M

l

C n. 1 c i urn ' . , . . , . 12500i

Poha.lt 1°Pr*nr»r^T* .-,____....£ 0 OO

T cad , . . . . , . , . .2820

Mntf nr*«a i iim •-.- ——. — 01 Of)

Mrintf rin**^** -— — fifiO

PM

0 ' II ' P PM T. \j , u •- i • - — — -JL -— I'M \J

7 F * RM ^

i PM

1 ' ' pu .

1 F PM— .7. ' pu .

0 PM- -

5 ; PM —

i PM! i

pvi

i PM .* nn

McrcurT ' ^-K<T ** ' «• ! * c? T

Nicke l 102

C •• 1 xr**r* ^

Thallium 2

i

7-ir^r* 1 _ - 1 A 9 O n

iI

7

i ' PM

PM-R q p ; PM «r

? R ' PM,- J

PM.. ,t «•

fi U F FM J

0 PM '.u . , , rn ,! ! ' PM- .

O U AS -J1 1

1 11 i

! 1

FORM I - INson.

BOOOOO;/on

U.S. EPA - CLP1


EPA SAMPLE NO

X105


Contract: N.SAS No.:

CHICAGO REFINERS i SMELTER;SDG No.: —59—ID: —B115976—



CAS No. Anal7te 1 Concentration Q M' i !

7429744O-?fi — O

! 7440-38-2! 7440-39-3i 7440-41-7i 7440-43-97440-70-2

i 7440-47-^7440-48-4

! 7440-50-8: 7439-89-61 7439-92-1i 7439-95-4i 7439-96-5i 7439-97-6! 7440-02-2I 7440-09-7i 7782-49-2! 7440-22-4! 7440-23-5j 7440-28-0! 7440-62-2i 7440-66-6it

1

Color After: -Colorl*


•* Clariljss — Claril

1 1 °flO : PM

110 IT F PM Ti ,_

9\ .,-.-._,.. F * FM J

% ° fi PM ..

0 70 .. ; •• R PM .

° \ F PM 7T

32ROQ PM-1

21 Q . . , , , _ , PM . ,

9 A ,.,._.. R PM.

110 ' ' PM i

9 1 DOO i PM--

1 R 7 + t FM T

20300 i PM~~360 t ' PM !

"7r~~l_9 F - \°i T°fi S PM -

o o K o i PM 1

0 6 ft i W F ' FM "T1 q IT PM . j

oqn TT ! ' PM J

1 0 11 17 j T7W 7

oo 7 ! PM J

1 ? 0 i - PM -11 !

OOP . _ TT A I- <

i i i! i

FORM I - INSOIL B00001I 3/90

U.S. EPA - CLP1


EPA SAMPLE NO

X106

Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS 4 SMELTERSLab Code:Matrix (Soil): —Level (Low/Med):% Solids: -79.8-

Case No. SAS No.: SDG No.: —59—Lab Sample ID: —B115977—




Color Before: —BrowiColor After: -Colorless—Comments:

Clarity Before:Clarity After:

—Opaque-Clear—

Q M

1 7429-90-5

7440-36-0

7440 ? ft - 2

' 7440-39-3

7440-41-7' 744O — 41-Q

; 7440-70-21 7440-47-1

7440-48-4

i 7440-50-8' 7439 89 6i 7439-92-1

7439-95-47439-96-5

'

' 7440-02-2

, 7440-OQ-7

• 77R2-49-2

i 7440-22-4

' 7440-21-5

' 7440-28-0

i 7 4 4 O — R7— 21 7440— fifi— fi

i

ii1

Ant" i fflon v

RA T* i vi inR*»T*V! 1 i lira

f* A 1 £* i tm

m

Cobalt

Iron

Lead

Mfl t fTi^Qi n IB

Ni rlr*» 1

Q i 1 V^T*

THA! 1 i nm

7i nr*

191 OO

1°

153i

81 QO°7

9

°o°oo90

6°001 30

o.TJ— •

930ni

3601

550i

' PM - -

0 U P PM T

O p * fM. "^

PM . ->_X0 R PM

5 p , PM . T

• PM ,

1 ' ] PM. . .'

2 E PM i

! PM i

0 t FM - .L PM . ,

i: * pM ..,

35° 1 -r4>2l ' F \^- tJ

•j . PM. j

B.I ... , , PM . J

5O ' W F FM. \J~~^

8 11 ' PM i

U - , , PM— i6 lA F FM tr

5 PM- ..i

PM. -

O TT \C! j

! ii ' \

i iTexture: —Pint

Artifacts:

FORM I - INSOIL BOOOOI2 3/90

U.S. EPA - CLP1


EPA SAMPLE NO,

X107

Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERSLab Code:Matrix (Soil): —Level (Low/Med):X Solids: -82.1-



Concentration Units (nig/kg dry weight):

1 CAS No.

1 7429-90-57440-36-0

\ 7440-39-37440-41-7

i 7440-43-97440-70-2

I 7440-47-37440-48-47440-50-8

i Analyte Concentration • C i Q M! ' l >

A 1 11 mi mi m . , , .11100 ' PM. .

A nt i mnmr . - - - 140 < U F PM 7

> A T-tmn i c~ Q 4 c * + , T7M T

Rji r ium : - ... • fi^ 6 ' PM ..: 1

Rn-pvl 1 i nm •_ - n 7n ; n ; r>n

1 Q ' t? nu rr1 '

P/il r i i im 2fi20n l nu '

o K r>L«

Pnhn.1 t Q 7 n ' DM

Pnr»n*a i~ 1 1

1T *-,J I 0

•5 i PMi

n ' PM in n * tru-_ * ~^—— i ^ - . ~ ,

74 3 9 --9 5 4 u—,.— _..•:.._ ! 1 Term ' nw

*! A *3 Q Q £ _ £)

7440-02-2j 7440-09-7

7782-49-27440-22-47440-23-5

i 7440-28-0i

7440-66-6

U^—.M.I.-. ^-A^Jo A C*V i T? ' * < ? * ! •

NT rlrr 1 ,. . -. .2

Poi~ n î nm __-..-_.. 9SO

QrtH T iivk -_ -_ 41

TVkol 1 i nm

7 1 Til™ ^ *>

ii

r* l •%•*%•! 4- •«» o^h.^j-s-*»«^ •

Color After: -Colorless — Clarity After:

7 ° ! ' PM '•

0 I ' PM . J

051 U W F ! FM ft.

2 0 , ! - l I PM.. J

O il ! PM.— J

11 u ' F ! FM ;T

0 5 ! ' PM ;

n 1 i PM J10 II i A^. - 1

i 1 i |i i i1 i

i Pi r*AYB-m«- AT*^ "i fnr*+ T •

FORM I -SOIL BOOOOI3 3/90

U.S. EPA - CLP1


EPA SAMPLE NC

X108


Contract: N.SAS No.:

CHICAGO REFINERS i SMELTERSSDG No.: —59—

Lab Sample ID: —Bl 15979—Date Received: 11/15/91



Color Before: —Black-Color After: -Yellow—Comments:


Q M

7429-90-5

7440-36-0

7440-38-2: 7440-39-3

7440-41-7

' 7440-43-97440 70-2

7440-47-37440-48-4

7440-50-8

7439-89-67439-92-17439-95-47439-96-57439-97-67440-02-9

7440-09-7

7782-49-9

7440-22-4

7440-23-5

7440-28-07440-62-27440-fifi-fi

Ant" i monvA r*^#*r> i c*P o r» 4 nm

fTHT*oni 11 m

fohal t

T T*rtn

T.A oH

MAC? no Q i iim

MATtt fAnAQA

MoY*fMi T*V

Mi r*lr«»l

Q A 1 on i 11 IB

Q i 1 VAT*

C oH i HM

Th A 111 tin

7 i r\f+

PvAni HA

11700

130 U '

°5 7179 ;

in • R :

1 6 '1 9^00 '

°9 3?1 fiJ i . D |

389 ! '°150Q i

4*5510*500

1 TS 0 ; i

T^'Sj* 'Tfi 7

"'TiO

1 n1 R II !

?70 11

15 a

^1 O

1 fiOO ! i

i n T Ti

!

°M i

E PM .T

E * .. . pi/, T -• rn- v^PM .

PM

E PM , T1 PM . .

PM !

PM .

puj '

' pu .

* FM .

i PM .

* PM

E \S IT

PM

PM. .

+ F FM J

PM- i

PM — «

E . . . i FM . rr1

PM 1

PM '1 A^ - i1 !1

Texture: —Fine-Artifacts:

FORM I - INRfinnni/i

U.S. EPA - CLP1


EPA SAMPLE NO,

X109

Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS 4 SMELTERSl_lttU VvUUC •

Matrix ( S<Level ( Loi% Solids:

Color Bef<Color Aft«Comments:

3 il ) •i i ; .j /Mr>rl \ •

uaac; «w • . — -

-88.5-Concentration

CAS No.

7429-90-57440-36-07440-38-27440-39-3

7440-41-77440-43-97440-70-2

7440-47-37440-48-47440-50-87439-89-67439-92-17419-95-47439-96-57439-97-67 4 4 0 — 0 9 — 27440-09-77782-49-27440-22-47440-23-5744O ?ft — f)

7440-62-27440-66-6

— — — — — ijfivj rtu . . — — _

Lab SD

Jnits (mg/kg dry weight

Analyte Concentration i C;1


R T 7 0no i!

95 : '6 7 0

19 ' i! 1

0 0 :

19900 '

11 i ! !8 n_ t a : P '

19121100 '- i

298<5fi3QQ ' '

386 '

4^LF<* !°0 ft i

ftOO ! RQ fil1 <? ! II

*50° R

0 69 (A1 7 9

fifiO !o q - 1 ' n

1ii

p 1 n T- i t- ir A^t-oi-' . f l r n r

ouu n<J . . L> J —

Amr>1*» in- Rl 1 S9fiO

ate Received: 11/15/9

) .

Q : M :

PM -^

E . PM. J

E ^ pvf -.TPM - »

PM

E PM "T

PM--

PM . ,

PM '

PM-

PM.«,

t FM- .

PM--

^ PM-

E AS. sT

PM .DM

I rn ,WF FM , L"T

PM -

PM . i

E . i ,. . . FM~ -TT

PM---

P M . (

AC . ,( ;I

;

A r+ \ ^nr*t" •> • . , . .

FORM I - INSOIL BOOOOI5 3/90

U.S. EPA - CLP1


EPA SAMPLE NO,

X110

Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERSLittu vûiac .

Matrix (SLevel ( LoiX Solids:

Color Bef<Color Aft«Comments:

n i M •

w/Mr-rf \ •

vâ^c iiv» • . — • • unu

-77.5-Concentration Units (mg/kg

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97d4n 7O— 9

74/10-47 — 1

7440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-27440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

T ah âmril ** TH* A I I ^ Q f l l


1 Analyte Concentration C Q M

A 1 11 mi niim < « — . 1 ^ 1 0 0 .i '

nu

A n t - i m n n v , - .. . -—,--14 0 Ui F PM !T

ATQc*ni r • 7 ft i F * FM T

R n T- -i urn ... - - - — « . fl *? 0 I PMnOT.— i I ^ um _ Q 7Q j R PM-.-

r*riHmiiin - -« 10 ° ^ n" ^

f f i l f - i i i m 1 -- (ii?fiO

r*Ki-rtm 1 11 IB . ? 1 Q

Pohftl i- .. - -11 5i

Pf-iTM-kAr °fi Q

TT-rin . -19SQO

T rtnrl . ._._ A Q 0i

MrtntTrtncar: - 929.o<.

fH r-lr*» 1 . . ._«-?? Q

Pnt* A-atti !!• .. ?^f iO .

*? i lTr«%f - « . . 20

^nrlinvi — 4 D 1 .

Thti 1 1 i iim .... --- ,- .- 1 4

VanoH i iim - ?Q 1

7 i nr* .. — — 11?

iPM

PM—

B, „ . pu

..j.,, PM

i i PM

' * FMi tripu1 . rM

t PM3^0 • -rfl °r E A4? J

; pu

. . . . ' P M

1 U WE FM f t .

U * , .. . - i PMU i PM —

U F ! FM J"! TM• PH

U A"? .I

I

!!

sr: -Colorless — Clarity After: —— r* 1 /* nr* - r - - AT'^ ' i 'Ff t i"*^^* — .-. . ..

FORM I - IN BOOOO i 6

U.S. EPA - CLP EPA SAMPLE NO,

INORGANIC ANALYSIS DATA SHEET i XI 11i

Lab Name :Lab Code :Matrix (S<Level (Loi% Solids:

-

-

Color BefcColor Aft«Comments:

ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERSf- M— • OAO vi~ . on/-> vr_ . en

-,il \ .

•r/Meri \ •L

-89.2-Concentration Units (mg/kg dry we

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-4 1-77440-43-97440-70-27440-47-37440-48-47440-50-874. Q ft Q — fi

741Q-99-1

7439 96-57439-97-67440-02-27440-09-77782-49-27440-22-47440-23-57440-28-07440-69-2

7440-66-6

»r: -Colorl*

Analyte Concentration C


i Clarilsss — Claril


i tfhf ) • ....,,

Q : M '

A °fiO PM _

110 TI ' F PM T90' c- * c-w T

1 01 6

1QQfiQO

TO C

fi •? Ft

710

PMPM

E ; PM IT

PM .,

PM ,1 DM }

DLf

. , i Q i on ' PM.°fiS 1 FM-

i i47°nn i PM -fifiO * n"

o- ™5u?

oo'o 1

730 BO g g0 0 TI

17 M101 _ n ,

1 * "

E A<v 1

' PM. -

PM ,

W R. — -• .. FM T

PM...-

PM- -

E_. «.— . 1., FM ^T

PM -

PM M

A<^ 1

'•

ty After: Clear-

FORM I - INSOTT. Rnnnni9

U.S. EPA - CLP EPA SAMPLE

INORGANIC ANALYSIS DATA SHEET j XI 12

Lab NameLab CodeMatrix (Level (LX Solids

: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS 4 SMELTERir>n*,p. Wo • OAC vr- . or\/i »T_ . c n

q0 : l ) .

nu /Mort \ •

: -76.5-Concentration Units (

T nh ^nnrnl r- T F » * R 1 1 S Q 1 1


m tf/lrtf HT*TT w ^ i r f h ' f r ' ^ * _ _, - _

CAS No. Analyte Concentration ' C; Q M

Color BeColor AfComments

' 7/1 9O — Qfi ^ ^ A l u m i n u mI !

1A.A.r\ — Tfi — fl A n t i m n m r

7 A A n Ifl 9 Ayisonio

7il dn^ 1 Q-. T R n y i n m ' .

744O 41-7 Re nr Il ium

1 A. 4D^ A T-- 1 : PaHmi i im

744O 7O ? f j i l r i i im ! .

' 7ddn 47 "\ Ph-romi urn '-

7440-df l -4 Coha.lt -. -

7-140 — fi — A Pfrnn^T*

' 7439-89-6 Iron 17410 12 1 T r>jid ... _ . .

i 74 in .OS d Mnffnr -^ i nm 3

'• 74 on ,. nc c M« nrf An*»-=tn

7^ ' i q^q7_e | Mm~riiT-vi i

7440-0? 9 NT r-k^l1 7/1 .4 n OQ 7 ' P n ^ a O Q i i i m

7700^40^9 ! «:^lAniiiiii

7440 ?2 4 S i lv fT*7440--?^-*? : ^nH i un

7 4 4 O ?ft-O TViJil 1 i iim

744O-fi2-2 VanAHi nm

7 4 4 O fifi-fi 7i nr-

i

ii

40OO , PM

1 4 0 ' i f ' F P M " T

9 *5 - ! ^ F 'f FM f _f

400 PM .- .

3 *5 : 1 PM .

o o p PM--J"

7flOO : ' ' PM -

*57 0 PM

6 1 - - ;. PM —HOO PM

6600 ! PM6 15 : * FM.

7°00 PM .

IRQ ' t PMt ou -» -» <s • T rn

~#4i^'i E : \2 T1° 0 ' PM

fiQO R * PM- - -'

0 *50- -U W F ! FM- -C

1 9 i PM m

pqn R PM- .

1 fi U W F FM IT

9 1 . R PM--

4 1! 70 . . I 1 PM--

U A m A ^ » — .

I

1

ter: —Colorless — Clarity Aftcl T* * f I ^fii* A l ^ ^ T ^ r t l ^ ^ ^ * .... .

FORM I - IN BOOOOOo

U.S. EPA - CLP1


EPA SAMPLE NO.

X113

Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERSLab Code:Matrix (Soil): —Level (Low/Med):% Solids: -74.9-




CAS No. Analyte Concentration Q M

' 749Q-QO 5

7440-36 0

7440-38-2

' 7440-3Q-3

7440-41-7

• 7440-43-Q

7440-70-7

7440-47-?

7440-48-47440-50-87 4 T q _ Q q _ f i

743q~q2-l7439-95-4

743q-q6-5

7439-97-6744O— O9— 9

7440-09-777R7-4.Q— 9

i7ddn-??-47ddO— 91— **744f i -? f t— O

7440-62-2

744O-6fi-fi1

Ant* i monv

R^Tvl 1 "i 11 m

Cobalt

T,*»Ari

M^T*r*iiT*v\i 4 Irol

C i 1 \r A v*

ThA.1 1 i tin

VAnnH i tin

7i nof^TTATl 1 HA

^ inn !

M O TJ

6 59 ^ 0 '

0 50 R1 6

700OO i '

1 fi \ ' i

7 3 B•57 ° !

1 'I'lOO '

103

1Q°00

\ °7

>^ i i°? 1 i

1 100 '0 5 3 T Io q |

4?0 TI

050 M

1 5 6

210

1 1 T Ii

ii

1 nM

E PM rrE ^t . ' pw *r

PM !

i PM i

E ; PM iT

PM —

PM j

PM --i

PM. . ,

PM

* PM,. -

i PM 't PM -J

E A*? IT

' PM '

PM i

¥ P FM fi.

i PM .

PMi-

4- p PM ^T

PM J

PM !

A- i1 j

ii

Color Before: —BrowiColor After: -Yellow-Comments:

Clarity Before:Clarity After:

—Opaque-Clear—

Texture: —Fine-Artifacts:

FORM I - INSOIL B000020

U.S. EPA - CLP1


EPA SAHPLE NO

X114

Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS &. SMELTERSLab Code:Matrix (Soil): —Level (Low/Med):% Solids: -76.8-




! CAS No. Analyte1 ;7499—90—5 • Aluminum

7440-36-0 Antimony, 7440-38-2 Arsenic7440-39-3 Barium7440-41 7 Bervllium

' 7440—43—9 Cadmium1

74.40 — 70-2 Calc ium

j 7440-47-3 Chromium7440-48-4 i Cobalt

\ 7440-50-8 ! Copper] 7439-89-6 Iron7439 92-1 Lead7439-95-4 ; Magnesium

j 7439-96-5 Manganese

1 7440-02-2 Nickel

i 7440-09-7 Potassium' 7782-49-2 Selenium

i 7440-22-4 Silver1 7440-23-5 Sodiuml 7440-28-0 Thalliumi 7440-62-2 Vanadium1 7440-66-6 Zinc

1i

!

Concentration C ! Q M

i 3600 * ' PM1 i i110 II F PM

1 9 fi 1 ' F * FM -

°fi fi B PM .

0 50 U PM\

0 99 U i F PM

\ "5*5 00 i PM

U 7 '' \ PM

1 R i H '• PMi

01 ? ! PM!

10300 ' PM '3 ft A * ' PM

9 9 inn ' ou

390 ! t ' PM""^ ~ft~ 5 1 C1 AC

13 3 ^ PMI ic *> A o ' nu '

O SO- *— U F ', FM

2 Q i n ' pM ;

100 u' i PM iU I ; ;

0.. _L_ . *4— F ! FM

107 B ' ! PM '

fl° 0 ! ' PM i

1 1 IT' ' A<n

i!

! i I

Color After: -Colorless — ClarihTT A^ÔT** ("* 1 f*fiT* AT"h 1 Af*^ W* __- -

1

T

T

T

[ium

FORM I - IN

U.S. EPA - CLP1


EPA SAMPLE NO,

X115

Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS & SMELTERSuau isuuc .

Matrix ( S<Level ( LoiX Solids:

Color Bef<Color Aft*Comments:

D i 1 ) ••r/Mr-H } •

_ TÛCoi-^l—Tn. D 1 1 R Q 1 O

-79.4-Concentration \

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-874^Q-ft<?-fi

7439-92-17439-95-47d^Q-Qfi-57439-97-6744ft— O9-?

744O-OQ 7

77R2-49-2

7440-22-4744O — 91 — *>

7440-28-07440-62-27440-66-6


Jni tn fmsf/lrtf HT*V wfîrfht"^*

1

Analyte Concentration I C Q M! i :


11 °Q f ' PM1 • •«

130 ; 17 F PM ,T5 8 i P * FM T

4fl 5 ' PM0 SO ; R PM0 1 : F PM J

74HQO ' PM-,700 pu

1 0 - r R PM ..

qni ' ^M jqo-M ! ' "M ;1 990 t PM !T7°00 : PM .

?70 * PM i4/UO.T37 1P1

-ft 50 at F A<^ ^T1 C ft U [ pu

fifiO B PM '

0 46- »— IT' W F FM..-.fl.

A an n PM_ .

0 70 • 1 F FM .T

76 H PM 1O7f> ; pM. _

1 ^ A*^ - ii

r

jr: -Colorless — ClarihvA-f+jar'* pi rriT" - Art i f firt.n *

FORM I - INSOIL B000006 3/90

U.S. EPA - CLP1


EPA SAMPLE NC'

X116

Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS 4 SMELTERSLab Code:Matrix (Soil): —Level (Low/Med):% Solids: -78.6-




CAS No. Concentration

Color Before: —BrownColor After: —ColorlessComments:


M

7429-90-57440-36-07440 38-2

i 7440-39-37440-41-7

• 7440-43-97440-70-2744O-47 37440-48-4

7440-50-87439-89-67439-92-1

7439-95 4

7439-96-57439-97-67440-02-27440-09-77782-49-27440-22-4

i 7440-23-57440-28-07440-62-27440-66-6

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromium0

IronLjG&d

Magnesium

MercuryNickelPotassiumSeleniumSilverSodiumThallium

ZincCyanide

i

T 1 30

onni

1 fi7'

611 1 OO

fMfl

630

28570

n

| ; ' PM. .

O n F PM ,."**1 F * FM . . J^-

8 ! B ' PM !A n i , n ; ' PM. .

6 ' F PM vTPM .. J

8 PM i

1 -0 OL*

DW :

PM ^

' FMt

PM -

t ! PM i0.3** ; L •_T 2J _ J E» * 0 ~

1

5 1

Q

105O9

1

53

a

PM i

B PM !

U i W F FM .. .Q

PM.-4

U ; i PM ..J

n • nu '.1 1

r»Li

.1 U i A°l .-i! 1

ii

Texture: MediumArtifacts:

FORM I - IN BOOOOO^

U.S. EPA - CLP1


EPA SAMPLE NO,

X117

Lab Name: ILLINOIS EPA CHAMPAIGN LABLab Code: Case No. :Matrix (Soil):Level (Low/Med):X Solids: -78.4-

Contract: N. CHICAGO REFINERS i SMELTERSSAS No.: SDG No.: —59—

Lab Sample ID: —B115982—Date Received: 11/15/91


CAS No. Analyte Concentration Q M

1 7429-90-5

7440-36-07440-38-27440-39-37440-41-77440-43-97440-70-2

7440-47-37440-4K-4744O-5O-R

7439-89-67439-92-17439-95-47439-96-574"lQ_u'7_fi

i 7440-02-27440-09-7

| 7782-49-27440-22-4

1 7440-23-5! 744O— 9 f t — O1 7440-62-2I 7440-66-6ii ..___

!

1 — »^«__- ii • •Ij


1 fi°00 I110 ; IT '09 o ! !

? fl 7

5? ft :

S I R i >I f i f t O Q

TRO !

39 0 ' 'R 1 ?nn ' 'fiOfiOG ''

1 T'OO '

SQftO ;

°760 '~ \i1ta I

>Il <=* 'n.4 | i1 07O '

410 ' TT !

8 4 - \

37 iO f i O C

2 fi- . 11

8 ^ . . p '- - 1 Of tÔf l '

11 - TT

[ Ii

' PM ^

E PM \T

S F * PM .T

PM ^j

i PM '

E PM. ,3*

' PM, tn {1 PM -i1 PM !

nM i

' PM. i

t ! FM '1 PM 1

t ! PM i

E i AS TPM I

! 1

! PM J

S f . ! PM ,T

PM i

1 PM

E ^ PM J*rPM

PM

, AC

I A-ii

Art i f act1 a • - -

FORM I - INSOIL

BOOOOI 73/90

U.S. EPA - CLP1


EPA SAMPLE NC

X118

Lab Name: ILLINOIS EPA CHAMPAIGN LAB Contract: N. CHICAGO REFINERS A. SMELTERSLab Code:Matrix (Soil): —Level (Low/Med):% Solids: -80.7-

Case No.: SAS No.: SDG No.: -59—Lab Sample ID: —B115983—


Concentration Units (ing/kg dry weight):

CAS No. Analyte Concentration ! C Q M

1 74?<?-Q0^5 ' A l u m i n u m ' 10800 PM ,

7 4 4 0 ^ T f i — 0 A n f i m o n v —60 4 ' i F PM "*"

7 4 4 0 T f i 2 A r ^ p r i - i « ~ ' . - 1 9 7 - ' - ' ^ F * FM 7*-

7 4 4 O TQ-^1 ' Rj iT-ium . T ? 1 ' i PM

7440 41 7 Ben-I l ium 7 5 : PM

7 4 4 O — 41— 9 r*AHmi iim 1 ft ^ ' ^ ^^

7440-70-2 r j i l r i nm .-.. -19TO n ' n»*I

744O — 47--T PhT^nmi i im ' • S 1 1 ' OXJ

J

744O-4H-4 Pobalt . ... . - - I f l S ' PM

74^9 ft 9 fi Tr-on ^^ f l f l

7419 92 1 ' r*»AH , 479

74?9 9^ — 4 Mntfn^ta-i iim fi^fl

7 A oq 07 c MoT^rîi'rT "^

1 7440-02-2 Nickel . -.-16

7440-09—7 Pot fl^tai nm 9?

77ft? 49 2 ô I o n i u m

0 : *'M

0 ' '•• * ' FM

o - ; PMO ' -t PM35.9^ : • . P ,"^KJ? CA i \ F '\<?0 PM

0 R PMoo o t? ' trw

7440 22 4 ' ^-i Ivo-r — . - 2° ° ! nu '

7440--23-5 Sodium 114

7440-2B-0 T h a l l i n n t 2

7440-R2 2 Vannî i iHi - — ..,5

' 74 4O fifi fi 7i nr- 1 9 4 C

i

0 B ' PM '

fi 6 Vl E ' FM '0 1 i PM

0 ' PM

1 0 U i ' A<?

t '

T

>_

T

T

Color Before: —Black-Color After: -Yellow-Comments:

Clarity Before: —Opaque-Clarity After: Clear-

Texture: -FineArtifacts:

FORM I - IN BOOOOI8

Documents

SCREENING SITE INSEPCTION ANALYTICAL RESULTS · Ncrtn cncogo R«rtn«ni I SnVUre:LC 067371583 SAMPLING POINT VCLA TILES SSI SEDUgCNT SAMPLE ANALYTICAL RESULTS 1 .2-C'cnk»asth«r»