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MAY 23 '97 03:17PM STERLING ANALYTICAL P' Sic2 Z-

SFUND RECORDS CENTER ^ /03 88224181 i

S T E R L I N G F A X C O V E R A n a . l y t l b a l L o b o r a t o r y

TO:

DATE:

NAME:

FAX NO.:

PHONE NO.:

FROM: NAME:

JOB/OVERHEAD NO.

CHECK ONE: ,

fyZJ NORMAL PROCESSING

• CONFIDENTIAL

I ~\ CALL TO CONFIRM ON ARRIVAL (310} 595-9324

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2860 Wolnut Avenue long Beach, CA 90806-1834

(800) 3669324 • (310) 5969324 (310) 595-6709 FAX

MAY 23 ' 97 03:18PM STERLING ANALYTICAL P.2'13

Client: Attn:

CET Environmental Services Mr. Mike Bundy

Client's Project: Date Received: Matrix: Units: Digestion Method:

Envlropur West, 9E04-000 03/21/97 Water m*/L EPA 3010

Lab No.: 17048-00! 17648-002 Client Sample I.D.: 1001H-T 1001 H-B

Date Sampled: 05/21/97 05/21/97 Date Digested: 05/23/97 05/23/97 Date Analyzed: 05/23/97 05/23/97

Analyst Initials: LP/DJ LP/DJ Dilution Factor 1 1

mm wmmm e»«c<

Antimony 0.005 0.007 ND Arsenic 0.005 0.072 0.051 Barium 0.001 0.076 0.083 Beryllium 0.001 ND ND •

Cadmium 0.003 ND ND Chromium 0.003 0.011 0.010 Cobalt 0.003 0.006 0.005 Copper 0.003 0.011 0.009 Lead 0.005 ND 0.006 (

Mercury " 0.004 ND ND Molybdenum 0.005 0.11 0.096 Nickel 0.003 0.15 0.13 Selenium 0.005 0.01! 0.007 Silver 0.001 0.004 0.004 Thallium 0.005 ND . ND Vanadium 0.003 0.009 0.008 Zinc 03)10 0.047 0.043

MDL * M«di»d Detcctien Limit ND * Nat Detected (Below DLR). DLR H MDL X Dilution Factor

* - Only lilted constituents designated wiU TTLC and 5TLC under CCR Tide 22 •• = Analysis by EPA Method 7470

Reviewed/Approved By: #2 / Date: C /97 Cheryl De U* Reyes Department Supervisor

r Imw w m iuinyW pnrt oftfib wlytied report

1510 E. 33rd Street Sinnal Hill CA 90807 Tel 562 989-4045 Fox: 562 989-4040

MAY 23 '97 03:18PM STERLING ANALYTICAL

Client CET Environmental Scniut, Inc. Attn: Mr. Mike Bundy

Cfioil'i Project: Enviroptir Wat, 9EQ44M0

Dale Rtttrnd: 05/21/97 Date Sampled: 05/21/97

17640-001 100IH-T EPA 410.1 (TRPH) 05/23/97 0.2 Water. ms/L 0.04 0.04 AK 17640-002 1001H-B EPA 410.1 (TRPH) OS/23/97 3.2 Water. ms/L 0.04 0L04 AK 17640-001 1001H-T EPA 335.2 (Total Cyanide) 05/22/97 0.04 Water. ms/L 0.02 0.02 HS 17649-002 1001H-B EPA 335.2 (Total Cyanide) 05/22/97 0.03 Water. mc/L 0.02 0.02 HS 17640-001 100IH-T EPA 150.1 (nH) OS/22/97 0.94 Water, pH units DC 17648-002 1001H-B EPA 150.1 (oH) 05/22/97 8.63 Water, pH units DC 176404)01 1001H-T EPA 376.2 (Sulfide) 05/22/97 1.4 Water, ms/L 0.05 0.0S AK 176404)02 1001H-B EPA 376.2 /Sulfide) 05/22/97 ND Water, me/L 0.05 0.05 AK

v (

MDL - Method Dctecum LMl I ND • Not Detected (Mow DLR) DF - OSutioa Fitter (DLR/MDL)

Review**/Approved Br D.tc:

Department Supervisor

TJ* aw letter •> an iMcfnl tan of ihta mimical rerun

, v -

Ttchnolotj t /tfcpmtwiJar 1510 E. 33rd Street Signal Hill. CA 90807 Tel: 562 989-4045 Fax: 562 989-4040

Spilu Rewwry md MPD Summary Rupert

MeOted:

Anatytt:

DataFHe:

EPA 7470

COR/D/

70JZS-1

Date: OJ-tt-97

Sample ID: 17471-001

Matrix: Water

MN.rn UNITS LCSCens LCSRf MBTH BLANK SPLCOKC 3 PK ADDED MS RESULT MSD RESULT HMS RfiC KMSD K£C tpn •an tlfmU Maw*y 0.8100 0.0107 107 ND ND O.OIOO 0.010] • 0101 103 100 66-134 3 26 #.004 I

>i -

< rvj U)

UJ N

3 t-i

AwrmaadOr CMDafitRiw Cheryl Da tU Reyea biorfiaiceStfpervuar

Data:. <sA»Ay

u \

w

fwwcrrf Ttchnctatr Labototoritt

Method: 418.1

Analyst: AK

OataFOa: 71S3-1W

Oate Analyze 03-23-97

Sample )0: Blank

Matrix: Water

ANALYTE UMTS CS Cone LCS R«s. %Rec METH BLANK SPLCONC SPXAOOEO MS RESULT MSDRESUL %MS REC %MSO RE RRO Unrit

20 TRPM mfl/l 4.00 4.28 107 NO NO 4.00 4 04 3.72 tot

MOL

0.04

Approved t»y: Cheryl Oe Ms Reyea Cheryl 0* Ms Royoa Inoryartee Supervisor

Oale:_

oi \

it)

t4 Tichtotofy Laboratoriri

Melhod: 335.2 Anatyal: HS Data F8e: 7142-1W

Date. 05/22/97

Sample ID: 17572-005

Matrix: Water

tnofgariJca Suparvtaor

•o

•-»

to

,-i' _ «/ Tttknofot * Laboratories

I

Method: 378-2

Analyil: AK

Data File: 7152-1W

Date: 03-22-87

Simple K> BLANK

Matrix: WATER

ANALYTE

SULFIDE

UNITS

MG/L

LCSCon

1.0

ICS Wei

0.07

ttWec

97

METH BLANK

NO

SPLCONC

NO

SFKAOOgP

1.0

MS RESULT

0.96

MSP RESUi

0.88 %MS REC

97

ttMSD we

<89

REC Umlt

70-120

RPO WFO limit

20

OLW

0.06

3 -<

ro U)

u>

8

cn Fl P

t—4

Approved by. Cheryl Oe LoTReyes Irarganlca SupeivUor

Dele: v/ ./7y7

\

U)

ttranetd Tttbnotofj Laboratories

MAY 23 ' 97 03:20PM STERLING ANALYTICAL P.8/13

CUtnr. CCT EmlrwMMMal Saratto, lac A«a» Mr. Mike Du*4y

r« i r f»

CDml'i Frajtel:

Halt I Malrtxi IXa: [itmflw Mrttrt:

tmkifw Wot. 9M44N

os/ii/rr Wat«r •ei 151*

mmm UhNa: MribaO DMi 17*00401 17*40402

Chow iaaim tfci - 1001 n-T IMID-D Datr SUMM: - OS/21/97 OS/31/97

OC Batch t: R970179W101 R9702T0W10I R970270WI0I Dala EHntM: OS/22/97 OS/22/97 0S/21/9T Pair Ambirfi 4501191 0S/22/97 OS/22/97 AaabM latdala: DC DC DC

BMaa Factar: I.I 20 20

\w* yw* if#*? i&jjSTj a-WllwwftatilnhnBn 10 H ND 2*0 NO 200 ND Miciwd 10 ii ND 2*0 973 200 494 Mi fl-CMw aiflijl)crinr to 10 ND 200 ND 2*1 ND 1-CMircfhtael 10 II ND 200 ND 200 ND 1 J-PltMll ihlBHW 10 It ND 2*0 ND 200 ND

1.2-lWi Ma. at. at. a» 10 It ND 200 ND ND

200

200 ND ND

MO rM»nhatac»jQulm 10 10 HO 20* ND 100 ND a-lfflwi <1 a aiaajlamliu 10 10 HO 2*0 ND 200 ND ilexacMareadiaMe 10 10 ND 200 ND 200 ND WlnMaiiai 10 10 ND 200 ND 20* ND Iraatucaac 10 10 ND 200 ND 20* ND 2'Nki«MmM 10 10 ND 100 ND 2M ND 2,4-D4ailbjl*hiaal 10 10 ND 2*0 ND 20* ND MO-CMaraMhaxTMnrthaar 10 10 ND 200 ND 20* ND M-Dlrllirufclaal 10 10 ND 200 ND 200 ND 1 •2.4-TricMaraOrawnc 10 10 ND 200 ND 200 ND NapMalM* 10 10 ND 200 ' ND 20* ND llnnMa ihiriliw 10 10 ND 200 ND 2*0 ND 4-<Mar»J-aM<MMM*el It It ND 200 ND 2*0 ND n«mUa«wlanala<ln 20 20 ND 400 -ND 400 ND 2.«-TrfcMai atilnaal 10 10 ND 200 ND 200 ND 2-CMai ana pMfcaluia 10 10 ND 200 ND 2*0 ND Plmi rtijlphlhalalt 10 10 ND 2*0 ND 20* ND AcovapOcO^Oiae 10 It ND 200 ND 20* ND M-DhNi Maluim 10 10 ND 200 ND 2*0 ND Accnaahtluat 10 10 ND 200 ND 2*0 ND L4-Dhrfuaa«naal 10 •• ND 200 ND 2001 ND

T .

MDL - Method Dvttttiea UmM ND - Nat Detected (Ddo* out) DLR - MDL x DOutiae FaeUr NA * Nat Aaalyaad

Ap|imMlpiin4 By: Date SqMMr

L Technology

—r 7*/0 £. iirrf 5/re<?r 5i>na/ Witf. CA 90507 7W: 552 989-4045 Fax: 562 989-4040

MAY 23 ' 97 03:21PM STERLING ANALYTICAL P.9/13

fBeat: (XT Eavfcaamcataf Jkiskts lac.

Amu Mr. Mlit tcaljr

Dare Htwlal. Malrtt: Hall*: Ciiradtai Mcihwli

9*1*41

Earfc.fT WCM. 9E04-M4

tsnim Water «w« 1511

Lmk N»: MdMJNaak I7M0-MI I744MM 1 | 1 1 CTM Swiiph l-D*; tmn-r imiii-b 1 1 1 1

*# 4-Nflraakaaal ,11 MI IN NI IN NI 1.1 Mwli *l*hiii« M NI IN NI Ml NI Ftearaw II • NI IN NO Ml NI Dkthjlpitfkalalt II NO IN ND IN ND 4-CM*i •ataail-pfeqirl rttat II NO 104 ND Ml NO 4.4-PlaHia-l m<Uiylphtn*t l« NO 104 ND 100 ND a-Nltr«**4lalitml*mlin II NP MO NO IM ND 4-Draa»afli«ej*.plntijl ether II NI) MO ND IN ND IlttatMaraWaniu II NI) M0 NO IM NO fnCwMiripkuwl II NP 100 NO IM ND Dmirtiwn II ND 100 NO 110 ND AJUkranat II NP 100 ND 100 ND 1)1 II tMjtpklll.llMt II no 100 ND 101 ND l^lu^tcaae^k^^^te II NO 100 ND 140 ND HiniHhn SI NO 1100 NO UN ND !>**. II no 100 ND 110 ND PwMh:a*j4aliili*l»l* II ii NO 100 NO Ml ND P»n«»[*|aathi mm II ii NO 110 . ND Ml ND 3J'-0kMaraWn>Mlac M ND 400 ND 401 ND Clmwa II ii ND 100 ND IM ND MtO-tdoBanjIlpMlaWt 10 ii NO 100 NO IM ND DU actilalirtialatc II NO 100 ND 2M ND B**a*Mft**r**ltitat II ii ND 100 ND IM ND Betuaftjtlaai aathuii 11 ii ND MO V NO IM ND lm>|a|nnM II ii ND m ND M0 ND IaliaaU.7.3 rUprrmt II ii NO MO NO IN ND MbauKUmlmttw II ii ND MO »nd ZM ND

II ii ND 100 ''no IM ND

MM»- IMNHt;

Sarrataat Hltoe. Limit* 411 IDA

HRcc Limit* Hit**, Lkait. ___ aaa-mm—a

n»aU< JZ

10 Z1-II9 11-110

500 14

11-110 10-111

31 0

11-110 11-110

l-CM*n»lua»l 15 54 0-111 54 33.1II 41 33-110 l.2-DMI*rat«n**at-44 45 I4-110 44 14-111 41 14-111 Nknkkmr« 54 35-114 50 35-114 51 J5-II4 l-FlamaHahta.il JJ «-H4 40 _ 43-114 41 43-114 W-Tilli aeatuhtaal 44 11-10 44 10-10 44 ' 10-10 TutlctllH* Hltf. - lUWI^. I.L_I

441 33-141 59 33-1411 411 33-1411 • ZZL 1 1

>1-1?

ND DLR

NA

Nat ItataOad (D*t*w DUQ MDL K DUatiaa Factar Net AaaljrtM

Ay|»rilflto>iwiil Pyj_ Data:

PtpMtiatat SaptnNar.

•r*r

1510 E. 33 rd Street Signal Hill, CA 90807 Tel: 562 989-4045 Fax: 562 989-4040

MAY 23 '97 03:21PM STERLING ANALYTICAL P.10/13

.(

Client: (IT I jlHrawwihl Strrico. lac Mm: Mr. Milu Dundy

CSenfa Project: EmirofKo- W«t, )E(44N

Date Received: Matrix: Unite:

05/21/97 Water U0I

Lab No.: Method Blank 17646-001 17646402 nwas.rt ,+ „,T- ..X ;

CBrat Sample LD.: - 1001H-T 1001H-B Data Sampled: — 05/llm 05/21/97 OCBatch 6: 097VOCWU4 Q97VOCW13I 097VOCW134

ifi

lafc: >r

DT 1

DT 16

DT 10 . •• . J •

(Moromeikaiie jfciUU l§.US.y

IK

IRSSEE

iWMSSL IKd ]«£ IK IKL 1IM ESKSSSa IKM

im ism® M Vinyl CJdortde S j ND sc ND 54 ND

™" 1

Bromomethane s S ND so ND SI ND CMoioetbane s s ND so ND SI ND - ——

T ncMoroOuoromrihane s s ND so ND SI ND 1,1 • DkMeroethene s ND so ND So Nb

• •

Mtrtiykne Chloride IS IS ND ISO ND ISO 370 •••

tram -1,2-Dictilorocthcoe s s ND so ND SO ND , ———

1,1 • Dichiaroetliafie 5 s ND so ND so ND " - •

Chloroform s s ND so ND so ND " — • * " • ~ — — •

1,2-DicMoroethaiie s s ND so ND so ND J

LLl.Tnddorocthalie 5 5 ND so ND so ND •

Carbon Tefrachloride s s ND 50 ND so ND •" • ** - —

Boam s. s ND so ND so ND l Diddoronropane s i ND so ND jo ND 1*ricMaroo(bcnc s s ND so ND so ND

I .

Bromodichlnremc thane s T ND so ND so ND 1 —

i**-

i

i

l

ri

s s ND SO ND so ND cb-l.J-Oaddoroproficac s s ND 50 ND jo ND

J

••

tram-lrMMcMorapropam s 5 ND so ND 50 ND 1 ~ ~ 1 •

1,14-Tnddoroettiatie s s ND so ND so ND Dibromeddorometbatw 5 s ND so ND so ND Btomoff S s Mi so ND So ND ToImm s s ND so ND so ND

""" 1 — —

Tetraddorsatbcne J s ND 50 ND so ND Chlorobmaene s 5 ND so ND so Nb UMbimm 5 s ND 50 ND so ND •— "

1,1,24-Tefradileroe thane s s ND so , ND so Fffi ' —

- DfeNorobemene s 5 ND so ND so ND • — — —

1,4 - 6kMbrobeiHtne ; 5 s ND so "155 50 ND " '

1,2 - Dkhlorobcntcne s s ""SID so Nb So Nb '**' 1 *

&8S&. 1 f

$iWveuSK*S& %$?<£?• 5£25«; »SurrofHr KRtc Limits 1 SRee. Urn** 1 KRec. LMta ' rm it±i DihfwwiftM wiKlhanc 110 56-1SO as SO-ISO 100 SO-ISO "

-ma • •

l fficMamduMdi IOS 66-120 84 80-120 83 60-120 "" " ——— • • V-

Toluene-dl 4-DrocnoOuorobcnzite

162

—iisi 63-121 66-133

90 as

63-121 u . | t t

95 M •

63-121 M.M. a ]«

' — a

ttfll _ - no . W r l i W 1 . _—L ' - •

DL - Me' DC iiFatfw

Reviewed/Approved By: D,,i:—s/zzfoy

*• iif h*i un^MnpdlMPM4l|>wyif a^o

JtPfcb*anced Technotofy v3 w s s ? m i s 1 0 E . 3 3 r d S t r e e t S i g n a l H i U . C A 9 0 9 0 7 T e l : 5 6 2 9 8 9 - 4 0 4 5 F a x : 5 6 2 9 8 9 - 4 0 4 0

mr 23 '97Report - WATER (ug/1) P.11/13

Method Title Last Update Response via

C:\HPCHEM\l\METH0DS\V0C3 5.M Volatile Organic Compounds Fri May 23 05:06:53 1997 Continuing Calibration

Non-Spiked Sample: Q97B2224.D

Spike Sample

Spike Duplicate Sample

File ID Sample Acq Tine

Q97S2242.D Blank SOppb MS 23 May 97 3:27 am

Q97S2243.D Blank SOppb MSD 23 May 97 3:54 am

Sample Spike Spike Dup Spike Dup RPD QC Cone Added Res Res %Rec %Rec RPD

0.0 50 61 60 122 121 1 19 ND 50 54 56 107 111 4 15 ND 50 52 52 104 104 0 16

ND 50 52 55 102 109 6 15 ND 50 51 53 102 105 3 14

Compound % Rec

1,1-dichloroethene benzene trichloroethene toluene chlorobenzene

49-154 67-128 67-130 74-123 80-122

QC Batch # : Q97VOCW134

m.

:»?•

Reviewed and Approved by: •

Organics Supervisor

Technology 15/0 E. 33rd Street Signal Hill. CA 90R07 Tel: 3 If) 0*9-404* Fnv ' If) 9*0.4040

MAY 23 '97 97 03:22PM STERLING ANALYTICAL Spike Recovery ana kfD si summary Report - WATER (ug/L) P. 12/13

Method Title Last Update Response via

C:\HPCHEM\1\METHODS\8 2 70-3.M 8270 TCL Thu May 22 11:40:42 1997 Initial Calibration

Non-Spiked Sample: R97B1148.D

Spike Sample

Spike Duplicate Sample

File ID Sample Acq Time

R97S1149.D BLK MS 1L-1ML E-5/22/97 22 May 97 12:47 pm

R97S1150.D BLK MSD 1L-1ML E-5/22/97 22 May 97 1:47 pm

Compound Sample Spike Spike ~ Cone Added Res

Dup Res

Spike %Rec

Dup %Rec

RPD . QC RPD

Limits % Rec

Phenol 0 . 0 200 71 74 35 37 5 42 12-110 2 -Chlorophenol 0.0 200 127 136 63 68 7 40 27-123 1,4 -Dichlorobenzene 0.0 100 64 71 64 71 10 28 36- 97 N-Nitroso-di-n-propy 0.0 100 70 77 70 76 9 38 41-116 1,2,4 -Trichlorobenze 0.0 100 76 86 76 86 12 28 39- 98 4 -Chloro- 3-methylphe 0.0 200 140 154 70 77 9 42 23- 97 Acenaphthene 0.0 100 67 74 67 74 11 31 46-118 4-Nitrophenol 0.0 200 75 74 37 37 1 50 10- 80 2,4-Dinitrotoluene 0.0 100 88 93 88 93 5 38 24- 94 Pentachlorophenol 0.0 200 135 146 68 73 8 50 9-103 Pyrene 0.0 100 . 80 87 80 87 8 31 26-127

«**• QC BATCH # :R978270W101

if*

Reviewed and Approved by: Date: Rene Rodriguez Organics Supervisor

Ttchmlaty 1510 F..33rd Street Signal Hill. CA 90807 Tel: 310 989-4045 Fax: 310 989-4040**'

Mttftod.

QAFto.

(Ma Fife

eoto LWOL

7143-1MW

(CAP70423-1

Oat* AnaVtad Date Otpeited-

SantptolO Ma»w

O605A7 0&25/67 17596401 WtiM

% -c rv> u)

tfl •vl

ANAtYfC UNITS ICS Con LCSRta LCSRac ME1H BLANK 3PLCONC SPKAOOEO MS RESULT MSO Rest*! %MS RCC «MS0 NEC * RCC Unit RPO Rft> 1M MOL Antfwont imqA 1JO an M NO NO :VO 4.4 4.4 88 00 04-110 0 16 0.005 Amrie moA 20 20 100 NO NO 10 4/4 4.5 60 to' 67-120 2 12 0.006 Banwii , r*1 1.0 1.1 110 NO 0.004 10 6.0 49 100 90 50-124 2 10 aooi Bwyftm mil 1.0 0 96 M NO NO 10 4.4 14 60 00 40-124 • 14 1001 CadWw* mgd • 1.0 1.0 too NO NO 10 4.4 4.4 60 00 50-122 • 11 aaoa ChmmhsB moA iso 0t$4 106 NO 0009 6.0 4.5 4.S 90 90 »«1 0 12 1003 Cobil «gll 1.0 1.1 no NO NO SO 4.0 4.6 96 90 00-116 0 9 1003 Cimr mod 2.0 2.1 106 NO 0010 5.0 6.0 SJO 100 •00 70-114 0 IS #4X73 Uad «od 2.0 2.0 100 NO NO 6.0 4.4 4.5 86 90 47-111 2 « 1005 MNytdtniw . mod 2.0 2.1 106 NO ott? 5.0 46 4.7 92 94 47-115 2 CO 1003

* ROM mod. 20 2.1 106 NO 0.004 fi.O 4.4 4.5 08 90 87 120 2 u aoas 8«Ma» nod 2J0 1.9 96 NO NO 10 4.1 4.2 02 44 41-136 2 46 1006 SiNar . 1.0 1.1 110 MO NO 5.0 4.0 3.9 00 70 24-156 2 25 1001 That!** •nod 20 20 100 NO NO SO 4.0 4.0 92 92 02-125 M 0.008 VMOOUH «4d 1.0 1.1 110 NO NO 10 4.7 4.7 94 94 67-130 0 O 0.009 21M «od 1.0 1.0 100 NO 0010 M 4.0 4.0 00 00 30-120 0 11 0.0»

U) rv)

CO

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