United States Environmental Protection AgencyOffice of Environmental Measurement & Evaluation

11 Technology DriveNorth Chelmsford, MA 01863-2431

Sample preparation and analysis was done following the EPA Region I SOP, FLASH6.SOP.

All samples were received and logged in by the laboratory according to the USEPA New England "Sample Login, Tracking and Sample Disposition Standard Operating Procedure", most current version.

Analytical Procedure:

Analyst:

John McKeown - Mail Code OSRR02-2US EPA New England R1

Analysis:Project:Project Number:

September 17, 2015

Paul Carroll

PJ'S Auto Park - Durham, MEFlash Point Determination

15090017

Laboratory Results

Flash Point determinations were made using a Stanhope-Seta Setaflash Tester. The SOP is based on ASTM Method D3278-78 " Standard Test Methods for Flash Point of Liquids by Setaflash Closed-Cup Apparatus"

If you have any questions please call me at 617-918-8340 .

Sincerely,

Results relate only to the items tested or to the samples as received by the Laboratory. This analytical report shall not be reproduced except in full, without written approval of the laboratory.

Report may contain multiple sections and each section will be numbered independently.

Data were reviewed in accordance with the internal verification procedures described in the EPA New England OEME Chemistry QA Plan.

09/10/2015Date Samples Received by the Laboratory:

15090017FLASH

Page 1 of 6

Digitally signed by Dan Boudreau DN: cn=Dan Boudreau, o=EPA, ou=EIA, email=boudreau.dan@epa.gov, c=US Date: 2015.09.17 14:26:33 -04'00'

& EPA Region 1, New England

Qualifiers:

RL = Reporting limitND = Not Detected above Reporting limitNA = Not Applicable due to high sample dilutions or sample interferencesNC = Not calculated since analyte concentration is ND.J = Estimated valueJ1 = Estimated value due to MS recovery outside accceptance criteriaJ2 = Estimated value due to LFB result outside acceptance criteriaJ3 = Estimated value due to RPD result outside acceptance criteriaJ4 = Estimated value due to LCS result outside acceptance criteria E = Estimated value exceeds the calibration rangeL = Estimated value is below the calibration rangeB = Analyte is associated with the lab blank or trip blank contamination. Values are qualified when the observed concentration of the contamination in the sample extract is less than 10 times the concentration in the blank.R = No recovery was calculated since the analyte concentration is greater than four times the spike level.P = The confirmation value exceeded 35% difference and is less than 100%. The lower value is reported.C = The identification has been confirmed by GC/MS.A = Suspected Aldol condensation product.N = Tentatively identified compound.

Page 2 of 6

Flash Point Determination

PJ'S Auto Park - Durham, ME

US ENVIRONMENTAL PROTECTION AGENCYNEW ENGLAND LABORATORY

Collected

ProductMatrix:

Field IDDate of

AnalysisLab IDFlash/ No Flash Result Degrees C Qualifier

Finite Flash PointResult Degrees C

Flash@6009/15/201515070053-0013 AB58333

Comments: Sample flashed at room temperature.

09/09/2015 20

Flash@6009/15/201515070053-0014 AB58334

Comments: Sample flashed at room temperature.

09/09/2015 21

Flash@6009/15/201515070053-0015 AB58335

Comments: Sample flashed at room temperature.

09/09/2015 21

Flash@6009/15/201515070053-0016 AB58336

Comments: Sample flashed at room temperature.

09/09/2015 22

Flash@6009/15/201515070053-0017 AB58337

Comments: Sample flashed at room temperature.

09/09/2015 21

Flash@6009/15/201515070053-0018 AB58338

Comments: Sample flashed at room temperature.

09/09/2015 20

No Flash09/15/201515070053-0019 AB58339

Comments:

09/09/2015 N/A

15090017FLASH

Page 3 of 6

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Contnct Name: Sara Evarts

Contact Phone: 9786211202

Mo: 1-091015,-13.i1i:;19-0001

C,·oler ;;:

Lab: NERLIOEME

Lab Phone: 617-918-8490

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15070053-0004 I SS-04 I PAHs Soil I 91912015 13:30 1 4 oz jar I 4C I 7

15070053-0004

15070053-0005

15070053-0005

15070053-0005

15070053-0005

15070053-0006

15070053-0006

15070053-0006

SS-04

SS-05

SS-05

SS-05

SS-05

SS-06

SS-06

SS-06

------+--------+--PCBs Soil 9/9/2015 13:30 1 4 oz jar 4C

----- - -voes Soil 9/9/2015 14:00 1 40 ml glass vial MeOH

Soil 9/9/2015 14:00

Soil 9/9/2015 14:00

1 4 oz jar 4C -

1 4 oz jar 4C Metals + Cyanide _ _ _j_ _ ___ ___j _ ____ --1-------1-- ---t--,----,----PAHs

PCBs Soil 9/9/2015 14:00 1 4 oz jar 4C

voes Soil 9/9/2015 13:45 1 40 ml glass vial MeOH

Metals + Cyanide Soil 9/9/2015 13:45 1 4 oz jar 4C

PAHs Soil 9/9/2015 13:45 1 4 oz jar 4C

SAMPLES TRANSFERRED FROM

Special Instructions: Please send results to OSC McKeown 617.918.1793. Note: samples contain suspeccted oil and gasoline. CHAIN OF CUSTODY#

Items/Reason Relinquished by (Signature and Organization) Dateff)me Received by (Signature and Organization) Datemme Sample Condition Upon Receipt

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C·GteShipped: 9i1 C':,·:o~ 5

CarnerName:

AirbillNo:

Lab# ---- 1 ;--Sample # Location

15070053-0006 SS-06 [ 15070053-0007 -- SS-104

Analyses

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CHA!N OF CUSTODY RECORD

PSs .c,u:o ParK SiteH.'.=

Contact Name: Sara Evarts

Contact Phone: 9786211202

No: 1-091015-1':!.4.539-0001

Cuc,;er #:

Lab: NERL/OEfviE

Lab Phone: 617-918-8490

I Matrix

--ISoil

Soil

) C-ollected --- j_S_ ample Time 11

· Num~b Container +._ P-reservative--,-i Lab QC 1 Conti___ 1

jg/9/2015 13:45 ____ - --r--- -~jar . 4 c-----l 9/9/20-15 '13:25 - --r --- 1i40-ml.glassvial f rvieOH - - r-

-- -r1i::n~ ---r,--_----~----,[~=~t+Cya,;d_=--- +~:::~~~ __ ::;:~~~~~ -- ~~~~--]:_~ :::;;~ ____ :~------ _I_ · --_-1 ----~0053-0007 _j___S~-:_1_()_~--- _PCBs __ _j ~o~ _ _,__!3~/2015 13:25 __ _ ___ 1_ 4 oz jar _ --~4 ~- ___ ~- __ _j

Soil 9/10/2015 09:00 \ 1 16 oz 4 C _ j

1 15070053-0007 ----~· -~·---·-

15070053-0007

SS-104

SS-104

15070053-0008 >----- -----1--------- -----

CNS2023 Cyanide

15070053-0009 fv1S01554 Metals ------

15070053-0010 TT2871 PCBs

15070053-0011 ML V0185 voes ~-----+--- ----+------

f-----

15070053-0012

15070053-0013

15070053-0014

15070053-0015

SS2324 PAHs

D-01 pH + Flashpoint

D-05 pH + Flashpoint

D-07 pH + Flashpoint

-----+Soil _______ 9/10/2015 _ 09:00 I _1__~033_lass 4 C ==~ Soil 9/10/2015 09:00 1 16 oz glass 4 C 1

---t-Soil ----9/10/2015-- 09:00 _____ 1 40mL-glas-svial- r.X~OH - I Soil - -~-- 9/10/2015 09:00 1 16 oz 4C -- ----- - - 7

Product 9/9/2015 10:14 1 8ozjar 4C I Sample

Product Sample

- ,_ 9/9/2015

9/9/2015

10:16

10:18

+--------

1 I 8 oz jar 4C

1 I 8 oz jar 4C Product Sample

'-- Product 15070053-0016 D-16 pH + Flashpoint 9/9/2015 10:21 1 I 8 oz jar 4C

15070053-0017 D-106 pH + Flashpoint

Sample

Product Sample

9/9/2015 11:29

Special Instructions: Please send results to OSC McKeown 617.918.1793. Note: samples contain suspeccted oil and gasoline.

Items/Reason Relinquished by (Signature and Organization) Date/Time Received by (Signature and Organization)

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SAMPLES TRANSFERRED FROM

CHAIN OF CUSTODY#

Date/Time Sample Condition Upon Receipt

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DateSh;pppr' '.;_'10/2015

Camt;1i\le1rn.;:

AirbillNo:

I Lab# Sample# j Location [ Analyses

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CHAIN OF CUSTODY RECORD

PJ's Auto Par'._ Si:" . ~.1E

Contact Narne: Sara Evans

Contact Phone: 9786211202

Mo: 1-091015-13.153<?-0001

Coe - : ,.;_

Lab: NE:RL/OEME:

Lab Phone: 617-918-8490

Collected i Sample TimeT -N ~:~ r c~;;-tci;;-;r- --p,;; se~~ tive-, Lab-QC __ _ l 9/9/2015 -- -- t 11 :32 - -- - -T-- -- ~8 oz jar- -- -- -i-4 C - - - --- - I

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Matrix

Product Sample

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~ )ii 9/9/2015---=113:35 ____ 1 4_o~j~ 4 C ---t-- ___ ,

Product Sample

Soil -----+-s,

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SAMPLES TRANSFERRED FROM

Special Instructions: Please send results to OSC McKeown 617.918.1793. Note: samples contain suspeccted oil and gasoline. CHAIN OF CUSTODY#

Items/Reason Relinquished by (Signature and Organization) Date/Time Re;;,eived by (Signature and Organization) Date/Time Sample Condition Upon Receipt

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