41
ROAD RESEARCH LABORATORY Ministry of Transport RRL REPORT LR 363 AIR-ENTRAINED CONCRETES: A SURVEY OF FACTORS AFFECTING AIR CONTENT AND A STUDY OF CONCRETE WORKABILITY by D. F. Cornelius, B.Sc. Materials Section Road Research Laboratory Crowthorne, Berkshire 1970

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Page 1: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

ROAD RESEARCH LABORATORY

Ministry of Transport

RRL REPORT LR 363

AIR-ENTRAINED CONCRETES:

A SURVEY OF FACTORS AFFECTING

AIR CONTENT AND A STUDY OF CONCRETE WORKABILITY

by

D. F. Cornelius, B.Sc.

Materials Section

Road Research Laboratory

Crowthorne, Berkshire

1970

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CONTENTS

Abstract

PART 1:

1.

2.

o

4.

A survey of some factors influencing the efficiency of air-entraining agents Introduction

Effect of various factors on air content 2.1 General

2.2 Effect of sand grading

2.3 Effect of sand content

2.4 Effect of cement content

2.5 Effect of organic impurities 2.6 Effect of alkali

2.7 Effect of specific surface

2.8 Effect of temperature

2.9 Effect of concrete workability

2.10 Effect of transporting concrete

Effect of entrained air on concrete strengths

Possible additions to specifications for air-entrained concretes 4.1 General

4.2 Alkali content of cement

4.3 Specific surface of cement

4.4 Organic impurities in cement

4.5 Effect of concrete temperature

4.6 Effect of entrained air on strength

Summary of existing knowledge

A study of the workability of air-entrained concretes

o

PART 2:

6. Scope of work

7. Materials and mix design

8. Experimental method

9. Results and discussion

10. Comparison of Compacting Factors and Vebe values

11. Effect of aggregate properties on workability measurements

12. Conclusions

13. Acknowledgements

14. References

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Q CROWN COPYRIGHT 1970 Extracts [rom the text may be reproduced

provided the source is acknowledged

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Ownership of the Transport Research Laboratory was transferred from the Department of Transport to a subsidiary of the Transport Research Foundation on I st April 1996.

This report has been reproduced by permission of the Controller of HMSO. Extracts from the text may be reproduced, except for commercial purposes, provided the source is acknowledged.

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AIR ENTRAINED CONCRETES: A SURVEY OF FACTORS AFFECTING

AIR CONTENT AND A STUDY OF CONCRETE WORKABILITY

ABSTRACT

Air-entrained concretes are used extensively in modern road con- struction as they are able to resist damage by frost and by the use of de-icing salts. Variations in the amount of entrained air lead to changes in concrete workability and to loss of concrete strength or durability depending upon whether there is an excess or deficiency of entrained air. The first part of the Report giwes the results of a survey of the literature which was made in order to identify the factors affecting the yield of entrained air from a given amount of admixture; suggestions are made for limiting the influence of the more important factors on site. The effect of'entrained air on con- crete strength is also described.

The second part of the Report describes a study of the effect of entrained air on the workability of various concretes as judged by the Compacting Factor test and the Vebe test which has recently become a British Standard test. These workability studies showed that the relation between Compacting Factor and Vebe value depends markedly upon the aggregate used in the concrete. Additional data are therefore presented to show the dependence of the relations between these workability measurements on the shape and surface texture of the aggregates.

PART I: ASURVEYOFSOME FACTORS INFLUENCING THE EFFICIENCY OF AIR-ENTRAINING AGENTS

I . INTRODUCTION

Air-entraining agents are used extensively for modem concrete road construction to prevent damage

by frost and by the use of de-icing salts. They have consequently been the subject Of a considerable

volume of research, particularly in America Where they have been used for many years. In countries

where frost damage is not a problem, air-entraining agent s are often used to improve the workability

and to reduce segregation, bleeding and shrinkage of concrete.

Variations in the amount of air entrained in concrete cause changes in the workability and

this can lead to difficulties in its placement. Of even greater importance are the loss of concrete

durability when insufficient air is entrained and the loss of concrete strength when an excessive

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amount of entrained air is present. It is obviously highly desirable, therefore, that the amount of

air entrained in concrete should be kept as constant as possible but site experience suggests that

• this is not always easily done. A literature review has, therefore, been carried out in order to

identify the factors influencing the yield (efficiency) of air, entraining agents, to indicate the extent

of their influence, and to consider the ways • in which such influence might be controlled on construc-

tion sites by appropriate Specifications. The effect that mixingprocedure and type of air-entraining

agent can have on the requirements for air-entraining agent is not discussed as in any given job these factors would not normally be varied.

The influence of air-entrainment on the flexural and compressive strengths of concrete is also described in this Report.

2. EFFECT OF VARIOUS FACTORS ON AIR CONTENT

2. I General Entrained air produces discrete cavities in the cement paste and these cavities do not normally

fill with water even in saturated concrete; They are thus able to relieve the hydraulic pressure

developed in capillaries in the paste in the initial stages of freezing. As freezing proceeds the

cavities limit the growth of microscopic bodies of ice in the cement paste, and thus protect thin

'shells ' of concrete surrounding them. It is therefore apparent that the thickness of cement paste

between adjacent air voids (bubble spacing) is critical, and this should be less than 0.25 mm 1 and

possibly as low as 0.05 mm 2. Bubbles should be as small as possible (their sizes usually range

from 0.05 mm to 1.25 mm in diameter) so that the total volume of entrained air is low and strength

losses due to the presence of entrained air are minimised. Although changes in the materials and

mix proportions of concrete can produce appreciable changes in the size distribution of entrained-air

voids 1,3,4,, about 9 per cent of air by volume of the mortar, properly distributed throughout the

cement paste, is usually sufficient to afford adequate durability 5.

Much of the fundamental research on factors influencing the efficiency of air-entraining agents

has been carried out on mortars but because the results of such research are equally applicable to

concretes,6, 7, data obtained with each type of material are given in this Report.

Several types of air-entraining agent are marketed and these have naturally been studied by

many research workers. However, rather more data are given herein for neutralised Vinsol resin

than for any other air-entraining agent as this is the type used most extensively in this country.

2,2 Effect of sand grading Sand grading has been reported as having a considerable influence on the quantity of air

entrained in sand-water mixtures 8, rather less influence on the air entrained in mortars and hardly

any on the air entrained in concrete 9. There is, however, conflicting evidence on this point as

Craven 10 reports that the amount of air entrained in concrete is dependent upon the quantity of sand

passing a sieve of 600 ttm aperture and retained on a sieve of 300/~m aperture (but he also varied

the cement content of his mixes at the same time and in a way that would enhance the effect attri- buted to sand grading). Walker and Bloem 11 found that the amount of air entrained in concrete is

related to fineness modulus; other studies suggest however that the relation is not general and that

it will differ for other sand gradings having the same fineness moduli.

2

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The present considered view 12 is that no one size of particle or one size group can have an

independent effect in a mixture comprising many sizes; more probably the change in air content

of a mixture is due to change in void content and possibly void size between the aggregate part ic les .

In any event, the nature of the relation between sand grading and the eff iciency of air-entraining

agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents.

2.3 Effect of sand content

The amount of ~ r that is entrained in concretes increases as the sand content of the mix

increases for concretes made both with and without air-entraining agents 13. Typical ly an increase

in sand content from 35 to 45 per cent increases the total quantity of entrained air by about 1'/2

percent (e.g. from 4~ per cent to 6 per cent).

2.4 Effect of cement content

Work on cement pastes I and on concrete 13 has shown that the amount of entrained a i rodecreases

with increasing cement content, this effect being most marked with the leaner mixes. Typical ly an

increase in cement content of 90 kg//m 3.reduces the volume of entrained air in concrete by about

1 per cent of the volume of the concrete. However, as the cement and sand contents were varied

together in these studies on concrete it is possible that observed differences in air content could he attributed, at least in part, to changes in the sand content. .~.

2.5 Effect of organic impurities ~

It has been shown 6 that cements with organic impurities, as defined by their acid-chloroform-

soluble content, require greater dosages of air-entraining agent (irrespective of the type of air-

entraining agent used) to achieve a given air content. Organic impurities in the cement have been

known to originate from ingress of lubricant at the grinding plant and such contamination of the ~ -

cement by as little as 1 part of oil ifi 5,000 can double the air-entraining agent requirement of a

concrete mix (Fig. 1).

2,6 Effect of alkali

Both the alkali content of the cement and the alkali content of the air-entraining agent i tself

affect the efficiency of the air-entraining agent. The alkali content of the cement reduces the yield

of air-entraining agents for increasing concentrations of alkali (expressed as Na20) up to about

1.5 per cent iFig. 1); increases in alkali concentration above this value have no effect . The alkali

content of the air-entraining agent i tself acts in such a way that one part of Na0H to one part of

Vinsol resin in solution gives the most entrained air in concrete for a constant dosage of Vinsol

resin l l , and Greening 6 was able to attribute differences in air content of two concretes and two

mortars to small differences in the alkali content of two neutralised Vinsol resin solutions (Table 1).

Small changes in the alkali content of an air-entraining agent do not affect its yield when

high alkali cements are used.

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TABLE I

Comparison of results with two different neutral ised Vinsol resin solutions

Na20 (per cent)

0.35

0.38

Per cent of air at equal amounts of neutralised

Vinsol resin

Concrete

5.5

7.4

Mortar

16.8

18.5

2.7 Effect of specific surface

The effect of the specific surface of cement on the yield of air-entraining agents has been

studied by grinding a single cement, with appropriate additions of gypsum, to different f inenesses .

Some of the resul ts of tes t s on a mortar and a concrete which were presented in tabular form in the

original paper 7 are given in Fig. 2. I t is clear from the regression lines of air content on specific

surface that the amounts of air entrained in both mortar and concrete are less when cement with a

high specif ic surface is used. The magnitude of this effect depends upon the type of air-entraining

agent used and can be such that the yield of an air-entraining agent is more than halved if the

specif ic surface of the cement is doubled from 2,500 to 5,000 cm2/g (Blaine).

2.8 Effect of temperature

The temperature of the mixed materials can have a marked and complex influence on the

eff iciency of air-entraining agents7,11,14. Although foaming (air-entraining) agents are usually

more effect ive in warm water than in cold and a given wieght of air occupies a greater volume at

high temperatures, these effects are more than offset by the greater loss of entrained air from the

concrete at the higher temperature and by the increase in chemical activity of the cement which

decreases the water available for the foaming process. Higher temperatures thus cause a reduction

in the amount of air entrained in the concrete for a given dosage of •admixture and Fig. 3 shows

that this decrease in air content with increase in temperature is the same for various types and

dosages of air-entraining agent. The size of this effect is such that the air-entraining agent

requirement at 20°C is about 30 per cent greater than that at 10°C.

2.9 Effect of concrete workability

A workable mix is able to hold more entrained air than a dry mix 15 but if the concrete is very

wet (slump greater than 200 ram) it is possible that the air may be mixed out of the concrete before

it is placed.

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2.10 Effect of transporting concrete

Recent experience on road-construction si tes in the U.K. has clearly demonstrated that the

air contents measured in concrete are affected by the treatment received by the concrete before it

is sampled. If sampling is carried out at the mixer, where it is convenient to measure air content

for the purpose of controlling the mix, then the measured quantity of entrained air can be significantly

higher than if it is carried out after it has been transported to the paver (Fig. 4). Not surprisingly,

it has been argued 16 that measurements of air content should be made on concrete which has received

typical job treatment in handling and in the amount of vibration it rece ives , and that whenever

practicable, the sample of concrete should be taken from the forms after vibration.

3. EFFECT OF ENTRAINED AIR ON CONCRETE STRENGTHS

The flexural strength of concrete is affected less than the compressive strength by a given amount

of entrained air 17, 18, the percentage changes in flexural strength being somewhat smaller than those

in compressive strength. This is i l lustrated by the typical data 18 given in Table 2 for two maximum

sizes of aggregate and three cement contents. In most instances the loss of concrete strength with

increasing air content is not linear, the strength loss for each one percent of entrained air increasing

with the amount of air entrained; however, no satisfactory explanation of this effect is given in the reference.

TABLE 2

Effect of entrained air on the strengths of medium-workability concretes

Cement Maximum content aggregate (kg/m3) size (mm)

225 38 19

310 38 19

390 38 19

Change in Flexural strength -- per cent

Air content

3% I 4%

- 3 . 0 - 4.8 + 4.5 + 4.4

-12 .0 - 8.1

-10 .5 - 5.7

-16 .0 -10 .4

-14 .8 - 8.4

5% 6%

- 8.5 -12 .6 + 2.0 0

-20 .0 -13 .0

-11 .0

-24 .0 -16 .2

-14 .4

Change in Compressive Strength- - per cent

Air content

[

- 1 . 2 - 7 . 2 - 1 6 . 0

• + 6 . 6 i + 6 . 8 + 5 . 0

-15 .9 -10 .8

222.0 -29 .0 -15 .2 -19 .0

-12 .3 -20 .0 -

- 9 . 9 - 1 5 . 6 -21 .0

6%

-24 .6 0

-36 ,0 "23 .4

-27 .0

The loss of concrete strength resulting from air-entrainment becomes smaller as the maximum size

of aggregate is decreased and this effect is attributed to the larger reduction in water requirement

for concretes made with the smaller size of aggregate. Strength losses due to entrained air are also

less marked in the leaner mixes (less than about 235 kg/m 3 of cement) 18, 19, and for some lean

mixes a significant increase in strength is obtained when the water content of the mix is reduced

to counteract the effect of entrained air on concrete workability 20.

5

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t

A similar study 21 of the relations between strength and air content for eight different Portland

cements using concretes with nominal air and cement contents of 4, per cent and 330 kg/m 3 respec- tively showed that even for given air and cement contents the percentage of strength loss is not

constant but depends upon the source of cement. It has also been shown I0 that for given air

and cement contents the percentage loss in strength depends upon the actual air-entraining agent

used. Shacklock and Keene 9'2 have studied the effect of entrained air upon the flexural and com-

pressive strengths of concrete for materials used in this country. In general their findings agree

with published American data described above.

4. POSSIBLE ADDITIONS TO SPECIFICATIONS FOR AIR-ENTRAINED CONCRETES

4.1 General

From the foregoing discussion it is clear that the process of entraining air in concrete is

complex ancl is affected by many factors. Some of these, such as aggregate grading, either have

relat ively lit t le influence or, as with sancl and cement contents, are unlikely to vary much in any

given job. In any event, these particular factors can be controlled on site so the extent to which

variations in them affect air-entraining agent efficiency may, for all practical purposes, be ignored.

In contrast, the factors which have considerable influence on the efficiency of air-entraining agents

and which may vary considerably on site are :-

alkali content of cement

specific surface of cement organic impurities in cement and

concrete temperature.

Ways of limiting the influence of these factors are now considered.

4.2 Alkali content of cement

If variations in alkali content of the cement are to have no influence on the efficiency of air-

entraining agents, it will be necessary to specify a minimum alkali content of about 1.5 per cent

(Fig. 1). However not only would this be outside the normal range (0.4 to 1.3) of alkali contents

for ordinary Portland cements but it would inhibit the desired increase in concrete strength after

28 clays 93 and could, in certain circumstances, leacl to alkali-aggregate reaction.

The air-entraining agent requirement of a concrete can vary by up to about 100 per cent

depending upon the alkali level of the cement so it is clearly desirable for the alkali content of

each cement delivery to si te to be stated by the supplier. It should then be possible to predict

any changes in air-entraining agent dosage that are required to accommodate changes in the alkali

level of the cement.

4.3 Specific surface of cement

The information given in this Report on the effect of specific surface on air-entraining agent

efficiency suggests that a change in specific surface from 2 500 to 3 000 cm2/g can increase the

admixture requirement by up to 25 per cent. As it is possible that this order of variation in specific

6

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surface can occur between batches of cement from the same works it is apparent that even greater

variations may be expected on sites where cement is received from two or more sources.

In order to control this source of variation it might be necessary to specify not only that the

cement should conform to B.S. 12 : 1958 (minimum specific surface of 2,250 cm2//g) but that an

upper limit to this specific surface should also be called for. Alternatively, and perhaps preferably,

cement supplied from a given source could be required to have specific surface values within a

limited range (+ 150 cm2//g, say). In these circumstances it may be an advantage on large construction

sites, where cement is obtained from more than one source, to use separate si los and mixers for

cements from different sources.

This type of system for separating the cements supplied from different sources would also help

when the alkali contents of the cements are appreciably different, and could, incidentally, reduce

the variability of the concrete production attributable to differences in the cements, particularly if

the mix proportions are suited to each particular cement.

4.4 Organic impurities in cement

It would appear from the data already considered that changes in the level of organic impurities

in the cement could give rise to the greatest changes in air-entraining agent requirement. Fortunately,

organic impurities are not likely to get into the cement in the normal course of production, so there

is little point in attempting to detect them, particularly as the normal methods of doing so are tedious

and can require extreme care. It is not envisaged, therefore, that the organic content of cements

would be measured as a routine site operation, but rather to cheek that organic impurities are not

getting into the cement (from whatever source) if large and inexplicable changes in air-entraining

agent efficiency should occur.

4.5 Effect of concrete temperature

Concrete temperature has a marked influence on the yield of air-entraining agents, reducing

their effectiveness by about 30 per cent as temperature increases from 10 ° to 20°C. However,

any changes in the temperature of the mix would normally occur slowly and therefore produce

quite small, and barely detectable, changes in the air content of concrete as discharged from the

mixer over a period of hours. It is thus quite easy to counter the effect of such changes in concrete

temperature by making small adjustments in air-entrainlng agent dosage from time-to-time during

the course of the concrete production.

4.6 Effect of entTained air on strength

The percentage change in concrete strength produced by a given amount of air depends upon

the maximum size of aggregate and the cement content of the concrete (Table 2). However, in any

given job only one maximum size of aggregate is normally used and the cement content is unlikely

to be varied significantly once the mix proportions have been established in trial mixes. The change

in concrete strength for a given amount of air should therefore remain sensibly constant in any one

construction job.

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5. SUHHARYOF EXISTING KNOWLEDGE

For a given dosage of air-entraining agent, the amount of air entrained in concrete is increased by increasing:-

sand content

alkali content of cement up to 1.5 per cent (expressed as Na20 ) concrete workability;

is decreased by increasing:-

cement content

specific surface of cement

organic impurities concrete temperature

handling and vibration;

and is not appreciably affected by changes in sand grading.

The percentage loss in concrete strength for each one per cent of entrained air is greatest for:-

high air contents

high cement contents

large maximum sizes of aggregate.

Air-entrainment produces smaller changes in the flexural strength of concrete than in the compressive strength.

8

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PART 2: A STUDY OF THE WORKABILITY OF AIR-ENTRAINED CONCRETES

6. SCOPE OF WORK

The present investigation was made to examine the effect of entrained air on the workability of

concrete for a range of concretes in order to obtain basic mix-design data, and to measure the

change in workability likely to arise on construction s i tes from changes in entrained-air con'tent of

the concrete within the limits of 3 - 6 per cent of entrained air permitted by the Ministry of

Transport 's 'Specification for Road and Bridge works'.

The opportunity was also taken to gain experience of the Vebe tes t which has been introduced

recently in the revised edition B.S. 1881 'Methods of Tes t ing Concrete ' as a method of measuring

concrete workability. Data relating the Compacting Factor to the Vebe value have, therefore, been

obtained for concretes with and without entrained air. Because it was found that the relat ions

between these two measures of concrete workability depended upon the aggregate used in the con-

crete, additional studies were made with plain concretes using aggregates widely different in shape

and surface texture.

7. MATERIALS AND MIX DESIGN

Three different coarse aggregates of 19 mm nominal maximum size were used. These were a rounded

quartzite gravel from Branston, Staffs., an irregular flint gravel from Chertsey, Surrey, and an

angular crushed granite from Charuwood, Leics .

The rounded and irregular aggregates were used with their own fine aggregates reconsti tuted

from single s izes of sand to give gradings approximately in the middle of Zones 2, 3, and 4 (Fig. 5).

The crushed-granite aggregate was used with its fines reconst i tuted either to produce a Zone 2

grading of the material as supplied from the quarry (Fig. 5 - Curve A) or to have a Zone 1 grading

fairly typical of many that are produced by the crushed-rock industry24 (Fig. 5 - Curve B); it was

al-~o used with the rounded quartzite sand reconstituted to give a Zone 2 grading.

The concrete mixes were designed, where appropriate, to Road Note No. 425 for the level of

workability required. When Zone 3 and Zone 4 sands were used the proportions of the coarse aggre-

gate were obtained by extrapolation of data from Road Note No. 4. The proportions of coarse and

fine aggregate used in these experiments are given in Table 3.

TABLE 3

Percentages of aggregate used with various gradings of fine aggregate

Aggregate size

19 - 9.5 mm 9.5 - 4.8 mm Fines

35 45 55 65 70

23 20 15 10 10

42 35 30 25 20

Fines Zones

1 2 and 4 2 and 3 3 and 4

4

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The effect of entrained air on concrete workability was studied for concretes with the combina-

tions of fine-aggregate grading and aggregate shape given in Table 4. Each concrete was used with

four levels of entrained air in the range 0 - 9 per cent and up to four aggregate/cement ratios in the

range 3.2 - 9.5. A free-water/cement ratio of 0.45 was used throughout unless otherwise indicated.

Neutralised Vinsol resin was used to entrain air in the plain concretes as designed. When

air-entraining agents were not used, the air-meter indicated that about 1 per cent of air was entrapped

within the concrete.

TABLE 4

Combinations of fine-aggregate grading and aggregate shape used at a free-water/cement ratio of 0,45

Fines

Zone

1

2

3

4

Percentage of fine aggregate

25 30 35

I

I R

AI* R

I

42

A

A = angular aggregate I = irregular aggregate R = rounded aggregate * = free-water/cement ratios of 0.40, 0.45, 0.50, 0.55

8. EXPERIHENTAL HETHOD

Coarse and fine aggregates were soaked separately for approximately 24 hours in order to obtain a

nominally complete state of absorption before mixing,'thereby preventing workability measurements

from being time-dependent as is the case when oven-dry aggregates are used. Air-entraining agent,

when required, was dispensed in about 10 per cent of the total mix water at the start of the mixing

process.

Concrete workability was measured by the Compacting Factor test and by the Vebe test as

described in B.S. 1881. Essent ia l ly the Vebe test consists of forming a slump cone within a

cylinder on a table and measuring the time in seconds required to remould the slump cone to the

shape of the cylinder when a given load is applied to the top bf the slumped concrete and the table

is subjected to precisely defined vibrations (Plates 1 to 4).

In general the degree of compaction at the end of the Vebe test is greater than that of the j

concrete in the slump cone, and so a distincti'6ii is made between the work done in remoulding the

concrete and that done in compacting it Bahrner 26 used a correction of the form:-

10

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V1 Vebe degrees =

V2 x Vebe seconds

where V 1 = remoulded volume and V 2 = volume of concrete before vibration (assumed to be equal to the volume of the slump cone).

However, it is generally held 27, 28, 29 that this correction is unnecessary for the range of workabili-

t ies encountered in normal practice and it is not given in the Vebe tes t in B.S. 1881 : 1970; all

Vebe values given in this Report will therefore be Vebe seconds.

Some difficulty was experienced in measuring accurately Vebe values for very workable con-

cretes (Vebe values less than 2 seconds) so data obtained on concretes with Vebe values less than

this are not given. The end-point of tests on concretes of very low workability (greater than 50

seconds Vebe value) was difficult to judge precisely, and estimation of the end-point could vary by

up to _+5 seconds for different operators, but this apparently large difference appears reasonable when

considered as a proportion of the measured Vebe value. In the Compacting Factor tes t some rich

concretes had a tendency to stick in the hoppers, particularly when concretes were made with angular

aggregates which had a considerable percentage of fines passing a sieve of 150 gm aperture; on

these occasions the concrete was rodded through the hoppers .

The air content of each mix was measured by the pressure method 20 and compaction of the

concrete was achieved in a standard manner by using a vibrating table. With the very workable

concretes, measured air contents could possibly be slightly low because of the tendency to vibrate

some entrained air out of the concrete even with relatively short periods of vibration. With the

concretes of very low workability measured air contents would tend to be high because of the

difficulty in vibrating out the entrapped air; on the other hand, the high internal friction of such

concretes could possibly prevent effective pressure transmission to all the entrained and entrapped

air bubbles so that a low estimate of the air content could possibly be obtained. Because of the

difficulty of compacting fully the less workable concretes, even with long periods of vibration, the

weight of the concrete compacted in a Compacting Factor receiving cylinder could be low thereby

giving an enhanced Compacting Factor value. In this type of situation the measured compacted

weight was compared with the theoretical compacted weight calculated from the mix proportions and

specific gravities of the mix constituents (Fig. 6) and when any appreciable discrepancy occurred

the theoretical compacted weight was used to give an estimate of the measured weight at full

compaction.

9. RESULTS AND DISCUSSION

Altogether about 150 measurements of Compacting Factor and Vebe value were made. From these

it was clear that the relation between the amount of air entrained in the concrete and the change

in concrete workability was not greatly affected by the range of materials or mix proportions used

(Figs. 7 and 8), although there was a tendency for concretes of high water/cement ratio and those

made with angular aggregates to exhibit a greater change in Compacting Factor for the addition of

a given amount of entrained air; this trend was less noticeable for workabilities measured by the

Vebe test.

II

Page 15: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

To a first approximation, the addition of 4~ per cent entrained air to a plain concrete increases

the Compacting Factor by about 0.06, and reduces the Vebe value by about two-thirds. It should be

noted, however, that a given change in the amount of air at low air contents produces a greater change

in workability than a similar change in the amount of air at high air contents. If the amount of

entrained air in a concrete production should vary from 3 to 6 per cent, as permitted by the Ministry

of Transport Specification for pavement-quality concrete, then the Compacting Factor will increase

by about 0.03, which is one half of the variation in Compacting Factor allowed by that specification.

The change in Vebe value (seconds) due to a comparable change in entrained air varies with the

workability of the concrete, but is such that the Vebe value for concretewith 3 per cent of entrained

air is about twice the Vebe value for the same concrete with 6 per cent of entrained air for any level

of concrete workability. Thus if limits are to be placed on workability, as measured by the Vebe

value, in any construction job it would appear more appropriate that they should be related to the

specified Vebe value by a geometric rather than an arithmetic progression.

The relative sensitivity of these tests to concretes of low workability is indicated by the

spacing of the curves in Figs. 7 and 8. The Vebe test shows much greater discrimination than the

Compacting Factor test between the two concretes represented by the circular symbols, and would

therefore appear preferable in assessing the behaviour of low-workability concretes under vibration.

The relations between workability and aggregate/cement ratio for concretes with no entrained

air and for concretes with 4~ per cent air are given in Figs. 9 and 10 for the Compacting Factor and

Vebe tests respectively. It can be seen that the addition of a given amount of air permits larger

increases in aggregate/cement ratio (for constant Compacting Factor) for concretes made with the

more rounded aggregates than for concretes made with angular aggregates. Conversely if a given

amount of air is added tO a concrete and no change in the aggregate/cement ratio is made then the

change in Compacting Factor is less for concretes made with the more rounded aggregates and

greater for concrete made with angular aggregate; this confirms the suggestion that this effect

exists30. These experiments do not support other data 20 which suggest that the change in Compact-

ing Factor due to a given amount of entrained air is influenced by the cement content of the concrete.

The effect of aggregate on the relation between the logarithm of the Vebe value and the aggregate/

cement ratio at different air contents is similar.

From the experimental data the relations between workability and water/cement ratio for con-

crete with no entrained air and concrete having 4~ per cent air are given in Fig. 11. With the

irregular aggregate used the addition of entrained air tends to produce a smaller change in work-

ability for the drier, less workable mixes (water/cement ratio less than 0.45) but produces about

the same change in workability for mixes with higher water/cement ratios; this is in broad agreement

with the findings of Wright 20.

10. COMPARISON OF COMPACTING FACTORS .AND VEBE VALUES

The Compacting Factor and Vebe values obtained in this study are plotted against each other in

Fig. 12 for concretes without entrained air and for those with more than 3 per cent air. Despite

the considerable scatter of the data, there appear to be separate Compacting Factor/Vebe relations

for concretes with and without entrained air although this type of effect has not been reported in

American studies31 on the relations between different methods of measuring concrete workability.

12

Page 16: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

It would appear that the change in 'grading' associated with the inclusion of air bubbles in the

mortar phase is sufficient to change the relation between these two measures of workability.

The curves for plain and air-entrained concretes made with gravel aggregate and natural sand

intersect at a Compacting Factor of about 0.84. Thus for pavement-quality concretes an air-entrained

concrete would be judged to be equally workable by both Compacting Factor and Vebe measurements.

For concretes of higher workability, an air-entrained concrete would appear more workable when

judged by the Vebe test than would the concrete without entrained air, even though they may have

the same Compacting Factor.

There appears to be an anomaly in the way in which the Compacting Factor/Vebe relation is

affected by the addition of entrained air. For concretes made with the gravel aggregates the

relations" for plain and air-entrained concretes intersectwhereas those of concretes made with the

crushed-rock aggregates do not, and for a given Vebe value the air-entrained concretes always have

a lower Compacting Factor.

The effect of aggregate on the Compacting Factor/Vebe relation is considerable although this

was not noted by Hughes 29 when he obtained data on the relation between Compacting Factor and

Vebe value for concretes made from a range of aggregates. The curves in Fig. 12 for the different

aggregates "are such that the Compacting Factor test discriminates against concretes made from'

crushed materials at Compacting Factor values below about 0.88, i.e. concretes made from crushed

materials would be judged to be insufficiently workable by the Compacting Factor test in comparison

with concretes made from uncrushed materials even though they may have the same Vebe value.

However, as the vibration experienced by concrete in the Vebe test is more akin to that used to

compact concrete against formwork than the single jolt experienced by the concrete in the Com-

pacting Factor test, the Vebe test may be considered to give a more realistic assessment of concrete

workability, especially with dry mixes27, 31. Thus concretes made from crushed materials which

would be judged to be of low workability by the Compacting Factor test might not be so in practice.

In view of the results obtained in this study it was decided to investigate further the role of

the aggregates in producing the observed changes in the Compacting Factor/Vebe relation.

I I . EFFECT OF AGGREGATE PROPERTIES ON WORKABILITY MEASUREMENTS

For these experiments a crushed gritstone from Ingleton, Yorkshire, a crushed flint-gravel from

Long'field, Kent, and an irregular, uncrushed, flint-gravel from Chertsey, Surrey, were used. Most

of the work was done with the fine aggregates having a Zone 1 grading as this was the natural

grading of the materials from Ingleton and Longfield. A free-water/cement ratio of 0.50 was used

throughout these experiments and the workability of the concretes was varied by changing the

aggregate/cement ratio only; none of the concretes was air-entrained. Details of the materials

and the mix proportions are given in Table 5.

The relations between the Compacting Factors and the Vebe values for concretes made from

these materials are shown in Fig. 13. The effect of aggregate on these workability relations

confirms the data already presented and gives more information on the factors causing changes

in these relations. 13

Page 17: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

W . J

I--

0

0

0

e~

N

e~

N

°,,~

0

~0

-=

0

O0

I

Ox

Ox

O0 CO O0 t~ l CO

0 0 0 ~0 0

C"x~ cq cq

~I I p , I p , I ~'b ~ i I

I~ I:I I:I I=I I= 0 0 0 0 0

l'q l'q N l~ DQ

~ ~ ~ ,

14

Page 18: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

Changes in the surface texture of the aggregate from rough to smooth for crushed aggregates

with similar gradings and shapes, change the Compacting Factor/Vebe relation from the position of

Curve A to that of Curve B. Likewise, changing the shape of the aggregate from one that is flaky

and elongated to one which is irregular produces a shift in the Compacting Faetor/Vebe relation

from the position of Curve B to that of Curve C for aggregates with smooth surfaces. Clearly, the

shift attributable to changes in the surface texture of the aggregate may not necessarily be the same

for rounded aggregate as for the crushed aggregates used here, neither will the shift due to changes

in aggregate shape necessarily be the same for aggregates with rough surfaces as for those with

smooth surfaces used here. Nevertheless the data do give some idea of the change in Compacting

• Factor/Vebe relation attributable to changes in the surface texture and the shape of the aggregates.

If the coarse aggregate used to produce Curve A is combined with the fine aggregate used to

produce Curve C, then Curve E is obtained i.e. changing the coarse aggregate shifts Curve C hardly

at all. In contrast, replacing a natural, uncrushed, flint sand of irregular shape by crushed-rock

fines of the same nominal grading accounts for nearly the whole range of movement of the Compacting

Factor/Vebe relation (i.e. from position E to position A) observed in these experiments. This

result is not altogether surprising as, although the fine aggregate comprised less than half the total

aggregate used in the concrete, its specific surface was about 15 to 20 times as great as that of

the coarse aggregate; it is therefore to be expected that the fine aggregate exerts a controlling

influence on the relation between these two measures of workability.

Finally, the effect of aggregate grading on Compacting Factor/Vebe relation was examined

using the uncrushed, irregularly shaped, flint gravel. The different gradings used (Table 4) produced

a slight change in the workability relation (Curves. C and D in Fig. 13). This is mainly due to the

greater sensitivity of the Vebe test to changes in the grading of the aggregate, as it can be seen

from Figs. 14 and 15 that changing the grading produced less change in Compacting Factor for a

given aggregate/cement ratio than the marked change in Vebe value for a given aggregate/cement

ratio. It is also clear that for concretes of low or very low workability (Compacting Factor less

than 0.85), the Vebe test has the greater sensitivity to changes in the surface texture and shape

of the aggregate.

This study has shown that the Compacting Factor and Vebe tests give different impressions

of the workability of the concrete; the question is, which is the more suitable test?

The Compacting Factor test is extremely simple and does not require electric power to be

available; it is therfore very suitable for use on construction sites. On the other hand, the Vebe

test is more sensitive to changes in the surface texture, shape, and grading of the aggregate,

particularly for concretes of low or very low workability, but it requires a power supply to drive

its vibrating table. It would therefore seem that the Compacting Factor test is more suitable as a control test on construction sites whereas the Vebe test appears superior as an aid to designing

concrete mixes because it gives a more realistic assessment of the behaviour of the concrete to be

expected under the vibration used to compact it against the forms.

12. CONCLUSIONS

. The increase in Compacting Factor and the percentage increase in Vebe value produced by the

addition of a given amount of entrained air to a concrete is not affected greatly by either the 15

Page 19: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

aggregate properties or the mix proportions of the concrete. There is, however, a tendency for

concretes made with the more rounded aggregates or lower water/cement ratios to exhibit

smaUer increases in workability for the addition of a given amount of entrained air.

2. To a first approximation, a change from 3 to 6 per cent in the amount of entrained air in a

concrete production increases the Compacting Factor by about 0.03 and halves the Vebe value

at all levels of worl~ability.

. The relation between Compacting Factor and Vebe value is most sensit ive to changes in the

surface texture of the fine aggregate. It is also affected by the shape and grading of aggregate

and by entrained air.

4. V'ebe value ismore sensit ive than Compacting Factor to changes in aggregate properties.

. The Vebe test is preferred for purposes of mix design and predicting the behaviour of concretes,

especial ly dry concretes, under vibration; but the Compacting Factor test is simpler to use

as a control tes t on site.

. When the workability of a concrete is specified as a Vebe value, it is more appropriate to choose

the upper and lower limits so that they form a geometric progression with the specified value

than that the specified value should be mid-way between them.

13. ACKNOWLEDGEMENTS

This Report was produced in the Materials Section of the Construction Division (Section Leader:

G. F. Salt). The experimental work was carried out by C. Corumluoglu and D. R. Hanger.

14. REFERENCES

. POWERS, T. C. Void sPacing as a basis fo r producing air-entrained concrete. J n l . Amer. .... "

Conc. Inst. 1954. 25 (9), 741-60.

2. POWERS, T. C. RILEM Bull. English Ed. 1958. 43/44, 97-9.

3. BRUERE, G.M. The relative importance of various physical and chemical factors on bubble

characterist ics in cement pastes . Aust. Jnl. App. Sc. 1961. 12 (1) 78-86.

4. TORRANS, P. H. and D. L. IVEY. Air void systems affected by chemical admixtures and

mixing methods. Highw. Res. Rec. No 226. Concrete admixtures, aggregates and durability.

47th Ann. Mtg. 1968.

. KLIEGER, P. Further studies on the effect of entrained air on strength and durability of

concrete with various s izes of aggregates. Highw. Res. Bd. Bul. 1956. 128, 1-19.

6. GREENING, N. R. Some causes for variation in required amount of air-entraining agent in

Portland cement mortars. Jnl. P.C.A Research and Devpt. Labs. 1967. 9 (2) 22-36.

16

Page 20: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

.

.

.

10.

11.

12.

13.

14.

SCRIPTURE, E. W. BENEDICT, S. W. and LITWINOWICZ, F . J . 'Effect of temperature and

surface area of the cement on air entrainment.' Jnl. Amer. Caner. Inst. 1951. 23 (3) 205-10.

KENNEDY, H. L. The function of entrained air in Portland cement. Jnl. Amer. Coner. Inst. 1944. 15 (6) 515-7.

SCRIPTURE, E. W., HORNIBROOK, F. B. and BRYANT, D. E. Influence of size grading of sand on air entrainment. Jnl. Amer. Concr. Inst. 1948. 20 (3) 217-28.

CRAVEN, M. A. Sand grading influence on air entrainment in concrete. Jnl. Amer. Cone. Inst. 1948. 20 (3) 205-15.

WALKER, S. and BLOEM, D. L. Studies of concrete containing entrained air. Jnl. Amer.

Cone. Inst. 1946. 17 (6) 629-39.

POWERS, T. C. Mixtures containing intentionally entrained air. Jnl. P.C.A. Res. and Devpt.

Labs. 1964. 6 (3)19-42.

SCRIP33_IRE, E. W. and LITWINOWICZ, F. J. Some factors affecting air entrainment. Jnl.

Amer. Cone. Inst. 1949. 20, (6) 433-42.

CORDON, W. A. Freezing and thawing of concrete: mechanisms and control. Amer. Cone.

Inst. Monograph No. 3. (Amer. Concr. Inst. and Iowa State University Press).

15. NEVILLE, A. M. Properties of concrete. London, 1963 (Pitman and Sons Ltd), p. 364.

16.

17.

18.

19.

20.

21.

TUTHILL, L. H. Entrained air loss in handling, placing and vibrating. Jnl. Amer. Caner.

Inst. 1948. 19 (6), 504.

GONNERMAN, H. F. Tests of concrete containing air-eutraining Portland cements or air-

entraining materials added to batch at mixer. Jnl. Amer. Cane. Inst. 1944. 15 p.477.

KLIEGER, P. Effect of entrained air on strength and durability of concretes made with various

maximum sizes of aggregates. Highw. Res. Bd. Proc. 1952. 31, 177-201.

BLANKS, R. F., and CORDON, W. A. Practices, experiences, and tests with air-entraining

agents in making durable concrete. Jnl. Amer. Cone. Inst. 1949. 20 (6) 469-87.

WRIGHT, P. J. F. Entrained air in concrete. Proc. Inst. Civ. Eng. 1953. 2 Pt. 1, Paper

5915. 337-58.

JACKSON, F. H. Age-strength relations for air-entrained concrete. Public Roads. 1952.

27 (2) 31-36.

17

Page 21: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

22.

23.

24.

25.

26.

27.

28.

29.

30.

31.

SHACKLOCK, B. W. and KEENE, P. W. Comparison of the compressive and flexnral strengths

of concrete with and without entrained air. Civ. Engng. and Publ. Wks. Rev. 1959. 54 (631)

77-80.

NEVILLE, A.M. Role of cement in creep of mortar. Jnl. Amer. Conc. Inst. 1959. 30 963-84.

d

TEYCHENNE, D. C. A survey of crushed stone sands for concrete. ]ournal of the British

Granite and Whinstone Federation. 1967, 7 (1), 53-60.

ROAD RESEARCH LABORATORY. Road Note No. 4. Design of Concrete Mixes. London 1950 H.M.S.O.

BAHRNER, V. Report on consistency tests on concrete made by means of the V.B. consisto-

meter. Joint Research Group on Vibration of Concrete. (Swedish Cement Assn. Malm~).

CUSENS, A. R. The measurement of the workability of dry concrete mixes. Mag. Concr. Res.

1956. 8 (22), 23-30.

KEENE, P. W. A preliminary examination of the V.B. consistometer. C. & C. A. Tech. Rep.

TRA/343 London 1960. (Cement and Conc. Assn.).

HUGHES, B. P. and B. BAHRAMIAM. Workability of concrete: a comparison of existing tests.

Jnl. of Mtls. 1967. 2 (3), 519-36.

CORDON, W.A. Entrained air - A factor in the design of concrete mixes. Jnl. Amer. Concr.

Inst. 1946. 17 (6), 605-20.

KLIEGER, P. Recommended practice for selecting proportions for no-slump concrete. Jnl.

Amer. Concr. Inst. 1965. 37 (1), 1-18.

18

Page 22: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

[]

Data from Ref 6

Z$ Clinker 5

I ' - I ,,

V

O ,

4

u

O_

O3

t--

U1 O~ l_

-6 I/1 ¢-

>

2

3

z~

5 % gypsum

cold grinding

Z$ n

V

0 .02% air

'~ i v

V V /. 3

/No air

V

0 0.5 1.0 . 1.5 2"0

Concentration of alkali ( as Na20 ) ( per cent by weight)

Fig. 1 EFFECT OF ALKALI CONCENTRATION ON VINSOL RESIN REQUIREMENT TO GIVE 19 PER CENT AIR IN MORTARS

MADE FROM CEMENTS, LABORATORY-GROUND wITH AND WITHOUT OIL

2.5

Page 23: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

i_

0

C

E UJ

18

16

1/,

12

10

Data from Ref. ?

~ D

Mortar (ASTM test )

Concrete (Constant workabi l i ty)

L

2000

Fig.2

3 000 4 000 Specific surface (cm2/gm) (Blaine)

EFFECT OF SPECIFIC SURFACEON AIR CONTENT OFAMORTAR AND A CONCRETE EACH WITH CONSTANT DOSAGE OF AIR-ENTRAINING AGENT (A.EA.)

5000

Page 24: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

160

0 o

0

w-

c~

L.. o--

<

I/.0

120

100

80

60

A O 0

Data from Ref.11

0"008 percent Vinso[ resin 0.020 percent Vinsol resin 26 '5ml Darex/sack

10 20 30 /.0 Concrete temperature (°C)

Fig.3 AIR CONTENrT OF CONCRETE AT VARIOUS TEMPERATURES AS A PERCENTAGE OF THAT AT 21"C FOR CONSTANT DOSAGE OF AIR-ENTRAINING AGENT

50

Page 25: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

0 Q

m "-M

r ' n

--,4

"-rt C )

( . n

0

~ 3 ¢0

Z

z - -4 m Z

U1

Q

Air content

~ o X

ET

gO

3 o" '10 4

0 " 0

'-'1

3 = - "10 0

¢D "10

0

( daily overage )

0

per cent

C~

I Q

I

"7 J

I~ (J') ~ ( , q < Q < D

~ 3 ~ 3

Q

C )

Page 26: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

" \ :g z

,

%

o .,~

L ,k', .-:-

",~,' o

0 0 0 0 0 0 0 0 0 0 0 0 (3') aO ~ ~ U~ ,,,I" ~ O4

eJn~,Jedo eAets uo4~ , Jeu!:j eSo~,ue0Jecl

Page 27: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

OJ

"10

U O Q .

E O U

O ~J

O O.t t -

l - -

13.?

13"6

13"5

13"4

13"3

i3'2

13.1

/

(6.5) O

(6.0} 0 /

'15.51} '/ /

/

/ /

/ /

/

I ReLation for~ f uL[ y- compacted concrete. ~

/ /

/

Mix details I rregutar, uncrushed flint - grovel aggregate 48 per cent of Zone 1 sand. Aggregate/cement ratios given in parenthesis Free- water / cement ratio = 0.50

13"1

Fig. 6

13"2 13"3 13"4 13"5 13"6 Measured compacted weight (kg)

COMPARISON OF MEASURED ANO THEORETICAL COMPACTED WEIGHTS FOR CONCRETES MAOE WITH VARIOUS AfGREGATE/CEMENT RATIOS

13"7

Page 28: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

L) I:;I

O~ i -

U O Q.

E O

0'96

0'92

0"88

0"84

0"80

0 .76

0 .72 " 0

Aggregate shape

Angular

I r regular

Rounded

Irregular

Irregular

Irregular Irregular

Ag0rego,e/ J Wo, er, I ,ne, cement cement content

rat io ratio (per cent)

3-2 0.45 35

6-3 0.45 35

9.5 0.45 35

4-6 0'40 35

8.9 0.55 35

8.5 0.45 30 6 '6 0.45 25

Fines zone

2 2

2

2

2

3 4

trapped

1 2 3 4 5 6 7 Total (entrapped + en t ra ined) air (per cent)

Fig. 7. EFFECT OF ENTRAINEO AIR ON THE COMPACTING FACTORS OF VARIOUS CONCRETES

Page 29: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

100

80

60

40

3O

20 (n

o

~ 10 ..Q

8

Agg regate

I Angutar I Irregular I Rounded I Irregular I Irregular

I I r r~utar 1 Irregul.ar

Aggregate/ cement

rat io

3-2 6"3

9.5 4'6 8.9

8'5 6"6

Water/ Fines cement content

ratio (per cent)

0"45 35 0"45 35

0.45 35 0.40 35 0.55 35

0.45 30 0.45 25

/ /

Entrapped

/ /

0 1 2 3 4 5 6 Total (entrapped + entrained) air (per cent)

Fig. 8. EFFECT OF ENTRAINEO AIR ON VEBE VALUES OF VARIOUS CONCRETES

? 8

Page 30: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

0"96

No entrained air

/,1/2 per cent air

A= Angular ] I : Irregu[ar I aggregate R = Rounded

Free-water/cement ratio : 0'45

Fine aggrega te : - 35 percent Zone 2 grading

(,3

¢-

( 3 .

E 0

(..3

0 92

0'88

0"84

080

0"76

0"72

A

.I

I l l l l

l \

'A

3 Z, 5 6 ? 8 9" Aggregate/cement ratio

Fig9 EFFECT OF AGGREGATE/CEMENT RATIO ON COHPACTING FACTOR FOR COHCRETES MADE WITH VARIOUS SHAPES OF AGGREGATE FOR NO ENTRAINED AIR

AND l, V2 PER CENT AIR(DERIVED DATA)

10

Page 31: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

(.,1 U~ 03 O

CO

OJ

100

80

60

40

30

20

10

8

6

No entrained air

41/2 per cent air

A = Angular I = Irregular R = Rounded

aggregate

Free-water/cement ratio = 0"45

Fine aggregate : - 35 percent Zone 2 grading

~A

A /

/ /

I I

/ /

R

// t l

r l /

/

4/ ,/

l / / I / / ,"'

/,,r / / II

II

II l I/ I

3 4 5 6 ? 8

Aggregate/cement rat io

Fig.lO EFFECT OF AGGREGATE/CEMENT RATIO ON VEBE VALUES FOR CONCRETES WITH VARIOUS SHAPES OF AGGREGATE FOR NO ENTRAINED

AIR AND 1,1/2 PER CENT AIR (OERIVEO OATA)

MADE

10

Page 32: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

U ~

c~N

O l ~ " "

. _ u 0

L- e -

O

I I I

.L. "~

r -

Z ",.t

. /

/ /

J

/ . /

/ /

/ '

/

/

0 O O C:~ 00: (Z) -4" o r ) (~1

alOeS 6Ol (s) aqaA

\ \

\ \,\

0

O

0 0

E

0

-4" ~

w

w ~

r¢~ i,=m

W Q , .

W

0

0 Unto

c~..o

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E u

. !

0 "4"

6

&.m.l

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O~ aO aO aO r'- • . . . . .

Jo~o~ 6u!~ooduJoo

Page 33: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

100

80

60

z,O

30

20

~ 10 O u

8

~ 6

0.72

Fig.12

0.76 0.80 0.8/, " 0.88 G92 G96 Compacting factor

RELATIONS BETWEEN COMPACTING FACTOR AND VEBE VALUE FOR CONCRETES MADE WITH ANO WITHOUT ENTRAINED AIR FOR DIFFERENT TYPES OF AGGREGATE -

Page 34: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

0 U

. 0

200

100

80

60

~.0

30

20

10

8

6

4

3

A

E :

o I

1.6/,

Symbot Description of aggregate Fines zone

[]

Angular, rough texture

Angutar, smooth texture Irregular, smooth texture

Irregular, smooth texture Coarse:as • Fine :as n

Free-water/cement ratio = O. 50

% ' [ ]

0.88 O. 92 O- 96 0.76 0.80 0.8&

Compacting factor

0.72 0.68

Fig. 13 EFFECT OF AG6REGATE PROPERTIES .ON RELATION BETWEEN COMPACTING FACTOR AND VEBE VALUE

Page 35: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

u O

O3 t -

O -

E O

(J

0.96

0.92

0.88

0.8/*

0.80

0.76

0-72

0.68

0.64

Symbol Description of aggregate Fines zone

• Angular, rough texture 1 A Angular, smooth texture 1 D Irregular.smooth texture 1 [] Irregular, smooth texture 3

[a~ [] Coarse as • " 1 Fine : as []

l i '~ ~ Free-water/cement ra t io=0.50

' ) .

3 4 5 6 ? 8 9 Aggregate/ cement ratio

Fig. 1/, EFFECT OF AGGREGATE / CEMENT RATIO ON COMPACTING FACTOR FOR CONCRETES MAI]E WITH VARIOUS AGGREGATES.

10

Page 36: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

0 u u~

o.

OJ .a

>

200

100

80

,60

/.0

30

20

10

8

6

3

Symbot

A rl

[]

Description of aggregate Fines zone

Angutar, rough texture Angutar, smooth texture Irregutar, smooth texture Irregutar, smooth texture Coarse:as • Fine: as A

1 1 1 3 1

Free-water / cement-ratio = 0.50

/

Fig.15

j ,,. l/:/ . / I,. ' 1 . 1 ~ /

/ , ;/j/ //7' ' ;

i I

A 5 6 ? 8

Aggregate / cement ratio

EFFECT OF AGGREGATE /CEHEII.T RATIO OH VEOE VALUE FOR CONCRETES NAOE WITH VARIOUS ~,G'GREGATES.

/

10

Page 37: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

e ,

, 7 : . ¸

PLATE 1 General view of Vebe apparatus

Neg No B2013/69

Page 38: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

S

PLATE 2 Neg No H2908/69

Concrete ready for workability measurement in Vebe apparatus

Page 39: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

I

PLATE3

End of Vebe test

Neg No H2909/69

Page 40: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

.g

.Q O

"6

c O

"6

.o u

0 u

0 u c

@

~D

0 Z

(1549) Dd635272 3,500 10170 H.P. Ltd. G1915 P R I N T E D IN E N G L A N D

Page 41: ROAD RESEARCH LABORATORY Ministry of Transport RRL … · agents is unimportant as sand grading has only a small effect on the yield of air-entraining agents. 2.3 Effect of sand content

ABSTRACT

Air-entrained concretes: a survey of factors affecting air content and a study of concrete workability: D . F . CORNELIUS, B.Sc.: Ministry of Transport, RRL Report LR 363: Crowthorne, 1970 (Road Research Laboratory). Air-entrained concretes are used exten- sively in modern road construction as they are able t o resis t damage by frost and by the use of de-icing salts. Variations in the amount of entrained air lead to changes in con- crete workability and to loss o f concrete strength or durability depending upon whether there is an excess of deficiency of entrained air. The first part of the Report gives the results of a survey of the literature which was made in order to identify the factors affect- ing the yield of entrained air from a given amount of admixture; suggest ions are made for limiting the influence of the more important factors on s i t e . The effect of entrained air on concrete strength is also described.

The second part of the Report describes a study of the effect of entrained air on the workability of various concretes as judged by the Compacting Factor test and the Vebe test which has recently become a British Standard test. These workability s tudies showed that the relation between Compacting Factor and Vebe value depends markedly upon the aggregate used in the concrete. Additional data are therefore presented to show the dependence of the relations between these workability measurements on the shape and surface texture of the aggregates.

ABSTRACT

Air-entrained concretes: a survey of factors affecting air content and a study of concrete workability: D. F . CORNELIUS, B.Sc.: Ministry of Transport, RRL Report LR 363: Crowthorne, 1970 (Road Research Laboratory). Air-entrained concretes are used exten- sively in modern road construction as they are able to. resis t damage by frost and by the use of de-icing salts. Variations in the amount of entrained air lead to changes in con- crete workability and to loss 'of concrete strength or durability depending upon whether there is an excess of deficiency of entrained air. The first part of the Report gives the results of a survey of the literature which was made in order to identify the factors affect- ing the yield of entrained air from a given amount of admixture; suggest ions are made for limiting the influence of the more important factors on site. The effect of entrained air on concrete strength is also described.

• The second part of the Report describes a study of the effect of entrained air on the workability of various concretes as judged by the Compacting Factor test and the Vebe test which has recently become a British Standard test. These workability s tudies showed that the relation between Compacting Factor and Vebe value depends markedly upon the aggregate used in the concrete. Additional data are therefore presented to show the dependence of the relations between these workability measurements on the shape and surface texture of the aggregates.