ENVIRODYNEENGINEERS

June 18, 19842044

Dr. William LangleyUSEPA, Region VI6608 Hornwood DriveMonterey Park Plaza, Building cHouston, TX 77074

Dear Dr. Langley:

Enclosed are the results of analysis of one soil sample for 2,3,7,8-TCDD fromC&se Mo. 2807 and three water samples for 2,3,7,8-TCDD from SAS 1153F. Thecontents of this report are listed on the following page.

The data for sample DF000402 was omitted from1984) because the extract was dropped in preparationsamples were analyzed according to the proctidu(July 1982). The detection limits for thes^ s.the suggested method detection limit of 0.005sample were available for analysis rather thanrecommended in Method 613.

the original report (June 1 2,ration. The three water

idure described in EPA Method 613samples are slightly higher thanug/1 because only 200 ml ofthe 1 liter sample volune

If you have any questions regarding these data, please contact me.

Sincerely,

Earl M. Hansen, Ph.D.Senior Associate

EMH/csgEnclosures

TABLE OF CONTENTS

Form NO.

B-1

B-2

B-3

B-4

Attachment No.

Data Summary

Initial Calibration Summary

Continuing Calibration Summary

GC Operating Conditions

Mass Chromatograms, Colunrj Performance Check

Mass Chromatograms Standards

Mass Chromatograms Samples

Partial Scan Data

Mass Chromatograms, Rejected Analyses

GC/MS Calculation Notebook! Pages

Analytical Chronology - GC/MS Logbook Pages

Chain of Custody/Packing list

FORM h-1. T<; l ) l ) DATA REPORT FORM

I.ab: Rr

i-asr No.

Batch/Shi

SampleNumber

MBDF000422

l)ro00424

ivirodyne

: 1153F

pnent No.

ExtraCleanup

NN

N

Er

SV

iqinee

ampleol une( m i s )

200225

212

rs , Inc

TCDDMeas

NDNO

ND

(ug/1). D.L.

0.00510.1)0770.0076O.OU87

GC/MS AnalysisInstr.1.0. Date Time

2 6/17 16172 6/17 1707

2 6/17 1808

Rel. lo32U/322

1 .051 .0)

1 .H6

n Abund.332/134

0.770.77D.8 )0 .7B

SurrogateMeas. »

y.77q.H6

10.1 1

(ng)Accy.

•)a•»•)

1)1

320

1 115

25

R322

1115

13

elative2

F

Ion57

11

5

'eport Date:

Column:

i Abundance3283

588476

582

Page 1 of 1

6/18/84

SP-2330

FRN332 334 No.

1279 1671 105541027 1339 10555

1233 1585 10557

Notes: RB = Reagent Blank P = Part ial Scan/Confirmatory Analysis D = Duplicatf /Fnrt i t ied Field BlankFB = Field Blank KRN = File Reference Number D.I,. = Detection L i m i t

M -= Native TCDD SpikeND = Not Detected

by

0 0 1 5 9 0

FORM B-1. TCni) DATA RKPORT FORM

Lab: E

CasB No

Batch/sh

Samplenumber

[1P000402

[nvirodyne ]

..: 2807

ipment No.

ExtraCleanup

N

FB = Fiffid

Engineers

WetWelyht( y r a m s )

10.0

Biflnk

i. Inc.

TCDDMeas.

Nt)

FRN =

(ppb)n.L.

0.10

File

GC/MSInstr.I .D.

2

Referencf

Analysis

Date Time

6/17 1'?12

• Nunber

Rel. 1'320/322

0.620.6H

on Abund. Surr332/334 Meas

0.77 9.74

D.T,. = n"tectj

q[ate*

./FOL i '

( n g )Accy.

l.l7

m i t

Relative320 322 25

10 15

ND = Not

Re

Ion7

9

ryt

!port Date:

Column!

Abundance328'1

650

acted

Page 1 of 1

6/18/84

SP-2330

PRN332 334 No.

1420 1853 10551!

"r-orrecteii for co by native TCDD; 0.91 of m/z 322 suht€whf{\.

0 0 1 5 9 1

FORM B-2. INITIAL CALIBRATION SUMMARY

Date(198

5/65/65/65/65/65/65/65/115/115/115/115/115/115/115/115/115/115/115/11

MeanAccuRel.

Solu

PCCC1CC2CC3CC4CC5

Instr. FRN Solution4) I.D. Number I.D.

2 10091 PC2 10092 CC12 10093 CC22 10094 CC32 10095 CC42 10096 .CC52 10099 PC2 10108 PC2 10109 CC12 10110 CC22 10111 CC32 10112 CC42 10113 CC52 10115 CC22 10116 CC42 10118 CC32 10119 CC52 10120 CC12 10121 PC

Accuracy, Surrogate Measurements:racy, Fortified/Spike Field Blank;Diff . ( % ) , Duplicate Analysis:

tion ID Codes:

= Performance check solution= Concentration calibration solution= Concentration calibration solution= Concentration calibration solution= Concentration calibration solution= Concentration calibration solution

MeasuNative

1.040.970.960.930.90

0.930.900.870.830.830.910.850.870.831 .02——

QUA]

/

=f=No. 1 =No. 2 =No. 3 =No. 4 =No. 5 =

red RFSurrogate

1.201 .091.08--

1.030.960.94--

0.93-

0.94

———1^08

[/rTY CONTROL/

———-/-/

0.2 ug/ml1.0 ug/ml5.0 ug/ml

20.0 ug/m140.0 ug/ml

TCDMean RF Used

Native Surrogate (Ap

SUMMARY '--^'^

No. of Data Pornts:Sample NO . /Sample No. /

J/iv^

D Isomer ResolutionPercent Valleyplies for PC only)

2

22

1.5

\\

- )

.ie cwf11^'

00

FORM B-3. CONTINUING CALIBRATION SUMMARY

Date Instr. FRN Solution(1984) I.D. Number I.D.

6/17 2 10552 PC6/17 2 10553 CC16/17 2 10565 PC6/17 2 10566 CC1

Mean Accuracy, Surrogate Measurements:

Accuracy, Fortified/Spike Field Blank;

Rel. Dif f . (» ) , Duplicate Analysis:

Solution ID Codes:

PC = Performance check solutionCC1 = Concentration calibration solutionCC2 = Concentration calibration solutionCC3 = Concentration calibration solutionCC4 = Concentration calibration solutionCC5 = Concentration calibration solution

MeasuNative

0.90

0.85

OUAI4r /--

———^\—--•NA

NA

NO. 1 =No. 2 =No. 3 =No. 4 =No. 5 =

red RFSurrogate

0.98

1 .07

LITY CONTROL

^

0.2 ug/ml1.0 ug/ml5.0 ug/ml

20.0 ug/ml40.0 ug/ml

TCDD Isomer ResolMean RF Used percent Valley

Native Surrogate (Applies for PC o

10.91 1.02

10.91 1.02

-SI1MMARY ^ V^

No. of Data Points: ?7.8*3 J i Y 7

•"-————^ I -

Sample /Ro. ' ' \

\ ^m P^-\ ^ ^ r / '

ut

nl

V1

v

-on

y)

^

0 0 1 5 9 3

FORM B-4. GC OPERATING CONDITIONSConditions B

Column Coating

Film thickness

Column Dimensions

Helium

Initial Temperature

Initial Time

Temperature program

2,3,7,8-TCDD Retention Time

SP-2330

0.20 urn

60 m x 0.25 mm

26 psi

160°C

3 minutes

25°/min to 240°C and hold-.

19.2 minutes

j-

l'"'1 •,

LCi• —0

ATTACHMENT 1

MASS CHROMATOGRAM, COLUMM PERFORMANCE CHECK

1368

10££2ITCDD C O L U M N PERF 1NCE CK COND B 2UL|e.-17-84 TW J(»» -w..a- ' is'e

454 fain

AA

.A--,

A

Aw"A""ABBHHI

,A^E3EOD

/ \ I'BAJJH

nEBCTO

AAA

u—A

A

A

r S | |

^

^•-•^

———'———————————————————-——————

^0

sn•;—

0

O P T I O N S

RREfl TflELE ENTRIES: FRN 10552

Entr^ T i m e

20.720.720.720.720.620.6

Mass

319.9321.9322.9327.9331.9333.9

flr-eel

2492.3160.

431.64.

599.731.

7S..1 0 0 . 1

13.'2.

18.23.

CRLCULRTE •/. ON ENTRY #:RRER TRBLE ENTRIES; PRN 10552

Entr-i^ Time

20.720.720.720.720.620.6

CRLCULRTE •/;

Mass

3 1 9 . 93 2 1 . 9 ••322.9327.9331 .9333.9

ON ENTRY «:

Rrca

2492.3180.431.64.

5 9 9 .731.

340.9435.0

58.98.7

82.0100 0

ITCDD C O L U M N PERt '^^MNCE CK COND B 2UL16-17-84 1545 J@*

^ ^l110'

ITCDD COLUMN P@ERFORMflNCE CK MI.^:»2 COHIi S 2LIL1 6 - 1 7 - 8 4 2 2 1 6 JJC

A A.M. Aii E^

A AM A

/ <

21

.A.

f l R E f l T f l E L E E N T R I E S : F R H 18565

E n t r1 y T i in e-

20. 628. 628 .£28.620.5

CflLCULRTE •/.

3 1 9 . 9321 . 9322. 9331. 9333. 9

ON ENTRY » ;

Rr-ea

6266.7966.1082.15B4.1825.

78. 9iBe.e

13.618.922.9

RREfl TRBLE ENTRIES; FRN 10565

E n t r- y T i n'i e-

1 20.62 20. 63 28. 64 20.65 20.5

CflLCULRTE •/.

Mass

3 1 9 . 93 2 1 . 93 2 2 . 9331 . 93 3 3 . 9

ON ENTRY » ;

Rrea

6286.7 9 6 6 .1062.1504.1825.

344.5436.55 9 . 3B 2 . 4

1 3 6 . 0

ITCDD COLUMN P(?Et?rORMFlNCE CK MIX«2 CONti B 2UL16-17-84 2 2 1 8 JJC

V ^—i—21

^'/^W ,o

ATTACHMENT.2

MASS CHROMATOGRAMS STANDARDS

RREfl TRBLE ENTRIES; FPH 18553

E n t r y T 1 fil 6 Mass

123456

CRLCURRER

Entry

123456

CRLCU

28.628.628.62B.620.620.6

LflTE •-:TRELE

T i m e

20.626. 626.620.626.620.6

LRTE •/.

256.93 1 9 . 93 2 1 . 9327. 93 3 1 . 9333.9

ON ENTRY »:ENTRIES: FRN

Mass

256.93 1 9 . 93 2 1 . 9327.93 3 1 . 9333.9

ON ENTRY «:

Rr'ea

1 1 1 .330.412.247.

1798.2321.

1B553

Rrea

1 1 1 .330.412.247.

1798.2321.

26.980. 1

100.660. B

436 .2563.0

4 .814.217.810.677.5

100. 0

RREfi TflELE ENTRIES: FRH 1 6 5 6 6

Entr',' T i me Rrea

28.728. 620. 620. 62 0 . 628. 6

CRLCULRTE

2 5 6 . 93 1 9 . 93 2 1 . 9327.93 3 1 . 9333.9

ON ENTRY » ;

245.803.

1063.7 1 9 .

4850.6284.

2 2 . 674.2

1 8 6 . 06 6 . 4

448.0573. 1

flRER TfiELE ENTRIES: FRN 18566

Entr;.' T i me-

20.720.628.620.620.628.6

CflLCULRTE \

Mass.

2 5 6 . 93 1 9 . 9321. 9327. 93 3 1 . 93 3 3.9

ON ENTRY » :

Rrea

245.883.

1083.7 1 9 .

4856.6264.

3 . 91 2 . 91 7 . 41 1 . 678.2

100.0

ATTACHMENT 3

MASS CHROMATOGRAMS SAMPLES3 RAMS

RREfl TRELE ENTRIES: FRH 18554

Entry T i m e Mass Rrea

123456

CRLCURRER

Entry

123456

CRLCU

26.28.28.2S.20.20.

LRTETRELE

T i r n

20.20.26.20.20.20.

LRTE

88eS88•/;

S

88888S'/,

256.3 1 9 .3 2 1 .327.331 .333.

ON ENTENTRIES

Mas

256.3 1 9 ,321 .327.3 3 1 .333.

ON ENT

999999RY *:! FRN

S.

99 ..9999RY «:

1 11 11 1

58812791 6 7 1

10554

Rrea

1 11 11 1

56812791 6 7 1

9 9 . 4105.2100.0

5475.81 1 9 1 9 . 115574.5

. 6

. 7

. 635.27 6 . 5

108.0

R R E R T f l E L E E N T R I E S : F R N 18555

Entr^' Time

1 20.82 28.S3 2 B . 74 28, 75 28.7

Mass

319.9321.9327.9331.9333.9

Rr-ea

15.15.

476.1827.1339.

180.9100. B

3179.06854.1893:3.2

CRLCULRTE •/; ON ENTRY » :RREfl TRBLE ENTRIES: FRH 18555

Entr^* T i m e

20 .620.820.720.720.7

CRLCULRTE ••'.

M&££

3 1 9 . 93 2 1 . 93 2 7 .9331 . 9333. 9

ON ENTRY » ;

Rrea

1 5 .1 5 .

476.1027.1339.

1. 11. 1

35.676.7

1 0 6 . 0

|2044-2Se7-lI53F;Dr"gS423 TOND B 2UL16-17-84 1737

-•,.-.. -i'--,A' -._'".y

787

28

f lREf l T f l B L E E N T R I E S ! F R N 18556

Entr",' T i f f i e Mass

2 0 . 628.820.820.820.8

CRLCULRTE

3 1 9 . 93 2 1 . 9327.93 3 1 . 9333. 9

ON ENTRY

20.20.

648.1537.1843.

9 9 . 7188.0

3 2 5 9 . 97727.I9 2 6 6 . 4

B R E R Tf lBLE E N T R I E S ; F R N 18556

E n t r y Time

20.828.820.820.820.8

CRLCULflTE •/.

Mass

319.9321.9327.9331 .9333. 9

ON E N T R ' i ' »:

Firea

26.20.

648.1537.1843.

1. 11. I

35.283. 4

180.0

f l R E R T R B L E E N T R I E S : FRt-1 10557

E n t r y T i m e

2 B . e20.820. S20.820.82 6 . 8

CflLCULRTE •/.

Mas-s

256. 93 1 9 . 93 2 1 . 93 2 7 .93 3 1 . 93 3 3 . 9

ON ENTRY »:

Rrea

5.25.1 3 .

582.1233.15S5.

36. 1185. 51B0. 6

4 3 1 6 . 39 1 4 8 . 9

1 1 7 6 4 . 4

FiRER TRBLE ENTRIES: FRN 10557

E n t r y T i m e

20.820.820.820.820.820.8

CRLCULRTE ;;

Mass

2 5 6 . 93 1 9 . 93 2 1 . 9 .3 2 7 . 93 3 1 . 93 3 3.9

ON ENTRY • :

flrea

5.25.13.

582.1233.15S5.

.31 . 6. 9

36.777.8

i a e . 0

™

2044-2807 :11E:THOi- BLBNK CONS E 2UL6-17-84 1846 JJC

A934

-I~19 23 £1

RRER TRBLE ENTRIES: FRN 18558

Eritr ' , ' T i m e

28.720.728.728 .720. 720.7

Mass2 5 6 . 93 1 9 . 93 2 1 . 9327.9331. 9333.9

Rr-ea

22.11.18.

743.1639.2064.

125.56 2 . 3

108.84248.19 3 6 5 . 7

1 1 7 9 5 . 6CRLCULRTE \ ON ENTRY t t :RRER TRBLE ENTRIES! FRN 10558

Ent ry T i m&

20.720.720.720.720.720.7

CRLCULRTE •/.

Mass

2 5 6 . 93 1 9 . 9 .3 2 1 . 9327.93 3 1 . 9333.9

ON ENTRY »:

Rrea

22.1 1 .18.

743.1 6 3 9 .2064.

1 . 1. 5. 8

3 6 . 07 9 . 4

100.0

B R E R T f l E L E E N T R I E S ; F R N 10559

Ent ry

1•->

3456

CRLCUflRER

Erit r','

123456

CflLCU

T 1 rn e

20. 626.620.62B. 626.620.6

LRTE 'ATRBLE

T i m e

20.620.620.620.620.620.6

LRTE \

Mass

256.93 1 9 . 93 2 1 . 9327.93 3 1 . 9333.9

ON ENTRY »;ENTRIES; FRN

Mass

256.93 1 9 . 93 2 1 . 9327.93 3 1 . 9333.9

ON ENTRY »!

Rrea

9 .10.1 5 ,

65B.1420.1853.

10559

Rrea

9 .10.1 5 .

650.1420.1853.

5 9 . 36 6 . 2

10B.04306.69 4 1 2 . 412277.0

. 5

. 6

. 835. 17 6 . 7

100. 0

ATTACHMJEMT 4

GC/MS CALCULATION NOTEBOOK PAGES

19Notebook No..D^^«

,

! ;i

•

'~r /^L^ ^, JuqA .'\; L<<V

(^VYe^-.. X" ]

'„ i-/-'' i i

^^^^^

- ———

. . . -——i

"•t-'Jfd on P«ge

',• - ' , 1 / ^Date

pRn.iFnT2C2^ -^-y o?o -APo-l-^

F-t?M^hA£) '-Tc-nTi ^ui; L»/<;i. !i=iflpf: ! i -vJ^ra ^.f i7a/-t a,i9 r-

~ » - / • ! . - ' V -/

!r R^; QA-JS-^ rc n o Co L •J Pert ^r^

: : 1 • Jol'sAa^'--/^0/^I : ; 1 , : i

, JAO/SAo) -- 7 ^[

J3aA5- / -' ^a': , 1 ' 1 • . ! ; ;

; t -PA. ' iC>.5A3 rc-r^p Li jLey<-^ isrio*+Aa'7 ;" ; ^

\ . • , 33,0 33o -/ :

. -132- ^ ; 3 ^

^ 3 ah °?^7 ••: —— - ..... 3^- . ,^'7<5?.,..

- - - - ...-5^--- -^a; r' -

^•r r.. w'- ^5'- •r ^-y -'' ! -y^l-"??? ^«3AlJ!

^ r - S.^.t - (^n- /^C ; W-t ^^j 0. 0(»

-tf.^.^Ss^ 3. o^^ -a t c ,7 - ( ^SF ; lYkT. . . . - - . - - & ^ - ? . J < - ; - .

; 23S, n ^i ^ a.? '5"^ ''

is 5, fd,T^ -' ,. - ^3.^ . . U?i . . .:

: L-^- . ^ i+l( ^„<5^)^^.&/(;^ /^<?</(f^^0.c^

; - . P-r, -.. ^ .X 30 / !,J ? T! i!^ .0. - 3

; !

•

! . , .— •

1 . . • • ' ' ' ' i . . - 1

Ji^j. f JJ.C^ ^. //^Y' ' / "S.gnea Date

/£>3 i? ^lll'l^ rnn,inu.dP,o

r ^flr. LL' ( ^^A A 7 q " ^3^.' ^^a..^ ,

^J • Jl .

ho^£ Ck ,c<rt> 8 <3^

'/o.

t1/. > ' ' '

1 CO»J.O R , c?^ .'57 --»o ''/ p o , ^ ' r iy .so^)- -

/ /n? "lOCi

o.xi-. o,.3 o ^oAa.1 ! l?• C-E

--o,9?^...o.9£..:, 7 - -

^..^•. ^.^ .............'o^,i 00

- 1 1IQQ

i i,-)0o»v.3-. O.OOS-I^-^O^

w- Q^ ^"• -- • '

\ •. \ , ,

^^*r^~^> '——\ '~^ ^ •^'

^^A . ^r

i/ ',0

% .-i———-———-- . . v0

.

— — - - . - .0

^- - .

^•^.-d-^^ Cf^Q.^t.- 1

A (TO (-t-.f'^"*' :• J

- - ,^a,^^T- '

^^ -

'ficA'.'. . .r, '

• - —

Con,.-.,,..r., •.. .

"^~ ^/^/ef.

Notebook NoP P OJ E CT_^ =>1M^aS01 -.05 P o o

^ e.^J.flLSAs .ap'44-aso q-._PO<i+icJ?. HJ:l(Ji<-—A<-V. -- .5l5^-_-^.,^-LS^.,- Jot:(t>^.- .

: _JAo._^^_i_..._JJ. ^ ^^J^, .._.. . ^_.Mt2.__._. __.. ._J^ < .J-fl-0 . . . .. _._.-_3.as . . . ,,-l^J^ .3L .

- - 333. . . . . .'(t^^ .0 ^ -. - .- ,..-33^.. ... -.AOl.^-f. JQO . .

. . . _._.-„....-.-..-.. .[.^ .. - - . ^. . - ^ - y• ^-OR ' (s" •r 'J\5aXoLJ'.yC' T'-^O^^) 0.9J^-1.0^.-^'. Iv'Ls'^O^lLm^lyr^

.C^-^- r?^ ^ x.^o / ^7<-^4 ,20L^ f Mp 9^^ ^ ^^Z «^__,. .. _ J. ,W^^^r^

—.^JC.-S.S'?. -^aoa^-^Eii?-c^ooowA, j.Ce^J B . ^u,y . Jo o^-.\. . . . . ——A57-—.- - - ^ . - " - - ^ ( ?- -^ - . - - .- . - ^ - .

. 3'5t0 . }Q ^ ^(t^ . - - - - - — . - . - - . . - -2o) 5 . . ._ ^a' .^ . y 0 C.3c3E' . . .((^"-' •' 3c - . . . . .3J.2, n^ -- n-7 .-33 ^J5i.J '". |;;0 . . . .

. . . . . . . , . . ^'\: c TJ '\5'QJi! 5 0" ao -1? 53') 0.9/ A. ' 3 c^ ^ 0</ 0 f '- Q. ;C -r^ | n

.ws. r^ - ^A-O XA'O / (/ ^o!a + /^£3y 0^--^=^- -- <? 7 . ._ . . .. . . . . .^ - ,^^i

^-<^_ - . .*—<(" - 4 " --i • "-^•y^^"-'^^ .CY.^-^. — ^C^'.y^fe.)

' . - - - - ^"/ . -'^-r1-"^c^-v^-. — ^'/c^'-y

- - - - /l/ -/(:

. . .^A. L///'"'

'- •cs - -, ^-^•^ / -- / ">.'" • ' -'^L^. ^- /^

P R OJ E CT_SQ_a3 ' OOai.57 Continued from Page- —_

Notebook No

i. rc.p0 a^O * / Orr ft. i . ^— - —^ fl . —~»<.J^c, ^-

• J^ .&5^--_-

_3ao_,__._s^_s..^...__• i^_-_39ia^. _ _.. _i .& 3 .- _. __(.£o-. _.._._. -_ai J' _''o9 •- .'c

-...3x3^ . . ' J ' 9 •[- . . ,-n .- .. . ^ - .___il3t? , -_ US^^ -/ - — _75 —•^_-__-_- - . - _ - _ _ . .

T c p p -- .^o3^j^3^J7--i£A'o^_^^o.^^.^O»S'J3 .L/^ ' 0 ^ .' -

r^ftr.^--. C?^^-^^;^^?^^^-^^^^^.?-^"^^^--^^.?., :-' '-"'/"c-. -0

?- o -

Notebook NoP R OJ E CT_ao_a3 -_ooAo^2_____<t//7lS-V

; •-$r-^J^s(^,_^LQ^_Le.,£.i. r^gp s-^o */ gp^y' 6 S,<-J! ' . .^-.-,.- &g7 an S ^ -^.s. -h,t- ^,fis^______'•- .

; - ..-.- - , , 333^ _ _ ^ ^ S J 3 3 , ^ . ___2^_K ' . ._.__. . . ._ _^ .' -_^__-_saa. _ . . J^.S 3 .. , _^..J-3... _ ._ _-^i^' .'•09 •- .•r" -^

Au) ^ i 0 ^ , r!

. _ . . .._i3a - ^y-S^<-'-^._ -_-3S ^-'. _ „_ __. _ . . - - _ _ . . • .,-,. ^-^ ___ i2 • } . _ _ _ _ _ _ L.-ti- .C-__J_o^a______________ .

T C D P ?£-- ^a3^J5-S3,!'».l Jla-Sfl'c'^-^^o.-f^.A ^0.°.5'3 ^ ./^ (- •3 ^ 1.—

':^-r.^,-- . ('.7^ q-JbJ / / ^.(-'^-"r^^a^O.O^^^^i-J 37'^'- '---'.'c 0

ATTACHMENT 5

ANALYTICAL CHRONOLOGIC - GC/MS LOGBOOK PAGES

oto^-a'iOT-^y-F f/Y\V-- lAoocdMfc^ -F KN JQJS < X .£) F/flCT m^s-^ QBT& 6 O?A,O1'ltHl TTC •)S'aJ3'C f « 7 ( » + 6/Y\V^^I»00

CftN^ •PK^^os.s-^ TCOO CB^y^^^LnS-oL crf^^> oLJ?< |KS- ;r-r<- , '^^\IS1S 3-3C Hl-t\SH -

C.R^(fl9 ^f>H IQ5~£3 TC.DD /o^e-eJ. sro»/ Co»«)t S ^AJ^J (p 30 JJC.

ci^Ndi^l ^KNJOS-S^ (3,&n4-a^o-7+(/&3^; irnfc+Yi.0 ft-x cano B A*^I w*^ ) ^•^ ^- '

CR»J(9^ ^K.^\Q££-£' £>oim-St'ro7-ft^3f--Wooo^a.3 ^-0 Q a^J?no73--3^

Cfc)J(cO| ^e.Nio&?(? o^o^•o!£o7-^A'3F.•0(t 000^3 CoNp P> oli\Vi')S'7.33'- ^^

Ce^t/^ ^HfJ105£'? o>02;^-s^o7-1^3?;0-<oooiA^ Coi^D 6 o?<J}1 ff rt & •T TCi e o & JJ-^

C^^bR 4'^^'o^^g ^o^i^-aso? n0aik°o '&LL{ Cfrn9 ft ^0)S^033-C. ' •

CRPb^f •FEO'o5£>(? ao^H-oifop-JD-Cooo^oa. ^(rrQ 6 o?-aJqia-ra'i^- ,-\

<^e^^ S")E-^)o£<i& o?Qt3i3-QQ3^7 (coa^o OptO ^"D 6 Q^J/''it-lJ-rc

CP.Md'l ^H)06(»; ^033-00^57 (,oa^3 Op-tO CCPT^ b -')-QAi'O M^ ^ r ^<

C.^^(,q ^(N^O^f;^ oioc33-OOA5L(!>OoH(( OptO C<rrS! B o^^,0^^ ^J^

C(?^fo^ ^PfJ^^fc^ o? Oo^-00^6-7. 6od^°( Oc-rr> ( rrSi 6 c^.Oa»» <~( sy-

CR^kq SR^ IO^ (<4 <^0al3-00o!&-? G0^3^0A)TD GcySfc ^^^'45 73^

C(Z»J (fq iFRt 1 0 5 b 5 T^DO <^1o^T-> PCR^ C^ ^^3. ^'- r\-'^.Aa;^ -3-3 •= . '-"

c.H^ W j?^ (o^t'G' 7 .00 ks^ l&ve/. STD^I Conofc a<i_9ol,3oo<tJ<-

ATTACHMENT 6

CHAIN OF CUSTODY/PACKING LIST

CLP Sample ManagementP.O. Box 818 - AlexandraPhone; 703/557-2490 -

Sampling Office:D^.AS.

Sampling Contact:IJIWCE 'St^H^,L-

(namey

l^ W»l,-fcfcc 1(phone)

SampleNumbers

i. nFo&Ol&i -''2. LiFftOOSOI. /

3. DFoRo4c^ ••4. O F f t ^ O M c ^5. OFftcO^OS -6. DFft f t040fc -/

7. PiFO^cyc'?- -/

8. ni-nft0</^9. D-F^O^&I

^0. 'DFoftc^lO ' '11. F.«a ^..lt "'12. F ^ i A ^>„^ •13.1».15.16.17.

IS.19.20.

Otticea, Virginia 22313FTS/557-2190

SPECIAL ANA1PACK

Sampling Date(s):^I^WDate Shipped:^lM/Site Name/Code;

^.h /^6i^w^^

Sampt.e.J Analysis,

.2 ^, ^ S'-T-fM^1 •i ,

i •i ,i 'i 't ,

1 ii (i ,( ,

/

LYTICAL SERVICE(ING LIST

Ship To: EyvJiftoOSlJt &IMHB\ . l L l f c l ^ALt.l-ATM& 6.0.

5t-. l-OLu-i> ,1<\&.l/•3,1^1

Attn:Fa.T-\- rt-fst^iAt-^

Ie DexriptionMatrix, Concentrationrtu>l /-^/i^L^k/Y-i

i

, ,

> ,• • woa.-<~-i

i / ^-^r^ "i- ^ i.

CA .—a^h

^

es For Lat

Date Sany ' yReceiveOb-^

Sample CReceip

Of

^dumber^0 ^-

a USE Only

nples Rec'd:f-^——

d By:/ - 9 - t y

^>nditionontat Labk

/

For Lab Use Only

White - SMO Copy, Yellow - Region Copy, Pink - Lab Copy for return to SMO, Gold - Lab Copy

UA ENVIRONMENTAL PROTECTION AGENCYCLP Sample Management OfficeP.O. Box 818 - Alexandria, Virginia 22313Phone: 703/557-2l|90 - FTS/557-2490

flKLX, __Atf Number^07-

SPECIAL ANALYTICAL SERVICEPACKING LIST

Sampling Office:T^l\^

Sampling Contact:3»>M-<- S^\M\^^-

(name)'

[^\U^<0.-^(.C>|•'• • (phone)

SampleNudbcrs

Sampling Date(s):5/3"-^>MDate Shipped:.^//HSit&Name/Code:

v^cVAEbW

Sampi.e.. Analysis,

Ship To:EAi»/ie.ciCMt'4E ^•"rtriEee1

laitl V-Ac-fc^"^ ®d•3+.l-o^&,^o.y^(

Attn;gai4 fta^S.o^

Ie DescriptionMatrix, Concentration

For Lab Use Only

Date Samples Rec'd:i-t-sV

Received By:,^/^-

Sample Condition onReceipt at Lab

i.2.3.t.5.6.7.8.9.

10.1 1 .12.13.14.

15.16.17.

18.19.20.

IYFC>OC,4.t5r^&&64il<.T^C.-O1^DFdiX^^Fr^^QFc>b&490n V f t n o ^ l lrip&oo4i3.nF 600 4/3DF^O^'rF,.llh\^npooo-^ai

/

-

Sl-\^&-V&^

1 1

1 ,

1 '

"

I '( 1

1 1

To at ' tsl

^fY\4A

i

•—)——

—]———

11

1 "

^v-^—a—"—'-

. Crr.

< .

\'

i

,

fT"-y uJc.^^li •K.is/ S/'li^C

For Lab Use Only

White - SMO Copy, Yellow - Region Copy, Pink - Lab Copy (or return to SMO, Gold - Lab Copy

€..»..<ONI«ici<iALrouiEC11.Office of Enforcemer

l-fl

CHAIN OF CUSTODY RECORD

REuluiJ6pint Internalioflal BIdg , 1201 .Elm St.

Dallas, Temi 75270PRO.) NO PROJECT NAME

SAMPLERS IS.,nk^J^^!S.^ -^..^C.^^9»1°"-*,$. l^^"-' -^ /—— ^ » **-

STATION LOCATION

Date/Time Received by: (Signature)RellnQuiitiad by: iS'frniuf*!

CONTAINEH

__,.g^^£.' ^^B aF.JA .'aS^ ;y^n>tfyJi_^r. i—f i if 6 r~———————,——aA ^5»s /'o. se'^d • M-> •Agl^.i.^ll/ddg^.f.,^'^' •7g^y.ffxu/<rv- Tfticirflrfl.»F.AiL*/»'. ''p -y^^^f /»/^.^iy-5%«. »p- -^F**^ •^A^f^t</'-/fc-fTi^vjt^iAv^^-_A»>^ voc^^f4*^^^k^^f.^n!FiWi s .d*.'y^Vc^£^^ t»» i tJ>^< •»<-•-

y-y^^

_y.

y^

' ^^^^ ••<:^.t/St^/g-y *'< • ••^ —

Received by: ls<yMiwel

F tloTrJt ?fP^^

^L - oV3g?

^X,v

Relinquished by: {Signature!elinquished by: {Signature! swt Date /Time Received by: {Swuturvl

•^^- ^/fy //•/^~Relinquished by: {S'ynaiufef Date Time Received by; fS'ynfti^

Received tor Labora ory by:ISiynmnf

Doinbunon. OfifnBl Arcomp«niei Shipmani. Copy 10 Cuordinalur I ield Fill

0 0