REQUEST FOR PROPOSALS BENEFICIAL REUSE ... RFP.pdfThe wastewater contains solid materials which are dewatered into a more concentrated sewage sludge cake and incinerated on site in

REQUEST FOR PROPOSALS

BENEFICIAL REUSE BIOSOLIDS INCINERATOR ASH

REGULATORY APPROVAL PROJECT

JULY 2016

BENEFICIAL REUSE OF BIOSOLIDS INCINERATOR ASH REGULATORY APPROVAL PROJECT

REQUEST FOR PROPOSAL JULY 2016

© NORTHEAST OHIO REGIONAL SEWER DISTRICT 2016 • PROPRIETARY BUSINESS INFORMATION

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This Request for Proposal (RFP) is being sent to interested parties for developing and implementing a Project for obtaining Regulatory Approval for the Beneficial Reuse of Biosolids Incinerator Ash generated at the Southerly Wastewater Treatment Center (WWTC) and Westerly WWTC for the Northeast Ohio Regional Sewer District (NEORSD). Proposals for providing these services will be received until the close of business (4:30 P.M.) on Friday, July 29, 2016. Proposals shall be no more than 25 printed pages and the font size shall be equivalent to Times New Roman 12 pt or larger (See Section 3.0). Proposals are to be delivered to: Julius Ciaccia, Chief Executive Officer Northeast Ohio Regional Sewer District 3900 Euclid Avenue Cleveland, OH 44115-2504 Attn: Robin Halperin, Manager of Regulatory Compliance Late submittals will not be considered. Questions regarding this RFP shall be directed to Robin Halperin by calling (216) 881-6600, ext. 6465 or at [email protected]. This RFP is organized as follows:

SECTION 1.0 INTRODUCTION SECTION 2.0 SCOPE OF SERVICES SECTION 3.0 PROPOSAL CONTENT & FORMAT SECTION 4.0 EVALUATION & SELECTION PROCESS

Various supporting and informational documents are referenced throughout this RFP. Unless otherwise noted, these documents are available on the Consultant and Contractor Resource Page on the District’s internet site (www.neorsd.org). Any future addenda related to this project will be posted to the NEORSD website under the “Bids and Proposals” section and within the NEORSD Sharefile system. ATTACHMENTS Attachment 1 Southerly WWTC Ash Analytical Report Attachment 2 Westerly WWTC Ash Analytical Report

mailto:[email protected]

http://www.neorsd.org/




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SECTION 1.0 INTRODUCTION 1.1 BACKGROUND INFORMATION The Northeast Ohio Regional Sewer District (District) is a political subdivision of the State of Ohio and organized under Chapter 6119 of the Ohio Revised Code. Originally named the Cleveland Regional Sewer District, it was created in 1972 to assume the ownership, operation and maintenance of wastewater collection, treatment and disposal facilities servicing the member communities in the Cleveland metropolitan area. The District currently operates three wastewater treatment plant facilities and a wastewater collection system. The District’s mission is to serve the public by providing cost-effective wastewater collection and treatment services that protect health and the environment. Southerly Wastewater Treatment Center The largest of the District’s wastewater treatment plans is the Southerly Wastewater Treatment Center (WWTC) located at 6000 Canal Road, Cuyahoga Heights, Ohio. Southerly serves a population of more than 601,000 in the Greater Cleveland area with an average daily flow of 125 million gallons per day (mgd). The facility can provide complete treatment to a maximum of 400 mgd, and an additional 335 mgd of storm water can receive primary treatment only. The plant receives wastewater 24 hours per day, seven days a week. The plant also receives and processes biosolids from the Easterly Wastewater Treatment Plant (WWTP). The wastewater contains solid materials which are dewatered into a more concentrated sewage sludge cake and incinerated on site in three (3) Fluidized Bed Incinerators (FBIs). Ash from the FBIs is mixed with water and conveyed as a slurry to one of three (3) ash lagoons. The ash lagoons are located at the southern end of the property, south of Canal Road between the Ohio Canal and the Cuyahoga River. In the lagoons, the ash is allowed to settle by gravity and the carrier water is returned to the WWTC for processing. A copy of the most recent analytical results for Southerly ash is found in Attachment 1. Ash is generated year round. After a period of time, the accumulated ash in the lagoons must be removed to allow room for new ash. Each lagoon holds approximately 30,000 cubic yards of ash. The Southerly WWTC generates approximately 25,000 – 30,000 cubic yards of ash each year. Previous ash lagoon cleaning projects entailed cleaning of the lagoons and placing the ash on-site in the South Fill Area and North Fill Area. The District no longer has space to store the ash removed from the lagoons due to the closure of the South Fill Area in 2007. Westerly Wastewater Treatment Center The Westerly WWTC sits on a 14-acre triangular site directly east of Edgewater State Park on the shore of Lake Erie. Westerly serves approximately 103,000 residents from Cleveland's west side. This treatment plant processes an average flow of 26 mgd of wastewater, and has a Combined Sewer Overflow Treatment Facility, which provides storage for 6 million gallons and preliminary treatment and settling for up to 300 mgd during wet weather flows. The plant




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receives wastewater 24 hours per day, seven days a week. Sludge removed from the wastewater treatment process is incinerated on-site in two (2) Multiple Hearth Incinerators (MHIs). Since Westerly lacks storage space for ash, the ash is removed from the MHIs and placed directly into hauling trucks for disposal. Westerly generates approximately 5,000 dry tons a year of ash. Approximately 330 truckloads of ash each year are removed from the Westerly WWTC. A copy of the most recent analytical results for Westerly ash is found in Attachment 2. 1.2 PROJECT PUPROSE The District is soliciting proposals for innovative, environmentally-friendly, sustainable and cost-effective approaches to reuse of the ash material from the Westerly and Southerly WWTCs. It is the District’s intent to hire one or more firms (Consultant) for Professional Services to identify viable reuse options for the ash and obtain the necessary regulatory approval for the identified reuse options. Consultants with beneficial reuse options for the District’s biosolids incinerator ash that are successful in obtaining the necessary regulatory approval will be eligible to submit proposals for the subsequent work which includes management of the Southerly Ash Lagoons and reuse of the District’s ash from Southerly and Westerly WWTCs.




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SECTION 2.0 SCOPE OF SERVICES

2.1 REQUESTED SERVICES The District is seeking consulting services for the following tasks: Task 1 – Reuse Options Identify innovative, environmentally responsible, cost-effective and sustainable solutions for the reuse of the ash material generated at Southerly and Westerly WWTCs. The District, in consultation with the Consultant, will select the most promising solutions for which to pursue regulatory approval.

Task 2 – Regulatory Approval Obtain Regulatory approval for the selected reuse options. Consultant shall conduct any required research, testing or other analyses needed to obtain regulatory approval for the reuse options. Consultant shall provide draft permit/regulatory approval applications for District review and approval prior to submission to the appropriate regulatory agency. Consultant shall respond to inquiries from regulatory agencies relating to the regulatory approval process for the selected beneficial reuse options.

Task 3 – Summary Report Prepare a Summary Report detailing the approved ash reuse option(s), implementation considerations, and estimation of the environmental benefit for each reuse option(s).

2.2 PROJECT MANAGEMENT Project Management is a critical activity to be included within the execution of all tasks identified above. Utilize procedures related to cost estimating, scheduling, project documentation, risk management, QA/QC and others as necessary to enhance budget, scope and time management. In order to ensure that tasks authorized under this contract are successfully completed in a timely manner and to the satisfaction of the District, the selected Consultant(s) shall provide Monthly Project Summary Reports, conduct Project Meetings as required and prepare Monthly Invoices. 2.3 DELIVERY OF SERVICES The selected Consultant(s) shall deliver all services under this RFP in a timely and effective manner to meet the District’s needs. The specific schedule for each task will be agreed upon between the District and the Consultant(s) at the time of contract award. The selected Consultant(s) shall begin work immediately upon authorization to proceed and shall adhere to the schedule mutually agreed upon by the District and the Consultant for said task. Adequate time shall be built into the schedule for each task to allow for sufficient review time of any data




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reports, permit applications, documents, etc. by District staff. All of these elements shall be discussed in a kickoff meeting to clarify the services requested. The selected Consultant(s) shall prepare and deliver all reports and deliverables in a professional, timely and efficient manner to the District. The exact deliverables and their associated timeframe will be determined jointly by the District and the Consultant(s) at the time of contract award. All reports shall include essential photographs, laboratory analyses, diagrams, maps, etc. 2.4 TRANSFER OF RECORDS It is the intent of the District that the work effort be conducted in a manner that maximizes the District’s flexibility regarding follow-up studies or compliance related efforts and other District projects. Software and software programs that would be necessary to achieve this shall be made available to the District. Utilization of proprietary software which cannot be made available to the District at the end of this project will not be allowed, unless it is essential for the project and unavoidable (e.g., air modeling). All records (project reports, meeting notes, data files, project data, original tracings, maps, field sketches, lab reports, data, graphic originals, electronic files, etc.) generated shall be the property of the District and shall be turned over to the District upon completion or as directed. All deliverables are required to be delivered to the District in hardcopy and electronic (original software and PDF) format. Depending on the size of the electronic deliverables, the Consultant may be required to provide and utilize portable hard drive(s) for delivery.




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SECTION 3.0 PROPOSAL CONTENT & FORMAT Each Consultant shall submit one original and four (4) copies of the proposal, as well as an electronic version, in .pdf format with bookmarks, on either a CD or USB drive. The font size on all submitted materials shall be equivalent to Times New Roman 12 pt or larger. Proposals shall be no more than 25 printed pages, with hard copies printed on sheets of double-sided recycled paper. All pages will be counted (i.e., each side of a sheet will count as a unique page, so one double-sided sheet will be counted as two pages) unless indicated otherwise in this RFP. Sheets that are 11”x17” shall be counted as two pages per side, or four pages if double sided. The following information shall be included in the proposal: 3.1 EXECUTIVE SUMMARY Include a concise synopsis of the proposal focused on how the Consultant will address the District’s key issues with the Consultant’s approach to the requested services as described in Section 2.0. 3.2 QUALIFICATIONS Because of the time sensitivity and critical nature of the work described within this RFP, the District seeks services from highly experienced and qualified Consultants. The Consultants must be able to staff this project with qualified individuals, experienced in the key technical disciplines needed, who shall remain committed to this work from inception through completion. A clear and comprehensive organization chart must be presented to illustrate the organization of the team and key team members, including subconsultants. The District is looking for Consultants that will provide excellent service and deliver quality work for the District. The District expects this quality service to extend through the entire duration of the Project. In this section of the Proposal, present the capabilities, skills, and experience of your firm/team, project manager and key technical staff. These factors will be strongly considered in selecting the successful Consultant for this Project. Consultant Qualifications Provide a statement of the firm’s/team’s qualifications, including brief resumes of key staff members (excluding the proposed project manager, who should be addressed as noted in below) and/or subconsultants proposed to work on the project. The information should be focused on experience on similar and/or complementary projects. The roles proposed for each subconsultant as well as their qualifications in that area shall also be identified in the Proposal. Your ability to identify and highlight key staff in the Proposal will be considered when evaluating your understanding of the Project.




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Include a description of three (3) of the most recent projects/programs/efforts that included similar scope of work. The following information shall be included for each project:

• Client • Client contact information • Project Description • Start and end dates of project • Key staff member’s role • Consultant fees and overall project budget • Consultant’s role in project – highlight roles of staff • Contact information of reference person for project Owner

It is expected that the Consultant will honor its proposed project staffing and proposed key individuals indicated as assigned to the project. Substitutions will not be allowed for the convenience of the Consultant. In the event a proposed individual becomes unavailable the firm must propose, in advance and in writing, a substitution. The District reserves the right to accept or reject any and all proposed substitutions. Proposed Project Manager The District expects the proposed project manager to lead the Consultant project team, be the single point of accountability for project delivery, and provide the primary point of communication between the District and project team. Describe the proposed project manager’s experience on similar projects, experience on other District projects, and skills and results supporting the ability to serve the District. The project manager is considered the most important key team member, and will be committed for the Project’s duration. Any change in project manager, or any other key team member, will require prior approval by the District. The Consultant’s proposed project manager must be experienced in projects of the magnitude and complexity of the services the Consultant is proposing to provide. It is expected that the Consultant’s proposed project manager will be available for frequent personal interaction with the District. In addition, the project manager must meet the following requirements:

• Must be experienced in multi-disciplined projects of the nature outlined in this RFP. • Must have had a key role in projects of similar or complementary nature. • Must have managed projects of a similar or greater complexity and/or size.

Previous Performance on District Projects Summarize your firm’s/team’s experience on District Projects. List the District staff that you worked with and would be most familiar with your work. Your prior performance on District projects is an important consideration in the selection process. The successful Consultant’s performance will be formally evaluated on this Project for use in subsequent procurements.




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Consultants that do not have prior experience working for the District will receive a neutral rating for this evaluation criterion. Business Opportunity Program Participation The District encourages MBE/WBE and SBE participation on this project; however, no specific subcontracting goals have been established. All certified firms will receive notification of the RFP and have the opportunity to submit individually or as a part of a team. While there are not specified goals, teaming with District-certified MBE/WBE and SBE firms will be considered as part of the proposal evaluation. The Consultant shall provide a summary of the proposed percentage of Minority and Women Business Enterprises (MBE/WBE) and Small Business Enterprises (SBE) participation in the project. 3.3 TECHNICAL APPROACH The Consultant’s technical approach to the project is a very important component of the selection. In the Proposal, the Consultant(s) is requested to demonstrate their project understanding, provide a summary of the critical issues, and describe the Consultant’s proposed sequence of activities to meet the District’s objectives. Project Understanding The Consultant should concisely demonstrate its understanding of the services for which they are submitting a proposal in this section of the Proposal. Key activities and approaches that improve the chances of success should be presented, along with key issues/challenges and how they will be addressed. Reuse Options The Consultant shall detail the proposed reuse options to be explored under this contract. For each proposed reuse option include, at a minimum, the following:

• Volume of ash on an annual basis • Material Processing Description • End Use/Users • Regulatory Approval Process • Challenges/Concerns

Critical Issues The Consultant should include a description of what they view as the critical issues associated with the contract and the attainment of regulatory approval in this section of the Proposal. Regulatory Approval Process The Consultant shall provide a detailed description of the process to be used to obtain regulatory approval for each proposed reuse option. This includes identifying the need for




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additional testing, analysis or other data gathering. Consultant shall demonstrate a thorough understanding of the process that is required to obtain regulatory approval for each proposed reuse option. Project Schedule The Consultant shall provide a schedule for the work to be performed including key milestones. 3.4 FEE PROPOSAL The Consultant shall provide a Fee Proposal which includes all costs associated with obtaining regulatory approval for each beneficial reuse option proposed. 3.4 STATEMENTS The Consultant(s) shall include a statement confirming that no personal or organizational conflicts of interest are known to exist. 3.5 DETAILED RESUMES Detailed resumes for key team members may be included as an appendix. No more than two pages per resume. Pages in this appendix are not included toward the total page count.




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SECTION 4.0 EVALUATION & SELECTION PROCESS 4.1 WRITTEN PROPOSALS The written Proposals will be evaluated and scored by a District Selection Committee utilizing the following criteria:

Written Qualifications - 30% of Total Score • Firm/Team Qualifications – 15% • Proposed Project Manager – 15%

Technical Approach - 70% of Total Score

• Project Understanding – 10% • Reuse Options – 20% • Critical Issues – 10% • Regulatory Approval Process -20% • Project Schedule – 10%

4.2 INTERVIEWS Upon completion of the scoring and ranking of the written submittals, the District may select the top ranked firms to deliver a presentation and provide further clarification of their approach. The District may prepare and submit a list of questions to each of the short-listed firms to address during their interview. Upon completion of interviews, the District Selection Committee will score each firm according to the following criteria:

Presentation & Interview (50 additional points) • Quality and clarity of presentation – 10 points • Project Manager’s ability to communicate project understanding – 15 points • Team Support on Project Understanding and Questions – 10 points • Adequacy of Response to District Questions – 15 points

For evaluations taken to the presentation stage, the scores for the Presentation and Interview will be combined with the scores from the evaluation of the written submittals to determine the overall ranking of the short-listed firms.

END OF RFP

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Canton4101 Shuffel Street NWNorth Canton, OH 44720Tel: (330)497-9396

TestAmerica Job ID: 240-65485-1Client Project/Site: SOUTHERLY WWTC-ASH (SWWTC)

For:Northeast Ohio Regional Sewer District3900 Euclid AvenueCleveland, Ohio 44115

Attn: Ms. Sarah Rehner

Authorized for release by:6/14/2016 3:21:21 PM

Nathan Pietras, Project Manager II(330)[email protected]

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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https://secure.testamericainc.com/TotalAccess/login.aspx

http://www.testamericainc.com/AskTheExpert/Expert_index.htm

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Table of Contents

Client: Northeast Ohio Regional Sewer DistrictProject/Site: SOUTHERLY WWTC-ASH (SWWTC)

TestAmerica Job ID: 240-65485-1

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Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44

Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 51

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52

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Definitions/GlossaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District

Project/Site: SOUTHERLY WWTC-ASH (SWWTC)

Qualifiers

GC/MS VOA

Qualifier Description

B Compound was found in the blank and sample.

Qualifier

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

* LCS or LCSD is outside acceptance limits.

GC/MS Semi VOA



Qualifier


F1 MS and/or MSD Recovery is outside acceptance limits.

GC Semi VOA


X Surrogate is outside control limits

Qualifier

Metals



Qualifier


General Chemistry



Qualifier

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Case NarrativeClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65485-1Project/Site: SOUTHERLY WWTC-ASH (SWWTC)

Job ID: 240-65485-1

Laboratory: TestAmerica Canton

Narrative

Job Narrative240-65485-1

Comments

No additional comments.

Receipt

The sample was received on 6/1/2016 10:20 AM; the sample arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 2.3º C.

GC/MS VOA Method(s) 8260B: The laboratory control sample (LCS) for preparation batch 240-233606 and analytical batch 240-233711 recovered

outside control limits for 1,1,1-trichloroethane. This analyte was biased high in the LCS and was not detected in the associated samples;

therefore, the data have been reported.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

GC/MS Semi VOA

Method(s) 8270C: The laboratory control sample (LCS) for 233013 associated with sample SOUTHERLY WWTC-ASH (SWWTC) (240-65485-1), recovered outside control limits for the following analyte: N-Nitrosodiphenylamine. This analyte was biased high in the LCS and was not detected in the associated sample; therefore, the data have been reported.

Method(s) 8270C: The laboratory control sample (LCS) for 233761 recovered outside control limits for Caprolactam. The associated

sample, SOUTHERLY WWTC-ASH (SWWTC) (240-65485-1), was re-prepared and re-analyzed with the Caprolactam recovery in the LCS (prep batch 234253) again failing to meet acceptance criteria. The initial results have been reported as has Caprolactam from the reextracted results.


GC Semi VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

General Chemistry

No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

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Method SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District


Method Method Description LaboratoryProtocol

SW8468260B Volatile Organic Compounds (GC/MS) TAL CAN

SW8468270C Semivolatile Organic Compounds (GC/MS) TAL CAN

SW8468081B Organochlorine Pesticides (GC) TAL CAN

SW8468082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography TAL CAN

SW8466020A Metals (ICP/MS) TAL CAN

SW8467470A Mercury (CVAA) TAL CAN


SW8467196A Chromium, Hexavalent TAL CAN

EPAMoisture Percent Moisture TAL CAN

Protocol References:

EPA = US Environmental Protection Agency

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL CAN = TestAmerica Canton, 4101 Shuffel Street NW, North Canton, OH 44720, TEL (330)497-9396

TestAmerica Canton

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Sample SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Solid 05/31/16 13:25 06/01/16 10:20

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Detection SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District


Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC) Lab Sample ID: 240-65485-1

☼Acetone

RL

20 ug/Kg

MDL

5.7

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA1J B6.2 8260B

☼2-Butanone (MEK) 20 ug/Kg1.1 Total/NA12.8 J B 8260B

☼Toluene 5.0 ug/Kg0.27 Total/NA10.69 J 8260B

Chloroform 1.0 ug/L0.25 SPLP11.3 B 8260B

Methylene Chloride 1.0 ug/L0.33 SPLP13.0 B 8260B

☼Naphthalene 6.6 ug/Kg0.81 Total/NA14.0 J 8270C

Naphthalene 0.19 ug/L0.060 ASTM Leach10.31 8270C

☼Silver 0.19 mg/Kg0.0014 Total/NA22.8 B 6020A

☼Aluminum 9.6 mg/Kg0.60 Total/NA27800 B 6020A

☼Arsenic 0.96 mg/Kg0.025 Total/NA25.9 B 6020A

☼Barium 0.96 mg/Kg0.21 Total/NA2120 6020A

☼Beryllium 0.19 mg/Kg0.011 Total/NA20.28 B 6020A

☼Cadmium 0.19 mg/Kg0.0036 Total/NA21.2 B 6020A

☼Cobalt 0.19 mg/Kg0.0016 Total/NA235 B 6020A

☼Chromium 0.39 mg/Kg0.058 Total/NA248 B 6020A

☼Copper 0.39 mg/Kg0.094 Total/NA2100 B 6020A

☼Iron 19 mg/Kg3.1 Total/NA219000 B 6020A

☼Manganese 0.96 mg/Kg0.12 Total/NA21000 B 6020A

☼Nickel 0.39 mg/Kg0.038 Total/NA2750 B 6020A

☼Lead 0.19 mg/Kg0.043 Total/NA224 B 6020A

☼Antimony 0.39 mg/Kg0.014 Total/NA20.39 6020A

☼Selenium 0.96 mg/Kg0.039 Total/NA21.0 B 6020A

☼Thallium 0.39 mg/Kg0.018 Total/NA20.11 J 6020A

☼Vanadium 0.96 mg/Kg0.036 Total/NA214 6020A

☼Zinc 3.9 mg/Kg0.48 Total/NA294 B 6020A

☼Calcium 190 mg/Kg21 Total/NA212000 B 6020A

☼Potassium 190 mg/Kg4.7 Total/NA22000 B 6020A

☼Magnesium 190 mg/Kg3.9 Total/NA282000 B 6020A

☼Sodium 190 mg/Kg8.4 Total/NA2410 B 6020A

Aluminum 50 ug/L9.0 ASTM Leach111000 6020A

Arsenic 5.0 ug/L0.49 ASTM Leach110 6020A

Barium 5.0 ug/L1.1 ASTM Leach129 6020A

Beryllium 1.0 ug/L0.053 ASTM Leach10.33 J 6020A

Cadmium 1.0 ug/L0.061 ASTM Leach10.44 J 6020A

Cobalt 1.0 ug/L0.021 ASTM Leach10.45 J B 6020A

Chromium 2.0 ug/L0.60 ASTM Leach13.9 6020A

Nickel 2.0 ug/L0.23 ASTM Leach10.33 J B 6020A

Lead 1.0 ug/L0.11 ASTM Leach10.17 J 6020A

Antimony 2.0 ug/L0.16 ASTM Leach13.4 6020A

Selenium 5.0 ug/L0.25 ASTM Leach123 B 6020A

Thallium 1.0 ug/L0.074 ASTM Leach10.27 J 6020A

Vanadium 5.0 ug/L0.23 ASTM Leach181 6020A

Calcium 1000 ug/L240 ASTM Leach178000 6020A

Potassium 1000 ug/L30 ASTM Leach14200 6020A

Magnesium 1000 ug/L48 ASTM Leach11100 6020A

Sodium 1000 ug/L68 ASTM Leach11700 B 6020A

Mercury 0.20 ug/L0.090 ASTM Leach10.093 J B 7470A

Cr (VI) 0.020 mg/L0.0021 ASTM Leach10.0058 J 7196A

TestAmerica Canton

This Detection Summary does not include radiochemical test results.

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Client Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District


Lab Sample ID: 240-65485-1Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Matrix: SolidDate Collected: 05/31/16 13:25

Date Received: 06/01/16 10:20

Method: 8260B - Volatile Organic Compounds (GC/MS) - SPLPRL MDL

Acetone ND 10 0.94 ug/L 06/08/16 20:25 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

1.0 0.35 ug/L 06/08/16 20:25 1Benzene ND

1.0 0.29 ug/L 06/08/16 20:25 1Dichlorobromomethane ND

1.0 0.56 ug/L 06/08/16 20:25 1Bromoform ND

1.0 0.44 ug/L 06/08/16 20:25 1Bromomethane ND

10 0.53 ug/L 06/08/16 20:25 12-Butanone (MEK) ND

1.0 0.38 ug/L 06/08/16 20:25 1Carbon disulfide ND

1.0 0.43 ug/L 06/08/16 20:25 1Carbon tetrachloride ND

1.0 0.25 ug/L 06/08/16 20:25 1Chlorobenzene ND

1.0 0.32 ug/L 06/08/16 20:25 1Chloroethane ND

1.0 0.25 ug/L 06/08/16 20:25 1Chloroform 1.3 B

1.0 0.44 ug/L 06/08/16 20:25 1Chloromethane ND

1.0 0.30 ug/L 06/08/16 20:25 11,1-Dichloroethane ND


1.0 0.45 ug/L 06/08/16 20:25 11,1-Dichloroethene ND

1.0 0.25 ug/L 06/08/16 20:25 11,2-Dichloropropane ND

1.0 0.46 ug/L 06/08/16 20:25 1cis-1,3-Dichloropropene ND

1.0 0.56 ug/L 06/08/16 20:25 1trans-1,3-Dichloropropene ND

1.0 0.25 ug/L 06/08/16 20:25 1Ethylbenzene ND

10 0.48 ug/L 06/08/16 20:25 12-Hexanone ND

1.0 0.33 ug/L 06/08/16 20:25 1Methylene Chloride 3.0 B

10 0.99 ug/L 06/08/16 20:25 14-Methyl-2-pentanone (MIBK) ND

1.0 0.45 ug/L 06/08/16 20:25 1Styrene ND

1.0 0.22 ug/L 06/08/16 20:25 11,1,2,2-Tetrachloroethane ND

1.0 0.31 ug/L 06/08/16 20:25 1Tetrachloroethene ND

1.0 0.23 ug/L 06/08/16 20:25 1Toluene ND

1.0 0.22 ug/L 06/08/16 20:25 1Trichloroethene ND

1.0 0.29 ug/L 06/08/16 20:25 1Vinyl chloride ND

2.0 0.52 ug/L 06/08/16 20:25 1Xylenes, Total ND

1.0 0.44 ug/L 06/08/16 20:25 11,1,1-Trichloroethane ND *

1.0 0.24 ug/L 06/08/16 20:25 11,1,2-Trichloroethane ND

1.0 0.45 ug/L 06/08/16 20:25 1Cyclohexane ND

2.0 0.82 ug/L 06/08/16 20:25 11,2-Dibromo-3-Chloropropane ND

1.0 0.32 ug/L 06/08/16 20:25 1Ethylene Dibromide ND

1.0 0.32 ug/L 06/08/16 20:25 1Dichlorodifluoromethane ND

1.0 0.26 ug/L 06/08/16 20:25 1cis-1,2-Dichloroethene ND

1.0 0.30 ug/L 06/08/16 20:25 1trans-1,2-Dichloroethene ND

1.0 0.35 ug/L 06/08/16 20:25 1Isopropylbenzene ND

10 2.3 ug/L 06/08/16 20:25 1Methyl acetate ND

1.0 0.20 ug/L 06/08/16 20:25 1Methyl tert-butyl ether ND

1.0 0.45 ug/L 06/08/16 20:25 11,1,2-Trichloro-1,2,2-trifluoroethane ND

1.0 0.32 ug/L 06/08/16 20:25 11,2,4-Trichlorobenzene ND

1.0 0.25 ug/L 06/08/16 20:25 11,2-Dichlorobenzene ND



1.0 0.49 ug/L 06/08/16 20:25 1Trichlorofluoromethane ND

1.0 0.43 ug/L 06/08/16 20:25 1Chlorodibromomethane ND

1.0 0.43 ug/L 06/08/16 20:25 1Methylcyclohexane ND

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1,2-Dichloroethane-d4 (Surr) 100 78 - 125 06/08/16 20:25 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

4-Bromofluorobenzene (Surr) 83 06/08/16 20:25 161 - 120

Toluene-d8 (Surr) 92 06/08/16 20:25 180 - 120

Dibromofluoromethane (Surr) 102 06/08/16 20:25 179 - 120

Method: 8270C - Semivolatile Organic Compounds (GC/MS) - ASTM LeachRL MDL

Acenaphthene ND 0.19 0.042 ug/L 06/09/16 07:34 06/09/16 20:29 1


0.19 0.046 ug/L 06/09/16 07:34 06/09/16 20:29 1Acenaphthylene ND

0.95 0.32 ug/L 06/09/16 07:34 06/09/16 20:29 1Acetophenone ND

0.19 0.084 ug/L 06/09/16 07:34 06/09/16 20:29 1Anthracene ND

0.95 0.32 ug/L 06/09/16 07:34 06/09/16 20:29 1Atrazine ND

0.95 0.37 ug/L 06/09/16 07:34 06/09/16 20:29 1Benzaldehyde ND

0.19 0.028 ug/L 06/09/16 07:34 06/09/16 20:29 1Benzo[a]anthracene ND

0.19 0.038 ug/L 06/09/16 07:34 06/09/16 20:29 1Benzo[b]fluoranthene ND

0.19 0.043 ug/L 06/09/16 07:34 06/09/16 20:29 1Benzo[k]fluoranthene ND

0.19 0.044 ug/L 06/09/16 07:34 06/09/16 20:29 1Benzo[g,h,i]perylene ND

0.19 0.049 ug/L 06/09/16 07:34 06/09/16 20:29 1Benzo[a]pyrene ND

1.9 0.25 ug/L 06/09/16 07:34 06/09/16 20:29 1Butyl benzyl phthalate ND

0.95 0.12 ug/L 06/09/16 07:34 06/09/16 20:29 11,1'-Biphenyl ND

0.95 0.30 ug/L 06/09/16 07:34 06/09/16 20:29 1Bis(2-chloroethoxy)methane ND

0.95 0.095 ug/L 06/09/16 07:34 06/09/16 20:29 1Bis(2-chloroethyl)ether ND

4.8 1.6 ug/L 06/09/16 07:34 06/09/16 20:29 1Bis(2-ethylhexyl) phthalate ND

1.9 0.21 ug/L 06/09/16 07:34 06/09/16 20:29 14-Bromophenyl phenyl ether ND

4.8 0.19 ug/L 06/09/16 07:34 06/09/16 20:29 1Caprolactam ND F1 *

0.95 0.27 ug/L 06/09/16 07:34 06/09/16 20:29 1Carbazole ND

1.9 0.20 ug/L 06/09/16 07:34 06/09/16 20:29 14-Chloroaniline ND

1.9 0.20 ug/L 06/09/16 07:34 06/09/16 20:29 14-Chloro-3-methylphenol ND

0.95 0.095 ug/L 06/09/16 07:34 06/09/16 20:29 12-Chloronaphthalene ND

0.95 0.28 ug/L 06/09/16 07:34 06/09/16 20:29 12-Chlorophenol ND

1.9 0.29 ug/L 06/09/16 07:34 06/09/16 20:29 14-Chlorophenyl phenyl ether ND

0.19 0.048 ug/L 06/09/16 07:34 06/09/16 20:29 1Chrysene ND

0.19 0.086 ug/L 06/09/16 07:34 06/09/16 20:29 12-Methylnaphthalene ND

1.9 0.76 ug/L 06/09/16 07:34 06/09/16 20:29 13 & 4 Methylphenol ND

0.19 0.042 ug/L 06/09/16 07:34 06/09/16 20:29 1Dibenz(a,h)anthracene ND

0.95 0.019 ug/L 06/09/16 07:34 06/09/16 20:29 1Dibenzofuran ND

4.8 0.35 ug/L 06/09/16 07:34 06/09/16 20:29 13,3'-Dichlorobenzidine ND

1.9 0.18 ug/L 06/09/16 07:34 06/09/16 20:29 12,4-Dichlorophenol ND

1.9 0.57 ug/L 06/09/16 07:34 06/09/16 20:29 1Diethyl phthalate ND

1.9 0.24 ug/L 06/09/16 07:34 06/09/16 20:29 12,4-Dimethylphenol ND

1.9 0.28 ug/L 06/09/16 07:34 06/09/16 20:29 1Dimethyl phthalate ND

4.8 2.3 ug/L 06/09/16 07:34 06/09/16 20:29 14,6-Dinitro-2-methylphenol ND

4.8 0.30 ug/L 06/09/16 07:34 06/09/16 20:29 12,4-Dinitrophenol ND

4.8 0.24 ug/L 06/09/16 07:34 06/09/16 20:29 12,4-Dinitrotoluene ND

4.8 1.6 ug/L 06/09/16 07:34 06/09/16 20:29 1Di-n-butyl phthalate ND

1.9 0.22 ug/L 06/09/16 07:34 06/09/16 20:29 1Di-n-octyl phthalate ND

0.19 0.042 ug/L 06/09/16 07:34 06/09/16 20:29 1Fluoranthene ND

0.19 0.039 ug/L 06/09/16 07:34 06/09/16 20:29 1Fluorene ND

0.19 0.081 ug/L 06/09/16 07:34 06/09/16 20:29 1Hexachlorobenzene ND

0.95 0.26 ug/L 06/09/16 07:34 06/09/16 20:29 1Hexachlorobutadiene ND

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Method: 8270C - Semivolatile Organic Compounds (GC/MS) - ASTM Leach (Continued)RL MDL

Hexachlorocyclopentadiene ND 9.5 0.23 ug/L 06/09/16 07:34 06/09/16 20:29 1


0.95 0.18 ug/L 06/09/16 07:34 06/09/16 20:29 1Hexachloroethane ND

0.19 0.041 ug/L 06/09/16 07:34 06/09/16 20:29 1Indeno[1,2,3-cd]pyrene ND

0.95 0.26 ug/L 06/09/16 07:34 06/09/16 20:29 1Isophorone ND

0.95 0.16 ug/L 06/09/16 07:34 06/09/16 20:29 12-Methylphenol ND

0.19 0.060 ug/L 06/09/16 07:34 06/09/16 20:29 1Naphthalene 0.31

1.9 0.20 ug/L 06/09/16 07:34 06/09/16 20:29 12-Nitroaniline ND



0.95 0.038 ug/L 06/09/16 07:34 06/09/16 20:29 1Nitrobenzene ND

1.9 0.27 ug/L 06/09/16 07:34 06/09/16 20:29 12-Nitrophenol ND


0.95 0.30 ug/L 06/09/16 07:34 06/09/16 20:29 1N-Nitrosodiphenylamine ND

0.95 0.23 ug/L 06/09/16 07:34 06/09/16 20:29 1N-Nitrosodi-n-propylamine ND

0.95 0.38 ug/L 06/09/16 07:34 06/09/16 20:29 1bis (2-chloroisopropyl) ether ND

4.8 0.26 ug/L 06/09/16 07:34 06/09/16 20:29 1Pentachlorophenol ND

0.19 0.059 ug/L 06/09/16 07:34 06/09/16 20:29 1Phenanthrene ND

0.95 0.57 ug/L 06/09/16 07:34 06/09/16 20:29 1Phenol ND

0.19 0.040 ug/L 06/09/16 07:34 06/09/16 20:29 1Pyrene ND

4.8 0.29 ug/L 06/09/16 07:34 06/09/16 20:29 12,4,5-Trichlorophenol ND



2-Fluorobiphenyl (Surr) 79 42 - 120 06/09/16 07:34 06/09/16 20:29 1


2-Fluorophenol (Surr) 36 06/09/16 07:34 06/09/16 20:29 110 - 120

2,4,6-Tribromophenol (Surr) 67 06/09/16 07:34 06/09/16 20:29 135 - 125

Nitrobenzene-d5 (Surr) 76 06/09/16 07:34 06/09/16 20:29 136 - 120

Phenol-d5 (Surr) 21 06/09/16 07:34 06/09/16 20:29 110 - 120

Terphenyl-d14 (Surr) 69 06/09/16 07:34 06/09/16 20:29 117 - 120

Method: 8270C - Semivolatile Organic Compounds (GC/MS) - ASTM Leach - RERL MDL

Caprolactam ND * 5.0 0.20 ug/L 06/13/16 11:40 06/14/16 09:49 1







Phenol-d5 (Surr) 22 06/13/16 11:40 06/14/16 09:49 110 - 120

Terphenyl-d14 (Surr) 65 06/13/16 11:40 06/14/16 09:49 117 - 120

Method: 8081B - Organochlorine Pesticides (GC) - ASTM LeachRL MDL

4,4'-DDD ND 0.048 0.017 ug/L 06/09/16 06:31 06/13/16 14:40 1


0.048 0.011 ug/L 06/09/16 06:31 06/13/16 14:40 14,4'-DDE ND

0.048 0.016 ug/L 06/09/16 06:31 06/13/16 14:40 14,4'-DDT ND

0.048 0.012 ug/L 06/09/16 06:31 06/13/16 14:40 1Aldrin ND

0.048 0.013 ug/L 06/09/16 06:31 06/13/16 14:40 1alpha-BHC ND

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Method: 8081B - Organochlorine Pesticides (GC) - ASTM Leach (Continued)RL MDL

beta-BHC ND 0.048 0.017 ug/L 06/09/16 06:31 06/13/16 14:40 1


0.048 0.011 ug/L 06/09/16 06:31 06/13/16 14:40 1alpha-Chlordane ND

0.048 0.028 ug/L 06/09/16 06:31 06/13/16 14:40 1delta-BHC ND

0.048 0.012 ug/L 06/09/16 06:31 06/13/16 14:40 1gamma-BHC (Lindane) ND

0.048 0.012 ug/L 06/09/16 06:31 06/13/16 14:40 1gamma-Chlordane ND

0.048 0.012 ug/L 06/09/16 06:31 06/13/16 14:40 1Dieldrin ND

0.048 0.015 ug/L 06/09/16 06:31 06/13/16 14:40 1Endosulfan I ND

0.048 0.014 ug/L 06/09/16 06:31 06/13/16 14:40 1Endosulfan II ND

0.048 0.014 ug/L 06/09/16 06:31 06/13/16 14:40 1Endosulfan sulfate ND

0.048 0.012 ug/L 06/09/16 06:31 06/13/16 14:40 1Endrin ND

0.048 0.017 ug/L 06/09/16 06:31 06/13/16 14:40 1Endrin aldehyde ND

0.048 0.015 ug/L 06/09/16 06:31 06/13/16 14:40 1Endrin ketone ND

0.048 0.013 ug/L 06/09/16 06:31 06/13/16 14:40 1Heptachlor ND

0.048 0.014 ug/L 06/09/16 06:31 06/13/16 14:40 1Heptachlor epoxide ND

0.095 0.012 ug/L 06/09/16 06:31 06/13/16 14:40 1Methoxychlor ND

1.9 0.19 ug/L 06/09/16 06:31 06/13/16 14:40 1Toxaphene ND

DCB Decachlorobiphenyl 52 30 - 128 06/09/16 06:31 06/13/16 14:40 1


DCB Decachlorobiphenyl 51 06/09/16 06:31 06/13/16 14:40 130 - 128

Tetrachloro-m-xylene 81 06/09/16 06:31 06/13/16 14:40 136 - 124


Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography - ASTM LeachRL MDL

Aroclor-1016 ND 0.095 0.048 ug/L 06/09/16 06:29 06/13/16 09:21 1


0.095 0.086 ug/L 06/09/16 06:29 06/13/16 09:21 1Aroclor-1221 ND

0.095 0.067 ug/L 06/09/16 06:29 06/13/16 09:21 1Aroclor-1232 ND

0.095 0.057 ug/L 06/09/16 06:29 06/13/16 09:21 1Aroclor-1242 ND

0.095 0.048 ug/L 06/09/16 06:29 06/13/16 09:21 1Aroclor-1248 ND

0.095 0.029 ug/L 06/09/16 06:29 06/13/16 09:21 1Aroclor-1254 ND

0.095 0.038 ug/L 06/09/16 06:29 06/13/16 09:21 1Aroclor-1260 ND

Tetrachloro-m-xylene 53 21 - 120 06/09/16 06:29 06/13/16 09:21 1



Method: 6020A - Metals (ICP/MS) - ASTM LeachRL MDL

Silver ND 1.0 0.020 ug/L 06/08/16 13:00 06/09/16 14:08 1


50 9.0 ug/L 06/08/16 13:00 06/09/16 14:08 1Aluminum 11000

5.0 0.49 ug/L 06/08/16 13:00 06/09/16 14:08 1Arsenic 10

5.0 1.1 ug/L 06/08/16 13:00 06/09/16 14:08 1Barium 29

1.0 0.053 ug/L 06/08/16 13:00 06/09/16 14:08 1Beryllium 0.33 J

1.0 0.061 ug/L 06/08/16 13:00 06/09/16 14:08 1Cadmium 0.44 J

1.0 0.021 ug/L 06/08/16 13:00 06/09/16 14:08 1Cobalt 0.45 J B

2.0 0.60 ug/L 06/08/16 13:00 06/09/16 14:08 1Chromium 3.9

2.0 0.75 ug/L 06/08/16 13:00 06/09/16 14:08 1Copper ND

100 16 ug/L 06/08/16 13:00 06/09/16 14:08 1Iron ND

5.0 1.1 ug/L 06/08/16 13:00 06/09/16 14:08 1Manganese ND

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Method: 6020A - Metals (ICP/MS) - ASTM Leach (Continued)RL MDL

Nickel 0.33 J B 2.0 0.23 ug/L 06/08/16 13:00 06/09/16 14:08 1


1.0 0.11 ug/L 06/08/16 13:00 06/09/16 14:08 1Lead 0.17 J

2.0 0.16 ug/L 06/08/16 13:00 06/09/16 14:08 1Antimony 3.4

5.0 0.25 ug/L 06/08/16 13:00 06/09/16 14:08 1Selenium 23 B

1.0 0.074 ug/L 06/08/16 13:00 06/09/16 14:08 1Thallium 0.27 J

5.0 0.23 ug/L 06/08/16 13:00 06/09/16 14:08 1Vanadium 81

20 7.3 ug/L 06/08/16 13:00 06/09/16 14:08 1Zinc ND

1000 240 ug/L 06/08/16 13:00 06/09/16 14:08 1Calcium 78000

1000 30 ug/L 06/08/16 13:00 06/09/16 14:08 1Potassium 4200

1000 48 ug/L 06/08/16 13:00 06/09/16 14:08 1Magnesium 1100

1000 68 ug/L 06/08/16 13:00 06/09/16 14:08 1Sodium 1700 B

Method: 7470A - Mercury (CVAA) - ASTM LeachRL MDL

Mercury 0.093 J B 0.20 0.090 ug/L 06/08/16 13:30 06/09/16 12:18 1


General ChemistryRL MDL

Percent Solids 99.7 0.1 0.1 % 06/02/16 10:25 1


0.1 0.1 % 06/02/16 10:25 1Percent Moisture 0.3

General Chemistry - ASTM LeachRL MDL

Cr (VI) 0.0058 J 0.020 0.0021 mg/L 06/08/16 13:35 1


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Percent Solids: 99.7Date Received: 06/01/16 10:20

Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL

Acetone 6.2 J B 20 5.7 ug/Kg ☼ 06/03/16 10:36 06/03/16 18:41 1


5.0 0.90 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Benzene ND

5.0 0.29 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Dichlorobromomethane ND

5.0 0.24 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Bromoform ND

5.0 0.42 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Bromomethane ND

20 1.1 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼2-Butanone (MEK) 2.8 J B

5.0 0.59 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Carbon disulfide ND

5.0 0.65 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Carbon tetrachloride ND

5.0 0.53 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Chlorobenzene ND

5.0 0.44 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Chloroethane ND

5.0 0.36 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Chloroform ND

5.0 0.79 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Chloromethane ND

5.0 0.34 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,1-Dichloroethane ND


5.0 0.80 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,1-Dichloroethene ND

5.0 0.14 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,2-Dichloropropane ND

5.0 0.71 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼cis-1,3-Dichloropropene ND

5.0 0.29 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼trans-1,3-Dichloropropene ND

5.0 0.32 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Ethylbenzene ND

20 0.68 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼2-Hexanone ND

5.0 0.74 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Methylene Chloride ND

20 1.2 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼4-Methyl-2-pentanone (MIBK) ND

5.0 0.40 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Styrene ND

5.0 0.31 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,1,2,2-Tetrachloroethane ND

5.0 0.80 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Tetrachloroethene ND

5.0 0.27 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Toluene 0.69 J

5.0 0.38 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Trichloroethene ND

5.0 0.30 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Vinyl chloride ND

10 0.54 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Xylenes, Total ND

5.0 0.65 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,1,1-Trichloroethane ND


10 0.48 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Cyclohexane ND

10 2.7 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,2-Dibromo-3-Chloropropane ND

5.0 0.53 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Ethylene Dibromide ND

5.0 0.28 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Dichlorodifluoromethane ND

5.0 0.28 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼cis-1,2-Dichloroethene ND

5.0 0.32 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼trans-1,2-Dichloroethene ND

5.0 0.20 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Isopropylbenzene ND

10 2.0 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Methyl acetate ND

5.0 0.43 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Methyl tert-butyl ether ND

5.0 0.42 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND

5.0 0.38 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,2,4-Trichlorobenzene ND

5.0 0.34 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼1,2-Dichlorobenzene ND



5.0 0.29 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Trichlorofluoromethane ND

5.0 0.37 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Chlorodibromomethane ND

10 0.58 ug/Kg 06/03/16 10:36 06/03/16 18:41 1☼Methylcyclohexane ND

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1,2-Dichloroethane-d4 (Surr) 100 58 - 123 06/03/16 10:36 06/03/16 18:41 1


4-Bromofluorobenzene (Surr) 97 06/03/16 10:36 06/03/16 18:41 152 - 136

Toluene-d8 (Surr) 104 06/03/16 10:36 06/03/16 18:41 167 - 125

Dibromofluoromethane (Surr) 97 06/03/16 10:36 06/03/16 18:41 137 - 132

Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL

bis (2-chloroisopropyl) ether ND 99 9.4 ug/Kg ☼ 06/03/16 08:23 06/07/16 11:12 1


150 25 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2,4,5-Trichlorophenol ND

150 8.8 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2,4,6-Trichlorophenol ND

150 20 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2,4-Dichlorophenol ND

150 20 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2,4-Dimethylphenol ND

330 21 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2,4-Dinitrophenol ND

200 17 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2,4-Dinitrotoluene ND


49 0.44 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2-Chloronaphthalene ND

49 8.1 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2-Chlorophenol ND

6.6 0.49 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2-Methylnaphthalene ND

200 11 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2-Methylphenol ND

200 9.0 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2-Nitroaniline ND

49 8.2 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼2-Nitrophenol ND

99 18 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼3,3'-Dichlorobenzidine ND

200 16 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼3-Nitroaniline ND

150 9.1 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼4,6-Dinitro-2-methylphenol ND

49 13 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼4-Bromophenyl phenyl ether ND

150 21 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼4-Chloro-3-methylphenol ND

150 17 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼4-Chloroaniline ND

49 13 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼4-Chlorophenyl phenyl ether ND


330 17 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼4-Nitrophenol ND

6.6 0.75 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Acenaphthene ND

6.6 0.35 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Acenaphthylene ND

99 9.1 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Acetophenone ND

6.6 0.77 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Anthracene ND

200 9.0 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Atrazine ND

6.6 0.62 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Benzo[a]anthracene ND

6.6 0.63 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Benzo[a]pyrene ND

6.6 0.58 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Benzo[b]fluoranthene ND

6.6 0.35 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Benzo[g,h,i]perylene ND

6.6 0.67 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Benzo[k]fluoranthene ND

99 22 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Bis(2-chloroethoxy)methane ND

99 2.0 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Bis(2-chloroethyl)ether ND

69 19 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Bis(2-ethylhexyl) phthalate ND

69 9.9 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Butyl benzyl phthalate ND

6.6 1.1 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Chrysene ND

6.6 0.65 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Dibenz(a,h)anthracene ND

49 0.65 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Dibenzofuran ND

69 16 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Diethyl phthalate ND

69 17 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Dimethyl phthalate ND

69 15 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Di-n-butyl phthalate ND

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Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL

Di-n-octyl phthalate ND 69 7.8 ug/Kg ☼ 06/03/16 08:23 06/07/16 11:12 1


6.6 0.54 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Fluoranthene ND

6.6 0.52 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Fluorene ND

6.6 2.1 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Hexachlorobenzene ND

49 5.5 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Hexachlorobutadiene ND

330 8.0 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Hexachlorocyclopentadiene ND

49 8.9 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Hexachloroethane ND

6.6 0.35 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Indeno[1,2,3-cd]pyrene ND

49 13 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Isophorone ND

6.6 0.81 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Naphthalene 4.0 J

99 2.2 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Nitrobenzene ND

49 6.2 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼N-Nitrosodi-n-propylamine ND

49 21 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼N-Nitrosodiphenylamine ND *

150 9.0 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Pentachlorophenol ND

49 7.2 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Phenol ND

6.6 0.72 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Phenanthrene ND

6.6 0.43 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼Pyrene ND

400 20 ug/Kg 06/03/16 08:23 06/07/16 11:12 1☼3 & 4 Methylphenol ND






Phenol-d5 (Surr) 74 06/03/16 08:23 06/07/16 11:12 132 - 120

Terphenyl-d14 (Surr) 111 06/03/16 08:23 06/07/16 11:12 147 - 120

Method: 8081B - Organochlorine Pesticides (GC)RL MDL

4,4'-DDD ND 1.7 0.20 ug/Kg ☼ 06/03/16 07:28 06/10/16 16:02 1


1.7 0.27 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼4,4'-DDE ND

1.7 0.31 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼4,4'-DDT ND

1.7 0.20 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Aldrin ND

1.7 0.60 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼alpha-BHC ND

1.7 0.25 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼alpha-Chlordane ND

1.7 0.36 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼beta-BHC ND

1.7 0.22 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼delta-BHC ND

1.7 0.16 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Dieldrin ND

1.7 0.25 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Endosulfan I ND

1.7 0.38 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Endosulfan II ND

1.7 0.34 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Endosulfan sulfate ND

1.7 0.21 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Endrin ND

1.7 0.32 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Endrin aldehyde ND

1.7 0.42 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Endrin ketone ND

1.7 0.46 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼gamma-BHC (Lindane) ND

1.7 0.86 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼gamma-Chlordane ND

1.7 0.70 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Heptachlor ND

1.7 0.40 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Heptachlor epoxide ND

67 9.9 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Toxaphene ND

3.3 0.54 ug/Kg 06/03/16 07:28 06/10/16 16:02 1☼Methoxychlor ND

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Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyRL MDL

Aroclor-1016 ND 33 12 ug/Kg ☼ 06/03/16 07:23 06/06/16 14:28 1


33 16 ug/Kg 06/03/16 07:23 06/06/16 14:28 1☼Aroclor-1221 ND

33 20 ug/Kg 06/03/16 07:23 06/06/16 14:28 1☼Aroclor-1232 ND

33 11 ug/Kg 06/03/16 07:23 06/06/16 14:28 1☼Aroclor-1242 ND

33 8.0 ug/Kg 06/03/16 07:23 06/06/16 14:28 1☼Aroclor-1248 ND

33 14 ug/Kg 06/03/16 07:23 06/06/16 14:28 1☼Aroclor-1254 ND

33 9.0 ug/Kg 06/03/16 07:23 06/06/16 14:28 1☼Aroclor-1260 ND




Method: 6020A - Metals (ICP/MS)RL MDL

Silver 2.8 B 0.19 0.0014 mg/Kg ☼ 06/02/16 11:09 06/03/16 21:54 2


9.6 0.60 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Aluminum 7800 B

0.96 0.025 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Arsenic 5.9 B

0.96 0.21 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Barium 120

0.19 0.011 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Beryllium 0.28 B

0.19 0.0036 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Cadmium 1.2 B

0.19 0.0016 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Cobalt 35 B

0.39 0.058 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Chromium 48 B

0.39 0.094 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Copper 100 B

19 3.1 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Iron 19000 B

0.96 0.12 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Manganese 1000 B

0.39 0.038 mg/Kg 06/02/16 11:09 06/06/16 14:26 2☼Nickel 750 B

0.19 0.043 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Lead 24 B

0.39 0.014 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Antimony 0.39

0.96 0.039 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Selenium 1.0 B

0.39 0.018 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Thallium 0.11 J

0.96 0.036 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Vanadium 14

3.9 0.48 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Zinc 94 B

190 21 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Calcium 12000 B

190 4.7 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Potassium 2000 B

190 3.9 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Magnesium 82000 B

190 8.4 mg/Kg 06/02/16 11:09 06/03/16 21:54 2☼Sodium 410 B

Method: 7471A - Mercury (CVAA)RL MDL

Mercury ND 0.11 0.015 mg/Kg ☼ 06/02/16 15:00 06/03/16 07:42 1



Cr (VI) ND 0.79 0.15 mg/Kg ☼ 06/09/16 09:04 06/09/16 13:44 1


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Surrogate SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District


Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (58-123) (52-136) (67-125) (37-132)

12DCE BFB TOL DBFM

100 97 104 97240-65485-1

Percent Surrogate Recovery (Acceptance Limits)

SOUTHERLY WWTC-ASH (SWWTC)

90 94 103 96LCS 240-233030/5 Lab Control Sample

91 93 101 96MB 240-233030/6 Method Blank

Surrogate Legend

12DCE = 1,2-Dichloroethane-d4 (Surr)

BFB = 4-Bromofluorobenzene (Surr)

TOL = Toluene-d8 (Surr)

DBFM = Dibromofluoromethane (Surr)



12DCE BFB TOL DBFM

96 88 93 103LCS 240-233711/6


Lab Control Sample

Surrogate Legend





Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: SPLPMatrix: Solid


12DCE BFB TOL DBFM

100 83 92 102240-65485-1



101 84 89 102LB 240-233606/1-A MB Method Blank

Surrogate Legend





Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (39-120) (33-120) (10-120) (32-120) (32-120) (47-120)

FBP 2FP TBP NBZ PHL TPH

91 74 41 80 74 111240-65485-1



94 82 75 8384 113LCS 240-233013/18-A Lab Control Sample

92 77 59 7991 103MB 240-233013/17-A Method Blank

Surrogate Legend

FBP = 2-Fluorobiphenyl (Surr)

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2FP = 2-Fluorophenol (Surr)

TBP = 2,4,6-Tribromophenol (Surr)

NBZ = Nitrobenzene-d5 (Surr)

PHL = Phenol-d5 (Surr)

TPH = Terphenyl-d14 (Surr)




87 41 87 94 24 78LCS 240-233761/5-A


Lab Control Sample


74 39 68 2473 76MB 240-233761/4-A Method Blank

80 37 96 2284 82MB 240-234253/3-A Method Blank

Surrogate Legend







Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep Type: ASTM LeachMatrix: Solid



79 36 67 76 21 69240-65485-1



77 35 88 2280 65240-65485-1 - RE SOUTHERLY WWTC-ASH

(SWWTC)81 27 82 1584 60240-65485-1 MS SOUTHERLY WWTC-ASH

(SWWTC)

Surrogate Legend







Method: 8081B - Organochlorine Pesticides (GC)Prep Type: Total/NAMatrix: Solid


DCB1 DCB2 TCX1 TCX2

66 56 90 83LCS 240-233753/5-A


Lab Control Sample

48 48 90 85MB 240-233753/4-A Method Blank

Surrogate Legend

DCB = DCB Decachlorobiphenyl

TCX = Tetrachloro-m-xylene

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DCB1 DCB2 TCX1 TCX2

59 83 68 56240-65485-1



79 74 70 60LCS 240-233006/6-A Lab Control Sample

81 85 77 64MB 240-233006/5-A Method Blank

Surrogate Legend



Method: 8081B - Organochlorine Pesticides (GC)Prep Type: ASTM LeachMatrix: Solid


DCB1 DCB2 TCX1 TCX2

52 51 81 37240-65485-1



30 29 X 80 80240-65485-1 MS SOUTHERLY WWTC-ASH

(SWWTC)

Surrogate Legend



Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (14-128) (10-132)

TCX2 DCB2

60 63240-65485-1



66 80LCS 240-233005/13-A Lab Control Sample

64 79MB 240-233005/12-A Method Blank

Surrogate Legend





TCX2 DCB2

60 36LCS 240-233752/5-A


Lab Control Sample

59 33MB 240-233752/4-A Method Blank

Surrogate Legend



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Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep Type: ASTM LeachMatrix: Solid


TCX2 DCB2

53 15240-65485-1



59 11240-65485-1 MS SOUTHERLY WWTC-ASH

(SWWTC)

Surrogate Legend



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QC Sample ResultsTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District


Method: 8260B - Volatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 240-233030/6Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233030

RL MDL

Acetone 7.04 J 20 5.7 ug/Kg 06/03/16 11:24 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier

ND 0.905.0 ug/Kg 06/03/16 11:24 1Benzene

ND 0.295.0 ug/Kg 06/03/16 11:24 1Dichlorobromomethane

ND 0.245.0 ug/Kg 06/03/16 11:24 1Bromoform

ND 0.425.0 ug/Kg 06/03/16 11:24 1Bromomethane

1.22 J 1.120 ug/Kg 06/03/16 11:24 12-Butanone (MEK)

ND 0.595.0 ug/Kg 06/03/16 11:24 1Carbon disulfide

ND 0.655.0 ug/Kg 06/03/16 11:24 1Carbon tetrachloride

ND 0.535.0 ug/Kg 06/03/16 11:24 1Chlorobenzene

ND 0.445.0 ug/Kg 06/03/16 11:24 1Chloroethane

ND 0.365.0 ug/Kg 06/03/16 11:24 1Chloroform

ND 0.795.0 ug/Kg 06/03/16 11:24 1Chloromethane

ND 0.345.0 ug/Kg 06/03/16 11:24 11,1-Dichloroethane


ND 0.805.0 ug/Kg 06/03/16 11:24 11,1-Dichloroethene

ND 0.145.0 ug/Kg 06/03/16 11:24 11,2-Dichloropropane

ND 0.715.0 ug/Kg 06/03/16 11:24 1cis-1,3-Dichloropropene

ND 0.295.0 ug/Kg 06/03/16 11:24 1trans-1,3-Dichloropropene

ND 0.325.0 ug/Kg 06/03/16 11:24 1Ethylbenzene

ND 0.6820 ug/Kg 06/03/16 11:24 12-Hexanone

ND 0.745.0 ug/Kg 06/03/16 11:24 1Methylene Chloride

ND 1.220 ug/Kg 06/03/16 11:24 14-Methyl-2-pentanone (MIBK)

ND 0.405.0 ug/Kg 06/03/16 11:24 1Styrene

ND 0.315.0 ug/Kg 06/03/16 11:24 11,1,2,2-Tetrachloroethane

ND 0.805.0 ug/Kg 06/03/16 11:24 1Tetrachloroethene

ND 0.275.0 ug/Kg 06/03/16 11:24 1Toluene

ND 0.385.0 ug/Kg 06/03/16 11:24 1Trichloroethene

ND 0.305.0 ug/Kg 06/03/16 11:24 1Vinyl chloride

ND 0.5410 ug/Kg 06/03/16 11:24 1Xylenes, Total

ND 0.655.0 ug/Kg 06/03/16 11:24 11,1,1-Trichloroethane


ND 0.4810 ug/Kg 06/03/16 11:24 1Cyclohexane

ND 2.710 ug/Kg 06/03/16 11:24 11,2-Dibromo-3-Chloropropane

ND 0.535.0 ug/Kg 06/03/16 11:24 1Ethylene Dibromide

ND 0.285.0 ug/Kg 06/03/16 11:24 1Dichlorodifluoromethane

ND 0.285.0 ug/Kg 06/03/16 11:24 1cis-1,2-Dichloroethene

ND 0.325.0 ug/Kg 06/03/16 11:24 1trans-1,2-Dichloroethene

ND 0.205.0 ug/Kg 06/03/16 11:24 1Isopropylbenzene

ND 2.010 ug/Kg 06/03/16 11:24 1Methyl acetate

ND 0.435.0 ug/Kg 06/03/16 11:24 1Methyl tert-butyl ether

ND 0.425.0 ug/Kg 06/03/16 11:24 11,1,2-Trichloro-1,2,2-trifluoroethane

ND 0.385.0 ug/Kg 06/03/16 11:24 11,2,4-Trichlorobenzene

ND 0.345.0 ug/Kg 06/03/16 11:24 11,2-Dichlorobenzene



ND 0.295.0 ug/Kg 06/03/16 11:24 1Trichlorofluoromethane

ND 0.375.0 ug/Kg 06/03/16 11:24 1Chlorodibromomethane

ND 0.5810 ug/Kg 06/03/16 11:24 1Methylcyclohexane

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MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery

93 06/03/16 11:24 14-Bromofluorobenzene (Surr) 52 - 136

101 06/03/16 11:24 1Toluene-d8 (Surr) 67 - 125

96 06/03/16 11:24 1Dibromofluoromethane (Surr) 37 - 132

Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233030/5Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233030

Acetone 100 107 ug/Kg 107 41 - 137

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

Benzene 50.0 51.6 ug/Kg 103 79 - 120

Dichlorobromomethane 50.0 54.1 ug/Kg 108 80 - 122

Bromoform 50.0 53.3 ug/Kg 107 62 - 133

Bromomethane 20.0 14.1 ug/Kg 71 42 - 136

2-Butanone (MEK) 100 110 ug/Kg 110 52 - 131

Carbon disulfide 50.0 60.8 ug/Kg 122 62 - 146

Carbon tetrachloride 50.0 51.9 ug/Kg 104 71 - 129

Chlorobenzene 50.0 51.0 ug/Kg 102 78 - 120

Chloroethane 20.0 16.9 ug/Kg 85 58 - 120

Chloroform 50.0 51.3 ug/Kg 103 77 - 120

Chloromethane 20.0 14.8 ug/Kg 74 50 - 120

1,1-Dichloroethane 50.0 50.1 ug/Kg 100 76 - 120


1,1-Dichloroethene 50.0 53.9 ug/Kg 108 75 - 135

1,2-Dichloropropane 50.0 52.1 ug/Kg 104 80 - 120

cis-1,3-Dichloropropene 50.0 55.8 ug/Kg 112 74 - 128

trans-1,3-Dichloropropene 50.0 50.6 ug/Kg 101 73 - 131

Ethylbenzene 50.0 52.7 ug/Kg 105 79 - 120

2-Hexanone 100 118 ug/Kg 118 64 - 136

Methylene Chloride 50.0 49.5 ug/Kg 99 75 - 120

4-Methyl-2-pentanone (MIBK) 100 123 ug/Kg 123 67 - 135

Styrene 50.0 54.1 ug/Kg 108 80 - 120

1,1,2,2-Tetrachloroethane 50.0 56.1 ug/Kg 112 77 - 123

Tetrachloroethene 50.0 53.0 ug/Kg 106 79 - 120

Toluene 50.0 50.9 ug/Kg 102 75 - 120

Trichloroethene 50.0 54.9 ug/Kg 110 79 - 120

Vinyl chloride 20.0 14.5 ug/Kg 73 57 - 120

Xylenes, Total 100 106 ug/Kg 106 80 - 120

1,1,1-Trichloroethane 50.0 52.3 ug/Kg 105 77 - 126


Cyclohexane 50.0 52.1 ug/Kg 104 66 - 120

1,2-Dibromo-3-Chloropropane 50.0 57.9 ug/Kg 116 61 - 132

Ethylene Dibromide 50.0 57.6 ug/Kg 115 80 - 120

Dichlorodifluoromethane 20.0 9.78 ug/Kg 49 26 - 120

cis-1,2-Dichloroethene 50.0 52.2 ug/Kg 104 76 - 120

trans-1,2-Dichloroethene 50.0 55.2 ug/Kg 110 78 - 120

Isopropylbenzene 50.0 56.0 ug/Kg 112 76 - 122

Methyl acetate 250 300 ug/Kg 120 57 - 130

Methyl tert-butyl ether 50.0 50.5 ug/Kg 101 49 - 165

1,1,2-Trichloro-1,2,2-trifluoroetha

ne

50.0 52.7 ug/Kg 105 80 - 138

1,2,4-Trichlorobenzene 50.0 49.4 ug/Kg 99 64 - 124

1,2-Dichlorobenzene 50.0 50.3 ug/Kg 101 76 - 120

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Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued)



Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Trichlorofluoromethane 20.0 17.2 ug/Kg 86 57 - 146

Methylcyclohexane 50.0 51.2 ug/Kg 102 70 - 126

m-Xylene & p-Xylene 50.0 52.9 ug/Kg 106 80 - 120

o-Xylene 50.0 52.7 ug/Kg 105 80 - 120

1,2-Dichloroethane-d4 (Surr) 58 - 123

Surrogate

90

LCS LCS

Qualifier Limits%Recovery

944-Bromofluorobenzene (Surr) 52 - 136

103Toluene-d8 (Surr) 67 - 125

96Dibromofluoromethane (Surr) 37 - 132


Acetone 40.0 35.6 ug/L 89 34 - 148

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Benzene 20.0 22.6 ug/L 113 80 - 120

Dichlorobromomethane 20.0 21.9 ug/L 109 80 - 120

Bromoform 20.0 24.3 ug/L 122 56 - 122

Bromomethane 20.0 23.5 ug/L 118 38 - 132

2-Butanone (MEK) 40.0 43.2 ug/L 108 56 - 138

Carbon disulfide 20.0 26.5 ug/L 132 65 - 144

Carbon tetrachloride 20.0 23.6 ug/L 118 77 - 131

Chlorobenzene 20.0 21.2 ug/L 106 80 - 120

Chloroethane 20.0 24.0 ug/L 120 36 - 126

Chloroform 20.0 23.0 ug/L 115 80 - 120

Chloromethane 20.0 23.8 ug/L 119 48 - 133

1,1-Dichloroethane 20.0 22.0 ug/L 110 79 - 125


1,1-Dichloroethene 20.0 24.8 ug/L 124 76 - 124

1,2-Dichloropropane 20.0 22.3 ug/L 111 78 - 124

cis-1,3-Dichloropropene 20.0 23.4 ug/L 117 74 - 126

trans-1,3-Dichloropropene 20.0 18.4 ug/L 92 75 - 131

Ethylbenzene 20.0 19.9 ug/L 99 80 - 120

2-Hexanone 40.0 42.8 ug/L 107 55 - 141

Methylene Chloride 20.0 22.2 ug/L 111 77 - 129

4-Methyl-2-pentanone (MIBK) 40.0 44.2 ug/L 111 64 - 135

Styrene 20.0 20.6 ug/L 103 76 - 122

1,1,2,2-Tetrachloroethane 20.0 19.7 ug/L 99 71 - 123

Tetrachloroethene 20.0 20.9 ug/L 104 78 - 121

Toluene 20.0 22.4 ug/L 112 80 - 120

Trichloroethene 20.0 24.1 ug/L 121 80 - 121

Vinyl chloride 20.0 23.6 ug/L 118 52 - 121

Xylenes, Total 40.0 42.0 ug/L 105 80 - 120

1,1,1-Trichloroethane 20.0 25.6 * ug/L 128 77 - 123

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1,1,2-Trichloroethane 20.0 21.9 ug/L 110 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Cyclohexane 20.0 21.0 ug/L 105 60 - 140

1,2-Dibromo-3-Chloropropane 20.0 22.6 ug/L 113 50 - 132

Ethylene Dibromide 20.0 22.2 ug/L 111 80 - 120

Dichlorodifluoromethane 20.0 23.1 ug/L 115 23 - 136

cis-1,2-Dichloroethene 20.0 22.1 ug/L 111 79 - 120

trans-1,2-Dichloroethene 20.0 22.8 ug/L 114 80 - 124

Isopropylbenzene 20.0 20.3 ug/L 102 77 - 120

Methyl acetate 100 113 ug/L 113 67 - 131

Methyl tert-butyl ether 20.0 23.0 ug/L 115 69 - 121


ne

20.0 23.4 ug/L 117 67 - 138

1,2,4-Trichlorobenzene 20.0 20.1 ug/L 100 61 - 120

1,2-Dichlorobenzene 20.0 19.6 ug/L 98 79 - 120



Trichlorofluoromethane 20.0 21.8 ug/L 109 61 - 133

Methylcyclohexane 20.0 19.9 ug/L 100 61 - 134

m-Xylene & p-Xylene 20.0 21.4 ug/L 107 80 - 120

o-Xylene 20.0 20.6 ug/L 103 80 - 120


Surrogate

96

LCS LCS





Client Sample ID: Method BlankLab Sample ID: LB 240-233606/1-A MBMatrix: Solid Prep Type: SPLPAnalysis Batch: 233711

RL MDL

Acetone 1.76 J 10 0.94 ug/L 06/08/16 20:01 1

MB MB


ND 0.351.0 ug/L 06/08/16 20:01 1Benzene

ND 0.291.0 ug/L 06/08/16 20:01 1Dichlorobromomethane

ND 0.561.0 ug/L 06/08/16 20:01 1Bromoform

ND 0.441.0 ug/L 06/08/16 20:01 1Bromomethane

ND 0.5310 ug/L 06/08/16 20:01 12-Butanone (MEK)

ND 0.381.0 ug/L 06/08/16 20:01 1Carbon disulfide

ND 0.431.0 ug/L 06/08/16 20:01 1Carbon tetrachloride

ND 0.251.0 ug/L 06/08/16 20:01 1Chlorobenzene

ND 0.321.0 ug/L 06/08/16 20:01 1Chloroethane

1.24 0.251.0 ug/L 06/08/16 20:01 1Chloroform

ND 0.441.0 ug/L 06/08/16 20:01 1Chloromethane

ND 0.301.0 ug/L 06/08/16 20:01 11,1-Dichloroethane


ND 0.451.0 ug/L 06/08/16 20:01 11,1-Dichloroethene

ND 0.251.0 ug/L 06/08/16 20:01 11,2-Dichloropropane

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RL MDL

cis-1,3-Dichloropropene ND 1.0 0.46 ug/L 06/08/16 20:01 1

MB MB


ND 0.561.0 ug/L 06/08/16 20:01 1trans-1,3-Dichloropropene

ND 0.251.0 ug/L 06/08/16 20:01 1Ethylbenzene

ND 0.4810 ug/L 06/08/16 20:01 12-Hexanone

2.74 0.331.0 ug/L 06/08/16 20:01 1Methylene Chloride

ND 0.9910 ug/L 06/08/16 20:01 14-Methyl-2-pentanone (MIBK)

ND 0.451.0 ug/L 06/08/16 20:01 1Styrene

ND 0.221.0 ug/L 06/08/16 20:01 11,1,2,2-Tetrachloroethane

ND 0.311.0 ug/L 06/08/16 20:01 1Tetrachloroethene

ND 0.231.0 ug/L 06/08/16 20:01 1Toluene

ND 0.221.0 ug/L 06/08/16 20:01 1Trichloroethene

ND 0.291.0 ug/L 06/08/16 20:01 1Vinyl chloride

ND 0.522.0 ug/L 06/08/16 20:01 1Xylenes, Total

ND 0.441.0 ug/L 06/08/16 20:01 11,1,1-Trichloroethane


ND 0.451.0 ug/L 06/08/16 20:01 1Cyclohexane

ND 0.822.0 ug/L 06/08/16 20:01 11,2-Dibromo-3-Chloropropane

ND 0.321.0 ug/L 06/08/16 20:01 1Ethylene Dibromide

ND 0.321.0 ug/L 06/08/16 20:01 1Dichlorodifluoromethane

ND 0.261.0 ug/L 06/08/16 20:01 1cis-1,2-Dichloroethene

ND 0.301.0 ug/L 06/08/16 20:01 1trans-1,2-Dichloroethene

ND 0.351.0 ug/L 06/08/16 20:01 1Isopropylbenzene

ND 2.310 ug/L 06/08/16 20:01 1Methyl acetate

ND 0.201.0 ug/L 06/08/16 20:01 1Methyl tert-butyl ether

ND 0.451.0 ug/L 06/08/16 20:01 11,1,2-Trichloro-1,2,2-trifluoroethane

ND 0.321.0 ug/L 06/08/16 20:01 11,2,4-Trichlorobenzene

ND 0.251.0 ug/L 06/08/16 20:01 11,2-Dichlorobenzene



ND 0.491.0 ug/L 06/08/16 20:01 1Trichlorofluoromethane

ND 0.431.0 ug/L 06/08/16 20:01 1Chlorodibromomethane

ND 0.431.0 ug/L 06/08/16 20:01 1Methylcyclohexane


MB MB



89 06/08/16 20:01 1Toluene-d8 (Surr) 80 - 120


Method: 8270C - Semivolatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 240-233013/17-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233383 Prep Batch: 233013

RL MDL

2-Chloronaphthalene ND 50 0.45 ug/Kg 06/03/16 08:23 06/07/16 10:25 1

MB MB


ND 8.250 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Chlorophenol

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Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)


RL MDL

4-Bromophenyl phenyl ether ND 50 13 ug/Kg 06/03/16 08:23 06/07/16 10:25 1

MB MB


ND 21150 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Chloro-3-methylphenol

ND 0.506.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Methylnaphthalene

ND 17150 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Chloroaniline

ND 1350 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Chlorophenyl phenyl ether

ND 18100 ug/Kg 06/03/16 08:23 06/07/16 10:25 13,3'-Dichlorobenzidine

ND 0.766.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Acenaphthene

ND 20150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4-Dichlorophenol

ND 0.356.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Acenaphthylene

ND 9.2100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Acetophenone

ND 20150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4-Dimethylphenol

ND 0.786.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Anthracene

ND 9.1200 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Atrazine

ND 9.2150 ug/Kg 06/03/16 08:23 06/07/16 10:25 14,6-Dinitro-2-methylphenol

ND 0.636.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[a]anthracene

ND 21330 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4-Dinitrophenol

ND 0.646.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[a]pyrene

ND 17200 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4-Dinitrotoluene

ND 0.596.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[b]fluoranthene

ND 0.356.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[g,h,i]perylene

ND 0.686.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[k]fluoranthene

ND 22100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Bis(2-chloroethoxy)methane

ND 2.0100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Bis(2-chloroethyl)ether

ND 1970 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Bis(2-ethylhexyl) phthalate

ND 1070 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Butyl benzyl phthalate

ND 1.16.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Chrysene

ND 0.666.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Dibenz(a,h)anthracene

ND 0.6650 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Dibenzofuran

ND 1670 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Diethyl phthalate

ND 11200 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Methylphenol

ND 1770 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Dimethyl phthalate

27.9 J 1570 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Di-n-butyl phthalate

ND 9.1200 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Nitroaniline

ND 7.970 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Di-n-octyl phthalate

ND 16200 ug/Kg 06/03/16 08:23 06/07/16 10:25 13-Nitroaniline

ND 0.556.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Fluoranthene


ND 0.536.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Fluorene

ND 2.16.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachlorobenzene

ND 8.350 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Nitrophenol

ND 5.650 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachlorobutadiene

ND 17330 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Nitrophenol

ND 8.1330 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachlorocyclopentadiene

ND 9.050 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachloroethane

ND 0.356.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Indeno[1,2,3-cd]pyrene

ND 9.5100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1bis (2-chloroisopropyl) ether

ND 1350 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Isophorone

ND 0.826.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Naphthalene

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RL MDL

Nitrobenzene ND 100 2.2 ug/Kg 06/03/16 08:23 06/07/16 10:25 1

MB MB


ND 6.350 ug/Kg 06/03/16 08:23 06/07/16 10:25 1N-Nitrosodi-n-propylamine

ND 2150 ug/Kg 06/03/16 08:23 06/07/16 10:25 1N-Nitrosodiphenylamine

ND 25150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4,5-Trichlorophenol

ND 9.1150 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Pentachlorophenol

ND 8.9150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4,6-Trichlorophenol

ND 7.350 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Phenol

ND 0.736.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Phenanthrene

ND 0.446.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Pyrene

ND 20400 ug/Kg 06/03/16 08:23 06/07/16 10:25 13 & 4 Methylphenol


2-Fluorobiphenyl (Surr) 92 39 - 120 06/07/16 10:25 1

MB MB

Surrogate

06/03/16 08:23

Dil FacPrepared AnalyzedQualifier Limits%Recovery

77 06/03/16 08:23 06/07/16 10:25 12-Fluorophenol (Surr) 33 - 120

59 06/03/16 08:23 06/07/16 10:25 12,4,6-Tribromophenol (Surr) 10 - 120

91 06/03/16 08:23 06/07/16 10:25 1Nitrobenzene-d5 (Surr) 32 - 120

79 06/03/16 08:23 06/07/16 10:25 1Phenol-d5 (Surr) 32 - 120

103 06/03/16 08:23 06/07/16 10:25 1Terphenyl-d14 (Surr) 47 - 120

Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233013/18-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233383 Prep Batch: 233013

2-Chloronaphthalene 667 612 ug/Kg 92 54 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

2-Chlorophenol 667 624 ug/Kg 94 50 - 120

4-Bromophenyl phenyl ether 667 770 ug/Kg 116 48 - 120

4-Chloro-3-methylphenol 667 523 ug/Kg 78 52 - 120

2-Methylnaphthalene 667 644 ug/Kg 97 53 - 120

4-Chloroaniline 667 387 ug/Kg 58 41 - 120

4-Chlorophenyl phenyl ether 667 712 ug/Kg 107 56 - 120

3,3'-Dichlorobenzidine 1330 1000 ug/Kg 75 39 - 120

Acenaphthene 667 602 ug/Kg 90 55 - 120

2,4-Dichlorophenol 667 612 ug/Kg 92 51 - 120

Acenaphthylene 667 632 ug/Kg 95 54 - 120

Acetophenone 667 589 ug/Kg 88 49 - 120

2,4-Dimethylphenol 667 448 ug/Kg 67 34 - 120

Anthracene 667 620 ug/Kg 93 59 - 120

Atrazine 1330 1460 ug/Kg 110 56 - 120

4,6-Dinitro-2-methylphenol 1330 849 ug/Kg 64 23 - 120

Benzo[a]anthracene 667 648 ug/Kg 97 60 - 120

2,4-Dinitrophenol 1330 503 ug/Kg 38 10 - 120

Benzo[a]pyrene 667 745 ug/Kg 112 61 - 120

2,4-Dinitrotoluene 667 716 ug/Kg 107 57 - 120

Benzo[b]fluoranthene 667 736 ug/Kg 110 60 - 120

Benzo[g,h,i]perylene 667 686 ug/Kg 103 60 - 120

Benzo[k]fluoranthene 667 759 ug/Kg 114 61 - 120

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Bis(2-chloroethoxy)methane 667 569 ug/Kg 85 53 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Bis(2-chloroethyl)ether 667 548 ug/Kg 82 45 - 120

Bis(2-ethylhexyl) phthalate 667 665 ug/Kg 100 57 - 120

Butyl benzyl phthalate 667 653 ug/Kg 98 58 - 120

Chrysene 667 637 ug/Kg 96 62 - 120

Dibenz(a,h)anthracene 667 736 ug/Kg 110 59 - 120

Dibenzofuran 667 658 ug/Kg 99 57 - 120

Diethyl phthalate 667 665 ug/Kg 100 58 - 120

2-Methylphenol 667 617 ug/Kg 93 48 - 120

Dimethyl phthalate 667 708 ug/Kg 106 59 - 120

Di-n-butyl phthalate 667 669 ug/Kg 100 54 - 120

2-Nitroaniline 667 641 ug/Kg 96 50 - 120

Di-n-octyl phthalate 667 703 ug/Kg 105 54 - 120


Fluoranthene 667 624 ug/Kg 94 57 - 120


Fluorene 667 674 ug/Kg 101 56 - 120

Hexachlorobenzene 667 770 ug/Kg 115 43 - 120

2-Nitrophenol 667 609 ug/Kg 91 49 - 120

Hexachlorobutadiene 667 597 ug/Kg 90 48 - 120


Hexachlorocyclopentadiene 667 352 ug/Kg 53 23 - 120

Hexachloroethane 667 576 ug/Kg 86 46 - 120

Indeno[1,2,3-cd]pyrene 667 710 ug/Kg 106 62 - 120

bis (2-chloroisopropyl) ether 667 556 ug/Kg 83 34 - 120

Isophorone 667 552 ug/Kg 83 54 - 120

Naphthalene 667 601 ug/Kg 90 53 - 120

Nitrobenzene 667 554 ug/Kg 83 50 - 120

N-Nitrosodi-n-propylamine 667 595 ug/Kg 89 49 - 120

N-Nitrosodiphenylamine 667 812 * ug/Kg 122 52 - 120

2,4,5-Trichlorophenol 667 566 ug/Kg 85 31 - 120

Pentachlorophenol 1330 676 ug/Kg 51 23 - 120


Phenol 667 567 ug/Kg 85 49 - 120

Phenanthrene 667 619 ug/Kg 93 58 - 120

Pyrene 667 639 ug/Kg 96 57 - 120

3 & 4 Methylphenol 667 594 ug/Kg 89 49 - 120


2-Fluorobiphenyl (Surr) 39 - 120

Surrogate

94

LCS LCS


822-Fluorophenol (Surr) 33 - 120

752,4,6-Tribromophenol (Surr) 10 - 120

84Nitrobenzene-d5 (Surr) 32 - 120

83Phenol-d5 (Surr) 32 - 120

113Terphenyl-d14 (Surr) 47 - 120

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RL MDL

Benzaldehyde ND 1.0 0.39 ug/L 06/09/16 07:34 06/10/16 09:52 1

MB MB


ND 0.131.0 ug/L 06/09/16 07:34 06/10/16 09:52 11,1'-Biphenyl

0.977 J 0.205.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Caprolactam

ND 0.281.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Carbazole

ND 0.101.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Chloronaphthalene

ND 0.291.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Chlorophenol

ND 0.222.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Bromophenyl phenyl ether

ND 0.212.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Chloro-3-methylphenol

ND 0.0900.20 ug/L 06/09/16 07:34 06/10/16 09:52 12-Methylnaphthalene

ND 0.212.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Chloroaniline

ND 0.302.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Chlorophenyl phenyl ether

ND 0.375.0 ug/L 06/09/16 07:34 06/10/16 09:52 13,3'-Dichlorobenzidine

ND 0.0440.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Acenaphthene

ND 0.192.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4-Dichlorophenol

ND 0.0480.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Acenaphthylene

ND 0.341.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Acetophenone

ND 0.252.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4-Dimethylphenol

ND 0.0880.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Anthracene

ND 0.341.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Atrazine

ND 2.45.0 ug/L 06/09/16 07:34 06/10/16 09:52 14,6-Dinitro-2-methylphenol

ND 0.0300.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[a]anthracene

ND 0.325.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4-Dinitrophenol

ND 0.0510.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[a]pyrene

ND 0.255.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4-Dinitrotoluene

ND 0.0390.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[b]fluoranthene

ND 0.0460.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[g,h,i]perylene

ND 0.0450.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[k]fluoranthene

ND 0.321.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Bis(2-chloroethoxy)methane

ND 0.101.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Bis(2-chloroethyl)ether

ND 1.75.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Bis(2-ethylhexyl) phthalate

ND 0.262.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Butyl benzyl phthalate

ND 0.0500.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Chrysene

ND 0.0450.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Dibenz(a,h)anthracene

ND 0.0201.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Dibenzofuran

ND 0.602.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Diethyl phthalate

ND 0.171.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Methylphenol

ND 0.292.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Dimethyl phthalate

ND 1.75.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Di-n-butyl phthalate

ND 0.212.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Nitroaniline

ND 0.232.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Di-n-octyl phthalate


ND 0.0450.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Fluoranthene


ND 0.0410.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Fluorene

ND 0.0850.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Hexachlorobenzene

ND 0.282.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Nitrophenol

ND 0.271.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Hexachlorobutadiene


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RL MDL

Hexachlorocyclopentadiene ND 10 0.24 ug/L 06/09/16 07:34 06/10/16 09:52 1

MB MB


ND 0.191.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Hexachloroethane

ND 0.0430.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Indeno[1,2,3-cd]pyrene

ND 0.401.0 ug/L 06/09/16 07:34 06/10/16 09:52 1bis (2-chloroisopropyl) ether

ND 0.271.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Isophorone

ND 0.0630.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Naphthalene

ND 0.0401.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Nitrobenzene

ND 0.241.0 ug/L 06/09/16 07:34 06/10/16 09:52 1N-Nitrosodi-n-propylamine

ND 0.311.0 ug/L 06/09/16 07:34 06/10/16 09:52 1N-Nitrosodiphenylamine

ND 0.305.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4,5-Trichlorophenol

ND 0.275.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Pentachlorophenol


ND 0.601.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Phenol

ND 0.0620.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Phenanthrene

ND 0.0420.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Pyrene

ND 0.802.0 ug/L 06/09/16 07:34 06/10/16 09:52 13 & 4 Methylphenol



MB MB

Surrogate

06/09/16 07:34





24 06/09/16 07:34 06/10/16 09:52 1Phenol-d5 (Surr) 10 - 120

76 06/09/16 07:34 06/10/16 09:52 1Terphenyl-d14 (Surr) 17 - 120


Benzaldehyde 40.0 37.0 ug/L 93 60 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

1,1'-Biphenyl 20.0 17.6 ug/L 88 58 - 120

Caprolactam 40.0 3.29 J * ug/L 8 10 - 120

Carbazole 20.0 20.0 ug/L 100 60 - 126

2-Chloronaphthalene 20.0 17.9 ug/L 89 56 - 120

2-Chlorophenol 20.0 15.9 ug/L 79 57 - 120

4-Bromophenyl phenyl ether 20.0 19.3 ug/L 97 52 - 128

4-Chloro-3-methylphenol 20.0 17.7 ug/L 89 59 - 120

2-Methylnaphthalene 20.0 18.0 ug/L 90 58 - 120

4-Chloroaniline 20.0 4.65 ug/L 23 10 - 120

4-Chlorophenyl phenyl ether 20.0 18.1 ug/L 91 58 - 120

3,3'-Dichlorobenzidine 40.0 31.8 ug/L 80 10 - 134

Acenaphthene 20.0 17.9 ug/L 89 57 - 120

2,4-Dichlorophenol 20.0 18.3 ug/L 92 57 - 120

Acenaphthylene 20.0 18.7 ug/L 94 55 - 120

Acetophenone 20.0 18.1 ug/L 90 60 - 120

2,4-Dimethylphenol 20.0 17.6 ug/L 88 55 - 120

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Anthracene 20.0 19.9 ug/L 99 58 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Atrazine 40.0 39.5 ug/L 99 61 - 132

4,6-Dinitro-2-methylphenol 40.0 35.5 ug/L 89 35 - 140

Benzo[a]anthracene 20.0 17.1 ug/L 86 59 - 120

2,4-Dinitrophenol 40.0 30.0 ug/L 75 18 - 127

Benzo[a]pyrene 20.0 16.6 ug/L 83 60 - 120

2,4-Dinitrotoluene 20.0 18.7 ug/L 93 65 - 120

Benzo[b]fluoranthene 20.0 17.0 ug/L 85 62 - 120

Benzo[g,h,i]perylene 20.0 17.7 ug/L 88 59 - 120

Benzo[k]fluoranthene 20.0 18.1 ug/L 90 57 - 120

Bis(2-chloroethoxy)methane 20.0 18.7 ug/L 94 61 - 120

Bis(2-chloroethyl)ether 20.0 17.6 ug/L 88 55 - 120

Bis(2-ethylhexyl) phthalate 20.0 14.4 ug/L 72 62 - 123

Butyl benzyl phthalate 20.0 16.7 ug/L 83 61 - 120

Chrysene 20.0 16.9 ug/L 84 61 - 120

Dibenz(a,h)anthracene 20.0 14.8 ug/L 74 61 - 120

Dibenzofuran 20.0 18.1 ug/L 91 58 - 120

Diethyl phthalate 20.0 19.0 ug/L 95 62 - 120

2-Methylphenol 20.0 13.1 ug/L 65 52 - 120

Dimethyl phthalate 20.0 19.2 ug/L 96 62 - 120

Di-n-butyl phthalate 20.0 19.9 ug/L 99 59 - 128

2-Nitroaniline 20.0 20.1 ug/L 100 56 - 123

Di-n-octyl phthalate 20.0 13.7 ug/L 68 58 - 120


Fluoranthene 20.0 19.5 ug/L 97 57 - 123


Fluorene 20.0 18.9 ug/L 94 56 - 120

Hexachlorobenzene 20.0 18.5 ug/L 92 47 - 127

2-Nitrophenol 20.0 17.2 ug/L 86 62 - 120

Hexachlorobutadiene 20.0 17.0 ug/L 85 50 - 120

4-Nitrophenol 40.0 12.1 ug/L 30 16 - 120

Hexachlorocyclopentadiene 20.0 16.3 ug/L 82 25 - 120

Hexachloroethane 20.0 16.6 ug/L 83 50 - 120

Indeno[1,2,3-cd]pyrene 20.0 15.4 ug/L 77 61 - 120

bis (2-chloroisopropyl) ether 20.0 18.0 ug/L 90 46 - 120

Isophorone 20.0 18.9 ug/L 95 61 - 120

Naphthalene 20.0 17.4 ug/L 87 54 - 120

Nitrobenzene 20.0 18.8 ug/L 94 58 - 120

N-Nitrosodi-n-propylamine 20.0 18.3 ug/L 91 60 - 120

N-Nitrosodiphenylamine 20.0 19.2 ug/L 96 54 - 122

2,4,5-Trichlorophenol 20.0 19.2 ug/L 96 57 - 120

Pentachlorophenol 40.0 37.2 ug/L 93 35 - 121


Phenol 20.0 5.06 ug/L 25 16 - 120

Phenanthrene 20.0 18.5 ug/L 93 58 - 120

Pyrene 20.0 19.3 ug/L 97 60 - 120

3 & 4 Methylphenol 20.0 11.7 ug/L 58 46 - 120


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Surrogate

87

LCS LCS








RL MDL

Caprolactam ND 5.0 0.20 ug/L 06/13/16 11:40 06/14/16 08:11 1

MB MB



MB MB

Surrogate

06/13/16 11:40





22 06/13/16 11:40 06/14/16 08:11 1Phenol-d5 (Surr) 10 - 120

82 06/13/16 11:40 06/14/16 08:11 1Terphenyl-d14 (Surr) 17 - 120



Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

72

LCS LCS







Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC)Lab Sample ID: 240-65485-1 MSMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233811 Prep Batch: 233761

Benzaldehyde ND 38.1 32.6 ug/L 86 42 - 120

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

1,1'-Biphenyl ND 19.0 15.4 ug/L 81 45 - 120

Caprolactam ND F1 * 38.1 2.36 J F1 ug/L 6 10 - 120

Carbazole ND 19.0 17.6 ug/L 93 55 - 120

2-Chloronaphthalene ND 19.0 15.6 ug/L 82 43 - 120

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2-Chlorophenol ND 19.0 12.7 ug/L 67 43 - 120

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

4-Bromophenyl phenyl ether ND 19.0 16.1 ug/L 85 32 - 120

4-Chloro-3-methylphenol ND 19.0 13.8 ug/L 73 49 - 120

2-Methylnaphthalene ND 19.0 15.8 ug/L 83 42 - 120

4-Chloroaniline ND 19.0 2.75 ug/L 14 10 - 120

4-Chlorophenyl phenyl ether ND 19.0 15.9 ug/L 83 41 - 120

3,3'-Dichlorobenzidine ND 38.1 26.4 ug/L 69 10 - 120

Acenaphthene ND 19.0 15.2 ug/L 80 37 - 120

2,4-Dichlorophenol ND 19.0 15.2 ug/L 80 44 - 120

Acenaphthylene ND 19.0 16.4 ug/L 86 40 - 120

Acetophenone ND 19.0 15.9 ug/L 83 43 - 120

2,4-Dimethylphenol ND 19.0 13.6 ug/L 71 38 - 120

Anthracene ND 19.0 17.1 ug/L 90 36 - 120

Atrazine ND 38.1 34.5 ug/L 90 50 - 122

4,6-Dinitro-2-methylphenol ND 38.1 21.9 ug/L 57 10 - 135

Benzo[a]anthracene ND 19.0 12.2 ug/L 64 18 - 120

2,4-Dinitrophenol ND 38.1 15.6 ug/L 41 10 - 122

Benzo[a]pyrene ND 19.0 10.5 ug/L 55 13 - 120

2,4-Dinitrotoluene ND 19.0 15.8 ug/L 83 50 - 120

Benzo[b]fluoranthene ND 19.0 11.5 ug/L 60 14 - 120

Benzo[g,h,i]perylene ND 19.0 10.6 ug/L 56 10 - 120

Benzo[k]fluoranthene ND 19.0 11.0 ug/L 58 13 - 120

Bis(2-chloroethoxy)methane ND 19.0 16.1 ug/L 85 50 - 120

Bis(2-chloroethyl)ether ND 19.0 15.2 ug/L 80 45 - 120

Bis(2-ethylhexyl) phthalate ND 19.0 9.57 ug/L 50 10 - 120

Butyl benzyl phthalate ND 19.0 14.3 ug/L 75 28 - 120

Chrysene ND 19.0 11.7 ug/L 61 17 - 120

Dibenz(a,h)anthracene ND 19.0 9.66 ug/L 51 10 - 120

Dibenzofuran ND 19.0 15.6 ug/L 82 44 - 120

Diethyl phthalate ND 19.0 16.8 ug/L 88 51 - 120

2-Methylphenol ND 19.0 9.49 ug/L 50 34 - 120

Dimethyl phthalate ND 19.0 16.6 ug/L 87 54 - 120

Di-n-butyl phthalate ND 19.0 16.8 ug/L 88 34 - 120

2-Nitroaniline ND 19.0 16.9 ug/L 89 49 - 120

Di-n-octyl phthalate ND 19.0 9.38 ug/L 49 10 - 120


Fluoranthene ND 19.0 16.3 ug/L 86 28 - 120


Fluorene ND 19.0 16.3 ug/L 85 38 - 120

Hexachlorobenzene ND 19.0 14.7 ug/L 77 17 - 120

2-Nitrophenol ND 19.0 14.7 ug/L 77 47 - 120

Hexachlorobutadiene ND 19.0 14.8 ug/L 77 32 - 120

4-Nitrophenol ND 38.1 6.93 ug/L 18 10 - 120

Hexachlorocyclopentadiene ND 19.0 9.31 J ug/L 49 10 - 120

Hexachloroethane ND 19.0 14.7 ug/L 77 10 - 120

Indeno[1,2,3-cd]pyrene ND 19.0 9.51 ug/L 50 10 - 120

bis (2-chloroisopropyl) ether ND 19.0 15.9 ug/L 84 39 - 120

Isophorone ND 19.0 16.3 ug/L 85 52 - 120

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Naphthalene 0.31 19.0 15.2 ug/L 78 37 - 120

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Nitrobenzene ND 19.0 15.9 ug/L 83 47 - 120

N-Nitrosodi-n-propylamine ND 19.0 16.5 ug/L 87 49 - 120

N-Nitrosodiphenylamine ND 19.0 16.9 ug/L 89 46 - 120

2,4,5-Trichlorophenol ND 19.0 16.4 ug/L 86 49 - 120

Pentachlorophenol ND 38.1 31.4 ug/L 83 32 - 120

2,4,6-Trichlorophenol ND 19.0 16.3 ug/L 86 51 - 120

Phenol ND 19.0 3.05 ug/L 16 10 - 120

Phenanthrene ND 19.0 15.9 ug/L 83 38 - 120

Pyrene ND 19.0 16.2 ug/L 85 26 - 120

3 & 4 Methylphenol ND 19.0 7.86 ug/L 41 26 - 120

2,6-Dinitrotoluene ND 19.0 17.6 ug/L 92 54 - 120


Surrogate

81

MS MS







Method: 8081B - Organochlorine Pesticides (GC)


RL MDL

4,4'-DDD ND 1.7 0.20 ug/Kg 06/03/16 07:28 06/10/16 17:39 1

MB MB


ND 0.271.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 14,4'-DDE

ND 0.311.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 14,4'-DDT

ND 0.201.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Aldrin

ND 0.601.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1alpha-BHC

ND 0.251.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1alpha-Chlordane

ND 0.361.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1beta-BHC

ND 0.221.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1delta-BHC

ND 0.161.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Dieldrin

ND 0.251.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endosulfan I

ND 0.381.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endosulfan II

ND 0.341.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endosulfan sulfate

ND 0.211.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endrin

ND 0.321.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endrin aldehyde

ND 0.421.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endrin ketone

ND 0.461.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1gamma-BHC (Lindane)

ND 0.861.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1gamma-Chlordane

ND 0.701.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Heptachlor

ND 0.401.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Heptachlor epoxide

ND 9.867 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Toxaphene

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Method: 8081B - Organochlorine Pesticides (GC) (Continued)


RL MDL

Methoxychlor ND 3.3 0.54 ug/Kg 06/03/16 07:28 06/10/16 17:39 1

MB MB


DCB Decachlorobiphenyl 81 42 - 138 06/10/16 17:39 1

MB MB

Surrogate

06/03/16 07:28


85 06/03/16 07:28 06/10/16 17:39 1DCB Decachlorobiphenyl 42 - 138

77 06/03/16 07:28 06/10/16 17:39 1Tetrachloro-m-xylene 31 - 159



4,4'-DDD 33.3 26.5 ug/Kg 80 47 - 157

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

4,4'-DDE 33.3 26.2 ug/Kg 79 56 - 125

4,4'-DDT 33.3 26.3 ug/Kg 79 57 - 142

Aldrin 33.3 23.5 ug/Kg 70 37 - 129

alpha-BHC 33.3 25.6 ug/Kg 77 50 - 125

alpha-Chlordane 33.3 24.8 ug/Kg 74 53 - 120

beta-BHC 33.3 24.7 ug/Kg 74 41 - 125

delta-BHC 33.3 21.6 ug/Kg 65 52 - 124

Dieldrin 33.3 25.9 ug/Kg 78 55 - 124

Endosulfan I 33.3 17.6 ug/Kg 53 18 - 120

Endosulfan II 33.3 20.8 ug/Kg 62 19 - 120

Endosulfan sulfate 33.3 24.6 ug/Kg 74 54 - 128

Endrin 33.3 27.5 ug/Kg 83 53 - 151

Endrin aldehyde 33.3 22.7 ug/Kg 68 44 - 130

Endrin ketone 33.3 24.3 ug/Kg 73 49 - 120

gamma-BHC (Lindane) 33.3 25.4 ug/Kg 76 50 - 123

gamma-Chlordane 33.3 25.2 ug/Kg 76 53 - 120

Heptachlor 33.3 27.0 ug/Kg 81 48 - 129

Heptachlor epoxide 33.3 25.4 ug/Kg 76 54 - 120

Methoxychlor 33.3 25.7 ug/Kg 77 52 - 147

DCB Decachlorobiphenyl 42 - 138

Surrogate

79

LCS LCS


74DCB Decachlorobiphenyl 42 - 138

70Tetrachloro-m-xylene 31 - 159



RL MDL

4,4'-DDD ND 0.050 0.018 ug/L 06/09/16 06:31 06/13/16 13:51 1

MB MB


ND 0.0120.050 ug/L 06/09/16 06:31 06/13/16 13:51 14,4'-DDE

ND 0.0170.050 ug/L 06/09/16 06:31 06/13/16 13:51 14,4'-DDT

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RL MDL

Aldrin ND 0.050 0.013 ug/L 06/09/16 06:31 06/13/16 13:51 1

MB MB


ND 0.0140.050 ug/L 06/09/16 06:31 06/13/16 13:51 1alpha-BHC

ND 0.0120.050 ug/L 06/09/16 06:31 06/13/16 13:51 1alpha-Chlordane

ND 0.0180.050 ug/L 06/09/16 06:31 06/13/16 13:51 1beta-BHC

ND 0.0290.050 ug/L 06/09/16 06:31 06/13/16 13:51 1delta-BHC

ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Dieldrin

ND 0.0160.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endosulfan I

ND 0.0150.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endosulfan II

ND 0.0150.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endosulfan sulfate

ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endrin

ND 0.0180.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endrin aldehyde

ND 0.0160.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endrin ketone

ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1gamma-BHC (Lindane)

ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1gamma-Chlordane

ND 0.0140.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Heptachlor

ND 0.0150.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Heptachlor epoxide

ND 0.202.0 ug/L 06/09/16 06:31 06/13/16 13:51 1Toxaphene

ND 0.0130.10 ug/L 06/09/16 06:31 06/13/16 13:51 1Methoxychlor


MB MB

Surrogate

06/09/16 06:31






4,4'-DDD 0.500 0.492 ug/L 98 54 - 163

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

4,4'-DDE 0.500 0.472 ug/L 94 60 - 146

4,4'-DDT 0.500 0.489 ug/L 98 56 - 160

Aldrin 0.500 0.439 ug/L 88 44 - 145

alpha-BHC 0.500 0.461 ug/L 92 53 - 148

alpha-Chlordane 0.500 0.475 ug/L 95 55 - 141

beta-BHC 0.500 0.469 ug/L 94 55 - 139

delta-BHC 0.500 0.409 ug/L 82 60 - 145

Dieldrin 0.500 0.485 ug/L 97 57 - 145

Endosulfan I 0.500 0.428 ug/L 86 26 - 120

Endosulfan II 0.500 0.460 ug/L 92 25 - 123

Endosulfan sulfate 0.500 0.471 ug/L 94 60 - 137

Endrin 0.500 0.462 ug/L 92 66 - 142

Endrin aldehyde 0.500 0.462 ug/L 92 59 - 120

Endrin ketone 0.500 0.481 ug/L 96 64 - 120

gamma-BHC (Lindane) 0.500 0.459 ug/L 92 53 - 144

gamma-Chlordane 0.500 0.483 ug/L 97 57 - 140

Heptachlor 0.500 0.441 ug/L 88 56 - 123

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Heptachlor epoxide 0.500 0.477 ug/L 95 44 - 151

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Methoxychlor 0.500 0.465 ug/L 93 56 - 153


Surrogate

66

LCS LCS






4,4'-DDD ND 0.476 0.410 ug/L 86 56 - 155

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

4,4'-DDE ND 0.476 0.388 ug/L 81 47 - 137

4,4'-DDT ND 0.476 0.399 ug/L 84 37 - 134

Aldrin ND 0.476 0.348 ug/L 73 51 - 120

alpha-BHC ND 0.476 0.447 ug/L 94 53 - 160

alpha-Chlordane ND 0.476 0.382 ug/L 80 42 - 153

beta-BHC ND 0.476 0.420 ug/L 88 42 - 160

delta-BHC ND 0.476 0.366 ug/L 77 49 - 160

Dieldrin ND 0.476 0.422 ug/L 89 48 - 160

Endosulfan I ND 0.476 0.395 ug/L 83 29 - 159

Endosulfan II ND 0.476 0.383 ug/L 81 35 - 142

Endosulfan sulfate ND 0.476 0.425 ug/L 89 47 - 150

Endrin ND 0.476 0.423 ug/L 89 50 - 149

Endrin aldehyde ND 0.476 0.414 ug/L 87 42 - 149

Endrin ketone ND 0.476 0.443 ug/L 93 39 - 138

gamma-BHC (Lindane) ND 0.476 0.437 ug/L 92 53 - 160

gamma-Chlordane ND 0.476 0.389 ug/L 82 45 - 153

Heptachlor ND 0.476 0.376 ug/L 79 36 - 128

Heptachlor epoxide ND 0.476 0.426 ug/L 89 35 - 160

Methoxychlor ND 0.476 0.397 ug/L 83 35 - 141


Surrogate

30

MS MS


29 XDCB Decachlorobiphenyl 30 - 128



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Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography


RL MDL

Aroclor-1016 ND 33 12 ug/Kg 06/03/16 07:23 06/06/16 15:06 1

MB MB


ND 1633 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1221

ND 2033 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1232

ND 1133 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1242

ND 8.033 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1248

ND 1433 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1254

ND 9.033 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1260

Tetrachloro-m-xylene 64 14 - 128 06/06/16 15:06 1

MB MB

Surrogate

06/03/16 07:23




Aroclor-1016 333 246 ug/Kg 74 47 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Aroclor-1260 333 277 ug/Kg 83 46 - 120

Tetrachloro-m-xylene 14 - 128

Surrogate

66

LCS LCS




RL MDL

Aroclor-1016 ND 0.10 0.050 ug/L 06/09/16 06:29 06/13/16 10:16 1

MB MB


ND 0.0900.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1221

ND 0.0700.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1232

ND 0.0600.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1242

ND 0.0500.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1248

ND 0.0300.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1254

ND 0.0400.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1260


MB MB

Surrogate

06/09/16 06:29




Aroclor-1016 2.50 1.60 ug/L 64 32 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

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Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)


Aroclor-1260 2.50 1.52 ug/L 61 36 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

60

LCS LCS




Aroclor-1016 ND 2.38 1.40 ug/L 59 24 - 121

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Aroclor-1260 ND 2.38 0.990 ug/L 42 10 - 120


Surrogate

59

MS MS



Method: 6020A - Metals (ICP/MS)

Client Sample ID: Method BlankLab Sample ID: MB 240-232891/1-A ^2Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233211 Prep Batch: 232891

RL MDL

Silver 0.00180 J 0.20 0.0014 mg/Kg 06/02/16 11:09 06/03/16 20:41 2

MB MB


1.64 J 0.6210 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Aluminum

0.0354 J 0.0261.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Arsenic

ND 0.221.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Barium

0.0228 J 0.0110.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Beryllium

0.00780 J 0.00370.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Cadmium

0.0170 J 0.00170.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Cobalt

0.347 J 0.0600.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Chromium

0.243 J 0.0970.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Copper

281 3.220 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Iron

1.73 0.121.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Manganese

0.0688 J 0.0450.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Lead

ND 0.0140.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Antimony

0.0472 J 0.0401.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Selenium

ND 0.0190.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Thallium

ND 0.0371.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Vanadium

1.17 J 0.504.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Zinc

34.7 J 22200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Calcium

8.60 J 4.9200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Potassium

7.73 J 4.0200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Magnesium

26.5 J 8.7200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Sodium

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Method: 6020A - Metals (ICP/MS) (Continued)


RL MDL

Nickel 0.0802 J 0.40 0.039 mg/Kg 06/02/16 11:09 06/06/16 14:18 2

MB MB


Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-232891/3-A ^2Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233211 Prep Batch: 232891

Silver 10.0 9.61 mg/Kg 96 60 - 114

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Aluminum 1000 964 mg/Kg 96 80 - 120

Arsenic 100 92.4 mg/Kg 92 73 - 110

Barium 100 95.2 mg/Kg 95 70 - 110

Beryllium 100 104 mg/Kg 104 79 - 110

Cadmium 100 92.8 mg/Kg 93 74 - 110

Cobalt 100 101 mg/Kg 101 74 - 110

Chromium 100 96.8 mg/Kg 97 70 - 110

Copper 100 98.5 mg/Kg 99 73 - 110

Iron 1000 982 mg/Kg 98 80 - 120

Manganese 100 98.4 mg/Kg 98 80 - 120

Lead 100 108 mg/Kg 108 75 - 110

Antimony 10.0 9.42 mg/Kg 94 68 - 113

Selenium 100 89.0 mg/Kg 89 65 - 110

Thallium 25.0 26.0 mg/Kg 104 71 - 110

Vanadium 100 96.6 mg/Kg 97 72 - 110

Zinc 100 95.9 mg/Kg 96 72 - 113

Calcium 1000 973 mg/Kg 97 80 - 120

Potassium 1000 1000 mg/Kg 100 80 - 120

Magnesium 1000 1000 mg/Kg 100 80 - 120

Sodium 1000 1010 mg/Kg 101 80 - 120


Nickel 100 99.0 mg/Kg 99 75 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Method BlankLab Sample ID: MB 240-233672/2-AMatrix: Solid Prep Type: Total RecoverableAnalysis Batch: 233954 Prep Batch: 233672

RL MDL

Silver ND 1.0 0.020 ug/L 06/08/16 13:00 06/09/16 13:40 1

MB MB


ND 9.050 ug/L 06/08/16 13:00 06/09/16 13:40 1Aluminum

ND 0.495.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Arsenic

ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Barium

ND 0.0531.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Beryllium

ND 0.0611.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Cadmium

ND 0.0211.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Cobalt

ND 0.602.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Chromium

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RL MDL

Copper ND 2.0 0.75 ug/L 06/08/16 13:00 06/09/16 13:40 1

MB MB


ND 16100 ug/L 06/08/16 13:00 06/09/16 13:40 1Iron

ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Manganese

ND 0.232.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Nickel

ND 0.111.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Lead

ND 0.162.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Antimony

0.288 J 0.255.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Selenium

ND 0.0741.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Thallium

ND 0.235.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Vanadium

ND 7.320 ug/L 06/08/16 13:00 06/09/16 13:40 1Zinc

ND 2401000 ug/L 06/08/16 13:00 06/09/16 13:40 1Calcium

ND 301000 ug/L 06/08/16 13:00 06/09/16 13:40 1Potassium

ND 481000 ug/L 06/08/16 13:00 06/09/16 13:40 1Magnesium

ND 681000 ug/L 06/08/16 13:00 06/09/16 13:40 1Sodium

Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233672/3-AMatrix: Solid Prep Type: Total RecoverableAnalysis Batch: 233954 Prep Batch: 233672

Silver 100 94.5 ug/L 95 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Aluminum 10000 10400 ug/L 104 80 - 120

Arsenic 1000 913 ug/L 91 80 - 120

Barium 1000 931 ug/L 93 80 - 120

Beryllium 1000 1140 ug/L 114 80 - 120

Cadmium 1000 927 ug/L 93 80 - 120

Cobalt 1000 952 ug/L 95 80 - 120

Chromium 1000 973 ug/L 97 80 - 120

Copper 1000 931 ug/L 93 80 - 120

Iron 10000 9370 ug/L 94 80 - 120

Manganese 1000 997 ug/L 100 80 - 120

Nickel 1000 966 ug/L 97 80 - 120

Lead 1000 823 ug/L 82 80 - 120

Antimony 100 94.0 ug/L 94 80 - 120

Selenium 1000 904 ug/L 90 80 - 120

Thallium 250 209 ug/L 84 80 - 120

Vanadium 1000 1010 ug/L 101 80 - 120

Zinc 1000 959 ug/L 96 80 - 120

Calcium 10000 10700 ug/L 107 80 - 120

Potassium 10000 9350 ug/L 93 80 - 120

Magnesium 10000 9570 ug/L 96 80 - 120

Sodium 10000 9620 ug/L 96 80 - 120

Client Sample ID: Method BlankLab Sample ID: LB 240-233529/1-CMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233954 Prep Batch: 233672

RL MDL

Silver ND 1.0 0.020 ug/L 06/08/16 13:00 06/09/16 13:36 1

LB LB


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RL MDL

Aluminum ND 50 9.0 ug/L 06/08/16 13:00 06/09/16 13:36 1

LB LB


ND 0.495.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Arsenic

ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Barium

ND 0.0531.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Beryllium

ND 0.0611.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Cadmium

0.115 J 0.0211.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Cobalt

ND 0.602.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Chromium

1.96 J 0.752.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Copper

ND 16100 ug/L 06/08/16 13:00 06/09/16 13:36 1Iron

ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Manganese

0.232 J 0.232.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Nickel

ND 0.111.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Lead

ND 0.162.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Antimony

ND 0.255.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Selenium

ND 0.0741.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Thallium

ND 0.235.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Vanadium

ND 7.320 ug/L 06/08/16 13:00 06/09/16 13:36 1Zinc

ND 2401000 ug/L 06/08/16 13:00 06/09/16 13:36 1Calcium

ND 301000 ug/L 06/08/16 13:00 06/09/16 13:36 1Potassium

ND 481000 ug/L 06/08/16 13:00 06/09/16 13:36 1Magnesium

184 J 681000 ug/L 06/08/16 13:00 06/09/16 13:36 1Sodium

Method: 7470A - Mercury (CVAA)


RL MDL

Mercury ND 0.20 0.090 ug/L 06/08/16 13:30 06/09/16 12:01 1

MB MB



Mercury 5.00 4.82 ug/L 96 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Method BlankLab Sample ID: LB 240-233529/1-DMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233843 Prep Batch: 233673

RL MDL

Mercury 0.0925 J 0.20 0.090 ug/L 06/08/16 13:30 06/09/16 11:58 1

LB LB


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RL MDL

Mercury ND 0.10 0.014 mg/Kg 06/02/16 15:00 06/03/16 07:27 1

MB MB



Mercury 0.833 0.865 mg/Kg 104 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Method: 7196A - Chromium, Hexavalent


RL MDL

Cr (VI) 0.358 J 0.80 0.15 mg/Kg 06/09/16 09:04 06/09/16 13:40 1

MB MB


Client Sample ID: Lab Control SampleLab Sample ID: LCSI 240-233791/11-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233886 Prep Batch: 233791

Cr (VI) 643 582 mg/Kg 90 75 - 125

Analyte

LCSI LCSI


Spike

Added

%Rec.

Limits

Client Sample ID: Lab Control SampleLab Sample ID: LCSS 240-233791/10-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233886 Prep Batch: 233791

Cr (VI) 20.0 18.5 mg/Kg 93 90 - 110

Analyte

LCSS LCSS


Spike

Added

%Rec.

Limits

Client Sample ID: Method BlankLab Sample ID: LB 240-233529/1-AMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233639

RL MDL

Cr (VI) ND 0.020 0.0021 mg/L 06/08/16 11:47 1

LB LB


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QC Association SummaryTestAmerica Job ID: 240-65485-1Client: Northeast Ohio Regional Sewer District


GC/MS VOA

Analysis Batch: 233030

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 8260B 233052240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA

Solid 8260BLCS 240-233030/5 Lab Control Sample Total/NA

Solid 8260BMB 240-233030/6 Method Blank Total/NA

Prep Batch: 233052


Solid 5030A240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA

Leach Batch: 233606


Solid 1312240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) SPLP

Solid 1312LB 240-233606/1-A MB Method Blank SPLP



Solid 8260B 233606240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) SPLP

Solid 8260B 233606LB 240-233606/1-A MB Method Blank SPLP


GC/MS Semi VOA

Prep Batch: 233013


Solid 3540C240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA

Solid 3540CLCS 240-233013/18-A Lab Control Sample Total/NA

Solid 3540CMB 240-233013/17-A Method Blank Total/NA



Solid 8270C 233013240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA

Solid 8270C 233013LCS 240-233013/18-A Lab Control Sample Total/NA

Solid 8270C 233013MB 240-233013/17-A Method Blank Total/NA

Leach Batch: 233529


Solid D3987-85240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach

Solid D3987-85240-65485-1 MS SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach

Prep Batch: 233761


Solid 3510C 233529240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach

Solid 3510C 233529240-65485-1 MS SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach







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GC/MS Semi VOA (Continued)





Leach Batch: 234140


Solid D3987-85240-65485-1 - RE SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach

Prep Batch: 234253


Solid 3510C 234140240-65485-1 - RE SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach





Solid 8270C 234253240-65485-1 - RE SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach



GC Semi VOA

Prep Batch: 233005





Prep Batch: 233006







Solid 8082A 233005240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA

Solid 8082A 233005LCS 240-233005/13-A Lab Control Sample Total/NA

Solid 8082A 233005MB 240-233005/12-A Method Blank Total/NA

Leach Batch: 233529



Solid D3987-85240-65485-1 MS SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach

Prep Batch: 233752






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GC Semi VOA (Continued)

Prep Batch: 233753








Solid 8081B 233006240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA

Solid 8081B 233006LCS 240-233006/6-A Lab Control Sample Total/NA

Solid 8081B 233006MB 240-233006/5-A Method Blank Total/NA



Solid 8082A 233752240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach

Solid 8082A 233752240-65485-1 MS SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach





Solid 8081B 233753240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach

Solid 8081B 233753240-65485-1 MS SOUTHERLY WWTC-ASH (SWWTC) ASTM Leach



Metals

Prep Batch: 232891


Solid 3050B240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA

Solid 3050BLCS 240-232891/3-A ^2 Lab Control Sample Total/NA

Solid 3050BMB 240-232891/1-A ^2 Method Blank Total/NA

Prep Batch: 232940



Solid 7471ALCS 240-232940/2-A Lab Control Sample Total/NA

Solid 7471AMB 240-232940/1-A Method Blank Total/NA









Solid 6020A 232891LCS 240-232891/3-A ^2 Lab Control Sample Total/NA

Solid 6020A 232891MB 240-232891/1-A ^2 Method Blank Total/NA

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Metals (Continued)






Leach Batch: 233529



Solid D3987-85LB 240-233529/1-C Method Blank ASTM Leach

Solid D3987-85LB 240-233529/1-D Method Blank ASTM Leach

Prep Batch: 233672



Solid 3005A 233529LB 240-233529/1-C Method Blank ASTM Leach

Solid 3005ALCS 240-233672/3-A Lab Control Sample Total Recoverable

Solid 3005AMB 240-233672/2-A Method Blank Total Recoverable

Prep Batch: 233673



Solid 7470A 233529LB 240-233529/1-D Method Blank ASTM Leach













Solid 6020A 233672LCS 240-233672/3-A Lab Control Sample Total Recoverable

Solid 6020A 233672MB 240-233672/2-A Method Blank Total Recoverable

General Chemistry



Solid Moisture240-65485-1 SOUTHERLY WWTC-ASH (SWWTC) Total/NA

Leach Batch: 233529



Solid D3987-85LB 240-233529/1-A Method Blank ASTM Leach

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General Chemistry (Continued)




Solid 7196A 233529LB 240-233529/1-A Method Blank ASTM Leach

Prep Batch: 233791



Solid 3060ALCSI 240-233791/11-A Lab Control Sample Total/NA

Solid 3060ALCSS 240-233791/10-A Lab Control Sample Total/NA





Solid 7196A 233791LCSI 240-233791/11-A Lab Control Sample Total/NA

Solid 7196A 233791LCSS 240-233791/10-A Lab Control Sample Total/NA


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Lab ChronicleClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65485-1Project/Site: SOUTHERLY WWTC-ASH (SWWTC)

Client Sample ID: SOUTHERLY WWTC-ASH (SWWTC) Lab Sample ID: 240-65485-1Matrix: SolidDate Collected: 05/31/16 13:25


Leach 1312 06/07/16 20:15 DRJ233606 TAL CAN

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

SPLP

Analysis 8260B 1 233711 06/08/16 20:25 TJL1 TAL CANSPLP

Leach D3987-85 233529 06/07/16 16:30 DRJ TAL CANASTM Leach

Prep 3510C 233761 06/09/16 07:34 CSC TAL CANASTM Leach

Analysis 8270C 1 233811 06/09/16 20:29 JMG TAL CANASTM Leach

Leach D3987-85 RE 234140 06/12/16 16:25 DRJ TAL CANASTM Leach

Prep 3510C RE 234253 06/13/16 11:40 JDR TAL CANASTM Leach

Analysis 8270C RE 1 234362 06/14/16 09:49 MRU TAL CANASTM Leach



Analysis 8081B 1 234206 06/13/16 14:40 BPM TAL CANASTM Leach



Analysis 8082A 1 234149 06/13/16 09:21 SEM TAL CANASTM Leach


Prep 3005A 233672 06/08/16 13:00 AJC TAL CANASTM Leach

Analysis 6020A 1 233954 06/09/16 14:08 AS1 TAL CANASTM Leach



Analysis 7470A 1 233843 06/09/16 12:18 WKD TAL CANASTM Leach


Analysis 7196A 1 233639 06/08/16 13:35 GNR TAL CANASTM Leach

Analysis Moisture 1 232880 06/02/16 10:25 LCN TAL CANTotal/NA



Prep 5030A 06/03/16 10:36 SAM233052 TAL CAN

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8260B 1 233030 06/03/16 18:41 SAM TAL CANTotal/NA

Prep 3540C 233013 06/03/16 08:23 DT TAL CANTotal/NA

Analysis 8270C 1 233383 06/07/16 11:12 JMG TAL CANTotal/NA


Analysis 8081B 1 233996 06/10/16 16:02 BPM TAL CANTotal/NA


Analysis 8082A 1 233178 06/06/16 14:28 HMB TAL CANTotal/NA

Prep 3050B 232891 06/02/16 11:09 DEE TAL CANTotal/NA

Analysis 6020A 2 233211 06/03/16 21:54 AS1 TAL CANTotal/NA



Prep 7471A 232940 06/02/16 15:00 DEE TAL CANTotal/NA

Analysis 7471A 1 233026 06/03/16 07:42 WKD TAL CANTotal/NA

Prep 3060A 233791 06/09/16 09:04 DTN TAL CANTotal/NA

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Lab ChronicleClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65485-1Project/Site: SOUTHERLY WWTC-ASH (SWWTC)



Analysis 7196A 06/09/16 13:44 DTN1 233886 TAL CAN

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA



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Certification SummaryClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65485-1Project/Site: SOUTHERLY WWTC-ASH (SWWTC)

Laboratory: TestAmerica CantonAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

California 01144CA9NELAP 06-30-14 *

California State Program 9 2927 04-30-17

Connecticut State Program 1 PH-0590 12-31-17

Florida NELAP 4 E87225 06-30-16 *

Illinois NELAP 5 200004 07-31-16 *

Kansas NELAP 7 E-10336 07-31-16 *

Kentucky (UST) State Program 4 58 02-23-17

Kentucky (WW) State Program 4 98016 12-31-16

L-A-B DoD ELAP L2315 07-18-16

Minnesota NELAP 5 039-999-348 12-31-16

Nevada State Program 9 OH-000482008A 07-31-16 *

New Jersey NELAP 2 OH001 06-30-16 *

New York NELAP 2 10975 03-31-17

Ohio VAP State Program 5 CL0024 09-14-17

Oregon NELAP 10 4062 02-23-17

Pennsylvania NELAP 3 68-00340 08-31-16 *

Texas NELAP 6 T104704517-15-5 08-31-16 *

USDA Federal P330-13-00319 11-26-16

Virginia NELAP 3 460175 09-14-16

Washington State Program 10 C971 01-12-17

West Virginia DEP State Program 3 210 12-31-16

Wisconsin State Program 5 999518190 08-31-16 *

TestAmerica Canton

* Certification renewal pending - certification considered valid.

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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Canton4101 Shuffel Street NWNorth Canton, OH 44720Tel: (330)497-9396

TestAmerica Job ID: 240-65486-1Client Project/Site: WESTERLY WWTC-ASH (WWWTC)

For:Northeast Ohio Regional Sewer District3900 Euclid AvenueCleveland, Ohio 44115

Attn: Ms. Sarah Rehner

Authorized for release by:6/14/2016 3:31:56 PM

Nathan Pietras, Project Manager II(330)[email protected]

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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https://secure.testamericainc.com/TotalAccess/login.aspx

http://www.testamericainc.com/AskTheExpert/Expert_index.htm

http://www.testamericainc.com


Table of Contents

Client: Northeast Ohio Regional Sewer DistrictProject/Site: WESTERLY WWTC-ASH (WWWTC)

TestAmerica Job ID: 240-65486-1

Page 2 of 55TestAmerica Canton

6/14/2016

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 8

Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 17

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21

QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45

Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 50

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53

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Definitions/GlossaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District

Project/Site: WESTERLY WWTC-ASH (WWWTC)

Qualifiers

GC/MS VOA



Qualifier



GC/MS Semi VOA



Qualifier


Metals



Qualifier


4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not

applicable.

General Chemistry



Qualifier


Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)

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Case NarrativeClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65486-1Project/Site: WESTERLY WWTC-ASH (WWWTC)

Job ID: 240-65486-1

Laboratory: TestAmerica Canton

Narrative

Job Narrative240-65486-1

Comments

No additional comments.

Receipt

The sample was received on 6/1/2016 10:20 AM; the sample arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 1.1º C.

GC/MS VOA Method(s) 8260B: Additional 5 mL of water added due to absorption of the soil for sample WESTERLY WWTC-ASH (WWWTC)

(240-65486-1)

Method(s) 8260B: The laboratory control sample (LCS) for preparation batch 240-233606 and analytical batch 240-233711 recovered outside control limits for 1,1,1-trichloroethane. This analyte was biased high in the LCS and was not detected in the associated samples; therefore, the data have been reported.


GC/MS Semi VOA Method(s) 8270C: The following sample was diluted due to the nature of the sample matrix: WESTERLY WWTC-ASH (WWWTC) (240-65486-1). Elevated reporting limits (RLs) are provided.

Method(s) 8270C: The laboratory control sample (LCS) for 233013 associated with sample WESTERLY WWTC-ASH (WWWTC) (240-65486-1), recovered outside control limits for the following analyte: N-Nitrosodiphenylamine. This analyte was biased high in the LCS and was not detected in the associated sample; therefore, the data have been reported.

Method(s) 8270C: The laboratory control sample (LCS) for 233761 recovered outside control limits for Caprolactam. The associated sample, WESTERLY WWTC-ASH (WWWTC) (240-65486-1), was re-prepared and re-analyzed with the Caprolactam recovery in the LCS (prep batch 234253) again failing to meet acceptance criteria. The initial results have been reported as has Caprolactam from the reextracted results.


GC Semi VOA

No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

General Chemistry No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

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Method SummaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District


Method Method Description LaboratoryProtocol

SW8468260B Volatile Organic Compounds (GC/MS) TAL CAN

SW8468270C Semivolatile Organic Compounds (GC/MS) TAL CAN

SW8468081B Organochlorine Pesticides (GC) TAL CAN

SW8468082A Polychlorinated Biphenyls (PCBs) by Gas Chromatography TAL CAN

SW8466020A Metals (ICP/MS) TAL CAN



SW8467196A Chromium, Hexavalent TAL CAN

EPAMoisture Percent Moisture TAL CAN

Protocol References:

EPA = US Environmental Protection Agency

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.



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Sample SummaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District


Lab Sample ID Client Sample ID ReceivedCollectedMatrix

240-65486-1 WESTERLY WWTC-ASH (WWWTC) Solid 05/31/16 14:10 06/01/16 10:20

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Detection SummaryTestAmerica Job ID: 240-65486-1Client: Northeast Ohio Regional Sewer District


Client Sample ID: WESTERLY WWTC-ASH (WWWTC) Lab Sample ID: 240-65486-1

☼Acetone

RL

19 ug/Kg

MDL

5.3

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA1J B7.8 8260B

☼Styrene 4.7 ug/Kg0.38 Total/NA11.1 J 8260B

☼Toluene 4.7 ug/Kg0.25 Total/NA10.34 J 8260B

Acetone 10 ug/L0.94 SPLP15.1 J B 8260B

Chloroform 1.0 ug/L0.25 SPLP11.1 B 8260B

Methylene Chloride 1.0 ug/L0.33 SPLP13.1 B 8260B

Styrene 1.0 ug/L0.45 SPLP10.53 J 8260B

N-Nitrosodiphenylamine 0.95 ug/L0.30 ASTM Leach12.8 8270C

☼Silver 0.19 mg/Kg0.0013 Total/NA24.0 B 6020A

☼Aluminum 9.4 mg/Kg0.58 Total/NA220000 B 6020A

☼Arsenic 0.94 mg/Kg0.024 Total/NA220 B 6020A

☼Barium 0.94 mg/Kg0.21 Total/NA2660 6020A

☼Beryllium 0.19 mg/Kg0.010 Total/NA21.1 B 6020A

☼Cadmium 0.19 mg/Kg0.0035 Total/NA27.1 B 6020A

☼Cobalt 0.19 mg/Kg0.0016 Total/NA213 B 6020A

☼Chromium 0.38 mg/Kg0.056 Total/NA2440 B 6020A

☼Copper 0.38 mg/Kg0.091 Total/NA2350 B 6020A

☼Iron 190 mg/Kg30 Total/NA2062000 B 6020A

☼Manganese 0.94 mg/Kg0.11 Total/NA2540 B 6020A

☼Nickel 0.38 mg/Kg0.037 Total/NA280 B 6020A

☼Lead 0.19 mg/Kg0.042 Total/NA2310 B 6020A

☼Antimony 0.38 mg/Kg0.013 Total/NA22.4 6020A

☼Selenium 0.94 mg/Kg0.038 Total/NA24.2 B 6020A

☼Thallium 0.38 mg/Kg0.018 Total/NA20.63 6020A

☼Vanadium 0.94 mg/Kg0.035 Total/NA260 6020A

☼Zinc 3.8 mg/Kg0.47 Total/NA2870 B 6020A

☼Calcium 190 mg/Kg21 Total/NA257000 B 6020A

☼Potassium 190 mg/Kg4.6 Total/NA26300 B 6020A

☼Magnesium 190 mg/Kg3.8 Total/NA215000 B 6020A

☼Sodium 190 mg/Kg8.2 Total/NA21300 B 6020A

Aluminum 50 ug/L9.0 ASTM Leach14100 6020A

Arsenic 5.0 ug/L0.49 ASTM Leach11.6 J 6020A

Barium 5.0 ug/L1.1 ASTM Leach1140 6020A

Beryllium 1.0 ug/L0.053 ASTM Leach10.16 J 6020A

Cadmium 1.0 ug/L0.061 ASTM Leach10.24 J 6020A

Cobalt 1.0 ug/L0.021 ASTM Leach10.19 J B 6020A

Chromium 2.0 ug/L0.60 ASTM Leach11500 6020A

Lead 1.0 ug/L0.11 ASTM Leach10.70 J 6020A

Antimony 2.0 ug/L0.16 ASTM Leach12.4 6020A

Selenium 5.0 ug/L0.25 ASTM Leach117 B 6020A

Thallium 1.0 ug/L0.074 ASTM Leach10.19 J 6020A

Vanadium 5.0 ug/L0.23 ASTM Leach198 6020A

Calcium 1000 ug/L240 ASTM Leach1250000 6020A

Potassium 1000 ug/L30 ASTM Leach111000 6020A

Magnesium 1000 ug/L48 ASTM Leach1140 J 6020A

Sodium 1000 ug/L68 ASTM Leach14200 B 6020A

☼Cr (VI) 0.79 mg/Kg0.15 Total/NA120 B 7196A

Cr (VI) 0.020 mg/L0.0021 ASTM Leach10.28 7196A

TestAmerica Canton

This Detection Summary does not include radiochemical test results.

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Lab Sample ID: 240-65486-1Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Matrix: SolidDate Collected: 05/31/16 14:10


Method: 8260B - Volatile Organic Compounds (GC/MS) - SPLPRL MDL

Acetone 5.1 J B 10 0.94 ug/L 06/08/16 20:49 1


1.0 0.35 ug/L 06/08/16 20:49 1Benzene ND

1.0 0.29 ug/L 06/08/16 20:49 1Dichlorobromomethane ND

1.0 0.56 ug/L 06/08/16 20:49 1Bromoform ND

1.0 0.44 ug/L 06/08/16 20:49 1Bromomethane ND

10 0.53 ug/L 06/08/16 20:49 12-Butanone (MEK) ND

1.0 0.38 ug/L 06/08/16 20:49 1Carbon disulfide ND

1.0 0.43 ug/L 06/08/16 20:49 1Carbon tetrachloride ND

1.0 0.25 ug/L 06/08/16 20:49 1Chlorobenzene ND

1.0 0.32 ug/L 06/08/16 20:49 1Chloroethane ND

1.0 0.25 ug/L 06/08/16 20:49 1Chloroform 1.1 B

1.0 0.44 ug/L 06/08/16 20:49 1Chloromethane ND



1.0 0.45 ug/L 06/08/16 20:49 11,1-Dichloroethene ND

1.0 0.25 ug/L 06/08/16 20:49 11,2-Dichloropropane ND

1.0 0.46 ug/L 06/08/16 20:49 1cis-1,3-Dichloropropene ND

1.0 0.56 ug/L 06/08/16 20:49 1trans-1,3-Dichloropropene ND

1.0 0.25 ug/L 06/08/16 20:49 1Ethylbenzene ND

10 0.48 ug/L 06/08/16 20:49 12-Hexanone ND

1.0 0.33 ug/L 06/08/16 20:49 1Methylene Chloride 3.1 B

10 0.99 ug/L 06/08/16 20:49 14-Methyl-2-pentanone (MIBK) ND

1.0 0.45 ug/L 06/08/16 20:49 1Styrene 0.53 J

1.0 0.22 ug/L 06/08/16 20:49 11,1,2,2-Tetrachloroethane ND

1.0 0.31 ug/L 06/08/16 20:49 1Tetrachloroethene ND

1.0 0.23 ug/L 06/08/16 20:49 1Toluene ND

1.0 0.22 ug/L 06/08/16 20:49 1Trichloroethene ND

1.0 0.29 ug/L 06/08/16 20:49 1Vinyl chloride ND

2.0 0.52 ug/L 06/08/16 20:49 1Xylenes, Total ND

1.0 0.44 ug/L 06/08/16 20:49 11,1,1-Trichloroethane ND *

1.0 0.24 ug/L 06/08/16 20:49 11,1,2-Trichloroethane ND

1.0 0.45 ug/L 06/08/16 20:49 1Cyclohexane ND

2.0 0.82 ug/L 06/08/16 20:49 11,2-Dibromo-3-Chloropropane ND

1.0 0.32 ug/L 06/08/16 20:49 1Ethylene Dibromide ND

1.0 0.32 ug/L 06/08/16 20:49 1Dichlorodifluoromethane ND

1.0 0.26 ug/L 06/08/16 20:49 1cis-1,2-Dichloroethene ND

1.0 0.30 ug/L 06/08/16 20:49 1trans-1,2-Dichloroethene ND

1.0 0.35 ug/L 06/08/16 20:49 1Isopropylbenzene ND

10 2.3 ug/L 06/08/16 20:49 1Methyl acetate ND

1.0 0.20 ug/L 06/08/16 20:49 1Methyl tert-butyl ether ND

1.0 0.45 ug/L 06/08/16 20:49 11,1,2-Trichloro-1,2,2-trifluoroethane ND

1.0 0.32 ug/L 06/08/16 20:49 11,2,4-Trichlorobenzene ND




1.0 0.49 ug/L 06/08/16 20:49 1Trichlorofluoromethane ND

1.0 0.43 ug/L 06/08/16 20:49 1Chlorodibromomethane ND

1.0 0.43 ug/L 06/08/16 20:49 1Methylcyclohexane ND

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4-Bromofluorobenzene (Surr) 86 06/08/16 20:49 161 - 120

Toluene-d8 (Surr) 94 06/08/16 20:49 180 - 120

Dibromofluoromethane (Surr) 87 06/08/16 20:49 179 - 120

Method: 8270C - Semivolatile Organic Compounds (GC/MS) - ASTM LeachRL MDL

Acenaphthene ND 0.19 0.042 ug/L 06/09/16 07:34 06/09/16 21:17 1


0.19 0.046 ug/L 06/09/16 07:34 06/09/16 21:17 1Acenaphthylene ND

0.95 0.32 ug/L 06/09/16 07:34 06/09/16 21:17 1Acetophenone ND

0.19 0.084 ug/L 06/09/16 07:34 06/09/16 21:17 1Anthracene ND

0.95 0.32 ug/L 06/09/16 07:34 06/09/16 21:17 1Atrazine ND

0.95 0.37 ug/L 06/09/16 07:34 06/09/16 21:17 1Benzaldehyde ND

0.19 0.028 ug/L 06/09/16 07:34 06/09/16 21:17 1Benzo[a]anthracene ND

0.19 0.038 ug/L 06/09/16 07:34 06/09/16 21:17 1Benzo[b]fluoranthene ND

0.19 0.043 ug/L 06/09/16 07:34 06/09/16 21:17 1Benzo[k]fluoranthene ND

0.19 0.044 ug/L 06/09/16 07:34 06/09/16 21:17 1Benzo[g,h,i]perylene ND

0.19 0.049 ug/L 06/09/16 07:34 06/09/16 21:17 1Benzo[a]pyrene ND

1.9 0.25 ug/L 06/09/16 07:34 06/09/16 21:17 1Butyl benzyl phthalate ND

0.95 0.12 ug/L 06/09/16 07:34 06/09/16 21:17 11,1'-Biphenyl ND

0.95 0.30 ug/L 06/09/16 07:34 06/09/16 21:17 1Bis(2-chloroethoxy)methane ND

0.95 0.095 ug/L 06/09/16 07:34 06/09/16 21:17 1Bis(2-chloroethyl)ether ND

4.8 1.6 ug/L 06/09/16 07:34 06/09/16 21:17 1Bis(2-ethylhexyl) phthalate ND

1.9 0.21 ug/L 06/09/16 07:34 06/09/16 21:17 14-Bromophenyl phenyl ether ND

4.8 0.19 ug/L 06/09/16 07:34 06/09/16 21:17 1Caprolactam ND *

0.95 0.27 ug/L 06/09/16 07:34 06/09/16 21:17 1Carbazole ND

1.9 0.20 ug/L 06/09/16 07:34 06/09/16 21:17 14-Chloroaniline ND

1.9 0.20 ug/L 06/09/16 07:34 06/09/16 21:17 14-Chloro-3-methylphenol ND

0.95 0.095 ug/L 06/09/16 07:34 06/09/16 21:17 12-Chloronaphthalene ND

0.95 0.28 ug/L 06/09/16 07:34 06/09/16 21:17 12-Chlorophenol ND

1.9 0.29 ug/L 06/09/16 07:34 06/09/16 21:17 14-Chlorophenyl phenyl ether ND

0.19 0.048 ug/L 06/09/16 07:34 06/09/16 21:17 1Chrysene ND

0.19 0.086 ug/L 06/09/16 07:34 06/09/16 21:17 12-Methylnaphthalene ND

1.9 0.76 ug/L 06/09/16 07:34 06/09/16 21:17 13 & 4 Methylphenol ND

0.19 0.042 ug/L 06/09/16 07:34 06/09/16 21:17 1Dibenz(a,h)anthracene ND

0.95 0.019 ug/L 06/09/16 07:34 06/09/16 21:17 1Dibenzofuran ND

4.8 0.35 ug/L 06/09/16 07:34 06/09/16 21:17 13,3'-Dichlorobenzidine ND

1.9 0.18 ug/L 06/09/16 07:34 06/09/16 21:17 12,4-Dichlorophenol ND

1.9 0.57 ug/L 06/09/16 07:34 06/09/16 21:17 1Diethyl phthalate ND

1.9 0.24 ug/L 06/09/16 07:34 06/09/16 21:17 12,4-Dimethylphenol ND

1.9 0.28 ug/L 06/09/16 07:34 06/09/16 21:17 1Dimethyl phthalate ND

4.8 2.3 ug/L 06/09/16 07:34 06/09/16 21:17 14,6-Dinitro-2-methylphenol ND

4.8 0.30 ug/L 06/09/16 07:34 06/09/16 21:17 12,4-Dinitrophenol ND


4.8 1.6 ug/L 06/09/16 07:34 06/09/16 21:17 1Di-n-butyl phthalate ND

1.9 0.22 ug/L 06/09/16 07:34 06/09/16 21:17 1Di-n-octyl phthalate ND

0.19 0.042 ug/L 06/09/16 07:34 06/09/16 21:17 1Fluoranthene ND

0.19 0.039 ug/L 06/09/16 07:34 06/09/16 21:17 1Fluorene ND

0.19 0.081 ug/L 06/09/16 07:34 06/09/16 21:17 1Hexachlorobenzene ND

0.95 0.26 ug/L 06/09/16 07:34 06/09/16 21:17 1Hexachlorobutadiene ND

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Method: 8270C - Semivolatile Organic Compounds (GC/MS) - ASTM Leach (Continued)RL MDL

Hexachlorocyclopentadiene ND 9.5 0.23 ug/L 06/09/16 07:34 06/09/16 21:17 1


0.95 0.18 ug/L 06/09/16 07:34 06/09/16 21:17 1Hexachloroethane ND

0.19 0.041 ug/L 06/09/16 07:34 06/09/16 21:17 1Indeno[1,2,3-cd]pyrene ND

0.95 0.26 ug/L 06/09/16 07:34 06/09/16 21:17 1Isophorone ND

0.95 0.16 ug/L 06/09/16 07:34 06/09/16 21:17 12-Methylphenol ND

0.19 0.060 ug/L 06/09/16 07:34 06/09/16 21:17 1Naphthalene ND




0.95 0.038 ug/L 06/09/16 07:34 06/09/16 21:17 1Nitrobenzene ND



0.95 0.30 ug/L 06/09/16 07:34 06/09/16 21:17 1N-Nitrosodiphenylamine 2.8

0.95 0.23 ug/L 06/09/16 07:34 06/09/16 21:17 1N-Nitrosodi-n-propylamine ND

0.95 0.38 ug/L 06/09/16 07:34 06/09/16 21:17 1bis (2-chloroisopropyl) ether ND

4.8 0.26 ug/L 06/09/16 07:34 06/09/16 21:17 1Pentachlorophenol ND

0.19 0.059 ug/L 06/09/16 07:34 06/09/16 21:17 1Phenanthrene ND

0.95 0.57 ug/L 06/09/16 07:34 06/09/16 21:17 1Phenol ND

0.19 0.040 ug/L 06/09/16 07:34 06/09/16 21:17 1Pyrene ND









Phenol-d5 (Surr) 19 06/09/16 07:34 06/09/16 21:17 110 - 120

Terphenyl-d14 (Surr) 89 06/09/16 07:34 06/09/16 21:17 117 - 120

Method: 8270C - Semivolatile Organic Compounds (GC/MS) - ASTM Leach - RERL MDL

Caprolactam ND * 5.0 0.20 ug/L 06/13/16 11:40 06/14/16 10:13 1







Phenol-d5 (Surr) 24 06/13/16 11:40 06/14/16 10:13 110 - 120

Terphenyl-d14 (Surr) 65 06/13/16 11:40 06/14/16 10:13 117 - 120

Method: 8081B - Organochlorine Pesticides (GC) - ASTM LeachRL MDL

4,4'-DDD ND 0.048 0.017 ug/L 06/09/16 06:31 06/13/16 15:28 1


0.048 0.011 ug/L 06/09/16 06:31 06/13/16 15:28 14,4'-DDE ND

0.048 0.016 ug/L 06/09/16 06:31 06/13/16 15:28 14,4'-DDT ND

0.048 0.012 ug/L 06/09/16 06:31 06/13/16 15:28 1Aldrin ND

0.048 0.013 ug/L 06/09/16 06:31 06/13/16 15:28 1alpha-BHC ND

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Method: 8081B - Organochlorine Pesticides (GC) - ASTM Leach (Continued)RL MDL

beta-BHC ND 0.048 0.017 ug/L 06/09/16 06:31 06/13/16 15:28 1


0.048 0.011 ug/L 06/09/16 06:31 06/13/16 15:28 1alpha-Chlordane ND

0.048 0.028 ug/L 06/09/16 06:31 06/13/16 15:28 1delta-BHC ND

0.048 0.012 ug/L 06/09/16 06:31 06/13/16 15:28 1gamma-BHC (Lindane) ND

0.048 0.012 ug/L 06/09/16 06:31 06/13/16 15:28 1gamma-Chlordane ND

0.048 0.012 ug/L 06/09/16 06:31 06/13/16 15:28 1Dieldrin ND

0.048 0.015 ug/L 06/09/16 06:31 06/13/16 15:28 1Endosulfan I ND

0.048 0.014 ug/L 06/09/16 06:31 06/13/16 15:28 1Endosulfan II ND

0.048 0.014 ug/L 06/09/16 06:31 06/13/16 15:28 1Endosulfan sulfate ND

0.048 0.012 ug/L 06/09/16 06:31 06/13/16 15:28 1Endrin ND

0.048 0.017 ug/L 06/09/16 06:31 06/13/16 15:28 1Endrin aldehyde ND

0.048 0.015 ug/L 06/09/16 06:31 06/13/16 15:28 1Endrin ketone ND

0.048 0.013 ug/L 06/09/16 06:31 06/13/16 15:28 1Heptachlor ND

0.048 0.014 ug/L 06/09/16 06:31 06/13/16 15:28 1Heptachlor epoxide ND

0.095 0.012 ug/L 06/09/16 06:31 06/13/16 15:28 1Methoxychlor ND

1.9 0.19 ug/L 06/09/16 06:31 06/13/16 15:28 1Toxaphene ND






Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography - ASTM LeachRL MDL

Aroclor-1016 ND 0.095 0.048 ug/L 06/09/16 06:29 06/13/16 09:58 1


0.095 0.086 ug/L 06/09/16 06:29 06/13/16 09:58 1Aroclor-1221 ND

0.095 0.067 ug/L 06/09/16 06:29 06/13/16 09:58 1Aroclor-1232 ND

0.095 0.057 ug/L 06/09/16 06:29 06/13/16 09:58 1Aroclor-1242 ND

0.095 0.048 ug/L 06/09/16 06:29 06/13/16 09:58 1Aroclor-1248 ND

0.095 0.029 ug/L 06/09/16 06:29 06/13/16 09:58 1Aroclor-1254 ND

0.095 0.038 ug/L 06/09/16 06:29 06/13/16 09:58 1Aroclor-1260 ND




Method: 6020A - Metals (ICP/MS) - ASTM LeachRL MDL

Silver ND 1.0 0.020 ug/L 06/08/16 13:00 06/09/16 13:48 1


50 9.0 ug/L 06/08/16 13:00 06/09/16 13:48 1Aluminum 4100

5.0 0.49 ug/L 06/08/16 13:00 06/09/16 13:48 1Arsenic 1.6 J

5.0 1.1 ug/L 06/08/16 13:00 06/09/16 13:48 1Barium 140

1.0 0.053 ug/L 06/08/16 13:00 06/09/16 13:48 1Beryllium 0.16 J

1.0 0.061 ug/L 06/08/16 13:00 06/09/16 13:48 1Cadmium 0.24 J

1.0 0.021 ug/L 06/08/16 13:00 06/09/16 13:48 1Cobalt 0.19 J B

2.0 0.60 ug/L 06/08/16 13:00 06/09/16 13:48 1Chromium 1500

2.0 0.75 ug/L 06/08/16 13:00 06/09/16 13:48 1Copper ND

100 16 ug/L 06/08/16 13:00 06/09/16 13:48 1Iron ND

5.0 1.1 ug/L 06/08/16 13:00 06/09/16 13:48 1Manganese ND

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Method: 6020A - Metals (ICP/MS) - ASTM Leach (Continued)RL MDL

Nickel ND 2.0 0.23 ug/L 06/08/16 13:00 06/09/16 13:48 1


1.0 0.11 ug/L 06/08/16 13:00 06/09/16 13:48 1Lead 0.70 J

2.0 0.16 ug/L 06/08/16 13:00 06/09/16 13:48 1Antimony 2.4

5.0 0.25 ug/L 06/08/16 13:00 06/09/16 13:48 1Selenium 17 B

1.0 0.074 ug/L 06/08/16 13:00 06/09/16 13:48 1Thallium 0.19 J

5.0 0.23 ug/L 06/08/16 13:00 06/09/16 13:48 1Vanadium 98

20 7.3 ug/L 06/08/16 13:00 06/09/16 13:48 1Zinc ND

1000 240 ug/L 06/08/16 13:00 06/09/16 13:48 1Calcium 250000

1000 30 ug/L 06/08/16 13:00 06/09/16 13:48 1Potassium 11000

1000 48 ug/L 06/08/16 13:00 06/09/16 13:48 1Magnesium 140 J

1000 68 ug/L 06/08/16 13:00 06/09/16 13:48 1Sodium 4200 B

Method: 7470A - Mercury (CVAA) - ASTM LeachRL MDL

Mercury ND 0.20 0.090 ug/L 06/08/16 13:30 06/09/16 12:05 1



Percent Solids 99.7 0.1 0.1 % 06/02/16 10:25 1


0.1 0.1 % 06/02/16 10:25 1Percent Moisture 0.3

General Chemistry - ASTM LeachRL MDL

Cr (VI) 0.28 0.020 0.0021 mg/L 06/08/16 13:35 1


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Method: 8260B - Volatile Organic Compounds (GC/MS)RL MDL

Acetone 7.8 J B 19 5.3 ug/Kg ☼ 06/03/16 10:36 06/03/16 19:07 1


4.7 0.84 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Benzene ND

4.7 0.27 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Dichlorobromomethane ND

4.7 0.23 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Bromoform ND

4.7 0.39 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Bromomethane ND

19 1.1 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼2-Butanone (MEK) ND

4.7 0.55 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Carbon disulfide ND

4.7 0.61 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Carbon tetrachloride ND

4.7 0.50 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Chlorobenzene ND

4.7 0.41 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Chloroethane ND

4.7 0.34 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Chloroform ND

4.7 0.74 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Chloromethane ND



4.7 0.75 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,1-Dichloroethene ND

4.7 0.13 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,2-Dichloropropane ND

4.7 0.67 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼cis-1,3-Dichloropropene ND

4.7 0.27 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼trans-1,3-Dichloropropene ND

4.7 0.30 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Ethylbenzene ND

19 0.64 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼2-Hexanone ND

4.7 0.69 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Methylene Chloride ND

19 1.1 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼4-Methyl-2-pentanone (MIBK) ND

4.7 0.38 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Styrene 1.1 J

4.7 0.29 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,1,2,2-Tetrachloroethane ND

4.7 0.75 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Tetrachloroethene ND

4.7 0.25 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Toluene 0.34 J

4.7 0.36 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Trichloroethene ND

4.7 0.28 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Vinyl chloride ND

9.4 0.51 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Xylenes, Total ND



9.4 0.45 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Cyclohexane ND

9.4 2.5 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,2-Dibromo-3-Chloropropane ND

4.7 0.50 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Ethylene Dibromide ND

4.7 0.26 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Dichlorodifluoromethane ND

4.7 0.26 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼cis-1,2-Dichloroethene ND

4.7 0.30 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼trans-1,2-Dichloroethene ND

4.7 0.19 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Isopropylbenzene ND

9.4 1.9 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Methyl acetate ND

4.7 0.40 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Methyl tert-butyl ether ND

4.7 0.39 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,1,2-Trichloro-1,2,2-trifluoroethane ND

4.7 0.36 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼1,2,4-Trichlorobenzene ND




4.7 0.27 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Trichlorofluoromethane ND

4.7 0.35 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Chlorodibromomethane ND

9.4 0.54 ug/Kg 06/03/16 10:36 06/03/16 19:07 1☼Methylcyclohexane ND

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1,2-Dichloroethane-d4 (Surr) 97 58 - 123 06/03/16 10:36 06/03/16 19:07 1


4-Bromofluorobenzene (Surr) 98 06/03/16 10:36 06/03/16 19:07 152 - 136

Toluene-d8 (Surr) 101 06/03/16 10:36 06/03/16 19:07 167 - 125

Dibromofluoromethane (Surr) 79 06/03/16 10:36 06/03/16 19:07 137 - 132

Method: 8270C - Semivolatile Organic Compounds (GC/MS)RL MDL

bis (2-chloroisopropyl) ether ND 400 38 ug/Kg ☼ 06/03/16 08:23 06/08/16 21:44 4




610 81 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2,4-Dichlorophenol ND

610 81 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2,4-Dimethylphenol ND

1300 85 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2,4-Dinitrophenol ND



200 1.8 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2-Chloronaphthalene ND

200 33 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2-Chlorophenol ND

27 2.0 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2-Methylnaphthalene ND

810 44 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼2-Methylphenol ND



400 73 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼3,3'-Dichlorobenzidine ND


610 37 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼4,6-Dinitro-2-methylphenol ND

200 53 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼4-Bromophenyl phenyl ether ND

610 85 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼4-Chloro-3-methylphenol ND

610 69 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼4-Chloroaniline ND

200 53 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼4-Chlorophenyl phenyl ether ND



27 3.1 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Acenaphthene ND

27 1.4 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Acenaphthylene ND

400 37 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Acetophenone ND

27 3.2 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Anthracene ND

810 37 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Atrazine ND

27 2.5 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Benzo[a]anthracene ND

27 2.6 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Benzo[a]pyrene ND

27 2.4 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Benzo[b]fluoranthene ND

27 1.4 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Benzo[g,h,i]perylene ND

27 2.7 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Benzo[k]fluoranthene ND

400 89 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Bis(2-chloroethoxy)methane ND

400 8.1 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Bis(2-chloroethyl)ether ND

280 77 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Bis(2-ethylhexyl) phthalate ND

280 40 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Butyl benzyl phthalate ND

27 4.4 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Chrysene ND

27 2.7 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Dibenz(a,h)anthracene ND

200 2.7 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Dibenzofuran ND

280 65 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Diethyl phthalate ND

280 69 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Dimethyl phthalate ND

280 61 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Di-n-butyl phthalate ND

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Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued)RL MDL

Di-n-octyl phthalate ND 280 32 ug/Kg ☼ 06/03/16 08:23 06/08/16 21:44 4


27 2.2 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Fluoranthene ND

27 2.1 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Fluorene ND

27 8.5 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Hexachlorobenzene ND

200 23 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Hexachlorobutadiene ND

1300 33 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Hexachlorocyclopentadiene ND

200 36 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Hexachloroethane ND

27 1.4 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Indeno[1,2,3-cd]pyrene ND

200 53 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Isophorone ND

27 3.3 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Naphthalene ND

400 8.9 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Nitrobenzene ND

200 25 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼N-Nitrosodi-n-propylamine ND

200 85 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼N-Nitrosodiphenylamine ND *

610 37 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Pentachlorophenol ND

200 30 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Phenol ND

27 3.0 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Phenanthrene ND

27 1.8 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼Pyrene ND

1600 81 ug/Kg 06/03/16 08:23 06/08/16 21:44 4☼3 & 4 Methylphenol ND






Phenol-d5 (Surr) 47 06/03/16 08:23 06/08/16 21:44 432 - 120

Terphenyl-d14 (Surr) 78 06/03/16 08:23 06/08/16 21:44 447 - 120

Method: 8081B - Organochlorine Pesticides (GC)RL MDL

4,4'-DDD ND 1.7 0.20 ug/Kg ☼ 06/03/16 07:28 06/10/16 16:27 1


1.7 0.28 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼4,4'-DDE ND

1.7 0.32 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼4,4'-DDT ND

1.7 0.20 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Aldrin ND

1.7 0.61 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼alpha-BHC ND

1.7 0.25 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼alpha-Chlordane ND

1.7 0.37 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼beta-BHC ND

1.7 0.22 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼delta-BHC ND

1.7 0.16 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Dieldrin ND

1.7 0.25 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Endosulfan I ND

1.7 0.39 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Endosulfan II ND

1.7 0.35 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Endosulfan sulfate ND

1.7 0.21 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Endrin ND

1.7 0.33 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Endrin aldehyde ND

1.7 0.43 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Endrin ketone ND

1.7 0.47 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼gamma-BHC (Lindane) ND

1.7 0.88 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼gamma-Chlordane ND

1.7 0.71 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Heptachlor ND

1.7 0.41 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Heptachlor epoxide ND

68 10 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Toxaphene ND

3.4 0.55 ug/Kg 06/03/16 07:28 06/10/16 16:27 1☼Methoxychlor ND

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Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyRL MDL

Aroclor-1016 ND 34 12 ug/Kg ☼ 06/03/16 07:23 06/06/16 14:47 1


34 16 ug/Kg 06/03/16 07:23 06/06/16 14:47 1☼Aroclor-1221 ND

34 20 ug/Kg 06/03/16 07:23 06/06/16 14:47 1☼Aroclor-1232 ND

34 11 ug/Kg 06/03/16 07:23 06/06/16 14:47 1☼Aroclor-1242 ND

34 8.2 ug/Kg 06/03/16 07:23 06/06/16 14:47 1☼Aroclor-1248 ND

34 14 ug/Kg 06/03/16 07:23 06/06/16 14:47 1☼Aroclor-1254 ND

34 9.2 ug/Kg 06/03/16 07:23 06/06/16 14:47 1☼Aroclor-1260 ND




Method: 6020A - Metals (ICP/MS)RL MDL

Silver 4.0 B 0.19 0.0013 mg/Kg ☼ 06/02/16 11:09 06/03/16 21:58 2


9.4 0.58 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Aluminum 20000 B

0.94 0.024 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Arsenic 20 B

0.94 0.21 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Barium 660

0.19 0.010 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Beryllium 1.1 B

0.19 0.0035 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Cadmium 7.1 B

0.19 0.0016 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Cobalt 13 B

0.38 0.056 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Chromium 440 B

0.38 0.091 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Copper 350 B

190 30 mg/Kg 06/02/16 11:09 06/06/16 14:34 20☼Iron 62000 B

0.94 0.11 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Manganese 540 B

0.38 0.037 mg/Kg 06/02/16 11:09 06/06/16 14:30 2☼Nickel 80 B

0.19 0.042 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Lead 310 B

0.38 0.013 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Antimony 2.4

0.94 0.038 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Selenium 4.2 B

0.38 0.018 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Thallium 0.63

0.94 0.035 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Vanadium 60

3.8 0.47 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Zinc 870 B

190 21 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Calcium 57000 B

190 4.6 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Potassium 6300 B

190 3.8 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Magnesium 15000 B

190 8.2 mg/Kg 06/02/16 11:09 06/03/16 21:58 2☼Sodium 1300 B

Method: 7471A - Mercury (CVAA)RL MDL

Mercury ND 0.11 0.016 mg/Kg ☼ 06/02/16 15:00 06/03/16 07:44 1



Cr (VI) 20 B 0.79 0.15 mg/Kg ☼ 06/09/16 09:04 06/09/16 13:45 1


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12DCE BFB TOL DBFM

97 98 101 79240-65486-1


WESTERLY WWTC-ASH (WWWTC)

90 94 103 96LCS 240-233030/5 Lab Control Sample

91 93 101 96MB 240-233030/6 Method Blank

Surrogate Legend







12DCE BFB TOL DBFM

96 88 93 103LCS 240-233711/6


Lab Control Sample

Surrogate Legend





Method: 8260B - Volatile Organic Compounds (GC/MS)Prep Type: SPLPMatrix: Solid


12DCE BFB TOL DBFM

97 86 94 87240-65486-1



101 84 89 102LB 240-233606/1-A MB Method Blank

Surrogate Legend








60 44 31 61 47 78240-65486-1




92 77 59 7991 103MB 240-233013/17-A Method Blank

Surrogate Legend


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87 41 87 94 24 78LCS 240-233761/5-A


Lab Control Sample


74 39 68 2473 76MB 240-233761/4-A Method Blank

80 37 96 2284 82MB 240-234253/3-A Method Blank

Surrogate Legend







Method: 8270C - Semivolatile Organic Compounds (GC/MS)Prep Type: ASTM LeachMatrix: Solid



86 34 78 82 19 89240-65486-1



74 41 82 2480 65240-65486-1 - RE WESTERLY WWTC-ASH

(WWWTC)

Surrogate Legend









DCB1 DCB2 TCX1 TCX2

66 56 90 83LCS 240-233753/5-A


Lab Control Sample

48 48 90 85MB 240-233753/4-A Method Blank

Surrogate Legend



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DCB1 DCB2 TCX1 TCX2

87 80 87 77240-65486-1



84 90 93 88240-65486-1 MS WESTERLY WWTC-ASH

(WWWTC)81 81 84 76240-65486-1 MSD WESTERLY WWTC-ASH

(WWWTC)79 74 70 60LCS 240-233006/6-A Lab Control Sample

81 85 77 64MB 240-233006/5-A Method Blank

Surrogate Legend



Method: 8081B - Organochlorine Pesticides (GC)Prep Type: ASTM LeachMatrix: Solid


DCB1 DCB2 TCX1 TCX2

33 31 85 81240-65486-1



Surrogate Legend





TCX2 DCB2

76 75240-65486-1



66 80LCS 240-233005/13-A Lab Control Sample

64 79MB 240-233005/12-A Method Blank

Surrogate Legend





TCX2 DCB2

60 36LCS 240-233752/5-A


Lab Control Sample

59 33MB 240-233752/4-A Method Blank

Surrogate Legend



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Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas ChromatographyPrep Type: ASTM LeachMatrix: Solid


TCX2 DCB2

60 16240-65486-1



Surrogate Legend



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Method: 8260B - Volatile Organic Compounds (GC/MS)

Client Sample ID: Method BlankLab Sample ID: MB 240-233030/6Matrix: Solid Prep Type: Total/NAAnalysis Batch: 233030

RL MDL

Acetone 7.04 J 20 5.7 ug/Kg 06/03/16 11:24 1

MB MB


ND 0.905.0 ug/Kg 06/03/16 11:24 1Benzene

ND 0.295.0 ug/Kg 06/03/16 11:24 1Dichlorobromomethane

ND 0.245.0 ug/Kg 06/03/16 11:24 1Bromoform

ND 0.425.0 ug/Kg 06/03/16 11:24 1Bromomethane

1.22 J 1.120 ug/Kg 06/03/16 11:24 12-Butanone (MEK)

ND 0.595.0 ug/Kg 06/03/16 11:24 1Carbon disulfide

ND 0.655.0 ug/Kg 06/03/16 11:24 1Carbon tetrachloride

ND 0.535.0 ug/Kg 06/03/16 11:24 1Chlorobenzene

ND 0.445.0 ug/Kg 06/03/16 11:24 1Chloroethane

ND 0.365.0 ug/Kg 06/03/16 11:24 1Chloroform

ND 0.795.0 ug/Kg 06/03/16 11:24 1Chloromethane



ND 0.805.0 ug/Kg 06/03/16 11:24 11,1-Dichloroethene

ND 0.145.0 ug/Kg 06/03/16 11:24 11,2-Dichloropropane

ND 0.715.0 ug/Kg 06/03/16 11:24 1cis-1,3-Dichloropropene

ND 0.295.0 ug/Kg 06/03/16 11:24 1trans-1,3-Dichloropropene

ND 0.325.0 ug/Kg 06/03/16 11:24 1Ethylbenzene

ND 0.6820 ug/Kg 06/03/16 11:24 12-Hexanone

ND 0.745.0 ug/Kg 06/03/16 11:24 1Methylene Chloride

ND 1.220 ug/Kg 06/03/16 11:24 14-Methyl-2-pentanone (MIBK)

ND 0.405.0 ug/Kg 06/03/16 11:24 1Styrene

ND 0.315.0 ug/Kg 06/03/16 11:24 11,1,2,2-Tetrachloroethane

ND 0.805.0 ug/Kg 06/03/16 11:24 1Tetrachloroethene

ND 0.275.0 ug/Kg 06/03/16 11:24 1Toluene

ND 0.385.0 ug/Kg 06/03/16 11:24 1Trichloroethene

ND 0.305.0 ug/Kg 06/03/16 11:24 1Vinyl chloride

ND 0.5410 ug/Kg 06/03/16 11:24 1Xylenes, Total



ND 0.4810 ug/Kg 06/03/16 11:24 1Cyclohexane

ND 2.710 ug/Kg 06/03/16 11:24 11,2-Dibromo-3-Chloropropane

ND 0.535.0 ug/Kg 06/03/16 11:24 1Ethylene Dibromide

ND 0.285.0 ug/Kg 06/03/16 11:24 1Dichlorodifluoromethane

ND 0.285.0 ug/Kg 06/03/16 11:24 1cis-1,2-Dichloroethene

ND 0.325.0 ug/Kg 06/03/16 11:24 1trans-1,2-Dichloroethene

ND 0.205.0 ug/Kg 06/03/16 11:24 1Isopropylbenzene

ND 2.010 ug/Kg 06/03/16 11:24 1Methyl acetate

ND 0.435.0 ug/Kg 06/03/16 11:24 1Methyl tert-butyl ether

ND 0.425.0 ug/Kg 06/03/16 11:24 11,1,2-Trichloro-1,2,2-trifluoroethane

ND 0.385.0 ug/Kg 06/03/16 11:24 11,2,4-Trichlorobenzene




ND 0.295.0 ug/Kg 06/03/16 11:24 1Trichlorofluoromethane

ND 0.375.0 ug/Kg 06/03/16 11:24 1Chlorodibromomethane

ND 0.5810 ug/Kg 06/03/16 11:24 1Methylcyclohexane

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MB MB



101 06/03/16 11:24 1Toluene-d8 (Surr) 67 - 125



Acetone 100 107 ug/Kg 107 41 - 137

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Benzene 50.0 51.6 ug/Kg 103 79 - 120

Dichlorobromomethane 50.0 54.1 ug/Kg 108 80 - 122

Bromoform 50.0 53.3 ug/Kg 107 62 - 133

Bromomethane 20.0 14.1 ug/Kg 71 42 - 136

2-Butanone (MEK) 100 110 ug/Kg 110 52 - 131

Carbon disulfide 50.0 60.8 ug/Kg 122 62 - 146

Carbon tetrachloride 50.0 51.9 ug/Kg 104 71 - 129

Chlorobenzene 50.0 51.0 ug/Kg 102 78 - 120

Chloroethane 20.0 16.9 ug/Kg 85 58 - 120

Chloroform 50.0 51.3 ug/Kg 103 77 - 120

Chloromethane 20.0 14.8 ug/Kg 74 50 - 120



1,1-Dichloroethene 50.0 53.9 ug/Kg 108 75 - 135

1,2-Dichloropropane 50.0 52.1 ug/Kg 104 80 - 120

cis-1,3-Dichloropropene 50.0 55.8 ug/Kg 112 74 - 128

trans-1,3-Dichloropropene 50.0 50.6 ug/Kg 101 73 - 131

Ethylbenzene 50.0 52.7 ug/Kg 105 79 - 120

2-Hexanone 100 118 ug/Kg 118 64 - 136

Methylene Chloride 50.0 49.5 ug/Kg 99 75 - 120

4-Methyl-2-pentanone (MIBK) 100 123 ug/Kg 123 67 - 135

Styrene 50.0 54.1 ug/Kg 108 80 - 120

1,1,2,2-Tetrachloroethane 50.0 56.1 ug/Kg 112 77 - 123

Tetrachloroethene 50.0 53.0 ug/Kg 106 79 - 120

Toluene 50.0 50.9 ug/Kg 102 75 - 120

Trichloroethene 50.0 54.9 ug/Kg 110 79 - 120

Vinyl chloride 20.0 14.5 ug/Kg 73 57 - 120

Xylenes, Total 100 106 ug/Kg 106 80 - 120



Cyclohexane 50.0 52.1 ug/Kg 104 66 - 120

1,2-Dibromo-3-Chloropropane 50.0 57.9 ug/Kg 116 61 - 132

Ethylene Dibromide 50.0 57.6 ug/Kg 115 80 - 120

Dichlorodifluoromethane 20.0 9.78 ug/Kg 49 26 - 120

cis-1,2-Dichloroethene 50.0 52.2 ug/Kg 104 76 - 120

trans-1,2-Dichloroethene 50.0 55.2 ug/Kg 110 78 - 120

Isopropylbenzene 50.0 56.0 ug/Kg 112 76 - 122

Methyl acetate 250 300 ug/Kg 120 57 - 130

Methyl tert-butyl ether 50.0 50.5 ug/Kg 101 49 - 165


ne

50.0 52.7 ug/Kg 105 80 - 138

1,2,4-Trichlorobenzene 50.0 49.4 ug/Kg 99 64 - 124


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Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Trichlorofluoromethane 20.0 17.2 ug/Kg 86 57 - 146

Methylcyclohexane 50.0 51.2 ug/Kg 102 70 - 126

m-Xylene & p-Xylene 50.0 52.9 ug/Kg 106 80 - 120

o-Xylene 50.0 52.7 ug/Kg 105 80 - 120


Surrogate

90

LCS LCS






Acetone 40.0 35.6 ug/L 89 34 - 148

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Benzene 20.0 22.6 ug/L 113 80 - 120

Dichlorobromomethane 20.0 21.9 ug/L 109 80 - 120

Bromoform 20.0 24.3 ug/L 122 56 - 122

Bromomethane 20.0 23.5 ug/L 118 38 - 132

2-Butanone (MEK) 40.0 43.2 ug/L 108 56 - 138

Carbon disulfide 20.0 26.5 ug/L 132 65 - 144

Carbon tetrachloride 20.0 23.6 ug/L 118 77 - 131

Chlorobenzene 20.0 21.2 ug/L 106 80 - 120

Chloroethane 20.0 24.0 ug/L 120 36 - 126

Chloroform 20.0 23.0 ug/L 115 80 - 120

Chloromethane 20.0 23.8 ug/L 119 48 - 133



1,1-Dichloroethene 20.0 24.8 ug/L 124 76 - 124

1,2-Dichloropropane 20.0 22.3 ug/L 111 78 - 124

cis-1,3-Dichloropropene 20.0 23.4 ug/L 117 74 - 126

trans-1,3-Dichloropropene 20.0 18.4 ug/L 92 75 - 131

Ethylbenzene 20.0 19.9 ug/L 99 80 - 120

2-Hexanone 40.0 42.8 ug/L 107 55 - 141

Methylene Chloride 20.0 22.2 ug/L 111 77 - 129

4-Methyl-2-pentanone (MIBK) 40.0 44.2 ug/L 111 64 - 135

Styrene 20.0 20.6 ug/L 103 76 - 122

1,1,2,2-Tetrachloroethane 20.0 19.7 ug/L 99 71 - 123

Tetrachloroethene 20.0 20.9 ug/L 104 78 - 121

Toluene 20.0 22.4 ug/L 112 80 - 120

Trichloroethene 20.0 24.1 ug/L 121 80 - 121

Vinyl chloride 20.0 23.6 ug/L 118 52 - 121

Xylenes, Total 40.0 42.0 ug/L 105 80 - 120

1,1,1-Trichloroethane 20.0 25.6 * ug/L 128 77 - 123

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1,1,2-Trichloroethane 20.0 21.9 ug/L 110 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Cyclohexane 20.0 21.0 ug/L 105 60 - 140

1,2-Dibromo-3-Chloropropane 20.0 22.6 ug/L 113 50 - 132

Ethylene Dibromide 20.0 22.2 ug/L 111 80 - 120

Dichlorodifluoromethane 20.0 23.1 ug/L 115 23 - 136

cis-1,2-Dichloroethene 20.0 22.1 ug/L 111 79 - 120

trans-1,2-Dichloroethene 20.0 22.8 ug/L 114 80 - 124

Isopropylbenzene 20.0 20.3 ug/L 102 77 - 120

Methyl acetate 100 113 ug/L 113 67 - 131

Methyl tert-butyl ether 20.0 23.0 ug/L 115 69 - 121


ne

20.0 23.4 ug/L 117 67 - 138

1,2,4-Trichlorobenzene 20.0 20.1 ug/L 100 61 - 120




Trichlorofluoromethane 20.0 21.8 ug/L 109 61 - 133

Methylcyclohexane 20.0 19.9 ug/L 100 61 - 134

m-Xylene & p-Xylene 20.0 21.4 ug/L 107 80 - 120

o-Xylene 20.0 20.6 ug/L 103 80 - 120


Surrogate

96

LCS LCS






RL MDL

Acetone 1.76 J 10 0.94 ug/L 06/08/16 20:01 1

MB MB


ND 0.351.0 ug/L 06/08/16 20:01 1Benzene

ND 0.291.0 ug/L 06/08/16 20:01 1Dichlorobromomethane

ND 0.561.0 ug/L 06/08/16 20:01 1Bromoform

ND 0.441.0 ug/L 06/08/16 20:01 1Bromomethane

ND 0.5310 ug/L 06/08/16 20:01 12-Butanone (MEK)

ND 0.381.0 ug/L 06/08/16 20:01 1Carbon disulfide

ND 0.431.0 ug/L 06/08/16 20:01 1Carbon tetrachloride

ND 0.251.0 ug/L 06/08/16 20:01 1Chlorobenzene

ND 0.321.0 ug/L 06/08/16 20:01 1Chloroethane

1.24 0.251.0 ug/L 06/08/16 20:01 1Chloroform

ND 0.441.0 ug/L 06/08/16 20:01 1Chloromethane



ND 0.451.0 ug/L 06/08/16 20:01 11,1-Dichloroethene

ND 0.251.0 ug/L 06/08/16 20:01 11,2-Dichloropropane

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RL MDL

cis-1,3-Dichloropropene ND 1.0 0.46 ug/L 06/08/16 20:01 1

MB MB


ND 0.561.0 ug/L 06/08/16 20:01 1trans-1,3-Dichloropropene

ND 0.251.0 ug/L 06/08/16 20:01 1Ethylbenzene

ND 0.4810 ug/L 06/08/16 20:01 12-Hexanone

2.74 0.331.0 ug/L 06/08/16 20:01 1Methylene Chloride

ND 0.9910 ug/L 06/08/16 20:01 14-Methyl-2-pentanone (MIBK)

ND 0.451.0 ug/L 06/08/16 20:01 1Styrene

ND 0.221.0 ug/L 06/08/16 20:01 11,1,2,2-Tetrachloroethane

ND 0.311.0 ug/L 06/08/16 20:01 1Tetrachloroethene

ND 0.231.0 ug/L 06/08/16 20:01 1Toluene

ND 0.221.0 ug/L 06/08/16 20:01 1Trichloroethene

ND 0.291.0 ug/L 06/08/16 20:01 1Vinyl chloride

ND 0.522.0 ug/L 06/08/16 20:01 1Xylenes, Total



ND 0.451.0 ug/L 06/08/16 20:01 1Cyclohexane

ND 0.822.0 ug/L 06/08/16 20:01 11,2-Dibromo-3-Chloropropane

ND 0.321.0 ug/L 06/08/16 20:01 1Ethylene Dibromide

ND 0.321.0 ug/L 06/08/16 20:01 1Dichlorodifluoromethane

ND 0.261.0 ug/L 06/08/16 20:01 1cis-1,2-Dichloroethene

ND 0.301.0 ug/L 06/08/16 20:01 1trans-1,2-Dichloroethene

ND 0.351.0 ug/L 06/08/16 20:01 1Isopropylbenzene

ND 2.310 ug/L 06/08/16 20:01 1Methyl acetate

ND 0.201.0 ug/L 06/08/16 20:01 1Methyl tert-butyl ether

ND 0.451.0 ug/L 06/08/16 20:01 11,1,2-Trichloro-1,2,2-trifluoroethane

ND 0.321.0 ug/L 06/08/16 20:01 11,2,4-Trichlorobenzene




ND 0.491.0 ug/L 06/08/16 20:01 1Trichlorofluoromethane

ND 0.431.0 ug/L 06/08/16 20:01 1Chlorodibromomethane

ND 0.431.0 ug/L 06/08/16 20:01 1Methylcyclohexane


MB MB



89 06/08/16 20:01 1Toluene-d8 (Surr) 80 - 120


Method: 8270C - Semivolatile Organic Compounds (GC/MS)


RL MDL

2-Chloronaphthalene ND 50 0.45 ug/Kg 06/03/16 08:23 06/07/16 10:25 1

MB MB


ND 8.250 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Chlorophenol

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RL MDL

4-Bromophenyl phenyl ether ND 50 13 ug/Kg 06/03/16 08:23 06/07/16 10:25 1

MB MB


ND 21150 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Chloro-3-methylphenol

ND 0.506.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Methylnaphthalene

ND 17150 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Chloroaniline

ND 1350 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Chlorophenyl phenyl ether

ND 18100 ug/Kg 06/03/16 08:23 06/07/16 10:25 13,3'-Dichlorobenzidine

ND 0.766.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Acenaphthene

ND 20150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4-Dichlorophenol

ND 0.356.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Acenaphthylene

ND 9.2100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Acetophenone

ND 20150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4-Dimethylphenol

ND 0.786.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Anthracene

ND 9.1200 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Atrazine

ND 9.2150 ug/Kg 06/03/16 08:23 06/07/16 10:25 14,6-Dinitro-2-methylphenol

ND 0.636.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[a]anthracene

ND 21330 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4-Dinitrophenol

ND 0.646.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[a]pyrene


ND 0.596.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[b]fluoranthene

ND 0.356.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[g,h,i]perylene

ND 0.686.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Benzo[k]fluoranthene

ND 22100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Bis(2-chloroethoxy)methane

ND 2.0100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Bis(2-chloroethyl)ether

ND 1970 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Bis(2-ethylhexyl) phthalate

ND 1070 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Butyl benzyl phthalate

ND 1.16.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Chrysene

ND 0.666.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Dibenz(a,h)anthracene

ND 0.6650 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Dibenzofuran

ND 1670 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Diethyl phthalate

ND 11200 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Methylphenol

ND 1770 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Dimethyl phthalate

27.9 J 1570 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Di-n-butyl phthalate

ND 9.1200 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Nitroaniline

ND 7.970 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Di-n-octyl phthalate


ND 0.556.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Fluoranthene


ND 0.536.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Fluorene

ND 2.16.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachlorobenzene

ND 8.350 ug/Kg 06/03/16 08:23 06/07/16 10:25 12-Nitrophenol

ND 5.650 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachlorobutadiene

ND 17330 ug/Kg 06/03/16 08:23 06/07/16 10:25 14-Nitrophenol

ND 8.1330 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachlorocyclopentadiene

ND 9.050 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Hexachloroethane

ND 0.356.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Indeno[1,2,3-cd]pyrene

ND 9.5100 ug/Kg 06/03/16 08:23 06/07/16 10:25 1bis (2-chloroisopropyl) ether

ND 1350 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Isophorone

ND 0.826.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Naphthalene

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RL MDL

Nitrobenzene ND 100 2.2 ug/Kg 06/03/16 08:23 06/07/16 10:25 1

MB MB


ND 6.350 ug/Kg 06/03/16 08:23 06/07/16 10:25 1N-Nitrosodi-n-propylamine

ND 2150 ug/Kg 06/03/16 08:23 06/07/16 10:25 1N-Nitrosodiphenylamine

ND 25150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4,5-Trichlorophenol

ND 9.1150 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Pentachlorophenol

ND 8.9150 ug/Kg 06/03/16 08:23 06/07/16 10:25 12,4,6-Trichlorophenol

ND 7.350 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Phenol

ND 0.736.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Phenanthrene

ND 0.446.7 ug/Kg 06/03/16 08:23 06/07/16 10:25 1Pyrene

ND 20400 ug/Kg 06/03/16 08:23 06/07/16 10:25 13 & 4 Methylphenol



MB MB

Surrogate

06/03/16 08:23





79 06/03/16 08:23 06/07/16 10:25 1Phenol-d5 (Surr) 32 - 120

103 06/03/16 08:23 06/07/16 10:25 1Terphenyl-d14 (Surr) 47 - 120


2-Chloronaphthalene 667 612 ug/Kg 92 54 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

2-Chlorophenol 667 624 ug/Kg 94 50 - 120

4-Bromophenyl phenyl ether 667 770 ug/Kg 116 48 - 120

4-Chloro-3-methylphenol 667 523 ug/Kg 78 52 - 120

2-Methylnaphthalene 667 644 ug/Kg 97 53 - 120

4-Chloroaniline 667 387 ug/Kg 58 41 - 120

4-Chlorophenyl phenyl ether 667 712 ug/Kg 107 56 - 120

3,3'-Dichlorobenzidine 1330 1000 ug/Kg 75 39 - 120

Acenaphthene 667 602 ug/Kg 90 55 - 120

2,4-Dichlorophenol 667 612 ug/Kg 92 51 - 120

Acenaphthylene 667 632 ug/Kg 95 54 - 120

Acetophenone 667 589 ug/Kg 88 49 - 120

2,4-Dimethylphenol 667 448 ug/Kg 67 34 - 120

Anthracene 667 620 ug/Kg 93 59 - 120

Atrazine 1330 1460 ug/Kg 110 56 - 120

4,6-Dinitro-2-methylphenol 1330 849 ug/Kg 64 23 - 120

Benzo[a]anthracene 667 648 ug/Kg 97 60 - 120

2,4-Dinitrophenol 1330 503 ug/Kg 38 10 - 120

Benzo[a]pyrene 667 745 ug/Kg 112 61 - 120


Benzo[b]fluoranthene 667 736 ug/Kg 110 60 - 120

Benzo[g,h,i]perylene 667 686 ug/Kg 103 60 - 120

Benzo[k]fluoranthene 667 759 ug/Kg 114 61 - 120

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Bis(2-chloroethoxy)methane 667 569 ug/Kg 85 53 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Bis(2-chloroethyl)ether 667 548 ug/Kg 82 45 - 120

Bis(2-ethylhexyl) phthalate 667 665 ug/Kg 100 57 - 120

Butyl benzyl phthalate 667 653 ug/Kg 98 58 - 120

Chrysene 667 637 ug/Kg 96 62 - 120

Dibenz(a,h)anthracene 667 736 ug/Kg 110 59 - 120

Dibenzofuran 667 658 ug/Kg 99 57 - 120

Diethyl phthalate 667 665 ug/Kg 100 58 - 120

2-Methylphenol 667 617 ug/Kg 93 48 - 120

Dimethyl phthalate 667 708 ug/Kg 106 59 - 120

Di-n-butyl phthalate 667 669 ug/Kg 100 54 - 120


Di-n-octyl phthalate 667 703 ug/Kg 105 54 - 120


Fluoranthene 667 624 ug/Kg 94 57 - 120


Fluorene 667 674 ug/Kg 101 56 - 120

Hexachlorobenzene 667 770 ug/Kg 115 43 - 120


Hexachlorobutadiene 667 597 ug/Kg 90 48 - 120


Hexachlorocyclopentadiene 667 352 ug/Kg 53 23 - 120

Hexachloroethane 667 576 ug/Kg 86 46 - 120

Indeno[1,2,3-cd]pyrene 667 710 ug/Kg 106 62 - 120

bis (2-chloroisopropyl) ether 667 556 ug/Kg 83 34 - 120

Isophorone 667 552 ug/Kg 83 54 - 120

Naphthalene 667 601 ug/Kg 90 53 - 120

Nitrobenzene 667 554 ug/Kg 83 50 - 120

N-Nitrosodi-n-propylamine 667 595 ug/Kg 89 49 - 120

N-Nitrosodiphenylamine 667 812 * ug/Kg 122 52 - 120


Pentachlorophenol 1330 676 ug/Kg 51 23 - 120


Phenol 667 567 ug/Kg 85 49 - 120

Phenanthrene 667 619 ug/Kg 93 58 - 120

Pyrene 667 639 ug/Kg 96 57 - 120

3 & 4 Methylphenol 667 594 ug/Kg 89 49 - 120



Surrogate

94

LCS LCS







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RL MDL

Benzaldehyde ND 1.0 0.39 ug/L 06/09/16 07:34 06/10/16 09:52 1

MB MB


ND 0.131.0 ug/L 06/09/16 07:34 06/10/16 09:52 11,1'-Biphenyl

0.977 J 0.205.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Caprolactam

ND 0.281.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Carbazole

ND 0.101.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Chloronaphthalene

ND 0.291.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Chlorophenol

ND 0.222.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Bromophenyl phenyl ether

ND 0.212.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Chloro-3-methylphenol

ND 0.0900.20 ug/L 06/09/16 07:34 06/10/16 09:52 12-Methylnaphthalene

ND 0.212.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Chloroaniline

ND 0.302.0 ug/L 06/09/16 07:34 06/10/16 09:52 14-Chlorophenyl phenyl ether

ND 0.375.0 ug/L 06/09/16 07:34 06/10/16 09:52 13,3'-Dichlorobenzidine

ND 0.0440.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Acenaphthene

ND 0.192.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4-Dichlorophenol

ND 0.0480.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Acenaphthylene

ND 0.341.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Acetophenone

ND 0.252.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4-Dimethylphenol

ND 0.0880.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Anthracene

ND 0.341.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Atrazine

ND 2.45.0 ug/L 06/09/16 07:34 06/10/16 09:52 14,6-Dinitro-2-methylphenol

ND 0.0300.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[a]anthracene

ND 0.325.0 ug/L 06/09/16 07:34 06/10/16 09:52 12,4-Dinitrophenol

ND 0.0510.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[a]pyrene


ND 0.0390.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[b]fluoranthene

ND 0.0460.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[g,h,i]perylene

ND 0.0450.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Benzo[k]fluoranthene

ND 0.321.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Bis(2-chloroethoxy)methane

ND 0.101.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Bis(2-chloroethyl)ether

ND 1.75.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Bis(2-ethylhexyl) phthalate

ND 0.262.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Butyl benzyl phthalate

ND 0.0500.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Chrysene

ND 0.0450.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Dibenz(a,h)anthracene

ND 0.0201.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Dibenzofuran

ND 0.602.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Diethyl phthalate

ND 0.171.0 ug/L 06/09/16 07:34 06/10/16 09:52 12-Methylphenol

ND 0.292.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Dimethyl phthalate

ND 1.75.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Di-n-butyl phthalate


ND 0.232.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Di-n-octyl phthalate


ND 0.0450.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Fluoranthene


ND 0.0410.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Fluorene

ND 0.0850.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Hexachlorobenzene


ND 0.271.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Hexachlorobutadiene


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RL MDL

Hexachlorocyclopentadiene ND 10 0.24 ug/L 06/09/16 07:34 06/10/16 09:52 1

MB MB


ND 0.191.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Hexachloroethane

ND 0.0430.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Indeno[1,2,3-cd]pyrene

ND 0.401.0 ug/L 06/09/16 07:34 06/10/16 09:52 1bis (2-chloroisopropyl) ether

ND 0.271.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Isophorone

ND 0.0630.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Naphthalene

ND 0.0401.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Nitrobenzene

ND 0.241.0 ug/L 06/09/16 07:34 06/10/16 09:52 1N-Nitrosodi-n-propylamine

ND 0.311.0 ug/L 06/09/16 07:34 06/10/16 09:52 1N-Nitrosodiphenylamine


ND 0.275.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Pentachlorophenol


ND 0.601.0 ug/L 06/09/16 07:34 06/10/16 09:52 1Phenol

ND 0.0620.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Phenanthrene

ND 0.0420.20 ug/L 06/09/16 07:34 06/10/16 09:52 1Pyrene

ND 0.802.0 ug/L 06/09/16 07:34 06/10/16 09:52 13 & 4 Methylphenol



MB MB

Surrogate

06/09/16 07:34





24 06/09/16 07:34 06/10/16 09:52 1Phenol-d5 (Surr) 10 - 120

76 06/09/16 07:34 06/10/16 09:52 1Terphenyl-d14 (Surr) 17 - 120


Benzaldehyde 40.0 37.0 ug/L 93 60 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

1,1'-Biphenyl 20.0 17.6 ug/L 88 58 - 120


Carbazole 20.0 20.0 ug/L 100 60 - 126

2-Chloronaphthalene 20.0 17.9 ug/L 89 56 - 120

2-Chlorophenol 20.0 15.9 ug/L 79 57 - 120

4-Bromophenyl phenyl ether 20.0 19.3 ug/L 97 52 - 128

4-Chloro-3-methylphenol 20.0 17.7 ug/L 89 59 - 120

2-Methylnaphthalene 20.0 18.0 ug/L 90 58 - 120

4-Chloroaniline 20.0 4.65 ug/L 23 10 - 120

4-Chlorophenyl phenyl ether 20.0 18.1 ug/L 91 58 - 120

3,3'-Dichlorobenzidine 40.0 31.8 ug/L 80 10 - 134

Acenaphthene 20.0 17.9 ug/L 89 57 - 120

2,4-Dichlorophenol 20.0 18.3 ug/L 92 57 - 120

Acenaphthylene 20.0 18.7 ug/L 94 55 - 120

Acetophenone 20.0 18.1 ug/L 90 60 - 120

2,4-Dimethylphenol 20.0 17.6 ug/L 88 55 - 120

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Anthracene 20.0 19.9 ug/L 99 58 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Atrazine 40.0 39.5 ug/L 99 61 - 132

4,6-Dinitro-2-methylphenol 40.0 35.5 ug/L 89 35 - 140

Benzo[a]anthracene 20.0 17.1 ug/L 86 59 - 120

2,4-Dinitrophenol 40.0 30.0 ug/L 75 18 - 127

Benzo[a]pyrene 20.0 16.6 ug/L 83 60 - 120


Benzo[b]fluoranthene 20.0 17.0 ug/L 85 62 - 120

Benzo[g,h,i]perylene 20.0 17.7 ug/L 88 59 - 120

Benzo[k]fluoranthene 20.0 18.1 ug/L 90 57 - 120

Bis(2-chloroethoxy)methane 20.0 18.7 ug/L 94 61 - 120

Bis(2-chloroethyl)ether 20.0 17.6 ug/L 88 55 - 120

Bis(2-ethylhexyl) phthalate 20.0 14.4 ug/L 72 62 - 123

Butyl benzyl phthalate 20.0 16.7 ug/L 83 61 - 120

Chrysene 20.0 16.9 ug/L 84 61 - 120

Dibenz(a,h)anthracene 20.0 14.8 ug/L 74 61 - 120

Dibenzofuran 20.0 18.1 ug/L 91 58 - 120

Diethyl phthalate 20.0 19.0 ug/L 95 62 - 120

2-Methylphenol 20.0 13.1 ug/L 65 52 - 120

Dimethyl phthalate 20.0 19.2 ug/L 96 62 - 120

Di-n-butyl phthalate 20.0 19.9 ug/L 99 59 - 128


Di-n-octyl phthalate 20.0 13.7 ug/L 68 58 - 120


Fluoranthene 20.0 19.5 ug/L 97 57 - 123


Fluorene 20.0 18.9 ug/L 94 56 - 120

Hexachlorobenzene 20.0 18.5 ug/L 92 47 - 127

2-Nitrophenol 20.0 17.2 ug/L 86 62 - 120

Hexachlorobutadiene 20.0 17.0 ug/L 85 50 - 120

4-Nitrophenol 40.0 12.1 ug/L 30 16 - 120

Hexachlorocyclopentadiene 20.0 16.3 ug/L 82 25 - 120

Hexachloroethane 20.0 16.6 ug/L 83 50 - 120

Indeno[1,2,3-cd]pyrene 20.0 15.4 ug/L 77 61 - 120

bis (2-chloroisopropyl) ether 20.0 18.0 ug/L 90 46 - 120

Isophorone 20.0 18.9 ug/L 95 61 - 120

Naphthalene 20.0 17.4 ug/L 87 54 - 120

Nitrobenzene 20.0 18.8 ug/L 94 58 - 120

N-Nitrosodi-n-propylamine 20.0 18.3 ug/L 91 60 - 120

N-Nitrosodiphenylamine 20.0 19.2 ug/L 96 54 - 122


Pentachlorophenol 40.0 37.2 ug/L 93 35 - 121


Phenol 20.0 5.06 ug/L 25 16 - 120

Phenanthrene 20.0 18.5 ug/L 93 58 - 120

Pyrene 20.0 19.3 ug/L 97 60 - 120

3 & 4 Methylphenol 20.0 11.7 ug/L 58 46 - 120


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Surrogate

87

LCS LCS








RL MDL

Caprolactam ND 5.0 0.20 ug/L 06/13/16 11:40 06/14/16 08:11 1

MB MB



MB MB

Surrogate

06/13/16 11:40





22 06/13/16 11:40 06/14/16 08:11 1Phenol-d5 (Surr) 10 - 120

82 06/13/16 11:40 06/14/16 08:11 1Terphenyl-d14 (Surr) 17 - 120



Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

72

LCS LCS







Method: 8081B - Organochlorine Pesticides (GC)


RL MDL

4,4'-DDD ND 1.7 0.20 ug/Kg 06/03/16 07:28 06/10/16 17:39 1

MB MB


ND 0.271.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 14,4'-DDE

ND 0.311.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 14,4'-DDT

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RL MDL

Aldrin ND 1.7 0.20 ug/Kg 06/03/16 07:28 06/10/16 17:39 1

MB MB


ND 0.601.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1alpha-BHC

ND 0.251.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1alpha-Chlordane

ND 0.361.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1beta-BHC

ND 0.221.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1delta-BHC

ND 0.161.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Dieldrin

ND 0.251.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endosulfan I

ND 0.381.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endosulfan II

ND 0.341.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endosulfan sulfate

ND 0.211.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endrin

ND 0.321.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endrin aldehyde

ND 0.421.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Endrin ketone

ND 0.461.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1gamma-BHC (Lindane)

ND 0.861.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1gamma-Chlordane

ND 0.701.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Heptachlor

ND 0.401.7 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Heptachlor epoxide

ND 9.867 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Toxaphene

ND 0.543.3 ug/Kg 06/03/16 07:28 06/10/16 17:39 1Methoxychlor


MB MB

Surrogate

06/03/16 07:28






4,4'-DDD 33.3 26.5 ug/Kg 80 47 - 157

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

4,4'-DDE 33.3 26.2 ug/Kg 79 56 - 125

4,4'-DDT 33.3 26.3 ug/Kg 79 57 - 142

Aldrin 33.3 23.5 ug/Kg 70 37 - 129

alpha-BHC 33.3 25.6 ug/Kg 77 50 - 125

alpha-Chlordane 33.3 24.8 ug/Kg 74 53 - 120

beta-BHC 33.3 24.7 ug/Kg 74 41 - 125

delta-BHC 33.3 21.6 ug/Kg 65 52 - 124

Dieldrin 33.3 25.9 ug/Kg 78 55 - 124

Endosulfan I 33.3 17.6 ug/Kg 53 18 - 120

Endosulfan II 33.3 20.8 ug/Kg 62 19 - 120

Endosulfan sulfate 33.3 24.6 ug/Kg 74 54 - 128

Endrin 33.3 27.5 ug/Kg 83 53 - 151

Endrin aldehyde 33.3 22.7 ug/Kg 68 44 - 130

Endrin ketone 33.3 24.3 ug/Kg 73 49 - 120

gamma-BHC (Lindane) 33.3 25.4 ug/Kg 76 50 - 123

gamma-Chlordane 33.3 25.2 ug/Kg 76 53 - 120

Heptachlor 33.3 27.0 ug/Kg 81 48 - 129

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Heptachlor epoxide 33.3 25.4 ug/Kg 76 54 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Methoxychlor 33.3 25.7 ug/Kg 77 52 - 147


Surrogate

79

LCS LCS





Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Lab Sample ID: 240-65486-1 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233996 Prep Batch: 233006

4,4'-DDD ND 33.8 29.5 ug/Kg 87 17 - 160☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

4,4'-DDE ND 33.8 29.5 ug/Kg 87 26 - 136☼

4,4'-DDT ND 33.8 29.5 ug/Kg 88 22 - 151☼

Aldrin ND 33.8 26.6 ug/Kg 79 22 - 128☼

alpha-BHC ND 33.8 30.0 ug/Kg 89 21 - 141☼

alpha-Chlordane ND 33.8 27.9 ug/Kg 83 22 - 124☼

beta-BHC ND 33.8 29.9 ug/Kg 89 14 - 139☼

delta-BHC ND 33.8 24.5 ug/Kg 73 22 - 130☼

Dieldrin ND 33.8 29.2 ug/Kg 86 25 - 133☼

Endosulfan I ND 33.8 19.5 ug/Kg 58 10 - 120☼

Endosulfan II ND 33.8 23.2 ug/Kg 69 13 - 120☼

Endosulfan sulfate ND 33.8 27.6 ug/Kg 82 24 - 131☼

Endrin ND 33.8 31.3 ug/Kg 93 27 - 158☼

Endrin aldehyde ND 33.8 23.0 ug/Kg 68 22 - 119☼

Endrin ketone ND 33.8 27.1 ug/Kg 80 21 - 120☼

gamma-BHC (Lindane) ND 33.8 32.5 ug/Kg 96 21 - 134☼

gamma-Chlordane ND 33.8 28.7 ug/Kg 85 28 - 130☼

Heptachlor ND 33.8 31.1 ug/Kg 92 26 - 133☼

Heptachlor epoxide ND 33.8 28.8 ug/Kg 85 27 - 127☼

Methoxychlor ND 33.8 28.7 ug/Kg 85 24 - 150☼


Surrogate

84

MS MS





Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Lab Sample ID: 240-65486-1 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233996 Prep Batch: 233006

4,4'-DDD ND 33.5 27.2 ug/Kg 81 17 - 160 8 40☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

4,4'-DDE ND 33.5 26.8 ug/Kg 80 26 - 136 10 40☼

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Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Lab Sample ID: 240-65486-1 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233996 Prep Batch: 233006

4,4'-DDT ND 33.5 26.6 ug/Kg 79 22 - 151 11 40☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Aldrin ND 33.5 24.0 ug/Kg 72 22 - 128 11 40☼

alpha-BHC ND 33.5 26.7 ug/Kg 80 21 - 141 11 40☼

alpha-Chlordane ND 33.5 25.5 ug/Kg 76 22 - 124 9 40☼

beta-BHC ND 33.5 27.5 ug/Kg 82 14 - 139 8 40☼

delta-BHC ND 33.5 23.0 ug/Kg 69 22 - 130 7 40☼

Dieldrin ND 33.5 26.7 ug/Kg 80 25 - 133 9 40☼

Endosulfan I ND 33.5 18.2 ug/Kg 54 10 - 120 7 40☼

Endosulfan II ND 33.5 21.3 ug/Kg 64 13 - 120 8 40☼

Endosulfan sulfate ND 33.5 25.1 ug/Kg 75 24 - 131 9 40☼

Endrin ND 33.5 28.6 ug/Kg 85 27 - 158 9 40☼

Endrin aldehyde ND 33.5 21.4 ug/Kg 64 22 - 119 7 40☼

Endrin ketone ND 33.5 25.0 ug/Kg 75 21 - 120 8 40☼

gamma-BHC (Lindane) ND 33.5 28.4 ug/Kg 85 21 - 134 13 40☼

gamma-Chlordane ND 33.5 26.0 ug/Kg 78 28 - 130 10 40☼

Heptachlor ND 33.5 27.4 ug/Kg 82 26 - 133 13 40☼

Heptachlor epoxide ND 33.5 26.1 ug/Kg 78 27 - 127 10 40☼

Methoxychlor ND 33.5 26.0 ug/Kg 78 24 - 150 10 40☼


Surrogate

81

MSD MSD






RL MDL

4,4'-DDD ND 0.050 0.018 ug/L 06/09/16 06:31 06/13/16 13:51 1

MB MB


ND 0.0120.050 ug/L 06/09/16 06:31 06/13/16 13:51 14,4'-DDE

ND 0.0170.050 ug/L 06/09/16 06:31 06/13/16 13:51 14,4'-DDT

ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Aldrin

ND 0.0140.050 ug/L 06/09/16 06:31 06/13/16 13:51 1alpha-BHC

ND 0.0120.050 ug/L 06/09/16 06:31 06/13/16 13:51 1alpha-Chlordane

ND 0.0180.050 ug/L 06/09/16 06:31 06/13/16 13:51 1beta-BHC

ND 0.0290.050 ug/L 06/09/16 06:31 06/13/16 13:51 1delta-BHC

ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Dieldrin

ND 0.0160.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endosulfan I

ND 0.0150.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endosulfan II

ND 0.0150.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endosulfan sulfate

ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endrin

ND 0.0180.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endrin aldehyde

ND 0.0160.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Endrin ketone

ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1gamma-BHC (Lindane)

ND 0.0130.050 ug/L 06/09/16 06:31 06/13/16 13:51 1gamma-Chlordane

ND 0.0140.050 ug/L 06/09/16 06:31 06/13/16 13:51 1Heptachlor

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RL MDL

Heptachlor epoxide ND 0.050 0.015 ug/L 06/09/16 06:31 06/13/16 13:51 1

MB MB


ND 0.202.0 ug/L 06/09/16 06:31 06/13/16 13:51 1Toxaphene

ND 0.0130.10 ug/L 06/09/16 06:31 06/13/16 13:51 1Methoxychlor


MB MB

Surrogate

06/09/16 06:31






4,4'-DDD 0.500 0.492 ug/L 98 54 - 163

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

4,4'-DDE 0.500 0.472 ug/L 94 60 - 146

4,4'-DDT 0.500 0.489 ug/L 98 56 - 160

Aldrin 0.500 0.439 ug/L 88 44 - 145

alpha-BHC 0.500 0.461 ug/L 92 53 - 148

alpha-Chlordane 0.500 0.475 ug/L 95 55 - 141

beta-BHC 0.500 0.469 ug/L 94 55 - 139

delta-BHC 0.500 0.409 ug/L 82 60 - 145

Dieldrin 0.500 0.485 ug/L 97 57 - 145

Endosulfan I 0.500 0.428 ug/L 86 26 - 120

Endosulfan II 0.500 0.460 ug/L 92 25 - 123

Endosulfan sulfate 0.500 0.471 ug/L 94 60 - 137

Endrin 0.500 0.462 ug/L 92 66 - 142

Endrin aldehyde 0.500 0.462 ug/L 92 59 - 120

Endrin ketone 0.500 0.481 ug/L 96 64 - 120

gamma-BHC (Lindane) 0.500 0.459 ug/L 92 53 - 144

gamma-Chlordane 0.500 0.483 ug/L 97 57 - 140

Heptachlor 0.500 0.441 ug/L 88 56 - 123

Heptachlor epoxide 0.500 0.477 ug/L 95 44 - 151

Methoxychlor 0.500 0.465 ug/L 93 56 - 153


Surrogate

66

LCS LCS





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Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography


RL MDL

Aroclor-1016 ND 33 12 ug/Kg 06/03/16 07:23 06/06/16 15:06 1

MB MB


ND 1633 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1221

ND 2033 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1232

ND 1133 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1242

ND 8.033 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1248

ND 1433 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1254

ND 9.033 ug/Kg 06/03/16 07:23 06/06/16 15:06 1Aroclor-1260


MB MB

Surrogate

06/03/16 07:23




Aroclor-1016 333 246 ug/Kg 74 47 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Aroclor-1260 333 277 ug/Kg 83 46 - 120


Surrogate

66

LCS LCS




RL MDL

Aroclor-1016 ND 0.10 0.050 ug/L 06/09/16 06:29 06/13/16 10:16 1

MB MB


ND 0.0900.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1221

ND 0.0700.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1232

ND 0.0600.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1242

ND 0.0500.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1248

ND 0.0300.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1254

ND 0.0400.10 ug/L 06/09/16 06:29 06/13/16 10:16 1Aroclor-1260


MB MB

Surrogate

06/09/16 06:29




Aroclor-1016 2.50 1.60 ug/L 64 32 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

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Method: 8082A - Polychlorinated Biphenyls (PCBs) by Gas Chromatography (Continued)


Aroclor-1260 2.50 1.52 ug/L 61 36 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

60

LCS LCS



Method: 6020A - Metals (ICP/MS)


RL MDL

Silver 0.00180 J 0.20 0.0014 mg/Kg 06/02/16 11:09 06/03/16 20:41 2

MB MB


1.64 J 0.6210 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Aluminum

0.0354 J 0.0261.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Arsenic

ND 0.221.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Barium

0.0228 J 0.0110.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Beryllium

0.00780 J 0.00370.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Cadmium

0.0170 J 0.00170.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Cobalt

0.347 J 0.0600.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Chromium

0.243 J 0.0970.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Copper

281 3.220 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Iron

1.73 0.121.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Manganese

0.0688 J 0.0450.20 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Lead

ND 0.0140.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Antimony

0.0472 J 0.0401.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Selenium

ND 0.0190.40 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Thallium

ND 0.0371.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Vanadium

1.17 J 0.504.0 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Zinc

34.7 J 22200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Calcium

8.60 J 4.9200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Potassium

7.73 J 4.0200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Magnesium

26.5 J 8.7200 mg/Kg 06/02/16 11:09 06/03/16 20:41 2Sodium


RL MDL

Nickel 0.0802 J 0.40 0.039 mg/Kg 06/02/16 11:09 06/06/16 14:18 2

MB MB



Silver 10.0 9.61 mg/Kg 96 60 - 114

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

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Aluminum 1000 964 mg/Kg 96 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Arsenic 100 92.4 mg/Kg 92 73 - 110

Barium 100 95.2 mg/Kg 95 70 - 110

Beryllium 100 104 mg/Kg 104 79 - 110

Cadmium 100 92.8 mg/Kg 93 74 - 110

Cobalt 100 101 mg/Kg 101 74 - 110

Chromium 100 96.8 mg/Kg 97 70 - 110

Copper 100 98.5 mg/Kg 99 73 - 110

Iron 1000 982 mg/Kg 98 80 - 120

Manganese 100 98.4 mg/Kg 98 80 - 120

Lead 100 108 mg/Kg 108 75 - 110

Antimony 10.0 9.42 mg/Kg 94 68 - 113

Selenium 100 89.0 mg/Kg 89 65 - 110

Thallium 25.0 26.0 mg/Kg 104 71 - 110

Vanadium 100 96.6 mg/Kg 97 72 - 110

Zinc 100 95.9 mg/Kg 96 72 - 113

Calcium 1000 973 mg/Kg 97 80 - 120

Potassium 1000 1000 mg/Kg 100 80 - 120

Magnesium 1000 1000 mg/Kg 100 80 - 120

Sodium 1000 1010 mg/Kg 101 80 - 120


Nickel 100 99.0 mg/Kg 99 75 - 110

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


RL MDL

Silver ND 1.0 0.020 ug/L 06/08/16 13:00 06/09/16 13:40 1

MB MB


ND 9.050 ug/L 06/08/16 13:00 06/09/16 13:40 1Aluminum

ND 0.495.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Arsenic

ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Barium

ND 0.0531.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Beryllium

ND 0.0611.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Cadmium

ND 0.0211.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Cobalt

ND 0.602.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Chromium

ND 0.752.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Copper

ND 16100 ug/L 06/08/16 13:00 06/09/16 13:40 1Iron

ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Manganese

ND 0.232.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Nickel

ND 0.111.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Lead

ND 0.162.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Antimony

0.288 J 0.255.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Selenium

ND 0.0741.0 ug/L 06/08/16 13:00 06/09/16 13:40 1Thallium

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RL MDL

Vanadium ND 5.0 0.23 ug/L 06/08/16 13:00 06/09/16 13:40 1

MB MB


ND 7.320 ug/L 06/08/16 13:00 06/09/16 13:40 1Zinc

ND 2401000 ug/L 06/08/16 13:00 06/09/16 13:40 1Calcium

ND 301000 ug/L 06/08/16 13:00 06/09/16 13:40 1Potassium

ND 481000 ug/L 06/08/16 13:00 06/09/16 13:40 1Magnesium

ND 681000 ug/L 06/08/16 13:00 06/09/16 13:40 1Sodium

Client Sample ID: Lab Control SampleLab Sample ID: LCS 240-233672/3-AMatrix: Solid Prep Type: Total RecoverableAnalysis Batch: 233954 Prep Batch: 233672

Silver 100 94.5 ug/L 95 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Aluminum 10000 10400 ug/L 104 80 - 120

Arsenic 1000 913 ug/L 91 80 - 120

Barium 1000 931 ug/L 93 80 - 120

Beryllium 1000 1140 ug/L 114 80 - 120

Cadmium 1000 927 ug/L 93 80 - 120

Cobalt 1000 952 ug/L 95 80 - 120

Chromium 1000 973 ug/L 97 80 - 120

Copper 1000 931 ug/L 93 80 - 120

Iron 10000 9370 ug/L 94 80 - 120

Manganese 1000 997 ug/L 100 80 - 120

Nickel 1000 966 ug/L 97 80 - 120

Lead 1000 823 ug/L 82 80 - 120

Antimony 100 94.0 ug/L 94 80 - 120

Selenium 1000 904 ug/L 90 80 - 120

Thallium 250 209 ug/L 84 80 - 120

Vanadium 1000 1010 ug/L 101 80 - 120

Zinc 1000 959 ug/L 96 80 - 120

Calcium 10000 10700 ug/L 107 80 - 120

Potassium 10000 9350 ug/L 93 80 - 120

Magnesium 10000 9570 ug/L 96 80 - 120

Sodium 10000 9620 ug/L 96 80 - 120


RL MDL

Silver ND 1.0 0.020 ug/L 06/08/16 13:00 06/09/16 13:36 1

LB LB


ND 9.050 ug/L 06/08/16 13:00 06/09/16 13:36 1Aluminum

ND 0.495.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Arsenic

ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Barium

ND 0.0531.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Beryllium

ND 0.0611.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Cadmium

0.115 J 0.0211.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Cobalt

ND 0.602.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Chromium

1.96 J 0.752.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Copper

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RL MDL

Iron ND 100 16 ug/L 06/08/16 13:00 06/09/16 13:36 1

LB LB


ND 1.15.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Manganese

0.232 J 0.232.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Nickel

ND 0.111.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Lead

ND 0.162.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Antimony

ND 0.255.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Selenium

ND 0.0741.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Thallium

ND 0.235.0 ug/L 06/08/16 13:00 06/09/16 13:36 1Vanadium

ND 7.320 ug/L 06/08/16 13:00 06/09/16 13:36 1Zinc

ND 2401000 ug/L 06/08/16 13:00 06/09/16 13:36 1Calcium

ND 301000 ug/L 06/08/16 13:00 06/09/16 13:36 1Potassium

ND 481000 ug/L 06/08/16 13:00 06/09/16 13:36 1Magnesium

184 J 681000 ug/L 06/08/16 13:00 06/09/16 13:36 1Sodium

Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Lab Sample ID: 240-65486-1 MSMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233954 Prep Batch: 233672

Silver ND 100 93.6 ug/L 94 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Aluminum 4100 10000 15000 ug/L 109 75 - 125

Arsenic 1.6 J 1000 992 ug/L 99 75 - 125

Barium 140 1000 1120 ug/L 98 75 - 125

Beryllium 0.16 J 1000 1180 ug/L 118 75 - 125

Cadmium 0.24 J 1000 951 ug/L 95 75 - 125

Cobalt 0.19 J B 1000 973 ug/L 97 75 - 125

Chromium 1500 1000 2500 ug/L 99 75 - 125

Copper ND 1000 921 ug/L 92 75 - 125

Iron ND 10000 9500 ug/L 95 75 - 125

Manganese ND 1000 1010 ug/L 101 75 - 125

Nickel ND 1000 970 ug/L 97 75 - 125

Lead 0.70 J 1000 860 ug/L 86 75 - 125

Antimony 2.4 100 102 ug/L 100 75 - 125

Selenium 17 B 1000 986 ug/L 97 75 - 125

Thallium 0.19 J 250 222 ug/L 89 75 - 125

Vanadium 98 1000 1130 ug/L 103 75 - 125

Zinc ND 1000 950 ug/L 95 75 - 125

Calcium 250000 10000 259000 4 ug/L 99 75 - 125

Potassium 11000 10000 20400 ug/L 95 75 - 125

Magnesium 140 J 10000 9860 ug/L 97 75 - 125

Sodium 4200 B 10000 14100 ug/L 98 75 - 125

Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Lab Sample ID: 240-65486-1 MSDMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233954 Prep Batch: 233672

Silver ND 100 93.6 ug/L 94 75 - 125 0 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Aluminum 4100 10000 14800 ug/L 107 75 - 125 1 20

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Arsenic 1.6 J 1000 986 ug/L 98 75 - 125 1 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium 140 1000 1100 ug/L 97 75 - 125 1 20

Beryllium 0.16 J 1000 1170 ug/L 117 75 - 125 1 20

Cadmium 0.24 J 1000 940 ug/L 94 75 - 125 1 20

Cobalt 0.19 J B 1000 941 ug/L 94 75 - 125 3 20

Chromium 1500 1000 2440 ug/L 93 75 - 125 3 20

Copper ND 1000 901 ug/L 90 75 - 125 2 20

Iron ND 10000 9260 ug/L 93 75 - 125 3 20

Manganese ND 1000 982 ug/L 98 75 - 125 2 20

Nickel ND 1000 957 ug/L 96 75 - 125 1 20

Lead 0.70 J 1000 842 ug/L 84 75 - 125 2 20

Antimony 2.4 100 101 ug/L 98 75 - 125 1 20

Selenium 17 B 1000 977 ug/L 96 75 - 125 1 20

Thallium 0.19 J 250 218 ug/L 87 75 - 125 2 20

Vanadium 98 1000 1130 ug/L 103 75 - 125 0 20

Zinc ND 1000 924 ug/L 92 75 - 125 3 20

Calcium 250000 10000 255000 4 ug/L 62 75 - 125 1 20

Potassium 11000 10000 20100 ug/L 92 75 - 125 1 20

Magnesium 140 J 10000 9710 ug/L 96 75 - 125 2 20

Sodium 4200 B 10000 13900 ug/L 96 75 - 125 1 20



RL MDL

Mercury ND 0.20 0.090 ug/L 06/08/16 13:30 06/09/16 12:01 1

MB MB



Mercury 5.00 4.82 ug/L 96 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Method BlankLab Sample ID: LB 240-233529/1-DMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233843 Prep Batch: 233673

RL MDL

Mercury 0.0925 J 0.20 0.090 ug/L 06/08/16 13:30 06/09/16 11:58 1

LB LB


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Method: 7470A - Mercury (CVAA) (Continued)

Client Sample ID: WESTERLY WWTC-ASH (WWWTC)Lab Sample ID: 240-65486-1 MSMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233843 Prep Batch: 233673

Mercury ND 5.00 5.02 ug/L 100 80 - 120

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Mercury ND 5.00 4.89 ug/L 98 80 - 120 3 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD



RL MDL

Mercury ND 0.10 0.014 mg/Kg 06/02/16 15:00 06/03/16 07:27 1

MB MB



Mercury 0.833 0.865 mg/Kg 104 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Method: 7196A - Chromium, Hexavalent


RL MDL

Cr (VI) 0.358 J 0.80 0.15 mg/Kg 06/09/16 09:04 06/09/16 13:40 1

MB MB


Client Sample ID: Lab Control SampleLab Sample ID: LCSI 240-233791/11-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233886 Prep Batch: 233791

Cr (VI) 643 582 mg/Kg 90 75 - 125

Analyte

LCSI LCSI


Spike

Added

%Rec.

Limits

Client Sample ID: Lab Control SampleLab Sample ID: LCSS 240-233791/10-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 233886 Prep Batch: 233791

Cr (VI) 20.0 18.5 mg/Kg 93 90 - 110

Analyte

LCSS LCSS


Spike

Added

%Rec.

Limits

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Method: 7196A - Chromium, Hexavalent (Continued)

Client Sample ID: Method BlankLab Sample ID: LB 240-233529/1-AMatrix: Solid Prep Type: ASTM LeachAnalysis Batch: 233639

RL MDL

Cr (VI) ND 0.020 0.0021 mg/L 06/08/16 11:47 1

LB LB


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GC/MS VOA



Solid 8260B 233052240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA


Solid 8260BMB 240-233030/6 Method Blank Total/NA

Prep Batch: 233052


Solid 5030A240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA

Leach Batch: 233606


Solid 1312240-65486-1 WESTERLY WWTC-ASH (WWWTC) SPLP

Solid 1312LB 240-233606/1-A MB Method Blank SPLP



Solid 8260B 233606240-65486-1 WESTERLY WWTC-ASH (WWWTC) SPLP

Solid 8260B 233606LB 240-233606/1-A MB Method Blank SPLP


GC/MS Semi VOA

Prep Batch: 233013


Solid 3540C240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA







Leach Batch: 233529


Solid D3987-85240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach



Solid 8270C 233013240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA

Prep Batch: 233761


Solid 3510C 233529240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach






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GC/MS Semi VOA (Continued)





Leach Batch: 234140


Solid D3987-85240-65486-1 - RE WESTERLY WWTC-ASH (WWWTC) ASTM Leach

Prep Batch: 234253


Solid 3510C 234140240-65486-1 - RE WESTERLY WWTC-ASH (WWWTC) ASTM Leach





Solid 8270C 234253240-65486-1 - RE WESTERLY WWTC-ASH (WWWTC) ASTM Leach



GC Semi VOA

Prep Batch: 233005





Prep Batch: 233006



Solid 3540C240-65486-1 MS WESTERLY WWTC-ASH (WWWTC) Total/NA

Solid 3540C240-65486-1 MSD WESTERLY WWTC-ASH (WWWTC) Total/NA





Solid 8082A 233005240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA



Leach Batch: 233529



Prep Batch: 233752





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GC Semi VOA (Continued)

Prep Batch: 233753







Solid 8081B 233006240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA

Solid 8081B 233006240-65486-1 MS WESTERLY WWTC-ASH (WWWTC) Total/NA

Solid 8081B 233006240-65486-1 MSD WESTERLY WWTC-ASH (WWWTC) Total/NA





Solid 8082A 233752240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach





Solid 8081B 233753240-65486-1 WESTERLY WWTC-ASH (WWWTC) ASTM Leach



Metals

Prep Batch: 232891


Solid 3050B240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA

Solid 3050BLCS 240-232891/3-A ^2 Lab Control Sample Total/NA

Solid 3050BMB 240-232891/1-A ^2 Method Blank Total/NA

Prep Batch: 232940















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Metals (Continued)







Leach Batch: 233529



Solid D3987-85240-65486-1 MS WESTERLY WWTC-ASH (WWWTC) ASTM Leach

Solid D3987-85240-65486-1 MSD WESTERLY WWTC-ASH (WWWTC) ASTM Leach

Solid D3987-85LB 240-233529/1-C Method Blank ASTM Leach

Solid D3987-85LB 240-233529/1-D Method Blank ASTM Leach

Prep Batch: 233672



Solid 3005A 233529240-65486-1 MS WESTERLY WWTC-ASH (WWWTC) ASTM Leach

Solid 3005A 233529240-65486-1 MSD WESTERLY WWTC-ASH (WWWTC) ASTM Leach


Solid 3005ALCS 240-233672/3-A Lab Control Sample Total Recoverable

Solid 3005AMB 240-233672/2-A Method Blank Total Recoverable

Prep Batch: 233673






















Solid 6020A 233672LCS 240-233672/3-A Lab Control Sample Total Recoverable

Solid 6020A 233672MB 240-233672/2-A Method Blank Total Recoverable

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General Chemistry



Solid Moisture240-65486-1 WESTERLY WWTC-ASH (WWWTC) Total/NA

Leach Batch: 233529



Solid D3987-85LB 240-233529/1-A Method Blank ASTM Leach




Solid 7196A 233529LB 240-233529/1-A Method Blank ASTM Leach

Prep Batch: 233791



Solid 3060ALCSI 240-233791/11-A Lab Control Sample Total/NA

Solid 3060ALCSS 240-233791/10-A Lab Control Sample Total/NA





Solid 7196A 233791LCSI 240-233791/11-A Lab Control Sample Total/NA

Solid 7196A 233791LCSS 240-233791/10-A Lab Control Sample Total/NA


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Lab ChronicleClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65486-1Project/Site: WESTERLY WWTC-ASH (WWWTC)

Client Sample ID: WESTERLY WWTC-ASH (WWWTC) Lab Sample ID: 240-65486-1Matrix: SolidDate Collected: 05/31/16 14:10


Leach 1312 06/07/16 20:15 DRJ233606 TAL CAN

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

SPLP

Analysis 8260B 1 233711 06/08/16 20:49 TJL1 TAL CANSPLP



Analysis 8270C 1 233811 06/09/16 21:17 JMG TAL CANASTM Leach

Leach D3987-85 RE 234140 06/12/16 16:25 DRJ TAL CANASTM Leach

Prep 3510C RE 234253 06/13/16 11:40 JDR TAL CANASTM Leach

Analysis 8270C RE 1 234362 06/14/16 10:13 MRU TAL CANASTM Leach



Analysis 8081B 1 234206 06/13/16 15:28 BPM TAL CANASTM Leach



Analysis 8082A 1 234149 06/13/16 09:58 SEM TAL CANASTM Leach



Analysis 6020A 1 233954 06/09/16 13:48 AS1 TAL CANASTM Leach



Analysis 7470A 1 233843 06/09/16 12:05 WKD TAL CANASTM Leach


Analysis 7196A 1 233639 06/08/16 13:35 GNR TAL CANASTM Leach

Analysis Moisture 1 232880 06/02/16 10:25 LCN TAL CANTotal/NA



Prep 5030A 06/03/16 10:36 SAM233052 TAL CAN

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8260B 1 233030 06/03/16 19:07 SAM TAL CANTotal/NA


Analysis 8270C 4 233573 06/08/16 21:44 JMG TAL CANTotal/NA


Analysis 8081B 1 233996 06/10/16 16:27 BPM TAL CANTotal/NA


Analysis 8082A 1 233178 06/06/16 14:47 HMB TAL CANTotal/NA







Prep 7471A 232940 06/02/16 15:00 DEE TAL CANTotal/NA

TestAmerica Canton

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Lab ChronicleClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65486-1Project/Site: WESTERLY WWTC-ASH (WWWTC)



Analysis 7471A 06/03/16 07:44 WKD1 233026 TAL CAN

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Prep 3060A 233791 06/09/16 09:04 DTN TAL CANTotal/NA

Analysis 7196A 1 233886 06/09/16 13:45 DTN TAL CANTotal/NA



TestAmerica Canton

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Certification SummaryClient: Northeast Ohio Regional Sewer District TestAmerica Job ID: 240-65486-1Project/Site: WESTERLY WWTC-ASH (WWWTC)

Laboratory: TestAmerica CantonAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

California 01144CA9NELAP 06-30-14 *

California State Program 9 2927 04-30-17

Connecticut State Program 1 PH-0590 12-31-17

Florida NELAP 4 E87225 06-30-16 *

Illinois NELAP 5 200004 07-31-16 *

Kansas NELAP 7 E-10336 07-31-16 *

Kentucky (UST) State Program 4 58 02-23-17

Kentucky (WW) State Program 4 98016 12-31-16

L-A-B DoD ELAP L2315 07-18-16

Minnesota NELAP 5 039-999-348 12-31-16

Nevada State Program 9 OH-000482008A 07-31-16 *

New Jersey NELAP 2 OH001 06-30-16 *

New York NELAP 2 10975 03-31-17

Ohio VAP State Program 5 CL0024 09-14-17

Oregon NELAP 10 4062 02-23-17

Pennsylvania NELAP 3 68-00340 08-31-16 *

Texas NELAP 6 T104704517-15-5 08-31-16 *

USDA Federal P330-13-00319 11-26-16

Virginia NELAP 3 460175 09-14-16

Washington State Program 10 C971 01-12-17

West Virginia DEP State Program 3 210 12-31-16

Wisconsin State Program 5 999518190 08-31-16 *

TestAmerica Canton

* Certification renewal pending - certification considered valid.

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Documents

REQUEST FOR PROPOSALS BENEFICIAL REUSE ... RFP.pdfThe wastewater contains solid materials which are dewatered into a more concentrated sewage sludge cake and incinerated on site in