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Reproducibility of soil compaction curve Item type text; Thesis-Reproduction (electronic) Authors Agah, Hamid, 1939- Publisher The University of Arizona. Rights Copyright © is held by the author. Digital access to this material is made possible by the University Libraries, University of Arizona. Further transmission, reproduction or presentation (such as public display or performance) of protected items is prohibited except with permission of the author. Downloaded 5-Mar-2016 10:54:11 Link to item http://hdl.handle.net/10150/347630

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Page 1: Reproducibility of soil compaction curve

Reproducibility of soil compaction curve

Item type text; Thesis-Reproduction (electronic)

Authors Agah, Hamid, 1939-

Publisher The University of Arizona.

Rights Copyright © is held by the author. Digital access to thismaterial is made possible by the University Libraries,University of Arizona. Further transmission, reproductionor presentation (such as public display or performance) ofprotected items is prohibited except with permission of theauthor.

Downloaded 5-Mar-2016 10:54:11

Link to item http://hdl.handle.net/10150/347630

Page 2: Reproducibility of soil compaction curve

REPRODUCIBILITY OF SOIL COMPACTION CURVE

by

Hamid Agah

A Thesis Submitted to the Faculty of the

DEPARTMENT OF CIVIL ENGINEERING

In Partial Fulfillment of the Requirements For the Degree of

MASTER OF SCIENCE

' In the Graduate College

THE UNIVERSITY OF ARIZONA

19 6 8

Page 3: Reproducibility of soil compaction curve

STATEMENT BY AUTHOR

This thesis has been submitted in partial fulfillment of re­quirements for an advanced degree at The University of Arizona and is deposited in the University Library to be made available to borrowers under rules of the Library.

Brief quotations from this thesis are allowable without special permission, provided that accurate acknowledgment of source is made. Requests for permission for extended quotation from or reproduction of this manuscript in whole or in part may be granted by the head of the major department or the Dean of the Graduate College when in his judg­ment the proposed use of the material is in the interests of scholar­ship. In all other instances, however, permission must be obtained from the author.

SIGNED: A

APPROVAL BY THESIS DIRECTOR

This thesis has been approved on the date shown below:

/ ~ / _______H. Sultan

Assoc. Prof. of Civil Engineering

Page 4: Reproducibility of soil compaction curve

ACKNOWLEDGMENT

The author expresses his appreciation to Dr. H. Sultan, his

thesis director, for the considerable time he spent in making very

constructive criticism in the course of directing this study. This

contribution was invaluable.

Sincere gratitude is extended to Professors R. L. Sloane and

D. Woods for their assistance in this research. They have been a source

of encouragement to the author as outstanding teachers during the course

of his studies.

Finally, this work would not have been possible without the

love, encouragement, patience and support from the authors’ parents.

This I cannot ever adequately acknowledge.

Page 5: Reproducibility of soil compaction curve

TABLE OF CONTENTS

Chapter Page

LIST OF ILLUSTRATXONSo & o © e ® e e e ® o o 6 8 & ® e o ® e & e e © © e 6 9 9 © B e B e e © ® © VI

LIST OF T A B L E S v l x x

ABSTRACT©@@@@©@@@@@©@@@©©@@@@@©@@@@©©©©@@@@@©@@©@©@@©@0000© xx

I 0 INTRODUCTION @eee@oG«>e@@0@8@@8@©@o@@@8@0@@@@*)060@o0O@@©0@®@o I

IeI SCOpe690ee0tieee©e»®©s©6®oeo»0oeee60eeoe8eaeoceeeeo 2I e 2 Definitions e e e ® e e e e e ® 6 e © e e > 9 e e e < > e e o © ® » e e e © e e e ® e » e e e o 3

EQUIPMENT AND MATERIALS0 e, e e e e e e e o o e e e e e e a e e o e . e e a e e e o e a

2 o I Equipmenteeo®6e®©0ee96oeee»6 e e oeeeeeeoeeoeoeeeeee® 62 e 2 Materials Used © GGe@@ea@0*0@*9@@@@e©e@e6a6@ee8oea@0 D

3 o TEST P ROCEDURE eoeeo®6ee®eeeeeeooe®eeeeGQde©®06®e©6. 09e®©»e0Q 12

3 o 1 P aramete rs oo06OQ©0oo®««©®c/®®0edoe©©0©©eeeeo©©«&0®© 123 © 2 Sample Preparation© ® © © © © © e© ©©©e©©®©©©®®®®©®©©©©©©© 123 © 3 COmpaCtlOn Tests ©®ee»ee0o©ee©e©e©®eeeee»©e8e®©ee®o 13

40 DATA ANALYSIS AND RESULTSee@aeo»e©eeoe**aeoe*@ee@eeee«ea*0@ 16

4 © 1 ASTM Curves ©....... *.......... 164 © 2 Cubic CUrVeS eeeeeeoee*®©©©®©© ©©eoeGoeeeaeee eee©ae© 244 93 Reproducibility Evaluation,.# # e • 294,4 Moisture Content Patterns © ® ©»«e»©»© © 6»8 © © © © © ©»© © © © 364©5 Gradation Change©©©©e©©©©©©©®©©©©®©©©®®©©®©©®*©©©© 39.

Se DISCUSSION OF RESULTSeeeeoeeeeeeeeeeeeeeeeeeoeoeeoeeee®©©©®® 42

9G00Qeo0»0O00e®eeeee0o< 00O6eoeae©eee»ee060O8®eeti@oe®©ei

e e e e e e e o e a o e e ®

5.1 Comparison of Cubic Model vs. ASTM Method.5.2 Controlled Tests5.3 Plasticity5.4 Gradation Effect5.5 Layer-Thickness Effect......5.6 Manual [email protected].@............................ 465.7 Moisture Content Patterns......................... 47

42434445 45

Page 6: Reproducibility of soil compaction curve

V

TABLE OF CONTENTS— Continued

Chapter Page

6 o CONCLUSIONS e e e e e e e e o e e e e e o e e o e e e e e e e e e e o e e e o e e e e o d e e e e e e e e e 4 9

6 © 1 Summarye e e o e e e e e e e e e e e e e B e e o e o o e c a e e e o e e o e e e e e e e e e 496 a 2 FUture ReSe archo©©e©eeeo0©©o©ee©O9®ee©e®©©eo^e&eQd 50

APPENDIX - LEAST SQUARES SOLUTION FOR THE PARAMETERS OF ACUBIC POLYNOMIAL© e e e e e o o e e e e o e o e o e e e e e e o e o o e o e e © 52

REFERENCESo«o«o«o»«ooO@O9©o®eo0eoae00©0o©0000©©©000e©©e©9Oo 61

Page 7: Reproducibility of soil compaction curve

LIST OF ILLUSTRATIONS

Figure . Page

1« Rainhart Automatic Tamper No» 662, with the Mold.,.....,.,... 7

2. Range of Gradation of Sand.@@@...,...,,...,@,..@..,@,...@8.,. 10

3, Moisture Density Curves for Controlled Tests Plotted, UsingASTM Standard Method.........e,....,.,........,....,......... 17

Moisture Density Curves for Sand and 10% Kaolinite Plotted,Using ASTM Standard Method..................o...............@ IS

Moisture Density Curves for Sand and 2% Bentonite Plotted,Using ASTM Standard Method..............o.................... 19

Moisture Density Curves for Random Gradation Sand Plotted,Using ASTM Standard Method.............o..................... 20

' p

7. Moisture Density Curves for Variable Layer-ThicknessCompacted Sand Plotted, Using ASTM Standard Method........... 21

8. Moisture Density Curves for Manually Compacted Sand Plotted,Using ASTM Standard Method.............o,...................o .22

9. Moisture Density Mean Curves Plotted, Using ASTM Standard M e t h o d 23

10, Moisture Density Curves for Controlled Tests Plotted, UsingCubic Regression Method, . e . o e . e o . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 25

11. Moisture Density Curves for Sand and 10% Kaolinite Plotted,Using Cubic Regression Method....e........................... 26

12. Moisture Density Curves for Sand and 2% Bentonite Plotted,Using Cubic Regression M e t h o d . . . . . . . e . . . . . . . . . . . . . . . . . 27

13. Moisture Density Mean Curves Plotted, Using Cubic RegressionM e t h o d . . . . . . . . . . d O Q d . e , . . e , o o e , . . o e . e . e . o , o o , . . . . . . . . . . . . . . . . 28

14. Moisture Density Mean Curves for Controlled Tests Plotted,Using ASTM Standard and Cubic Regression Methods............. 30

15. Moisture Density Mean Curves for Sand and 10% KaolinitePlotted, Using ASTM Standard and Cubic Regression Methods.... 31

VI

Page 8: Reproducibility of soil compaction curve

vii

LIST OF ILLUSTRATIONS— Continued

Figure Page

16o Moisture Density Mean Curves for Sand and 2% BentonitePlotted, Using ASTM Standard and Cubic Regression Methods.e * 32

17. Moisture Density Mean Curves for Random Gradation SandPlotted, Using ASTM Standard and Cubic Regression Methods... 33

18. Moisture Density Mean Curves for Variable Layer-Thickness Compacted Sand Plotted, Using ASTM Standard and Cubic. Regression Methods.......................................... 34

19. Moisture Density Mean Curves for Manually Compacted Sand Plotted, Using ASTM Standard and Cubic Regression Methods... 35

20. Effect of Compaction on Gradation of Sand................... 41

Page 9: Reproducibility of soil compaction curve

LIST OF TABLES

Table - Page

1. Reproducibility of Compaction in Terms of Standard Deviation of Each Group and Percent of Overlap Area ofMean of Each Group from Mean of Controlled Tests............ 37

2. Effect of Plasticity on Reproducibility of CompactionCurve in Terms of Standard Deviation for Each Parameter..... 38

3. Standard Deviations in Layer Moisture Content (MaximumValue for Each Test)................. 40

A.I. Cubic Regression Coefficients and Correlation Indices, forMoisture-Density Curves ........ 57

A.2. The Deviations of Maximum Density and the Percent OverlapArea from the Mean of the Same Parameter 58

A.3. The Deviations of Maximum Density and the Percent OverlapArea from the Mean of the Same Parameter.................... 59

A.4. The Deviations of Maximum Density and the Percent OverlapArea from the Mean of the Controlled Tests.................. 60

viii

Page 10: Reproducibility of soil compaction curve

ABSTRACT

The effects of four parameters on the degree of reproducibility

of soil compaction curve were investigated. These parameters were:

placticity; gradation; layer-thickness; and manual compaction. The

variations of the moisture contents within the compacted specimens were

checked to determine their significance. The degree of reproducibility

was computed by four different methods, and compared. Attempts were

made to characterize the moisture-density relationship by mathematical

models. '

Page 11: Reproducibility of soil compaction curve

CHAPTER 1

INTRODUCTION

The term compaction refers to the practice of artificially

densifying a soil mass by rolling, tamping, vibrating, or other means,

The moisture-density relationship of a soil gives approximate infor­

mation on the gradation; the sensitivity to moisture content, and the

load carrying capacity of the soil. The more important reasons for

compaction of soils are: to increase the strength; to reduce compres­

sibility, to control volume change tendencies; to control resilience

properties; to decrease permeability; and to reduce frost susceptibility.

Several factors influence the value of density obtained by

compaction. Of primary importance are: the moisture content of the

soil; the gradation and physical properties of the soil; and the type

and amount of compactive effort among others. Of lesser significance is

the temperature of the soil and water. For fine-grained cohesive soils,

the soil structure is a very important factor in affecting the soil

strength.

Thirty five years ago, Proctor (9), a pioneer in the field of

compaction, determined that by moving the soil particles and water into

the soil voids, the soil density can be increased. He determined the

relationship between the compactive effort and the density obtained as

a result of this effort. The compaction test he designed is the basis

of all the present laboratory impact methods of testing. The laboratory

Page 12: Reproducibility of soil compaction curve

results are hard to duplicate in the field because of differences in

confinement, compactive effort, reuse of soils, layer thickness,

accuracy of measurement and the method of compaction. The-basic

difference between various laboratory methods of testing lies in the

amount and method of application of the compactive energy.

1.1 Scope

In writing specifications for earthwork construction contracts,

it is usually specified that the field density should not be less than

a certain percentage of the maximum dry density obtained in the labo­

ratory. Also, the moisture content should be within certain limits from

the laboratory optimum value. Therefore, it is implicitly assumed that

a high degree of reproducibility is expected in conducting the laboratory

compaction tests.

As stated previously several factors do influence the degree of

compaction and obviously many more would influence, to various extents,

the degree of reproducibility of the compaction curve. Consequently,

since the laboratory compaction curve is the basis of the specification

guidelines, it is of interest to investigate its degree of repro­

ducibility. Further the quantitative magnitudes of deviations from the

implicit uniqueness assumption are of interest.

The purpose of this investigation is to study the possible effect

of a number of experimental parameters on the degree of reproducibility

Page 13: Reproducibility of soil compaction curve

of the compaction curve. An attempt also is made to explore the

possibility of establishing a mathematical expression for the compaction

curve, and to measure the degree of reproducibility by a statistical

method.

1.2 Definitions

The following symbols and notations have been adopted for use in

this thesis, and are defined as follows:

Soil Definitions:

Dry density, (y^) - The weight of soil grains per unit volume

of soil mass.

Moisture content, (W) - The weight of moisture filling the soil

voids, as percent of dry weight.

Compaction test - Compacting the soil following a specified

procedure. It is referred to as the test for simplicity.

Compaction curve - The plot of moisture-density relationship

obtained from the compaction test. This is referred to as the

curve for simplicity.

Maximum dry density, (Max. y^) - The density at the peak of the

compaction curve.

Optimum moisture content, (O.M.C.) - The moisture content at the

point of maximum density (peak) on the curve.

Plasticity index, (P.I.) - A measure of the plasticity range of

soils, as measured by the Atterberg Limits, It is usually

expressed as moisture content in percent of dry weight.

Page 14: Reproducibility of soil compaction curve

Mechanical compaction - The test run by the use of a motor-

operated automatic tamper.

Manual compaction - The test run by the use of a hand-operated

tamper.

Deviation of Maximum dry density, (A Max. y^) - The deviation of

maximum dry density of each test from the maximum dry density of

the mean curve of the group; in percent.

ASTM method - By connecting the test data points with a smooth

curve, a compaction curve is produced. This is the method

designated in the ASTM D 69B-64T test.

Overlap area - The area under a curve bounded by the vertical

lines at _+ 2% of optimum moisture content, and a horizontal line

at 95% of maximum dry density is defined. The portion that the

defined area of any curve has in common with the defined area of

the mean curve, is referred to as the overlap area. When this

overlap area is expressed as a percent of the defined area of

the mean, it is called percent overlap area. This is a method

of measuring the degree of reproducibility of the curves.

Statistical Definitions:

Mean - The value that is computed by adding all the items in a

set, and dividing the total by the number of items used. This

is how the mean curve for each group of the tests was obtained.

Random data - Implies that every individual in the population

has an equal chance of being selected on the next draw. This is

how the random gradation samples were obtained.

Page 15: Reproducibility of soil compaction curve

Cubic regression curve - I s a type of curve used to describe the

trend of the data. The mathematical expression for the curve is 2 3D = A + B W + C W + F W . Where, D (density) is the dependent

variable and W (moisture content) is the independent variable.

In this work the curve of regression was fitted by the method of

least squares.

Least squares method - Is a method of obtaining the best fit

curve to a set of data points. This unique curve is the one

about which the sum of squares of deviations of the observed

value from the expected value of the dependent variable will be

a minimum. This method is illustrated in the Appendix for a

cubic model.

Standard deviation, (S) - It is a measure of the scatter of

items about the arithmetic mean of the sample. The mathematical

expression is given in the Appendix.

Correlation index, (R) - It is a measure of the closeness of the

points of the curve of relation. Its value ranges from zero for

no correlation to one for perfect correlation. The mathematical 2expression for R is also given in the Appendix.

Page 16: Reproducibility of soil compaction curve

CHAPTER 2

EQUIPMENT AND MATERIALS

2.1 Equipment

The following compaction equipment was used during the course of

the laboratory work for this study:

Automatic Tamper. The Rainhart Automatic Tamper No. 662 shown

in Figure 1 was used. This method is referred to as mechanical com­

paction method. This tamper was cleaned, lubricated and adjusted for

the ASTM test designated D 698 - 64T. This is the so-called Standard

Proctor or Standard AASHO test. The loading speed and the blow spacing

were kept constant through the whole series of tests. The tamper has a

circular segment face (90° angle), with a radius of approximately 2

inches.

The load is lifted by means of a grabber, which is moved by a

cable. This load is released when the grabber reaches the upper end Of

a bar on which it moves. The load falls for the specified height and is

picked up again. The height of the drop is self-adjusting. This tamper

is widely used in the laboratories and is calibrated to apply the same

compactive energy as indicated for method "A" of the ASTM designated

test. It has the same weight of the hammer and the height of the drop

as the manual tamper. It can also be adjusted for the Modified Proctor

test.

6

Page 17: Reproducibility of soil compaction curve

7

FIGURE 1. Rainhart Automatic Tamper No. 662, with the Mold.

Page 18: Reproducibility of soil compaction curve

ASTM D 698 - 64T test. The tamper has a flat circular face 2 inches in

diameter and a weight of 5,5 pounds. The tamper has an arrangement that

controls the height of the drop to a free fall of 12 inches above the

surface of the soil in the mold. The load is to be applied vertically

to the soil, and the load spacing should be kept reasonably constant.

The vertical application of the load and the spacing will become more

consistent with experience, but the human factor would undoubtedly be

always present. The soil grains should not be allowed in the space

between the tamper and the cylinder around it, as this would not allow

the completely free fall of the tamper.

Mold, The mold used for all the tests is the one designated by

method "A" of the ASTM test. This is a cylinder of 4 inches in diameter

and a height of 4,584 inches. The volume of the mold is 1/30 cubic feet.

The mold has a detachable collar assembly of approximately 2,5 inches in

height, to permit the preparation of the sample to the desired height,

which is about 1/2 inch above the mold top. The mold and the collar are

fastened firmly to a detachable base plate. The same mold was used

throughout all the tests, and was prevented from rusting by a light

lubrication each day. It was weighed at the beginning of each test.

This mold is shown in Figure 1, attached to the base of the automatic

tamper by two clamps. The mold was held between the feet during the

manual compaction.

Page 19: Reproducibility of soil compaction curve

2.2 Materials Used

The soils used were sand, sand-kaolinite and sand-bentonite

mixtures. The sand was from a location on the Hughes Access Road, on

the south si4e of Tucson. This sand is being used by the New Pueblo

Construction Company, in asphaltic concrete mixes. The small percentage

(less than 6%) of particles larger than number 4 sieve present in the

sand, was discarded before the soil was brought to the laboratory. This

sand is well-graded with very little fines.

The specific gravity of the sand is 2.67, and it is non-plastic

as was determined by the Atterberg Limits. The grain-size distribution

of the sand as obtained by six sieve analyses is shown in Figure 2.

The range and the selected size distribution for five groups of tests

are shown in this figure.

The kaolinite used is commercially processed and distributed by

the Georgia Kaolin Company of Dry Branch, Georgia. This has the trade

name of Hydrite-UF. The kaolinite has a well defined platey, hexagonal

shape, and has a very small particle size (UF means ultra-fine)(7).

The specific gravity was determined to be 2,72 and the plasticity index

is above 30. Trial samples were run with 4%, 6% and 10% kaolinite re­

placing the smallest sand grains. The plasticity index for these

mixtures were 1, 6 and 8 in that order. The sand with 10% kaolinite

having a plasticity index of 8 was selected for a group of tests to

study the effect of plasticity on the degree of reproducibility. This

mixture has approximately the same gradation as the sand selected for

the controlled tests.

Page 20: Reproducibility of soil compaction curve

100

90

80

70

60

50

40

30

20

10

0 J

RANGE

G R A I N S I Z E IN M M 1

60 40 20S T A N D A R D SIEVE NUMBER

F IGURE 2 R A N G E OF GRADAT ION OF SA N D

Page 21: Reproducibility of soil compaction curve

11

The bentonite has a plasticity index of around 600, and is

from Wyoming. Trial samples of the sand-bentonite mixture of 2% and

3% bentonite were tested for plasticity. The plasticity index of 2%

bentonite mixture was 14 and the 3% bentonite had a plasticity index

of 30. The bentonite replaced some of the fine particles (passing No,

200 sieve), so that the gradation curve of the mixture is the same as

the controlled sand. The sand with 2% bentonite having a plasticity

index of 14 was selected for another group of tests to study the effect

of plasticity on the degree of reproducibility. With these two mixtures

the plasticities were increased, while the gradation stayed relatively

unchanged.

Page 22: Reproducibility of soil compaction curve

CHAPTER 3

TEST PROCEDURE

3.1 Parameters

The effect of four factors on the degree of reproducibility is

investigated in this study. These four factors are: gradation; vari­

ation in layer-thickness; manual compaction; and plasticity. In

addition, the reproducibility of a group of tests under controlled

condition is determined, and is used as a basis of comparison to

evaluate the influence of the above four factors. Considering the time

limitation of this study, it was decided that five tests in each group

would be a sufficient number, to study the effect of the pertinent para­

meter on the degree of reproducibility.

To determine the effect of plasticity on reproducibility of

compaction, the plasticity indices of 8 and 14 were selected after

preliminary testing as indicated previously. These are compared with

the controlled tests, in which the non-plastic controlled gradation sand

was used.

3.2 Sample Preparation

The selected sand of Figure 2 were used for groups of tests in:

this study. Approximately 150 kilograms of sand was obtained from the

location noted previously and air-dried. The hygroscopic moisture

content of the air-dried sand was determined, and was used to correct

12

Page 23: Reproducibility of soil compaction curve

13

the weight of grain size distribution in preparing the controlled

gradation. This moisture determination was also used to correct the

initial moisture content for all the compaction tests. The sand was

broken into its individual particles by a rubber-tipped pestle, and a

quantity sufficient for twenty five tests was sieved.

Fifteen samples were prepared from the sieved sand by mixing

weighed quantities of each grain size to obtain the selected gradation.

These samples of four kilograms each were prepared for the controlled

test group; variable layer-thickness group; and the manual compaction

group.

Two other groups of samples were prepared with the sieved sand,

in accordance with the selected gradation, and adding the 10% kaolinite

and 2% bentonite as indicated earlier. Finally, five samples were taken

at random from the original unsieved sand, to study the effect of vari­

ation in grain size distribution. These samples fall within the range

of the particle size distribution shown in Figure 2.

3.3 Compaction Tests

All the tests were generally conducted in accordance with the

impact-type test, ASTM designation D698 - 64T Method A, commonly referred

to as the Standard Proctor. The total compactive energy for the test is 312,400 ft-lb/ft . For this test the number of layers is three and the

number of blows of the hammer per layer is 25. The 5.5 pound hammer is

dropped for a free fall of 12 inches. The placing of the layers and the

determination of moisture content differed from the ASTM designated

procedure in this study, and they will be discussed here. All the tests

Page 24: Reproducibility of soil compaction curve

14were conducted in the following manner, except as noted at the end of

this chapter.

General Procedure. For all the test groups the automatic tamper

of Figure 1 was used. For each compaction test six or seven points were

run, at least two of which were on the wet-side of the optimum moisture

content. All the specimens were mixed thoroughly before addition of

water, particularly in the case of the soils with kaolinite and bento­

nite. The initial moisture content of 5% was selected after a trial

sample was run. The samples were mixed for this moisture content and

allowed to temper overnight, in accordance with the ASTM procedure. The

moisture content was raised in increments of approximately 2%, and

generally up to a moisture content of 17%.

After each compaction data point was obtained the soil removed

from the mold was completely remixed with the original sample, and then

water was added. During the weighing of moisture samples the soil was

covered with a moist cloth to protect it from surface evaporation. For

each data point an equal weight of soil was used for each layer. This

kept the layer thickness for the tests constant, and was necessary ifJ

the influence of each factor was to be determined independently.

Another variation from the ASTM procedure was the moisture

content determination. For each point on the moisture-density curve,

four moisture samples were obtained. One sample was obtained for each

individual layer, and one for the whole specimen as indicated in the

ASTM procedure. This was done to study the possible significance of

layer moisture content variations. Due to the large number of samples

Page 25: Reproducibility of soil compaction curve

15

needed for moisture content determinations per test, 30-50 gram

specimens were used for moisture determination instead of 100 grams.

After the compaction tests on the controlled sand samples, a

grain size distribution test was conducted. This was done for the

manual and mechanical compaction to determine their effect on gradation.

Controlled Tests. These tests were conducted using controlled-

gradation sand as indicated in the General Procedure above.

Plasticity Tests. Tests were conducted using the sand with 10%

kaolinite, and the sand with 2% bentonite in the manner indicated by the

General Procedure.

Random Gradation Tests. These tests were conducted on the

random sand samples in the same manner as that indicated in the General

Procedure.

Variable Layer-thickness Tests. Tests were conducted on the

controlled-gradation sand, but the quantity of soil placed was not

weighed, as was the case in the General Procedure. The variations

of the quantities of the soil in the three layers were within the limits

of normal practice. This was done to isolate the effect of layer thick­

ness variation on the reproducibility.

Manually Compacted Tests. These tests were conducted on the

controlled-gradation sand, but using the manual tamper instead of the

automatic tamper that was used in the General Procedure.

Page 26: Reproducibility of soil compaction curve

CHAPTER 4

DATA ANALYSIS AND RESULTS

4.1 ASTM Curves

The moisture-density data points obtained during the thirty

compaction tests are plotted as curves. The points for each test are

connected by a smooth curve, as indicated in the ASTM test procedure

designation D698 - 64T. These are the ASTM curves of Figures 3 through

8. The five tests in each group are plotted in one figure. The data

points are shown on each figure. For each group the mean of the five

curves was computed, and is plotted as the mean curve of the group.

This mean curve was plotted by use of the mean value of dry densities of

five curves at 2% moisture content intervals. The mean value of the

controlled tests was also plotted on all the figures of the non-plastic

soils. The mean curves for all the four groups of tests on sand are

plotted in Figure 9.

In general it can be seen that the data points for the controlled

tests, sand +10% kaolinite, sand +2% bentonite and manual compaction

follow their individual curves closely. The variable layer-thickness

group curves have the largest number of data points that do not fall on

the curves. The sand +2% bentonite group has the best fit of the curves

to the data points of all the groups, and the controlled tests show

better fit than the random gradation group.

16

Page 27: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(Y

d)

pcf

126

FIVE TESTS

MEAN OF FIVE T E S T S

MOISTURE CONTENT (W) IN PERCENT

FIGURE 3 M O I S T U R E D EN SI TY CURVES FOR CO NT R OL LE D T E S T S P L O T T E D , USI NG A S T M S T AN D A R DM E T H O D

Page 28: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(Y

d)

pcf

126

124

122

120 ' I---

118

F IV E TESTS116M E A N OF FIVE T EST S

114

112

1105 6 127 9 10 II8 13 14 15

MOISTURE CONTENT (W) IN PERCENT

F IGURE 4 M O I S T U R E D E N S I T Y C U R V E S FOR SAND AND 10 % K A O L I N I T E P L O T T E D , USI NG ASTMS T A N D A R D M ET HO D

oo

Page 29: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(Y

d)

pcf

126

116 F I V E T E ST S

- - MEAN OF F I V E T E S T S114

112

110 106 7 8 II 125 9 13 14 15MOISTURE CONTENT (w) IN PERCENT

F IG UR E 5 M O I S T U R E D E N S I T Y CURV ES FOR S A N D AND 2 % B E N T O N I T E P L O T T E D , U S I N G AS T M

S T A N D A R D M E T H O D

Page 30: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(Y

d )

pc

f

126

F I V E T E ST S124M E A N OF F IV E T E S T S

M E A N OF C O N T R O L L E DJ E S T S22

120

MOISTURE CONTENT (W) IN PERCENT

FIGURE 6 M O I S T U R E D E N S I T Y C U R V E S FOR RANDOM GR AD AT I ON SAND P L O TT E D, USING AST M

S T A N D A R D M E T H OD

K)O

Page 31: Reproducibility of soil compaction curve

pd (PR)

A1ISN3Q

A

dQ

FIVE TESTS124— MEAN OF F I V E TESTS

M E A N OF CO NT R OL LE DTESTS122

__l

5 6 7 8 9 10MOISTURE CONTENT (W) IN PERCENT

FIGURE 7 M O I S TU R E D E N S I T Y CURV ES FOR V A R I A B L E LAYER-THI CK NESS COMPACTED SAND PL OTT ED,USING A S T M S T ANDARD M ET HO D

to

Page 32: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(Y

d )

pcf

128

126

124

122

o I120

118

116F IVE T E ST S

- - M E AN OF FIVE T E ST S114

M E AN OF CO NT R OL LE D TESTS

112

110

MOISTURE CONTENT (W) IN PERCENT

F I G U R E 8 M O I S T U R E D E N S I T Y CURV ES FOR MANUALLY COMPACTED SAN D P L O T T E D , USING A S T MS T A ND AR D METHOD

NJ

Page 33: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(Y

d )p

cf

126

X124

122

120

— CONTROLLED TESTS

— M ANUAL COMPACTION

- - RAN DO M GRADATION

V AR IA BL E L AYER —THI CKNES S

114

MOISTURE CONTENT (W) IN PERCENT

FIGURE 9 M O I S T U R E D E N S I T Y MEAN CURVES PLOTTED, USING AS T M STANDARD METHOD

K)UJ

Page 34: Reproducibility of soil compaction curve

4.2 Cubic Curves

The method of least squares was employed to compute the values

of coefficients for the mathematical expression that would give the

equation of the compaction curve. Initially it was assumed that the

compaction curve would generally have a parabolic shape. The coef­

ficients for a parabolic equation were determined by the indicated

method. The values of these coefficients for each test and the mean of

each group were obtained by use of computer programming. The degree of

fit of these curves to the test data points were checked by the use of

correlation index.

Using the parabolic model the correlation indices obtained were

in the acceptable range (above 0.75), however the plotted results showed

that there were considerable divergences in the peak region of the

curves. This is the critical region of the compaction curve, since the

peak point lies within this range. Therefore, the parabolic model was

rejected and the cubic model was tried.

The method of least squares for the cubic equation is illustrated

in the Appendix. The equations for the coefficients of the cubic model

were programmed for the computer. The values of the coefficients of the

cubic equation for some of the individual compaction tests, and those

for the mean curves of all groups are given in Table A.1 in the Appendix.

The correlation indices for the curves are also given in the same table.

The cubic model gave excellent correlation. The correlation

indices ranged from 0.97 to 1.00. The curves obtained using these coef­

ficients are presented in Figures 10 through 13. In the first three

Page 35: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(*

d)

pcf

126

124

122

120

118

FIVE TESTS116- - MEAN OF FIVE

T E S T S114 r

112

110

M O IS T U R E CONTENT (W) IN PERCENT

FIGURE 10 M O IS T U R E DE N SI TY CUR V ES FOR C O N T R O L L E D T ES T S P L O T T E D , USING CUBI C REGRESSI ON

M E T H O D

K)cn

Page 36: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(Y

d )

pcf

M EA N OF F IV E T E ST S

MOISTURE CONTENT (W) IN PERCENT

FIGURE II M O I S T U R E D E N S I T Y CURVES FOR SAND A N D 10 % K A O L I N I T E P L O T T E D , U S I N G CUBICR E G R E S S I O N METHOD

K)O

Page 37: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(Y

d)

pcf

126

124

122

120

118FI VE TESTS

116MEAN OF F IVE T E S T S

114

112

110

M O IS T U R E CONTENT (W) IN PERCENT

F I G U R E 12 M O I S T U R E DE N SI TY CURV ES FOR SAND AND 2 % BENTONI TE P L O T T E D , USI NG CUBIC

R E G R E S S I O N MET HOD

N>

Page 38: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(Y

d)

pcf

26

24

122 — k

120

C O NT R OL LE D T E S T

MANUAL COMPACTION

RANDOM G RADAT IO N

------------- V A R I A B L E - L A Y E RTHI CKNESS

11010 125 6 7 8 9 14

M O IS TU R E CONTENT (W) IN PERCENT

F IG U RE 13 M O I S T U R E D E N S I T Y M E A N CURVES P L O T T E D , USING CUBIC REGRESSION M E T H O D

N>00

Page 39: Reproducibility of soil compaction curve

29

figures the curves for all the five tests in each group, as well as

their mean curve are plotted. In Figure 13 the mean curves for the four

non-plastic groups are plotted.

In Figures 14 through 19 the mean curves of each group are

plotted by the ASTM method and by the cubic method, for comparison

purposes. As will be shown later the correlation indices are not a

sufficient criterion for the reproducibility.

4.3 Reproducibility Evaluation

In general four methods are used here to evaluate the degree of

reproducibility of the tests in each group, and to compare each group to

the controlled-tests group.

The first method measures the percent overlap area of the mean

of each group with the mean of the controlled tests. This is an area

that may be specified on a certain construction contract. For this

analysis it was assumed that the specification indicates 95% of the

maximum density and 2% of the optimum moisture content of the com­

paction test, as determined by the ASTM D 698 - 64T Method A test. This

is the actual requirement on many contracts. This indicates that any

point within the area bounded by the requirement and the curve would be

acceptable in the field. The boundary of the indicated areas are shown

in Figures 6, 7 and 8.

The overlap area was indicated on each figure and was measured

by a planimeter. The planimeter had a precision of one-hundredth of a

square inch. The average of three readings was recorded as the overlap

area. The measured areas and the computation for this method are shown

Page 40: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(

) p

cf

26

124

122

120

A ST M S T AN D A R D

CUBIC REG RE S SI ON

114

110

M O IS TU R E CONTENT (W ) IN PERCENT

F I G U R E 14 M O IS T U R E D E N S I T Y M EA N CURVES FOR C O N T R O L L E D TESTS P L O T T E D USI NG ASTM STANDARDAND C U B I C R E G R E S S I O N M E T H O D S

tzJO

Page 41: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(Y

d )

pcf

126

24

x122

120

A S T M STANDARD

CUBIC REGRESSION

MOISTURE CONTENT (W) IN PERCENT

FIGURE 15 M O I S TU R E D E N S I T Y M EA N C U R V E S FOR S A N D AND 1 0 % K A O L I N I T E P L O T T E D , USING

A S T M S T A N D A R D A N D CUBIC R E G R E S S I O N M E T H O D S

tzl

Page 42: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(Y

d )

pcf

26

124

22

20

A S T M STANDARD

- - CUBIC REGRESSI ON

M O IS T U R E CONTENT (W) IN PERCENT

FIGURE 16 M O I S T U R E D E N S I T Y M E A N C U R V ES FOR SAND AND 2 % B E N T O N I T E P L O T T E D , USlKlGA S T M S T A N D A R D AND CUBI C R E G R E S S I O N METHODS

wNJ

Page 43: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(Y

d )

pcf

126

124

122

120

A S T M STANDARD

- - CUBIC REGRESSI ON

MOISTURE CONTENT (W) IN PERCENT

F I G U R E 17 M O I S T U R E D E N S I T Y M E A N C U R V E S FOR RANDOM G R ADAT I ON SAND P L O T T E D USING A S T MS T A N D AR D AND CUBIC R EG RE SS ION M ET H OD S

(y4

Page 44: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(X

d )

pcf

26

24

122

120

116 A S T M S T A ND AR D

CUBIC R E G R E S S I O N

5 76 8M O IS T U R E CONTENT ( W ) IN PERCENT

FIGURE 18 M O I S T U R E D EN SI TY MEAN CURVES FOR VARIABLE L A YE R- THI CKNES S COMPACTED SANDP L O T T E D , U S I N G AS T M STANDARD AND CUBIC REGRESSI ON METHODS

Page 45: Reproducibility of soil compaction curve

DRY

DE

NS

ITY

(*

d)

pcf

126

124

22

__J120

ASTM STANDARD

- - CUBIC REGRESSION

105 8 126 7 9 13 14MOISTURE CONTENT (W) IN PERCENT

FIGURE 19 M O I S T U R E D E N S I T Y ME AN CURVES FOR M A N U A L L Y COMPACTED S A N D P L O T T E D , USINGA S T M S T A N D A R D AND CUBI C R E G R E S S I O N M ET HODS

in

Page 46: Reproducibility of soil compaction curve

in Tables A.2, A.3 and A.4 in the Appendix. The overlap area of the

sand-clay mixtures were not compared with the controlled tests on sand,

since they are, essentially, different soils. The results of this

method are presented in Table 1.

The second method assumes that the specification requires 100%

of the maximum dry density. The Arizona Highway Department, for example,

requires 100% of the maximum density for highway base courses, as deter­

mined by the method used in this work. The deviation of the maximum

density of the mean of each group from the mean of the controlled tests

is determined. This is expressed as a percent of the maximum density of

the mean of the controlled tests. The results for this method of

analysis'are also presented in Table 1.

The third method measures the standard deviation of the overlap

area of the curves within each group. The results are presented in

Tables 1 and 2. The fourth method measures the standard deviation of

the maximum densities of the curves within each group. The results for

this measure of the reproducibility are also shown in Tables 1 and 2.

The maximum density of each group as well as the optimum

moisture content are also presented in these tables for comparison

purposes. Whenever possible the reproducibility results for the cubic

and ASTM methods were compared. The cubic curves for individual tests

were plotted only for the controlled group, as shown in Table 2.

4.4 Moisture Content Patterns

The nonuniformity of moisture content within the compacted

specimen causes different degrees of compaction in the layers. The

Page 47: Reproducibility of soil compaction curve

TABLE 1. Reproducibility of Compaction in Terms of Standard Deviation of Each Group and Percent of

Overlap Area of Mean of Each Group from Mean of the Controlled Tests

ASTM METHOD CUBIC METHOD

PARAMETERMax.Yd

pcfO.M.C.

%

&Max.

%

OverlapArea

%

S'.Areas

%

SMax.

%

Max.Yd

pcfO.M.C.

%

AMax. y^

%

Overlap . Area

%

CONTROLLED TESTS 124.0 11.3 0 100 7.7 0.32 123.5 11.3 0 100

RANDOM GRADATION SAND 122.8 11.3 1.0 78 4.9 0.14 122.2 11.3 1.0 75

VARIABLE LAYER THICKNESS SAND 122.8 11.3 1.0 79 10.0 0,28 121.8 11.3 1.4 72

MANUALLY COMPACTED SAND 126.3 10.5 1.9 50 5.2 0.23 125,6 10.5 1.7 52

Page 48: Reproducibility of soil compaction curve

TABLE 2, Effect of Plasticity on Reproducibility of Compaction Curve in Terms of Standard Deviation

for Each Parameter

ASTM METHOD CUBIC METHOD

PARAMETERP.I. Max.

Ydpcf

O.M.C.%

SAreas

%

S : Max.

% .

Max.Yd

pcfO.M.C.

%

SAreas

%

SMax.

%

CONTROLLED TESTS NP 124.0 11.3 7.7 0.32 123.5 11.3 7.8 0.27

SAND + 10% KAOLINITE 8 124.7 10.3 7.9 0.30 123.7 11.3 4.2 0.18

SAND + 2% BENTONITE 14 121.8 11.5 1.7 0.09 121.1 11.3 4.5 0.24

C/J00

Page 49: Reproducibility of soil compaction curve

39

standard deviation in the moisture contents between the three layers

in each test are presented in Table 3. The maximum standard deviation

value for each test, and the moisture content at which it occurred are

presented in this table. In addition, the layer within which the

largest moisture content occurred per compacted specimen was noted for

possible variation patterns.

4.5 Gradation Change

The reuse of the soil, for all the six to seven data points in

the compaction test, affects the particle sizes. As the soil is reused

some of the particles break into smaller particles. Grain size analyses

were conducted on specimens compacted by both mechanical and manual

compaction. For comparison purposes, these gradation curves are shown

in Figure 20, along with the controlled grain size distribution before

the compaction.

Page 50: Reproducibility of soil compaction curve

40

TABLE 3. Standard Deviations in Layer Moisture Content (Maximum Value

for Each Test)

PARAMETER P.I. O.M.C.%" TEST NO. W% S%

1 8.5 .552 13.7 .43

CONTROLLED TESTS NP 11.3 3 15.6 .534 8.4 .295 12.0 .39

1 12.9 .402 14.0 .50

SAND + 10% KAOLINITE 8 10.3 3 9.8 .364 12.7 ,275 13.5 .26

1 15.8 .322 10.8 .30

SAND + 2% BENTONITE 14 11.5 3 10.2 .344 12.3 .305 16.0 .23

1 11.9 .342 15.0 .23

RANDOM GRADATION SAND NP 11.3 3 9.7 .294 12.4 .305 15.7 .40

1 13.2 .562 15.1 .43

VARIABLE LAYER THICKNESS NP, 11.3 3 13.6 .37SAND 4 16.0 .22

5 11.2 . 56

1 14.6 . 352 6.5 .24

MANUALLY COMPACTED SAND NP 10.5 3 14.1 .244 10.3 .305 12.4 .34

Page 51: Reproducibility of soil compaction curve

100

90

80

70

60

50

40

30

20

10

0

BEFORE COMPACTI ON

■— A F T E R MANUAL COMPACTION

- - AF TE R MECHANI CAL COMPACTION

0.1 1.0G R A I N S I ZE IN MM

2 0 0 140 4 0 20 10 4S T A N D A R D SIZE NUMBER

2 0 E F F E C T OF COMPACTION ON GRADATI ON OF SAND

Page 52: Reproducibility of soil compaction curve

CHAPTER 5

DISCUSSION OF RESULTS

5.1 Comparison of Cubic Model vs. ASTM Method

The curves plotted by the cubic method and the ASTM method are

compared in Figures 14 through 19. The ASTM curves in general have

higher peaks than the cubic curves. Both methods give approximately

the same optimum moisture content except for the sand-kaolinite mixture.

The curves for the controlled tests, random gradation and manually

compacted groups show close correlation. The sand-bentonite mixture and

the variable layer-thickness group show some divergence between the two

methods. Figure 15 indicates the poor correlation between the two

methods for the sand-kaolinite mixture.

The maximum density deviations and the percent overlap areas of

the sand group show very good correlation between the two methods as

seen in Table 1. The standard deviations of the higher plasticity groups

showed poor correlation between the two methods as outlined in Table 2.

It is likely that a higher order model (e.g. a fourth order equation)

would be more representive for plastic soils. However, the additional ̂

computations involved will outweigh the resulting degree of refinement.

For higher plasticity soils. Table 2 shows poor agreement of the

standard deviations for the two methods, while Table A.1 in the Appendix

indicates that the correlation indices for the cubic model are excellent.

' 42

Page 53: Reproducibility of soil compaction curve

43This confirms the fact that was stated earlier that the correlation

index is an overall measure of the fit and not particularly indicative

of the fit at the peak region.

It can be stated that the cubic equation is a valid mathematical

expression for the moisture-density relationship of the well-graded sand

used for this study. However, this model is not representative of soils

whose density is very sensitive to moisture content.

5.2 Controlled Tests

The curves in Figure 3 indicate that, with the degree of control

possible in this study, the reproducibility was not perfect. The

standard deviation of the overlap areas, which is the most representative

indication of the degree of reproducibility of the curve is 7.7%. This

indicates that with this degree of control the test cannot be uniquely

conducted. The standard deviation of maximum density is relatively

small (0.32%). However, the overlap area is more representative of the

type of soil and test conducted than the peak point of the curve, whose

determination depends on the chance of obtaining a data point at that

location of the curve. The large standard deviation of overlap areas

can be attributed to the sensitivity of the area to slight changes in

the optimum moisture content.

Although the degree of reproducibility is not perfect with the

imposed control, nevertheless, it is far better than that obtained for

a fine sand by other researchers (6). The deviation of maximum density

for that research was almost four times that obtained with the controlled

tests in this study. In the above mentioned research (6) the results

Page 54: Reproducibility of soil compaction curve

44

were obtained by five operators, and the control was much less than in

the present study. The optimum moisture contents did not appreciably

vary in this study. This indicates that the compactive energy did not

change during the course of the five controlled tests.

5.3 Plasticity

The standard deviation values for the maximum dry density and

the overlap areas for the sand-kaolinite and the sand-bentonite mixtures

are compared with the controlled tests in Table 2. The degree of

reproducibility of the tests greatly improves with the sand-bentonite

mixture. This is not the case with the sand-kaolinite mixture, which

had a lower plasticity.

The bentonite (predominantly montomorillonitic) has a greater

surface area and plasticity than the kaolinite and is more sensitive to

water. However, the density of the sand-kaolinite mixture proved to be

more sensitive to moisture variations than the density of the sand-

bentonite mixture, as seen in Figures 15 and 16, The larger portion of

kaolinite (10%) as compared to the bentonite portion (2%) in the mixture

is probably the cause of this sensitivity. This larger portion of fines

does also account for the larger maximum densities of the kaolinite

group.

The test results indicate that the degree of reproducibility of

the higher plasticity groups is influenced by the mineral component and

the percentage of fine particles more than the plasticity indices. The

results show that the optimum moisture contents did not exhibit appreci­

able variations.

Page 55: Reproducibility of soil compaction curve

45

5.4 Gradation Effect

The standard deviations for this group are less than that of the

controlled tests as seen in Table 1. This is opposite to what should be

expected. However, in comparing Figures 3 and 6, it can be seen that,

with the random gradation group a larger number of points fall outside

the smoothly drawn curves than with the controlled tests. This points

out the degree of bias introduced by the ASTM method of plotting the

curves.

Figure 9 indicates that the random gradation sand had a lower

maximum density than the controlled tests, and this is reflected in the

overlap area of 78% as shown in Table 1. This is due to a larger per­

centage of finer particles (about 2%) in the controlled tests as

compared with that in the random gradation. Method of preparing the

controlled gradation sand introduced the larger percentage of finer

particles.

The results here show that a slight change in the gradation from

the controlled tests causes the area overlap to be reduced to 78%. This

indicates that the reproducibility of the curves is sensitive to small

gradation changes. The optimum moisture contents did not vary appreci­

ably in this group.

5.5 Layer-Thickness Effect

Table 1 indicates that the standard deviation of overlap areas

increased to 10%, as compared to 7.7% for the controlled tests. Further­

more, the overlap area of this group is 79% when compared with the

controlled test group. There are small variations in the optimum

Page 56: Reproducibility of soil compaction curve

46moisture contents between the tests in this group, as seen in Figure 7.

These variations in optimum moisture contents are more responsible for

reducing the degree of reproducibility than the small change in the

maximum densities. These variations in the optimum moisture content can

be attributed to the nonuniformity in the moisture content of the layers

(see Table 3), which was due to the variations in layer thicknesses.

The standard deviation of maximum density is small but that is

not a very good indication of the relationship as indicated earlier.

Therefore, it can be stated that variation in layer-thickness, within the

normal limits accepted in practice, significantly influences the degree

of reproducibility.

5.6 Manual Compaction

This factor has the greatest effect on the degree of repro­

ducibility of sand than any other group, when compared to the controlled-

tests group. Table 1 shows that the overlap area is 50%, and the

deviation of the maximum density is 1.9% from that of the controlled

tests group. The density of this method is greater than the controlled-

jtests group by the indicated percent, as seen in Figure 13.

These results suggest that the manual tamper applied greater

compactive energy to the sand specimens than the mechanical tamper

(controlled tests). This point is further confirmed by the results of

the gradation analysis of Figure 20 and the lowering of optimum moisture

contents as indicated in Table 1. Similar results were found during the

earlier research on a sandy soil (6). The 1.9% increase in the maximum

density by the use of manual compaction is very close to the 1.7%

Page 57: Reproducibility of soil compaction curve

47increase obtained in that earlier research. The larger energy applied

causes the greater breakdown of particles; the higher density; the lower

optimum moisture content; and consequently decreases the degree of repro­

ducibility of this group of tests, when compared with the controlled-

tests group.

The greater density obtained by the manual tamper may be

attributed to one or more of the following factors:

(a) The application of the load is not completely vertical in

manual compaction, and thus has a horizontal component.

This may have a kneading effect that will increase the

density.

(b) The drag effect of the cable of the mechanical tamper could

reduce the compactive energy of this method.

(c) The poor adjustment of the free fall, among other

factors, also may influence the energy transmitted in the

compact ion test.

The standard deviation of areas for this group is 5,2% as

compared with the 7.7% of the controlled-tests. The greater uniformity

of moisture content in the three layers (Table 3); the larger percentage

of the fines; and the increased energy are probable causes for the

improvement of reproducibility within this group.

5.7 Moisture Content Patterns

The maxima of the standard deviations for the layer moisture

contents are presented in Table 3. It is observed that the large

Majority (70%) of the maximum deviations take place on the wet-side of

Page 58: Reproducibility of soil compaction curve

48

the optimum. In this region the water has a higher potential mobility

under the application of tamper loads. This may account for the larger

deviations observed in that region."

The moisture content for each data point was computed as the

arithmetic mean of the moisture content of the three layers. As a

result of the greater deviations in the layer moisture contents the data

points are less dependable on the wet-side of the optimum than on the

dry-side of the optimum. This suggests that, in the case of divergence

of the data points from the smooth curve, more weight should be given

to the points on the dry-side of the optimum.

There was no definite pattern indicating which layer has the

maximum moisture content. However, in about half of the tests the

middle layer was observed to have the greatest moisture content of the

three layers. The maximum variation in layer moisture content was

1.1%.

Page 59: Reproducibility of soil compaction curve

CHAPTER 6

. CONCLUSIONS

6.1 Summary

This study was initiated with the aim of determining the

influence of a number of parameters on the degree of reproducibility of

the compaction curve of soils. It was also intended that this degree of

reproducibility would be measured in a statistical manner, and that

mathematical expressions for the compaction curve would be investigated.

The following conclusions can be drawn from this study:

1. The standard deviation and the percent overlap area were

determined to be valid statistical methods of measuring the

degree of reproducibility.

2. Absolute reproducibility is not obtainable with the degree of

control possible with the present methods of test.

3. The degree of reproducibility increased sharply when 2% bentonite

was added to the sand.

4. Reasonable variations in layer-thickness decreased the degree

of reproducibility.

5. Reproducibility is sensitive to a small change in gradation.

6. Reproducibility showed no appreciable change when 10% kaolinite

replaced the finer particles in the soil.

49

Page 60: Reproducibility of soil compaction curve

50

7. Manual compaction increases the maximum density as compared to

mechanical compaction. Manual compaction shows poor correlation

as determined by the controlled tests.

8. The reproducibility of the manual compaction (within its group)

was better than that of the mechanical compaction.

9. The maximum deviation in the layer moisture contents generally

occurs on the wet-side of the optimum moisture content.

10. The cubic equation is a good approximation of the moisture-

density relationship of the well-graded sand used in this

research. It is probable that the cubic equation or a

modification of it can be used as the moisture-density curve

equation for any well-graded sand.

11. For high plasticity soils, this cubic expression is not a valid

representation of the moisture-density relationship.

12. Manual compaction and variations in layer-thickness (in that

order) have the largest influence on the reproducibility. These

parameters should be controlled during the compaction tests if

reproducible results are to be expected.

6.2 Future Research

From the analysis of the results of this research the following

suggestions are made for future research:

1. The effect of plasticity should be further studied by using only

one type of clay mineral, to isolate the independent effect of

plasticity on reproducibility.

Page 61: Reproducibility of soil compaction curve

The effect of compaction method on the reproducibility should

be studied.

The number of tests conducted to study the degree of repro­

ducibility should be increased.

The causes of the greater energy transmitted to the soil with

the manual tamper, as compared to the mechanical tamper, should

be investigated.

Page 62: Reproducibility of soil compaction curve

APPENDIX

LEAST SQUARES SOLUTION FOR THE PARAMETERS OF A CUBIC POLYNOMIAL

MODEL:

DE = A BW CW2 * FW3

WHERE:

Dg = Expected Value of Dry Density

W = Moisture Content

SUM OF SQUARES 2

2 N o N5 = 2 , (D:. - D ) = V (D. - A - BW - CW - FW )

i=l 1 h i=l 1

WHERE:

D^ = Observed Value of Dry Density

N = Number of Observations

MINIMIZE S2 :

Page 63: Reproducibility of soil compaction curve

as N0 = 2 % (D. - A - BW - CWZ - FW3)(~W2)

SC" i=l 1

(A. 3) 0 = % ^ " A f ̂ ” B % W3 - C f W4 - F f W5i=l i=l i=l 1=1 1=1

as3F"

= 0 =N2 I 1=1 1

A - BW - CW FW3)(-W3)

(A. 4) 0 =N N _ . N . N ' N ,I D.W - A % W - B I W - C % W - F % W

1=1 1=1 1=1 1=1 1=1

CLEARING A FROM EQUATIONS A.l AND A.2 AND ADDING:

r N N N -I N _ ( N X2'0 = I Dj. I W - N y D.W + B N I W - I w. 1=1 1 1=1 i=l 1 . 1=1 '1=1 /

N N N ,q r N N N -1(A.5) ♦ C N y w - I w y w ❖ F. n y w -■ I w % w3

i=i 1=1 i=i i=i 1=1 1=1

CLEARING A FROM EQUATIONS A.2 and A.3 AND ADDING:

N N „ N N -I N N „ / N _\2l0 = I D.W I W - 1 W % D.W * B, I w y w .■ Iw1=1 1=1 1=1 1=1 1=1 i=i '1=1 ^

(A. 6) + Cr N N . N _ N _I W I w4 - I w2 % w3

1=1 1=1 1=1 1=1

CLEARING A FROM EQUATIONS A.3 AND A.4 AND ADDING

N N . N „ N I W % w5 - I W2 % w 1=1 1=1 1=1 1=1

0 =r N N N _ N _

y d .w y w3 - y d .w 3 y w2.1=1 1 i=i i=i 1 i=i

+ B N .,2 r ..,4 NI r i r . i t

Li=l 1=1 \l=l

(A. 7) * CN „ N- N _ N ..% w2 % w5 - I w3 I w4 1=1 1=1 1=1 1=1

4- F - N 2 v ..,6 N 3 % ,.,51% w % w - % w % w1=1 1=1 1=1 1=1 .

Page 64: Reproducibility of soil compaction curve

54WHEN:

N N NI D I W - n y

1=1 1=1 1=1

. r 2 f ? \ 2S5 N 2 w - y w

1=1 U = 1 /

N N NS n y w - I w y

1=1 1=1 i=i

N 4 N NS n y w4 - I w y

i=i 1=1 i=i

N N Nes I d w y w2 - y

i=i 1 i=i i=i

N= I WNI w3 - ( ! w2)2

1=1 1=1 \i=i jN= I W

NI w4 N - N- y w2 y1=1 1=1 1=1 1=1

N- I w NI w5 N N- 1 "2 I1=1 1=1 1=1 1=1

N - 1 Diw2 N

I_ N

w - y d .w 3 T w2

N= I w2Ny w4 -f ? w3)21=1 i=i \i=l )

N. - 1 w2

NI w5 -N „ NI w3 I w4

1=1 1=1 1=1 1=1N- I w2

NI w6 -N „ NI W3 I w5

1=1 1=1 1=1 1=1

Page 65: Reproducibility of soil compaction curve

55THUS:

+ BR2 * CR3 + FR4 = 0 (A.8)

S1 + BS2 + CS3 + FS4 = 0 (A.9)

Pj + BP2 + CP3 + PP4 = 0 (A.10)

CLEARING B FROM EQUATIONS A.8 AND A,9 AND ADDING:

(R1s 2 - r 2s1) + c (r3s 2 - r 2s 3) + f (r4s2 - r 2s4) = 0 (A.11)

CLEARING B FROM EQUATIONS A.9 AND A.10 AND ADDING:

CS1P2 - W + C(S3P2 - S2P3̂ + p (S4P2 - S2P4) = 0 (A.12)

WHEN:

Ql * R1S2 - R2S1

^2 = R3S2 “ R2S3

^3 = R4S2 " R2S4

^4 = S1P2 “ S2P1

% " S3P2 ~ S2P3

% " S4P2 - S2P4

THUS:

Qx + CQ2 + FQ3 = 0 (A.13)

Page 66: Reproducibility of soil compaction curve

56

Q4 + CQ5 * FQ6 = 0. (A„14)

CLEARING C FROM EQUATIONS A.13 AND A.14 AND ADDING:

„ Q2 % - ^ 5' % - ^ 2 %

SOLVING FOR C IN EQUATION A.13:

FQ3 + Q,

SOLVING FOR B IN EQUATION A.8:

CR + FR, = R.B =

R2

SOLVING FOR A IN EQUATION A.l:N N . N 0 N -^ D. - B £ W - C I W - F I W

& i^l 1 1=1 1=1 1=1= , — - ,

CORRELATION INDEX (R):N „

2 A ̂ ̂R = 1.0 N ,I (Dj, - D)2 1=1

WHERE:

N

STANDARD DEVIATION (S):N „I (Di - D)2

S = 1=1 1N - 1

Page 67: Reproducibility of soil compaction curve

57

TABLE A.I. Cubic Regression Coefficients and Correlation Indices, forMoisture-Density Curves.

Parameter P.I. Test No. A B C F R2

Controlled TestsNP

12345

122.53120.53 115.51 111.24 109.96

-4.688-4.317-2.614-1.034-1.094

.855

.852

.640

.453

.513

-.038 -.039 -.031 -.024 - -.028

.972

.967

.956:

.981

.984Sand + 10% Kaolinite

8

12345

78.4561.6345.2489.7767.55

6.55310.05715.9082.7079.198

-.048 -.259 -.905 .356

-. 297

-.015 - .013 .010

-.029 -.007

.961

.981

.986

.969

.959

Sand t 2% Bentonite

w::12345

112.4757.1399.0799.8296.57

-2.2308.9742.4971.8672.950

.581-.499.082.167.056

-.028.006

-.012-.015-.011

.995

.977

.954

.959

.975

Controlled Tests NP; 114.39 -2.155 .594 -.029 .953

Sand +■ 10% Kaolinite 8 68.47 9.168 -. 285 -.008 .946

Sand * 2% Bentonite 14 m©> 89.53 5.104 -.155 -.005 .949

Random Gradation Sand NP 1 122.45 -4.529 .775 -.033 .940

Variable Layer- Thickness Sand NP 1a 113.38 -1.508 .452 -.022 .939

Manually Compacted Sand NP 114.69 -1.347 .551 -.031 .950

Page 68: Reproducibility of soil compaction curve

58

TABLE A.2. The Deviations of Maximum Density and the Percent OverlapArea from the Mean of the Same Parameter.

Max. Overlap A Overlap Ave. A Ave. ofParameter P.I. Test No. Yd Area Max. y. Area Max. y , Overlap

. pcf Inches % d % % Areas %

Controlled 1 124.1 3.70 0.1 91Tests 2 125.0 3.23 0.8 79

NP 3 124.2 3.83 0.2 94 0.3 894 123.8 3.40 0.2 845 124.0 4.01 0.0 98

Mean 124.0 4.07 - -

Sand + 10% 1 125.6 2.83 0.7 80Kaolinite 2 124.8 3.43 0.1 97

8 3 124.3 3.37 0.3 96 0.4 924 124.6 3.48 0.1 995 123.8 3.10 0.7 88

Mean 124.7 3.52 - -

Sand + 2% 1 121.7 3.74 0.1 93Bentonite 2 121.7 3.76 0.1 93

14 3 122.0 3.78 0.2 94 0.1 944 121.8 3.76 0.0 935 121.8 3.93 0.0 97

Mean 121.8 4.03 - -

Page 69: Reproducibility of soil compaction curve

59

TABLE A.3. The Deviations of Maximum Density and the Percent OverlapArea from the Mean of the Same Parameter.

Max. Overlap A Overlap Ave. A Ave. ofParameter Test No. Yd Area Max. v,i Area Max. y. Overlap

. P cf . Inches % d % % Areas %

Random Gradation 1 123.2 3.50 0.3 86Sand 2 123.0 3.88 0.2 95

3 122.8 3.54 0.0 87 0.1 914 122.6 3.68 0.2 905 122.8 3.97 0.0 97

Mean 122.8 4.08 - -

Variable Layer- 1 122.6 3.88 0.2 95Thickness Sand 2 122.0 3.15 . 0.6 77

3 123.0 3.92 0.2 96 0.4 . 894 122.6 4.00 0.2 985 123.8 3.25 0.8 79

Mean 122.8 4.10 - -

Manually Compacted 1 126.5 3.92 0.2 94Sand 2 127.2 3.37 0.7 81

3 126.6 3.72 0.2 89 0.4 864 125.6 3.45 0.6 835 125.7 3.57 0.5 85

Mean 126.3 4.18 - -

Page 70: Reproducibility of soil compaction curve

60

TABLE A.4. The Deviations of Maximum Density and the Percent OverlapArea from the Mean of the Controlled Tests.

Parameter Test No.Max,YS'

OverlapAreaInches

AMax. y ,

% d

Overlap Ave. A Ave. of Area Max. y. Overlap

% % Areas %

Random Gradation 1 123.2 3.17 0.6 78Sand 2 123.0 3.23 0.8 79

3 122.8 2.98 1.0 73 0,9 754 122.6 2.90 1.1 715 122.8 3.07 1.0 75

Mean 124.0 4.07 - -

Variable Layer- 1 122.6 2.94 1.1 72Thickness Sand 2 122.0 2.42 1.6 60

3 123.0 3.32 0.8 82 1.0 764 122.6 3.14 1.1 775 123.8 3.61 0.2 89

Mean 124.0 4.07 - -

Manually Compacted 1 126.5 1.94 2.0 48Sand 2 127.2 1.46 2.6 36

3 126.6 1.73 2.1 43 1.9 484 125.6 2.29 1.3 565 125.7 2.24 1.4 55

Mean 124.0 4.07 - -

Page 71: Reproducibility of soil compaction curve

REFERENCES

1. Arizona Highway Department. "Manual of Compaction Control Methods,"Phoenix, Arizona, 1963.

2. American Society for Testing Materials. "Compaction of Soils,"Special Technical Publication No. 377, 1964.

3. American Society for Testing Materials. "ASTM Standards," Part 11,1966.

4. Grim, R. E. Clay Mineralogy, McGraw-Hill, 1953.

5. Highway Research Board. "Symposium on Compaction of Earthwork andGranular Bases," Highway Research Record No. 177, 1967.

6. Johnson, A. W., and J. R. Sallberg. "Factors Influencing CompactionTest Results," Bulletin No. 319, Highway Research Board, 1962.

7. Kell, T. R. "The Influence of Compaction Method on Fabric ofCompacted Clay," unpublished Master's Thesis, The University of Arizona, 1964.

8. Lambe, T. W. Soil Testing for Engineers, John Wiley 8 Sons,Inc.,Tenth Printing, 1965.

9. Proctor, R. R. "Design and Construction of Rolled Earth Dams,"Engineering News Record, August 31, September 7, 21, 28, 1933.

10. Seed, H. B., J. K. Mitchell, and C. K. Chan. "The Strength ofCompacted Cohesive Soils," American Society of Civil Engineers, Proceedings: Research Conference on Shear Strength of CohesiveSoils, Boulder, Colorado, pp. 877-964, 1960.

11. Turnbull, W. J. "Field Investigation, Technique of FieldObservation Including Compaction Control, Soil Stabilization," Proceedings: Third International Conference on Soil Mechanicsand Foundation Engineering, Vol. II, pp. 319-333, Switzerland, 1953.

61