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    TRAINING REPORT

    OF

    PHASE 1AT PARAMOUNT LTD, VADODARA

    SUBMITTED AS A PARTIAL FULFILLMENT TOWARDS THE

    BACHELORS DEGREE IN THE FIELD OF CHEMICAL ENGINEERING.

    PREPARED BY:

    ARPIT D THUMAR.

    (ID-064060)

    DEPARTMENT OF CHEMICAL ENGINEERING

    FACULTY OF TECHNOLOGY,

    DHARMSINHDESAIUNIVERSITY,

    COLLEGE ROAD, NADIAD-387001

    JANUARY 2013

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    PREFACE

    Theory of any subject is important but without its practical knowledge it becomes useless for

    the technical students. A technical student cannot be a perfect engineer or technologist

    without practical understanding of the scenario of the branch. Hence this training provides a

    golden opportunity for all the students.

    The principle objective of the training report is to get details about the operation

    process & operation condition which are carried out in the industries and more about theequipment used in the chemical industries. Thus it is important for every person to be

    exposed to training in some kind of an industry or other to enhance ones knowledge.

    In the context, our college Dharmsinh Desai University, Nadiad arranges an Industrial

    Training Program.

    Prepared by:

    ARPIT D THUMAR

    B.Tech.Chemical (8th

    Semester)

    D.D.U, Nadiad

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    ACKNOWLEDGEMENT

    This training report takes effort, hard work and time. Many people are involved in it directly

    or indirectly during the course of my training work I have been guided by many. It is my

    sincere desire to express thanks for their guidance and support.

    I would like to take this opportunity to thanks Mr. SAMIR TULI (MANAGING

    DIRECTOR) and Mrs. MANJU PILLAI (Manager) for their guidance.

    I am also thankful to

    Mr. RITESH H ANASANE (Deputy Manager, HYDROCARBON SECTION)

    Ms. KHAYTI SHAH (Chemist)

    Mr. RAMESH SINGH (Process engineer)

    Last but not the least I would like to thank head of department of Chemical Engineering-

    Dharmsinh Desai University, Dr. PREMAL SHUKLA for sending me to such a reputed

    company which has really helped me in boarding the horizon of my knowledge and I am also

    thankful to my guide Assistant Professor HITESH PANCHAL for giving me such a great

    guidance.

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    6.1 PRESSURE MEASURING INSTRUMENTS

    6.2 FLOW MEASURING INSTRIMENTS

    6.3 TEMPERATURE MEASURING INSTRUMENTS

    6.4LEVEL MEASURING INSTRUMENTS

    7 PFD 30

    7.1 INTRODUCTION

    7.2 PFD WILL CONTAIN

    7.3 PFD WILL NOT INCLUDE

    7.4 STANDARDS

    7.5 TRACING OF LINES

    8 BASICS OF P&ID 32

    8.1 LEGENDS

    8.2 P&ID

    8.3 CHECKLIST FOR HEAT EXCHANGER

    8.4 CHECKLIST FOR PUMPS

    9 PUMP HYDRAULICS 43

    9.1 DEFINITION

    9.2 EXAMPLE

    9.3 NPSH

    9.4 SAMPLE CALCULATION

    10 R&D PARAMETERS 49

    10.1 DEFINITION

    10.2 GPCB NORMS

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    WORLD BANK etc.

    The Manufacturing Unit of PARAMOUNT is fully equipped with the most modern

    machinery & facilities to manufacture wide range of equipment. In-house facilities for testing

    & inspection make it completes to produce high quality equipment. PARAMOUNT

    Manufacturing facilities are approved by most of leading consultants. PARAMOUNT also

    exports some systems and equipment that are exported to Far East Countries as well as USA.

    During last two decades PARAMOUNT have designed and executed over 200 installations,

    in all the related fields referred above. It is worth mentioning that some of these installations

    include tertiary treatment of waste water, for using it for industrial purposes such as cooling,

    feed to DM or R.O. Plant to produce water of ultra-fine quality.

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    1.1 Products:

    In Effluent & Waste Water Treatment we undertake the turnkey execution of complete

    treatment plants, from concept to commissioning. The equipments & systems we offer

    are Advanced Oil/Solid Separation Systems (Tilted Plate Interceptors), D.M.Plants,

    Reverse Osmosis & Ultrafiltration Systems. We indigenously manufacture & supply the

    whole range of equipments like Clarifiers, Clariflocculators, Surface Aerators,

    Agitators/Flash Mixers, Thickeners, Dissolved Air Flotation Units and Plastic Media for

    Bio-Towers, Bio-Tower etc.

    1.2 Competitors:

    UPL ENVIORNMENTAL ENGINEERS LIMITED

    KADAM ENVIORNMENTAL CONSULTANT

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    2. PROCESS ENGINEERING:

    In paramount process engineering which includes tendering activities, basic engineering and

    detail engineering activities.

    2.1 In general the basic engineering documents consist of following:

    1. Introduction/coversheet

    2. Design basis

    3. Treatment philosophy/treatment scheme

    4. Process description

    5. Products of treatment

    6. Equipment list

    7. Utilities & chemical composition

    8. Unit size calculations-Equipment sizing

    9. Hydraulic calculations-Pumps

    10. Process datasheet for Equipments

    11. Process datasheet for Pumps

    12. Process datasheet for Instruments

    13. Process flow diagram

    14. Legend sheet and P&ID

    15. Layout

    16. Hydraulic flow diagram

    17. Hydraulic calculation-Gravity

    18. Process control narrative

    2.2 Activities involved during detail engineering are following:

    1. Updating BEP documents as and when required

    2. General Arrangement drawing

    3. Line schedule

    4. Updating datasheet for MR/PR

    5. MR/PR activities

    6. Operation & maintenance manual

    7. As built documents and drawings

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    3. PIPING CLASS & MOC SELECTION GUIDELINES:

    3.1 Check list for material selection:

    1. Properties of material (corrosion, mechanical, physical, appearance)

    2. Ease of fabrication

    3. Compatibility with existing equipment

    4. specification coverage

    5. Availability of design data

    6. Expected total life of plant or process

    7. Estimated service life of material

    8. Reliability (safety and economic consequences of failure)

    9. Need for further testing

    10. Material and its fabrication cost

    11. Return on investment analysis

    12. Maintenance and inspection cost13. Comparison with other corrosion control methods

    14. Availability and delivery time

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    3.2 Selection of material based on application/Fluid/Service:

    MATERIAL ENVIORNMENT

    Aluminium Water and steam, NaCL, sea atmosphere

    Copper alloys(Brass) Ammonical solutions, amines, mercury-salt

    solutions

    Austenitic stainless steels Chlorides, including FeCl2,FeCl3,NaCl,sea

    enviornments,H2SO4,flurodies,condensing

    steam from chloride waters

    Ferritic stainless steels Chlorides, NaCL, fluorides, bromides,

    iodides, caustics, nitrates, water steam

    Carbon and low alloy steels HCL, caustics, nitrates,HNO3,HCN,H2S,

    H2SO4,sea water

    High strength alloy Sea and industrial environments

    Magnesium alloys Tap water, sodium chloride solutions

    Lead Lead acetate solutionsNickel Bromides, caustics, H2SO4

    Monel Fused caustic soda, hydrochloric and

    hydrofluoric acids

    Titanium Sea environments, NaCL in environments

    288 C, silver and AgCl, fuming HNO3,

    chlorinated or fluorinated hydrocarbons

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    3.3 Selection of material based on different concentrations of solutions:

    METALS H2SO4 H2SO4 NaHSO4 NaHSO3 HCL HCL HNO3 HNO3 HF NaoH

    CONC,, DILUTE SOLUTION SOLUTION CONC. . DILUTE CONC.. DILUTE 50% 50%

    1 TANTALUM A A A A A A A A X X2 ALLOY 20 A A A A X X A A B B

    3 HASTELLOY B A B B C A B X X B A

    4 HASTELLOY C A B A A B A B A A B

    5 S.S-316 B B B B X X A A C A

    6 S.S-304 C C C C X X A A X A

    7 CR-SI STEEL A A A X B A B B X C

    8 CARBON STEEL B X X X X X X X X A

    9 BRASS X C C C X X X X X C

    10 COPPER C B B B X C X X B B

    11 ALLUMINIUM C C C B X X C X X X

    A=EXCELLENT,B=GOOD,C=FAIR,D=UNSATISFACTORY

    3.4 Piping material specification index:

    SR NO PIPING LINE RATING CA MATERIAL

    1 A19A 150 3 CARBON STEEL

    2 A1K 150 0 SS304

    3 A1Z 150 0 HDPE

    4 A22N 150 1.5 SS316

    5 A2A 150 1.5 CARBOON STEEL

    6 A3A 150 1.5 CARBOON STEEL

    7 A3Y 150 0 RUBBER LINED CS

    For example:

    A3A

    1) FIRST LETTER : RATING e.g. A-150 class

    2) MIDDLE NUMBER : CORROSION ALLOWANCE e.g.1.5 (mm required as CA)

    3) THIRD LETTER : MATERIAL e.g. A-carbon steel

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    4. VALVES:

    4.1 Definition:

    A valve is a mechanical device that controls the flow of fluid and pressure within a system by

    performing any of the following functions:

    Stopping and starting fluid flow

    Varying the amount of the fluid flow

    Controlling the direction of the fluid flow

    Regulating downstream system or process pressure

    Receiving component or piping over pressure

    Plug and Globe valve

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    4.2 Valve types and application:

    SR.NO. VALVE TYPE ADVANTAGES DISADVANTAGES APPLICATION

    1 GATE VALVE Low pessure drop when, Gate valves have slow - Gate valves are used primarily

    fully open and tight sealing. response characteristics and for on-off application.

    require large actuating forces. they are suited for high temp.

    It causes vibration,seat and &pressure with wide variety

    disc wear in partial open of fluids.they are not normally

    condition. used for slurries,viscous fluids.

    2 GLOBE VALVE Faster to open or close,most High pressure drop compare Globe valves are used primarily

    reliable form of sealing, to gate valve. for throttling purposes.

    throttling to control the flow globe valve may be consider

    to any desired degree and a general purpose flow control

    positive shut off. valve specifically used for

    high temperature applications.

    3 PLUG VALVE Normally small in size - operating torque is quite high. Plug valves are extensively

    requires less head room and lubricated plug valves require used in refinery ,petrochemical

    available in wide range of periodic lubrication and lubri- and chemical industries.

    materials.they provide tight cant may react with the fluid it is also used for on-off service.

    shut off,quick opening and being carried.

    low pressure drop.

    4 BALL VALVE Low pressure drop,tight shut- Fluid trapped in the ball in the Ball valves are used in a wide

    off,quarter turn operation, closed position may cause range of applications including

    easy to maintain,low torque. problem of build up of vapour flow control,pressure control

    they are small in size and low pressure and corrosion. and shut off.they are used for

    in weight. corrosive fluids,cryogenic liquid

    very viscous fluids and slurries.

    These valves are also used in

    refinery,petrochemical andLPG application due to bubble

    tight shut off.

    5 BUTTERFLY Simple,compact form,Quick Seals may be damaged if the Mainly used in low pressure

    VALVE Opening,good controllability velocity is high.Usually require applications where leakage

    low pressure drop ,low high actuating forces,limited is relatively unimportant.

    weight and cost. to low pressure and elasto- it is now widely being used

    mer limits the temperature. in majority of process

    applications.

    SR NO VALVE TYPE ADVANTAGES DISADVANTAGES APPLICATION

    6 DIAPHRAGM The diaphragm completely For high pressure application Due to its economy,the

    VALVE keeps the working parts in the valve operation is quite diaphragm valve finds a vastisolation from process difficult. application for handling and

    liquids. corrosive liquids at low temp-

    earature.and they are also

    used fertilizer,chemical

    industry,water treatment

    plants.

    7 CHECK Minimizes water hammer The pressure drop across the Extensively used in process

    VALVE and avoids reverse flow. valve is quite high and after industry for avoiding the back

    continuous operation the flow and for piping with steam

    composition of the seat gets handling.

    disturbed re adjustment is

    very difficult.

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    4.3 Valve selection process:

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    4.4 Control valve:

    Process plants consist of hundreds, or even thousands, of control loops all networked together

    to produce a product to be offered for sale. Each of these control loops is designed to

    keep some important process variable such as pressure, flow, level, temperature, etc. within a

    required operating range to ensure the quality of the end product. Each of these loops receives

    and internally creates disturbances that detrimentally affect the process variable, and

    interaction from other loops in the network provides disturbances that influence the process

    variable.

    To reduce the effect of these load disturbances, sensors and transmitters collect information

    about the process variable and its relationship to some desired set point. A controller then

    processes this information and decides what must be done to get the process variable back to

    where it should be after a load disturbance occurs. When all the measuring, comparing, and

    calculating are done, some type of final control element must implement the strategy selected

    by the controller. The most common final control element in the process control industries is

    the control valve. The control valve manipulates a flowing fluid, such as gas, steam, water, or

    chemical compounds, to compensate for the load disturbance and keep the regulated process

    variable as close as possible to the desired set point.

    4.4.1 Loop for ON/OFF valve:

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    4.4.2 Loop for control valve:

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    5. PUMPS:

    Definition:

    Pump is a device that imparts energy to a fluid passing through it to enable the fluid to move

    from one point to another.

    In practice, pumps change both the velocity and the pressure passing through them.

    Pumps fall into two broad classes:

    1) Positive Displacement Pumps

    2) Rotor dynamic Pumps

    5.1 Positive Displacement Pumps:

    Working Principles:

    1. Fluid is displaced from the suction to the discharge by the mechanical variation of the

    volume of chamber or chambers at every stroke or rotation of the pump

    2. Volume of pump chamber alternately increases to draw the liquid in from suction pipe& then decreased to force the liquid out into the delivery pipe

    3. This may be done by either a reciprocating motion of a piston or by a rotary motion of

    specially designed vanes, gears or screws

    Characteristic:

    1. Self-priming

    2. All the valves at the discharge side of the pumps must be kept open prior starting

    3. Failure to do so will cause rapid increase of fluid pressure, leading to failure at the

    weakest point in the system

    4. Relief valve is always fitted in the system to avoid such failure

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    Subdivided into Two main categories:

    1. Reciprocating Pumps

    - Where plunger or piston is reciprocated in a fluid cylinder

    - Suitable for delivering small quantities at high pressure

    2. Rotary Pumps ( Gear, Screw, Vane pumps )

    - Where the liquid is forced through the pump casing by means of screws, gears or vanes

    - used for delivering moderate quantity at moderate pressure

    5.1.1 Reciprocating Pump:

    Main Components:

    1. Cylinder

    2. Piston

    3. Piston rod

    4. Gland

    5. Suction valve

    6. Discharge valve

    Pump may be of Single acting or Double acting type

    Single Acting Reciprocating Pump:

    1. There is one suction & one discharge per cycle

    2. Piston moves down during suction stroke

    3. Causes low pressure to create & fluid to flow into cylinder by opening suction valve

    4. Piston moves up during discharge stroke

    5. Causes fluid to be compressed and pressurised

    6. Discharge takes place by opening discharge v/v by high pressure fluid

    SUCTION STROKE DISCH STROKE

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    5.1.2 Gear Pump:

    1. It is a positive displacement pump

    2. It consists of two meshing gears with one driving the other

    3. Fluid flows between the casing and the gear teeth

    4. Commonly employed for lube & fuel oil transfer

    5. Must have relief valve installed in the system

    5.1.3 Screw Pump:

    1. Screw pumps are positive displacement pumps

    2. Screws are meshed together with one driving other

    3. Fluid is displaced through the recesses between the screws and the casing

    4. May have single, double or triple screws

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    5.1.3 Vane Pump:

    1. Vane pumps are positive displacement pumps

    2. Rotors having slots for vanes

    3. Centre of rotor is eccentric with casing

    4. This causes vanes to move in and out as the rotor rotates

    5. Causes change in volume in the respective chamber, similar to reciprocating pump

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    5.2 Roto dynamic Pumps:

    1. Often Known as dynamic pumps or centrifugal pumps

    2. Centrifugal pumps are more suitable for delivery of large quantities at low discharge

    pressure

    3. Are Non-self-priming pumps

    4. Loses suction and unable to pump once air gets into the pump system

    5. Must be primed before starting

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    Centr if ugal Pump:

    Main Components:

    1. Impeller

    2. Impeller wear ring

    3. Volute Casing

    4. Shaft

    5. Ball bearing

    6. Gland

    Working Principle:

    1. Impeller rotates at high speed

    2. Fluid enters through the eye of the impeller

    3. Fluid is thrown by centrifugal force from the centre (suction side) radially outwards to

    the periphery of impeller (discharge side)

    4. High velocity fluid enters the stationary volute casing

    5. Volute casing converts the kinetic energy of fluid into pressure energy at the

    discharge of the pump.

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    8 Lobe pump Two lobes rotating Used in nuclear, food

    processing and chemical

    units for handling

    sensitive fluids

    9 Piston and plunger pump Reciprocating and positive

    displacement type

    Pumping for ammonia

    and carbonate at high

    pressure

    10 Diaphragm pump Pumping by means of

    pulsating elastic or flexible

    diaphragms of rubber,

    plastic etc.

    Used for pumping slurry,

    sludge or chemical

    solutions

    11 Rotary gear pump Helical type of gears with

    meshing of gears

    Used for viscous liquids

    in the viscosity range up

    to 1000cp

    5.4 Standard arrangement for pumps:

    5.4.1: Loop for screw pump:

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    5.4.2 Loop for centrifugal pump:

    5.4.3 Loop for reciprocating pump:

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    5.5 Trouble shooting:

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    5.5.1 Trouble shooting for centrifugal pump:

    Capacityt

    oo

    low

    Headtoo

    low

    Poororno

    suction

    Intermitte

    nt

    delivery

    Noisy

    o

    eration

    Pump

    leaking

    Power

    consumpt

    io

    ntoohigh

    Bearing

    temptoo

    hih

    Pumpcom

    es

    tostopjams

    Speed too

    low

    A A

    Casing or

    shaft

    sealing

    leaking

    B B B B B

    Suction lifttoo high

    B B B B

    Viscosity

    of delivery

    liquid too

    high

    C C C C C C

    Specific

    gravity of

    delivery

    liquid too

    high

    D D D

    Improper

    installation

    strain on

    the pump

    hose or

    jamming

    parts in

    the pump

    E E E E E

    Wear rings

    clearancetoo big

    due to

    wear

    F F F F

    Wrong

    direction

    of rotation

    G G

    Discharge

    line

    friction

    loss high

    H H

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    A Check the frequency and voltage of incoming supply

    B Ensure if the trouble is caused by the casing, shaft, sealing, suction pipe, foot valve or suction

    strainer .Accordingly take the following action

    Renew the gasket on the casing Tighten the gland or renew the packing ring

    Ensure the leak tightness of the suction pipe

    Check the leak tightness of the foot valve

    Clean the suction strainer

    C Clean the suction pipe, foot valve and suction strainer. If needed, replace the flange gasket.

    Check the suction pipe

    D Pump model and motor rating are determined on the basis of data specified in the purchase

    order. Troubles arising due to different data can be cleared only after consulting the pump

    supplier

    E Readjust the alignment of the pump and motor. Check that no stress is transmitted by piping

    and flange connection.

    F Discharge the pump and replace the defective parts

    G Replace the wear rings

    H Interchange the phase conditions of the motor

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    6. INSTRUMENTS-TYPES & APPLICATION:

    6.1 Pressure measuring instruments:

    6.2 Flow measuring instruments:

    Sr No TYPE APPLICATION REMARKS

    1 Magnetic Flow meter Used for slurry , acid Provided with

    upstream and

    downstream isolation

    valve, not used for gas

    application

    2 Vortex Meter Used for high

    turndown Ratio

    Provided with

    upstream and

    downstream isolation

    valve

    3 Vane/Turbine Type Clean fluid gas High accuracy

    4 Orifice meter Used for clean liquid

    service

    For size < 2

    5 Rota meter Used where local

    indication is required

    Size up to 3

    Sr No TYPE APPLICATION REMARKS

    1 Diaphragm pressure

    gauge

    Used for liquids

    containing solid

    particles or suspension

    Provided with isolation

    valve

    2 Bourdon Type Pressure

    Gauge

    Used for clean liquid Isolation valve is

    provided, used for

    steam line

    3 Differential type

    pressure instrument

    To be provided with

    upstream and

    downstream isolation

    valve

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    6.3 Temperature measuring instruments:

    Sr No TYPE APPLICATION REMARKS

    1 RTD Used where

    temperature of

    liquid/gas is up to 600

    No isolation valve is

    required

    2 Thermocouple Used for High

    Temperature

    application Range

    between 0-2500

    No isolation valve is

    required

    3 Temperature Gauge For Local indication.

    Range from 0-600

    6.4 Level measuring instruments:

    Sr No TYPE APPLICATION REMARKS

    1 Differential Pressure

    Type

    For Liquid Level

    Measurement

    Side Mounted

    2 Radar Type Top mounted ,The

    measurement

    accuracy is unaffected

    by changes in density,

    conductivity and

    dielectric constant of

    the product being

    measured or by air

    movement above the

    Product.

    3 Ultra Sonic Top mounted,

    Cheaper than Radar

    4 dipstick Used only for vented

    and underground tank

    Fast insertion,

    insertion with an

    angle

    5 Float and Tape Type Widely used in water

    storage tank

    Used mainly for open

    tanks local level

    indication

    6 Tabular gauge glass Used in low pressure

    services to avoid

    breakage

    Fitted externally

    7 Level switch Emergency shutdown,

    alarming, on/offapplication

    Point level sensor which

    moves with the liquidsurface

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    7. BASICS OF PFD (PROCESS FLOW DIAGRAM):

    7.1 Introduction:

    In PFD the Entire process is represented sequentially by means of equipment symbols and

    lines indicating all equipment and flow directions.

    Symbols are based on codes and standards Consists of Pictorial interrelationship between

    various unit operations and process units.

    Material balance at all major steps.

    Energy balance in the form of specific heat, temperature and state of materials.

    A PFD can be computer generated from process simulators (see List of ChemicalProcess Simulators), CAD packages, or flow chart software using a library of chemical

    engineering symbols.

    Rules and symbols are available from standardization organizations such as DIN, ISOor ANSI.

    Often PFDs are produced on large sheets of paper.

    PFDs of many commercial processes can be found in the literature, specifically inencyclopaedias of chemical technology.

    7.2 A typical PFD will consist of following things:

    Process piping

    Major bypass and recirculation lines Major equipment symbols, names and identification numbers

    Flow directions

    Control loops that affect operation of the system

    Interconnection with other systems

    System ratings and operational values as minimum, normal and maximum flow,temperature and pressure

    Composition of fluids

    7.2.1 Following things should be considered while making PFD:

    It is desirable to show equipments at theirrelative positions.E.g. Pumps at ground level

    Main process streams are always in bold.

    Streams are numbered within diamond.

    Equipments are numberedbased on function or Area or both.

    Also show utilities and ETPs.

    While continuing on other sheet, must indicate

    Interconnection between various streams.

    Horizontal lines are dominant Number streams left to right when possible

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    7.3PFD will not include:

    Pipe classes or piping line numbers

    Process control instrumentation (sensors and final elements)

    Minor bypass lines

    Isolation and shutoff valves

    Maintenance vents and drains

    Relief and safety valves

    Flanges

    7.4 Standards used for making PFD:

    ISO 10628: Flow Diagrams for Process Plants - General Rules

    ANSI Y32.11: Graphical Symbols for Process Flow Diagrams (withdrawn 2003)

    SAA AS 1109: Graphical Symbols for Process Flow Diagrams for the Food Industry.

    7.5 Tracing of Primary Chemicals in PFD:

    Reactants: start with the feed (LHS of PFD) and trace chemicals forward towardreactor.

    Products: start with the product (RHS of= PFD) and trace chemicals backward towardreactor.

    Tactics applicable for tracing lines in PFD:

    (1) Any unit operation, or group of operations, that has a single or multiple input stream(s)

    and a single output stream is traced in a forward direction. If chemical A is present in any

    input stream, it must appear in the single output stream.

    (2) Any unit operation, or group of operations, that has a single input and single or multiple

    output stream(s) is traced in a backward direction. If chemical A is present in any output

    stream, it must appear in the single input stream.(3) Systems such as distillation columns are composed of multiple unit operations with a

    single input or output stream. It is sometimes necessary to consider such equipment

    combinations as blocks before implementing Tactics (1) and (2).

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    8. BASICS OF P&ID:

    8.1 Legends:

    Legends are the basic requirement for making of P&ID. They contain symbols for different

    equipments, instruments and lines present in a plant.

    8.1.1 Instrument Legend:

    Property

    Measured

    First

    Letter

    Indicating

    only

    Recording

    only

    Controlling

    Only

    Indicating

    andcontrolling

    Recording

    andcontrolling

    Flow Rate F FI FR FC FIC FRC

    Level L LI LR LC LIC LRC

    Pressure P PI PR PC PIC PRC

    Quality Q QI QR QC QIC QRC

    Radiation R RI RR RC RIC RRC

    Temperature T TI TR TC TIC TRC

    Weight W WI WR WC WIC WRC

    Instrument Short-Hand Symbols or Bubbles Used in P&IDs:

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    Basic Instrumentation Symbols:

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    Designation of letters used in making P&ID:

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    8.1.2 Legends for fluids:

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    8.1.4 Flow Sensors Symbols Used in P&IDs:

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    8.1.5 Valve Failure Modes Symbols Used in P&IDs:

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    8.1.6 Valve Actuator Types Used in P&IDs:

    8.1.7 Valves Symbols Used in P&IDs:

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    8.1.8 Line Type & Control Signals Symbols Used in P&IDs:

    8.1.9 Piping Connection Symbols Used in P&IDs:

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    8.2 P&ID:

    8.2.1 Definition:

    P&ID is defined by theInstitute of Instrumentation and Controlas follows: A diagram which shows the interconnection of process equipment and the instrumentation

    used to control the process.

    In the process industry, a standard set of symbols is used to prepare drawings of processes.

    The instrument symbols used in these drawings are generally based on Instrumentation,

    Systems, and Automation Society (ISA) Standard S5. 1.

    The primary schematic drawing used for laying out a process control installation.

    In term of processing Facilities It is a pictorial presentation of

    Key piping and instrument details

    Control and shutdown schemes

    Safety and regulatory requirements and

    Basic start up and operational information

    8.2.2 P&ID will contain:

    P&ID will include following things:

    1. Instrumentation and designations2. Mechanical equipment with names and numbers3. All valves and their identifications4. Process piping, sizes and identification5. Miscellanea - vents, drains, special fittings, sampling lines, reducers, increasers andswages

    6. Permanent start-up and flush lines7. Flow directions8. Interconnections references

    9. Control inputs and outputs, interlocks10. Interfaces for class changes

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    9. PUMP HYDRAULICS:

    9.1 Definition:

    9.1.1 Suction Head:

    If the water to be pumped has its surface ABOVE the center of the pump, then this

    relationship is called a "suction head". More technically, it is the positive vertical distance

    between the pump datum and the liquid surface in the suction well.

    9.1.2 Static Head:

    "Static head is the distance that the water is to be lifted."

    Therefore, if the liquid level is above the datum, then it is a "positive value", as the water

    does not need to be pumped to that elevation. In the calculation:(Static Head, ft.) = (Discharge Head, ft.) - (Suction Head, ft.)

    "Once more for emphasis", the suction elevation is subtracted from the discharge head as the

    water is already at a positive, "not needed to be pumped elevation" ABOVE the pump. This

    resulting value is known as the static head.

    9.1.3 Discharge Head:

    It is the vertical distance between the pump datum point and the liquid surface in the

    receiving tank. The pump datum is at the center line for horizontal pumps and at the entrance

    eye of the impeller for vertical pumps.

    9.1.4 Friction Head:

    It is the head necessary to overcome the friction in the pipes, fittings, valves, elbows, etc.

    This information is gathered empirically, and then recorded in tables so that we can estimate

    these values according to the flow, the pipe size, the pipes material it is constructed out of,

    pipe age and any deposits, the type of valve, etc. This additional resistance to flow must be

    compensated for, in order to deliver the desired flow rate. Please refer to the illustrations for

    suction head and suction lift, where you will notice that the friction head in feet, is added to

    the static head which results in a new value called the Total Head or Total Dynamic Head.

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    9.2 Example:

    In the calculation:

    (Static Head, ft) = (Discharge head, ft) - (Suction Elev. ft)

    Note that the suction elevation (lift) is below the pump datum. In this case the elevation is anegative number (minus) and therefore "a minus subtracting a minus is a positive value in

    the equation. To illustrate a suction liquid level 5 feet BELOW the pump datum, with a

    Discharge head of 35 ft.

    (40 ft.) = (35 ft.) - (-5 ft.)

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    9.3 Net Positive Suction Head (NPSH):

    In a hydraulic circuit, net positive suction head (NPSH) is the difference between the actual pressure

    of a liquid in a pipeline and the liquid's vapor pressure at a given temperature.

    NPSH is an important parameter to take into account when designing a circuit: whenever theliquid pressure drops below the vapor pressure, liquid boiling occurs, and the final effect will

    be cavitation: vapor bubbles may reduce or stop the liquid flow, as well as damage the

    system.

    Centrifugal pumps are particularly vulnerable especially when pumping heated solution near

    the vapor pressure, whereas positive displacement pumps are less affected by cavitation, as

    they are better able to pump two-phase flow (the mixture of gas and liquid), however, the

    resultant flow rate of the pump will be diminishedbecause of the gas volumetrically

    displacing a disproportion of liquid. Careful design is required to pump high temperature

    liquids with a centrifugal pump when the liquid is near its boiling point.

    The violent collapse of the cavitation bubble creates a shock wave that can carve material

    from internal pump components (usually the leading edge of the impeller) and creates noise

    often described as "pumping gravel". Additionally, the inevitable increase in vibration can

    cause other mechanical faults in the pump and associated equipment.

    NPSH (Net Positive Suction Head) = hss + hps - hfs - hvp ;

    hss = static suction head ;

    hps = atmospheric pressure acting on the surface of the liquid ;

    hfs = head loss due to friction in the pipe ;

    hvp = vapour pressure ;

    http://en.wikipedia.org/wiki/Hydraulichttp://en.wikipedia.org/wiki/Vapor_pressurehttp://en.wikipedia.org/wiki/Boilinghttp://en.wikipedia.org/wiki/Cavitationhttp://en.wikipedia.org/wiki/Centrifugal_pumphttp://en.wikipedia.org/wiki/Pump#Positive_displacement_pumphttp://en.wikipedia.org/wiki/Pump#Positive_displacement_pumphttp://en.wikipedia.org/wiki/Centrifugal_pumphttp://en.wikipedia.org/wiki/Cavitationhttp://en.wikipedia.org/wiki/Boilinghttp://en.wikipedia.org/wiki/Vapor_pressurehttp://en.wikipedia.org/wiki/Hydraulic
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    9.4 sample calculation:

    Q Calculate NPSH available, discharge pressure, differential pressure, differential head for the pump

    carrying effluent from aeration tank to flocculation tank with the following data given.

    Data Given:

    =10cp

    =1000 kg/

    Q=666 l/h

    d=25mm

    Answer:

    Q=A*v

    = * *v

    V=0.37m/s

    Re= = = 1000

    Re 5cp so it is viscous fluid

    f= = 0.016 ; f=friction factor

    Friction loss in fitting K Qty Equivalent length

    =

    Entry loss 0.5 1 0.781

    90 Bend 0.45 4 2.81

    Tee strainer 2 1 3.125

    Ball Valve 0.5 2 1.56

    Tee st run 2 1 3.125

    Check valve 1 0 0

    Reducer 2 0 0

    Net Equivalent length 11.01

    Straight Pipe Length=10m;

    L=10 + 11.401=20.85m

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    Friction Loss = = =0.45

    Pump suction centre line =27.7m

    Minimum Water level in the Tank=28.8m

    Vapour Pressure =0.75m

    Top of the unit of flocculation tank=21.65m

    NPSH (Net Positive Suction Head) = hss + hps - hfs - hvp

    = (28.8-27.7) + 10.3 - 0.75 - 0.45

    = 10.2m

    For Discharge

    d=20mm

    Q=700 l/h

    From pump to Header=5m

    From Header to flocculation tank=320m

    Q=A*v

    = = * *v = 0.6m/sec

    Re= = = 1220

    Re

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    10.2 GPCB Norms for Effluent Water:

    Sr No Term mg/l or ppm

    1 COD 250

    2 BOD 100

    3 TDS 5000

    4 TSS 100

    5 Chloride 600

    6 Sulphate 1000

    7 Phenolic 1

    8 Oil and grease 10