Quantitative Analysis Summary Report

189.0000

Accuracy

99.57

100.97

100.34

98.61

100.60

86.68

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

4.1733

Final Conc

24.8930

50.4860

125.4191

246.5235

503.0092

163.8184

Resp Ratio

0.5683

1.1754

3.1011

6.6792

16.1584

4223

4417

4173

4243

3717

4228

2400

5192

12941

28338

60068

17646

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

7-amino clonazepam

7-amino clonazepam

7-amino clonazepam

7-amino clonazepam

7-amino clonazepam

7-amino clonazepam

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Benzos Mix Unit Pos APCI Segs.m

Benzos Mix Unit Pos APCI Segs.m

Benzos Mix Unit Pos APCI Segs.m

Quantitation Results7-amino clonazepamData File Compound ISTD Response ISTD Resp

Acq Method File

Benzos Mix Unit Pos APCI Segs.m

Benzos Mix Unit Pos APCI Segs.m

Benzos Mix Unit Pos APCI Segs.m

Benzos Mix Unit Pos APCI Segs.m

Benzos Mix Unit Pos APCI Segs.m

QC1

Sample Type

Calibration

Calibration

Calibration

Calibration

Calibration

Blank

Sample

QC

-1.00

-1.00

Level

L1

L2

L3

L4

L5

-1.00

-1.00

-1.00

-1.00

-1.00

-1.00

Benzo QC

Position

P1-F3

P1-F4

P1-F5

P1-F6

P1-F7

P1-F2

P1-F9

P1-F8

Benzo Cal09.d

Benzo Cal08.d

Sample Name

25 Std

50 Std

125 Std

250 Std

500 Std

Blank

123456

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal02.d

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Sequence TableData File Inj Vol

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:28 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:28:35.48856-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 1 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Summary Report

92.64

flunitrazepam

Accuracy

99.54

102.97

95.12

100.19

103.08

3.6723

95.4207

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

103.0000

Final Conc

24.8839

51.4854

118.8979

250.4847

515.3953

8516

8840

Resp Ratio

0.5192

1.1632

2.7953

5.9811

12.3948

0.0056

2.2269

56764

119448

48

19686

ISTD Resp

8704

8909

8960

9490

9637

clonazepam

clonazepam

ISTD

D4-clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal08.d

Compound

clonazepam

clonazepam

clonazepam

clonazepam

clonazepam

clonazepamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Response

4519

10363

25046

Accuracy

101.39

96.13

104.50

98.89

99.89

10.1229

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

Final Conc

25.3477

48.0629

130.6195

247.2174

499.4428

4599

Resp Ratio

1.0045

1.9755

5.7017

11.4914

26.1271

0.3668

ISTD Resp

4223

4417

4173

4243

3717

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

Response

4242

8725

23794

48755

97125

1687

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal09.d

Compound

zopiclone

zopiclone

zopiclone

zopiclone

zopiclone

zopiclone

99.00

zopicloneData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

Accuracy

100.73

96.82

108.81

94.43

101.73

99.0015

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

100.0000

Final Conc

25.1833

48.4112

136.0114

236.0636

508.6383

4228

Resp Ratio

0.2461

0.5181

1.6064

2.9698

7.3365

1.1346

ISTD Resp

4223

4417

4173

4243

3717

D4-7-amino clonazepam

Response

1039

2288

6704

12600

27273

4797

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepamBenzo Cal07.d

Benzo Cal08.d

Compound

7-amino flunitrazepam

7-amino flunitrazepam

7-amino flunitrazepam

7-amino flunitrazepam

7-amino flunitrazepam

7-amino flunitrazepam

7-amino flunitrazepamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 2 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Summary Report

Accuracy

101.91

96.71

100.62

102.15

Exp Conc

25.0000

50.0000

125.0000

250.0000

Final Conc

25.4768

48.3550

125.7753

255.3699

Resp Ratio

0.5228

0.8937

2.2815

5.0634

ISTD Resp

10316

10731

11176

11064

Response

5393

9590

25498

56020

ISTD

D5-oxazepam

D5-oxazepam

D5-oxazepam

D5-oxazepam

Compound

oxazepam

oxazepam

oxazepam

oxazepam

oxazepamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

104.0000

Accuracy

98.43

104.11

98.32

105.32

95.28

93.99

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

24.6068

52.0534

122.8973

263.2900

476.3922

97.746813759

Resp Ratio

0.0852

0.1882

0.4539

0.9806

1.7801

0.3596

5947

12184

22776

4947

ISTD Resp

12909

13606

13101

12424

12795

triazolam

ISTD

D5-temazepam

D5-temazepam

D5-temazepam

D5-temazepam

D5-temazepam

D5-temazepam

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Compound

triazolam

triazolam

triazolam

triazolam

triazolam

triazolamData File

Benzo Cal03.d

Benzo Cal04.d

Response

1100

2560

Final Conc

Accuracy

101.15

97.27

98.68

106.58

97.49

3.5495

3.8224

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

Final Conc

25.2873

48.6334

123.3556

266.4532

487.4619

8516

8160

Resp Ratio

0.2897

0.5977

1.5835

3.4714

6.3872

0.0029

0.0065

32945

61553

25

53

ISTD Resp

8704

8909

8960

9490

9637

alpha-OH alprazolam

alpha-OH alprazolam

ISTD

D4-clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal09.d

Compound

alpha-OH alprazolam

alpha-OH alprazolam

alpha-OH alprazolam

alpha-OH alprazolam

alpha-OH alprazolam

alpha-OH alprazolamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Response

2521

5325

14188

101.40

96.56

101.71

99.42

101.33

3.1130

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

0.0000

14.9478

0.0240

0.0047

Final Conc

25.3495

48.2786

127.1428

248.5578

506.6413

3.7616

8960

9490

9637

8516

8840

Resp Ratio

0.6646

1.3451

3.6855

7.2888

D4-clonazepam

Response

5785

11983

33023

69174

144052

204

42

flunitrazepam

flunitrazepam

flunitrazepam

ISTD

D4-clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal08.d

Compound

flunitrazepam

flunitrazepam

flunitrazepam

flunitrazepam

Data File

Benzo Cal03.d

Benzo Cal04.d

ISTD Resp

8704

8909

Accuracy

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 3 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Summary Report

Final Conc Exp Conc AccuracyData File Compound ISTD Response ISTD Resp Resp Ratio

Accuracy

101.01

98.16

97.81

105.63

Exp Conc

25.0000

50.0000

125.0000

250.0000

Final Conc

25.2525

49.0808

122.2640

264.0711

Resp Ratio

0.1597

0.3151

0.8085

1.8343

ISTD Resp

12909

13606

13101

12424

Response

2062

4287

10592

22790

ISTD

D5-temazepam

D5-temazepam

D5-temazepam

D5-temazepam

Compound

desalkylflurazepam

desalkylflurazepam

desalkylflurazepam

desalkylflurazepam

desalkylflurazepamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

56.0000

Accuracy

100.01

100.32

98.42

101.95

99.43

94.52

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

0.0014

0.7419

Final Conc

25.0026

50.1603

123.0284

254.8781

497.1498

0.0000

52.9328

Resp Ratio

0.3485

0.7023

1.7841

3.9568

8.6720

14

8260

ISTD Resp

10316

10731

11176

11064

10219

10196

11134

Response

3595

7536

19938

43776

88618

D5-oxazepam

D5-oxazepam

D5-oxazepam

D5-oxazepam

D5-oxazepam

D5-oxazepam

lorazepam

lorazepam

lorazepam

lorazepam

lorazepam

lorazepam

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal08.d

91.22

lorazepamData File

Benzo Cal03.d

Compound

lorazepam

ISTD

D5-oxazepam

500.0000

102.0000

Accuracy

100.55

97.86

104.59

96.92

100.82

242.2913

504.1232

2.1557

145.6462

93.0424

Exp Conc

25.0000

50.0000

125.0000

250.0000

7427

Resp Ratio

0.5034

1.0320

2.9265

5.7023

13.0904

0.0024

3.2845

2.0386

21422

15140

ISTD Resp

6986

6858

6538

7240

6451

6786

6522

D5-alprazolam

D5-alprazolam

D5-alprazolam

Response

3517

7077

19133

41287

84446

16

alprazolam

alprazolam

alprazolam

alprazolam

ISTD

D5-alprazolam

D5-alprazolam

D5-alprazolam

D5-alprazolam

D5-alprazolam

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal09.d

Benzo Cal08.d

Compound

alprazolam

alprazolam

alprazolam

alprazolam

alprazolamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Final Conc

25.1376

48.9314

130.7423

Accuracy

99.84

100.46

99.48

100.27

99.96

0.0000

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

Final Conc

24.9591

50.2325

124.3526

250.6731

499.7925

10196

Resp Ratio

0.3578

0.6893

1.7357

3.7742

8.7367

0.0033

ISTD Resp

10316

10731

11176

11064

10219

D5-oxazepam

Response

3691

7397

19398

41757

89279

34

ISTD

D5-oxazepam

D5-oxazepam

D5-oxazepam

D5-oxazepam

D5-oxazepamBenzo Cal07.d

Benzo Cal02.d

Compound

flurazepam

flurazepam

flurazepam

flurazepam

flurazepam

flurazepam

flurazepamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

105.0000

99.02

99.73

500.0000

0.0042

1.8838

495.0952

0.0000

104.7185

11.7231

43

20974

10219

10428

11134

119797

oxazepam

D5-oxazepam

D5-oxazepam

D5-oxazepam

Benzo Cal07.d

Benzo Cal09.d

Benzo Cal08.d

oxazepam

oxazepam

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 4 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Summary Report

AccuracyData File Compound ISTD Response ISTD Resp Resp Ratio Final Conc

Accuracy

105.87

90.60

101.52

110.29

Exp Conc

25.0000

50.0000

125.0000

250.0000

Final Conc

26.4673

45.3001

126.9027

275.7316

Resp Ratio

0.5443

0.8937

2.5097

5.8837

ISTD Resp

4039

4931

4723

4113

Response

2199

4407

11852

24202

ISTD

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

Compound

midazolam

midazolam

midazolam

midazolam

midazolamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

0.0000

Accuracy

105.54

90.18

96.46

110.17

103.28

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

0.0017

0.0025

Final Conc

26.3845

45.0893

120.5695

275.4278

516.4187

4.6309

4.6528

Resp Ratio

0.7927

1.4729

4.2177

9.8489

18.6123

7

10

ISTD Resp

4039

4931

4723

4113

4463

3974

4054

Response

3202

7264

19918

40513

83063

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

nordiazepam

nordiazepam

nordiazepam

nordiazepam

nordiazepam

nordiazepam

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal08.d

nordiazepamData File

Benzo Cal03.d

Compound

nordiazepam

ISTD

D5-nordiazepam

500.0000

0.0000

Accuracy

109.18

87.70

102.41

112.66

95.88

281.6412

479.3994

0.0000

0.0000

0.0000

Exp Conc

25.0000

50.0000

125.0000

250.0000

4054

Resp Ratio

0.5871

0.8780

2.4551

5.7596

10.8233

0.0034

0.0046

0.0039

20

16

ISTD Resp

4039

4931

4723

4113

4463

3974

4277

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

Response

2372

4330

11594

23692

48302

14

chlordiazepoxide

chlordiazepoxide

chlordiazepoxide

chlordiazepoxide

ISTD

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal09.d

Benzo Cal08.d

Compound

chlordiazepoxide

chlordiazepoxide

chlordiazepoxide

chlordiazepoxide

92.50

chlordiazepoxideData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Final Conc

27.2942

43.8520

128.0163

Accuracy

100.55

99.24

97.74

104.29

98.70

98.9742

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

107.0000

Final Conc

25.1369

49.6216

122.1752

260.7158

493.4810

13759

Resp Ratio

0.2765

0.5463

1.3739

3.0711

6.2682

1.1047

ISTD Resp

12909

13606

13101

12424

12795

D5-temazepam

Response

3570

7433

17999

38157

80203

15199

ISTD

D5-temazepam

D5-temazepam

D5-temazepam

D5-temazepam

D5-temazepamBenzo Cal07.d

Benzo Cal08.d

Compound

temazepam

temazepam

temazepam

temazepam

temazepam

temazepam

temazepamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

101.0000

98.25

90.74

500.0000

Exp Conc

0.0014

0.5991

491.2347

0.5431

91.6483

3.6690

17

8243

12795

12490

13759

46946

desalkylflurazepam

D5-temazepam

D5-temazepam

D5-temazepam

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal08.d

desalkylflurazepam

desalkylflurazepam

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 5 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Summary Report

Data File Compound ISTD Response ISTD Resp Resp Ratio Final Conc Exp Conc Accuracy

0.0000

Accuracy

105.49

91.25

100.48

111.13

96.36

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

0.0099

0.0019

Final Conc

26.3715

45.6232

125.5977

277.8351

481.8240

0.0000

0.0000

Resp Ratio

0.3975

0.6594

1.8318

4.4382

8.7005

39

8

ISTD Resp

4039

4931

4723

4113

4463

3974

4054

Response

1605

3252

8651

18256

38828

diazepam

ISTD

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal08.d

Compound

diazepam

diazepam

diazepam

diazepam

diazepam

diazepam

diazepamData File

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

54.0000

96.46

114.51

500.0000

0.0034

1.2078

482.3231

0.0000

61.8378

11.4809

13

4897

4463

3974

4054

51236

midazolam

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

Benzo Cal07.d

Benzo Cal02.d

Benzo Cal08.d

midazolam

midazolam

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 6 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Calibration Report

1.0810

RF

1.0383

1.1632

1.1181

1.1962

1.2395

19686

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

103.0000

Response

4519

10363

25046

56764

119448

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

176.8048

clonazepamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

174.0720

178.1724

179.2014

189.8098

192.7394

8840

Exp Conc

50.0000

50.0000

50.0000

50.0000

50.0000

50.0000

Response

8704

8909

8960

9490

9637

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

0.0000

D4-clonazepamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

2.0091

1.9755

2.2807

2.2983

2.6127

0

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

0.0000

Response

4242

8725

23794

48755

97125

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

Method

0.5673

zopicloneCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

0.4922

0.5181

0.6425

0.5940

0.7337

4797

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

100.0000

Response

1039

2288

6704

12600

27273

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

1.1040

7-amino flunitrazepamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

1.1365

1.1754

1.2404

1.3358

1.6158

17646

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

189.0000

Response

2400

5192

12941

28338

60068

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

84.5651

7-amino clonazepamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

84.4553

88.3336

83.4643

84.8546

74.3485

4228

Exp Conc

50.0000

50.0000

50.0000

50.0000

50.0000

50.0000

Response

4223

4417

4173

4243

3717

QC1

Enabled

Level

L1

L2

L3

L4

L5

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

Calibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Benzo Cal06.d

Benzo Cal07.d

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Calibration InformationD4-7-amino clonazepam

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:28 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:28:35.48856-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 7 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Calibration Report

RF

1.0067

1.0320

1.1706

1.1405

Exp Conc

25.0000

50.0000

125.0000

250.0000

Response

3517

7077

19133

41287L4

Enabled

Benzo Cal06.d

CalType

Calibration

Calibration

Calibration

Calibration

0.0000

alprazolamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

0.7156

0.6893

0.6943

0.7548

0.8737

0

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

0.0000

Response

3691

7397

19398

41757

89279

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

Method

0.8970

flurazepamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

1.0455

0.8937

0.9126

1.0127

1.1723

20974

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

105.0000

Response

5393

9590

25498

56020

119797

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

148.5355

oxazepamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

139.7284

137.1589

130.7560

144.8098

129.0196

7427

Exp Conc

50.0000

50.0000

50.0000

50.0000

50.0000

50.0000

Response

6986

6858

6538

7240

6451

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

0.1729

D5-alprazolamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

0.1704

0.1882

0.1816

0.1961

0.1780

4947

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

104.0000

Response

1100

2560

5947

12184

22776

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

0.0000

triazolamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

0.5794

0.5977

0.6334

0.6943

0.6387

0

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

0.0000

Response

2521

5325

14188

32945

61553

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

Method

INF

alpha-OH alprazolamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

1.3293

1.3451

1.4742

1.4578

1.4948

42

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

0.0000

Response

5785

11983

33023

69174

144052

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

flunitrazepamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 8 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Calibration Report

Calibration STD CalType Level Enabled Response Exp Conc RF

RF

80.7832

Exp Conc

50.0000

Response

4039

Enabled

CalType

Calibration

INF

D5-nordiazepamCalibration STD

Benzo Cal03.d

Level

L1

RF

1.1743

0.8780

0.9820

1.1519

1.0823

16

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

0.0000

Response

2372

4330

11594

23692

48302

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

0.5162

chlordiazepoxideCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

0.5531

0.5463

0.5496

0.6142

0.6268

15199

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

107.0000

Response

3570

7433

17999

38157

80203

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

275.1746

temazepamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

258.1721

272.1143

262.0138

248.4878

255.9025

13759

Exp Conc

50.0000

50.0000

50.0000

50.0000

50.0000

50.0000

Response

12909

13606

13101

12424

12795

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

0.2966

D5-temazepamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

0.3195

0.3151

0.3234

0.3669

0.3669

8243

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

101.0000

Response

2062

4287

10592

22790

46946

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

0.6624

desalkylflurazepamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

0.6969

0.7023

0.7136

0.7914

0.8672

8260

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

56.0000

Response

3595

7536

19938

43776

88618

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

222.6771

lorazepamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

206.3131

214.6182

223.5166

221.2732

204.3773

11134

Exp Conc

50.0000

50.0000

50.0000

50.0000

50.0000

50.0000

Response

10316

10731

11176

11064

10219

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

0.9993

D5-oxazepamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

1.3090

15140

500.0000

102.0000

84446L5

QC1

Benzo Cal07.d

Benzo Cal08.d

Calibration

QC

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 9 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Calibration Report

Level Enabled Response Exp Conc RF

INF

Calibration STD CalType

RF

0.7949

0.6594

0.7327

0.8876

0.8700

8

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

0.0000

Response

1605

3252

8651

18256

38828

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

1.1184

diazepamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

1.0887

0.8937

1.0039

1.1767

1.1481

4897

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

54.0000

Response

2199

4407

11852

24202

51236

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

INF

midazolamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

RF

1.5855

1.4729

1.6871

1.9698

1.8612

10

Exp Conc

25.0000

50.0000

125.0000

250.0000

500.0000

0.0000

Response

3202

7264

19918

40513

83063

L4

L5

QC1

Enabled

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

CalType

Calibration

Calibration

Calibration

Calibration

Calibration

QC

81.0869

nordiazepamCalibration STD

Benzo Cal03.d

Benzo Cal04.d

Benzo Cal05.d

Level

L1

L2

L3

98.6271

94.4506

82.2686

89.2556

4054

50.0000

50.0000

50.0000

50.0000

50.0000

4931

4723

4113

4463

L4

L5

QC1

Benzo Cal06.d

Benzo Cal07.d

Benzo Cal08.d

Calibration

Calibration

Calibration

Calibration

QC

Benzo Cal04.d

Benzo Cal05.d

L2

L3

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 10 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

26.3715

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

25.0026

25.2525

25.1369

27.2942

26.3845

26.4673

25.3495

25.2873

24.6068

25.4768

24.9591

25.1376

0.2765

0.5871

0.7927

0.5443

0.3975

Final Conc

24.8930

25.1833

25.3477

24.8839

0.0852

0.5228

0.3578

0.5034

0.3485

0.1597

4039

4039

4039

Resp Ratio

0.5683

0.2461

1.0045

0.5192

0.6646

0.2897

10316

6986

10316

12909

12909

4039

1605

ISTD Resp

4223

4223

4223

8704

8704

8704

12909

10316

3595

2062

3570

2372

3202

2199

5785

2521

1100

5393

3691

3517

4.653

5.391

5.816

6.334

6.438

Response

2400

1039

4242

4519

3.902

4.169

4.035

4.056

4.106

4.545

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

RT

0.982

1.174

2.465

3.194

3.286

3.518

D5-oxazepam

D5-alprazolam

D5-oxazepam

D5-temazepam

D5-temazepam

D5-nordiazepam

diazepam

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D5-temazepam

D5-oxazepam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

midazolam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

alprazolam

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

Position P1-F3 Dilution 1

Sample Info Comment

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 2007-03-08 10:50

Sample Type Calibration Level L1

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Analysis Info

Data File Benzo Cal03.d Sample Name 25 Std

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:28 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:28:35.48856-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 11 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

45.6232

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

50.1603

49.0808

49.6216

43.8520

45.0893

45.3001

48.2786

48.6334

52.0534

48.3550

50.2325

48.9314

0.5463

0.8780

1.4729

0.8937

0.6594

Final Conc

50.4860

48.4112

48.0629

51.4854

0.1882

0.8937

0.6893

1.0320

0.7023

0.3151

4931

4931

4931

Resp Ratio

1.1754

0.5181

1.9755

1.1632

1.3451

0.5977

10731

6858

10731

13606

13606

4931

3252

ISTD Resp

4417

4417

4417

8909

8909

8909

13606

10731

7536

4287

7433

4330

7264

4407

11983

5325

2560

9590

7397

7077

4.658

5.404

5.831

6.324

6.449

Response

5192

2288

8725

10363

3.905

4.170

4.031

4.058

4.110

4.540

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

RT

0.982

1.178

2.467

3.192

3.287

3.513

D5-oxazepam

D5-alprazolam

D5-oxazepam

D5-temazepam

D5-temazepam

D5-nordiazepam

diazepam

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D5-temazepam

D5-oxazepam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

midazolam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

alprazolam

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

Position P1-F4 Dilution 1

Sample Info Comment

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 2007-03-08 11:00

Sample Type Calibration Level L2

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Analysis Info

Data File Benzo Cal04.d Sample Name 50 Std

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:28 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:28:35.48856-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 12 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

125.5977

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

123.0284

122.2640

122.1752

128.0163

120.5695

126.9027

127.1428

123.3556

122.8973

125.7753

124.3526

130.7423

1.3739

2.4551

4.2177

2.5097

1.8318

Final Conc

125.4191

136.0114

130.6195

118.8979

0.4539

2.2815

1.7357

2.9265

1.7841

0.8085

4723

4723

4723

Resp Ratio

3.1011

1.6064

5.7017

2.7953

3.6855

1.5835

11176

6538

11176

13101

13101

4723

8651

ISTD Resp

4173

4173

4173

8960

8960

8960

13101

11176

19938

10592

17999

11594

19918

11852

33023

14188

5947

25498

19398

19133

4.650

5.392

5.814

6.327

6.437

Response

12941

6704

23794

25046

3.898

4.165

4.018

4.054

4.106

4.534

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

RT

0.982

1.176

2.465

3.188

3.286

3.509

D5-oxazepam

D5-alprazolam

D5-oxazepam

D5-temazepam

D5-temazepam

D5-nordiazepam

diazepam

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D5-temazepam

D5-oxazepam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

midazolam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

alprazolam

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

Position P1-F5 Dilution 1

Sample Info Comment

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 2007-03-08 11:11

Sample Type Calibration Level L3

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Analysis Info

Data File Benzo Cal05.d Sample Name 125 Std

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:28 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:28:35.48856-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 13 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

277.8351

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

254.8781

264.0711

260.7158

281.6412

275.4278

275.7316

248.5578

266.4532

263.2900

255.3699

250.6731

242.2913

3.0711

5.7596

9.8489

5.8837

4.4382

Final Conc

246.5235

236.0636

247.2174

250.4847

0.9806

5.0634

3.7742

5.7023

3.9568

1.8343

4113

4113

4113

Resp Ratio

6.6792

2.9698

11.4914

5.9811

7.2888

3.4714

11064

7240

11064

12424

12424

4113

18256

ISTD Resp

4243

4243

4243

9490

9490

9490

12424

11064

43776

22790

38157

23692

40513

24202

69174

32945

12184

56020

41757

41287

4.662

5.400

5.833

6.315

6.447

Response

28338

12600

48755

56764

3.906

4.175

4.025

4.064

4.111

4.545

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

RT

0.984

1.179

2.470

3.196

3.292

3.517

D5-oxazepam

D5-alprazolam

D5-oxazepam

D5-temazepam

D5-temazepam

D5-nordiazepam

diazepam

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D5-temazepam

D5-oxazepam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

midazolam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

alprazolam

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

Position P1-F6 Dilution 1

Sample Info Comment

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 2007-03-08 11:21

Sample Type Calibration Level L4

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Analysis Info

Data File Benzo Cal06.d Sample Name 250 Std

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:28 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:28:35.48856-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 14 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

481.8240

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

497.1498

491.2347

493.4810

479.3994

516.4187

482.3231

506.6413

487.4619

476.3922

495.0952

499.7925

504.1232

6.2682

10.8233

18.6123

11.4809

8.7005

Final Conc

503.0092

508.6383

499.4428

515.3953

1.7801

11.7231

8.7367

13.0904

8.6720

3.6690

4463

4463

4463

Resp Ratio

16.1584

7.3365

26.1271

12.3948

14.9478

6.3872

10219

6451

10219

12795

12795

4463

38828

ISTD Resp

3717

3717

3717

9637

9637

9637

12795

10219

88618

46946

80203

48302

83063

51236

144052

61553

22776

119797

89279

84446

4.660

5.399

5.827

6.319

6.443

Response

60068

27273

97125

119448

3.910

4.177

4.024

4.065

4.114

4.548

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

RT

0.983

1.180

2.471

3.200

3.295

3.518

D5-oxazepam

D5-alprazolam

D5-oxazepam

D5-temazepam

D5-temazepam

D5-nordiazepam

diazepam

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-clonazepam

D4-clonazepam

D4-clonazepam

D5-temazepam

D5-oxazepam

lorazepam

desalkylflurazepam

temazepam

chlordiazepoxide

nordiazepam

midazolam

flunitrazepam

alpha-OH alprazolam

triazolam

oxazepam

flurazepam

alprazolam

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

zopiclone

clonazepam

Position P1-F7 Dilution 1

Sample Info Comment

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 2007-03-08 11:31

Sample Type Calibration Level L5

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Analysis Info

Data File Benzo Cal07.d Sample Name 500 Std

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:28 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:28:35.48856-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 15 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml0.0000

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

2.1557

0.0000

0.5431

0.0000

4.6309

0.0000

0.0014

0.0034

0.0017

0.0034

0.0099

Final Conc

3.6723

3.7616

3.5495

0.0000

3974

3974

3974

Resp Ratio

0.0056

0.0240

0.0029

0.0033

0.0024

0.0014

39

ISTD Resp

8516

8516

8516

10196

6786

10196

12490

3974

16

14

17

14

7

13

4.614

5.409

5.239

6.531

6.529

Response

48

204

25

34

D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

RT

3.301

3.311

2.958

4.012

3.953

4.225

diazepam

ISTD

D4-clonazepam

D4-clonazepam

D4-clonazepam

D5-oxazepam

D5-alprazolam

D5-oxazepam

D5-temazepam

D5-nordiazepam

alprazolam

lorazepam

desalkylflurazepam

chlordiazepoxide

nordiazepam

midazolam

Quantitation Results

Compound

clonazepam

flunitrazepam

alpha-OH alprazolam

flurazepam

Position P1-F2 Dilution 1

Sample Info Comment

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 2007-03-08 10:40

Sample Type Blank Level

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Analysis Info

Data File Benzo Cal02.d Sample Name Blank

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:28 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:28:35.48856-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 16 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Sample Report

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

Final Conc

10.1229

3.8224

0.0000

145.6462

0.0000

Resp Ratio

0.3668

0.0065

0.0042

3.2845

0.0046

ISTD Resp

4599

8160

10428

6522

4277

Response

1687

53

43

21422

20

RT

2.463

3.507

3.749

4.058

5.355chlordiazepoxide

ISTD

D4-7-amino clonazepam

D4-clonazepam

D5-oxazepam

D5-alprazolam

D5-nordiazepam

Quantitation Results

Compound

zopiclone

alpha-OH alprazolam

oxazepam

alprazolam

Position P1-F9 Dilution 1

Sample Info Comment

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 2007-03-08 12:01

Sample Type Sample Level

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Analysis Info

Data File Benzo Cal09.d Sample Name 123456

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:28 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:28:35.48856-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 17 of 18 Printed at: 9:29 PM on: 2/26/2010

Quantitative Analysis Sample Report

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml61.8378

0.0000

Units

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml

ng/ml93.0424

52.9328

91.6483

98.9742

0.0000

4.65280.0025

1.2078

0.0019

Final Conc

163.8184

99.0015

95.4207

3.1130

97.7468

104.71851.8838

2.0386

0.7419

0.5991

1.1047

0.0039

Resp Ratio

4.1733

1.1346

2.2269

0.0047

0.3596

13759

13759

4054

4054

4054

40548

ISTD Resp

4228

4228

8840

8840

13759

11134

7427

111348260

8243

15199

16

10

48976.325

6.863

Response

17646

4797

19686

42

4947

20974

151404.056

4.115

4.541

4.655

5.319

5.892D5-nordiazepam

D5-nordiazepam

D5-nordiazepam

RT

0.982

1.180

3.195

3.272

3.901

4.171D5-oxazepam

D5-alprazolam

D5-oxazepam

D5-temazepam

D5-temazepam

D5-nordiazepamchlordiazepoxide

nordiazepam

midazolam

diazepam

ISTD

D4-7-amino clonazepam

D4-7-amino clonazepam

D4-clonazepam

D4-clonazepam

D5-temazepamtriazolam

oxazepam

alprazolam

lorazepam

desalkylflurazepam

temazepam

Quantitation Results

Compound

7-amino clonazepam

7-amino flunitrazepam

clonazepam

flunitrazepam

Position P1-F8 Dilution 1

Sample Info Comment

Acq Method File Benzos Mix Unit Pos APCI Segs.m Acq Time 2007-03-08 11:51

Sample Type QC Level QC1

Last Calib Update 11/30/2007 12:55 PM Batch State Processed

Analysis Info

Data File Benzo Cal08.d Sample Name Benzo QC

Analysis Time 11/30/2007 12:55 PM Analyst Name mtischler

Report Time 2/26/2010 9:28 PM Reporter Name mtischler

Batch Info2007-11-30T12:55:32.828125-08:00 2010-02-26T21:28:35.48856-08:00 2007-11-30T12:55:31.796875-08:00

Batch Data Path C:\MassHunter\Data\BenzosInUrine\QuantResults\BenzosInUrine.batch.bin

QuantReport_ISTD_ResultsComplete_B_04_00.xlsx Page 18 of 18 Printed at: 9:29 PM on: 2/26/2010