Project Location Purpose Field Activities

SOIL INVESTIGATION REPORT

ARNOLD DRIVE AT AGUA CALIENTE ROAD ROUNDABOUT PROJECT

PM 14.89 – 15.12 (Arnold Drive) PM 10.00 – 10.12 (Agua Caliente Road)

January 3, 2013

This soil investigation report describes the results of the tests conducted by the County of Sonoma, Department of Transportation and Public Works (County) for soil investigations within the Arnold Drive and Agua Caliente Road Roundabout project area.

Project Location The investigation was performed on Arnold Drive (post mile 15.01) and Agua Caliente Road (post mile 10.00), Sonoma County, California. See Attachment a, Vicinity Map.

Purpose The primary objective of the investigation was to evaluate whether impacts due to aerially deposited lead (ADL), metals, and petroleum hydrocarbons exist in the surface and subsurface soils within the depths of expected excavation within the project boundaries. The County will use the information obtained from this investigation to coordinate roadway improvements, determine soil disposal costs, and identify health and safety concerns during construction. Since surplus soil may be taken to the Sonoma County Central Landfill, some of the tests were conducted to meet disposal criteria at that site.

Field Activities The County conducted 16 borings for soil investigation. Soil borings were performed at Arnold Drive and Agua Caliente Road. Soil boring locations were modified from the work plan depending on field accessibility and marked locations of underground utilities. Boring holes were located by swing ties from existing surveyed topographic features and survey monumentation. Bore hole locations are shown on the exhibit in Attachment b.

All soil borings were taken at a depth between 0.5’and 2.5’ below ground surface using power and hand augers, and hand trowels. Sixteen soil samples were collected. Four samples were combined into one composite producing four total composite samples. Completed soil boreholes were backfilled to the surface with the soil cuttings. Sampling equipment was cleansed between each sample using Alconox followed by a double rinse with deionized water. Soil samples were collected in pre-cleaned/unused stainless steel tubes. The tubes were sealed, labeled, placed on ice in a cooler, and transported to Alpha Analytical Laboratories, 208 Mason Street, Ukiah, California, a laboratory certified to conduct the tests.

Laboratory Analysis Samples were analyzed in the following manner: All soil samples were analyzed for Title 22 metals using EPA Test Method 6000/7000

series; where TTLC lead was greater than 50 ppm, selected samples were ran for the Waste Extraction Test (WET).

All samples were tested for: o TPHd and TPHmo by EPA Method 8015m with silica gel cleanup. o TPHg, BTEX, and MTBE using EPA Test Method 8260. o Oil and grease by standard method 5520 with silica gel cleanup.

One sample was tested for Organochlorine Pesticides and PCBs using EPA Test Method 8081/8082.

One composite sample was tested by the following tests: o VOCs by method 8260. o SVOC by method 8270. o TCLP Phenol by method 8270 o TCLP PCB’s by method 8080.

One sample was tested for reactivity, corrosivity, and ignitability (RCI).

The results of the investigations are tabulated in Attachment c. The lab results are included in Attachment d.

Results None of the tests for metals exceeded the regulatory values per the California Code of Regulations, Title 22. All 4 samples were tested for CAM 17 metals. Two samples 2-2D and 4A-4D had total lead levels exceeding 50 ppm and these were tested with the Waste Extraction Test (WET) method. The WET results were 2.2 ppm for sample 2A-2D and 3.3 ppm for sample 4A-4D. Both values are less than the 5 ppm allowed. This soil may be used in embankments.

All samples were tested for Total Petroleum Hydrocarbons-diesel (TPHd). The Environmental Screening Level (ESLs) per the San Francisco Bay RWQCB is 4200 ppm for gas and diesel. Composite samples 1 and 4 tested at 35 and 16 ppm for diesel. All samples were tested for oil and grease. Composite sample 4A-4D tested at 460 mg/kg. Though this is much less than the allowed environmental screening level, it is high enough to prevent disposal at the County's Central Landfill. The Environmental Screening Levels (ES Ls) per the San Francisco Bay RWQCB is 12000 ppm for residual fuels.

All four composite samples were tested for volatile organic carbon. One was tested for Phenol and poly carbonated biphenyls. The test results did not detect the presence of any of these chemicals.

Report Prepared By:

~~Rex Cummins Senior Engineer

Attachments

a. VICINITY MAP b. SOIL SAMPLE LOCATION MAP c. SOIL SAMPLE ANALYTICAL RES UL TS CHART d. CHEMICAL EXAMINATION REPORTS

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ATTACHMENT a

Vicinity Map Arnold Drive at Agua Caliente Road

Roundabout Intersection Project Author : PRND Cai:o~~hy :D . Re nier File Nurrber: S:\G!S·DATA\ffilVD_BASE\PRM) Departrrert A'ojeds\En ~rormenlal Revie w\A.rnokl l'.X at A~a Caienle PD.Jnd about -Vicin t y.mxd Dcte:OU)5Q012

1 inch = 1,000 feet

Figure 1

County of Sonoma !· -

·

~

Widening Areas

~Cross Hatched

Attachment cSoil Sample Analytical Results

Arnold Drive at Agua Caliente Road Roundabout

Sonoma County, CA

Sample Date Sample TPHd TPHg Oil & VOCs SVOCs TCLP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Lead Mercury Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc WET

Location Sampled Type Grease PCBs Lead

and ID (Composite?) (ppm) (ppm) (mg/kg) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm) (ppm)Environmental Screening Level * 12000 4200 12000 <0.01 <0.01 5 500 500 10000 75 100 2500 8000 2500 1000 20 3500 2000 100 500 700 2400 5000 5

1A-1D 0.5'-2.5' Depth, (1) 09/13/2011 YES 35 -- <250 <0.005 -- <0.2 <15 6.6 130 0.86 <1.0 48 18 43 15 <0.20 <10 41 <1.0 <5.0 <7.0 85 130 --

2A-2D 0.5'-2.5' Depth 09/13/2011 YES 14 -- <250 <0.005 -- -- <15 <5.0 87 <0.75 <1.0 36 15 30 54 <0.20 <10 22 <1.0 <5.0 <7.0 74 78 2.2

3A-3D 0.5'-2.5' Depth 09/13/2011 YES 4 -- <250 <0.005 -- -- <15 5.8 130 1.0 <1.0 42 18 30 14 <0.20 <10 26 <1.0 <5.0 <7.0 76 47 --

4A-4D 0.5'-1.0' Depth (2) 09/13/2011 YES 16 -- 460 0.0062 -- -- <15 5.1 130 0.84 <1.0 43 17 34 79 <0.20 <10 30 <1.0 <5.0 <7.0 74 62 3.3

ANALYTICAL LABORATORY: ANALYTICAL METHODS:

Alpha Analytical TPHg = Total Petroleum Hydrocarbons as gasoline according to EPA Method 8015 Modified

TPHd = Total Petroleum Hydrocarbons as diesel according to EPA Method 8015 Modified

TPHmo = Total Petroleum Hydrocarbons as motor oil according to EPA Method 8015 Modified

VOCs = Volatile Organic Compounds according to EPA Method 8260 B

EXPLANATION: SVOCs = Semivolatile Organic Compounds according to EPA Method 8270 C

ppm = parts per million TCLP = Toxicity Characteristic Leaching Potential

PCBs = Polychlorinated Biphenyls according to EPA Method 8082

WET=Waste Extraction Test

ND=Not Detected1 = Sample was also reported as ND for reactive cyanide and sulfide, has a flashpoint of above 220 degrees F and a pH of 7.2.2 = Volatile Organic Compounds Not detected except for methyl tert-butyl ether*Environmental Screening Levels for Hydrocarbons are from Table K-3, Direct Exposure Soil Screening Levels Construction/Trench Worker Exposure Scenario, California Regional Water Quality Board, San Francisco Bay Region. Metal standards are from California Code ofRegulations Title 22, Chapter 11, Article 3 . Volatile, Semivolatile, and PCB levels are acceptance standards for a Class III landfill.

U:\Pro_rec\2166-Arnold at Agua\2-Project Design\Materials\Soil Investigation Report\Arnold Dr Roundabout Soil Tests Summary Sept. 15 2011.xls 1 1/3/2013

Attachment D

e-mail: [email protected]

Corporate: 208 Mason St., Ukiah, CA 95482 • Phone: (707) 468-0401 • Fax: (707) 468-5267 Service Center: 6398 Dougherty Rd., Suite 35, Dublin, CA 94568 • Phone: (925) 828-6226 • Fax: (925) 828-6309

ELAP Certificate Numbers 1551 and 2728

30 September 2011

Sonoma Co. Dept. Public Works Testing Lab

Attn: Victor Hayes

2688 Ventura Ave.

Santa Rosa, CA 95403

RE: Arnold Drive Roundabout

Work Order: 1 II0676

Enclosed are the results of analyses for samples received by the laboratory on 09/15111 16:30. lfyou have any questions concerning this report, please feel free to contact me.

Sincerely,

Jeanette L. Poplin For Karen A. Daly Project Manager

Sonoma Co. Dept. Public Works Testing Lab2688 Ventura Ave. 09/30/11 10:26Santa Rosa, CA 95403 Project No:

Page 1 of 37

Project ID: C02166Arnold Drive RoundaboutAttn: Victor Hayes

CHEMICAL EXAMINATION REPORT

Order Number Receipt Date/Time Client Code Client PO/Reference

11I0676 09/15/2011 16:30 SCPWTL 3501-09

Report Date:

ANALYTICAL REPORT FOR SAMPLES

Sample ID Laboratory ID Matrix Date Sampled Date Received

Comp 1A-1D 0.5'-2.5' 11I0676-01 Soil 09/13/11 10:30 09/15/11 16:30

Comp 2A-2D 0.5'-2.0' 11I0676-02 Soil 09/13/11 11:25 09/15/11 16:30

Comp 3A-3D 0.5'-1.5' 11I0676-03 Soil 09/13/11 13:00 09/15/11 16:30

Comp 4A-4D 0.5'-1.0' 11I0676-04 Soil 09/13/11 14:00 09/15/11 16:30

The results in this report apply to the samples analyzed in accordance with the chain

of custody document. This analytical report must be reproduced in its entirety.

Bruce GoveLaboratory Director

9/30/2011


Page 2 of 37



Order Number

11I0676 09/15/2011 16:30 SCPWTL 3501-09

Alpha Analytical Laboratories, Inc.

Receipt Date/Time Client Code Client PO/Reference

Report Date:

DILUTIONANALYZED RESULT NOTEPQL PREPAREDBATCHMETHOD

Sample Type: Soil Sampled: 09/13/11 10:30Comp 1A-1D 0.5'-2.5' (11I0676-01)

Metals by EPA 6000/7000 Series Methods

Antimony EPA 6010 09/22/11 15:2509/16/11 13:40AI11612 1 ND mg/kg 15

"EPA 7060Arsenic 09/27/11 12:03" 10 6.6 " 5.0

"EPA 6010Barium 09/22/11 15:25" 1 130 " 10

""Beryllium "" " 0.86 " 0.75

Cadmium " """ " ND " 1.0

""Chromium "" " 48 " 5.0

""Cobalt "" " 18 " 10

""Copper "" " 43 " 10

""Lead "" " 15 " 5.0

Mercury EPA 7471 09/26/11 09:2809/23/11 07:16AI12302 " ND " 0.20

Molybdenum EPA 6010 09/22/11 15:2509/16/11 13:40AI11612 " ND " 10

""Nickel "" " 41 " 10

Selenium EPA 7740 09/23/11 13:25"" " ND " 1.0

Silver EPA 6010 09/22/11 15:25"" " ND " 5.0

Thallium " """ " ND " 7.0

""Vanadium "" " 85 " 5.0

""Zinc "" " 130 " 10

RCRA Hazardous Characteristics by EPA Methods

AI12832EPA 9045CCorrosivity 09/27/11 10:0009/27/11 09:00 1 7.2 pH Units 1.0

Reactive Sulfide SW846 Ch.7 09/22/11 16:1509/21/11 09:37AI12129 " ND mg/kg 500

Ignitability by Flashpoint EPA 1010 09/22/11 13:1509/22/11 07:40AI12205 " >220 °F 40

Reactive Cyanide SW846 Ch.7 09/23/11 14:4909/21/11 09:34AI12128 " ND mg/kg 250

9/30/2011



Laboratory DirectorBruce Gove


Page 3 of 37




11I0676 09/15/2011 16:30 SCPWTL 3501-09

Report Date:




Conventional Chemistry Parameters by APHA/EPA Methods

Oil & Grease (HEM-SG) EPA 9071B 09/28/11 15:3009/21/11 08:30AI12120 1 ND mg/kg 250

TPH by EPA/LUFT GC/GCMS Methods

AI119248015DROTPH as Diesel D-0909/27/11 14:0909/19/11 10:59 10 35 mg/kg 10

" " 87.4 % 28-129Surrogate: Tetratetracontane ""

Volatile Organic Compounds by EPA Method 8260B

Acetone EPA 8260B 09/23/11 01:2909/22/11 13:25AI12726 1 ND mg/kg 0.020

Benzene " """ " ND " 0.0050

Bromobenzene " """ " ND " 0.0050

Bromochloromethane " """ " ND " 0.0050

Bromodichloromethane " """ " ND " 0.0050

Bromoform " """ " ND " 0.0050

Bromomethane " """ " ND " 0.0050

n-Butylbenzene " """ " ND " 0.0050

sec-Butylbenzene " """ " ND " 0.0050

tert-Butylbenzene " """ " ND " 0.0050

Carbon tetrachloride " """ " ND " 0.0050

Chlorobenzene " """ " ND " 0.0050

Chloroethane " """ " ND " 0.0050

Chloroform " """ " ND " 0.0050

Chloromethane " """ " ND " 0.0050

2-Chlorotoluene " """ " ND " 0.0050

4-Chlorotoluene " """ " ND " 0.0050

Dibromochloromethane " """ " ND " 0.0050

1,2-Dibromo-3-chloropropane " """ " ND " 0.0050

9/30/2011





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11I0676 09/15/2011 16:30 SCPWTL 3501-09

Report Date:




Volatile Organic Compounds by EPA Method 8260B (cont'd)

1,2-Dibromoethane (EDB) EPA 8260B 09/23/11 01:29"" " ND " 0.0050

Dibromomethane " """ " ND " 0.0050

1,2-Dichlorobenzene " """ " ND " 0.0050



Dichlorodifluoromethane " """ " ND " 0.0050

1,1-Dichloroethane " """ " ND " 0.0050

1,2-Dichloroethane " """ " ND " 0.0050

1,1-Dichloroethene " """ " ND " 0.0050

cis-1,2-Dichloroethene " """ " ND " 0.0050

trans-1,2-Dichloroethene " """ " ND " 0.0050

1,2-Dichloropropane " """ " ND " 0.0050



1,1-Dichloropropene " """ " ND " 0.0050

cis-1,3-Dichloropropene " """ " ND " 0.0050

trans-1,3-Dichloropropene " """ " ND " 0.0050

Ethylbenzene " """ " ND " 0.0050

Hexachlorobutadiene " """ " ND " 0.0050

Isopropylbenzene " """ " ND " 0.0050

p-Isopropyltoluene " """ " ND " 0.0050

Methyl ethyl ketone " """ " ND " 0.015

Methyl isobutyl ketone " """ " ND " 0.010

Methyl tert-butyl ether " """ " ND " 0.0050

Methylene chloride " """ " ND " 0.0050

9/30/2011





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11I0676 09/15/2011 16:30 SCPWTL 3501-09

Report Date:





Naphthalene EPA 8260B 09/23/11 01:29"" " ND " 0.0050

n-Propylbenzene " """ " ND " 0.0050

Styrene " """ " ND " 0.0050

1,1,1,2-Tetrachloroethane " """ " ND " 0.0050

1,1,2,2-Tetrachloroethane " """ " ND " 0.0050

Tetrachloroethene " """ " ND " 0.0050

Toluene " """ " ND " 0.0050

1,2,3-Trichlorobenzene " """ " ND " 0.0050

1,2,4-Trichlorobenzene " """ " ND " 0.0050

1,1,1-Trichloroethane " """ " ND " 0.0050

1,1,2-Trichloroethane " """ " ND " 0.0050

Trichloroethene " """ " ND " 0.0050

Trichlorofluoromethane " """ " ND " 0.0050

Trichlorotrifluoroethane " """ " ND " 0.0050

1,2,3-Trichloropropane " """ " ND " 0.0050

1,2,4-Trimethylbenzene " """ " ND " 0.0050

1,3,5-Trimethylbenzene " """ " ND " 0.0050

Vinyl chloride " """ " ND " 0.0050

m,p-Xylene " """ " ND " 0.0050

o-Xylene " """ " ND " 0.0050

Xylenes (total) " """ " ND " 0.0050

" " 77.2 % 38-163Surrogate: Bromofluorobenzene ""

" " 82.3 % 39-154Surrogate: Dibromofluoromethane ""

" " 92.9 % 51-161Surrogate: Toluene-d8 ""

9/30/2011




CHEMICAL EXAMINATION REPORT Page 6 of 37

Sonoma Co. Dept. Public Works Testing Lab2688 Ventura Ave. Report Date: 09/30/11 10:26Santa Rosa, CA 95403 Project No: C02166Attn: Victor Hayes Project ID: Arnold Drive Roundabout


11I0676 09/15/2011 16:30 SCPWTL 3501-09


METHOD BATCH PREPARED ANALYZED DILUTION RESULT PQL NOTE

Comp 1A-1D 0.5'-2.5' (11I0676-01) Sample Type: Soil Sampled: 09/13/11 10:30

Polychlorinated Biphenyls by EPA Method 8082

PCB-1016 EPA 8082 AI11913 09/19/11 08:35 09/27/11 00:14 1 ND mg/kg 0.20

PCB-1221 " " " " " ND " 0.20

PCB-1232 " " " " " ND " 0.20

PCB-1242 " " " " " ND " 0.20

PCB-1248 " " " " " ND " 0.20

PCB-1254 " " " " " ND " 0.20

PCB-1260 " " " " " ND " 0.20

PCB-1262 " " " " " ND " 0.20

Surrogate: Tetrachloro-meta-xylene " " " " 104 % 10-150

Surrogate: Decachlorobiphenyl " " " " 138 % 32-190

Semivolatile Organic Compounds by EPA Method 8270C R-06

Acenaphthene EPA 8270C AI12137 09/21/11 13:59 09/28/11 09:43 5 ND mg/kg 0.31

Acenaphthylene " " " " " ND " 0.31

Anthracene " " " " " ND " 0.31

Benzidine " " " " " ND " 8.0

Benzo (a) anthracene " " " " " ND " 1.6

Benzo (a) pyrene " " " " " ND " 0.31

Benzo (b) fluoranthene " " " " " ND " 0.31

Benzo (g,h,i) perylene " " " " " ND " 0.31

Benzo (k) fluoranthene " " " " " ND " 0.31

Benzoic acid " " " " " ND " 8.0

Benzyl alcohol " " " " " ND " 3.3

Bis(2-chloroethoxy)methane " " " " " ND " 1.6

Bis(2-chloroethyl)ether " " " " " ND " 1.6

Bis(2-chloroisopropyl)ether " " " " " ND " 1.6



Bruce Gove 9/30/2011Laboratory Director




11I0676 09/15/2011 16:30 SCPWTL 3501-09




Semivolatile Organic Compounds by EPA Method 8270C (cont'd) R-06

Bis(2-ethylhexyl)phthalate EPA 8270C " " 09/28/11 09:43 " ND " 1.6

4-Bromophenyl phenyl ether " " " " " ND " 1.6

Butyl benzyl phthalate " " " " " ND " 1.6

4-Chloro-3-methylphenol " " " " " ND " 1.6

4-Chloroaniline " " " " " ND " 3.3

2-Chloronaphthalene " " " " " ND " 1.6

2-Chlorophenol " " " " " ND " 1.6

4-Chlorophenyl phenyl ether " " " " " ND " 1.6

Chrysene " " " " " ND " 0.31

Di-n-butyl phthalate " " " " " ND " 1.6

Di-n-octyl phthalate " " " " " ND " 1.6

Dibenz (a,h) anthracene " " " " " ND " 0.31

Dibenzofuran " " " " " ND " 1.6

1,2-Dichlorobenzene " " " " " ND " 1.6



3,3´-Dichlorobenzidine " " " " " ND " 3.3

2,4-Dichlorophenol " " " " " ND " 1.6

Diethyl phthalate " " " " " ND " 1.6

Dimethyl phthalate " " " " " ND " 1.6

2,4-Dimethylphenol " " " " " ND " 1.6

4,6-Dinitro-2-methylphenol " " " " " ND " 8.0

2,4-Dinitrophenol " " " " " ND " 8.0

2,4-Dinitrotoluene " " " " " ND " 1.6

2,6-Dinitrotoluene " " " " " ND " 1.6



9/30/2011Laboratory DirectorBruce Gove




11I0676 09/15/2011 16:30 SCPWTL 3501-09





1,2-Diphenylhydrazine EPA 8270C " " 09/28/11 09:43 " ND " 1.6

Fluoranthene " " " " " ND " 0.31

Fluorene " " " " " ND " 0.31

Hexachlorobenzene " " " " " ND " 1.6

Hexachlorobutadiene " " " " " ND " 1.6

Hexachlorocyclopentadiene " " " " " ND " 8.0

Hexachloroethane " " " " " ND " 1.6

Indeno (1,2,3-cd) pyrene " " " " " ND " 0.31

Isophorone " " " " " ND " 1.6

2-Methylnaphthalene " " " " " ND " 0.31

2-Methylphenol (o-cresol) " " " " " ND " 1.6

3 & 4-Methylphenol (m,p-cresol) " " " " " ND " 1.6

N-Nitrosodi-n-propylamine " " " " " ND " 1.6

N-Nitrosodimethylamine " " " " " ND " 3.3

N-Nitrosodiphenylamine " " " " " ND " 1.6

Naphthalene " " " " " ND " 0.31

2-Nitroaniline " " " " " ND " 8.0



Nitrobenzene " " " " " ND " 1.6

2-Nitrophenol " " " " " ND " 8.0

4-Nitrophenol " " " " " ND " 8.0

Pentachlorophenol " " " " " ND " 8.0

Phenanthrene " " " " " ND " 0.31

Phenol " " " " " ND " 1.6







11I0676 09/15/2011 16:30 SCPWTL 3501-09





Pyrene EPA 8270C " " 09/28/11 09:43 " ND " 0.31

1,2,4-Trichlorobenzene " " " " " ND " 1.6

2,4,5-Trichlorophenol " " " " " ND " 1.6

2,4,6-Trichlorophenol " " " " " ND " 1.6

Surrogate: 2-Fluorobiphenyl " " " " 76.4 % 61-117

Surrogate: 2-Fluorophenol " " " " 68.8 % 50-113

Surrogate: Nitrobenzene-d5 " " " " 69.6 % 47-123

Surrogate: p-Terphenyl-d14 " " " " 94.2 % 63-133

Surrogate: Phenol-d6 " " " " 72.4 % 49-119

Surrogate: 2,4,6-Tribromophenol " " " " 76.3 % 52-129



Antimony EPA 6010 AI11612 09/16/11 13:40 09/22/11 15:29 1 ND mg/kg 15

Arsenic EPA 7060 " " 09/27/11 12:20 10 ND " 5.0 R-01

Barium EPA 6010 " " 09/22/11 15:29 1 87 " 10

Beryllium " " " " " ND " 0.75

Cadmium " " " " " ND " 1.0

Chromium " " " " " 36 " 5.0

Cobalt " " " " " 15 " 10

Copper " " " " " 30 " 10

Lead " " " " " 54 " 5.0

Mercury EPA 7471 AI12302 09/23/11 07:16 09/26/11 09:38 " ND " 0.20

Molybdenum EPA 6010 AI11612 09/16/11 13:40 09/22/11 15:29 " ND " 10

Nickel " " " " " 22 " 10

Selenium EPA 7740 " " 09/23/11 13:31 " ND " 1.0

Silver EPA 6010 " " 09/22/11 15:29 " ND " 5.0

Thallium " " " " " ND " 7.0







11I0676 09/15/2011 16:30 SCPWTL 3501-09




Metals by EPA 6000/7000 Series Methods (cont'd)

Vanadium EPA 6010 " " 09/22/11 15:29 " 74 " 5.0

Zinc " " " " " 78 " 10

STLC Metals by EPA 6000/7000 Series Methods

Lead EPA 6010 AI12912 09/29/11 09:13 09/29/11 12:13 1 2.2 mg/l 0.50


Oil & Grease (HEM-SG) EPA 9071B AI12120 09/21/11 08:30 09/28/11 15:30 1 ND mg/kg 250


TPH as Diesel 8015DRO AI11924 09/19/11 10:59 09/27/11 14:43 10 14 mg/kg 10 D-09

Surrogate: Tetratetracontane " " " " 72.4 % 28-129


Benzene EPA 8260B AI12726 09/22/11 13:25 09/23/11 02:02 1 ND mg/kg 0.0050

Toluene " " " " " ND " 0.0050

Ethylbenzene " " " " " ND " 0.0050

Xylenes (total) " " " " " ND " 0.0050

Methyl tert-butyl ether " " " " " ND " 0.0050

Surrogate: Bromofluorobenzene " " " " 80.5 % 38-163

Surrogate: Dibromofluoromethane " " " " 86.6 % 39-154

Surrogate: Toluene-d8 " " " " 97.9 % 51-161




Arsenic EPA 7060 " " 09/27/11 12:25 10 5.8 " 5.0

Barium EPA 6010 " " 09/22/11 15:33 1 130 " 10

Beryllium " " " " " 1.0 " 0.75







11I0676 09/15/2011 16:30 SCPWTL 3501-09




Metals by EPA 6000/7000 Series Methods (cont'd)

Cadmium EPA 6010 " " 09/22/11 15:33 " ND " 1.0

Chromium " " " " " 42 " 5.0

Cobalt " " " " " 18 " 10

Copper " " " " " 30 " 10

Lead " " " " " 14 " 5.0

Mercury EPA 7471 AI12302 09/23/11 07:16 09/26/11 09:40 " ND " 0.20


Nickel " " " " " 26 " 10

Selenium EPA 7740 " " 09/23/11 13:37 " ND " 1.0

Silver EPA 6010 " " 09/22/11 15:33 " ND " 5.0

Thallium " " " " " ND " 7.0

Vanadium " " " " " 76 " 5.0

Zinc " " " " " 47 " 10


Oil & Grease (HEM-SG) EPA 9071B AI12120 09/21/11 08:30 09/28/11 15:30 1 ND mg/kg 250


TPH as Diesel 8015DRO AI11924 09/19/11 10:59 09/27/11 18:10 1 4.0 mg/kg 1.0 D-09




Toluene " " " " " ND " 0.0050


Xylenes (total) " " " " " ND " 0.0050

Methyl tert-butyl ether " " " " " 0.0076 " 0.0050








11I0676 09/15/2011 16:30 SCPWTL 3501-09





Surrogate: Dibromofluoromethane EPA 8260B " " 09/23/11 02:36 83.7 % 39-154





Arsenic EPA 7060 " " 09/27/11 12:30 10 5.1 " 5.0

Barium EPA 6010 " " 09/22/11 15:37 1 130 " 10

Beryllium " " " " " 0.84 " 0.75

Cadmium " " " " " ND " 1.0

Chromium " " " " " 43 " 5.0

Cobalt " " " " " 17 " 10

Copper " " " " " 34 " 10

Lead " " " " " 79 " 5.0

Mercury EPA 7471 AI12302 09/23/11 07:16 09/26/11 09:47 " ND " 0.20


Nickel " " " " " 30 " 10

Selenium EPA 7740 " " 09/23/11 13:42 " ND " 1.0

Silver EPA 6010 " " 09/22/11 15:37 " ND " 5.0

Thallium " " " " " ND " 7.0

Vanadium " " " " " 74 " 5.0

Zinc " " " " " 62 " 10







11I0676 09/15/2011 16:30 SCPWTL 3501-09




STLC Metals by EPA 6000/7000 Series Methods

Lead EPA 6010 AI12912 09/29/11 09:13 09/29/11 12:19 1 3.3 mg/l 0.50


Oil & Grease (HEM-SG) EPA 9071B AI12120 09/21/11 08:30 09/28/11 15:30 1 460 mg/kg 250


TPH as Diesel 8015DRO AI11924 09/19/11 10:59 09/27/11 15:52 10 16 mg/kg 10 D-09




Toluene " " " " " ND " 0.0050


Xylenes (total) " " " " " ND " 0.0050

Methyl tert-butyl ether " " " " " 0.0062 " 0.0050


Surrogate: Dibromofluoromethane " " " " 85.4 % 39-154








11I0676 09/15/2011 16:30 SCPWTL 3501-09

Metals by EPA 6000/7000 Series Methods - Quality Control

Spike Source %REC RPD

Analyte(s) Result PQL Units Level Result %REC Limits RPD Limit Flag

Batch AI11612 - EPA 3051 Microwave

Blank (AI11612-BLK1) Prepared: 09/16/11 Analyzed: 09/22/11

Antimony ND 15 mg/kg

Barium ND 10 "

Beryllium ND 0.75 "

Cadmium ND 1.0 "

Chromium ND 5.0 "

Cobalt ND 10 "

Copper ND 10 "

Lead ND 5.0 "

Molybdenum ND 10 "

Nickel ND 10 "

Selenium ND 1.0 "

Silver ND 5.0 "

Thallium ND 7.0 "

Vanadium ND 5.0 "

Zinc ND 10 "

LCS (AI11612-BS1) Prepared: 09/16/11 Analyzed: 09/22/11

Antimony 19.5 15 mg/kg 20.0 97.3 85-115

Barium 19.6 10 " 20.0 98.2 85-115

Beryllium 19.8 0.75 " 20.0 98.9 85-115

Cadmium 18.3 1.0 " 19.2 95.3 85-115

Chromium 18.7 5.0 " 19.2 97.6 85-115

Cobalt 19.4 10 " 20.0 96.9 85-115

Copper 22.4 10 " 20.0 112 85-115

Lead 18.8 5.0 " 20.0 94.2 85-115

Molybdenum 19.8 10 " 20.0 98.9 85-115







11I0676 09/15/2011 16:30 SCPWTL 3501-09






Nickel 19.9 10 " 20.0 99.4 85-115

Selenium 2.07 1.0 " 2.00 103 68-118

Silver 20.2 5.0 " 20.0 101 78-108

Thallium 18.9 7.0 " 20.0 94.4 85-115

Vanadium 19.5 5.0 " 20.0 97.4 85-115

Zinc 19.0 10 " 20.0 95.0 85-115

Duplicate (AI11612-DUP1) Source: 11I0497-02 Prepared: 09/16/11 Analyzed: 09/22/11

Antimony ND 15 mg/kg ND 20

Arsenic 16.5 10 " 15.8 4.82 20

Barium 137 10 " 136 0.864 20

Beryllium 0.250 0.75 " ND 20

Cadmium 0.370 1.0 " ND 20

Chromium 19.1 5.0 " 19.9 4.04 20

Cobalt 11.7 10 " 12.3 4.68 20

Copper 301 10 " 240 22.6 20 QM-04

Lead 15.5 5.0 " 14.8 4.55 20

Molybdenum 0.456 10 " ND 20

Nickel 11.7 10 " 12.2 3.60 20

Selenium ND 1.0 " ND 20

Silver ND 5.0 " ND 20

Thallium ND 7.0 " ND 20

Vanadium 62.2 5.0 " 66.0 5.91 20

Zinc 60.7 10 " 60.4 0.607 20

Matrix Spike (AI11612-MS1) Source: 11I0497-02 Prepared: 09/16/11 Analyzed: 09/22/11

Antimony 11.8 15 mg/kg 20.0 ND 58.9 70-130 QM-01







11I0676 09/15/2011 16:30 SCPWTL 3501-09






Arsenic 18.0 10 " 2.00 15.8 109 70-130

Barium 148 10 " 20.0 136 61.6 70-130 QM-4X

Beryllium 16.9 0.75 " 20.0 ND 83.3 70-130

Cadmium 16.3 1.0 " 19.2 ND 83.1 70-130

Chromium 36.3 5.0 " 19.2 19.9 85.2 70-130

Cobalt 28.6 10 " 20.0 12.3 81.8 70-130

Copper 275 10 " 20.0 240 176 70-130 QM-4X

Lead 30.8 5.0 " 20.0 14.8 80.1 70-130

Molybdenum 15.2 10 " 20.0 ND 73.6 70-130

Nickel 28.7 10 " 20.0 12.2 82.6 70-130

Selenium 1.57 1.0 " 2.00 ND 78.6 7-107

Silver 17.8 5.0 " 20.0 ND 89.0 70-130

Thallium 14.8 7.0 " 20.0 ND 74.2 70-130

Vanadium 82.8 5.0 " 20.0 66.0 83.7 70-130

Zinc 77.9 10 " 20.0 60.4 87.6 70-130


Antimony 13.2 15 mg/kg 20.0 ND 65.8 70-130 QM-01

Arsenic 7.96 10 " 2.00 ND 102 70-130

Barium 184 10 " 20.0 165 96.4 70-130

Beryllium 17.2 0.75 " 20.0 ND 84.1 70-130

Cadmium 15.9 1.0 " 19.2 ND 82.8 70-130

Chromium 93.6 5.0 " 19.2 83.3 53.5 70-130 QM-4X

Cobalt 30.8 10 " 20.0 15.2 78.1 70-130

Copper 63.5 10 " 20.0 45.9 87.7 70-130

Lead 36.7 5.0 " 20.0 27.3 47.0 70-130 QM-04

Molybdenum 16.0 10 " 20.0 ND 76.0 70-130







11I0676 09/15/2011 16:30 SCPWTL 3501-09






Nickel 131 10 " 20.0 116 75.4 70-130

Selenium 1.44 1.0 " 2.00 ND 72.2 7-107

Silver 17.1 5.0 " 20.0 ND 85.3 70-130

Thallium 14.1 7.0 " 20.0 ND 70.6 70-130

Vanadium 60.5 5.0 " 20.0 44.4 80.2 70-130

Zinc 98.7 10 " 20.0 82.3 82.1 70-130

Matrix Spike Dup (AI11612-MSD1) Source: 11I0497-02 Prepared: 09/16/11 Analyzed: 09/22/11

Antimony 12.7 15 mg/kg 20.0 ND 63.4 70-130 7.25 20 QM-01

Arsenic 17.4 10 " 2.00 15.8 80.2 70-130 3.31 20

Barium 151 10 " 20.0 136 76.7 70-130 2.01 20

Beryllium 17.8 0.75 " 20.0 ND 87.9 70-130 5.29 20

Cadmium 16.7 1.0 " 19.2 ND 85.3 70-130 2.58 20

Chromium 32.9 5.0 " 19.2 19.9 67.6 70-130 9.76 20 QM-04

Cobalt 28.0 10 " 20.0 12.3 78.7 70-130 2.19 20

Copper 275 10 " 20.0 240 176 70-130 0.00378 20 QM-4X

Lead 29.9 5.0 " 20.0 14.8 75.5 70-130 3.04 20

Molybdenum 15.3 10 " 20.0 ND 74.0 70-130 0.508 20

Nickel 27.8 10 " 20.0 12.2 78.2 70-130 3.13 20

Selenium 1.74 1.0 " 2.00 ND 86.8 7-107 9.94 20

Silver 17.7 5.0 " 20.0 ND 88.6 70-130 0.456 20

Thallium 15.5 7.0 " 20.0 ND 77.4 70-130 4.28 20

Vanadium 74.4 5.0 " 20.0 66.0 41.7 70-130 10.7 20 QM-4X

Zinc 70.8 10 " 20.0 60.4 52.4 70-130 9.47 20 QM-04

Batch AI12302 - EPA 7471A Hg Soil








11I0676 09/15/2011 16:30 SCPWTL 3501-09




Batch AI12302 - EPA 7471A Hg Soil


Mercury ND 0.20 mg/kg


Mercury 0.855 0.20 mg/kg 1.00 85.5 80-120


Mercury ND 0.20 mg/kg ND 20


Mercury 0.885 0.20 mg/kg 1.00 ND 88.5 60-140


Mercury 0.905 0.20 mg/kg 1.00 ND 90.5 60-140 2.23 20







11I0676 09/15/2011 16:30 SCPWTL 3501-09

STLC Metals by EPA 6000/7000 Series Methods - Quality Control



Batch AI12912 - WET/3015

Blank (AI12912-BLK1) Prepared & Analyzed: 09/29/11

Lead ND 0.50 mg/l

LCS (AI12912-BS1) Prepared & Analyzed: 09/29/11

Lead 1.70 0.50 mg/l 2.00 85.2 85-115

Duplicate (AI12912-DUP1) Source: 11I0676-02 Prepared & Analyzed: 09/29/11

Lead 2.26 0.50 mg/l 2.25 0.719 20

Matrix Spike (AI12912-MS1) Source: 11I0676-02 Prepared & Analyzed: 09/29/11

Lead 3.92 0.50 mg/l 2.00 2.25 83.8 70-130

Matrix Spike Dup (AI12912-MSD1) Source: 11I0676-02 Prepared & Analyzed: 09/29/11

Lead 3.92 0.50 mg/l 2.00 2.25 83.5 70-130 0.129 20







11I0676 09/15/2011 16:30 SCPWTL 3501-09

RCRA Hazardous Characteristics by EPA Methods - Quality Control



Batch AI12128 - General Preparation


Reactive Cyanide ND 5000 mg/kg 991 0-10

LCS Dup (AI12128-BSD1) Prepared: 09/21/11 Analyzed: 09/23/11

Reactive Cyanide ND 5000 mg/kg 991 0-10 200



Reactive Sulfide ND 500 mg/kg


Reactive Sulfide 236 500 mg/kg 540 43.8 30-65


Reactive Sulfide 236 500 mg/kg 540 43.8 30-65 0.00 20

Batch AI12205 - General Prep


Ignitability by Flashpoint 83 40 °F 81.0 102 95-115

LCS Dup (AI12205-BSD1) Prepared & Analyzed: 09/22/11

Ignitability by Flashpoint 83 40 °F 81.0 102 95-115 0.00 11







11I0676 09/15/2011 16:30 SCPWTL 3501-09

Conventional Chemistry Parameters by APHA/EPA Methods - Quality Control





Oil & Grease (HEM-SG) ND 250 mg/kg


Oil & Grease (HEM-SG) 355 250 mg/kg 500 71.0 63-117


Oil & Grease (HEM-SG) 405 250 mg/kg 430 5.99 25


Oil & Grease (HEM-SG) 1080 250 mg/kg 500 430 130 63-117 QM-01


Oil & Grease (HEM-SG) 915 250 mg/kg 500 430 97.0 63-117 16.5 25







11I0676 09/15/2011 16:30 SCPWTL 3501-09

TPH by EPA/LUFT GC/GCMS Methods - Quality Control



Batch AI11924 - CA LUFT - orb shaker


TPH as Diesel ND 1.0 mg/kg

Surrogate: Tetratetracontane 1.04 " 1.20 86.7 28-129


TPH as Diesel 31.4 1.0 mg/kg 40.3 78.0 58-123



TPH as Diesel 34.0 1.0 mg/kg 40.3 84.6 58-123 8.12 25



TPH as Diesel 75.7 10 mg/kg 40.3 34.9 101 58-123



TPH as Diesel 60.8 10 mg/kg 40.3 34.9 64.5 58-123 21.8 25








11I0676 09/15/2011 16:30 SCPWTL 3501-09

Volatile Organic Compounds by EPA Method 8260B - Quality Control



Batch AI12726 - VOAs in Soil GCMS


Acetone ND 0.020 mg/kg

Benzene ND 0.0050 "

Benzene ND 0.0050 "

Toluene ND 0.0050 "

Ethylbenzene ND 0.0050 "

Bromobenzene ND 0.0050 "

Bromochloromethane ND 0.0050 "

Xylenes (total) ND 0.0050 "

Methyl tert-butyl ether ND 0.0050 "

Bromodichloromethane ND 0.0050 "

Bromoform ND 0.0050 "

Bromomethane ND 0.0050 "

n-Butylbenzene ND 0.0050 "

sec-Butylbenzene ND 0.0050 "

tert-Butylbenzene ND 0.0050 "

Carbon tetrachloride ND 0.0050 "

Chlorobenzene ND 0.0050 "

Chloroethane ND 0.0050 "

Chloroform ND 0.0050 "

Chloromethane ND 0.0050 "

2-Chlorotoluene ND 0.0050 "

4-Chlorotoluene ND 0.0050 "

Dibromochloromethane ND 0.0050 "

1,2-Dibromo-3-chloropropane ND 0.0050 "

1,2-Dibromoethane (EDB) ND 0.0050 "

Dibromomethane ND 0.0050 "







11I0676 09/15/2011 16:30 SCPWTL 3501-09






1,2-Dichlorobenzene ND 0.0050 "



Dichlorodifluoromethane ND 0.0050 "

1,1-Dichloroethane ND 0.0050 "

1,2-Dichloroethane ND 0.0050 "

1,1-Dichloroethene ND 0.0050 "

cis-1,2-Dichloroethene ND 0.0050 "

trans-1,2-Dichloroethene ND 0.0050 "

1,2-Dichloropropane ND 0.0050 "



1,1-Dichloropropene ND 0.0050 "

cis-1,3-Dichloropropene ND 0.0050 "

trans-1,3-Dichloropropene ND 0.0050 "

Ethylbenzene ND 0.0050 "

Hexachlorobutadiene ND 0.0050 "

Isopropylbenzene ND 0.0050 "

p-Isopropyltoluene ND 0.0050 "

Methyl ethyl ketone ND 0.015 "

Methyl isobutyl ketone ND 0.010 "

Methyl tert-butyl ether ND 0.0050 "

Methylene chloride ND 0.0050 "

Naphthalene ND 0.0050 "

n-Propylbenzene ND 0.0050 "

Styrene ND 0.0050 "







11I0676 09/15/2011 16:30 SCPWTL 3501-09






1,1,1,2-Tetrachloroethane ND 0.0050 "

1,1,2,2-Tetrachloroethane ND 0.0050 "

Tetrachloroethene ND 0.0050 "

Toluene ND 0.0050 "

1,2,3-Trichlorobenzene ND 0.0050 "


1,1,1-Trichloroethane ND 0.0050 "

1,1,2-Trichloroethane ND 0.0050 "

Trichloroethene ND 0.0050 "

Trichlorofluoromethane ND 0.0050 "

Trichlorotrifluoroethane ND 0.0050 "

1,2,3-Trichloropropane ND 0.0050 "

1,2,4-Trimethylbenzene ND 0.0050 "

1,3,5-Trimethylbenzene ND 0.0050 "

Vinyl chloride ND 0.0050 "

m,p-Xylene ND 0.0050 "

o-Xylene ND 0.0050 "

Xylenes (total) ND 0.0050 "

Surrogate: Bromofluorobenzene 0.0221 " 0.0250 88.7 38-163

Surrogate: Dibromofluoromethane 0.0205 " 0.0250 82.3 39-154

Surrogate: Toluene-d8 0.0217 " 0.0250 87.0 51-161











11I0676 09/15/2011 16:30 SCPWTL 3501-09






Benzene 0.0240 0.0050 mg/kg 0.0249 96.1 58-143

Benzene 0.0240 0.0050 " 0.0249 96.1 58-143

Toluene 0.0227 0.0050 " 0.0249 90.8 55-158

Chlorobenzene 0.0216 0.0050 " 0.0249 86.5 76-145

1,1-Dichloroethene 0.0212 0.0050 " 0.0249 84.8 77-142

Toluene 0.0227 0.0050 " 0.0249 90.8 55-158

Trichloroethene 0.0215 0.0050 " 0.0249 86.0 71-139








Benzene 0.0258 0.0050 mg/kg 0.0250 103 58-143 7.21 25

Toluene 0.0263 0.0050 " 0.0250 105 55-158 14.9 25

Benzene 0.0258 0.0050 " 0.0250 103 58-143 7.21 25

Chlorobenzene 0.0255 0.0050 " 0.0250 102 76-145 16.9 25

1,1-Dichloroethene 0.0209 0.0050 " 0.0250 83.4 77-142 1.44 25

Toluene 0.0263 0.0050 " 0.0250 105 55-158 14.9 25

Trichloroethene 0.0235 0.0050 " 0.0250 93.8 71-139 8.85 25










11I0676 09/15/2011 16:30 SCPWTL 3501-09










Benzene 0.0197 0.0050 mg/kg 0.0249 ND 79.1 37-149

Toluene 0.0183 0.0050 " 0.0249 ND 73.6 22-166

Benzene 0.0197 0.0050 " 0.0249 ND 79.1 37-149

Chlorobenzene 0.0132 0.0050 " 0.0249 ND 52.9 44-157

1,1-Dichloroethene 0.0188 0.0050 " 0.0249 ND 75.6 38-165

Toluene 0.0183 0.0050 " 0.0249 ND 73.6 22-166

Trichloroethene 0.0144 0.0050 " 0.0249 ND 57.9 51-146



Surrogate: Toluene-d8 0.0256 " 0.0249 103 51-161





Benzene 0.0194 0.0050 mg/kg 0.0250 ND 77.6 37-149 1.84 25

Toluene 0.0187 0.0050 " 0.0250 ND 74.8 22-166 1.66 25

Benzene 0.0194 0.0050 " 0.0250 ND 77.6 37-149 1.84 25

Chlorobenzene 0.0134 0.0050 " 0.0250 ND 53.6 44-157 1.38 25

1,1-Dichloroethene 0.0247 0.0050 " 0.0250 ND 98.9 38-165 26.8 25 QM-08

Toluene 0.0187 0.0050 " 0.0250 ND 74.8 22-166 1.66 25







11I0676 09/15/2011 16:30 SCPWTL 3501-09






Trichloroethene 0.0141 0.0050 " 0.0250 ND 56.6 51-146 2.21 25













11I0676 09/15/2011 16:30 SCPWTL 3501-09

Polychlorinated Biphenyls by EPA Method 8082 - Quality Control



Batch AI11913 - EPA 3540C Soxhlet


PCB-1016 ND 0.20 mg/kg

PCB-1221 ND 0.20 "

PCB-1232 ND 0.20 "

PCB-1242 ND 0.20 "

PCB-1248 ND 0.20 "

PCB-1254 ND 0.20 "

PCB-1260 ND 0.20 "

PCB-1262 ND 0.20 "

Surrogate: Tetrachloro-meta-xylene 0.0132 " 0.0125 106 10-150

Surrogate: Decachlorobiphenyl 0.0138 " 0.0125 110 32-190


PCB-1016 0.0933 0.20 mg/kg 0.100 93.3 61-153

PCB-1260 0.108 0.20 " 0.100 108 60-164




PCB-1016 0.111 0.20 mg/kg 0.100 111 61-153 17.3 35

PCB-1260 0.126 0.20 " 0.100 126 60-164 15.5 35




PCB-1016 0.280 0.20 mg/kg 0.250 ND 112 61-153

PCB-1260 0.324 0.20 " 0.250 ND 130 60-164







11I0676 09/15/2011 16:30 SCPWTL 3501-09

Polychlorinated Biphenyls by EPA Method 8082 - Quality Control



Batch AI11913 - EPA 3540C Soxhlet





PCB-1016 0.372 0.20 mg/kg 0.250 ND 149 61-153 28.2 35

PCB-1260 0.437 0.20 " 0.250 ND 175 60-164 29.5 35 QM-07









11I0676 09/15/2011 16:30 SCPWTL 3501-09

Semivolatile Organic Compounds by EPA Method 8270C - Quality Control



Batch AI12137 - EPA 3540C Soxhlet MS


Acenaphthene ND 0.062 mg/kg

Acenaphthylene ND 0.062 "

Anthracene ND 0.062 "

Benzidine ND 1.6 "

Benzo (a) anthracene ND 0.33 "

Benzo (a) pyrene ND 0.062 "

Benzo (b) fluoranthene ND 0.062 "

Benzo (g,h,i) perylene ND 0.062 "

Benzo (k) fluoranthene ND 0.062 "

Benzoic acid ND 1.6 "

Benzyl alcohol ND 0.66 "

Bis(2-chloroethoxy)methane ND 0.33 "

Bis(2-chloroethyl)ether ND 0.33 "

Bis(2-chloroisopropyl)ether ND 0.33 "

Bis(2-ethylhexyl)phthalate ND 0.33 "

4-Bromophenyl phenyl ether ND 0.33 "

Butyl benzyl phthalate ND 0.33 "

4-Chloro-3-methylphenol ND 0.33 "

4-Chloroaniline ND 0.66 "

2-Chloronaphthalene ND 0.33 "

2-Chlorophenol ND 0.33 "

4-Chlorophenyl phenyl ether ND 0.33 "

Chrysene ND 0.062 "

Di-n-butyl phthalate ND 0.33 "

Di-n-octyl phthalate ND 0.33 "

Dibenz (a,h) anthracene ND 0.062 "







11I0676 09/15/2011 16:30 SCPWTL 3501-09






Dibenzofuran ND 0.33 "




3,3´-Dichlorobenzidine ND 0.66 "

2,4-Dichlorophenol ND 0.33 "

Diethyl phthalate ND 0.33 "

Dimethyl phthalate ND 0.33 "

2,4-Dimethylphenol ND 0.33 "

4,6-Dinitro-2-methylphenol ND 1.6 "

2,4-Dinitrophenol ND 1.6 "

2,4-Dinitrotoluene ND 0.33 "

2,6-Dinitrotoluene ND 0.33 "

1,2-Diphenylhydrazine ND 0.33 "

Fluoranthene ND 0.062 "

Fluorene ND 0.062 "

Hexachlorobenzene ND 0.33 "

Hexachlorobutadiene ND 0.33 "

Hexachlorocyclopentadiene ND 1.6 "

Hexachloroethane ND 0.33 "

Indeno (1,2,3-cd) pyrene ND 0.062 "

Isophorone ND 0.33 "

2-Methylnaphthalene ND 0.062 "

2-Methylphenol (o-cresol) ND 0.33 "

3 & 4-Methylphenol (m,p-cresol) ND 0.33 "

N-Nitrosodi-n-propylamine ND 0.33 "







11I0676 09/15/2011 16:30 SCPWTL 3501-09






N-Nitrosodimethylamine ND 0.66 "

N-Nitrosodiphenylamine ND 0.33 "

Naphthalene ND 0.062 "

2-Nitroaniline ND 1.6 "



Nitrobenzene ND 0.33 "

2-Nitrophenol ND 1.6 "

4-Nitrophenol ND 1.6 "

Pentachlorophenol ND 1.6 "

Phenanthrene ND 0.062 "

Phenol ND 0.33 "

Pyrene ND 0.062 "


2,4,5-Trichlorophenol ND 0.33 "

2,4,6-Trichlorophenol ND 0.33 "

Surrogate: 2-Fluorobiphenyl 3.20 " 4.00 80.1 61-117

Surrogate: 2-Fluorophenol 3.06 " 4.00 76.4 50-113

Surrogate: Nitrobenzene-d5 3.13 " 4.00 78.2 47-123

Surrogate: p-Terphenyl-d14 3.46 " 4.00 86.6 63-133

Surrogate: Phenol-d6 3.20 " 4.00 80.0 49-119

Surrogate: 2,4,6-Tribromophenol 3.12 " 4.00 78.0 52-129


Acenaphthene 1.18 0.062 mg/kg 2.00 59.2 35-90

4-Chloro-3-methylphenol 3.07 0.33 " 4.00 76.7 55-105







11I0676 09/15/2011 16:30 SCPWTL 3501-09






2-Chlorophenol 3.06 0.33 " 4.00 76.6 55-100

1,4-Dichlorobenzene 1.55 0.33 " 2.00 77.4 55-100

2,4-Dinitrotoluene 1.44 0.33 " 2.00 72.2 65-100

N-Nitrosodi-n-propylamine 1.35 0.33 " 2.00 67.4 45-80

4-Nitrophenol 2.68 1.6 " 4.00 67.1 60-110

Pentachlorophenol 2.65 1.6 " 4.00 66.3 60-115

Phenol 2.79 0.33 " 4.00 69.8 55-100

Pyrene 1.57 0.062 " 2.00 78.7 50-100

1,2,4-Trichlorobenzene 1.51 0.33 " 2.00 75.4 55-95








Acenaphthene 1.13 0.062 mg/kg 2.00 56.6 35-90 4.58 25

4-Chloro-3-methylphenol 3.07 0.33 " 4.00 76.8 55-105 0.228 25

2-Chlorophenol 2.80 0.33 " 4.00 69.9 55-100 9.15 25

1,4-Dichlorobenzene 1.39 0.33 " 2.00 69.6 55-100 10.5 25

2,4-Dinitrotoluene 1.44 0.33 " 2.00 71.8 65-100 0.556 25

N-Nitrosodi-n-propylamine 1.24 0.33 " 2.00 61.8 45-80 8.74 25

4-Nitrophenol 2.69 1.6 " 4.00 67.2 60-110 0.0745 25

Pentachlorophenol 2.65 1.6 " 4.00 66.2 60-115 0.189 25

Phenol 2.60 0.33 " 4.00 65.0 55-100 7.15 25







11I0676 09/15/2011 16:30 SCPWTL 3501-09






Pyrene 1.56 0.062 " 2.00 78.0 50-100 0.893 25

1,2,4-Trichlorobenzene 1.35 0.33 " 2.00 67.4 55-95 11.3 25








Acenaphthene 1.06 0.062 mg/kg 2.00 ND 52.8 35-90

4-Chloro-3-methylphenol 2.64 0.33 " 4.00 ND 65.9 55-105

2-Chlorophenol 2.73 0.33 " 4.00 ND 68.2 55-100

1,4-Dichlorobenzene 1.36 0.33 " 2.00 ND 68.0 55-100

2,4-Dinitrotoluene 1.31 0.33 " 2.00 ND 65.4 65-100

N-Nitrosodi-n-propylamine 1.20 0.33 " 2.00 ND 59.8 45-80

4-Nitrophenol 2.52 1.6 " 4.00 ND 63.1 60-110

Pentachlorophenol 2.90 1.6 " 4.00 ND 72.5 60-115

Phenol 2.44 0.33 " 4.00 ND 60.9 55-100

Pyrene 1.62 0.062 " 2.00 ND 80.8 50-100

1,2,4-Trichlorobenzene 1.32 0.33 " 2.00 ND 66.2 55-95











11I0676 09/15/2011 16:30 SCPWTL 3501-09









Acenaphthene 1.17 0.062 mg/kg 2.00 ND 58.4 35-90 10.1 25

4-Chloro-3-methylphenol 2.99 0.33 " 4.00 ND 74.8 55-105 12.6 25

2-Chlorophenol 2.94 0.33 " 4.00 ND 73.4 55-100 7.31 25

1,4-Dichlorobenzene 1.47 0.33 " 2.00 ND 73.4 55-100 7.71 25

2,4-Dinitrotoluene 1.48 0.33 " 2.00 ND 74.2 65-100 12.8 25

N-Nitrosodi-n-propylamine 1.26 0.33 " 2.00 ND 62.9 45-80 4.97 25

4-Nitrophenol 2.82 1.6 " 4.00 ND 70.5 60-110 11.1 25

Pentachlorophenol 3.10 1.6 " 4.00 ND 77.4 60-115 6.54 25

Phenol 2.64 0.33 " 4.00 ND 66.0 55-100 8.03 25

Pyrene 1.79 0.062 " 2.00 ND 89.6 50-100 10.3 25

1,2,4-Trichlorobenzene 1.42 0.33 " 2.00 ND 71.2 55-95 7.35 25




Surrogate: p-Terphenyl-d14 4.06 " 4.00 101 63-133









11I0676 09/15/2011 16:30 SCPWTL 3501-09

Notes and Definitions

>220 >220

D-09 Results in the diesel organics range are primarily due to overlap from a heavy oil range product.

QM-01 The spike recovery for this QC sample is outside of established control limits possibly due to a sample matrix interference.

QM-04 High RPD and/or poor percent recovery may reflect sample non-homogeneity.

QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS

recovery.

QM-08 The RPD was outside acceptance limits for MS/MSD, possibly due to matrix interference. The LCS and/or LCSD were within

acceptance limits showing that the laboratory is in control and the data is acceptable.

QM-4X The spike recovery was outside of QC acceptance limits for the MS and/or MSD due to analyte concentration at 4 times or greater

the spike concentration. The QC batch was accepted based on LCS and/or LCSD recoveries within the acceptance limits.

R-01 The Reporting Limit for this analyte has been raised to account for matrix interference.

R-06 The Reporting Limits for this analysis have been raised to account for matrix interference.

DET Analyte DETECTED

ND Analyte NOT DETECTED at or above the reporting limit

NR Not Reported

dry Sample results reported on a dry weight basis

RPD Relative Percent Difference

PQL Practical Quantitation Limit

K PRIME, INC. LABORATORY REPORT

K PRIME PROJECT: 9984 CLIENT PROJECT: 1110676

METHOD: GRO-GASOLINE RANGE ORGANICS SAMPLE TYPE: SOIL REFERENCE: EPA 80158 UNITS: mg/Kg

SAMPLE ID LAB NO. DATE TIME BATCH DATE MRL SAMPLE GRO SAMPLED SAMPLED ID ANALYZED CONC PATTERN

COMP 1A-10 0.5'-2.5' 95142 09/13/2011 10:30 092011S1 09/20/2011 1.00 ND COMP 2A-2D 0.5'-2.0' 95143 09/13/2011 11:25 092011S1 09/20/2011 1.00 ND COMP 3A-3D 0.5'-1.5' 95144 09/13/2011 13:00 092011S1 09/20/2011 1.00 ND COMP 4A-4D 0.5'-1.0' 95145 09/13/2011 14:00 092011S1 09/20/2011 1.00 ND

NOTES: ND- NOT DETECTED AT OR ABOVE THE STATED METHOD REPORTING LIMIT NA- NOT APPLICABLE OR AVAILABLE MRL - METHOD REPORTING LIMIT AE - UNKNOWN HYDROCARBON WITH A SINGLE PEAK AN - UNKNOWN HYDROCARBON WITH SEVERAL PEAKS AS - HEAVIER HYDROCARBON THAN GASOLINE CONTRIBUTING TO GRO VALUE CO- HYDROCARBON RESPONSE IN GASOLINE RANGE BUT DOES NOT RESEMBLE GASOLINE

APPROVED BY~~ , ])2.,~!?/~o I ( DATE:

I

K PRIME, INC. METHOD BLANK ID: B092011S1 LABORATORY QC REPORT SAMPLE TYPE: SOIL

METHOD: GRO-GASOLINE RANGE ORGANICS REFERENCE: EPA 8015B BATCH#: 092011S1

DATE EXTRACTED: 09/20/2011 DATE ANALYZED: 09/20/2011

UNITS: mg/kg

COMPOUND NAME

ITPH-G

REPORTING LIMIT 1.00

SAMPLE CONC

ND

NOTES: ND - NOT DETECTED AT OR ABOVE THE STATED REPORTING LIMIT NA- NOT AVAILABLE OR APPLICABLE

ACCURACY (MATRIX SPIKE)

SAMPLE ID: DUPLICATE ID:

BATCH#: SAMPLE TYPE:

UNITS:

DATE EXTRACTED: DATE ANALYZED:

L092011S1 D092011S1 092011S1

SOIL mg/kg

09/20/2011 09/20/2011

PARAMETER SPIKE SAMPLE SPIKE RECOVERY LIMITS ADDED RESULT RESULT (%) (%)

TPH-G 5.00 ND 5.22 104 60-140

PRECISION (SPIKE DUPLICATE)

COMPOUND NAME REPORTING SPIKE DUPLICATE RPO LIMITS LIMIT RESULT RESULT (%) (%)

TPH-G 1.00 5.22 5.29 1.4 ±20

NOTES: ND- NOT DETECTED AT OR ABOVE THE STATED REPORTING LIMIT NA- NOT AVAILABLE OR APPLICABLE

,•

SOIL DISPOSAL ANALYTICAL REQUIREMENTS <1,500 YDS OF STOCKPILED SOIL

SCTPW ARNOLD DRIVE ROUNDABOUT

TOTAL OF 4 4-POINT COMPOSITE SAMPLE REQUIRED

ANALYZE 1 SAMPLE FOR:

TPHgasoline, BTEX and MtBE by EPA Method 8260 ltPHdiesel by EPA Method 8015modified -Oil and Grease by Standard Method 5520 with Silica Gel Cleanup tAM 17 Metals*

.-11CBs by EPA Method 8080 ~voes & Phenol by EPA Method 8270 ~OCs by EPA Method 8260 -"RCI

ANALYZE REMAINING 3 SAMPLES FOR:

TPHgasoline, BTEX and MtBE by EPA Method 8260 )fPHdiesel by EPA Method 8015modified ,,Oil and Grease by Standard Method 5520 with Silica Gel Cleanup ,,CAM 17 Metals*

*If total lead greater than 50 ppm, then analyze for STLC lead

SAMPLING PROTOCOL

Four (4) individual sample tubes will be collected at various locations on the stockpile (if stockpiled) at depths of no less than 1 foot below the surface. The 4 tubes collected for each sample will be labeled as a group (Cl Comp I .of 4, 2of 4, etc) and composited in the analytical laboratory as one sample prior to analysis. In-situ samples will also be collected and handled in the same manner. Include a map showing the sample locations along with the analytical data.

9/15/2011

SOIL DISPOSAL ANALYTICAL REQUIREMENTS <l,500 YDS OF STOCKPILED SOIL

SCTPW ARNOLD DRIVE ROUNDABOUT

TOTAL OF 4 4-POINT COMPOSITE SAMPLE REQUIRED

ANALYZE 1 SAMPLE FOR:

TPHgasoline, BTEX and MtBE by EPA Method 8260 TPHdiesel by EPA Method 8015modified Oil and Grease by Standard Method 5520 with Silica Gel Cleanup CAM 17 Metals* PCBs by EPA Method 8080 SVOCs & Phenol by EPA Method 8270 VOCs by EPA Method 8260 RCI

ANALYZE REMAINING 3 SAMPLES FOR:

TPHgasoline, BTEX and MtBE by EPA Method 8260 TPHdiesel by EPA Method 8015modified Oil and Grease by Standard Method 5520 with Silica Gel Cleanup CAM 17 Metals*

*If total lead greater than 50 ppm, then analyze for STLC lead

SAMPLING PROTOCOL

Four (4) individual sample tubes will be collected at various locations on the stockpile (if stockpiled) at depths of no less than 1 foot below the surface. The 4 tubes collected for each sample will be labeled as a group (CJ Comp 1 of 4, 2of 4, etc) and composited in the analytical laboratory as one sample prior to analysis. In-situ samples will also be collected and handled in the same manner. Include a map showing the sample locations along with the analytical data.

9/15/2011

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