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The solid constitute the most extensive group of insulating material. Based on
physical and chemical properties, structure and production characteristic, the solid
insulating material are divided into several subgroups such as laminated plastic, paper ad
fabrics. Furthermore, the liquid insulating are insulating oils, which include petroleum,
vegetable oil and synthetic oil. The liquid insulating has different types of insulation from
each other in viscosity and in the value of their electrical properties. The gases insulating
include air and sulfur hexafluoride. Air is a natural insulated use for air gape in electrical
machinery and electrical equipments.
1.0.1 Insulation in transformer
Transformer is a static device that can transform electrical energy from one
circuit to another without any direct electrical connection. It is the exclusive use of
electric power for electromagnetic induction to transfer power at the same
frequency, usually with changed values of voltage and current. The transformer has
two parts to produce magnetic flux is primary and secondary winding. The primary
winding can be produce magnetic flux when it is connected to electrical sources
such as power supply. The magnetic flux produces by primary winding will be pass
through the core. The varying magnetic flux will be produce to other core. This core
called the secondary winding. The secondary winding also would on the same core
and can give output for transformer [1]. The figure 1.1 show the magnetic flux
produced by primary and secondary winding.
Figure 1.1: The flux magnet produced by coil [1]
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The heat in the winding will be moved to the oil for generated in the
transformer. The oil will be heated and will flow into the radiator by convection. The
temperature of transformer will be increases are entirely due to heat in transformer
does not disappear that right. It will cause damage to the paper insulating and fluids
insulating medium in transformers. Temperature control is important to ensure a
long life for the transformer. Transformer cooling system can be accelerated rate of
heat dissipation in the transformer.
The critical part of a modem power system is the transformer life
management but the transformer life depended on the insulating medium use. The
strength will be increase in electrical insulation but it is depends on the distance
between coils and winding in a transformer. Most of transformers used mineral oil
as an insulator and also acts as a cooling medium. The mineral oil is an excellent
dielectric and cooling medium. Moreover, the limitations of mineral oil are low
biodegradation and panic threats to human beings and ecosystem. Nevertheless,
the mineral oil has poor performance at high temperature [13]. That why it is
restricted in ecologically sensitive locations (indoor type applications). Furthermore,
this oil is high cost, it used of such oils certain special transformer application only.
There are several important features in determining the oil is suitable for use in
transformer and it depends on the physical, chemical and electrical properties in
order to achieve characteristics of insulation in the transformer. Figure 1.2 show
electrical power transformers.
Figure 1.2: power transformer
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breakdown voltage, permittivity and lost factor. It also must be analyze the result base on
chemical and electrical characteristic and compare result with the standard.
1.4 Methodology
This project has several steps that must be followed during the conduct of the
project. It seeks to ensure that the project has to run smoothly and successfully as the
objectives of the project. The first step that needs to be conducted that study the sunflower
oil and mineral oil as well as the study of the transformer. Besides, it also needs to identify
the characteristics of the sunflower oil and also mineral oil that it meets the required
characteristics to be used as transformer oil. After identifying the characteristics of each
sample of oil, the preparation is required where the project is to use different brands of
sunflower oil that Sunlico and Adela and it has made in Malaysian. For each brand will be
divided into two oil that where the oil should not be heated and heated. So, the project
provides all four samples, two samples of oil that has been heated and the two oils are
unheated on both the brand. The next step to make measurement based on physical and
electrical properties. After get on each test result, it should be analyzed so that the oil is
suitable or not site as transformer oil. Figure 1.3 shows flow chat for this project
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Figure 1.3: Project flow
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1.5 Outline
This thesis has five chapters. At the first chapter discuss about the objective and
the scope in this project. Chapter 2 discuss about the literature review which is mineral oil,
sunflower oil, electrical and physical properties. Chapter 3 discusses about the procedure
in this project. Chapter 4 discusses about the result and analysis in and lastly chapter 5
discuses the conclusion and recommendation in this project.
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CHAPTER 2
LITERATURE REVIEW
2.0 Mineral oil
Mineral oil used as a coolant insulating fluids in power transformer. The first idea
for mineral oil is used in 1892 by general electric in transformer that been designed by Prof
Elihu Thomson [4]. The mineral oils such as petroleum have some structure such as
Paraffinic, aromatic and naphthenic. It is obtained after making the fractional distillation of
crude petroleum. Until today, mineral oil are used in liquid filled transformer as the
insulating liquid. When in the service, the mineral oil liquid in a transformer undergo a
constant heat produce by the operation of the transformer and consequently it degradation
because of ageing process. The dark color formation and resin acids or mud liquid is the
result of ageing process.
Oil to be used in transformers are made by many regional and international refining
companies, each using a particular crude oil and refined oil, such as shown in figure 2.1.
Figure 2.1: Classification of mineral oil
mineral oil
crude
mineral oil
refined
mineral oil
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The aim for refining mineral oil is to remove or reduce waxes, sulphur, nitrogen and
oxygen compound and the aromatic hydrocarbon. After refining process, the mineral oil
has good insulation properties. Table 2.0 show the main type of mineral oil
Table 2.0: The main type of mineral oil
Type of mineral oil Chemical structure comment
Paraffin
Methane (CH4) is a gas
normal butane (C4H10) and
iso butene
Naphtene
It has ring structures withsix carbon atoms (withinsix-member rings) orfourteen carbon atoms(withinthree member rings)
Aromatic
It has six-member ringstructures and two groups:mono-aromatics (singlerings) and poly-aromatics(twoor more rings).
Mineral oil have several advantages over the other types of oils, it has higher
resistance to aging method. The transformer oil must have required low viscosity because
it can better for cooling of transformer [5, 6]. Usually, the mineral oil used for insulation
because it has excellent dielectric properties such as high dielectric strength and low
dielectric losses but poor in flash point and fire point characteristics. However, the oils are
non biodegradable and good long term performance [2, 3].
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The transformer oils are classified as liquid insulating which a good insulating in
transformer, it has some of properties that need to know to determine to provide the oil to
use into transformer. Some of the properties that need to know is physical, chemical, and
electrical properties. There are some basic factors to show the electrical properties of the
transformer oil, such as breakdown voltage, dielectric dissipation factor, dielectric constant
and volume resistivity. Breakdown voltage is most important for estimate the transformer
oil capacity of tolerance to electrical stress. When the dielectric dissipation factor increases
as the resistance reduces, dielectric dissipation factor and resistivity directly affect the
insulation of the electrical equipment.
2.0.1 Mineral oil properties
All the insulation oil for transformer should follow this specification. Table
2.1 show the mineral oil properties
Table 2.1: mineral oil properties [13]
PropertyTest
methodMineral oil
Density at 20C,kg/dm3 ISO 3675 0.88
Viscosity at 40CcSt
ASTMD445
8.9
Viscosity at -30CcSt
ASTMD445
1.080
Pour point,C
ISO 3016 -63
Flashpoint,C
ISO 2719 146
Water content,ppm
IEC 60814 70
tanat 90C (50Hz)IEC 60247 0.001
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2.1 Sunflower oil
Natural ester fluids base on renewably sourced has provide to been used for
insulating liquid in transformer. The natural ester oil was used in transformers since 1990.
This is because the oil has the properties better than traditional mineral oils. In the recent
years, the natural ester appear of clean and function technologies in high demand to used
as ecofriendly but in newest version, it are derived by compressing plant and animal tissue
such as natural ester is slower ageing rate, less total operating cost (initial cost and
operating cost) and low noise level. Moreover, vegetable oil could be reduce the
exploitation and end life cost in transformers. It also could be safety and health problem
and appropriated responds to environment [2].
The natural esters like sunflower oil are used successfully in transformers [2]. For
this project, the sunflower oil use as an alternative for mineral oil in transformer because it
is non-fossil and also 100% environmental friendly. The first extraction of sunflower oil in
Europe was in the early 18th century. The sunflower oil is a combination of
monounsaturated and polyunsaturated fats at low levels of saturated fat, but it provides a
lot of vitamin E compare with other vegetables. Besides, the sunflower oil also has health
benefits, a good frying performance and value for a light taste.
Sunflower oil has a fatty acid consisting of a linear hydrocarbon chain and ended
with carbolic function. The molecules contain in the chain has an even number of carbon
atoms and the chain may be saturated or unsaturated chain is compose of mono-, tri-and
di-. Then even numbers of carbon atoms normally used for number 8 to 22 in triglycerids.
HOOC-(CH2)16-CH3 is a crude formula that represents the expression of C18:0 in which
both queries numbers correspond to the number of carbon atoms and unsaturated chains
to bound (s) in each molecule [7]. The natural of the fatty acids components of triglycerides
plays an important role for determining the physical chemical properties of bio-oil. Table
2.2 show the characteristic by the relative quantities of fatty acids.
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Table 2.2: Typical fatty acid profiles (%) of sunflower oil [7]
Fatty acids Sunflower oils
C16:0 5.77
C18:0 3.97
C18:1 27.2
C18:1(OH)* 0.00
C18:2 59.2
C18:3 0.23
C20:0 0.24
C20:1 0.13
C22:0 1.44
C22:1 0.00
Other 1.82
Therefore, higher viscosity of the oil because the chemical is stable in saturated
fatty acid but in triple unsaturated fatty acids, the viscosity is lower because the chemical is
unstable [2]. The sunflower oil insulation have tabulated in table 2.3. It shows sunflower oil
properties.
Table 2.3: Sunflower oils insulation properties [16]
Property Sunflower oil
Breakdown voltage (kV/m) 34
Flash point (C) 260
Fire point (C) 270
Viscosity (cSt) 132
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2.2 Electrical properties
2.2.1 Breakdown voltage
Breakdown voltage is one of important properties to define the efficiency of
oil as an insulator. The ability of the oil (acting as a dielectric) to oppose the flow of
a current is determine by test which show its dielectric strength. Among these are
the specific of resistance that a dielectric offers under moderate conditions of
voltage. Moreover, the ability to prevent arcing between two electrodes at high
electric potentials or to prevent arcing between the electric source and ground. The
quality of the oil can be influenced by the presence of impurities like humidity,
particles and gases. The presence of water in the oil can cause a rapid drop in the
dielectric strength. However, dielectric strength will increase if there are impurities
in the oil. Due to oil is used for insulation in a transformers, it have to release of
moisture and oxidation in the oil for need to make a strong insulating material in
transformers. [12].
The liquid fraction in the gas is connection dependent avalanche ionization
of atoms, causing the collision of electrons that have been supplied in the field. The
electrons must be removed from the liquid cathode available. Pure liquid is a liquid
that has a pure chemical which can not contain any impurities and simple structure
in pure chemistry. The breakdown mechanism explains breakdown only of highly
pure liquid and do not applied commercially available in liquid. Conductivity may be
obtained after the electric field is low at less than 1kV/cm. it will be due to impurities
found after purification. However, the current will increase as the area is high (>
100kV/cm) [12].
Breakdown strength affect the breakdown strength in oil once will affect the
insulation in the transformer. There are several factors that can affect the
breakdown strength to affect the breakdown strength of oil such as the field,
separation gap, the cathode work function and cathode temperature. Therefore, the
dielectric fluid includes a conduction mechanism of charge and the process leading
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to the breakdown. It is also important to develop high-voltage technology and pulse
power systems to form a transformer that works well. [12].
2.2.2 Dielectric loss, Tan
Dielectric dissipation factor is important properties in the liquid insulating.
The electrical energy absorbed by the material from the electric field and it will
appears in the form of heat within the material. The dielectric dissipation factor can
be expressed as
(1.0)
The electrical loss tangent is defined by the angle between the capacitor
impedance vector and negative reactive axis [16]. Figure 2.2 show the leakage
current per phase to an insulator.
Figure 2.2: The leakage current per phase to an insulator
The leakage current leads the voltage by 90 because the voltage is
instantaneous voltage. If not insulating, the current leads the voltage with an angle
little bit shorter the 90. It can generates a leakage current,
and the
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displacement current . From the phasor diagram in figure 2.2, it can be
represents the value of
. From this equation, applying the substitution on
I and IC, it will give final expression of
(2.0)
The dissipation according IEC 60247 is the tangent of the loss angle here is
described as the angle difference between applied voltage and the resulting current
deviation from
. The low value of tangent delta is needed so that insulation oil
can works as good insulation oil. If the value of tangent is high, it could be an
indication of presence of contaminants in liquid transformer.
2.2.3 Permittivity
The dielectric constant is purely a relative number comparing the capacity of
a material for storing electricity to that of air. It also depends on the physical
parameters of temperature density, molecular weight and dipole moment. The
capacity of the material for storing electricity decreases as the frequency rises
above the corresponding orientation time. The dipoles not longer fully orient
themselves, the material could be hold as large an electric decrease [16].
The relationship between the dielectric constant and the loss factor as the
frequency can be increases. The equation for the complex dielectric constant:
(3.0)
Where the imaginary represents the magnitude of the dielectric loss can
be contribute by the leakage current and the polarization, is complex permittivity.
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2.3 Physical properties
2.3.1 Viscosity
Viscosity of liquid used in electrical equipment can be provided the
information on flow characteristic and heat transfer properties. It is known as the
drag where it will measure the frictional properties of the liquid. It also has a
function of temperature and pressure in the liquid. While the viscosity of liquid and
gases will be change with temperature and pressure, it can be effect viscosity in
different ways [8]. The function of the moving part such as pump can be effect if the
viscosity is higher than at room temperature. The start up of apparatus in cold
climates will be effect in high viscosity. Viscosity of the oil will be affected by the
pressure drop, flow rate of oil and oil cooling system.
Dynamic viscosity and kinematic viscosity is two distinct forms in the
viscosity. Dynamic viscosity is the tangent force in the slide. The area of tangent
force per units is required to slide one layer (A) against another layer (B) are
maintain at a unit distance [9]. Figure 2.3 shows the simple shear of the liquid film.
Figure 2.3: Simple shear of the liquid film [9]
In figure 2.3, Force (F) causes layers A and B to slides at velocities V 1and
V2. Since the viscosity of the fluids is defined is a measure of the resistive flow
under gravity [9]. Kinematic viscosity requires of density of the liquid () at the
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pressure and the time of flow is proportional to the kinematic viscosity of the fluids
(). Kinematic can be by the relationship [9].
(4.0)
Where is dynamic viscosity.
The units of kinematic viscosity is the centistokes (cSt) and used by the
international standard organization (ISO). Viscosity classification using ISO shows
in table 2.4.
Table 2.4: ISO grade classification (ISO 3446) [10]
ISO viscosity grade
notification
Kinematic viscosity
limits, cSt at 40C
Midpoint kinematic
viscosity, cSt at
40CMin Max
ISO VG 2
ISO VG 3
ISO VG 5
ISO VG 7
1.98
2.88
4.14
6.12
2.42
3.52
5.06
7.48
2.2
3.2
4.6
6.8
ISO VG 10ISO VG 15
ISO VG 22
ISO VG 32
ISO VG 46
ISO VG 68
ISO VG 100
ISO VG 150
9.0013.5
19.8
28.8
41.4
61.2
90.0
135
11.016.5
24.2
35.2
50.6
74.8
110
165
1015
22
32
46
68
100
150
ISO VG 220
ISO VG 320
ISO VG 460
ISO VG 680
ISO VG 1000
ISO VG 1500
198
288
414
612
900
1350
242
352
506
748
1100
1650
220
320
460
680
1000
1500
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2.3.2 Moisture content
Moisture in transformer oil has the effects the insulation of solid and liquid
insulation. Therefore, the dielectric breakdown strength of the insulation will have
the effect of the water. Its water content will be rises above two to three percent by
weight after the breakdown of the paper insulation decreases [11]. Moisture in the
oil shows up above 50 to 60ppm but it is depends on temperature. Accepted of
water in oil are shows in table 2.5.
Table 2.5: Maximum allowable moisture in oil [12]
Voltage level (kV) Maximum moisture (ppm)
5 30
15 30
35 25
69 20
138 and up 15
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CHAPTER 3
METHODOLOGY
3.0 Sample
In this experiment, the sunflower oil use for the sample but it have different brand
from the local market. Every brand needs to provide two samples of the oils which
one of the sample have to remove moisture and other samples used the original oil
which dont remove moisture of the oils. It aims to compare between the samples
from in terms of electrical and physical properties. Therefore, it is should to make
measurements using several parameters including breakdown strength, dielectric
dissipation, permittivity, viscosity and moisture content
3.1 The oil sample conditioning
The samples have to prepare bottles or jar was required to clean to prevent
moisture in the oil increased in the period in which the oil is stored in the container. In the
event of humidity in oil will be affect to the dielectric properties such as dielectric loss and
breakdown stress in the oil. Fuel humidity is likely to require a reduction of thermal aging
on the dielectric properties. Therefore, test humidity needed to reduce humidity on the oil
through a vacuum process. The oven equipped with a heating device to speed up the
evaporation process using a low temperature to remove moisture. It can reduce the
problem of unstable thermal degradation of the materials. The temperature use in this oven
is 100C and took one day for this process. Figure 3.1 shows the sample after heated
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Figure 3.0: The sample after heated
3.2 Breakdown voltage measurement
The breakdown voltage was measured according standard IEC 60156 insulating
liquid. It also measured for this property containing two electrodes of specified gap is
2.5mm and high voltage applied in this sample. The frequency is 50Hz will be applied with
increasing the voltage at a rate of 2kV/s until breakdown occurs. This measure needs to
take a reading at least five value of the average value from this samples. There has
several procedures that should be followed. Figure 3.1 show breakdown voltage
equipment.
Figure 3.1: breakdown voltage equipment
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3.2.1 Sample preparations
The electrode and test cup should be clean up and dry until completely. It is
performed to prevent pollution or have oil or other solvent during this test. If
have another solution, the average value is not same or opposite of the
value on electrical properties in literature review.
The distance between the two electrodes must set 2.5mm. After that, the
electrode should be locked to prevent movement of the electrode such that
the electrode comes into contact between the electrodes. Figure 3.2 show
gap between electrode
Figure 3.2: Gap 2.5mm in test cup
The samples have to be filled in the test cup until it is almost full and will
leave about 3% of the cup as a free space for air. Time must be set for
make measurement.
3.2.2 Measurement procedures
After measurement, record the data for the first measuring. After record n
want to start next measure, should be wait 1 minute that have no gas
bubbles present within the electrode gap.
2.5mm
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This measurement needs to be repeated with the same sample up to 5
times of the measurement to see the average value.
3.3 Viscosity measurement
This test measure according to the ASTM D445 and this measurement equipment
named as viscometer. It intended to get the viscosity found in the oil. This viscometer used
spindle to find the speed that should be used to take a more accurate reading of a sample.
The spindle has a variety of different sizes and it depends on the viscosity, spindle use a
small sample size which is suitable for high viscosity. The measurement of sunflower oil
use spindle size s-02. Figure 3.2 show viscometer equipment for measure viscometer.
Figure 3.3: Viscometer
The speed used to take readings of 100, 60, 50, 30, 20 and 10 rpm where in each
speed has some value percentage torch to determine the necessary speed to make
viscosity measurements for these samples. The value for percentage torch needed for a
speed is above 10% because the value for viscosity is accurate. If the value is below 10%,
Spindle(s-02)
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the value of viscosity is not accurate. Therefore, the speed cant be used to take readings
for the viscosity. So, this sample used speed 100rpm and the value of torch is 28.4%.
3.3.1 Measurement procedure
Make sure the spindle and beaker to be used for this measurement
in a clean and dry before use. Its because, to avoid no solution
available on the equipment prior to conducting the test.
500ml oil must be prepared in a beaker and make sure there are no
air bubbles in the spindle. The used of oil also depends on the
spindle where the oil is needed for these measurements have
exceeded any marks or labels on the spindle.
Set time and speed required for this test. The time required is 5
minutes while the speed is 100rpm after knowing the torch at each
speed in which more than 10%.
Readings must be repeated three times on each sample during the
test. Record for all the result.
3.4 Moisture content measurement
The measurement of moisture in oil has two methods which Karl Fischer reaction
method and the pressure gauge method. Usually, this test measured according standard
IEC 60814 and use Karl Fischer for this test. The oil in the transformer is designed to
provide good electrical insulation for work in the transformer. When the moisture in the oils
has to increase, the properties of the oil will be reduced at the expense of the breakdown
voltage. However, the properties of the oil are important when the temperature changes in
a transformer.
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While performing this test, the oil temperature must be set to see a change of water
in the oil. Temperature is also important where the acid will be formed during the oxidation
of the oil. Therefore, the water will dissolve in oil due to acids formed during oxidation.
Water content in the oil is measured as ppm.
3.5 Dielectric measurement
The measurement of dielectric dissipation factor and permittivity test has to
according for standard IEC 60247. This test was conducted using cells in which the cell
has two parts, low voltage and high voltage. The samples used must meet the cell to
prevent the air accumulates in the cell during the test done. This test measured the empty
condition and there is the capacitance is determined to do the measurement. This sample
make measurement using Schering bridge with gas a standards capacitor. This cells must
are clean before performing any tests. It is done to avoid contamination in the cell.
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CHAPTER 4
INITIAL WORK
4.0 Result and discussion
4.0.1 Breakdown voltage
The result for measured the breakdown voltage of sunflower oil have been
listed according to the sample to be used for this measurement. This measurement
is done by using four samples, two samples of oil that has been heated and the rest
of the sample is unheated. For each sample to be perform the measurement of the
five tests. Table 4.0 shows the results obtained from these measurements.
Table 4.0: Result for breakdown voltage measurement of the sample
Sample
Breakdown voltage (kV)
Average value(kV)Measurement 1 2 3 4 5
Sunlico
Heated 10.0 9.3 16.2 9.3 10.3 11.0
Unheated 10.0 9.5 10.2 15.2 16.1 12.2
Adela
Heated 59.8 47.8 57.2 61.8 31.1 51.5
Unheated 12.5 12.6 14.2 17.3 12.0 13.7
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Based on table 4.0 above, it shows the readings taken during a breakdown
voltage measurement on four samples of different brands. Based on the average
value of the oil that has been heated to a brand Adela is a high value of 51.5kV.
This is because the oil has been heated with low humidity so it does not affect the
breakdown voltage. If compared with mineral oil exist in the literature review is
more than 70kV compared with sunflower oil. According to the characteristics of
transformer oil, the value of the breakdown voltage is ideal for use as liquid
insulation for high efficiency and good for insulation and will be use in the
transformer.
The value of breakdown voltage are low, it is likely due to the high moisture
in the oil and not good for insulation. The measured for the brand sunlico, the
difference for heated and unheated are lower value in breakdown voltage. it is not
good to used in a transformer due to its efficiency of the insulation is low. The
insulation in transformers is important to respond with a very high resistance to the
flow of electric current in a transformer. The minimum value of the breakdown
voltage to safety used in transformer is 30kV [14].
4.0.2 Viscosity
The measurement for the viscosity of the oil is only done for the sample of
the oil that has been heated. The sample must be performed by three time of test.
The results obtained are recorded for this measurement in Table 4.1
Table 4.1: Result for viscosity measurement of the heated sample
Sample for heated
Cp (MPa s-1) at 100rpm
1 2 3
Sunlico 113.6 113.6 113.6
Adela 114.4 114.4 114.4
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Based on the result of the measurement of viscosity, the value in the two
samples no difference. The sample for the brand sunlico is 113.6 MPa s -1, while
114.4 MPa s-1is the viscosity of the sample for brand Adela. Based on the viscosity
of mineral oil is 8.9 cSt at temperature 40C. The sample used for this
measurement is the oil has been heated and has also reduced the moisture in the
oil.
The viscosity is the flow resistance in the normal state. The transformer
requires that transformer oil has a lower viscosity to reduce the resistance to the
flow of oil that does not touch the convectional cooling transformer. It is also safe
for use in transformer condition better on a long run as cooling. If high viscosity, it is
not suitable for use in a transformer because the transformer cooling process
requires high temperatures. Usually, the temperature is reduced to increase the
viscous liquid. Therefore, the viscosity should be high for the cooling process in
transformers. The sunflower oil can be used as the viscosity is high and similar for
mineral oil [15, 17].
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2013. Vol. 20: p. No. 3
[3] D.C. Abeysundara, C.W.a.J.R.L., K.A.I. Gunatunga and K.C. Obadage, Coconut
oil as an alternative to transformer oil. ERU Symposium, November 2001.
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applications magazine. may/june 2002.
[5] Milan Spohner, "Comparison of mineral oil with natural and synthetic oil".
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Ester,IEEE, 2008.
[7] HOANG, Y.B.a.L.C., Vegetable oils as substitute for mineral insulating oils inmedium voltage equipments. 2004.
[8] base oil handbook, NYNAS.
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Springer, 2007.
[10] T. V. O. a. G. L. Grune, "Low temperature viscosity behavior of transformer oils".
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