OPERATING DIVISIONS

rlflSSQURI

Bonne Terre

Bowling Green

Buchanan County 1

Cameron

Cape Girardeau

East Central Missouri Water ampSewer

Authority

Elsberry

Franklin County 1

Franklin County 3

Henry County Water Company

Henry County 3

Lake Ozark Osage Beach

Lincoln County 1

Nevada

Parkville

Phelps County 2

Platte County C-1

Ralls County 1

Russelville

St Charles County 2

St Genevieve

Sedalia

Versailles

IOVVA

Maquoketa

Tipton

Professional Water and Wastewater Operations

OPERATIONS REPORT - NEVADA DIVISION

July 2012 Report to the City of Nevada

Water Treatment Plant Operations amp Maintenance bull The 1 high service pump was sent to JCI for rebuild per Capital

Improvement Plan bull A new block heater was installed on the West generator bull Damaged drain piping was replaced in the chlorine room bull Water stability goals have been achieved by making adjustments to blend

flow rates and pH bull Staff installed a new site glass on the anti-sealant tank bull Staff installed a new safety showereyewash station near chemical rooms bull A utility sink was installed in the RO room on the lower level near

chemical rooms bull Staff replaced level indicator on the North water tower bull Sample taps were replaced in the RO room

Waste Water Treatment Plant Operations amp Maintenance bull Staff continued land applying biosolids this month bull Lift station wet wells were cleaned this month bull Oil and air filters were changed on all four aeration blowers bull Staff repaired drain valves on East and West oxidation ditches bull Staff installed submersible pump in lift station 1 Repairs were made by

JCI

Waste Water Collection I Water Distribution bull Staff performed 93 water shut off and 48 water turn on in one day bull Several yard repairs were done from previous service work bull Meadow Lane sewer extension inspection was overseen and documented

by staff Also a CCTV inspection was done on this new installation bull Staff installed a new brake box in fleet vehicle reinforced loading ramps

and repaired trailer brakes on equipment trailer bull One fleet vehicle received a tune-up ignition repair and air conditioning

repair and recharge bull Staff repaired several water service leaks during the month We speculate

the dry weather is causing more service leaks to appear

Recommendations bull Change language of City code Sec 40-4 and 40-11 to minimize possible

liability Responsibility should be from the water main to the first point of shut off whether it is a corporate shut off (curb stop) or inside the meter box

bull Replace jetter truck due to major repairs that are needed and undersized brake system for the existing chassis

1UliiiiCC Professional Water and Wastewater Operations

OPERATIONS REPORT - NEVADA DIVISION

WATER TREATMENT PLANT PERFORMANCE

4Log SamplIDgr

I

i

Parameter Monthly A vera2e pH 889 Temperature 211 Lowest Ch residual 21

B t I IR ltac erlO oglca esu s Date Results (Absent or Present) 7912 A 723112 A

Flow Totals (Million Gallons per Day) Meter Avera2e Daily Flow Total Monthly Flow Feed 102 MGD 3147 MG Product 084MGD 2617 MG Blend 026 MGD 808 MG Brine 020MGD 634 MG Distribution 109MGD 3376 MG

bull WATER RESOURCESshyce Professional Water and Wastewater Operattons

OPERATIONS REPORT - NEVADA DIVISION

W ASTE WATER TREATMENT PLANT PERFORMANCE

NPDES Effluent Limits Parameter Monthly Average Permit Limit pH 69 max and 67 min 60 - 90 TSS 7mgL 30 mgL BODs 4mgL 30 mgL NH3-N 008 mgL 140 mgL

Flow Totals (Million Gallons per Day) Average Daiy Flow Total Monthly Flow 096 MGD 2962 MG

Biosolids Report Period Year to Date

Quantity Applied 8 dry tons 486 dry tons Acres Applied 22 acres applied 72 acres applied

luuailceProfessional Walaquor and Wastewalaquor Operations

OPERArIONS REPORT - NEVADA DIVISION

June 2012 Service Work Orders

This Period Year To Date

Action Issued Completed Voided Outstanding Issued Completed Voided Outstanding

Connect 51 48 3 a 394 360 26 8

Disconnect 35 28 1 6 253 224 13 15

Cut Off a a a a a a a a

Meter Info 185 182 2 1 1117 1071 16 29

Meter Change 41 40 a 1 211 204 a 6

OCCChange 80 78 2 a 517 488 16 13

Reinstate 130 130 a a 494 493 2 8 Service Change a a a a 1 a 1 a

Miscellaneous 10 10 a a 229 196 8 25

ITOTALS 532 516 8 8 3216 3036 83 104

146 WaterSewer utility locates during the month

1uuaiiCC Professional Water and Wastewater Operations

OPERATIONS REPORT - NEVADA DIVISION

Water Loss

Total Water Delivered

January February March 23285000 April 31797000 May 31000000 June 29080000 July August September October November December

Identified Water Loss

175000 39500

2145000 47000

Billed Consumption

21119200 21686200 19733143 20157450

Unidentified Water Loss

1990800 10071300 9121857 8875550

Water Loss

85 317 294 305

I I

I

I I

IYTD Total 1115162000 1 2406500 I 82695993 I 30059507 1 250

Identified Water Loss Detail

Leaks January February March 25000 April 25000 May 100000 June 20000 July August

September October

November December

Flushing Fire Dept

8000 12000 2000 12500

1970000 75000 2000 25000

Other Total I

I

130000 175000 I

0 39500 I

0 2145000

0 47000 I

0 o i

OJ o i

01 01

1YTD Total 1 170000 1982000 124500 130000 2406500 I

lMllaDCeProfessional Water and Wastewater Operations

OPERATIONS REPORT - NEVADA DIVISION

June 2012 Water Loss Detail Explanation

Leaks This column is an estimation of leaks that were known during the reporting period During the month an estimated 20000 gallons were lost from service leaks throughout the distribution system

Flushing The Flushing column reflects an estimation of water lost from the routine flushing ofdead end mains in the system or if a customer had a dirty water complaint the area may get flushed if it appears to be from the distribution system Approximately 2000 gallons were used for flushing

Fire Dept The column represents water used by the Fire dept for fighting fires and training exercises This month approximately 25000 gallons were used for the purpose offirefighting and training

Other This is a miscellaneous column to catch out of the ordinary water uses Nothing to report in this column for the month

20000 Leaks 2000 Flushing 25000 Fire Dept

+0 Other =47000 Total

Water Loss Calculation

Water Loss The water loss is calculated by subtracting the Identified Water Loss (47000) and the Billed Consumption (20157450) from the Total Water Delivered (29080000) to come up with the Unidentified Water Loss (8875550) To calculate the Water Loss divide Unidentified Water Loss into Total Water Delivered

29080000 - (47000 + 20157450) = 8875550

887555029080000 = 0305 or 305

G MISSOURI OEPARTMENT OF NATURAL RESOURCES - WATER PROTECTION PROGRAM

~ ~ MONTHLY COMPLIANCE MONITORING REPORT FOR GROUNDWATER SYSTEMS

PJ8l1C WATpoundR SYSYEM IWoIf IPUIIlIC WAllR 1)1gt1110110 NVMIA jCOUHPICity of Nevada Me 5010562 Vernon

Mtnlmum Residual __ z Minim Residual _ Minimum Re5idual

4-Ioa SatnoIe locabon 4-109 Sm~LocatIOn 4-1Og Sample Location MonthI pH Tamp LowestF pH Temp LOWHtFre pH Temp lowMtF V degc Chlonne (mgll) degc Chlorine (mgl1)

I~middotmiddotmiddot--middotmiddot degc ChlorlM (mgll)

2~---664 211 23 fmiddot-- shy ---shy -shy-- shy877 21 Lo 23

--~-- ----- shy3 888 208 23 4 892 20A 23 5 890 212 23

6 88]_ I- 211 __ 22

1- 7 22 8_~ 215 ----- -----~-

--___ ------ shy----- shy f----_ k___ ~middot__ shy - ~

8 896 208 18-9 893 211 21

10 888 213 19

[11_ 885 _21Q_ 22 --rmiddot----middot shy ----~-~-~

h~- 894 206 19 13 911 215 21

14 883 210 20 I 15 884 211 23 I

16 880 212 21

~ 887 212 22 18 877 208 21

t-19 897 ~1 19~-----------shy120 902 206 ~ 1 7

r -- shy -- ---shy -~-----i---- _- shy - t--middot i 21 ~JL12 208 19_h----shy _-- shy ~--------

22 892 215 20 i 23 888 211 21 i 24 878 210 22 -125 892 211 22 i 26 806 O8 21 j2j ~--~ shy

906 208 21 t

I~8 864 214 19

I E4129 893 211 25 f3tf 914 212 19 -i 31 898 213 21 II Was the diSinfectant t9sidual ever less than the Slate reqUIred level for 4-109 InactIvation 01 viruses at thiS enlry POintIOYn III No _ If 0 old the wa1er system collect grab samples every four hours until the d-ls--lnfe--cta---n7t-re-s~id-u--alw-a-s--a--bo-ve~lhe--S~--ale required level

I 0 Va ~ No Ifm enswet yes to this question attach the resuU~~- theELsarl)II~19thslrn~L ___ i (For IyqmS serving more than 33(0) Old continuous monitOring equipment fail at any time during this reportll1g penoo

1I DYII2I No (For systems serving I1lQ(6 than 3300) If monitoring equipment taded were grab samples collected every 4 hours until the I conllnuous monitonng equipment was returned to SftlV1Ce gJ~Jttach itab sample results to this form)

RSON 1Ii5A ~ _----__---------1 -I

I 61 PAJIili2

1-751-=~ry~+HhltIo=iPflIlll_-_----__---- --==Tomiddot~-i~-middot~ (9 t~-_-~-l Jose h Ti

Laboratory Log-In and Chlorine Report form

(Julv 2012)

Sample ID Date I Time Received Received

Initals Supply 10 Date

Taken

middot~ (

- -) I

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Time Taken

Location Chlorine

Free I Total

Collectors Initials

~( Slt-i j ( of -(

L h fl- (ISshy

~- I i J -~ 7 )l J Iv IG I J 11lt

tlf bull ( I r iI r l f~ ~-_I h ff-I~middot C~

lr t r --) - ~ 1 ~Lt Icph L1 fl 117

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Remarks

- - -

Laboratory Log-In and Chlorine Report form

Sample 10 Date Time

Initals Supply 10Received Received

1 ~( J -)2shy ICCmiddot( 7f -I(~12

)gt 1amp 7l~( h 110 ~ M~ ))1 ~)~S

l~ G- L -d tshy II ~o5 Ct~ 02J5

_----shy _ _shy

Date Taken

Time location

Taken

7f J1Z escSshy laquo7 IS j illt- ~s middot r)

1-1 ~ d10S S~o H1t+t t S r bleAt I If I ) ifl)S 110 ~Ymiddottt b~Xt

shy __shy _

Chlorine Collectors Remarks

Free Total Initials

1Z Z nrF

- 1J1 f - 51 if

Missouri Dcpartmcnt Of latural Resources Public Drinkine Water Program

PO 80x 176 kfrcrson (it~ to 65102 (573)751-5331

Public Vater System Bacteriological Report

S ~aml NEVADA PWS If) M050 I 05tl2

Mail 10 JOSEPH TIPPER

1300 W CHERRY County VERNON

NEVADA MO 64772 Plcase n(llll~ u- (I IllY name and addres lhangls

Sample TypeIgtal( (lIlhrhd ColIlCtor

ROlltine07092012 MF lab RtSuitl Io~ation Nanl( Location II)Lab SamplE m

NEVADA~ A120 SASH

Coliform IIhent Sample considtred safe

26566

Sample T~I)( Dau Colletmiddotted ColleClor

Routine070912012 MF Iah Rtmiddot ults Ioration alUr loCalioll II)Lab SampltlO

71 HWY N NEVADA4 A

Coliform absent Samplt (onsidCndsaft

265M

Sample T~pt nail Coller led Collerl()r

Routine07092012 MF

Lab Sampl( m Location janie Lmalioll Ill Iah RIiull

50 I S JEFFERSON NEVADA5 A

(ouror absent Sample considered safe

26565

~

Santl)- Typt COIltllIr

07092012 MF Routine

Lab SlImpie III 1lnalion SlUt Iocalion IIgt Iah RlSUItS

41 I S WESl NEVADA2 A26563

Note to public water systems If you take a routine sample from a well rather than your distrIbution system a violation may be Issued by Missouri Public Drinking Water Branch

i-ridul July Il 101

Q -_

lissouri Department Of Natural Resources i_~~ Public Drinking Water ProJram

PO Box 176 Jefferson Cit) I0 65102 (573)751-5331

Public Water System Bacteriological Report

NEVADA PS I) M05010562rws 1I111t

JOSEPI TIPPER lail to Counl) VERNON 1300 W CHERRY

NEVADA MO 64772 Plcmc Il(llify us Ill any name and addrcs challgl

Samllil TYPl I)lltl (ullechd Collector

Routine07 )9 W12 MF Iab Relulll Lab SlImpll III LOC8110n Iianl Location II)

26567 1300 W CHERRY NEVADAI A

(oliform absent Samplf fonsidered safe ~~ t4_-mc-W ~

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

middotridIJYbullbullIul 13 101

IWS alllt

laillo

i~sotJri Dep_urment Of turall~((lurn Iuhlir flrinldlll WU(r lrIIJraOl

VO Rn 171 Jcff(middotrion (it 10 hS 1112

NIVAI)

JOSEPU TIPPER

I 30n W CH ERR Y NI ADA MO (-4112

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07 B2012

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111 IhlIl~ U 111111

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R()UlllC

LmlIliulI II)

I m11 intI I D

llllpk I ~ lit

Imiddotcutlll~middot

I all 1UII

Note to public water systems If you lake a routine sample from a well rather than your distribution system a violation may be issued by Missouri Public Drinking Waler Branch

IriJIII)-

shyI~-~f r -----1

I

4 (D Iissouri Illpartmcnl Of atunlJ icsOUrltCli L ~_ __ _ uhlie UrinkinJ Wllu Irolram

PO Bo 17h hfhrwll Ci~ 1O h~ 1tI

Jmiddotuhlic ate S~slcm Bll(tlrioloJical I~cporl

NFADA II) ~H raquo)(J IOh

ailltl JOSEI)II lWPLR

I ~oo CHERRY (Hunl VERNON

NlADA MO hmiddotP Pill IlOlin li 11 HI

II lIll ltllld 1hlr t L hIII~

l1Ipk T~ p I)alt (nlll(tli ( nlhctur

Rwin0 3 201 MF

Ioealillll II) I all 1(11 Ill SlImpl III

411 ~ WIS I

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

I riduy III1 - III

MI~~OUftl DePARTMENT OF NATURAL RESOURCES DIVISION OF ENVIRONMENTAL QUALITY

Discharge Monitoring Report For Municipal Wastewater Treatment Plants

N- OF FACILITY lOCA11UN iampCrTY ~ _shyNvada 1IItit WIItIIf rnt 117 s 1338 ROid NevIIda VERNONISOUTHWEST

IIR-r OUTFALL NUllBER TYPI ACLTY

IIIIyl2012 M0-00891 09 001 OXIDATION OtTCH INFLUENT FFFI JFIIIT

rNCiI -rAlp E OtL DATE FLOW BOD TSS u~s BOD TSS TEMP DO

IIIGO mall mall mall mall mall mall CFUllOOMl C mQt1 mQt1 mgI

1 067 00

2 O~9 00 226

I 3 089 00 122 118 67 3 7 005 228

4 091 00 227

5 096 00 44 375 lt10 200 58 2440 NO

6 100 00 228

7 099 00

8 098 00

9 166 00 231

10 139 00 229

11 095 00 44 275 61 4 5 007 227

12 099 00 lt10 229

13 104 T 226

14 102 00

15 100 00 16

099 00 225

17 100 00 229

i 18 103 00 118 113 69 3 4 008 229

19 102 T 733 230

20 101 00 229

I 21 095 00

122 096 00

23 099 00 232

24 098 00 234 i

25 099 00 131 199 69 6 11 01 233

26 035 T lt10 236

27 042 00 235

28 087 00

29 093 T

30 061 T 26

31 100 T 247

[Total 2982

iAVQ 096 t04 176 4 7 0CJ8 44 375 187 230 58 244 N()

Min 035 67 Max 166 00 89

lA8ORATORY TEST REQUIRED FOR wACTIVATED SlUDGEwPROCESSES

Aeration Baaln ()Ditch Etc

~ Sludge0 MIXED UQUOR Outside I A 00 -MLSS Settlbullbullbllity

Temp - Ambient 3 Disposal30 min E 30mtnW Temperature

CDT East East r E mgII mgII ml ml c OF bull Galions LbsDry Wt 1 88 C 915

2 31 1625 200 200 227 77 C 800

3 18 1322 200 200 229 76 PC 800

4 22 200 200 227 78 C 815

5 30 1678 200 200 222 77 C 800

6 31 1381 200 200 229 75 C 800

7 77 C 715

8 79 C 800

9 10 1850 200 200 229 77 PC 800

10 40 2215 200 229 76 PC 800

11 14 2132 220 226 75 C 800

12 40 2116 220 223 77 C 800

13 27 1935 220 225 73 PC 800

14 80 C 900

15 80 PC 900

16 27 2287 210 226 77 PC 800

11 26 1880 200 226 75 C 800

18 23 1679 180 226 78 C 800

19 26 1515 200 227 72 PC 800

20 27 1163 160 228 71 C 800

21 91 C 1230

22 89 C 845

23 23 1461 150 231 80 C 800

24 25 1412 200 231 78 800 21000 332f

25 29 1413 180 232 77 C 800 24000 4003

26 28 1395 150 234 91 PC 930

27 23 1451 150 240 75 C 800

28 63 C 730

29 79 C 800

30 10 1550 150 231 78 PC 800 15000 2127

31 18 1451 180 100 234 78 PC 800 27000 6305 COMMENTS ~ nICI ncrbull - IVII ICIU 1e5Ui lur I UUlI -IV U~ I VICII _ ILUI1 v ClIIU UI 6shy

GGA results were 1585 mglL on 7312 GGA results were 1339 mglL on 71112

GGA results were 852 on 718112 GGA results were 1433 mglL on 72512

7ull~4i( TlnE DATE

8312PLANT SUPERVISOR Ai 1ampllo~ TITlE DATE tishy LOCAL MANAGER

In tbe weather column use tbe follOWing symbols R-nun S-snow C-clear PC-partly doudy ()overcast

-Required Daily Required llweek

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

1UliiiiCC Professional Water and Wastewater Operations

OPERATIONS REPORT - NEVADA DIVISION

WATER TREATMENT PLANT PERFORMANCE

4Log SamplIDgr

I

i

Parameter Monthly A vera2e pH 889 Temperature 211 Lowest Ch residual 21

B t I IR ltac erlO oglca esu s Date Results (Absent or Present) 7912 A 723112 A

Flow Totals (Million Gallons per Day) Meter Avera2e Daily Flow Total Monthly Flow Feed 102 MGD 3147 MG Product 084MGD 2617 MG Blend 026 MGD 808 MG Brine 020MGD 634 MG Distribution 109MGD 3376 MG

bull WATER RESOURCESshyce Professional Water and Wastewater Operattons

OPERATIONS REPORT - NEVADA DIVISION

W ASTE WATER TREATMENT PLANT PERFORMANCE

NPDES Effluent Limits Parameter Monthly Average Permit Limit pH 69 max and 67 min 60 - 90 TSS 7mgL 30 mgL BODs 4mgL 30 mgL NH3-N 008 mgL 140 mgL

Flow Totals (Million Gallons per Day) Average Daiy Flow Total Monthly Flow 096 MGD 2962 MG

Biosolids Report Period Year to Date

Quantity Applied 8 dry tons 486 dry tons Acres Applied 22 acres applied 72 acres applied

luuailceProfessional Walaquor and Wastewalaquor Operations

OPERArIONS REPORT - NEVADA DIVISION

June 2012 Service Work Orders

This Period Year To Date

Action Issued Completed Voided Outstanding Issued Completed Voided Outstanding

Connect 51 48 3 a 394 360 26 8

Disconnect 35 28 1 6 253 224 13 15

Cut Off a a a a a a a a

Meter Info 185 182 2 1 1117 1071 16 29

Meter Change 41 40 a 1 211 204 a 6

OCCChange 80 78 2 a 517 488 16 13

Reinstate 130 130 a a 494 493 2 8 Service Change a a a a 1 a 1 a

Miscellaneous 10 10 a a 229 196 8 25

ITOTALS 532 516 8 8 3216 3036 83 104

146 WaterSewer utility locates during the month

1uuaiiCC Professional Water and Wastewater Operations

OPERATIONS REPORT - NEVADA DIVISION

Water Loss

Total Water Delivered

January February March 23285000 April 31797000 May 31000000 June 29080000 July August September October November December

Identified Water Loss

175000 39500

2145000 47000

Billed Consumption

21119200 21686200 19733143 20157450

Unidentified Water Loss

1990800 10071300 9121857 8875550

Water Loss

85 317 294 305

I I

I

I I

IYTD Total 1115162000 1 2406500 I 82695993 I 30059507 1 250

Identified Water Loss Detail

Leaks January February March 25000 April 25000 May 100000 June 20000 July August

September October

November December

Flushing Fire Dept

8000 12000 2000 12500

1970000 75000 2000 25000

Other Total I

I

130000 175000 I

0 39500 I

0 2145000

0 47000 I

0 o i

OJ o i

01 01

1YTD Total 1 170000 1982000 124500 130000 2406500 I

lMllaDCeProfessional Water and Wastewater Operations

OPERATIONS REPORT - NEVADA DIVISION

June 2012 Water Loss Detail Explanation

Leaks This column is an estimation of leaks that were known during the reporting period During the month an estimated 20000 gallons were lost from service leaks throughout the distribution system

Flushing The Flushing column reflects an estimation of water lost from the routine flushing ofdead end mains in the system or if a customer had a dirty water complaint the area may get flushed if it appears to be from the distribution system Approximately 2000 gallons were used for flushing

Fire Dept The column represents water used by the Fire dept for fighting fires and training exercises This month approximately 25000 gallons were used for the purpose offirefighting and training

Other This is a miscellaneous column to catch out of the ordinary water uses Nothing to report in this column for the month

20000 Leaks 2000 Flushing 25000 Fire Dept

+0 Other =47000 Total

Water Loss Calculation

Water Loss The water loss is calculated by subtracting the Identified Water Loss (47000) and the Billed Consumption (20157450) from the Total Water Delivered (29080000) to come up with the Unidentified Water Loss (8875550) To calculate the Water Loss divide Unidentified Water Loss into Total Water Delivered

29080000 - (47000 + 20157450) = 8875550

887555029080000 = 0305 or 305

G MISSOURI OEPARTMENT OF NATURAL RESOURCES - WATER PROTECTION PROGRAM

~ ~ MONTHLY COMPLIANCE MONITORING REPORT FOR GROUNDWATER SYSTEMS

PJ8l1C WATpoundR SYSYEM IWoIf IPUIIlIC WAllR 1)1gt1110110 NVMIA jCOUHPICity of Nevada Me 5010562 Vernon

Mtnlmum Residual __ z Minim Residual _ Minimum Re5idual

4-Ioa SatnoIe locabon 4-109 Sm~LocatIOn 4-1Og Sample Location MonthI pH Tamp LowestF pH Temp LOWHtFre pH Temp lowMtF V degc Chlonne (mgll) degc Chlorine (mgl1)

I~middotmiddotmiddot--middotmiddot degc ChlorlM (mgll)

2~---664 211 23 fmiddot-- shy ---shy -shy-- shy877 21 Lo 23

--~-- ----- shy3 888 208 23 4 892 20A 23 5 890 212 23

6 88]_ I- 211 __ 22

1- 7 22 8_~ 215 ----- -----~-

--___ ------ shy----- shy f----_ k___ ~middot__ shy - ~

8 896 208 18-9 893 211 21

10 888 213 19

[11_ 885 _21Q_ 22 --rmiddot----middot shy ----~-~-~

h~- 894 206 19 13 911 215 21

14 883 210 20 I 15 884 211 23 I

16 880 212 21

~ 887 212 22 18 877 208 21

t-19 897 ~1 19~-----------shy120 902 206 ~ 1 7

r -- shy -- ---shy -~-----i---- _- shy - t--middot i 21 ~JL12 208 19_h----shy _-- shy ~--------

22 892 215 20 i 23 888 211 21 i 24 878 210 22 -125 892 211 22 i 26 806 O8 21 j2j ~--~ shy

906 208 21 t

I~8 864 214 19

I E4129 893 211 25 f3tf 914 212 19 -i 31 898 213 21 II Was the diSinfectant t9sidual ever less than the Slate reqUIred level for 4-109 InactIvation 01 viruses at thiS enlry POintIOYn III No _ If 0 old the wa1er system collect grab samples every four hours until the d-ls--lnfe--cta---n7t-re-s~id-u--alw-a-s--a--bo-ve~lhe--S~--ale required level

I 0 Va ~ No Ifm enswet yes to this question attach the resuU~~- theELsarl)II~19thslrn~L ___ i (For IyqmS serving more than 33(0) Old continuous monitOring equipment fail at any time during this reportll1g penoo

1I DYII2I No (For systems serving I1lQ(6 than 3300) If monitoring equipment taded were grab samples collected every 4 hours until the I conllnuous monitonng equipment was returned to SftlV1Ce gJ~Jttach itab sample results to this form)

RSON 1Ii5A ~ _----__---------1 -I

I 61 PAJIili2

1-751-=~ry~+HhltIo=iPflIlll_-_----__---- --==Tomiddot~-i~-middot~ (9 t~-_-~-l Jose h Ti

Laboratory Log-In and Chlorine Report form

(Julv 2012)

Sample ID Date I Time Received Received

Initals Supply 10 Date

Taken

middot~ (

- -) I

30 l Y 11 I I I

f it Il

15 I j

SJ (( 1 (

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71711 Irl12

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Y)~2 b12 1) ~J L

rIshy il~ ~ 1dlj

I~ It III IllL lt I 711

- ( I 1 (i I

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r Clc) )fl 7170 fc IC- J51 (7) 11shy

Ie 16Yi1jfitz 5lpoundJ~2 (]2 SlICSeuro I I-~ 3hL~

7 5(ltlt I I 1j~

11 iLI u-sL ~ I )V 2

Time Taken

Location Chlorine

Free I Total

Collectors Initials

~( Slt-i j ( of -(

L h fl- (ISshy

~- I i J -~ 7 )l J Iv IG I J 11lt

tlf bull ( I r iI r l f~ ~-_I h ff-I~middot C~

lr t r --) - ~ 1 ~Lt Icph L1 fl 117

I

i kT 1- if ipoundI t Ni IV(J_ h 1

~ I I I 1shy

c)~ I I ~ 1-) i L ii I I ) l lrr NCA r-r L l L

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tl~

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t ( ~r ~ J J LI I (~ J~ c

[ i ltj- 7

bull ~l j t- L I Jshy if I f IJ 1

Yc- L ~ _ ~-- r i )- C i ) J t ff r~ ( 7

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J )4 qoq tv 11h ---shycSl pound+ 1 ramp X Yk exuIrl ( ( ltl-

I

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- - -

Laboratory Log-In and Chlorine Report form

Sample 10 Date Time

Initals Supply 10Received Received

1 ~( J -)2shy ICCmiddot( 7f -I(~12

)gt 1amp 7l~( h 110 ~ M~ ))1 ~)~S

l~ G- L -d tshy II ~o5 Ct~ 02J5

_----shy _ _shy

Date Taken

Time location

Taken

7f J1Z escSshy laquo7 IS j illt- ~s middot r)

1-1 ~ d10S S~o H1t+t t S r bleAt I If I ) ifl)S 110 ~Ymiddottt b~Xt

shy __shy _

Chlorine Collectors Remarks

Free Total Initials

1Z Z nrF

- 1J1 f - 51 if

Missouri Dcpartmcnt Of latural Resources Public Drinkine Water Program

PO 80x 176 kfrcrson (it~ to 65102 (573)751-5331

Public Vater System Bacteriological Report

S ~aml NEVADA PWS If) M050 I 05tl2

Mail 10 JOSEPH TIPPER

1300 W CHERRY County VERNON

NEVADA MO 64772 Plcase n(llll~ u- (I IllY name and addres lhangls

Sample TypeIgtal( (lIlhrhd ColIlCtor

ROlltine07092012 MF lab RtSuitl Io~ation Nanl( Location II)Lab SamplE m

NEVADA~ A120 SASH

Coliform IIhent Sample considtred safe

26566

Sample T~I)( Dau Colletmiddotted ColleClor

Routine070912012 MF Iah Rtmiddot ults Ioration alUr loCalioll II)Lab SampltlO

71 HWY N NEVADA4 A

Coliform absent Samplt (onsidCndsaft

265M

Sample T~pt nail Coller led Collerl()r

Routine07092012 MF

Lab Sampl( m Location janie Lmalioll Ill Iah RIiull

50 I S JEFFERSON NEVADA5 A

(ouror absent Sample considered safe

26565

~

Santl)- Typt COIltllIr

07092012 MF Routine

Lab SlImpie III 1lnalion SlUt Iocalion IIgt Iah RlSUItS

41 I S WESl NEVADA2 A26563

Note to public water systems If you take a routine sample from a well rather than your distrIbution system a violation may be Issued by Missouri Public Drinking Water Branch

i-ridul July Il 101

Q -_

lissouri Department Of Natural Resources i_~~ Public Drinking Water ProJram

PO Box 176 Jefferson Cit) I0 65102 (573)751-5331

Public Water System Bacteriological Report

NEVADA PS I) M05010562rws 1I111t

JOSEPI TIPPER lail to Counl) VERNON 1300 W CHERRY

NEVADA MO 64772 Plcmc Il(llify us Ill any name and addrcs challgl

Samllil TYPl I)lltl (ullechd Collector

Routine07 )9 W12 MF Iab Relulll Lab SlImpll III LOC8110n Iianl Location II)

26567 1300 W CHERRY NEVADAI A

(oliform absent Samplf fonsidered safe ~~ t4_-mc-W ~

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

middotridIJYbullbullIul 13 101

IWS alllt

laillo

i~sotJri Dep_urment Of turall~((lurn Iuhlir flrinldlll WU(r lrIIJraOl

VO Rn 171 Jcff(middotrion (it 10 hS 1112

NIVAI)

JOSEPU TIPPER

I 30n W CH ERR Y NI ADA MO (-4112

Ihue (ollltld

lPOI)

LlIh Slimple 11)

2Q342

1)11 ( IIlied ttl

07 B2012

Lllh ~IUIIJlh In

nle (nllfhd

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II

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~II

11 11 Y l

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( IIIIII~ VERNON

111 IhlIl~ U 111111

I)IIIW HId dfmiddot dlIII11l

1(1(31 ion II) Inh ~(lh

R()UlllC

LmlIliulI II)

I m11 intI I D

llllpk I ~ lit

Imiddotcutlll~middot

I all 1UII

Note to public water systems If you lake a routine sample from a well rather than your distribution system a violation may be issued by Missouri Public Drinking Waler Branch

IriJIII)-

shyI~-~f r -----1

I

4 (D Iissouri Illpartmcnl Of atunlJ icsOUrltCli L ~_ __ _ uhlie UrinkinJ Wllu Irolram

PO Bo 17h hfhrwll Ci~ 1O h~ 1tI

Jmiddotuhlic ate S~slcm Bll(tlrioloJical I~cporl

NFADA II) ~H raquo)(J IOh

ailltl JOSEI)II lWPLR

I ~oo CHERRY (Hunl VERNON

NlADA MO hmiddotP Pill IlOlin li 11 HI

II lIll ltllld 1hlr t L hIII~

l1Ipk T~ p I)alt (nlll(tli ( nlhctur

Rwin0 3 201 MF

Ioealillll II) I all 1(11 Ill SlImpl III

411 ~ WIS I

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

I riduy III1 - III

MI~~OUftl DePARTMENT OF NATURAL RESOURCES DIVISION OF ENVIRONMENTAL QUALITY

Discharge Monitoring Report For Municipal Wastewater Treatment Plants

N- OF FACILITY lOCA11UN iampCrTY ~ _shyNvada 1IItit WIItIIf rnt 117 s 1338 ROid NevIIda VERNONISOUTHWEST

IIR-r OUTFALL NUllBER TYPI ACLTY

IIIIyl2012 M0-00891 09 001 OXIDATION OtTCH INFLUENT FFFI JFIIIT

rNCiI -rAlp E OtL DATE FLOW BOD TSS u~s BOD TSS TEMP DO

IIIGO mall mall mall mall mall mall CFUllOOMl C mQt1 mQt1 mgI

1 067 00

2 O~9 00 226

I 3 089 00 122 118 67 3 7 005 228

4 091 00 227

5 096 00 44 375 lt10 200 58 2440 NO

6 100 00 228

7 099 00

8 098 00

9 166 00 231

10 139 00 229

11 095 00 44 275 61 4 5 007 227

12 099 00 lt10 229

13 104 T 226

14 102 00

15 100 00 16

099 00 225

17 100 00 229

i 18 103 00 118 113 69 3 4 008 229

19 102 T 733 230

20 101 00 229

I 21 095 00

122 096 00

23 099 00 232

24 098 00 234 i

25 099 00 131 199 69 6 11 01 233

26 035 T lt10 236

27 042 00 235

28 087 00

29 093 T

30 061 T 26

31 100 T 247

[Total 2982

iAVQ 096 t04 176 4 7 0CJ8 44 375 187 230 58 244 N()

Min 035 67 Max 166 00 89

lA8ORATORY TEST REQUIRED FOR wACTIVATED SlUDGEwPROCESSES

Aeration Baaln ()Ditch Etc

~ Sludge0 MIXED UQUOR Outside I A 00 -MLSS Settlbullbullbllity

Temp - Ambient 3 Disposal30 min E 30mtnW Temperature

CDT East East r E mgII mgII ml ml c OF bull Galions LbsDry Wt 1 88 C 915

2 31 1625 200 200 227 77 C 800

3 18 1322 200 200 229 76 PC 800

4 22 200 200 227 78 C 815

5 30 1678 200 200 222 77 C 800

6 31 1381 200 200 229 75 C 800

7 77 C 715

8 79 C 800

9 10 1850 200 200 229 77 PC 800

10 40 2215 200 229 76 PC 800

11 14 2132 220 226 75 C 800

12 40 2116 220 223 77 C 800

13 27 1935 220 225 73 PC 800

14 80 C 900

15 80 PC 900

16 27 2287 210 226 77 PC 800

11 26 1880 200 226 75 C 800

18 23 1679 180 226 78 C 800

19 26 1515 200 227 72 PC 800

20 27 1163 160 228 71 C 800

21 91 C 1230

22 89 C 845

23 23 1461 150 231 80 C 800

24 25 1412 200 231 78 800 21000 332f

25 29 1413 180 232 77 C 800 24000 4003

26 28 1395 150 234 91 PC 930

27 23 1451 150 240 75 C 800

28 63 C 730

29 79 C 800

30 10 1550 150 231 78 PC 800 15000 2127

31 18 1451 180 100 234 78 PC 800 27000 6305 COMMENTS ~ nICI ncrbull - IVII ICIU 1e5Ui lur I UUlI -IV U~ I VICII _ ILUI1 v ClIIU UI 6shy

GGA results were 1585 mglL on 7312 GGA results were 1339 mglL on 71112

GGA results were 852 on 718112 GGA results were 1433 mglL on 72512

7ull~4i( TlnE DATE

8312PLANT SUPERVISOR Ai 1ampllo~ TITlE DATE tishy LOCAL MANAGER

In tbe weather column use tbe follOWing symbols R-nun S-snow C-clear PC-partly doudy ()overcast

-Required Daily Required llweek

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

bull WATER RESOURCESshyce Professional Water and Wastewater Operattons

OPERATIONS REPORT - NEVADA DIVISION

W ASTE WATER TREATMENT PLANT PERFORMANCE

NPDES Effluent Limits Parameter Monthly Average Permit Limit pH 69 max and 67 min 60 - 90 TSS 7mgL 30 mgL BODs 4mgL 30 mgL NH3-N 008 mgL 140 mgL

Flow Totals (Million Gallons per Day) Average Daiy Flow Total Monthly Flow 096 MGD 2962 MG

Biosolids Report Period Year to Date

Quantity Applied 8 dry tons 486 dry tons Acres Applied 22 acres applied 72 acres applied

luuailceProfessional Walaquor and Wastewalaquor Operations

OPERArIONS REPORT - NEVADA DIVISION

June 2012 Service Work Orders

This Period Year To Date

Action Issued Completed Voided Outstanding Issued Completed Voided Outstanding

Connect 51 48 3 a 394 360 26 8

Disconnect 35 28 1 6 253 224 13 15

Cut Off a a a a a a a a

Meter Info 185 182 2 1 1117 1071 16 29

Meter Change 41 40 a 1 211 204 a 6

OCCChange 80 78 2 a 517 488 16 13

Reinstate 130 130 a a 494 493 2 8 Service Change a a a a 1 a 1 a

Miscellaneous 10 10 a a 229 196 8 25

ITOTALS 532 516 8 8 3216 3036 83 104

146 WaterSewer utility locates during the month

1uuaiiCC Professional Water and Wastewater Operations

OPERATIONS REPORT - NEVADA DIVISION

Water Loss

Total Water Delivered

January February March 23285000 April 31797000 May 31000000 June 29080000 July August September October November December

Identified Water Loss

175000 39500

2145000 47000

Billed Consumption

21119200 21686200 19733143 20157450

Unidentified Water Loss

1990800 10071300 9121857 8875550

Water Loss

85 317 294 305

I I

I

I I

IYTD Total 1115162000 1 2406500 I 82695993 I 30059507 1 250

Identified Water Loss Detail

Leaks January February March 25000 April 25000 May 100000 June 20000 July August

September October

November December

Flushing Fire Dept

8000 12000 2000 12500

1970000 75000 2000 25000

Other Total I

I

130000 175000 I

0 39500 I

0 2145000

0 47000 I

0 o i

OJ o i

01 01

1YTD Total 1 170000 1982000 124500 130000 2406500 I

lMllaDCeProfessional Water and Wastewater Operations

OPERATIONS REPORT - NEVADA DIVISION

June 2012 Water Loss Detail Explanation

Leaks This column is an estimation of leaks that were known during the reporting period During the month an estimated 20000 gallons were lost from service leaks throughout the distribution system

Flushing The Flushing column reflects an estimation of water lost from the routine flushing ofdead end mains in the system or if a customer had a dirty water complaint the area may get flushed if it appears to be from the distribution system Approximately 2000 gallons were used for flushing

Fire Dept The column represents water used by the Fire dept for fighting fires and training exercises This month approximately 25000 gallons were used for the purpose offirefighting and training

Other This is a miscellaneous column to catch out of the ordinary water uses Nothing to report in this column for the month

20000 Leaks 2000 Flushing 25000 Fire Dept

+0 Other =47000 Total

Water Loss Calculation

Water Loss The water loss is calculated by subtracting the Identified Water Loss (47000) and the Billed Consumption (20157450) from the Total Water Delivered (29080000) to come up with the Unidentified Water Loss (8875550) To calculate the Water Loss divide Unidentified Water Loss into Total Water Delivered

29080000 - (47000 + 20157450) = 8875550

887555029080000 = 0305 or 305

G MISSOURI OEPARTMENT OF NATURAL RESOURCES - WATER PROTECTION PROGRAM

~ ~ MONTHLY COMPLIANCE MONITORING REPORT FOR GROUNDWATER SYSTEMS

PJ8l1C WATpoundR SYSYEM IWoIf IPUIIlIC WAllR 1)1gt1110110 NVMIA jCOUHPICity of Nevada Me 5010562 Vernon

Mtnlmum Residual __ z Minim Residual _ Minimum Re5idual

4-Ioa SatnoIe locabon 4-109 Sm~LocatIOn 4-1Og Sample Location MonthI pH Tamp LowestF pH Temp LOWHtFre pH Temp lowMtF V degc Chlonne (mgll) degc Chlorine (mgl1)

I~middotmiddotmiddot--middotmiddot degc ChlorlM (mgll)

2~---664 211 23 fmiddot-- shy ---shy -shy-- shy877 21 Lo 23

--~-- ----- shy3 888 208 23 4 892 20A 23 5 890 212 23

6 88]_ I- 211 __ 22

1- 7 22 8_~ 215 ----- -----~-

--___ ------ shy----- shy f----_ k___ ~middot__ shy - ~

8 896 208 18-9 893 211 21

10 888 213 19

[11_ 885 _21Q_ 22 --rmiddot----middot shy ----~-~-~

h~- 894 206 19 13 911 215 21

14 883 210 20 I 15 884 211 23 I

16 880 212 21

~ 887 212 22 18 877 208 21

t-19 897 ~1 19~-----------shy120 902 206 ~ 1 7

r -- shy -- ---shy -~-----i---- _- shy - t--middot i 21 ~JL12 208 19_h----shy _-- shy ~--------

22 892 215 20 i 23 888 211 21 i 24 878 210 22 -125 892 211 22 i 26 806 O8 21 j2j ~--~ shy

906 208 21 t

I~8 864 214 19

I E4129 893 211 25 f3tf 914 212 19 -i 31 898 213 21 II Was the diSinfectant t9sidual ever less than the Slate reqUIred level for 4-109 InactIvation 01 viruses at thiS enlry POintIOYn III No _ If 0 old the wa1er system collect grab samples every four hours until the d-ls--lnfe--cta---n7t-re-s~id-u--alw-a-s--a--bo-ve~lhe--S~--ale required level

I 0 Va ~ No Ifm enswet yes to this question attach the resuU~~- theELsarl)II~19thslrn~L ___ i (For IyqmS serving more than 33(0) Old continuous monitOring equipment fail at any time during this reportll1g penoo

1I DYII2I No (For systems serving I1lQ(6 than 3300) If monitoring equipment taded were grab samples collected every 4 hours until the I conllnuous monitonng equipment was returned to SftlV1Ce gJ~Jttach itab sample results to this form)

RSON 1Ii5A ~ _----__---------1 -I

I 61 PAJIili2

1-751-=~ry~+HhltIo=iPflIlll_-_----__---- --==Tomiddot~-i~-middot~ (9 t~-_-~-l Jose h Ti

Laboratory Log-In and Chlorine Report form

(Julv 2012)

Sample ID Date I Time Received Received

Initals Supply 10 Date

Taken

middot~ (

- -) I

30 l Y 11 I I I

f it Il

15 I j

SJ (( 1 (

7 J 2

1 I r

~~~ I~

Jc (

II V

I j J

3lt I

b ampf Lf S 7btC

j)3

3rltl-7

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17-IP

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l I

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) I

111shy

II ~lt II _

r7

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fI I ~

I i 112

J i 1 (2

71i71fl I

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Jpound I dH1lshy

Y)~2 b12 1) ~J L

rIshy il~ ~ 1dlj

I~ It III IllL lt I 711

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12 ( I r I Ci r t)

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r Clc) )fl 7170 fc IC- J51 (7) 11shy

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7 5(ltlt I I 1j~

11 iLI u-sL ~ I )V 2

Time Taken

Location Chlorine

Free I Total

Collectors Initials

~( Slt-i j ( of -(

L h fl- (ISshy

~- I i J -~ 7 )l J Iv IG I J 11lt

tlf bull ( I r iI r l f~ ~-_I h ff-I~middot C~

lr t r --) - ~ 1 ~Lt Icph L1 fl 117

I

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tl~

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L ( IAII

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t ( ~r ~ J J LI I (~ J~ c

[ i ltj- 7

bull ~l j t- L I Jshy if I f IJ 1

Yc- L ~ _ ~-- r i )- C i ) J t ff r~ ( 7

13 l 4~g pound Wlj)Oh Ishy shy

J )4 qoq tv 11h ---shycSl pound+ 1 ramp X Yk exuIrl ( ( ltl-

I

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- - -

Laboratory Log-In and Chlorine Report form

Sample 10 Date Time

Initals Supply 10Received Received

1 ~( J -)2shy ICCmiddot( 7f -I(~12

)gt 1amp 7l~( h 110 ~ M~ ))1 ~)~S

l~ G- L -d tshy II ~o5 Ct~ 02J5

_----shy _ _shy

Date Taken

Time location

Taken

7f J1Z escSshy laquo7 IS j illt- ~s middot r)

1-1 ~ d10S S~o H1t+t t S r bleAt I If I ) ifl)S 110 ~Ymiddottt b~Xt

shy __shy _

Chlorine Collectors Remarks

Free Total Initials

1Z Z nrF

- 1J1 f - 51 if

Missouri Dcpartmcnt Of latural Resources Public Drinkine Water Program

PO 80x 176 kfrcrson (it~ to 65102 (573)751-5331

Public Vater System Bacteriological Report

S ~aml NEVADA PWS If) M050 I 05tl2

Mail 10 JOSEPH TIPPER

1300 W CHERRY County VERNON

NEVADA MO 64772 Plcase n(llll~ u- (I IllY name and addres lhangls

Sample TypeIgtal( (lIlhrhd ColIlCtor

ROlltine07092012 MF lab RtSuitl Io~ation Nanl( Location II)Lab SamplE m

NEVADA~ A120 SASH

Coliform IIhent Sample considtred safe

26566

Sample T~I)( Dau Colletmiddotted ColleClor

Routine070912012 MF Iah Rtmiddot ults Ioration alUr loCalioll II)Lab SampltlO

71 HWY N NEVADA4 A

Coliform absent Samplt (onsidCndsaft

265M

Sample T~pt nail Coller led Collerl()r

Routine07092012 MF

Lab Sampl( m Location janie Lmalioll Ill Iah RIiull

50 I S JEFFERSON NEVADA5 A

(ouror absent Sample considered safe

26565

~

Santl)- Typt COIltllIr

07092012 MF Routine

Lab SlImpie III 1lnalion SlUt Iocalion IIgt Iah RlSUItS

41 I S WESl NEVADA2 A26563

Note to public water systems If you take a routine sample from a well rather than your distrIbution system a violation may be Issued by Missouri Public Drinking Water Branch

i-ridul July Il 101

Q -_

lissouri Department Of Natural Resources i_~~ Public Drinking Water ProJram

PO Box 176 Jefferson Cit) I0 65102 (573)751-5331

Public Water System Bacteriological Report

NEVADA PS I) M05010562rws 1I111t

JOSEPI TIPPER lail to Counl) VERNON 1300 W CHERRY

NEVADA MO 64772 Plcmc Il(llify us Ill any name and addrcs challgl

Samllil TYPl I)lltl (ullechd Collector

Routine07 )9 W12 MF Iab Relulll Lab SlImpll III LOC8110n Iianl Location II)

26567 1300 W CHERRY NEVADAI A

(oliform absent Samplf fonsidered safe ~~ t4_-mc-W ~

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

middotridIJYbullbullIul 13 101

IWS alllt

laillo

i~sotJri Dep_urment Of turall~((lurn Iuhlir flrinldlll WU(r lrIIJraOl

VO Rn 171 Jcff(middotrion (it 10 hS 1112

NIVAI)

JOSEPU TIPPER

I 30n W CH ERR Y NI ADA MO (-4112

Ihue (ollltld

lPOI)

LlIh Slimple 11)

2Q342

1)11 ( IIlied ttl

07 B2012

Lllh ~IUIIJlh In

nle (nllfhd

(J72J012

I Il 11 In

I h SlIupll I()

II

UOO W ClIIRRY

11

LW S ASII

( lIl(middottor

~II

11 11 Y l

Ml

( IIIIII~ VERNON

111 IhlIl~ U 111111

I)IIIW HId dfmiddot dlIII11l

1(1(31 ion II) Inh ~(lh

R()UlllC

LmlIliulI II)

I m11 intI I D

llllpk I ~ lit

Imiddotcutlll~middot

I all 1UII

Note to public water systems If you lake a routine sample from a well rather than your distribution system a violation may be issued by Missouri Public Drinking Waler Branch

IriJIII)-

shyI~-~f r -----1

I

4 (D Iissouri Illpartmcnl Of atunlJ icsOUrltCli L ~_ __ _ uhlie UrinkinJ Wllu Irolram

PO Bo 17h hfhrwll Ci~ 1O h~ 1tI

Jmiddotuhlic ate S~slcm Bll(tlrioloJical I~cporl

NFADA II) ~H raquo)(J IOh

ailltl JOSEI)II lWPLR

I ~oo CHERRY (Hunl VERNON

NlADA MO hmiddotP Pill IlOlin li 11 HI

II lIll ltllld 1hlr t L hIII~

l1Ipk T~ p I)alt (nlll(tli ( nlhctur

Rwin0 3 201 MF

Ioealillll II) I all 1(11 Ill SlImpl III

411 ~ WIS I

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

I riduy III1 - III

MI~~OUftl DePARTMENT OF NATURAL RESOURCES DIVISION OF ENVIRONMENTAL QUALITY

Discharge Monitoring Report For Municipal Wastewater Treatment Plants

N- OF FACILITY lOCA11UN iampCrTY ~ _shyNvada 1IItit WIItIIf rnt 117 s 1338 ROid NevIIda VERNONISOUTHWEST

IIR-r OUTFALL NUllBER TYPI ACLTY

IIIIyl2012 M0-00891 09 001 OXIDATION OtTCH INFLUENT FFFI JFIIIT

rNCiI -rAlp E OtL DATE FLOW BOD TSS u~s BOD TSS TEMP DO

IIIGO mall mall mall mall mall mall CFUllOOMl C mQt1 mQt1 mgI

1 067 00

2 O~9 00 226

I 3 089 00 122 118 67 3 7 005 228

4 091 00 227

5 096 00 44 375 lt10 200 58 2440 NO

6 100 00 228

7 099 00

8 098 00

9 166 00 231

10 139 00 229

11 095 00 44 275 61 4 5 007 227

12 099 00 lt10 229

13 104 T 226

14 102 00

15 100 00 16

099 00 225

17 100 00 229

i 18 103 00 118 113 69 3 4 008 229

19 102 T 733 230

20 101 00 229

I 21 095 00

122 096 00

23 099 00 232

24 098 00 234 i

25 099 00 131 199 69 6 11 01 233

26 035 T lt10 236

27 042 00 235

28 087 00

29 093 T

30 061 T 26

31 100 T 247

[Total 2982

iAVQ 096 t04 176 4 7 0CJ8 44 375 187 230 58 244 N()

Min 035 67 Max 166 00 89

lA8ORATORY TEST REQUIRED FOR wACTIVATED SlUDGEwPROCESSES

Aeration Baaln ()Ditch Etc

~ Sludge0 MIXED UQUOR Outside I A 00 -MLSS Settlbullbullbllity

Temp - Ambient 3 Disposal30 min E 30mtnW Temperature

CDT East East r E mgII mgII ml ml c OF bull Galions LbsDry Wt 1 88 C 915

2 31 1625 200 200 227 77 C 800

3 18 1322 200 200 229 76 PC 800

4 22 200 200 227 78 C 815

5 30 1678 200 200 222 77 C 800

6 31 1381 200 200 229 75 C 800

7 77 C 715

8 79 C 800

9 10 1850 200 200 229 77 PC 800

10 40 2215 200 229 76 PC 800

11 14 2132 220 226 75 C 800

12 40 2116 220 223 77 C 800

13 27 1935 220 225 73 PC 800

14 80 C 900

15 80 PC 900

16 27 2287 210 226 77 PC 800

11 26 1880 200 226 75 C 800

18 23 1679 180 226 78 C 800

19 26 1515 200 227 72 PC 800

20 27 1163 160 228 71 C 800

21 91 C 1230

22 89 C 845

23 23 1461 150 231 80 C 800

24 25 1412 200 231 78 800 21000 332f

25 29 1413 180 232 77 C 800 24000 4003

26 28 1395 150 234 91 PC 930

27 23 1451 150 240 75 C 800

28 63 C 730

29 79 C 800

30 10 1550 150 231 78 PC 800 15000 2127

31 18 1451 180 100 234 78 PC 800 27000 6305 COMMENTS ~ nICI ncrbull - IVII ICIU 1e5Ui lur I UUlI -IV U~ I VICII _ ILUI1 v ClIIU UI 6shy

GGA results were 1585 mglL on 7312 GGA results were 1339 mglL on 71112

GGA results were 852 on 718112 GGA results were 1433 mglL on 72512

7ull~4i( TlnE DATE

8312PLANT SUPERVISOR Ai 1ampllo~ TITlE DATE tishy LOCAL MANAGER

In tbe weather column use tbe follOWing symbols R-nun S-snow C-clear PC-partly doudy ()overcast

-Required Daily Required llweek

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

luuailceProfessional Walaquor and Wastewalaquor Operations

OPERArIONS REPORT - NEVADA DIVISION

June 2012 Service Work Orders

This Period Year To Date

Action Issued Completed Voided Outstanding Issued Completed Voided Outstanding

Connect 51 48 3 a 394 360 26 8

Disconnect 35 28 1 6 253 224 13 15

Cut Off a a a a a a a a

Meter Info 185 182 2 1 1117 1071 16 29

Meter Change 41 40 a 1 211 204 a 6

OCCChange 80 78 2 a 517 488 16 13

Reinstate 130 130 a a 494 493 2 8 Service Change a a a a 1 a 1 a

Miscellaneous 10 10 a a 229 196 8 25

ITOTALS 532 516 8 8 3216 3036 83 104

146 WaterSewer utility locates during the month

1uuaiiCC Professional Water and Wastewater Operations

OPERATIONS REPORT - NEVADA DIVISION

Water Loss

Total Water Delivered

January February March 23285000 April 31797000 May 31000000 June 29080000 July August September October November December

Identified Water Loss

175000 39500

2145000 47000

Billed Consumption

21119200 21686200 19733143 20157450

Unidentified Water Loss

1990800 10071300 9121857 8875550

Water Loss

85 317 294 305

I I

I

I I

IYTD Total 1115162000 1 2406500 I 82695993 I 30059507 1 250

Identified Water Loss Detail

Leaks January February March 25000 April 25000 May 100000 June 20000 July August

September October

November December

Flushing Fire Dept

8000 12000 2000 12500

1970000 75000 2000 25000

Other Total I

I

130000 175000 I

0 39500 I

0 2145000

0 47000 I

0 o i

OJ o i

01 01

1YTD Total 1 170000 1982000 124500 130000 2406500 I

lMllaDCeProfessional Water and Wastewater Operations

OPERATIONS REPORT - NEVADA DIVISION

June 2012 Water Loss Detail Explanation

Leaks This column is an estimation of leaks that were known during the reporting period During the month an estimated 20000 gallons were lost from service leaks throughout the distribution system

Flushing The Flushing column reflects an estimation of water lost from the routine flushing ofdead end mains in the system or if a customer had a dirty water complaint the area may get flushed if it appears to be from the distribution system Approximately 2000 gallons were used for flushing

Fire Dept The column represents water used by the Fire dept for fighting fires and training exercises This month approximately 25000 gallons were used for the purpose offirefighting and training

Other This is a miscellaneous column to catch out of the ordinary water uses Nothing to report in this column for the month

20000 Leaks 2000 Flushing 25000 Fire Dept

+0 Other =47000 Total

Water Loss Calculation

Water Loss The water loss is calculated by subtracting the Identified Water Loss (47000) and the Billed Consumption (20157450) from the Total Water Delivered (29080000) to come up with the Unidentified Water Loss (8875550) To calculate the Water Loss divide Unidentified Water Loss into Total Water Delivered

29080000 - (47000 + 20157450) = 8875550

887555029080000 = 0305 or 305

G MISSOURI OEPARTMENT OF NATURAL RESOURCES - WATER PROTECTION PROGRAM

~ ~ MONTHLY COMPLIANCE MONITORING REPORT FOR GROUNDWATER SYSTEMS

PJ8l1C WATpoundR SYSYEM IWoIf IPUIIlIC WAllR 1)1gt1110110 NVMIA jCOUHPICity of Nevada Me 5010562 Vernon

Mtnlmum Residual __ z Minim Residual _ Minimum Re5idual

4-Ioa SatnoIe locabon 4-109 Sm~LocatIOn 4-1Og Sample Location MonthI pH Tamp LowestF pH Temp LOWHtFre pH Temp lowMtF V degc Chlonne (mgll) degc Chlorine (mgl1)

I~middotmiddotmiddot--middotmiddot degc ChlorlM (mgll)

2~---664 211 23 fmiddot-- shy ---shy -shy-- shy877 21 Lo 23

--~-- ----- shy3 888 208 23 4 892 20A 23 5 890 212 23

6 88]_ I- 211 __ 22

1- 7 22 8_~ 215 ----- -----~-

--___ ------ shy----- shy f----_ k___ ~middot__ shy - ~

8 896 208 18-9 893 211 21

10 888 213 19

[11_ 885 _21Q_ 22 --rmiddot----middot shy ----~-~-~

h~- 894 206 19 13 911 215 21

14 883 210 20 I 15 884 211 23 I

16 880 212 21

~ 887 212 22 18 877 208 21

t-19 897 ~1 19~-----------shy120 902 206 ~ 1 7

r -- shy -- ---shy -~-----i---- _- shy - t--middot i 21 ~JL12 208 19_h----shy _-- shy ~--------

22 892 215 20 i 23 888 211 21 i 24 878 210 22 -125 892 211 22 i 26 806 O8 21 j2j ~--~ shy

906 208 21 t

I~8 864 214 19

I E4129 893 211 25 f3tf 914 212 19 -i 31 898 213 21 II Was the diSinfectant t9sidual ever less than the Slate reqUIred level for 4-109 InactIvation 01 viruses at thiS enlry POintIOYn III No _ If 0 old the wa1er system collect grab samples every four hours until the d-ls--lnfe--cta---n7t-re-s~id-u--alw-a-s--a--bo-ve~lhe--S~--ale required level

I 0 Va ~ No Ifm enswet yes to this question attach the resuU~~- theELsarl)II~19thslrn~L ___ i (For IyqmS serving more than 33(0) Old continuous monitOring equipment fail at any time during this reportll1g penoo

1I DYII2I No (For systems serving I1lQ(6 than 3300) If monitoring equipment taded were grab samples collected every 4 hours until the I conllnuous monitonng equipment was returned to SftlV1Ce gJ~Jttach itab sample results to this form)

RSON 1Ii5A ~ _----__---------1 -I

I 61 PAJIili2

1-751-=~ry~+HhltIo=iPflIlll_-_----__---- --==Tomiddot~-i~-middot~ (9 t~-_-~-l Jose h Ti

Laboratory Log-In and Chlorine Report form

(Julv 2012)

Sample ID Date I Time Received Received

Initals Supply 10 Date

Taken

middot~ (

- -) I

30 l Y 11 I I I

f it Il

15 I j

SJ (( 1 (

7 J 2

1 I r

~~~ I~

Jc (

II V

I j J

3lt I

b ampf Lf S 7btC

j)3

3rltl-7

72lc (

17-IP

J ) (

l I

lt12

gtI L

) I

111shy

II ~lt II _

r7

7lt II

fI I ~

I i 112

J i 1 (2

71i71fl I

71711 Irl12

Jpound I dH1lshy

Y)~2 b12 1) ~J L

rIshy il~ ~ 1dlj

I~ It III IllL lt I 711

- ( I 1 (i I

12 ( I r I Ci r t)

- I( ( (

~t( (~ It f( C i

I

II I f ~

rl Ie I

I r L

I

lt l f (

0ilt 2

c r~ -~ I Lc ~ ~~ ~I Irl (

eer

tr

c- (

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rr shy

7

if

ICc ( I IT

cclflf (SOC lAP

2~ I-J)( fI

ICc 1-

Ieee I rr

(c I ~h

Ie cc If

5 (lt4shy shy

i ( ~(- ~

--s[(r)c

ltv[ S lt

i 1 I ~

1 Ie I leiIt

7kI( I

jCr laquo I i 12 - J ~ C

r Clc) )fl 7170 fc IC- J51 (7) 11shy

Ie 16Yi1jfitz 5lpoundJ~2 (]2 SlICSeuro I I-~ 3hL~

7 5(ltlt I I 1j~

11 iLI u-sL ~ I )V 2

Time Taken

Location Chlorine

Free I Total

Collectors Initials

~( Slt-i j ( of -(

L h fl- (ISshy

~- I i J -~ 7 )l J Iv IG I J 11lt

tlf bull ( I r iI r l f~ ~-_I h ff-I~middot C~

lr t r --) - ~ 1 ~Lt Icph L1 fl 117

I

i kT 1- if ipoundI t Ni IV(J_ h 1

~ I I I 1shy

c)~ I I ~ 1-) i L ii I I ) l lrr NCA r-r L l L

C (t

~ -shy

1 I bull1

tl~

ltj 0 I h1 (~

I II fi h~jT

L ( IAII

c 7( 1(1p

lt 1 I ~lrf t t i I I J L -shy c

( -7 I ( Z-J II)J

( Jt ( i--rgt- (shy i ----~-f ~i~ II Jmiddotf pound

t ( ~r ~ J J LI I (~ J~ c

[ i ltj- 7

bull ~l j t- L I Jshy if I f IJ 1

Yc- L ~ _ ~-- r i )- C i ) J t ff r~ ( 7

13 l 4~g pound Wlj)Oh Ishy shy

J )4 qoq tv 11h ---shycSl pound+ 1 ramp X Yk exuIrl ( ( ltl-

I

L ~- 3c( I Ci-(~(L I 2J

( -) -ltII j tUjshy J

( J c)~_ lL 1+ 11 I

( ff 1-1- 71 shy (

7 sshy

(

-

~

9 i

)0

ccsshy

2 ~ -

2(

r-

I C

f rshy

Ir

Ji

()tr

- poundI

fl 0

II (f~

tu

rnF

)(

Remarks

- - -

Laboratory Log-In and Chlorine Report form

Sample 10 Date Time

Initals Supply 10Received Received

1 ~( J -)2shy ICCmiddot( 7f -I(~12

)gt 1amp 7l~( h 110 ~ M~ ))1 ~)~S

l~ G- L -d tshy II ~o5 Ct~ 02J5

_----shy _ _shy

Date Taken

Time location

Taken

7f J1Z escSshy laquo7 IS j illt- ~s middot r)

1-1 ~ d10S S~o H1t+t t S r bleAt I If I ) ifl)S 110 ~Ymiddottt b~Xt

shy __shy _

Chlorine Collectors Remarks

Free Total Initials

1Z Z nrF

- 1J1 f - 51 if

Missouri Dcpartmcnt Of latural Resources Public Drinkine Water Program

PO 80x 176 kfrcrson (it~ to 65102 (573)751-5331

Public Vater System Bacteriological Report

S ~aml NEVADA PWS If) M050 I 05tl2

Mail 10 JOSEPH TIPPER

1300 W CHERRY County VERNON

NEVADA MO 64772 Plcase n(llll~ u- (I IllY name and addres lhangls

Sample TypeIgtal( (lIlhrhd ColIlCtor

ROlltine07092012 MF lab RtSuitl Io~ation Nanl( Location II)Lab SamplE m

NEVADA~ A120 SASH

Coliform IIhent Sample considtred safe

26566

Sample T~I)( Dau Colletmiddotted ColleClor

Routine070912012 MF Iah Rtmiddot ults Ioration alUr loCalioll II)Lab SampltlO

71 HWY N NEVADA4 A

Coliform absent Samplt (onsidCndsaft

265M

Sample T~pt nail Coller led Collerl()r

Routine07092012 MF

Lab Sampl( m Location janie Lmalioll Ill Iah RIiull

50 I S JEFFERSON NEVADA5 A

(ouror absent Sample considered safe

26565

~

Santl)- Typt COIltllIr

07092012 MF Routine

Lab SlImpie III 1lnalion SlUt Iocalion IIgt Iah RlSUItS

41 I S WESl NEVADA2 A26563

Note to public water systems If you take a routine sample from a well rather than your distrIbution system a violation may be Issued by Missouri Public Drinking Water Branch

i-ridul July Il 101

Q -_

lissouri Department Of Natural Resources i_~~ Public Drinking Water ProJram

PO Box 176 Jefferson Cit) I0 65102 (573)751-5331

Public Water System Bacteriological Report

NEVADA PS I) M05010562rws 1I111t

JOSEPI TIPPER lail to Counl) VERNON 1300 W CHERRY

NEVADA MO 64772 Plcmc Il(llify us Ill any name and addrcs challgl

Samllil TYPl I)lltl (ullechd Collector

Routine07 )9 W12 MF Iab Relulll Lab SlImpll III LOC8110n Iianl Location II)

26567 1300 W CHERRY NEVADAI A

(oliform absent Samplf fonsidered safe ~~ t4_-mc-W ~

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

middotridIJYbullbullIul 13 101

IWS alllt

laillo

i~sotJri Dep_urment Of turall~((lurn Iuhlir flrinldlll WU(r lrIIJraOl

VO Rn 171 Jcff(middotrion (it 10 hS 1112

NIVAI)

JOSEPU TIPPER

I 30n W CH ERR Y NI ADA MO (-4112

Ihue (ollltld

lPOI)

LlIh Slimple 11)

2Q342

1)11 ( IIlied ttl

07 B2012

Lllh ~IUIIJlh In

nle (nllfhd

(J72J012

I Il 11 In

I h SlIupll I()

II

UOO W ClIIRRY

11

LW S ASII

( lIl(middottor

~II

11 11 Y l

Ml

( IIIIII~ VERNON

111 IhlIl~ U 111111

I)IIIW HId dfmiddot dlIII11l

1(1(31 ion II) Inh ~(lh

R()UlllC

LmlIliulI II)

I m11 intI I D

llllpk I ~ lit

Imiddotcutlll~middot

I all 1UII

Note to public water systems If you lake a routine sample from a well rather than your distribution system a violation may be issued by Missouri Public Drinking Waler Branch

IriJIII)-

shyI~-~f r -----1

I

4 (D Iissouri Illpartmcnl Of atunlJ icsOUrltCli L ~_ __ _ uhlie UrinkinJ Wllu Irolram

PO Bo 17h hfhrwll Ci~ 1O h~ 1tI

Jmiddotuhlic ate S~slcm Bll(tlrioloJical I~cporl

NFADA II) ~H raquo)(J IOh

ailltl JOSEI)II lWPLR

I ~oo CHERRY (Hunl VERNON

NlADA MO hmiddotP Pill IlOlin li 11 HI

II lIll ltllld 1hlr t L hIII~

l1Ipk T~ p I)alt (nlll(tli ( nlhctur

Rwin0 3 201 MF

Ioealillll II) I all 1(11 Ill SlImpl III

411 ~ WIS I

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

I riduy III1 - III

MI~~OUftl DePARTMENT OF NATURAL RESOURCES DIVISION OF ENVIRONMENTAL QUALITY

Discharge Monitoring Report For Municipal Wastewater Treatment Plants

N- OF FACILITY lOCA11UN iampCrTY ~ _shyNvada 1IItit WIItIIf rnt 117 s 1338 ROid NevIIda VERNONISOUTHWEST

IIR-r OUTFALL NUllBER TYPI ACLTY

IIIIyl2012 M0-00891 09 001 OXIDATION OtTCH INFLUENT FFFI JFIIIT

rNCiI -rAlp E OtL DATE FLOW BOD TSS u~s BOD TSS TEMP DO

IIIGO mall mall mall mall mall mall CFUllOOMl C mQt1 mQt1 mgI

1 067 00

2 O~9 00 226

I 3 089 00 122 118 67 3 7 005 228

4 091 00 227

5 096 00 44 375 lt10 200 58 2440 NO

6 100 00 228

7 099 00

8 098 00

9 166 00 231

10 139 00 229

11 095 00 44 275 61 4 5 007 227

12 099 00 lt10 229

13 104 T 226

14 102 00

15 100 00 16

099 00 225

17 100 00 229

i 18 103 00 118 113 69 3 4 008 229

19 102 T 733 230

20 101 00 229

I 21 095 00

122 096 00

23 099 00 232

24 098 00 234 i

25 099 00 131 199 69 6 11 01 233

26 035 T lt10 236

27 042 00 235

28 087 00

29 093 T

30 061 T 26

31 100 T 247

[Total 2982

iAVQ 096 t04 176 4 7 0CJ8 44 375 187 230 58 244 N()

Min 035 67 Max 166 00 89

lA8ORATORY TEST REQUIRED FOR wACTIVATED SlUDGEwPROCESSES

Aeration Baaln ()Ditch Etc

~ Sludge0 MIXED UQUOR Outside I A 00 -MLSS Settlbullbullbllity

Temp - Ambient 3 Disposal30 min E 30mtnW Temperature

CDT East East r E mgII mgII ml ml c OF bull Galions LbsDry Wt 1 88 C 915

2 31 1625 200 200 227 77 C 800

3 18 1322 200 200 229 76 PC 800

4 22 200 200 227 78 C 815

5 30 1678 200 200 222 77 C 800

6 31 1381 200 200 229 75 C 800

7 77 C 715

8 79 C 800

9 10 1850 200 200 229 77 PC 800

10 40 2215 200 229 76 PC 800

11 14 2132 220 226 75 C 800

12 40 2116 220 223 77 C 800

13 27 1935 220 225 73 PC 800

14 80 C 900

15 80 PC 900

16 27 2287 210 226 77 PC 800

11 26 1880 200 226 75 C 800

18 23 1679 180 226 78 C 800

19 26 1515 200 227 72 PC 800

20 27 1163 160 228 71 C 800

21 91 C 1230

22 89 C 845

23 23 1461 150 231 80 C 800

24 25 1412 200 231 78 800 21000 332f

25 29 1413 180 232 77 C 800 24000 4003

26 28 1395 150 234 91 PC 930

27 23 1451 150 240 75 C 800

28 63 C 730

29 79 C 800

30 10 1550 150 231 78 PC 800 15000 2127

31 18 1451 180 100 234 78 PC 800 27000 6305 COMMENTS ~ nICI ncrbull - IVII ICIU 1e5Ui lur I UUlI -IV U~ I VICII _ ILUI1 v ClIIU UI 6shy

GGA results were 1585 mglL on 7312 GGA results were 1339 mglL on 71112

GGA results were 852 on 718112 GGA results were 1433 mglL on 72512

7ull~4i( TlnE DATE

8312PLANT SUPERVISOR Ai 1ampllo~ TITlE DATE tishy LOCAL MANAGER

In tbe weather column use tbe follOWing symbols R-nun S-snow C-clear PC-partly doudy ()overcast

-Required Daily Required llweek

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

1uuaiiCC Professional Water and Wastewater Operations

OPERATIONS REPORT - NEVADA DIVISION

Water Loss

Total Water Delivered

January February March 23285000 April 31797000 May 31000000 June 29080000 July August September October November December

Identified Water Loss

175000 39500

2145000 47000

Billed Consumption

21119200 21686200 19733143 20157450

Unidentified Water Loss

1990800 10071300 9121857 8875550

Water Loss

85 317 294 305

I I

I

I I

IYTD Total 1115162000 1 2406500 I 82695993 I 30059507 1 250

Identified Water Loss Detail

Leaks January February March 25000 April 25000 May 100000 June 20000 July August

September October

November December

Flushing Fire Dept

8000 12000 2000 12500

1970000 75000 2000 25000

Other Total I

I

130000 175000 I

0 39500 I

0 2145000

0 47000 I

0 o i

OJ o i

01 01

1YTD Total 1 170000 1982000 124500 130000 2406500 I

lMllaDCeProfessional Water and Wastewater Operations

OPERATIONS REPORT - NEVADA DIVISION

June 2012 Water Loss Detail Explanation

Leaks This column is an estimation of leaks that were known during the reporting period During the month an estimated 20000 gallons were lost from service leaks throughout the distribution system

Flushing The Flushing column reflects an estimation of water lost from the routine flushing ofdead end mains in the system or if a customer had a dirty water complaint the area may get flushed if it appears to be from the distribution system Approximately 2000 gallons were used for flushing

Fire Dept The column represents water used by the Fire dept for fighting fires and training exercises This month approximately 25000 gallons were used for the purpose offirefighting and training

Other This is a miscellaneous column to catch out of the ordinary water uses Nothing to report in this column for the month

20000 Leaks 2000 Flushing 25000 Fire Dept

+0 Other =47000 Total

Water Loss Calculation

Water Loss The water loss is calculated by subtracting the Identified Water Loss (47000) and the Billed Consumption (20157450) from the Total Water Delivered (29080000) to come up with the Unidentified Water Loss (8875550) To calculate the Water Loss divide Unidentified Water Loss into Total Water Delivered

29080000 - (47000 + 20157450) = 8875550

887555029080000 = 0305 or 305

G MISSOURI OEPARTMENT OF NATURAL RESOURCES - WATER PROTECTION PROGRAM

~ ~ MONTHLY COMPLIANCE MONITORING REPORT FOR GROUNDWATER SYSTEMS

PJ8l1C WATpoundR SYSYEM IWoIf IPUIIlIC WAllR 1)1gt1110110 NVMIA jCOUHPICity of Nevada Me 5010562 Vernon

Mtnlmum Residual __ z Minim Residual _ Minimum Re5idual

4-Ioa SatnoIe locabon 4-109 Sm~LocatIOn 4-1Og Sample Location MonthI pH Tamp LowestF pH Temp LOWHtFre pH Temp lowMtF V degc Chlonne (mgll) degc Chlorine (mgl1)

I~middotmiddotmiddot--middotmiddot degc ChlorlM (mgll)

2~---664 211 23 fmiddot-- shy ---shy -shy-- shy877 21 Lo 23

--~-- ----- shy3 888 208 23 4 892 20A 23 5 890 212 23

6 88]_ I- 211 __ 22

1- 7 22 8_~ 215 ----- -----~-

--___ ------ shy----- shy f----_ k___ ~middot__ shy - ~

8 896 208 18-9 893 211 21

10 888 213 19

[11_ 885 _21Q_ 22 --rmiddot----middot shy ----~-~-~

h~- 894 206 19 13 911 215 21

14 883 210 20 I 15 884 211 23 I

16 880 212 21

~ 887 212 22 18 877 208 21

t-19 897 ~1 19~-----------shy120 902 206 ~ 1 7

r -- shy -- ---shy -~-----i---- _- shy - t--middot i 21 ~JL12 208 19_h----shy _-- shy ~--------

22 892 215 20 i 23 888 211 21 i 24 878 210 22 -125 892 211 22 i 26 806 O8 21 j2j ~--~ shy

906 208 21 t

I~8 864 214 19

I E4129 893 211 25 f3tf 914 212 19 -i 31 898 213 21 II Was the diSinfectant t9sidual ever less than the Slate reqUIred level for 4-109 InactIvation 01 viruses at thiS enlry POintIOYn III No _ If 0 old the wa1er system collect grab samples every four hours until the d-ls--lnfe--cta---n7t-re-s~id-u--alw-a-s--a--bo-ve~lhe--S~--ale required level

I 0 Va ~ No Ifm enswet yes to this question attach the resuU~~- theELsarl)II~19thslrn~L ___ i (For IyqmS serving more than 33(0) Old continuous monitOring equipment fail at any time during this reportll1g penoo

1I DYII2I No (For systems serving I1lQ(6 than 3300) If monitoring equipment taded were grab samples collected every 4 hours until the I conllnuous monitonng equipment was returned to SftlV1Ce gJ~Jttach itab sample results to this form)

RSON 1Ii5A ~ _----__---------1 -I

I 61 PAJIili2

1-751-=~ry~+HhltIo=iPflIlll_-_----__---- --==Tomiddot~-i~-middot~ (9 t~-_-~-l Jose h Ti

Laboratory Log-In and Chlorine Report form

(Julv 2012)

Sample ID Date I Time Received Received

Initals Supply 10 Date

Taken

middot~ (

- -) I

30 l Y 11 I I I

f it Il

15 I j

SJ (( 1 (

7 J 2

1 I r

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Jc (

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b ampf Lf S 7btC

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lt12

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111shy

II ~lt II _

r7

7lt II

fI I ~

I i 112

J i 1 (2

71i71fl I

71711 Irl12

Jpound I dH1lshy

Y)~2 b12 1) ~J L

rIshy il~ ~ 1dlj

I~ It III IllL lt I 711

- ( I 1 (i I

12 ( I r I Ci r t)

- I( ( (

~t( (~ It f( C i

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I

lt l f (

0ilt 2

c r~ -~ I Lc ~ ~~ ~I Irl (

eer

tr

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rr shy

7

if

ICc ( I IT

cclflf (SOC lAP

2~ I-J)( fI

ICc 1-

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5 (lt4shy shy

i ( ~(- ~

--s[(r)c

ltv[ S lt

i 1 I ~

1 Ie I leiIt

7kI( I

jCr laquo I i 12 - J ~ C

r Clc) )fl 7170 fc IC- J51 (7) 11shy

Ie 16Yi1jfitz 5lpoundJ~2 (]2 SlICSeuro I I-~ 3hL~

7 5(ltlt I I 1j~

11 iLI u-sL ~ I )V 2

Time Taken

Location Chlorine

Free I Total

Collectors Initials

~( Slt-i j ( of -(

L h fl- (ISshy

~- I i J -~ 7 )l J Iv IG I J 11lt

tlf bull ( I r iI r l f~ ~-_I h ff-I~middot C~

lr t r --) - ~ 1 ~Lt Icph L1 fl 117

I

i kT 1- if ipoundI t Ni IV(J_ h 1

~ I I I 1shy

c)~ I I ~ 1-) i L ii I I ) l lrr NCA r-r L l L

C (t

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1 I bull1

tl~

ltj 0 I h1 (~

I II fi h~jT

L ( IAII

c 7( 1(1p

lt 1 I ~lrf t t i I I J L -shy c

( -7 I ( Z-J II)J

( Jt ( i--rgt- (shy i ----~-f ~i~ II Jmiddotf pound

t ( ~r ~ J J LI I (~ J~ c

[ i ltj- 7

bull ~l j t- L I Jshy if I f IJ 1

Yc- L ~ _ ~-- r i )- C i ) J t ff r~ ( 7

13 l 4~g pound Wlj)Oh Ishy shy

J )4 qoq tv 11h ---shycSl pound+ 1 ramp X Yk exuIrl ( ( ltl-

I

L ~- 3c( I Ci-(~(L I 2J

( -) -ltII j tUjshy J

( J c)~_ lL 1+ 11 I

( ff 1-1- 71 shy (

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-

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2(

r-

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f rshy

Ir

Ji

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- poundI

fl 0

II (f~

tu

rnF

)(

Remarks

- - -

Laboratory Log-In and Chlorine Report form

Sample 10 Date Time

Initals Supply 10Received Received

1 ~( J -)2shy ICCmiddot( 7f -I(~12

)gt 1amp 7l~( h 110 ~ M~ ))1 ~)~S

l~ G- L -d tshy II ~o5 Ct~ 02J5

_----shy _ _shy

Date Taken

Time location

Taken

7f J1Z escSshy laquo7 IS j illt- ~s middot r)

1-1 ~ d10S S~o H1t+t t S r bleAt I If I ) ifl)S 110 ~Ymiddottt b~Xt

shy __shy _

Chlorine Collectors Remarks

Free Total Initials

1Z Z nrF

- 1J1 f - 51 if

Missouri Dcpartmcnt Of latural Resources Public Drinkine Water Program

PO 80x 176 kfrcrson (it~ to 65102 (573)751-5331

Public Vater System Bacteriological Report

S ~aml NEVADA PWS If) M050 I 05tl2

Mail 10 JOSEPH TIPPER

1300 W CHERRY County VERNON

NEVADA MO 64772 Plcase n(llll~ u- (I IllY name and addres lhangls

Sample TypeIgtal( (lIlhrhd ColIlCtor

ROlltine07092012 MF lab RtSuitl Io~ation Nanl( Location II)Lab SamplE m

NEVADA~ A120 SASH

Coliform IIhent Sample considtred safe

26566

Sample T~I)( Dau Colletmiddotted ColleClor

Routine070912012 MF Iah Rtmiddot ults Ioration alUr loCalioll II)Lab SampltlO

71 HWY N NEVADA4 A

Coliform absent Samplt (onsidCndsaft

265M

Sample T~pt nail Coller led Collerl()r

Routine07092012 MF

Lab Sampl( m Location janie Lmalioll Ill Iah RIiull

50 I S JEFFERSON NEVADA5 A

(ouror absent Sample considered safe

26565

~

Santl)- Typt COIltllIr

07092012 MF Routine

Lab SlImpie III 1lnalion SlUt Iocalion IIgt Iah RlSUItS

41 I S WESl NEVADA2 A26563

Note to public water systems If you take a routine sample from a well rather than your distrIbution system a violation may be Issued by Missouri Public Drinking Water Branch

i-ridul July Il 101

Q -_

lissouri Department Of Natural Resources i_~~ Public Drinking Water ProJram

PO Box 176 Jefferson Cit) I0 65102 (573)751-5331

Public Water System Bacteriological Report

NEVADA PS I) M05010562rws 1I111t

JOSEPI TIPPER lail to Counl) VERNON 1300 W CHERRY

NEVADA MO 64772 Plcmc Il(llify us Ill any name and addrcs challgl

Samllil TYPl I)lltl (ullechd Collector

Routine07 )9 W12 MF Iab Relulll Lab SlImpll III LOC8110n Iianl Location II)

26567 1300 W CHERRY NEVADAI A

(oliform absent Samplf fonsidered safe ~~ t4_-mc-W ~

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

middotridIJYbullbullIul 13 101

IWS alllt

laillo

i~sotJri Dep_urment Of turall~((lurn Iuhlir flrinldlll WU(r lrIIJraOl

VO Rn 171 Jcff(middotrion (it 10 hS 1112

NIVAI)

JOSEPU TIPPER

I 30n W CH ERR Y NI ADA MO (-4112

Ihue (ollltld

lPOI)

LlIh Slimple 11)

2Q342

1)11 ( IIlied ttl

07 B2012

Lllh ~IUIIJlh In

nle (nllfhd

(J72J012

I Il 11 In

I h SlIupll I()

II

UOO W ClIIRRY

11

LW S ASII

( lIl(middottor

~II

11 11 Y l

Ml

( IIIIII~ VERNON

111 IhlIl~ U 111111

I)IIIW HId dfmiddot dlIII11l

1(1(31 ion II) Inh ~(lh

R()UlllC

LmlIliulI II)

I m11 intI I D

llllpk I ~ lit

Imiddotcutlll~middot

I all 1UII

Note to public water systems If you lake a routine sample from a well rather than your distribution system a violation may be issued by Missouri Public Drinking Waler Branch

IriJIII)-

shyI~-~f r -----1

I

4 (D Iissouri Illpartmcnl Of atunlJ icsOUrltCli L ~_ __ _ uhlie UrinkinJ Wllu Irolram

PO Bo 17h hfhrwll Ci~ 1O h~ 1tI

Jmiddotuhlic ate S~slcm Bll(tlrioloJical I~cporl

NFADA II) ~H raquo)(J IOh

ailltl JOSEI)II lWPLR

I ~oo CHERRY (Hunl VERNON

NlADA MO hmiddotP Pill IlOlin li 11 HI

II lIll ltllld 1hlr t L hIII~

l1Ipk T~ p I)alt (nlll(tli ( nlhctur

Rwin0 3 201 MF

Ioealillll II) I all 1(11 Ill SlImpl III

411 ~ WIS I

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

I riduy III1 - III

MI~~OUftl DePARTMENT OF NATURAL RESOURCES DIVISION OF ENVIRONMENTAL QUALITY

Discharge Monitoring Report For Municipal Wastewater Treatment Plants

N- OF FACILITY lOCA11UN iampCrTY ~ _shyNvada 1IItit WIItIIf rnt 117 s 1338 ROid NevIIda VERNONISOUTHWEST

IIR-r OUTFALL NUllBER TYPI ACLTY

IIIIyl2012 M0-00891 09 001 OXIDATION OtTCH INFLUENT FFFI JFIIIT

rNCiI -rAlp E OtL DATE FLOW BOD TSS u~s BOD TSS TEMP DO

IIIGO mall mall mall mall mall mall CFUllOOMl C mQt1 mQt1 mgI

1 067 00

2 O~9 00 226

I 3 089 00 122 118 67 3 7 005 228

4 091 00 227

5 096 00 44 375 lt10 200 58 2440 NO

6 100 00 228

7 099 00

8 098 00

9 166 00 231

10 139 00 229

11 095 00 44 275 61 4 5 007 227

12 099 00 lt10 229

13 104 T 226

14 102 00

15 100 00 16

099 00 225

17 100 00 229

i 18 103 00 118 113 69 3 4 008 229

19 102 T 733 230

20 101 00 229

I 21 095 00

122 096 00

23 099 00 232

24 098 00 234 i

25 099 00 131 199 69 6 11 01 233

26 035 T lt10 236

27 042 00 235

28 087 00

29 093 T

30 061 T 26

31 100 T 247

[Total 2982

iAVQ 096 t04 176 4 7 0CJ8 44 375 187 230 58 244 N()

Min 035 67 Max 166 00 89

lA8ORATORY TEST REQUIRED FOR wACTIVATED SlUDGEwPROCESSES

Aeration Baaln ()Ditch Etc

~ Sludge0 MIXED UQUOR Outside I A 00 -MLSS Settlbullbullbllity

Temp - Ambient 3 Disposal30 min E 30mtnW Temperature

CDT East East r E mgII mgII ml ml c OF bull Galions LbsDry Wt 1 88 C 915

2 31 1625 200 200 227 77 C 800

3 18 1322 200 200 229 76 PC 800

4 22 200 200 227 78 C 815

5 30 1678 200 200 222 77 C 800

6 31 1381 200 200 229 75 C 800

7 77 C 715

8 79 C 800

9 10 1850 200 200 229 77 PC 800

10 40 2215 200 229 76 PC 800

11 14 2132 220 226 75 C 800

12 40 2116 220 223 77 C 800

13 27 1935 220 225 73 PC 800

14 80 C 900

15 80 PC 900

16 27 2287 210 226 77 PC 800

11 26 1880 200 226 75 C 800

18 23 1679 180 226 78 C 800

19 26 1515 200 227 72 PC 800

20 27 1163 160 228 71 C 800

21 91 C 1230

22 89 C 845

23 23 1461 150 231 80 C 800

24 25 1412 200 231 78 800 21000 332f

25 29 1413 180 232 77 C 800 24000 4003

26 28 1395 150 234 91 PC 930

27 23 1451 150 240 75 C 800

28 63 C 730

29 79 C 800

30 10 1550 150 231 78 PC 800 15000 2127

31 18 1451 180 100 234 78 PC 800 27000 6305 COMMENTS ~ nICI ncrbull - IVII ICIU 1e5Ui lur I UUlI -IV U~ I VICII _ ILUI1 v ClIIU UI 6shy

GGA results were 1585 mglL on 7312 GGA results were 1339 mglL on 71112

GGA results were 852 on 718112 GGA results were 1433 mglL on 72512

7ull~4i( TlnE DATE

8312PLANT SUPERVISOR Ai 1ampllo~ TITlE DATE tishy LOCAL MANAGER

In tbe weather column use tbe follOWing symbols R-nun S-snow C-clear PC-partly doudy ()overcast

-Required Daily Required llweek

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

lMllaDCeProfessional Water and Wastewater Operations

OPERATIONS REPORT - NEVADA DIVISION

June 2012 Water Loss Detail Explanation

Leaks This column is an estimation of leaks that were known during the reporting period During the month an estimated 20000 gallons were lost from service leaks throughout the distribution system

Flushing The Flushing column reflects an estimation of water lost from the routine flushing ofdead end mains in the system or if a customer had a dirty water complaint the area may get flushed if it appears to be from the distribution system Approximately 2000 gallons were used for flushing

Fire Dept The column represents water used by the Fire dept for fighting fires and training exercises This month approximately 25000 gallons were used for the purpose offirefighting and training

Other This is a miscellaneous column to catch out of the ordinary water uses Nothing to report in this column for the month

20000 Leaks 2000 Flushing 25000 Fire Dept

+0 Other =47000 Total

Water Loss Calculation

Water Loss The water loss is calculated by subtracting the Identified Water Loss (47000) and the Billed Consumption (20157450) from the Total Water Delivered (29080000) to come up with the Unidentified Water Loss (8875550) To calculate the Water Loss divide Unidentified Water Loss into Total Water Delivered

29080000 - (47000 + 20157450) = 8875550

887555029080000 = 0305 or 305

G MISSOURI OEPARTMENT OF NATURAL RESOURCES - WATER PROTECTION PROGRAM

~ ~ MONTHLY COMPLIANCE MONITORING REPORT FOR GROUNDWATER SYSTEMS

PJ8l1C WATpoundR SYSYEM IWoIf IPUIIlIC WAllR 1)1gt1110110 NVMIA jCOUHPICity of Nevada Me 5010562 Vernon

Mtnlmum Residual __ z Minim Residual _ Minimum Re5idual

4-Ioa SatnoIe locabon 4-109 Sm~LocatIOn 4-1Og Sample Location MonthI pH Tamp LowestF pH Temp LOWHtFre pH Temp lowMtF V degc Chlonne (mgll) degc Chlorine (mgl1)

I~middotmiddotmiddot--middotmiddot degc ChlorlM (mgll)

2~---664 211 23 fmiddot-- shy ---shy -shy-- shy877 21 Lo 23

--~-- ----- shy3 888 208 23 4 892 20A 23 5 890 212 23

6 88]_ I- 211 __ 22

1- 7 22 8_~ 215 ----- -----~-

--___ ------ shy----- shy f----_ k___ ~middot__ shy - ~

8 896 208 18-9 893 211 21

10 888 213 19

[11_ 885 _21Q_ 22 --rmiddot----middot shy ----~-~-~

h~- 894 206 19 13 911 215 21

14 883 210 20 I 15 884 211 23 I

16 880 212 21

~ 887 212 22 18 877 208 21

t-19 897 ~1 19~-----------shy120 902 206 ~ 1 7

r -- shy -- ---shy -~-----i---- _- shy - t--middot i 21 ~JL12 208 19_h----shy _-- shy ~--------

22 892 215 20 i 23 888 211 21 i 24 878 210 22 -125 892 211 22 i 26 806 O8 21 j2j ~--~ shy

906 208 21 t

I~8 864 214 19

I E4129 893 211 25 f3tf 914 212 19 -i 31 898 213 21 II Was the diSinfectant t9sidual ever less than the Slate reqUIred level for 4-109 InactIvation 01 viruses at thiS enlry POintIOYn III No _ If 0 old the wa1er system collect grab samples every four hours until the d-ls--lnfe--cta---n7t-re-s~id-u--alw-a-s--a--bo-ve~lhe--S~--ale required level

I 0 Va ~ No Ifm enswet yes to this question attach the resuU~~- theELsarl)II~19thslrn~L ___ i (For IyqmS serving more than 33(0) Old continuous monitOring equipment fail at any time during this reportll1g penoo

1I DYII2I No (For systems serving I1lQ(6 than 3300) If monitoring equipment taded were grab samples collected every 4 hours until the I conllnuous monitonng equipment was returned to SftlV1Ce gJ~Jttach itab sample results to this form)

RSON 1Ii5A ~ _----__---------1 -I

I 61 PAJIili2

1-751-=~ry~+HhltIo=iPflIlll_-_----__---- --==Tomiddot~-i~-middot~ (9 t~-_-~-l Jose h Ti

Laboratory Log-In and Chlorine Report form

(Julv 2012)

Sample ID Date I Time Received Received

Initals Supply 10 Date

Taken

middot~ (

- -) I

30 l Y 11 I I I

f it Il

15 I j

SJ (( 1 (

7 J 2

1 I r

~~~ I~

Jc (

II V

I j J

3lt I

b ampf Lf S 7btC

j)3

3rltl-7

72lc (

17-IP

J ) (

l I

lt12

gtI L

) I

111shy

II ~lt II _

r7

7lt II

fI I ~

I i 112

J i 1 (2

71i71fl I

71711 Irl12

Jpound I dH1lshy

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rIshy il~ ~ 1dlj

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- ( I 1 (i I

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- I( ( (

~t( (~ It f( C i

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2~ I-J)( fI

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5 (lt4shy shy

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ltv[ S lt

i 1 I ~

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7kI( I

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r Clc) )fl 7170 fc IC- J51 (7) 11shy

Ie 16Yi1jfitz 5lpoundJ~2 (]2 SlICSeuro I I-~ 3hL~

7 5(ltlt I I 1j~

11 iLI u-sL ~ I )V 2

Time Taken

Location Chlorine

Free I Total

Collectors Initials

~( Slt-i j ( of -(

L h fl- (ISshy

~- I i J -~ 7 )l J Iv IG I J 11lt

tlf bull ( I r iI r l f~ ~-_I h ff-I~middot C~

lr t r --) - ~ 1 ~Lt Icph L1 fl 117

I

i kT 1- if ipoundI t Ni IV(J_ h 1

~ I I I 1shy

c)~ I I ~ 1-) i L ii I I ) l lrr NCA r-r L l L

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tl~

ltj 0 I h1 (~

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L ( IAII

c 7( 1(1p

lt 1 I ~lrf t t i I I J L -shy c

( -7 I ( Z-J II)J

( Jt ( i--rgt- (shy i ----~-f ~i~ II Jmiddotf pound

t ( ~r ~ J J LI I (~ J~ c

[ i ltj- 7

bull ~l j t- L I Jshy if I f IJ 1

Yc- L ~ _ ~-- r i )- C i ) J t ff r~ ( 7

13 l 4~g pound Wlj)Oh Ishy shy

J )4 qoq tv 11h ---shycSl pound+ 1 ramp X Yk exuIrl ( ( ltl-

I

L ~- 3c( I Ci-(~(L I 2J

( -) -ltII j tUjshy J

( J c)~_ lL 1+ 11 I

( ff 1-1- 71 shy (

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Remarks

- - -

Laboratory Log-In and Chlorine Report form

Sample 10 Date Time

Initals Supply 10Received Received

1 ~( J -)2shy ICCmiddot( 7f -I(~12

)gt 1amp 7l~( h 110 ~ M~ ))1 ~)~S

l~ G- L -d tshy II ~o5 Ct~ 02J5

_----shy _ _shy

Date Taken

Time location

Taken

7f J1Z escSshy laquo7 IS j illt- ~s middot r)

1-1 ~ d10S S~o H1t+t t S r bleAt I If I ) ifl)S 110 ~Ymiddottt b~Xt

shy __shy _

Chlorine Collectors Remarks

Free Total Initials

1Z Z nrF

- 1J1 f - 51 if

Missouri Dcpartmcnt Of latural Resources Public Drinkine Water Program

PO 80x 176 kfrcrson (it~ to 65102 (573)751-5331

Public Vater System Bacteriological Report

S ~aml NEVADA PWS If) M050 I 05tl2

Mail 10 JOSEPH TIPPER

1300 W CHERRY County VERNON

NEVADA MO 64772 Plcase n(llll~ u- (I IllY name and addres lhangls

Sample TypeIgtal( (lIlhrhd ColIlCtor

ROlltine07092012 MF lab RtSuitl Io~ation Nanl( Location II)Lab SamplE m

NEVADA~ A120 SASH

Coliform IIhent Sample considtred safe

26566

Sample T~I)( Dau Colletmiddotted ColleClor

Routine070912012 MF Iah Rtmiddot ults Ioration alUr loCalioll II)Lab SampltlO

71 HWY N NEVADA4 A

Coliform absent Samplt (onsidCndsaft

265M

Sample T~pt nail Coller led Collerl()r

Routine07092012 MF

Lab Sampl( m Location janie Lmalioll Ill Iah RIiull

50 I S JEFFERSON NEVADA5 A

(ouror absent Sample considered safe

26565

~

Santl)- Typt COIltllIr

07092012 MF Routine

Lab SlImpie III 1lnalion SlUt Iocalion IIgt Iah RlSUItS

41 I S WESl NEVADA2 A26563

Note to public water systems If you take a routine sample from a well rather than your distrIbution system a violation may be Issued by Missouri Public Drinking Water Branch

i-ridul July Il 101

Q -_

lissouri Department Of Natural Resources i_~~ Public Drinking Water ProJram

PO Box 176 Jefferson Cit) I0 65102 (573)751-5331

Public Water System Bacteriological Report

NEVADA PS I) M05010562rws 1I111t

JOSEPI TIPPER lail to Counl) VERNON 1300 W CHERRY

NEVADA MO 64772 Plcmc Il(llify us Ill any name and addrcs challgl

Samllil TYPl I)lltl (ullechd Collector

Routine07 )9 W12 MF Iab Relulll Lab SlImpll III LOC8110n Iianl Location II)

26567 1300 W CHERRY NEVADAI A

(oliform absent Samplf fonsidered safe ~~ t4_-mc-W ~

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

middotridIJYbullbullIul 13 101

IWS alllt

laillo

i~sotJri Dep_urment Of turall~((lurn Iuhlir flrinldlll WU(r lrIIJraOl

VO Rn 171 Jcff(middotrion (it 10 hS 1112

NIVAI)

JOSEPU TIPPER

I 30n W CH ERR Y NI ADA MO (-4112

Ihue (ollltld

lPOI)

LlIh Slimple 11)

2Q342

1)11 ( IIlied ttl

07 B2012

Lllh ~IUIIJlh In

nle (nllfhd

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11 11 Y l

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( IIIIII~ VERNON

111 IhlIl~ U 111111

I)IIIW HId dfmiddot dlIII11l

1(1(31 ion II) Inh ~(lh

R()UlllC

LmlIliulI II)

I m11 intI I D

llllpk I ~ lit

Imiddotcutlll~middot

I all 1UII

Note to public water systems If you lake a routine sample from a well rather than your distribution system a violation may be issued by Missouri Public Drinking Waler Branch

IriJIII)-

shyI~-~f r -----1

I

4 (D Iissouri Illpartmcnl Of atunlJ icsOUrltCli L ~_ __ _ uhlie UrinkinJ Wllu Irolram

PO Bo 17h hfhrwll Ci~ 1O h~ 1tI

Jmiddotuhlic ate S~slcm Bll(tlrioloJical I~cporl

NFADA II) ~H raquo)(J IOh

ailltl JOSEI)II lWPLR

I ~oo CHERRY (Hunl VERNON

NlADA MO hmiddotP Pill IlOlin li 11 HI

II lIll ltllld 1hlr t L hIII~

l1Ipk T~ p I)alt (nlll(tli ( nlhctur

Rwin0 3 201 MF

Ioealillll II) I all 1(11 Ill SlImpl III

411 ~ WIS I

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

I riduy III1 - III

MI~~OUftl DePARTMENT OF NATURAL RESOURCES DIVISION OF ENVIRONMENTAL QUALITY

Discharge Monitoring Report For Municipal Wastewater Treatment Plants

N- OF FACILITY lOCA11UN iampCrTY ~ _shyNvada 1IItit WIItIIf rnt 117 s 1338 ROid NevIIda VERNONISOUTHWEST

IIR-r OUTFALL NUllBER TYPI ACLTY

IIIIyl2012 M0-00891 09 001 OXIDATION OtTCH INFLUENT FFFI JFIIIT

rNCiI -rAlp E OtL DATE FLOW BOD TSS u~s BOD TSS TEMP DO

IIIGO mall mall mall mall mall mall CFUllOOMl C mQt1 mQt1 mgI

1 067 00

2 O~9 00 226

I 3 089 00 122 118 67 3 7 005 228

4 091 00 227

5 096 00 44 375 lt10 200 58 2440 NO

6 100 00 228

7 099 00

8 098 00

9 166 00 231

10 139 00 229

11 095 00 44 275 61 4 5 007 227

12 099 00 lt10 229

13 104 T 226

14 102 00

15 100 00 16

099 00 225

17 100 00 229

i 18 103 00 118 113 69 3 4 008 229

19 102 T 733 230

20 101 00 229

I 21 095 00

122 096 00

23 099 00 232

24 098 00 234 i

25 099 00 131 199 69 6 11 01 233

26 035 T lt10 236

27 042 00 235

28 087 00

29 093 T

30 061 T 26

31 100 T 247

[Total 2982

iAVQ 096 t04 176 4 7 0CJ8 44 375 187 230 58 244 N()

Min 035 67 Max 166 00 89

lA8ORATORY TEST REQUIRED FOR wACTIVATED SlUDGEwPROCESSES

Aeration Baaln ()Ditch Etc

~ Sludge0 MIXED UQUOR Outside I A 00 -MLSS Settlbullbullbllity

Temp - Ambient 3 Disposal30 min E 30mtnW Temperature

CDT East East r E mgII mgII ml ml c OF bull Galions LbsDry Wt 1 88 C 915

2 31 1625 200 200 227 77 C 800

3 18 1322 200 200 229 76 PC 800

4 22 200 200 227 78 C 815

5 30 1678 200 200 222 77 C 800

6 31 1381 200 200 229 75 C 800

7 77 C 715

8 79 C 800

9 10 1850 200 200 229 77 PC 800

10 40 2215 200 229 76 PC 800

11 14 2132 220 226 75 C 800

12 40 2116 220 223 77 C 800

13 27 1935 220 225 73 PC 800

14 80 C 900

15 80 PC 900

16 27 2287 210 226 77 PC 800

11 26 1880 200 226 75 C 800

18 23 1679 180 226 78 C 800

19 26 1515 200 227 72 PC 800

20 27 1163 160 228 71 C 800

21 91 C 1230

22 89 C 845

23 23 1461 150 231 80 C 800

24 25 1412 200 231 78 800 21000 332f

25 29 1413 180 232 77 C 800 24000 4003

26 28 1395 150 234 91 PC 930

27 23 1451 150 240 75 C 800

28 63 C 730

29 79 C 800

30 10 1550 150 231 78 PC 800 15000 2127

31 18 1451 180 100 234 78 PC 800 27000 6305 COMMENTS ~ nICI ncrbull - IVII ICIU 1e5Ui lur I UUlI -IV U~ I VICII _ ILUI1 v ClIIU UI 6shy

GGA results were 1585 mglL on 7312 GGA results were 1339 mglL on 71112

GGA results were 852 on 718112 GGA results were 1433 mglL on 72512

7ull~4i( TlnE DATE

8312PLANT SUPERVISOR Ai 1ampllo~ TITlE DATE tishy LOCAL MANAGER

In tbe weather column use tbe follOWing symbols R-nun S-snow C-clear PC-partly doudy ()overcast

-Required Daily Required llweek

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

G MISSOURI OEPARTMENT OF NATURAL RESOURCES - WATER PROTECTION PROGRAM

~ ~ MONTHLY COMPLIANCE MONITORING REPORT FOR GROUNDWATER SYSTEMS

PJ8l1C WATpoundR SYSYEM IWoIf IPUIIlIC WAllR 1)1gt1110110 NVMIA jCOUHPICity of Nevada Me 5010562 Vernon

Mtnlmum Residual __ z Minim Residual _ Minimum Re5idual

4-Ioa SatnoIe locabon 4-109 Sm~LocatIOn 4-1Og Sample Location MonthI pH Tamp LowestF pH Temp LOWHtFre pH Temp lowMtF V degc Chlonne (mgll) degc Chlorine (mgl1)

I~middotmiddotmiddot--middotmiddot degc ChlorlM (mgll)

2~---664 211 23 fmiddot-- shy ---shy -shy-- shy877 21 Lo 23

--~-- ----- shy3 888 208 23 4 892 20A 23 5 890 212 23

6 88]_ I- 211 __ 22

1- 7 22 8_~ 215 ----- -----~-

--___ ------ shy----- shy f----_ k___ ~middot__ shy - ~

8 896 208 18-9 893 211 21

10 888 213 19

[11_ 885 _21Q_ 22 --rmiddot----middot shy ----~-~-~

h~- 894 206 19 13 911 215 21

14 883 210 20 I 15 884 211 23 I

16 880 212 21

~ 887 212 22 18 877 208 21

t-19 897 ~1 19~-----------shy120 902 206 ~ 1 7

r -- shy -- ---shy -~-----i---- _- shy - t--middot i 21 ~JL12 208 19_h----shy _-- shy ~--------

22 892 215 20 i 23 888 211 21 i 24 878 210 22 -125 892 211 22 i 26 806 O8 21 j2j ~--~ shy

906 208 21 t

I~8 864 214 19

I E4129 893 211 25 f3tf 914 212 19 -i 31 898 213 21 II Was the diSinfectant t9sidual ever less than the Slate reqUIred level for 4-109 InactIvation 01 viruses at thiS enlry POintIOYn III No _ If 0 old the wa1er system collect grab samples every four hours until the d-ls--lnfe--cta---n7t-re-s~id-u--alw-a-s--a--bo-ve~lhe--S~--ale required level

I 0 Va ~ No Ifm enswet yes to this question attach the resuU~~- theELsarl)II~19thslrn~L ___ i (For IyqmS serving more than 33(0) Old continuous monitOring equipment fail at any time during this reportll1g penoo

1I DYII2I No (For systems serving I1lQ(6 than 3300) If monitoring equipment taded were grab samples collected every 4 hours until the I conllnuous monitonng equipment was returned to SftlV1Ce gJ~Jttach itab sample results to this form)

RSON 1Ii5A ~ _----__---------1 -I

I 61 PAJIili2

1-751-=~ry~+HhltIo=iPflIlll_-_----__---- --==Tomiddot~-i~-middot~ (9 t~-_-~-l Jose h Ti

Laboratory Log-In and Chlorine Report form

(Julv 2012)

Sample ID Date I Time Received Received

Initals Supply 10 Date

Taken

middot~ (

- -) I

30 l Y 11 I I I

f it Il

15 I j

SJ (( 1 (

7 J 2

1 I r

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I i 112

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Jpound I dH1lshy

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- ( I 1 (i I

12 ( I r I Ci r t)

- I( ( (

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I

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rl Ie I

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I

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c r~ -~ I Lc ~ ~~ ~I Irl (

eer

tr

c- (

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rr shy

7

if

ICc ( I IT

cclflf (SOC lAP

2~ I-J)( fI

ICc 1-

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Ie cc If

5 (lt4shy shy

i ( ~(- ~

--s[(r)c

ltv[ S lt

i 1 I ~

1 Ie I leiIt

7kI( I

jCr laquo I i 12 - J ~ C

r Clc) )fl 7170 fc IC- J51 (7) 11shy

Ie 16Yi1jfitz 5lpoundJ~2 (]2 SlICSeuro I I-~ 3hL~

7 5(ltlt I I 1j~

11 iLI u-sL ~ I )V 2

Time Taken

Location Chlorine

Free I Total

Collectors Initials

~( Slt-i j ( of -(

L h fl- (ISshy

~- I i J -~ 7 )l J Iv IG I J 11lt

tlf bull ( I r iI r l f~ ~-_I h ff-I~middot C~

lr t r --) - ~ 1 ~Lt Icph L1 fl 117

I

i kT 1- if ipoundI t Ni IV(J_ h 1

~ I I I 1shy

c)~ I I ~ 1-) i L ii I I ) l lrr NCA r-r L l L

C (t

~ -shy

1 I bull1

tl~

ltj 0 I h1 (~

I II fi h~jT

L ( IAII

c 7( 1(1p

lt 1 I ~lrf t t i I I J L -shy c

( -7 I ( Z-J II)J

( Jt ( i--rgt- (shy i ----~-f ~i~ II Jmiddotf pound

t ( ~r ~ J J LI I (~ J~ c

[ i ltj- 7

bull ~l j t- L I Jshy if I f IJ 1

Yc- L ~ _ ~-- r i )- C i ) J t ff r~ ( 7

13 l 4~g pound Wlj)Oh Ishy shy

J )4 qoq tv 11h ---shycSl pound+ 1 ramp X Yk exuIrl ( ( ltl-

I

L ~- 3c( I Ci-(~(L I 2J

( -) -ltII j tUjshy J

( J c)~_ lL 1+ 11 I

( ff 1-1- 71 shy (

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)(

Remarks

- - -

Laboratory Log-In and Chlorine Report form

Sample 10 Date Time

Initals Supply 10Received Received

1 ~( J -)2shy ICCmiddot( 7f -I(~12

)gt 1amp 7l~( h 110 ~ M~ ))1 ~)~S

l~ G- L -d tshy II ~o5 Ct~ 02J5

_----shy _ _shy

Date Taken

Time location

Taken

7f J1Z escSshy laquo7 IS j illt- ~s middot r)

1-1 ~ d10S S~o H1t+t t S r bleAt I If I ) ifl)S 110 ~Ymiddottt b~Xt

shy __shy _

Chlorine Collectors Remarks

Free Total Initials

1Z Z nrF

- 1J1 f - 51 if

Missouri Dcpartmcnt Of latural Resources Public Drinkine Water Program

PO 80x 176 kfrcrson (it~ to 65102 (573)751-5331

Public Vater System Bacteriological Report

S ~aml NEVADA PWS If) M050 I 05tl2

Mail 10 JOSEPH TIPPER

1300 W CHERRY County VERNON

NEVADA MO 64772 Plcase n(llll~ u- (I IllY name and addres lhangls

Sample TypeIgtal( (lIlhrhd ColIlCtor

ROlltine07092012 MF lab RtSuitl Io~ation Nanl( Location II)Lab SamplE m

NEVADA~ A120 SASH

Coliform IIhent Sample considtred safe

26566

Sample T~I)( Dau Colletmiddotted ColleClor

Routine070912012 MF Iah Rtmiddot ults Ioration alUr loCalioll II)Lab SampltlO

71 HWY N NEVADA4 A

Coliform absent Samplt (onsidCndsaft

265M

Sample T~pt nail Coller led Collerl()r

Routine07092012 MF

Lab Sampl( m Location janie Lmalioll Ill Iah RIiull

50 I S JEFFERSON NEVADA5 A

(ouror absent Sample considered safe

26565

~

Santl)- Typt COIltllIr

07092012 MF Routine

Lab SlImpie III 1lnalion SlUt Iocalion IIgt Iah RlSUItS

41 I S WESl NEVADA2 A26563

Note to public water systems If you take a routine sample from a well rather than your distrIbution system a violation may be Issued by Missouri Public Drinking Water Branch

i-ridul July Il 101

Q -_

lissouri Department Of Natural Resources i_~~ Public Drinking Water ProJram

PO Box 176 Jefferson Cit) I0 65102 (573)751-5331

Public Water System Bacteriological Report

NEVADA PS I) M05010562rws 1I111t

JOSEPI TIPPER lail to Counl) VERNON 1300 W CHERRY

NEVADA MO 64772 Plcmc Il(llify us Ill any name and addrcs challgl

Samllil TYPl I)lltl (ullechd Collector

Routine07 )9 W12 MF Iab Relulll Lab SlImpll III LOC8110n Iianl Location II)

26567 1300 W CHERRY NEVADAI A

(oliform absent Samplf fonsidered safe ~~ t4_-mc-W ~

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

middotridIJYbullbullIul 13 101

IWS alllt

laillo

i~sotJri Dep_urment Of turall~((lurn Iuhlir flrinldlll WU(r lrIIJraOl

VO Rn 171 Jcff(middotrion (it 10 hS 1112

NIVAI)

JOSEPU TIPPER

I 30n W CH ERR Y NI ADA MO (-4112

Ihue (ollltld

lPOI)

LlIh Slimple 11)

2Q342

1)11 ( IIlied ttl

07 B2012

Lllh ~IUIIJlh In

nle (nllfhd

(J72J012

I Il 11 In

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~II

11 11 Y l

Ml

( IIIIII~ VERNON

111 IhlIl~ U 111111

I)IIIW HId dfmiddot dlIII11l

1(1(31 ion II) Inh ~(lh

R()UlllC

LmlIliulI II)

I m11 intI I D

llllpk I ~ lit

Imiddotcutlll~middot

I all 1UII

Note to public water systems If you lake a routine sample from a well rather than your distribution system a violation may be issued by Missouri Public Drinking Waler Branch

IriJIII)-

shyI~-~f r -----1

I

4 (D Iissouri Illpartmcnl Of atunlJ icsOUrltCli L ~_ __ _ uhlie UrinkinJ Wllu Irolram

PO Bo 17h hfhrwll Ci~ 1O h~ 1tI

Jmiddotuhlic ate S~slcm Bll(tlrioloJical I~cporl

NFADA II) ~H raquo)(J IOh

ailltl JOSEI)II lWPLR

I ~oo CHERRY (Hunl VERNON

NlADA MO hmiddotP Pill IlOlin li 11 HI

II lIll ltllld 1hlr t L hIII~

l1Ipk T~ p I)alt (nlll(tli ( nlhctur

Rwin0 3 201 MF

Ioealillll II) I all 1(11 Ill SlImpl III

411 ~ WIS I

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

I riduy III1 - III

MI~~OUftl DePARTMENT OF NATURAL RESOURCES DIVISION OF ENVIRONMENTAL QUALITY

Discharge Monitoring Report For Municipal Wastewater Treatment Plants

N- OF FACILITY lOCA11UN iampCrTY ~ _shyNvada 1IItit WIItIIf rnt 117 s 1338 ROid NevIIda VERNONISOUTHWEST

IIR-r OUTFALL NUllBER TYPI ACLTY

IIIIyl2012 M0-00891 09 001 OXIDATION OtTCH INFLUENT FFFI JFIIIT

rNCiI -rAlp E OtL DATE FLOW BOD TSS u~s BOD TSS TEMP DO

IIIGO mall mall mall mall mall mall CFUllOOMl C mQt1 mQt1 mgI

1 067 00

2 O~9 00 226

I 3 089 00 122 118 67 3 7 005 228

4 091 00 227

5 096 00 44 375 lt10 200 58 2440 NO

6 100 00 228

7 099 00

8 098 00

9 166 00 231

10 139 00 229

11 095 00 44 275 61 4 5 007 227

12 099 00 lt10 229

13 104 T 226

14 102 00

15 100 00 16

099 00 225

17 100 00 229

i 18 103 00 118 113 69 3 4 008 229

19 102 T 733 230

20 101 00 229

I 21 095 00

122 096 00

23 099 00 232

24 098 00 234 i

25 099 00 131 199 69 6 11 01 233

26 035 T lt10 236

27 042 00 235

28 087 00

29 093 T

30 061 T 26

31 100 T 247

[Total 2982

iAVQ 096 t04 176 4 7 0CJ8 44 375 187 230 58 244 N()

Min 035 67 Max 166 00 89

lA8ORATORY TEST REQUIRED FOR wACTIVATED SlUDGEwPROCESSES

Aeration Baaln ()Ditch Etc

~ Sludge0 MIXED UQUOR Outside I A 00 -MLSS Settlbullbullbllity

Temp - Ambient 3 Disposal30 min E 30mtnW Temperature

CDT East East r E mgII mgII ml ml c OF bull Galions LbsDry Wt 1 88 C 915

2 31 1625 200 200 227 77 C 800

3 18 1322 200 200 229 76 PC 800

4 22 200 200 227 78 C 815

5 30 1678 200 200 222 77 C 800

6 31 1381 200 200 229 75 C 800

7 77 C 715

8 79 C 800

9 10 1850 200 200 229 77 PC 800

10 40 2215 200 229 76 PC 800

11 14 2132 220 226 75 C 800

12 40 2116 220 223 77 C 800

13 27 1935 220 225 73 PC 800

14 80 C 900

15 80 PC 900

16 27 2287 210 226 77 PC 800

11 26 1880 200 226 75 C 800

18 23 1679 180 226 78 C 800

19 26 1515 200 227 72 PC 800

20 27 1163 160 228 71 C 800

21 91 C 1230

22 89 C 845

23 23 1461 150 231 80 C 800

24 25 1412 200 231 78 800 21000 332f

25 29 1413 180 232 77 C 800 24000 4003

26 28 1395 150 234 91 PC 930

27 23 1451 150 240 75 C 800

28 63 C 730

29 79 C 800

30 10 1550 150 231 78 PC 800 15000 2127

31 18 1451 180 100 234 78 PC 800 27000 6305 COMMENTS ~ nICI ncrbull - IVII ICIU 1e5Ui lur I UUlI -IV U~ I VICII _ ILUI1 v ClIIU UI 6shy

GGA results were 1585 mglL on 7312 GGA results were 1339 mglL on 71112

GGA results were 852 on 718112 GGA results were 1433 mglL on 72512

7ull~4i( TlnE DATE

8312PLANT SUPERVISOR Ai 1ampllo~ TITlE DATE tishy LOCAL MANAGER

In tbe weather column use tbe follOWing symbols R-nun S-snow C-clear PC-partly doudy ()overcast

-Required Daily Required llweek

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

Laboratory Log-In and Chlorine Report form

(Julv 2012)

Sample ID Date I Time Received Received

Initals Supply 10 Date

Taken

middot~ (

- -) I

30 l Y 11 I I I

f it Il

15 I j

SJ (( 1 (

7 J 2

1 I r

~~~ I~

Jc (

II V

I j J

3lt I

b ampf Lf S 7btC

j)3

3rltl-7

72lc (

17-IP

J ) (

l I

lt12

gtI L

) I

111shy

II ~lt II _

r7

7lt II

fI I ~

I i 112

J i 1 (2

71i71fl I

71711 Irl12

Jpound I dH1lshy

Y)~2 b12 1) ~J L

rIshy il~ ~ 1dlj

I~ It III IllL lt I 711

- ( I 1 (i I

12 ( I r I Ci r t)

- I( ( (

~t( (~ It f( C i

I

II I f ~

rl Ie I

I r L

I

lt l f (

0ilt 2

c r~ -~ I Lc ~ ~~ ~I Irl (

eer

tr

c- (

(I t

rr shy

7

if

ICc ( I IT

cclflf (SOC lAP

2~ I-J)( fI

ICc 1-

Ieee I rr

(c I ~h

Ie cc If

5 (lt4shy shy

i ( ~(- ~

--s[(r)c

ltv[ S lt

i 1 I ~

1 Ie I leiIt

7kI( I

jCr laquo I i 12 - J ~ C

r Clc) )fl 7170 fc IC- J51 (7) 11shy

Ie 16Yi1jfitz 5lpoundJ~2 (]2 SlICSeuro I I-~ 3hL~

7 5(ltlt I I 1j~

11 iLI u-sL ~ I )V 2

Time Taken

Location Chlorine

Free I Total

Collectors Initials

~( Slt-i j ( of -(

L h fl- (ISshy

~- I i J -~ 7 )l J Iv IG I J 11lt

tlf bull ( I r iI r l f~ ~-_I h ff-I~middot C~

lr t r --) - ~ 1 ~Lt Icph L1 fl 117

I

i kT 1- if ipoundI t Ni IV(J_ h 1

~ I I I 1shy

c)~ I I ~ 1-) i L ii I I ) l lrr NCA r-r L l L

C (t

~ -shy

1 I bull1

tl~

ltj 0 I h1 (~

I II fi h~jT

L ( IAII

c 7( 1(1p

lt 1 I ~lrf t t i I I J L -shy c

( -7 I ( Z-J II)J

( Jt ( i--rgt- (shy i ----~-f ~i~ II Jmiddotf pound

t ( ~r ~ J J LI I (~ J~ c

[ i ltj- 7

bull ~l j t- L I Jshy if I f IJ 1

Yc- L ~ _ ~-- r i )- C i ) J t ff r~ ( 7

13 l 4~g pound Wlj)Oh Ishy shy

J )4 qoq tv 11h ---shycSl pound+ 1 ramp X Yk exuIrl ( ( ltl-

I

L ~- 3c( I Ci-(~(L I 2J

( -) -ltII j tUjshy J

( J c)~_ lL 1+ 11 I

( ff 1-1- 71 shy (

7 sshy

(

-

~

9 i

)0

ccsshy

2 ~ -

2(

r-

I C

f rshy

Ir

Ji

()tr

- poundI

fl 0

II (f~

tu

rnF

)(

Remarks

- - -

Laboratory Log-In and Chlorine Report form

Sample 10 Date Time

Initals Supply 10Received Received

1 ~( J -)2shy ICCmiddot( 7f -I(~12

)gt 1amp 7l~( h 110 ~ M~ ))1 ~)~S

l~ G- L -d tshy II ~o5 Ct~ 02J5

_----shy _ _shy

Date Taken

Time location

Taken

7f J1Z escSshy laquo7 IS j illt- ~s middot r)

1-1 ~ d10S S~o H1t+t t S r bleAt I If I ) ifl)S 110 ~Ymiddottt b~Xt

shy __shy _

Chlorine Collectors Remarks

Free Total Initials

1Z Z nrF

- 1J1 f - 51 if

Missouri Dcpartmcnt Of latural Resources Public Drinkine Water Program

PO 80x 176 kfrcrson (it~ to 65102 (573)751-5331

Public Vater System Bacteriological Report

S ~aml NEVADA PWS If) M050 I 05tl2

Mail 10 JOSEPH TIPPER

1300 W CHERRY County VERNON

NEVADA MO 64772 Plcase n(llll~ u- (I IllY name and addres lhangls

Sample TypeIgtal( (lIlhrhd ColIlCtor

ROlltine07092012 MF lab RtSuitl Io~ation Nanl( Location II)Lab SamplE m

NEVADA~ A120 SASH

Coliform IIhent Sample considtred safe

26566

Sample T~I)( Dau Colletmiddotted ColleClor

Routine070912012 MF Iah Rtmiddot ults Ioration alUr loCalioll II)Lab SampltlO

71 HWY N NEVADA4 A

Coliform absent Samplt (onsidCndsaft

265M

Sample T~pt nail Coller led Collerl()r

Routine07092012 MF

Lab Sampl( m Location janie Lmalioll Ill Iah RIiull

50 I S JEFFERSON NEVADA5 A

(ouror absent Sample considered safe

26565

~

Santl)- Typt COIltllIr

07092012 MF Routine

Lab SlImpie III 1lnalion SlUt Iocalion IIgt Iah RlSUItS

41 I S WESl NEVADA2 A26563

Note to public water systems If you take a routine sample from a well rather than your distrIbution system a violation may be Issued by Missouri Public Drinking Water Branch

i-ridul July Il 101

Q -_

lissouri Department Of Natural Resources i_~~ Public Drinking Water ProJram

PO Box 176 Jefferson Cit) I0 65102 (573)751-5331

Public Water System Bacteriological Report

NEVADA PS I) M05010562rws 1I111t

JOSEPI TIPPER lail to Counl) VERNON 1300 W CHERRY

NEVADA MO 64772 Plcmc Il(llify us Ill any name and addrcs challgl

Samllil TYPl I)lltl (ullechd Collector

Routine07 )9 W12 MF Iab Relulll Lab SlImpll III LOC8110n Iianl Location II)

26567 1300 W CHERRY NEVADAI A

(oliform absent Samplf fonsidered safe ~~ t4_-mc-W ~

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

middotridIJYbullbullIul 13 101

IWS alllt

laillo

i~sotJri Dep_urment Of turall~((lurn Iuhlir flrinldlll WU(r lrIIJraOl

VO Rn 171 Jcff(middotrion (it 10 hS 1112

NIVAI)

JOSEPU TIPPER

I 30n W CH ERR Y NI ADA MO (-4112

Ihue (ollltld

lPOI)

LlIh Slimple 11)

2Q342

1)11 ( IIlied ttl

07 B2012

Lllh ~IUIIJlh In

nle (nllfhd

(J72J012

I Il 11 In

I h SlIupll I()

II

UOO W ClIIRRY

11

LW S ASII

( lIl(middottor

~II

11 11 Y l

Ml

( IIIIII~ VERNON

111 IhlIl~ U 111111

I)IIIW HId dfmiddot dlIII11l

1(1(31 ion II) Inh ~(lh

R()UlllC

LmlIliulI II)

I m11 intI I D

llllpk I ~ lit

Imiddotcutlll~middot

I all 1UII

Note to public water systems If you lake a routine sample from a well rather than your distribution system a violation may be issued by Missouri Public Drinking Waler Branch

IriJIII)-

shyI~-~f r -----1

I

4 (D Iissouri Illpartmcnl Of atunlJ icsOUrltCli L ~_ __ _ uhlie UrinkinJ Wllu Irolram

PO Bo 17h hfhrwll Ci~ 1O h~ 1tI

Jmiddotuhlic ate S~slcm Bll(tlrioloJical I~cporl

NFADA II) ~H raquo)(J IOh

ailltl JOSEI)II lWPLR

I ~oo CHERRY (Hunl VERNON

NlADA MO hmiddotP Pill IlOlin li 11 HI

II lIll ltllld 1hlr t L hIII~

l1Ipk T~ p I)alt (nlll(tli ( nlhctur

Rwin0 3 201 MF

Ioealillll II) I all 1(11 Ill SlImpl III

411 ~ WIS I

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

I riduy III1 - III

MI~~OUftl DePARTMENT OF NATURAL RESOURCES DIVISION OF ENVIRONMENTAL QUALITY

Discharge Monitoring Report For Municipal Wastewater Treatment Plants

N- OF FACILITY lOCA11UN iampCrTY ~ _shyNvada 1IItit WIItIIf rnt 117 s 1338 ROid NevIIda VERNONISOUTHWEST

IIR-r OUTFALL NUllBER TYPI ACLTY

IIIIyl2012 M0-00891 09 001 OXIDATION OtTCH INFLUENT FFFI JFIIIT

rNCiI -rAlp E OtL DATE FLOW BOD TSS u~s BOD TSS TEMP DO

IIIGO mall mall mall mall mall mall CFUllOOMl C mQt1 mQt1 mgI

1 067 00

2 O~9 00 226

I 3 089 00 122 118 67 3 7 005 228

4 091 00 227

5 096 00 44 375 lt10 200 58 2440 NO

6 100 00 228

7 099 00

8 098 00

9 166 00 231

10 139 00 229

11 095 00 44 275 61 4 5 007 227

12 099 00 lt10 229

13 104 T 226

14 102 00

15 100 00 16

099 00 225

17 100 00 229

i 18 103 00 118 113 69 3 4 008 229

19 102 T 733 230

20 101 00 229

I 21 095 00

122 096 00

23 099 00 232

24 098 00 234 i

25 099 00 131 199 69 6 11 01 233

26 035 T lt10 236

27 042 00 235

28 087 00

29 093 T

30 061 T 26

31 100 T 247

[Total 2982

iAVQ 096 t04 176 4 7 0CJ8 44 375 187 230 58 244 N()

Min 035 67 Max 166 00 89

lA8ORATORY TEST REQUIRED FOR wACTIVATED SlUDGEwPROCESSES

Aeration Baaln ()Ditch Etc

~ Sludge0 MIXED UQUOR Outside I A 00 -MLSS Settlbullbullbllity

Temp - Ambient 3 Disposal30 min E 30mtnW Temperature

CDT East East r E mgII mgII ml ml c OF bull Galions LbsDry Wt 1 88 C 915

2 31 1625 200 200 227 77 C 800

3 18 1322 200 200 229 76 PC 800

4 22 200 200 227 78 C 815

5 30 1678 200 200 222 77 C 800

6 31 1381 200 200 229 75 C 800

7 77 C 715

8 79 C 800

9 10 1850 200 200 229 77 PC 800

10 40 2215 200 229 76 PC 800

11 14 2132 220 226 75 C 800

12 40 2116 220 223 77 C 800

13 27 1935 220 225 73 PC 800

14 80 C 900

15 80 PC 900

16 27 2287 210 226 77 PC 800

11 26 1880 200 226 75 C 800

18 23 1679 180 226 78 C 800

19 26 1515 200 227 72 PC 800

20 27 1163 160 228 71 C 800

21 91 C 1230

22 89 C 845

23 23 1461 150 231 80 C 800

24 25 1412 200 231 78 800 21000 332f

25 29 1413 180 232 77 C 800 24000 4003

26 28 1395 150 234 91 PC 930

27 23 1451 150 240 75 C 800

28 63 C 730

29 79 C 800

30 10 1550 150 231 78 PC 800 15000 2127

31 18 1451 180 100 234 78 PC 800 27000 6305 COMMENTS ~ nICI ncrbull - IVII ICIU 1e5Ui lur I UUlI -IV U~ I VICII _ ILUI1 v ClIIU UI 6shy

GGA results were 1585 mglL on 7312 GGA results were 1339 mglL on 71112

GGA results were 852 on 718112 GGA results were 1433 mglL on 72512

7ull~4i( TlnE DATE

8312PLANT SUPERVISOR Ai 1ampllo~ TITlE DATE tishy LOCAL MANAGER

In tbe weather column use tbe follOWing symbols R-nun S-snow C-clear PC-partly doudy ()overcast

-Required Daily Required llweek

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

- - -

Laboratory Log-In and Chlorine Report form

Sample 10 Date Time

Initals Supply 10Received Received

1 ~( J -)2shy ICCmiddot( 7f -I(~12

)gt 1amp 7l~( h 110 ~ M~ ))1 ~)~S

l~ G- L -d tshy II ~o5 Ct~ 02J5

_----shy _ _shy

Date Taken

Time location

Taken

7f J1Z escSshy laquo7 IS j illt- ~s middot r)

1-1 ~ d10S S~o H1t+t t S r bleAt I If I ) ifl)S 110 ~Ymiddottt b~Xt

shy __shy _

Chlorine Collectors Remarks

Free Total Initials

1Z Z nrF

- 1J1 f - 51 if

Missouri Dcpartmcnt Of latural Resources Public Drinkine Water Program

PO 80x 176 kfrcrson (it~ to 65102 (573)751-5331

Public Vater System Bacteriological Report

S ~aml NEVADA PWS If) M050 I 05tl2

Mail 10 JOSEPH TIPPER

1300 W CHERRY County VERNON

NEVADA MO 64772 Plcase n(llll~ u- (I IllY name and addres lhangls

Sample TypeIgtal( (lIlhrhd ColIlCtor

ROlltine07092012 MF lab RtSuitl Io~ation Nanl( Location II)Lab SamplE m

NEVADA~ A120 SASH

Coliform IIhent Sample considtred safe

26566

Sample T~I)( Dau Colletmiddotted ColleClor

Routine070912012 MF Iah Rtmiddot ults Ioration alUr loCalioll II)Lab SampltlO

71 HWY N NEVADA4 A

Coliform absent Samplt (onsidCndsaft

265M

Sample T~pt nail Coller led Collerl()r

Routine07092012 MF

Lab Sampl( m Location janie Lmalioll Ill Iah RIiull

50 I S JEFFERSON NEVADA5 A

(ouror absent Sample considered safe

26565

~

Santl)- Typt COIltllIr

07092012 MF Routine

Lab SlImpie III 1lnalion SlUt Iocalion IIgt Iah RlSUItS

41 I S WESl NEVADA2 A26563

Note to public water systems If you take a routine sample from a well rather than your distrIbution system a violation may be Issued by Missouri Public Drinking Water Branch

i-ridul July Il 101

Q -_

lissouri Department Of Natural Resources i_~~ Public Drinking Water ProJram

PO Box 176 Jefferson Cit) I0 65102 (573)751-5331

Public Water System Bacteriological Report

NEVADA PS I) M05010562rws 1I111t

JOSEPI TIPPER lail to Counl) VERNON 1300 W CHERRY

NEVADA MO 64772 Plcmc Il(llify us Ill any name and addrcs challgl

Samllil TYPl I)lltl (ullechd Collector

Routine07 )9 W12 MF Iab Relulll Lab SlImpll III LOC8110n Iianl Location II)

26567 1300 W CHERRY NEVADAI A

(oliform absent Samplf fonsidered safe ~~ t4_-mc-W ~

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

middotridIJYbullbullIul 13 101

IWS alllt

laillo

i~sotJri Dep_urment Of turall~((lurn Iuhlir flrinldlll WU(r lrIIJraOl

VO Rn 171 Jcff(middotrion (it 10 hS 1112

NIVAI)

JOSEPU TIPPER

I 30n W CH ERR Y NI ADA MO (-4112

Ihue (ollltld

lPOI)

LlIh Slimple 11)

2Q342

1)11 ( IIlied ttl

07 B2012

Lllh ~IUIIJlh In

nle (nllfhd

(J72J012

I Il 11 In

I h SlIupll I()

II

UOO W ClIIRRY

11

LW S ASII

( lIl(middottor

~II

11 11 Y l

Ml

( IIIIII~ VERNON

111 IhlIl~ U 111111

I)IIIW HId dfmiddot dlIII11l

1(1(31 ion II) Inh ~(lh

R()UlllC

LmlIliulI II)

I m11 intI I D

llllpk I ~ lit

Imiddotcutlll~middot

I all 1UII

Note to public water systems If you lake a routine sample from a well rather than your distribution system a violation may be issued by Missouri Public Drinking Waler Branch

IriJIII)-

shyI~-~f r -----1

I

4 (D Iissouri Illpartmcnl Of atunlJ icsOUrltCli L ~_ __ _ uhlie UrinkinJ Wllu Irolram

PO Bo 17h hfhrwll Ci~ 1O h~ 1tI

Jmiddotuhlic ate S~slcm Bll(tlrioloJical I~cporl

NFADA II) ~H raquo)(J IOh

ailltl JOSEI)II lWPLR

I ~oo CHERRY (Hunl VERNON

NlADA MO hmiddotP Pill IlOlin li 11 HI

II lIll ltllld 1hlr t L hIII~

l1Ipk T~ p I)alt (nlll(tli ( nlhctur

Rwin0 3 201 MF

Ioealillll II) I all 1(11 Ill SlImpl III

411 ~ WIS I

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

I riduy III1 - III

MI~~OUftl DePARTMENT OF NATURAL RESOURCES DIVISION OF ENVIRONMENTAL QUALITY

Discharge Monitoring Report For Municipal Wastewater Treatment Plants

N- OF FACILITY lOCA11UN iampCrTY ~ _shyNvada 1IItit WIItIIf rnt 117 s 1338 ROid NevIIda VERNONISOUTHWEST

IIR-r OUTFALL NUllBER TYPI ACLTY

IIIIyl2012 M0-00891 09 001 OXIDATION OtTCH INFLUENT FFFI JFIIIT

rNCiI -rAlp E OtL DATE FLOW BOD TSS u~s BOD TSS TEMP DO

IIIGO mall mall mall mall mall mall CFUllOOMl C mQt1 mQt1 mgI

1 067 00

2 O~9 00 226

I 3 089 00 122 118 67 3 7 005 228

4 091 00 227

5 096 00 44 375 lt10 200 58 2440 NO

6 100 00 228

7 099 00

8 098 00

9 166 00 231

10 139 00 229

11 095 00 44 275 61 4 5 007 227

12 099 00 lt10 229

13 104 T 226

14 102 00

15 100 00 16

099 00 225

17 100 00 229

i 18 103 00 118 113 69 3 4 008 229

19 102 T 733 230

20 101 00 229

I 21 095 00

122 096 00

23 099 00 232

24 098 00 234 i

25 099 00 131 199 69 6 11 01 233

26 035 T lt10 236

27 042 00 235

28 087 00

29 093 T

30 061 T 26

31 100 T 247

[Total 2982

iAVQ 096 t04 176 4 7 0CJ8 44 375 187 230 58 244 N()

Min 035 67 Max 166 00 89

lA8ORATORY TEST REQUIRED FOR wACTIVATED SlUDGEwPROCESSES

Aeration Baaln ()Ditch Etc

~ Sludge0 MIXED UQUOR Outside I A 00 -MLSS Settlbullbullbllity

Temp - Ambient 3 Disposal30 min E 30mtnW Temperature

CDT East East r E mgII mgII ml ml c OF bull Galions LbsDry Wt 1 88 C 915

2 31 1625 200 200 227 77 C 800

3 18 1322 200 200 229 76 PC 800

4 22 200 200 227 78 C 815

5 30 1678 200 200 222 77 C 800

6 31 1381 200 200 229 75 C 800

7 77 C 715

8 79 C 800

9 10 1850 200 200 229 77 PC 800

10 40 2215 200 229 76 PC 800

11 14 2132 220 226 75 C 800

12 40 2116 220 223 77 C 800

13 27 1935 220 225 73 PC 800

14 80 C 900

15 80 PC 900

16 27 2287 210 226 77 PC 800

11 26 1880 200 226 75 C 800

18 23 1679 180 226 78 C 800

19 26 1515 200 227 72 PC 800

20 27 1163 160 228 71 C 800

21 91 C 1230

22 89 C 845

23 23 1461 150 231 80 C 800

24 25 1412 200 231 78 800 21000 332f

25 29 1413 180 232 77 C 800 24000 4003

26 28 1395 150 234 91 PC 930

27 23 1451 150 240 75 C 800

28 63 C 730

29 79 C 800

30 10 1550 150 231 78 PC 800 15000 2127

31 18 1451 180 100 234 78 PC 800 27000 6305 COMMENTS ~ nICI ncrbull - IVII ICIU 1e5Ui lur I UUlI -IV U~ I VICII _ ILUI1 v ClIIU UI 6shy

GGA results were 1585 mglL on 7312 GGA results were 1339 mglL on 71112

GGA results were 852 on 718112 GGA results were 1433 mglL on 72512

7ull~4i( TlnE DATE

8312PLANT SUPERVISOR Ai 1ampllo~ TITlE DATE tishy LOCAL MANAGER

In tbe weather column use tbe follOWing symbols R-nun S-snow C-clear PC-partly doudy ()overcast

-Required Daily Required llweek

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

Missouri Dcpartmcnt Of latural Resources Public Drinkine Water Program

PO 80x 176 kfrcrson (it~ to 65102 (573)751-5331

Public Vater System Bacteriological Report

S ~aml NEVADA PWS If) M050 I 05tl2

Mail 10 JOSEPH TIPPER

1300 W CHERRY County VERNON

NEVADA MO 64772 Plcase n(llll~ u- (I IllY name and addres lhangls

Sample TypeIgtal( (lIlhrhd ColIlCtor

ROlltine07092012 MF lab RtSuitl Io~ation Nanl( Location II)Lab SamplE m

NEVADA~ A120 SASH

Coliform IIhent Sample considtred safe

26566

Sample T~I)( Dau Colletmiddotted ColleClor

Routine070912012 MF Iah Rtmiddot ults Ioration alUr loCalioll II)Lab SampltlO

71 HWY N NEVADA4 A

Coliform absent Samplt (onsidCndsaft

265M

Sample T~pt nail Coller led Collerl()r

Routine07092012 MF

Lab Sampl( m Location janie Lmalioll Ill Iah RIiull

50 I S JEFFERSON NEVADA5 A

(ouror absent Sample considered safe

26565

~

Santl)- Typt COIltllIr

07092012 MF Routine

Lab SlImpie III 1lnalion SlUt Iocalion IIgt Iah RlSUItS

41 I S WESl NEVADA2 A26563

Note to public water systems If you take a routine sample from a well rather than your distrIbution system a violation may be Issued by Missouri Public Drinking Water Branch

i-ridul July Il 101

Q -_

lissouri Department Of Natural Resources i_~~ Public Drinking Water ProJram

PO Box 176 Jefferson Cit) I0 65102 (573)751-5331

Public Water System Bacteriological Report

NEVADA PS I) M05010562rws 1I111t

JOSEPI TIPPER lail to Counl) VERNON 1300 W CHERRY

NEVADA MO 64772 Plcmc Il(llify us Ill any name and addrcs challgl

Samllil TYPl I)lltl (ullechd Collector

Routine07 )9 W12 MF Iab Relulll Lab SlImpll III LOC8110n Iianl Location II)

26567 1300 W CHERRY NEVADAI A

(oliform absent Samplf fonsidered safe ~~ t4_-mc-W ~

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

middotridIJYbullbullIul 13 101

IWS alllt

laillo

i~sotJri Dep_urment Of turall~((lurn Iuhlir flrinldlll WU(r lrIIJraOl

VO Rn 171 Jcff(middotrion (it 10 hS 1112

NIVAI)

JOSEPU TIPPER

I 30n W CH ERR Y NI ADA MO (-4112

Ihue (ollltld

lPOI)

LlIh Slimple 11)

2Q342

1)11 ( IIlied ttl

07 B2012

Lllh ~IUIIJlh In

nle (nllfhd

(J72J012

I Il 11 In

I h SlIupll I()

II

UOO W ClIIRRY

11

LW S ASII

( lIl(middottor

~II

11 11 Y l

Ml

( IIIIII~ VERNON

111 IhlIl~ U 111111

I)IIIW HId dfmiddot dlIII11l

1(1(31 ion II) Inh ~(lh

R()UlllC

LmlIliulI II)

I m11 intI I D

llllpk I ~ lit

Imiddotcutlll~middot

I all 1UII

Note to public water systems If you lake a routine sample from a well rather than your distribution system a violation may be issued by Missouri Public Drinking Waler Branch

IriJIII)-

shyI~-~f r -----1

I

4 (D Iissouri Illpartmcnl Of atunlJ icsOUrltCli L ~_ __ _ uhlie UrinkinJ Wllu Irolram

PO Bo 17h hfhrwll Ci~ 1O h~ 1tI

Jmiddotuhlic ate S~slcm Bll(tlrioloJical I~cporl

NFADA II) ~H raquo)(J IOh

ailltl JOSEI)II lWPLR

I ~oo CHERRY (Hunl VERNON

NlADA MO hmiddotP Pill IlOlin li 11 HI

II lIll ltllld 1hlr t L hIII~

l1Ipk T~ p I)alt (nlll(tli ( nlhctur

Rwin0 3 201 MF

Ioealillll II) I all 1(11 Ill SlImpl III

411 ~ WIS I

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

I riduy III1 - III

MI~~OUftl DePARTMENT OF NATURAL RESOURCES DIVISION OF ENVIRONMENTAL QUALITY

Discharge Monitoring Report For Municipal Wastewater Treatment Plants

N- OF FACILITY lOCA11UN iampCrTY ~ _shyNvada 1IItit WIItIIf rnt 117 s 1338 ROid NevIIda VERNONISOUTHWEST

IIR-r OUTFALL NUllBER TYPI ACLTY

IIIIyl2012 M0-00891 09 001 OXIDATION OtTCH INFLUENT FFFI JFIIIT

rNCiI -rAlp E OtL DATE FLOW BOD TSS u~s BOD TSS TEMP DO

IIIGO mall mall mall mall mall mall CFUllOOMl C mQt1 mQt1 mgI

1 067 00

2 O~9 00 226

I 3 089 00 122 118 67 3 7 005 228

4 091 00 227

5 096 00 44 375 lt10 200 58 2440 NO

6 100 00 228

7 099 00

8 098 00

9 166 00 231

10 139 00 229

11 095 00 44 275 61 4 5 007 227

12 099 00 lt10 229

13 104 T 226

14 102 00

15 100 00 16

099 00 225

17 100 00 229

i 18 103 00 118 113 69 3 4 008 229

19 102 T 733 230

20 101 00 229

I 21 095 00

122 096 00

23 099 00 232

24 098 00 234 i

25 099 00 131 199 69 6 11 01 233

26 035 T lt10 236

27 042 00 235

28 087 00

29 093 T

30 061 T 26

31 100 T 247

[Total 2982

iAVQ 096 t04 176 4 7 0CJ8 44 375 187 230 58 244 N()

Min 035 67 Max 166 00 89

lA8ORATORY TEST REQUIRED FOR wACTIVATED SlUDGEwPROCESSES

Aeration Baaln ()Ditch Etc

~ Sludge0 MIXED UQUOR Outside I A 00 -MLSS Settlbullbullbllity

Temp - Ambient 3 Disposal30 min E 30mtnW Temperature

CDT East East r E mgII mgII ml ml c OF bull Galions LbsDry Wt 1 88 C 915

2 31 1625 200 200 227 77 C 800

3 18 1322 200 200 229 76 PC 800

4 22 200 200 227 78 C 815

5 30 1678 200 200 222 77 C 800

6 31 1381 200 200 229 75 C 800

7 77 C 715

8 79 C 800

9 10 1850 200 200 229 77 PC 800

10 40 2215 200 229 76 PC 800

11 14 2132 220 226 75 C 800

12 40 2116 220 223 77 C 800

13 27 1935 220 225 73 PC 800

14 80 C 900

15 80 PC 900

16 27 2287 210 226 77 PC 800

11 26 1880 200 226 75 C 800

18 23 1679 180 226 78 C 800

19 26 1515 200 227 72 PC 800

20 27 1163 160 228 71 C 800

21 91 C 1230

22 89 C 845

23 23 1461 150 231 80 C 800

24 25 1412 200 231 78 800 21000 332f

25 29 1413 180 232 77 C 800 24000 4003

26 28 1395 150 234 91 PC 930

27 23 1451 150 240 75 C 800

28 63 C 730

29 79 C 800

30 10 1550 150 231 78 PC 800 15000 2127

31 18 1451 180 100 234 78 PC 800 27000 6305 COMMENTS ~ nICI ncrbull - IVII ICIU 1e5Ui lur I UUlI -IV U~ I VICII _ ILUI1 v ClIIU UI 6shy

GGA results were 1585 mglL on 7312 GGA results were 1339 mglL on 71112

GGA results were 852 on 718112 GGA results were 1433 mglL on 72512

7ull~4i( TlnE DATE

8312PLANT SUPERVISOR Ai 1ampllo~ TITlE DATE tishy LOCAL MANAGER

In tbe weather column use tbe follOWing symbols R-nun S-snow C-clear PC-partly doudy ()overcast

-Required Daily Required llweek

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

Q -_

lissouri Department Of Natural Resources i_~~ Public Drinking Water ProJram

PO Box 176 Jefferson Cit) I0 65102 (573)751-5331

Public Water System Bacteriological Report

NEVADA PS I) M05010562rws 1I111t

JOSEPI TIPPER lail to Counl) VERNON 1300 W CHERRY

NEVADA MO 64772 Plcmc Il(llify us Ill any name and addrcs challgl

Samllil TYPl I)lltl (ullechd Collector

Routine07 )9 W12 MF Iab Relulll Lab SlImpll III LOC8110n Iianl Location II)

26567 1300 W CHERRY NEVADAI A

(oliform absent Samplf fonsidered safe ~~ t4_-mc-W ~

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

middotridIJYbullbullIul 13 101

IWS alllt

laillo

i~sotJri Dep_urment Of turall~((lurn Iuhlir flrinldlll WU(r lrIIJraOl

VO Rn 171 Jcff(middotrion (it 10 hS 1112

NIVAI)

JOSEPU TIPPER

I 30n W CH ERR Y NI ADA MO (-4112

Ihue (ollltld

lPOI)

LlIh Slimple 11)

2Q342

1)11 ( IIlied ttl

07 B2012

Lllh ~IUIIJlh In

nle (nllfhd

(J72J012

I Il 11 In

I h SlIupll I()

II

UOO W ClIIRRY

11

LW S ASII

( lIl(middottor

~II

11 11 Y l

Ml

( IIIIII~ VERNON

111 IhlIl~ U 111111

I)IIIW HId dfmiddot dlIII11l

1(1(31 ion II) Inh ~(lh

R()UlllC

LmlIliulI II)

I m11 intI I D

llllpk I ~ lit

Imiddotcutlll~middot

I all 1UII

Note to public water systems If you lake a routine sample from a well rather than your distribution system a violation may be issued by Missouri Public Drinking Waler Branch

IriJIII)-

shyI~-~f r -----1

I

4 (D Iissouri Illpartmcnl Of atunlJ icsOUrltCli L ~_ __ _ uhlie UrinkinJ Wllu Irolram

PO Bo 17h hfhrwll Ci~ 1O h~ 1tI

Jmiddotuhlic ate S~slcm Bll(tlrioloJical I~cporl

NFADA II) ~H raquo)(J IOh

ailltl JOSEI)II lWPLR

I ~oo CHERRY (Hunl VERNON

NlADA MO hmiddotP Pill IlOlin li 11 HI

II lIll ltllld 1hlr t L hIII~

l1Ipk T~ p I)alt (nlll(tli ( nlhctur

Rwin0 3 201 MF

Ioealillll II) I all 1(11 Ill SlImpl III

411 ~ WIS I

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

I riduy III1 - III

MI~~OUftl DePARTMENT OF NATURAL RESOURCES DIVISION OF ENVIRONMENTAL QUALITY

Discharge Monitoring Report For Municipal Wastewater Treatment Plants

N- OF FACILITY lOCA11UN iampCrTY ~ _shyNvada 1IItit WIItIIf rnt 117 s 1338 ROid NevIIda VERNONISOUTHWEST

IIR-r OUTFALL NUllBER TYPI ACLTY

IIIIyl2012 M0-00891 09 001 OXIDATION OtTCH INFLUENT FFFI JFIIIT

rNCiI -rAlp E OtL DATE FLOW BOD TSS u~s BOD TSS TEMP DO

IIIGO mall mall mall mall mall mall CFUllOOMl C mQt1 mQt1 mgI

1 067 00

2 O~9 00 226

I 3 089 00 122 118 67 3 7 005 228

4 091 00 227

5 096 00 44 375 lt10 200 58 2440 NO

6 100 00 228

7 099 00

8 098 00

9 166 00 231

10 139 00 229

11 095 00 44 275 61 4 5 007 227

12 099 00 lt10 229

13 104 T 226

14 102 00

15 100 00 16

099 00 225

17 100 00 229

i 18 103 00 118 113 69 3 4 008 229

19 102 T 733 230

20 101 00 229

I 21 095 00

122 096 00

23 099 00 232

24 098 00 234 i

25 099 00 131 199 69 6 11 01 233

26 035 T lt10 236

27 042 00 235

28 087 00

29 093 T

30 061 T 26

31 100 T 247

[Total 2982

iAVQ 096 t04 176 4 7 0CJ8 44 375 187 230 58 244 N()

Min 035 67 Max 166 00 89

lA8ORATORY TEST REQUIRED FOR wACTIVATED SlUDGEwPROCESSES

Aeration Baaln ()Ditch Etc

~ Sludge0 MIXED UQUOR Outside I A 00 -MLSS Settlbullbullbllity

Temp - Ambient 3 Disposal30 min E 30mtnW Temperature

CDT East East r E mgII mgII ml ml c OF bull Galions LbsDry Wt 1 88 C 915

2 31 1625 200 200 227 77 C 800

3 18 1322 200 200 229 76 PC 800

4 22 200 200 227 78 C 815

5 30 1678 200 200 222 77 C 800

6 31 1381 200 200 229 75 C 800

7 77 C 715

8 79 C 800

9 10 1850 200 200 229 77 PC 800

10 40 2215 200 229 76 PC 800

11 14 2132 220 226 75 C 800

12 40 2116 220 223 77 C 800

13 27 1935 220 225 73 PC 800

14 80 C 900

15 80 PC 900

16 27 2287 210 226 77 PC 800

11 26 1880 200 226 75 C 800

18 23 1679 180 226 78 C 800

19 26 1515 200 227 72 PC 800

20 27 1163 160 228 71 C 800

21 91 C 1230

22 89 C 845

23 23 1461 150 231 80 C 800

24 25 1412 200 231 78 800 21000 332f

25 29 1413 180 232 77 C 800 24000 4003

26 28 1395 150 234 91 PC 930

27 23 1451 150 240 75 C 800

28 63 C 730

29 79 C 800

30 10 1550 150 231 78 PC 800 15000 2127

31 18 1451 180 100 234 78 PC 800 27000 6305 COMMENTS ~ nICI ncrbull - IVII ICIU 1e5Ui lur I UUlI -IV U~ I VICII _ ILUI1 v ClIIU UI 6shy

GGA results were 1585 mglL on 7312 GGA results were 1339 mglL on 71112

GGA results were 852 on 718112 GGA results were 1433 mglL on 72512

7ull~4i( TlnE DATE

8312PLANT SUPERVISOR Ai 1ampllo~ TITlE DATE tishy LOCAL MANAGER

In tbe weather column use tbe follOWing symbols R-nun S-snow C-clear PC-partly doudy ()overcast

-Required Daily Required llweek

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

IWS alllt

laillo

i~sotJri Dep_urment Of turall~((lurn Iuhlir flrinldlll WU(r lrIIJraOl

VO Rn 171 Jcff(middotrion (it 10 hS 1112

NIVAI)

JOSEPU TIPPER

I 30n W CH ERR Y NI ADA MO (-4112

Ihue (ollltld

lPOI)

LlIh Slimple 11)

2Q342

1)11 ( IIlied ttl

07 B2012

Lllh ~IUIIJlh In

nle (nllfhd

(J72J012

I Il 11 In

I h SlIupll I()

II

UOO W ClIIRRY

11

LW S ASII

( lIl(middottor

~II

11 11 Y l

Ml

( IIIIII~ VERNON

111 IhlIl~ U 111111

I)IIIW HId dfmiddot dlIII11l

1(1(31 ion II) Inh ~(lh

R()UlllC

LmlIliulI II)

I m11 intI I D

llllpk I ~ lit

Imiddotcutlll~middot

I all 1UII

Note to public water systems If you lake a routine sample from a well rather than your distribution system a violation may be issued by Missouri Public Drinking Waler Branch

IriJIII)-

shyI~-~f r -----1

I

4 (D Iissouri Illpartmcnl Of atunlJ icsOUrltCli L ~_ __ _ uhlie UrinkinJ Wllu Irolram

PO Bo 17h hfhrwll Ci~ 1O h~ 1tI

Jmiddotuhlic ate S~slcm Bll(tlrioloJical I~cporl

NFADA II) ~H raquo)(J IOh

ailltl JOSEI)II lWPLR

I ~oo CHERRY (Hunl VERNON

NlADA MO hmiddotP Pill IlOlin li 11 HI

II lIll ltllld 1hlr t L hIII~

l1Ipk T~ p I)alt (nlll(tli ( nlhctur

Rwin0 3 201 MF

Ioealillll II) I all 1(11 Ill SlImpl III

411 ~ WIS I

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

I riduy III1 - III

MI~~OUftl DePARTMENT OF NATURAL RESOURCES DIVISION OF ENVIRONMENTAL QUALITY

Discharge Monitoring Report For Municipal Wastewater Treatment Plants

N- OF FACILITY lOCA11UN iampCrTY ~ _shyNvada 1IItit WIItIIf rnt 117 s 1338 ROid NevIIda VERNONISOUTHWEST

IIR-r OUTFALL NUllBER TYPI ACLTY

IIIIyl2012 M0-00891 09 001 OXIDATION OtTCH INFLUENT FFFI JFIIIT

rNCiI -rAlp E OtL DATE FLOW BOD TSS u~s BOD TSS TEMP DO

IIIGO mall mall mall mall mall mall CFUllOOMl C mQt1 mQt1 mgI

1 067 00

2 O~9 00 226

I 3 089 00 122 118 67 3 7 005 228

4 091 00 227

5 096 00 44 375 lt10 200 58 2440 NO

6 100 00 228

7 099 00

8 098 00

9 166 00 231

10 139 00 229

11 095 00 44 275 61 4 5 007 227

12 099 00 lt10 229

13 104 T 226

14 102 00

15 100 00 16

099 00 225

17 100 00 229

i 18 103 00 118 113 69 3 4 008 229

19 102 T 733 230

20 101 00 229

I 21 095 00

122 096 00

23 099 00 232

24 098 00 234 i

25 099 00 131 199 69 6 11 01 233

26 035 T lt10 236

27 042 00 235

28 087 00

29 093 T

30 061 T 26

31 100 T 247

[Total 2982

iAVQ 096 t04 176 4 7 0CJ8 44 375 187 230 58 244 N()

Min 035 67 Max 166 00 89

lA8ORATORY TEST REQUIRED FOR wACTIVATED SlUDGEwPROCESSES

Aeration Baaln ()Ditch Etc

~ Sludge0 MIXED UQUOR Outside I A 00 -MLSS Settlbullbullbllity

Temp - Ambient 3 Disposal30 min E 30mtnW Temperature

CDT East East r E mgII mgII ml ml c OF bull Galions LbsDry Wt 1 88 C 915

2 31 1625 200 200 227 77 C 800

3 18 1322 200 200 229 76 PC 800

4 22 200 200 227 78 C 815

5 30 1678 200 200 222 77 C 800

6 31 1381 200 200 229 75 C 800

7 77 C 715

8 79 C 800

9 10 1850 200 200 229 77 PC 800

10 40 2215 200 229 76 PC 800

11 14 2132 220 226 75 C 800

12 40 2116 220 223 77 C 800

13 27 1935 220 225 73 PC 800

14 80 C 900

15 80 PC 900

16 27 2287 210 226 77 PC 800

11 26 1880 200 226 75 C 800

18 23 1679 180 226 78 C 800

19 26 1515 200 227 72 PC 800

20 27 1163 160 228 71 C 800

21 91 C 1230

22 89 C 845

23 23 1461 150 231 80 C 800

24 25 1412 200 231 78 800 21000 332f

25 29 1413 180 232 77 C 800 24000 4003

26 28 1395 150 234 91 PC 930

27 23 1451 150 240 75 C 800

28 63 C 730

29 79 C 800

30 10 1550 150 231 78 PC 800 15000 2127

31 18 1451 180 100 234 78 PC 800 27000 6305 COMMENTS ~ nICI ncrbull - IVII ICIU 1e5Ui lur I UUlI -IV U~ I VICII _ ILUI1 v ClIIU UI 6shy

GGA results were 1585 mglL on 7312 GGA results were 1339 mglL on 71112

GGA results were 852 on 718112 GGA results were 1433 mglL on 72512

7ull~4i( TlnE DATE

8312PLANT SUPERVISOR Ai 1ampllo~ TITlE DATE tishy LOCAL MANAGER

In tbe weather column use tbe follOWing symbols R-nun S-snow C-clear PC-partly doudy ()overcast

-Required Daily Required llweek

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

shyI~-~f r -----1

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ailltl JOSEI)II lWPLR

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411 ~ WIS I

Note to public water systems If you take a routine sample from a well rather than your distribution system a violation may be Issued by Missouri Public Drinking Water Branch

I riduy III1 - III

MI~~OUftl DePARTMENT OF NATURAL RESOURCES DIVISION OF ENVIRONMENTAL QUALITY

Discharge Monitoring Report For Municipal Wastewater Treatment Plants

N- OF FACILITY lOCA11UN iampCrTY ~ _shyNvada 1IItit WIItIIf rnt 117 s 1338 ROid NevIIda VERNONISOUTHWEST

IIR-r OUTFALL NUllBER TYPI ACLTY

IIIIyl2012 M0-00891 09 001 OXIDATION OtTCH INFLUENT FFFI JFIIIT

rNCiI -rAlp E OtL DATE FLOW BOD TSS u~s BOD TSS TEMP DO

IIIGO mall mall mall mall mall mall CFUllOOMl C mQt1 mQt1 mgI

1 067 00

2 O~9 00 226

I 3 089 00 122 118 67 3 7 005 228

4 091 00 227

5 096 00 44 375 lt10 200 58 2440 NO

6 100 00 228

7 099 00

8 098 00

9 166 00 231

10 139 00 229

11 095 00 44 275 61 4 5 007 227

12 099 00 lt10 229

13 104 T 226

14 102 00

15 100 00 16

099 00 225

17 100 00 229

i 18 103 00 118 113 69 3 4 008 229

19 102 T 733 230

20 101 00 229

I 21 095 00

122 096 00

23 099 00 232

24 098 00 234 i

25 099 00 131 199 69 6 11 01 233

26 035 T lt10 236

27 042 00 235

28 087 00

29 093 T

30 061 T 26

31 100 T 247

[Total 2982

iAVQ 096 t04 176 4 7 0CJ8 44 375 187 230 58 244 N()

Min 035 67 Max 166 00 89

lA8ORATORY TEST REQUIRED FOR wACTIVATED SlUDGEwPROCESSES

Aeration Baaln ()Ditch Etc

~ Sludge0 MIXED UQUOR Outside I A 00 -MLSS Settlbullbullbllity

Temp - Ambient 3 Disposal30 min E 30mtnW Temperature

CDT East East r E mgII mgII ml ml c OF bull Galions LbsDry Wt 1 88 C 915

2 31 1625 200 200 227 77 C 800

3 18 1322 200 200 229 76 PC 800

4 22 200 200 227 78 C 815

5 30 1678 200 200 222 77 C 800

6 31 1381 200 200 229 75 C 800

7 77 C 715

8 79 C 800

9 10 1850 200 200 229 77 PC 800

10 40 2215 200 229 76 PC 800

11 14 2132 220 226 75 C 800

12 40 2116 220 223 77 C 800

13 27 1935 220 225 73 PC 800

14 80 C 900

15 80 PC 900

16 27 2287 210 226 77 PC 800

11 26 1880 200 226 75 C 800

18 23 1679 180 226 78 C 800

19 26 1515 200 227 72 PC 800

20 27 1163 160 228 71 C 800

21 91 C 1230

22 89 C 845

23 23 1461 150 231 80 C 800

24 25 1412 200 231 78 800 21000 332f

25 29 1413 180 232 77 C 800 24000 4003

26 28 1395 150 234 91 PC 930

27 23 1451 150 240 75 C 800

28 63 C 730

29 79 C 800

30 10 1550 150 231 78 PC 800 15000 2127

31 18 1451 180 100 234 78 PC 800 27000 6305 COMMENTS ~ nICI ncrbull - IVII ICIU 1e5Ui lur I UUlI -IV U~ I VICII _ ILUI1 v ClIIU UI 6shy

GGA results were 1585 mglL on 7312 GGA results were 1339 mglL on 71112

GGA results were 852 on 718112 GGA results were 1433 mglL on 72512

7ull~4i( TlnE DATE

8312PLANT SUPERVISOR Ai 1ampllo~ TITlE DATE tishy LOCAL MANAGER

In tbe weather column use tbe follOWing symbols R-nun S-snow C-clear PC-partly doudy ()overcast

-Required Daily Required llweek

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

MI~~OUftl DePARTMENT OF NATURAL RESOURCES DIVISION OF ENVIRONMENTAL QUALITY

Discharge Monitoring Report For Municipal Wastewater Treatment Plants

N- OF FACILITY lOCA11UN iampCrTY ~ _shyNvada 1IItit WIItIIf rnt 117 s 1338 ROid NevIIda VERNONISOUTHWEST

IIR-r OUTFALL NUllBER TYPI ACLTY

IIIIyl2012 M0-00891 09 001 OXIDATION OtTCH INFLUENT FFFI JFIIIT

rNCiI -rAlp E OtL DATE FLOW BOD TSS u~s BOD TSS TEMP DO

IIIGO mall mall mall mall mall mall CFUllOOMl C mQt1 mQt1 mgI

1 067 00

2 O~9 00 226

I 3 089 00 122 118 67 3 7 005 228

4 091 00 227

5 096 00 44 375 lt10 200 58 2440 NO

6 100 00 228

7 099 00

8 098 00

9 166 00 231

10 139 00 229

11 095 00 44 275 61 4 5 007 227

12 099 00 lt10 229

13 104 T 226

14 102 00

15 100 00 16

099 00 225

17 100 00 229

i 18 103 00 118 113 69 3 4 008 229

19 102 T 733 230

20 101 00 229

I 21 095 00

122 096 00

23 099 00 232

24 098 00 234 i

25 099 00 131 199 69 6 11 01 233

26 035 T lt10 236

27 042 00 235

28 087 00

29 093 T

30 061 T 26

31 100 T 247

[Total 2982

iAVQ 096 t04 176 4 7 0CJ8 44 375 187 230 58 244 N()

Min 035 67 Max 166 00 89

lA8ORATORY TEST REQUIRED FOR wACTIVATED SlUDGEwPROCESSES

Aeration Baaln ()Ditch Etc

~ Sludge0 MIXED UQUOR Outside I A 00 -MLSS Settlbullbullbllity

Temp - Ambient 3 Disposal30 min E 30mtnW Temperature

CDT East East r E mgII mgII ml ml c OF bull Galions LbsDry Wt 1 88 C 915

2 31 1625 200 200 227 77 C 800

3 18 1322 200 200 229 76 PC 800

4 22 200 200 227 78 C 815

5 30 1678 200 200 222 77 C 800

6 31 1381 200 200 229 75 C 800

7 77 C 715

8 79 C 800

9 10 1850 200 200 229 77 PC 800

10 40 2215 200 229 76 PC 800

11 14 2132 220 226 75 C 800

12 40 2116 220 223 77 C 800

13 27 1935 220 225 73 PC 800

14 80 C 900

15 80 PC 900

16 27 2287 210 226 77 PC 800

11 26 1880 200 226 75 C 800

18 23 1679 180 226 78 C 800

19 26 1515 200 227 72 PC 800

20 27 1163 160 228 71 C 800

21 91 C 1230

22 89 C 845

23 23 1461 150 231 80 C 800

24 25 1412 200 231 78 800 21000 332f

25 29 1413 180 232 77 C 800 24000 4003

26 28 1395 150 234 91 PC 930

27 23 1451 150 240 75 C 800

28 63 C 730

29 79 C 800

30 10 1550 150 231 78 PC 800 15000 2127

31 18 1451 180 100 234 78 PC 800 27000 6305 COMMENTS ~ nICI ncrbull - IVII ICIU 1e5Ui lur I UUlI -IV U~ I VICII _ ILUI1 v ClIIU UI 6shy

GGA results were 1585 mglL on 7312 GGA results were 1339 mglL on 71112

GGA results were 852 on 718112 GGA results were 1433 mglL on 72512

7ull~4i( TlnE DATE

8312PLANT SUPERVISOR Ai 1ampllo~ TITlE DATE tishy LOCAL MANAGER

In tbe weather column use tbe follOWing symbols R-nun S-snow C-clear PC-partly doudy ()overcast

-Required Daily Required llweek

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

lA8ORATORY TEST REQUIRED FOR wACTIVATED SlUDGEwPROCESSES

Aeration Baaln ()Ditch Etc

~ Sludge0 MIXED UQUOR Outside I A 00 -MLSS Settlbullbullbllity

Temp - Ambient 3 Disposal30 min E 30mtnW Temperature

CDT East East r E mgII mgII ml ml c OF bull Galions LbsDry Wt 1 88 C 915

2 31 1625 200 200 227 77 C 800

3 18 1322 200 200 229 76 PC 800

4 22 200 200 227 78 C 815

5 30 1678 200 200 222 77 C 800

6 31 1381 200 200 229 75 C 800

7 77 C 715

8 79 C 800

9 10 1850 200 200 229 77 PC 800

10 40 2215 200 229 76 PC 800

11 14 2132 220 226 75 C 800

12 40 2116 220 223 77 C 800

13 27 1935 220 225 73 PC 800

14 80 C 900

15 80 PC 900

16 27 2287 210 226 77 PC 800

11 26 1880 200 226 75 C 800

18 23 1679 180 226 78 C 800

19 26 1515 200 227 72 PC 800

20 27 1163 160 228 71 C 800

21 91 C 1230

22 89 C 845

23 23 1461 150 231 80 C 800

24 25 1412 200 231 78 800 21000 332f

25 29 1413 180 232 77 C 800 24000 4003

26 28 1395 150 234 91 PC 930

27 23 1451 150 240 75 C 800

28 63 C 730

29 79 C 800

30 10 1550 150 231 78 PC 800 15000 2127

31 18 1451 180 100 234 78 PC 800 27000 6305 COMMENTS ~ nICI ncrbull - IVII ICIU 1e5Ui lur I UUlI -IV U~ I VICII _ ILUI1 v ClIIU UI 6shy

GGA results were 1585 mglL on 7312 GGA results were 1339 mglL on 71112

GGA results were 852 on 718112 GGA results were 1433 mglL on 72512

7ull~4i( TlnE DATE

8312PLANT SUPERVISOR Ai 1ampllo~ TITlE DATE tishy LOCAL MANAGER

In tbe weather column use tbe follOWing symbols R-nun S-snow C-clear PC-partly doudy ()overcast

-Required Daily Required llweek

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

CERTIFICATE OF RECOGNITION ERA congratulates

CITY OF NEVADA WWTP for your participation and successful evaluation in DMR-QA 32 We

recognize the performance of this laboratory for achieving acceptable evaluations for the following analytes

Ammonia as N Non-Filterable Residue (TSS)

BOD pH

5t1(~ Jay R McBurney Quality Program Manager

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

QERA A Waters Company

Mark Mendenhall City of Nevada WWTP City HallJWWTP 110 South Ash Street Nevada MO 64772middot3117

NPDES Permit M00089109

DMR-QA Study

Open Date 031912

Close Date 070612

Report Issued Date 072712

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

A Waters Company

July 272012

Mark Mendenhall City of Nevada WWTP City HallIWWTP 110 South Ash Street Nevada MO 64772-3117

Enclosed is your tinal report for ERAs DMR-QA 32 Proficiency Testing study Your final report includes an evaluation of every result submitted to your penn it Please note that reports were sent on your behalf to your state or regional DMRshyQA coordinator As the pennit holder you are required to review and sign the attached fonns and forward them to your DMR-QA coordinator Your Certificate of Recognition will be mailed at a later date

If you have any Not Acceptable- evaluations for the DMR-QA 32 study a letter of corrective action and an order fonn for the required remedial samples are attached for your convenience If you have a -Not Acceptable evaluation but there is not an order fonn or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

Thank you for your participation in ERAs DMR-QA 32 Proficiency Testing study If you have any questions please contact the proficiency testing department or me at 1-800-372middot0122

Your DMRmiddotQA coordinator is

USEPA Region VII Robert Bryant Water Enforcement 901 North Fifth Street Kansas City KS 66101 Phone 913-551-7354 Fax 913551middot7765 bryantrobertepagov

Sincerely

Jay R McBurney Quality Program Manager

attachments inn

16341 Table Mountain Parteway Golden Colorado 80403 800-372-0122 fax (303) 421-0159 wwweraqccom

ERA AWaters Company

DMRQA-32 Definitions ampStudy Discussion Study Dates 03119112 - 0710612

PMROA Study DefInitions

The Reported Value is the value that the laboratory reported to ERA

The ERA Assigned Values are compliant with the current FoPT tables A parameter not added to the standard is given an Assigned Value oflt PTRLmiddot per the guidelines contained in the 2009 TNt Standards The assigned values are directly traceable to the commercially prepared starting materials used to manufacture the PT standards

The Acceptance Limits are established per the criteria contained in the most current TNt FoPT tables or ERAs SOP for the Generation of Performance Acceptance Limits 1lot as applicable

The Performance Evaluation

Acceptable =Reported Value falls within the Acceptance Limits

Not Acceptable =Reported Value falls outside the Acceptance Limits

No Evaluation =Reported Value cannot be evaluated

Not Reported =No Value reported

The Method Description is the method the laboratory reported to ERA

Report Issued 0712712

PMROA Study Plscuulon

ERAs DMR-QA 32 Proficiency Testing study has been reviewed by ERA senior management and certified compliant with the requirements of the 2009 TNI PT Standards and the criteria contained in the current TNI FoPT tables

ERAs DMR-QA 32 study standards were examined for any anomalies A full review of all homogeneity stability and accuracy verification data was completed All analytical verification data for all analytes met the acceptance criteria contained in the 2009 TNI PT Standard and the criteria contained in the current TNI Fields of Proficlency Testing (FoPT) tables

The data submitted by partidpating laboratories was also examined for study anomalies There were no anomalies observed during the statistical review of the data

ERAs DMR-QA 32 study reports shall not be reproduced Elxcept in their entirety and not without the permission of the partidpating laboratories The report must not be used by the partidpating laboratories to claim product endorsement by any agency of the U S government

The data contained herein arEl confidential and intended for your use only

If you have any questions or concerns regarding your assessment in ERAs DMRQA Proficiency Testing program please contact our Profidency Testing Department at 1middot800-372-0122

enN eM ~ a I en 00

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E 0 C E ~ ~

C +-l -

E+- (f) I shy

Q) a (J) UJ Cl a Z

c I shy

~ ca

C ca gtCD Z 0

~ shyU Q)

E m Z

~ 0

+-

~ 0

0 m

J

o - 8 11

Q

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report ISlued 072712

WWTP Supervisor Study Dates 0311912 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

AUIyte Code Anayte Units

Performance Evaluation

Reported Value

Alllned Value

Acceptance limits

Method D crlptlon Study Mean Study

Standard Devllltlon

USEPA Lab Code

Study

WP IIlnetl1l CllttI 581

1505

1575

1610

1730

1125

1155

2000

1955

1950

lfJkalinity as CaCm

Chloride

ConductiVity at 2SmiddotC

Fluoride

Potassium

Sodium

Sulfate

Total Dissolved Solids a1180C

Total Solids all0SmiddotC

mgIl

mgIl

Ilmhoscm

mgIl

mgIl

mgIl

mgIl

mgll

mgll

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

460

497

353

150

341

SO5

407

274

262

431

489

368

144

354

SO2

399

246

253

369 -498

414-569

328middot 408

114-174

293middot421

426-577

323middot464

182middot 310

215 - 288

8M23208 1IIIh ED 1992

8M4500CI- E 18th ED 1992

SM2510a 18th ED 1992

EPA 300021 1993

EPA 2007 44 1994

EPA 2007 441994

EPA 3000 21 1993

SM2540C 18th ED 1992

SM2540B 18th ED 1992

436

494

368

142

349

503

396

246

254

208

215

864

00992

188

252

206

145

167

KSOOO21

KSOOO21

KSOOO21

KSOOO21

KSOOO21

KSOOO21

KSOOO21

KSOOO21

KSOOO21

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP 1I11Ift (Cllttl581 1505 Alkalinity as CaC 03 mglL Acceptable 460 431 369 - 498 SM2320B online 436 208 KSOOO21 WP204

1575 ~hloride mglL Acceptable 497 489 414 - 569 SM4500CI- Eonline 494 215 KSOOO21 WP204

1610 ~onductlvlty at 2SC ~mhoslcm Acceptable 353 368 328middot408 SM2510B online 368 864 KSOOO21 WP204

1730 Fluoride mglL Acceptable 150 144 114-174 EPA 9056 1994 142 00992 KSOOO21 WP204

1125 Potauium mgL Acceptable 34 354 293-421 EPA6010B 21996 349 188 KSOOO21 WP204

1155 Sodium mgL Acceptable 505 502 426middot577 EPA 6010B 1 1996 503 252 KSOOO21 WP204

2000 Sulfate mgL Acceptable 407 399 323 - 464 EPA 9056 1994 396 206 KSOOO21 WP204

1955 iTotal Dissolved Solids aI180C mgL Acceptable 274 246 182 - 310 SM2540C online 246 145 KSOO021 WP204

1950 Irotal Solklut lOSC shy ~IL_ Accetable 262 253 215middot288 SM2540B online 254 167 KSOOO21 WP204

mgJL EPA 3000 21 1993 KSO0021 WP204

IJmhoscm EPA 9050A 1 1996 KSO0021 WP204

bull All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 _20113 ~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 072712

WWTP Supervisor Study Dates 0311912 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-44a-2761

AIllIyte Code

Analyle Unlt$ Performance Evaluation

Reported Value

Aulgned Value

Aeptance Umlb

Method Ducriptlon Study Mean Study

Standard Deviation

USEPALab Code

Study

WP MlnetII (ca 51111 1575 EhIoride mgll Acceptable 482 489 414 - 569 EPA 9056 1994 494 215 KSOOO21 WP204

WP Hrd (cttI 580

1960

1035

1085

1550

1755

lion-Filterable Residue (TSS)

Calcium

Magnesium

Clkium Hardneas as CaCD3

olal Hardneaa as CaC03

mgIl

mgIl

mgIl

mgIl

mgIl

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

440

448

105

112

155

439

448

103

112

154

334 - 508

399middot509

876-118

998 127

136 - 176

S12540D 18th ED 1992

EPA 2007 44 1994

EPA 2007 441994

EPA 2007 44 1994

EPA 200744 1994

428

449

104

113

155

276

200

0622

472

574

KSOOO21

KS00021

KS00021

KSOOO21

KSOOO21

WP204

WP204

WP204

WP204

WP204 I

~ _ _ ___ __n ___

1960

1035

1085

1550

1755

Non-Filterable Residue (TSS)

plclum

Magnesium

Clkium HlIIdneas 88 CaC03

Tolal Hardness as CeC03

mgIl

mgIl

mgl

mgL

mgl

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

440

44B

105

112

155

439

448

103

112

154

334middot508

399middot509

876-118

998 - 127

136-176

SM2540D online

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

428

449

104

113

155

276

200

0622

472

574

KSOOO21

KS00021

KS00021

KSOOO21

KSOOO21

WP204

WP204

WP204

WP204

WP204

_ _ --- -_ --shy1550

1755

plcium Hardness as CaC03

Total Hardness as CaC03 --shy -shy

mgl

mgl --shy _ _shy

Acceptable

Acceptable

112

155

112

154

998 127

136middot176 --shy

SM2340B 18th ED 1992

SM2340B 18th ED 1992

113

155

472

574

KSOOO21

KS00021

WP204

WP204

All anafytes are included in ERAs A2LA accreditation lab Code 1539-01 I

SM2340B online WP204

SM2340B online WP204

SM2540D 21st ED DMRQA322005

SM4500H B 18th ED WP2041992

ot13 ~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 07127112

WWTP Supervisor Study Dates 03119112middot07106112 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Anatyte Coct AnaIyW Unit Performance

EV1Iluatlon Reported

Value Aliligned

Value Acceptance

Limits Method Deacrlpllon Study n

Study Stllndllrd DevIation

USEPALab Code

Study

WP pH caft 5711

1900 jpH SU Acceptable 633 631 611middot651 SM4500H+ a online 629 00470 KSOOO21 WP204

WPSlmpjbull Nutrients (caft 584)

1515 Ammoniaaa N

1820 Nitrate + Nitrite as N

1810 Nitrate as N

1870 jor1ho-Phosphate as P

su

SU

SU

mLlL

mUL

mgl

mgl

mgll

mgll

mgIl

I Acceetable 633 631

Acceptable 633 631

Acceptable 731 723

Acceptable 330 279

Acceptable 330 279

Acceptable 514 529

Acceptable 121 109

Acceptable 426 435

Acceptable 426 435

Acceptable 394 40l~

I 611 - 651 I EPA 9040621995 I

611 bull 651 I EPA 9040C 2002 I 703743 ISM4500~~ 21s1 ED

I 227 - 355 SM2540F 18th ED 1992

I 227middot355 SM2540F online

I 385 _ 6 75 ISM4500NH3 021st ED 2005

808 -136

354middot507

339 - 526

337 - 484

EPA 3501 2 1993

EPA 3532 2 1993

EPA 3532 2 1993

EPA365121993

629 00470

629 00470

727 00644

298 230

298 230

530 0467

110 0839

431 0214

431 0212

412 0204

KSOOO21

KSOOO21

MOOO982

KSOOO21

KSOOO21

MOOO982

KSOOO21

KSOOO21

KSOOO21

KSOOO21

WP204

WP204

OMRQA32

WP204

WP204

OMRQA32

WP204

WP204

WP204

WP204

EPA 3000 21 1993 KS00021

EPA 3000 21 1993 KS00021

EPA 3512 21993 KSOOO21 EPA 3654 1974 KSO0021

All analytes are included in ERAs A2LA accreditation Lab Code 1539-01

WP204

WP204

WP204

WP204

13 ~_

---

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 072712

WWTP Supervisor Study Dates 0311912middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Al1IIiyte Code

Anltyte Units Perforll1llnCll Evaluation

Reported Valul

Asalgned Value

Ac~ptanc Llmltll Mlthod D bullbullcrlpllon Study MIn

Study Sblndard DevIation

USEPAub Code Study

DIIRQA Demand (ClIf1 57aJ

1530 roo mgll Acceptable 815 904 457-135 514521082111 ED 2005

913 168 MOOO982 DMRQA32

_

EPA 3532 2 1993 KSO0021 WP204

EPA 3000 21 1993 KSOOO21 WP204

EPA 9056 1994 KS00021 WP204

r _ __

1530

1555

1565

IBOD

C800

COD

mgIl

mgll

mgIl

Acceptable

Acceptable

Acceptable

322

259

529

323

279

521

161 - 466

125 - 433

353 - 646

5M5210B 18th ED 1992

51452108 18th ED 1992

514522001811 ED 1992

319

295

519

530

490

542

KSOO021

KSOO021

KSOO021

WP204

WP204

WP204

WP Demand leaf1 571) 5M5210B online KSOO0211530 soo 319 530Acceptable 322 323 161 - 486 WP204mgll 5M5210B online KSOO021279 125middot433 295 490 WP2041555 Feoo mgl Acceptable 259

51452200 online KSOO021519 542 WP2041565 icoo Acceptable 521 353 - 648 mgll 529

EPA 4104 2 1993 KSOO021 WP204

EPA 1664A 1999 KSOO021 WP204

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 ~

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 - 0706112 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

AlUliyW Code

Anetytw Unlta Performance Evaluation

Reported Valua

Aaalgned Value

ACQplence Llmlta

Method DelCription Study Mean Study

Standard Deviation

USEPA Lab Code Study

WP TlIICe Metallea 586j

1000 AlUminum J91L Acceptable 772 778 619middot932 EPA 2007441994 782 446 KSOOO21 WP204

1005 Anllmony JgL Acceptable 416 413 286 - 499 EPA 2007 441994 402 211 KSOO021 WP204

1010 Araenic Jgl Acceptable 350 347 289 - 408 EPA 2007 441994 344 190 KSOOO21 WP204

1015 Barium JgL Acceptable 2350 2360 2050 - 2660 EPA 2007441994 2350 850 KSOOO21 WP204

1020 ~elytijum J91L Acceptable 462 454 386 - 513 EPA 2007 44 1994 444 202 KSOOO21 WP204

1025 BClron J91L Acceptable 1560 1660 1350 - 1930 EPA 2007 44 1994 1650 972 KSOO021 WP204

1030 centadmlum J9l Acceptable 439 427 364 -485 EPA 2007 44 1994 416 166 KSOOO21 WP204

1040 Chromium J91L Acceptable 534 541 471 - 612 EPA 2007 441994 537 224 KSOOO21 WP204

1050 Cobalt JglL Acceptable 397 362 317-406 EPA 2007 44 1994 374 159 KSOOO21 WP204

1055 Copper JgIL Acceptable 223 217 194 - 240 EPA 2007 441994 219 965 KSOOO21 WP204

1070 Iron JgIL Acceptable 1070 1070 946 - 1210 EPA 200744 1994 1080 495 KSOOO21 WP204

1075 Lead J9IL Acceptable 843 754 659middot845 EPA 2007 441994 756 325 KS00021 WP204

1090 ~nese 1J91L Acceptable 1930 1860 1670 - 2070 EPA 2007 441994 1900 732 KSOOO21 WP204

1100 Molybdenum JglL Acceptable 226 214 178 - 248 EPA 2007 44 1994 212 103 KSOOO21 WP204

1105 Nlckal Jell Acceptable 557 507 455 - 568 EPA 2007 44 1994 505 224 KSOOO21 WP204

1140 Selenium Jgl Acceptable 1600 1620 1290middot 1870 EPA 200144 1994 1590 969 KSOOO21 WP204

1150 SiMlr IJgL Acceptable 366 361 310 -414 EPA 2001 441994 360 203 KSOOO21 WP204

1160 Strontium 1JgL Acceptable 143 141 121 - 161 EPA 2001 44 1994 140 672 KSOOO21 WP204

1165 Thallium J9IL Not Acceptable 669 557 450 - 667 EPA 20074 41994 555 319 KSOOO21 WP204

1185 Vanadium JgL Acceptable 966 991 868-1110 EPA 200744 1994 980 446 KSOOO21 WP204

EPA 2007 44 1994 WP204

All analytes are included in ERAs A2LA accreditation Lab Gode 1539-01 _ of13 ~II

DMRQA32 Final Report ERA AWaters Company

NPoes Permit MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Illued 072712

WWTP Supervisor Study Dates 031912 middot070612 City of Neyada WWTP 16517 South 1338 Road Neyada MO 64772 417-448middot2761

Analyte Code

Analyte Unttll Performance Evaluation

Reported Value

Assigned Vllue

Accaptllnca Limb

Method DseMptlon Study Mean Study

Standard Devtatlon

USEPAub Code

Study

WP TRee _1 (calf 58B)

1000

1005

1010

1015

1020

1025

1030

1040

1050

1055

1070

1075

1090

1100

1105

1140

1150

1160

1165

1185

Aluminum

Antimony

Anlenic

Barium

Beryl~um

~on Cadmium

Chromium

Cobalt

Copper

Iron

fLead Manganese

Molybdenum

Nickel

Selenium

Silver

Strontium

Thallium

Vanedium

IJgIL

1J91L

1J91L

IJgIL

IJgIL

IJgIL

IJglL

IJglL

IJgIL

IJgIL

jJgL

IJglL

1J9L

IJglL

IJglL

1J91L

IJglL

IJgIL

jJgL

Jl9L_ _

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Not Acceptable

A~tatgt1ft

772

416

350

2350

462

1560

439

534

397

223

1070

843

1930

226

557

1600

366

143

669

966

778

413

347

2360

454

1660

427

541

362

217

1070

754

1860

214

507

1620

361

141

557

619middot932

286 -499

289 - 408

2050 - 2660

386 - 513

1350middot1930

364 - 485

471 - 612

317 - 406

194 - 240

946 - 1210

659 - 845

1670 - 2070

178 - 248

455 - 568

1290 - 1870

310 - 414

121 - 161

450 - 667

__99_1__ ~8-1110

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010821996

EPA 60108 21996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 60108 21996

EPA 6010B 21996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996 -shy

782

402

344 2350

444

1650

416

537

374

219

1080

756

1900

212

505

1590

360

140

555

980

446

211

190

850

202

972

166

224

159

965

495

325

732

103

224

969

203

672

319

446

KSOO021

KSOO021

KSOOO21

KSOOO21

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOOO21

KSoo021

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

EPA 60108 21996 WP204

_- ---- shy1030

1040

1075

jcadmium

[chromium

Lampad

jJglL

jJglL

IJgIL

Acceptable

Acceptable

Acceptable

439

534

843

427

541

754

364 - 485

471 612

659 - 845

EPA 6010C 2000

EPA 6010C 2000

EPA 6010C 2000

416

537

756

166

224

325

KSOOO21

KSOOO21

KSOO021

WP204

WP204

WP204

e All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 Pof13 ~

DMRQA32 Final Report ERA AWaters Company

NPoes Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 middot0706112 City of Nevada WWTP 16517 South 1338 Road Nevad MO 84m 417-448middot2761

Analyte Code Analyte Units Performanu

Evaluation Reported

Value Assigned

Value Acceptance

Lim Method DeSCription Study Mesn

Study Stndard DevIlItion

USEPA Lab Code Study

wp rce Metal (cetil586J Aluminum EPA 2008 55 19981000 KS00021 WP204 iAcceptable 778 782 446IJglL 800 619middot932 Antimony EPA 2008 55 19981005 KSOOO21Acceptable 211 WP204413 402IJglL 404 286middot499 Arsenic EPA 2008 55 19981010 Acceptable 190 KS00021 WP204370 347 289 - 408 3441J91L ~rium1015 EPA 2008 55 1998 850 KSOOO21 WP204Acceptable 2350IJglL 2360 2360 2050 - 2660 Betylhum EPA 2008 55 19981020 WP204KS00021gil Acceptable 444 202431 454 386 - 513 cadmium EPA 2008 55 19981030 KS00021Acceptable 166 WP204gil 416 427 416364 middot485 Chromium EPA 2008 55 19981040 224 KS00021Acceptable 541 537 WP204IJglL 551 471 - 612

Cobah EPA 2008 55 19981050 KS00021 WP204Acceptable 374 159IJglL 377 362 317 - 406

Copper EPA 2008 5519981055 KS00021Acceptable 965 WP204IJglL 221 217 219194middot240 Iron EPA 2008 55 19981070 gIL 1080 495 KS00021 WP204Acceptable 10701040 946 - 1210

ead EPA 2008 5519981075 gIL KSOO021 WP204Acceptable 756 325760 754 659- 845

EPA 2008 55 19981090 ~nese KS00021gIL Acceptable 1900 732 WP2041940 1860 1670middot2070

EPA 2008 55 1998~enum1100 KSOOO21gIL Acceptable 103 WP204213 214 212178middot248 Nickel EPA 2008 5519981105 gIL 224 KSOO021 WP204Acceptable 505512 507 455 - 568

1140 Selenium EPA 2008 55 1998giL 1590 KS00021Acceptable 1620 969 WP2041600 1290middot1870

EPA 2008 551998I 1150 ~lIver KS00021Acceptable WP204322 361 310-414 360 203IJgIL 1165 Thallium EPA 2008 551998 319 KSOO021Acceptable 557 555 WP204538 450middot6671JgL

1185 Vanadium Nol Accepteble EPA 2008 551998 KS00021446 WP204991 980IJglL 1440 868middot1110

EPA 2008 5519981190 Zinc KS00021giL Acceptable 977 462 WP204993 975 _838middot 11~0 - - bull- -~

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 _ of13 ~

DMRQA32 Final Report ERA A Waters Company

NPOES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP SupelVlsor Study Dates 03119112 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 84772 417-448middot2761

Analyta Analyt8Code Unite Performence Reported AIIIUned

Evaluation Value Value Acceplll nee

LImite IiMthod Oeerlpllon

Study USEPALabStudyMn Standard Study DevIation

Code i

WP Trce Metals (Clltti 586J 1000 [Aluminum IlglL Acceptable 800 778 619-932 EPA 8020A 1998 782 446 KSOOO21 WP204 I

1005 [Antimony IlglL Acceptable 404 413 286-499 EPA 8020A 1998 402 211 KSOO021 WP204

1010 iAraenk IlglL Acceptable 370 347 289 - 408 EPA 802011 1998 344 190 KSOOO21 WP204

1015 ~lium 1l91L Acceptable 2360 2360 2050 - 2660 EPA 8020A 1998 2350 850 KS00021 WP204

1020 Seryffium IlgIL Acceptable 431 454 386 - 513 EPA 8020A 1998 444 202 KSOOO21 WP204

1030 ~mium IlgIL Acceptable 416 427 364 - 485 EPA 6020A 1998 416 166 KSOOO21 WP204

1040 Chromium IlQIL Acceptable 551 541 471 - 612 EPA 6020A 1998 537 224 KSOO021 WP204

1050 Cabalaquo IlQIL Acceptable 377 362 317 - 406 EPA 8020A 1998 374 159 KSOOO21 WP204

1055 Copper 1l91L Acceptable 221 217 194middot240 EPA 8020A 1998 219 965 KSOO021 WP204

1070 lroo 1l91L Acceptable 1040 1070 9Mi-1210 EPA 602011 1998 1080 495 KSOOO21 WP204

1075 ~ad IlglL Acceptable 760 754 659 - 845 EPA 6020A 1998 756 325 KSOOO21 WP204

1090 Manganese IlgIL Acceptable 1940 1860 1670 - 2070 EPA 602011 1998 1900 732 KSOO021 WP204

1100 MolytxIenum IlglL Acceptable 213 214 178-248 EPA 6020A 1998 212 103 KSOOO21 WP204

1105 Nickel IlgL Acceptable 512 507 455 - 568 EPA 602011 1998 505 224 KSOOO21 WP204

1140 Selenium IlglL Acceptable 1600 1620 1290 - 1870 EPA 8020A 1998 1590 969 KSOO021 WP204

1150 Silver 1l9L Acceptable 322 361 310 - 414 EPA 8020A 1998 360 203 KSOO021 WP204

1165 Thatlium 1l9L Acceptable 538 557 450 - 667 EPA 8020A 1998 555 319 KSOO021 WP204

1185 Vanadium IlQL Not Acceptable 1440 991 868-1110 EPA 8020A 1998 980 446 KSOO021 WP204

1190 Zinc IJgL Acceptable 993 975 838 -1120 EPA 8020A 1998 977 462 KSOO021 WP204

EPA 2451 3 1994

EPA 747011 1 1994

SM3500Cr 0 18th ED 1992

KS00021 WP204

KS00021 WP204

KSOO021 WP204

All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 13~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 031912 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448~2761

AII~ Code Ane~ Unltll Performnce

evaluation Reported

1Ilue Aalilned

1Ilue ~ptenc

Umltll Method Deecrtptloll Study Men Study

Stanclllrd Oevilltion

USEPA Leb Coda Study

WP Hexvent Chromium (ttl aN) 1045 HellllY81ent Chromium IJQL ---1 Aclteptable 1 580 1 606 1 494 712 1 EPA 7196A 1 19921 6Q4 ~4 I KSOOO21 WP204 J

EPA 1801 2 1993 672 0483 KSOOO21 WP204

SM2130B 18th ED 672 0483 KSOO021 WP2041992

SM21308 online 672 0483 KSOO021 WP204

EPA9012A 0836 00962 KSOO021 WP204

SM4500CN E 18th 0836 00962 KSOO021 WP204ED 1992

SM4500CN E online I 0836 00962 KSOO021 WP204

EPA 4201 1978 0491 0101 KSOO021 WP204

EPA 9066 1986 0491 0101 KSOO021 WP204

SM4500CI E 18th ED I 0850 00673 KSOO021 WP2041992

ISM4500CI E online 0850 00673 KSOO021 WP204

SM4500Ct G 18th ED I 0850 00673 KSOO021 WP2041992

e All analy1es are included in ERAs A2LA accreditation Lab Code 1539middot01 Pag1Oof13

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 03119112 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

Anltya Code Anltya UnMa Performanee

EVlluation Reported

Vllue Anlgned

Vllue Acceptance

Umltll Method Oeecrlptlon Study Meln Study

Satndlrd DevIation

USEPA lab Code

Study

WP Totll Reldulll ChIorlfHIlc 587J 1940 ITotal Residual Chlorine

-shy I mgll I Acceptable I 945 I 0822 I 0594 - 103 LSM4500CI CO onNne I 0850 - 00673 KSOOO21 WP204

ISM4500f~218th EO I 134 159 KSOOO21 WP204

SM4SOOCI E online KSOOO21 WP204

ISM4~~18th Eol 134 159 KSOO021 WP204

SM4500CI G onMne I 134 159 KSOOO21 WP204

CNI Level TDlaI Residual Chlorine

Level T alai Residual Chlorine

Level Total Residual Chlorine

jlglL Acceptable 140 138 780 _198

Ievel TDIal Residual Chlorine

uolL

jlgL

IlnlL

Acceptable 138 138 780 -198

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 P oI

ERA A Waters Company

Study DMRQA-32

NPDES Permit M00089109

Laboratory Name City of Nevada WWTP

It 120113

DMRQA32 Final Report ERA A Waters Company

NPDES Permitll MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dales 031912 middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Analyte rlS End Point Code Performance Repolllld Anlgned evaluation Value Value

Acceptance Method O crlptlonLimite

Study USEPAlIIbStudy StMldard Code

Study DevIatIon

-- -shyDMRQA FathNd minnow (Tut Code 13) (cat WETOO2) 48Hr Acute Non-Renewal 25 C MHSF Poraum chloride

~- IlC50 Acceptable 512 456 I 239 - 674 I EPA 2000 456 109 KSOOO21-(------oP4RQA32

DMRQA Fathead minnow (Test Code 15) (cat WET004) Today Short temI ChroniC Dally Renewal MHSF Potalum chlol1de

0808

0810

0756

IC25 (ON) Growth

NOEC (ON) Growth

NOEC Survival

Acceptable

Acceptable

-- Acceptable

389

25

25

355

250

250

175 - 535

125 - 500

125 - SOO

EPA 1000 2002

EPA 1000 2002

EPA 1000 2002 -shy

355 900 KSOO021

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32

DMRQA Cerlodaphna dubla (Tut Code 19) (cat WETOOB) 48Hr Acute Renewal 25 C MHSF Potlllum chlorlde

[Os ILC50 Acceptable 442 342 I 179middot504 I EPA 2002 342 810 - LIltSOOO21 [ DMRciA3iJ

DMRQA Cerlodflphnla dubla (Tet Code 21) (cat WET010) Today Short term Chronic Dally Renewal MHSF Potlllum chloride

0767

0768

0766

IC25 Raproduction

NOEC ReproductIOn

NOEC Survival -~ -shy

Acceptable

Acceptable

Acceptable

283

25

25

259

250

250

123 - 395

125 - 500

125middot500

EPA 1002 2002

EPA 10022002

EPA 10022002-_ __ __ shy

259 679 KSOOO21

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32shyDMRQA Daphnia pulax (Tet Code 38) (ea WET015) 48Hr Acute Non-Renewal 25 C MHSF Potassium chloride

[0794 ILC50 I Acceptable I 565 525 I 232middot818 I EPA 2021 525 147~r-KSoo021 -r OMRQAi2---]

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 13of13 ~

AWaters Company

Pennittee Name City of Nevada WWTP Pennit Number MOO089109 EPA Lab Code KSOOO21

WET OrganismsITest ConditionsEnd Points Checklist

DMRQA Study 32 La bull Graded Result

Analyte Number Organisms I Conditions End Points Test

Required Acceptable

Not Accepblble (ComtctIYe

Action Required)

Fathead minnow (Test Code 13) 0754 48Hrbull Acute Non-Renewal 25middot C MHSF lC50

EPA 2000 0 lEI 0 Fathead minnow (Test Code 14) 0755 48Hrbull Acute Non-Renewal 25middot C 20 DMW LC50

0 0 0 Fathead minnow (Test Code 15) 0808 7 -day Short Ierm Chronic Daily Renewal MHSF IC25 (ON) Growth

EPA 1000 0 lEI 0 0810 7 -day Short term Chronic Daily Renewal MHSF NOEC (ON) Growth

EPA 1000 0 lEI 0 0756 7-day Short term Chronic Daily Renewal MHSF NOEC Survival

EPA 1000 0 IRI 0 Fathead minnow (Test Code 18) 0812 7 -day Short term Chronic Daily Renewal 20 DMW IC25 (ON) Growth

0 0 0 0814 7-day Short Ierm Chronic Daily Renewal 20 DMW NOEC (ON) Growth

0 0 0 0759 7-day Short term Chronic Daily Renewal 20 DMW NOEC Survival

0 0 0 CerIodaphnle dubla (Test Code 19) 0764 48Hr Acute Renewal 25middot C MHSF LCSO

EPA 2002 0 IXI 0 CerIodaphnla dubla (Test Code 20) 0765 48Hr Acute ReneWal 25- C 20 DMW LCSO

0 0 0 CerIodaphnla dubla (Tast Code 21) 0767

0768

0766

7-day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF

IC25 Reproduction

NOEC Reproduction

NOEC Survival

0

0

IXI

[8]

0

0 EPA 1002 0 lEI 0

CerIodaphnla dubla (Tn Code 22) one 7-day Short term Chronic Daily Renewal 20 DMW IC25 Reproduction

0771 7-day Short term Chronic Daily Renewal 20 DMW NOEC Reproduction 0 0 0

0769 7 -day Short term Chronic Daily Renewal 20 DMW NOEC Survival 0 0 0

0 0 0 Daphnia magna (Test Code 32) 0788 48Hr Acute Non-Renewal 25deg C MHSF LCSO

0 0 0

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

enN eM ~ a I en 00

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E 0 C E ~ ~

C +-l -

E+- (f) I shy

Q) a (J) UJ Cl a Z

c I shy

~ ca

C ca gtCD Z 0

~ shyU Q)

E m Z

~ 0

+-

~ 0

0 m

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DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report ISlued 072712

WWTP Supervisor Study Dates 0311912 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

AUIyte Code Anayte Units

Performance Evaluation

Reported Value

Alllned Value

Acceptance limits

Method D crlptlon Study Mean Study

Standard Devllltlon

USEPA Lab Code

Study

WP IIlnetl1l CllttI 581

1505

1575

1610

1730

1125

1155

2000

1955

1950

lfJkalinity as CaCm

Chloride

ConductiVity at 2SmiddotC

Fluoride

Potassium

Sodium

Sulfate

Total Dissolved Solids a1180C

Total Solids all0SmiddotC

mgIl

mgIl

Ilmhoscm

mgIl

mgIl

mgIl

mgIl

mgll

mgll

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

460

497

353

150

341

SO5

407

274

262

431

489

368

144

354

SO2

399

246

253

369 -498

414-569

328middot 408

114-174

293middot421

426-577

323middot464

182middot 310

215 - 288

8M23208 1IIIh ED 1992

8M4500CI- E 18th ED 1992

SM2510a 18th ED 1992

EPA 300021 1993

EPA 2007 44 1994

EPA 2007 441994

EPA 3000 21 1993

SM2540C 18th ED 1992

SM2540B 18th ED 1992

436

494

368

142

349

503

396

246

254

208

215

864

00992

188

252

206

145

167

KSOOO21

KSOOO21

KSOOO21

KSOOO21

KSOOO21

KSOOO21

KSOOO21

KSOOO21

KSOOO21

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP 1I11Ift (Cllttl581 1505 Alkalinity as CaC 03 mglL Acceptable 460 431 369 - 498 SM2320B online 436 208 KSOOO21 WP204

1575 ~hloride mglL Acceptable 497 489 414 - 569 SM4500CI- Eonline 494 215 KSOOO21 WP204

1610 ~onductlvlty at 2SC ~mhoslcm Acceptable 353 368 328middot408 SM2510B online 368 864 KSOOO21 WP204

1730 Fluoride mglL Acceptable 150 144 114-174 EPA 9056 1994 142 00992 KSOOO21 WP204

1125 Potauium mgL Acceptable 34 354 293-421 EPA6010B 21996 349 188 KSOOO21 WP204

1155 Sodium mgL Acceptable 505 502 426middot577 EPA 6010B 1 1996 503 252 KSOOO21 WP204

2000 Sulfate mgL Acceptable 407 399 323 - 464 EPA 9056 1994 396 206 KSOOO21 WP204

1955 iTotal Dissolved Solids aI180C mgL Acceptable 274 246 182 - 310 SM2540C online 246 145 KSOO021 WP204

1950 Irotal Solklut lOSC shy ~IL_ Accetable 262 253 215middot288 SM2540B online 254 167 KSOOO21 WP204

mgJL EPA 3000 21 1993 KSO0021 WP204

IJmhoscm EPA 9050A 1 1996 KSO0021 WP204

bull All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 _20113 ~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 072712

WWTP Supervisor Study Dates 0311912 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-44a-2761

AIllIyte Code

Analyle Unlt$ Performance Evaluation

Reported Value

Aulgned Value

Aeptance Umlb

Method Ducriptlon Study Mean Study

Standard Deviation

USEPALab Code

Study

WP MlnetII (ca 51111 1575 EhIoride mgll Acceptable 482 489 414 - 569 EPA 9056 1994 494 215 KSOOO21 WP204

WP Hrd (cttI 580

1960

1035

1085

1550

1755

lion-Filterable Residue (TSS)

Calcium

Magnesium

Clkium Hardneas as CaCD3

olal Hardneaa as CaC03

mgIl

mgIl

mgIl

mgIl

mgIl

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

440

448

105

112

155

439

448

103

112

154

334 - 508

399middot509

876-118

998 127

136 - 176

S12540D 18th ED 1992

EPA 2007 44 1994

EPA 2007 441994

EPA 2007 44 1994

EPA 200744 1994

428

449

104

113

155

276

200

0622

472

574

KSOOO21

KS00021

KS00021

KSOOO21

KSOOO21

WP204

WP204

WP204

WP204

WP204 I

~ _ _ ___ __n ___

1960

1035

1085

1550

1755

Non-Filterable Residue (TSS)

plclum

Magnesium

Clkium HlIIdneas 88 CaC03

Tolal Hardness as CeC03

mgIl

mgIl

mgl

mgL

mgl

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

440

44B

105

112

155

439

448

103

112

154

334middot508

399middot509

876-118

998 - 127

136-176

SM2540D online

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

428

449

104

113

155

276

200

0622

472

574

KSOOO21

KS00021

KS00021

KSOOO21

KSOOO21

WP204

WP204

WP204

WP204

WP204

_ _ --- -_ --shy1550

1755

plcium Hardness as CaC03

Total Hardness as CaC03 --shy -shy

mgl

mgl --shy _ _shy

Acceptable

Acceptable

112

155

112

154

998 127

136middot176 --shy

SM2340B 18th ED 1992

SM2340B 18th ED 1992

113

155

472

574

KSOOO21

KS00021

WP204

WP204

All anafytes are included in ERAs A2LA accreditation lab Code 1539-01 I

SM2340B online WP204

SM2340B online WP204

SM2540D 21st ED DMRQA322005

SM4500H B 18th ED WP2041992

ot13 ~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 07127112

WWTP Supervisor Study Dates 03119112middot07106112 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Anatyte Coct AnaIyW Unit Performance

EV1Iluatlon Reported

Value Aliligned

Value Acceptance

Limits Method Deacrlpllon Study n

Study Stllndllrd DevIation

USEPALab Code

Study

WP pH caft 5711

1900 jpH SU Acceptable 633 631 611middot651 SM4500H+ a online 629 00470 KSOOO21 WP204

WPSlmpjbull Nutrients (caft 584)

1515 Ammoniaaa N

1820 Nitrate + Nitrite as N

1810 Nitrate as N

1870 jor1ho-Phosphate as P

su

SU

SU

mLlL

mUL

mgl

mgl

mgll

mgll

mgIl

I Acceetable 633 631

Acceptable 633 631

Acceptable 731 723

Acceptable 330 279

Acceptable 330 279

Acceptable 514 529

Acceptable 121 109

Acceptable 426 435

Acceptable 426 435

Acceptable 394 40l~

I 611 - 651 I EPA 9040621995 I

611 bull 651 I EPA 9040C 2002 I 703743 ISM4500~~ 21s1 ED

I 227 - 355 SM2540F 18th ED 1992

I 227middot355 SM2540F online

I 385 _ 6 75 ISM4500NH3 021st ED 2005

808 -136

354middot507

339 - 526

337 - 484

EPA 3501 2 1993

EPA 3532 2 1993

EPA 3532 2 1993

EPA365121993

629 00470

629 00470

727 00644

298 230

298 230

530 0467

110 0839

431 0214

431 0212

412 0204

KSOOO21

KSOOO21

MOOO982

KSOOO21

KSOOO21

MOOO982

KSOOO21

KSOOO21

KSOOO21

KSOOO21

WP204

WP204

OMRQA32

WP204

WP204

OMRQA32

WP204

WP204

WP204

WP204

EPA 3000 21 1993 KS00021

EPA 3000 21 1993 KS00021

EPA 3512 21993 KSOOO21 EPA 3654 1974 KSO0021

All analytes are included in ERAs A2LA accreditation Lab Code 1539-01

WP204

WP204

WP204

WP204

13 ~_

---

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 072712

WWTP Supervisor Study Dates 0311912middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Al1IIiyte Code

Anltyte Units Perforll1llnCll Evaluation

Reported Valul

Asalgned Value

Ac~ptanc Llmltll Mlthod D bullbullcrlpllon Study MIn

Study Sblndard DevIation

USEPAub Code Study

DIIRQA Demand (ClIf1 57aJ

1530 roo mgll Acceptable 815 904 457-135 514521082111 ED 2005

913 168 MOOO982 DMRQA32

_

EPA 3532 2 1993 KSO0021 WP204

EPA 3000 21 1993 KSOOO21 WP204

EPA 9056 1994 KS00021 WP204

r _ __

1530

1555

1565

IBOD

C800

COD

mgIl

mgll

mgIl

Acceptable

Acceptable

Acceptable

322

259

529

323

279

521

161 - 466

125 - 433

353 - 646

5M5210B 18th ED 1992

51452108 18th ED 1992

514522001811 ED 1992

319

295

519

530

490

542

KSOO021

KSOO021

KSOO021

WP204

WP204

WP204

WP Demand leaf1 571) 5M5210B online KSOO0211530 soo 319 530Acceptable 322 323 161 - 486 WP204mgll 5M5210B online KSOO021279 125middot433 295 490 WP2041555 Feoo mgl Acceptable 259

51452200 online KSOO021519 542 WP2041565 icoo Acceptable 521 353 - 648 mgll 529

EPA 4104 2 1993 KSOO021 WP204

EPA 1664A 1999 KSOO021 WP204

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 ~

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 - 0706112 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

AlUliyW Code

Anetytw Unlta Performance Evaluation

Reported Valua

Aaalgned Value

ACQplence Llmlta

Method DelCription Study Mean Study

Standard Deviation

USEPA Lab Code Study

WP TlIICe Metallea 586j

1000 AlUminum J91L Acceptable 772 778 619middot932 EPA 2007441994 782 446 KSOOO21 WP204

1005 Anllmony JgL Acceptable 416 413 286 - 499 EPA 2007 441994 402 211 KSOO021 WP204

1010 Araenic Jgl Acceptable 350 347 289 - 408 EPA 2007 441994 344 190 KSOOO21 WP204

1015 Barium JgL Acceptable 2350 2360 2050 - 2660 EPA 2007441994 2350 850 KSOOO21 WP204

1020 ~elytijum J91L Acceptable 462 454 386 - 513 EPA 2007 44 1994 444 202 KSOOO21 WP204

1025 BClron J91L Acceptable 1560 1660 1350 - 1930 EPA 2007 44 1994 1650 972 KSOO021 WP204

1030 centadmlum J9l Acceptable 439 427 364 -485 EPA 2007 44 1994 416 166 KSOOO21 WP204

1040 Chromium J91L Acceptable 534 541 471 - 612 EPA 2007 441994 537 224 KSOOO21 WP204

1050 Cobalt JglL Acceptable 397 362 317-406 EPA 2007 44 1994 374 159 KSOOO21 WP204

1055 Copper JgIL Acceptable 223 217 194 - 240 EPA 2007 441994 219 965 KSOOO21 WP204

1070 Iron JgIL Acceptable 1070 1070 946 - 1210 EPA 200744 1994 1080 495 KSOOO21 WP204

1075 Lead J9IL Acceptable 843 754 659middot845 EPA 2007 441994 756 325 KS00021 WP204

1090 ~nese 1J91L Acceptable 1930 1860 1670 - 2070 EPA 2007 441994 1900 732 KSOOO21 WP204

1100 Molybdenum JglL Acceptable 226 214 178 - 248 EPA 2007 44 1994 212 103 KSOOO21 WP204

1105 Nlckal Jell Acceptable 557 507 455 - 568 EPA 2007 44 1994 505 224 KSOOO21 WP204

1140 Selenium Jgl Acceptable 1600 1620 1290middot 1870 EPA 200144 1994 1590 969 KSOOO21 WP204

1150 SiMlr IJgL Acceptable 366 361 310 -414 EPA 2001 441994 360 203 KSOOO21 WP204

1160 Strontium 1JgL Acceptable 143 141 121 - 161 EPA 2001 44 1994 140 672 KSOOO21 WP204

1165 Thallium J9IL Not Acceptable 669 557 450 - 667 EPA 20074 41994 555 319 KSOOO21 WP204

1185 Vanadium JgL Acceptable 966 991 868-1110 EPA 200744 1994 980 446 KSOOO21 WP204

EPA 2007 44 1994 WP204

All analytes are included in ERAs A2LA accreditation Lab Gode 1539-01 _ of13 ~II

DMRQA32 Final Report ERA AWaters Company

NPoes Permit MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Illued 072712

WWTP Supervisor Study Dates 031912 middot070612 City of Neyada WWTP 16517 South 1338 Road Neyada MO 64772 417-448middot2761

Analyte Code

Analyte Unttll Performance Evaluation

Reported Value

Assigned Vllue

Accaptllnca Limb

Method DseMptlon Study Mean Study

Standard Devtatlon

USEPAub Code

Study

WP TRee _1 (calf 58B)

1000

1005

1010

1015

1020

1025

1030

1040

1050

1055

1070

1075

1090

1100

1105

1140

1150

1160

1165

1185

Aluminum

Antimony

Anlenic

Barium

Beryl~um

~on Cadmium

Chromium

Cobalt

Copper

Iron

fLead Manganese

Molybdenum

Nickel

Selenium

Silver

Strontium

Thallium

Vanedium

IJgIL

1J91L

1J91L

IJgIL

IJgIL

IJgIL

IJglL

IJglL

IJgIL

IJgIL

jJgL

IJglL

1J9L

IJglL

IJglL

1J91L

IJglL

IJgIL

jJgL

Jl9L_ _

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Not Acceptable

A~tatgt1ft

772

416

350

2350

462

1560

439

534

397

223

1070

843

1930

226

557

1600

366

143

669

966

778

413

347

2360

454

1660

427

541

362

217

1070

754

1860

214

507

1620

361

141

557

619middot932

286 -499

289 - 408

2050 - 2660

386 - 513

1350middot1930

364 - 485

471 - 612

317 - 406

194 - 240

946 - 1210

659 - 845

1670 - 2070

178 - 248

455 - 568

1290 - 1870

310 - 414

121 - 161

450 - 667

__99_1__ ~8-1110

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010821996

EPA 60108 21996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 60108 21996

EPA 6010B 21996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996 -shy

782

402

344 2350

444

1650

416

537

374

219

1080

756

1900

212

505

1590

360

140

555

980

446

211

190

850

202

972

166

224

159

965

495

325

732

103

224

969

203

672

319

446

KSOO021

KSOO021

KSOOO21

KSOOO21

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOOO21

KSoo021

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

EPA 60108 21996 WP204

_- ---- shy1030

1040

1075

jcadmium

[chromium

Lampad

jJglL

jJglL

IJgIL

Acceptable

Acceptable

Acceptable

439

534

843

427

541

754

364 - 485

471 612

659 - 845

EPA 6010C 2000

EPA 6010C 2000

EPA 6010C 2000

416

537

756

166

224

325

KSOOO21

KSOOO21

KSOO021

WP204

WP204

WP204

e All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 Pof13 ~

DMRQA32 Final Report ERA AWaters Company

NPoes Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 middot0706112 City of Nevada WWTP 16517 South 1338 Road Nevad MO 84m 417-448middot2761

Analyte Code Analyte Units Performanu

Evaluation Reported

Value Assigned

Value Acceptance

Lim Method DeSCription Study Mesn

Study Stndard DevIlItion

USEPA Lab Code Study

wp rce Metal (cetil586J Aluminum EPA 2008 55 19981000 KS00021 WP204 iAcceptable 778 782 446IJglL 800 619middot932 Antimony EPA 2008 55 19981005 KSOOO21Acceptable 211 WP204413 402IJglL 404 286middot499 Arsenic EPA 2008 55 19981010 Acceptable 190 KS00021 WP204370 347 289 - 408 3441J91L ~rium1015 EPA 2008 55 1998 850 KSOOO21 WP204Acceptable 2350IJglL 2360 2360 2050 - 2660 Betylhum EPA 2008 55 19981020 WP204KS00021gil Acceptable 444 202431 454 386 - 513 cadmium EPA 2008 55 19981030 KS00021Acceptable 166 WP204gil 416 427 416364 middot485 Chromium EPA 2008 55 19981040 224 KS00021Acceptable 541 537 WP204IJglL 551 471 - 612

Cobah EPA 2008 55 19981050 KS00021 WP204Acceptable 374 159IJglL 377 362 317 - 406

Copper EPA 2008 5519981055 KS00021Acceptable 965 WP204IJglL 221 217 219194middot240 Iron EPA 2008 55 19981070 gIL 1080 495 KS00021 WP204Acceptable 10701040 946 - 1210

ead EPA 2008 5519981075 gIL KSOO021 WP204Acceptable 756 325760 754 659- 845

EPA 2008 55 19981090 ~nese KS00021gIL Acceptable 1900 732 WP2041940 1860 1670middot2070

EPA 2008 55 1998~enum1100 KSOOO21gIL Acceptable 103 WP204213 214 212178middot248 Nickel EPA 2008 5519981105 gIL 224 KSOO021 WP204Acceptable 505512 507 455 - 568

1140 Selenium EPA 2008 55 1998giL 1590 KS00021Acceptable 1620 969 WP2041600 1290middot1870

EPA 2008 551998I 1150 ~lIver KS00021Acceptable WP204322 361 310-414 360 203IJgIL 1165 Thallium EPA 2008 551998 319 KSOO021Acceptable 557 555 WP204538 450middot6671JgL

1185 Vanadium Nol Accepteble EPA 2008 551998 KS00021446 WP204991 980IJglL 1440 868middot1110

EPA 2008 5519981190 Zinc KS00021giL Acceptable 977 462 WP204993 975 _838middot 11~0 - - bull- -~

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 _ of13 ~

DMRQA32 Final Report ERA A Waters Company

NPOES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP SupelVlsor Study Dates 03119112 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 84772 417-448middot2761

Analyta Analyt8Code Unite Performence Reported AIIIUned

Evaluation Value Value Acceplll nee

LImite IiMthod Oeerlpllon

Study USEPALabStudyMn Standard Study DevIation

Code i

WP Trce Metals (Clltti 586J 1000 [Aluminum IlglL Acceptable 800 778 619-932 EPA 8020A 1998 782 446 KSOOO21 WP204 I

1005 [Antimony IlglL Acceptable 404 413 286-499 EPA 8020A 1998 402 211 KSOO021 WP204

1010 iAraenk IlglL Acceptable 370 347 289 - 408 EPA 802011 1998 344 190 KSOOO21 WP204

1015 ~lium 1l91L Acceptable 2360 2360 2050 - 2660 EPA 8020A 1998 2350 850 KS00021 WP204

1020 Seryffium IlgIL Acceptable 431 454 386 - 513 EPA 8020A 1998 444 202 KSOOO21 WP204

1030 ~mium IlgIL Acceptable 416 427 364 - 485 EPA 6020A 1998 416 166 KSOOO21 WP204

1040 Chromium IlQIL Acceptable 551 541 471 - 612 EPA 6020A 1998 537 224 KSOO021 WP204

1050 Cabalaquo IlQIL Acceptable 377 362 317 - 406 EPA 8020A 1998 374 159 KSOOO21 WP204

1055 Copper 1l91L Acceptable 221 217 194middot240 EPA 8020A 1998 219 965 KSOO021 WP204

1070 lroo 1l91L Acceptable 1040 1070 9Mi-1210 EPA 602011 1998 1080 495 KSOOO21 WP204

1075 ~ad IlglL Acceptable 760 754 659 - 845 EPA 6020A 1998 756 325 KSOOO21 WP204

1090 Manganese IlgIL Acceptable 1940 1860 1670 - 2070 EPA 602011 1998 1900 732 KSOO021 WP204

1100 MolytxIenum IlglL Acceptable 213 214 178-248 EPA 6020A 1998 212 103 KSOOO21 WP204

1105 Nickel IlgL Acceptable 512 507 455 - 568 EPA 602011 1998 505 224 KSOOO21 WP204

1140 Selenium IlglL Acceptable 1600 1620 1290 - 1870 EPA 8020A 1998 1590 969 KSOO021 WP204

1150 Silver 1l9L Acceptable 322 361 310 - 414 EPA 8020A 1998 360 203 KSOO021 WP204

1165 Thatlium 1l9L Acceptable 538 557 450 - 667 EPA 8020A 1998 555 319 KSOO021 WP204

1185 Vanadium IlQL Not Acceptable 1440 991 868-1110 EPA 8020A 1998 980 446 KSOO021 WP204

1190 Zinc IJgL Acceptable 993 975 838 -1120 EPA 8020A 1998 977 462 KSOO021 WP204

EPA 2451 3 1994

EPA 747011 1 1994

SM3500Cr 0 18th ED 1992

KS00021 WP204

KS00021 WP204

KSOO021 WP204

All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 13~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 031912 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448~2761

AII~ Code Ane~ Unltll Performnce

evaluation Reported

1Ilue Aalilned

1Ilue ~ptenc

Umltll Method Deecrtptloll Study Men Study

Stanclllrd Oevilltion

USEPA Leb Coda Study

WP Hexvent Chromium (ttl aN) 1045 HellllY81ent Chromium IJQL ---1 Aclteptable 1 580 1 606 1 494 712 1 EPA 7196A 1 19921 6Q4 ~4 I KSOOO21 WP204 J

EPA 1801 2 1993 672 0483 KSOOO21 WP204

SM2130B 18th ED 672 0483 KSOO021 WP2041992

SM21308 online 672 0483 KSOO021 WP204

EPA9012A 0836 00962 KSOO021 WP204

SM4500CN E 18th 0836 00962 KSOO021 WP204ED 1992

SM4500CN E online I 0836 00962 KSOO021 WP204

EPA 4201 1978 0491 0101 KSOO021 WP204

EPA 9066 1986 0491 0101 KSOO021 WP204

SM4500CI E 18th ED I 0850 00673 KSOO021 WP2041992

ISM4500CI E online 0850 00673 KSOO021 WP204

SM4500Ct G 18th ED I 0850 00673 KSOO021 WP2041992

e All analy1es are included in ERAs A2LA accreditation Lab Code 1539middot01 Pag1Oof13

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 03119112 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

Anltya Code Anltya UnMa Performanee

EVlluation Reported

Vllue Anlgned

Vllue Acceptance

Umltll Method Oeecrlptlon Study Meln Study

Satndlrd DevIation

USEPA lab Code

Study

WP Totll Reldulll ChIorlfHIlc 587J 1940 ITotal Residual Chlorine

-shy I mgll I Acceptable I 945 I 0822 I 0594 - 103 LSM4500CI CO onNne I 0850 - 00673 KSOOO21 WP204

ISM4500f~218th EO I 134 159 KSOOO21 WP204

SM4SOOCI E online KSOOO21 WP204

ISM4~~18th Eol 134 159 KSOO021 WP204

SM4500CI G onMne I 134 159 KSOOO21 WP204

CNI Level TDlaI Residual Chlorine

Level T alai Residual Chlorine

Level Total Residual Chlorine

jlglL Acceptable 140 138 780 _198

Ievel TDIal Residual Chlorine

uolL

jlgL

IlnlL

Acceptable 138 138 780 -198

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 P oI

ERA A Waters Company

Study DMRQA-32

NPDES Permit M00089109

Laboratory Name City of Nevada WWTP

It 120113

DMRQA32 Final Report ERA A Waters Company

NPDES Permitll MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dales 031912 middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Analyte rlS End Point Code Performance Repolllld Anlgned evaluation Value Value

Acceptance Method O crlptlonLimite

Study USEPAlIIbStudy StMldard Code

Study DevIatIon

-- -shyDMRQA FathNd minnow (Tut Code 13) (cat WETOO2) 48Hr Acute Non-Renewal 25 C MHSF Poraum chloride

~- IlC50 Acceptable 512 456 I 239 - 674 I EPA 2000 456 109 KSOOO21-(------oP4RQA32

DMRQA Fathead minnow (Test Code 15) (cat WET004) Today Short temI ChroniC Dally Renewal MHSF Potalum chlol1de

0808

0810

0756

IC25 (ON) Growth

NOEC (ON) Growth

NOEC Survival

Acceptable

Acceptable

-- Acceptable

389

25

25

355

250

250

175 - 535

125 - 500

125 - SOO

EPA 1000 2002

EPA 1000 2002

EPA 1000 2002 -shy

355 900 KSOO021

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32

DMRQA Cerlodaphna dubla (Tut Code 19) (cat WETOOB) 48Hr Acute Renewal 25 C MHSF Potlllum chlorlde

[Os ILC50 Acceptable 442 342 I 179middot504 I EPA 2002 342 810 - LIltSOOO21 [ DMRciA3iJ

DMRQA Cerlodflphnla dubla (Tet Code 21) (cat WET010) Today Short term Chronic Dally Renewal MHSF Potlllum chloride

0767

0768

0766

IC25 Raproduction

NOEC ReproductIOn

NOEC Survival -~ -shy

Acceptable

Acceptable

Acceptable

283

25

25

259

250

250

123 - 395

125 - 500

125middot500

EPA 1002 2002

EPA 10022002

EPA 10022002-_ __ __ shy

259 679 KSOOO21

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32shyDMRQA Daphnia pulax (Tet Code 38) (ea WET015) 48Hr Acute Non-Renewal 25 C MHSF Potassium chloride

[0794 ILC50 I Acceptable I 565 525 I 232middot818 I EPA 2021 525 147~r-KSoo021 -r OMRQAi2---]

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 13of13 ~

AWaters Company

Pennittee Name City of Nevada WWTP Pennit Number MOO089109 EPA Lab Code KSOOO21

WET OrganismsITest ConditionsEnd Points Checklist

DMRQA Study 32 La bull Graded Result

Analyte Number Organisms I Conditions End Points Test

Required Acceptable

Not Accepblble (ComtctIYe

Action Required)

Fathead minnow (Test Code 13) 0754 48Hrbull Acute Non-Renewal 25middot C MHSF lC50

EPA 2000 0 lEI 0 Fathead minnow (Test Code 14) 0755 48Hrbull Acute Non-Renewal 25middot C 20 DMW LC50

0 0 0 Fathead minnow (Test Code 15) 0808 7 -day Short Ierm Chronic Daily Renewal MHSF IC25 (ON) Growth

EPA 1000 0 lEI 0 0810 7 -day Short term Chronic Daily Renewal MHSF NOEC (ON) Growth

EPA 1000 0 lEI 0 0756 7-day Short term Chronic Daily Renewal MHSF NOEC Survival

EPA 1000 0 IRI 0 Fathead minnow (Test Code 18) 0812 7 -day Short term Chronic Daily Renewal 20 DMW IC25 (ON) Growth

0 0 0 0814 7-day Short Ierm Chronic Daily Renewal 20 DMW NOEC (ON) Growth

0 0 0 0759 7-day Short term Chronic Daily Renewal 20 DMW NOEC Survival

0 0 0 CerIodaphnle dubla (Test Code 19) 0764 48Hr Acute Renewal 25middot C MHSF LCSO

EPA 2002 0 IXI 0 CerIodaphnla dubla (Test Code 20) 0765 48Hr Acute ReneWal 25- C 20 DMW LCSO

0 0 0 CerIodaphnla dubla (Tast Code 21) 0767

0768

0766

7-day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF

IC25 Reproduction

NOEC Reproduction

NOEC Survival

0

0

IXI

[8]

0

0 EPA 1002 0 lEI 0

CerIodaphnla dubla (Tn Code 22) one 7-day Short term Chronic Daily Renewal 20 DMW IC25 Reproduction

0771 7-day Short term Chronic Daily Renewal 20 DMW NOEC Reproduction 0 0 0

0769 7 -day Short term Chronic Daily Renewal 20 DMW NOEC Survival 0 0 0

0 0 0 Daphnia magna (Test Code 32) 0788 48Hr Acute Non-Renewal 25deg C MHSF LCSO

0 0 0

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report ISlued 072712

WWTP Supervisor Study Dates 0311912 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

AUIyte Code Anayte Units

Performance Evaluation

Reported Value

Alllned Value

Acceptance limits

Method D crlptlon Study Mean Study

Standard Devllltlon

USEPA Lab Code

Study

WP IIlnetl1l CllttI 581

1505

1575

1610

1730

1125

1155

2000

1955

1950

lfJkalinity as CaCm

Chloride

ConductiVity at 2SmiddotC

Fluoride

Potassium

Sodium

Sulfate

Total Dissolved Solids a1180C

Total Solids all0SmiddotC

mgIl

mgIl

Ilmhoscm

mgIl

mgIl

mgIl

mgIl

mgll

mgll

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

460

497

353

150

341

SO5

407

274

262

431

489

368

144

354

SO2

399

246

253

369 -498

414-569

328middot 408

114-174

293middot421

426-577

323middot464

182middot 310

215 - 288

8M23208 1IIIh ED 1992

8M4500CI- E 18th ED 1992

SM2510a 18th ED 1992

EPA 300021 1993

EPA 2007 44 1994

EPA 2007 441994

EPA 3000 21 1993

SM2540C 18th ED 1992

SM2540B 18th ED 1992

436

494

368

142

349

503

396

246

254

208

215

864

00992

188

252

206

145

167

KSOOO21

KSOOO21

KSOOO21

KSOOO21

KSOOO21

KSOOO21

KSOOO21

KSOOO21

KSOOO21

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP 1I11Ift (Cllttl581 1505 Alkalinity as CaC 03 mglL Acceptable 460 431 369 - 498 SM2320B online 436 208 KSOOO21 WP204

1575 ~hloride mglL Acceptable 497 489 414 - 569 SM4500CI- Eonline 494 215 KSOOO21 WP204

1610 ~onductlvlty at 2SC ~mhoslcm Acceptable 353 368 328middot408 SM2510B online 368 864 KSOOO21 WP204

1730 Fluoride mglL Acceptable 150 144 114-174 EPA 9056 1994 142 00992 KSOOO21 WP204

1125 Potauium mgL Acceptable 34 354 293-421 EPA6010B 21996 349 188 KSOOO21 WP204

1155 Sodium mgL Acceptable 505 502 426middot577 EPA 6010B 1 1996 503 252 KSOOO21 WP204

2000 Sulfate mgL Acceptable 407 399 323 - 464 EPA 9056 1994 396 206 KSOOO21 WP204

1955 iTotal Dissolved Solids aI180C mgL Acceptable 274 246 182 - 310 SM2540C online 246 145 KSOO021 WP204

1950 Irotal Solklut lOSC shy ~IL_ Accetable 262 253 215middot288 SM2540B online 254 167 KSOOO21 WP204

mgJL EPA 3000 21 1993 KSO0021 WP204

IJmhoscm EPA 9050A 1 1996 KSO0021 WP204

bull All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 _20113 ~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 072712

WWTP Supervisor Study Dates 0311912 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-44a-2761

AIllIyte Code

Analyle Unlt$ Performance Evaluation

Reported Value

Aulgned Value

Aeptance Umlb

Method Ducriptlon Study Mean Study

Standard Deviation

USEPALab Code

Study

WP MlnetII (ca 51111 1575 EhIoride mgll Acceptable 482 489 414 - 569 EPA 9056 1994 494 215 KSOOO21 WP204

WP Hrd (cttI 580

1960

1035

1085

1550

1755

lion-Filterable Residue (TSS)

Calcium

Magnesium

Clkium Hardneas as CaCD3

olal Hardneaa as CaC03

mgIl

mgIl

mgIl

mgIl

mgIl

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

440

448

105

112

155

439

448

103

112

154

334 - 508

399middot509

876-118

998 127

136 - 176

S12540D 18th ED 1992

EPA 2007 44 1994

EPA 2007 441994

EPA 2007 44 1994

EPA 200744 1994

428

449

104

113

155

276

200

0622

472

574

KSOOO21

KS00021

KS00021

KSOOO21

KSOOO21

WP204

WP204

WP204

WP204

WP204 I

~ _ _ ___ __n ___

1960

1035

1085

1550

1755

Non-Filterable Residue (TSS)

plclum

Magnesium

Clkium HlIIdneas 88 CaC03

Tolal Hardness as CeC03

mgIl

mgIl

mgl

mgL

mgl

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

440

44B

105

112

155

439

448

103

112

154

334middot508

399middot509

876-118

998 - 127

136-176

SM2540D online

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

428

449

104

113

155

276

200

0622

472

574

KSOOO21

KS00021

KS00021

KSOOO21

KSOOO21

WP204

WP204

WP204

WP204

WP204

_ _ --- -_ --shy1550

1755

plcium Hardness as CaC03

Total Hardness as CaC03 --shy -shy

mgl

mgl --shy _ _shy

Acceptable

Acceptable

112

155

112

154

998 127

136middot176 --shy

SM2340B 18th ED 1992

SM2340B 18th ED 1992

113

155

472

574

KSOOO21

KS00021

WP204

WP204

All anafytes are included in ERAs A2LA accreditation lab Code 1539-01 I

SM2340B online WP204

SM2340B online WP204

SM2540D 21st ED DMRQA322005

SM4500H B 18th ED WP2041992

ot13 ~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 07127112

WWTP Supervisor Study Dates 03119112middot07106112 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Anatyte Coct AnaIyW Unit Performance

EV1Iluatlon Reported

Value Aliligned

Value Acceptance

Limits Method Deacrlpllon Study n

Study Stllndllrd DevIation

USEPALab Code

Study

WP pH caft 5711

1900 jpH SU Acceptable 633 631 611middot651 SM4500H+ a online 629 00470 KSOOO21 WP204

WPSlmpjbull Nutrients (caft 584)

1515 Ammoniaaa N

1820 Nitrate + Nitrite as N

1810 Nitrate as N

1870 jor1ho-Phosphate as P

su

SU

SU

mLlL

mUL

mgl

mgl

mgll

mgll

mgIl

I Acceetable 633 631

Acceptable 633 631

Acceptable 731 723

Acceptable 330 279

Acceptable 330 279

Acceptable 514 529

Acceptable 121 109

Acceptable 426 435

Acceptable 426 435

Acceptable 394 40l~

I 611 - 651 I EPA 9040621995 I

611 bull 651 I EPA 9040C 2002 I 703743 ISM4500~~ 21s1 ED

I 227 - 355 SM2540F 18th ED 1992

I 227middot355 SM2540F online

I 385 _ 6 75 ISM4500NH3 021st ED 2005

808 -136

354middot507

339 - 526

337 - 484

EPA 3501 2 1993

EPA 3532 2 1993

EPA 3532 2 1993

EPA365121993

629 00470

629 00470

727 00644

298 230

298 230

530 0467

110 0839

431 0214

431 0212

412 0204

KSOOO21

KSOOO21

MOOO982

KSOOO21

KSOOO21

MOOO982

KSOOO21

KSOOO21

KSOOO21

KSOOO21

WP204

WP204

OMRQA32

WP204

WP204

OMRQA32

WP204

WP204

WP204

WP204

EPA 3000 21 1993 KS00021

EPA 3000 21 1993 KS00021

EPA 3512 21993 KSOOO21 EPA 3654 1974 KSO0021

All analytes are included in ERAs A2LA accreditation Lab Code 1539-01

WP204

WP204

WP204

WP204

13 ~_

---

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 072712

WWTP Supervisor Study Dates 0311912middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Al1IIiyte Code

Anltyte Units Perforll1llnCll Evaluation

Reported Valul

Asalgned Value

Ac~ptanc Llmltll Mlthod D bullbullcrlpllon Study MIn

Study Sblndard DevIation

USEPAub Code Study

DIIRQA Demand (ClIf1 57aJ

1530 roo mgll Acceptable 815 904 457-135 514521082111 ED 2005

913 168 MOOO982 DMRQA32

_

EPA 3532 2 1993 KSO0021 WP204

EPA 3000 21 1993 KSOOO21 WP204

EPA 9056 1994 KS00021 WP204

r _ __

1530

1555

1565

IBOD

C800

COD

mgIl

mgll

mgIl

Acceptable

Acceptable

Acceptable

322

259

529

323

279

521

161 - 466

125 - 433

353 - 646

5M5210B 18th ED 1992

51452108 18th ED 1992

514522001811 ED 1992

319

295

519

530

490

542

KSOO021

KSOO021

KSOO021

WP204

WP204

WP204

WP Demand leaf1 571) 5M5210B online KSOO0211530 soo 319 530Acceptable 322 323 161 - 486 WP204mgll 5M5210B online KSOO021279 125middot433 295 490 WP2041555 Feoo mgl Acceptable 259

51452200 online KSOO021519 542 WP2041565 icoo Acceptable 521 353 - 648 mgll 529

EPA 4104 2 1993 KSOO021 WP204

EPA 1664A 1999 KSOO021 WP204

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 ~

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 - 0706112 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

AlUliyW Code

Anetytw Unlta Performance Evaluation

Reported Valua

Aaalgned Value

ACQplence Llmlta

Method DelCription Study Mean Study

Standard Deviation

USEPA Lab Code Study

WP TlIICe Metallea 586j

1000 AlUminum J91L Acceptable 772 778 619middot932 EPA 2007441994 782 446 KSOOO21 WP204

1005 Anllmony JgL Acceptable 416 413 286 - 499 EPA 2007 441994 402 211 KSOO021 WP204

1010 Araenic Jgl Acceptable 350 347 289 - 408 EPA 2007 441994 344 190 KSOOO21 WP204

1015 Barium JgL Acceptable 2350 2360 2050 - 2660 EPA 2007441994 2350 850 KSOOO21 WP204

1020 ~elytijum J91L Acceptable 462 454 386 - 513 EPA 2007 44 1994 444 202 KSOOO21 WP204

1025 BClron J91L Acceptable 1560 1660 1350 - 1930 EPA 2007 44 1994 1650 972 KSOO021 WP204

1030 centadmlum J9l Acceptable 439 427 364 -485 EPA 2007 44 1994 416 166 KSOOO21 WP204

1040 Chromium J91L Acceptable 534 541 471 - 612 EPA 2007 441994 537 224 KSOOO21 WP204

1050 Cobalt JglL Acceptable 397 362 317-406 EPA 2007 44 1994 374 159 KSOOO21 WP204

1055 Copper JgIL Acceptable 223 217 194 - 240 EPA 2007 441994 219 965 KSOOO21 WP204

1070 Iron JgIL Acceptable 1070 1070 946 - 1210 EPA 200744 1994 1080 495 KSOOO21 WP204

1075 Lead J9IL Acceptable 843 754 659middot845 EPA 2007 441994 756 325 KS00021 WP204

1090 ~nese 1J91L Acceptable 1930 1860 1670 - 2070 EPA 2007 441994 1900 732 KSOOO21 WP204

1100 Molybdenum JglL Acceptable 226 214 178 - 248 EPA 2007 44 1994 212 103 KSOOO21 WP204

1105 Nlckal Jell Acceptable 557 507 455 - 568 EPA 2007 44 1994 505 224 KSOOO21 WP204

1140 Selenium Jgl Acceptable 1600 1620 1290middot 1870 EPA 200144 1994 1590 969 KSOOO21 WP204

1150 SiMlr IJgL Acceptable 366 361 310 -414 EPA 2001 441994 360 203 KSOOO21 WP204

1160 Strontium 1JgL Acceptable 143 141 121 - 161 EPA 2001 44 1994 140 672 KSOOO21 WP204

1165 Thallium J9IL Not Acceptable 669 557 450 - 667 EPA 20074 41994 555 319 KSOOO21 WP204

1185 Vanadium JgL Acceptable 966 991 868-1110 EPA 200744 1994 980 446 KSOOO21 WP204

EPA 2007 44 1994 WP204

All analytes are included in ERAs A2LA accreditation Lab Gode 1539-01 _ of13 ~II

DMRQA32 Final Report ERA AWaters Company

NPoes Permit MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Illued 072712

WWTP Supervisor Study Dates 031912 middot070612 City of Neyada WWTP 16517 South 1338 Road Neyada MO 64772 417-448middot2761

Analyte Code

Analyte Unttll Performance Evaluation

Reported Value

Assigned Vllue

Accaptllnca Limb

Method DseMptlon Study Mean Study

Standard Devtatlon

USEPAub Code

Study

WP TRee _1 (calf 58B)

1000

1005

1010

1015

1020

1025

1030

1040

1050

1055

1070

1075

1090

1100

1105

1140

1150

1160

1165

1185

Aluminum

Antimony

Anlenic

Barium

Beryl~um

~on Cadmium

Chromium

Cobalt

Copper

Iron

fLead Manganese

Molybdenum

Nickel

Selenium

Silver

Strontium

Thallium

Vanedium

IJgIL

1J91L

1J91L

IJgIL

IJgIL

IJgIL

IJglL

IJglL

IJgIL

IJgIL

jJgL

IJglL

1J9L

IJglL

IJglL

1J91L

IJglL

IJgIL

jJgL

Jl9L_ _

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Not Acceptable

A~tatgt1ft

772

416

350

2350

462

1560

439

534

397

223

1070

843

1930

226

557

1600

366

143

669

966

778

413

347

2360

454

1660

427

541

362

217

1070

754

1860

214

507

1620

361

141

557

619middot932

286 -499

289 - 408

2050 - 2660

386 - 513

1350middot1930

364 - 485

471 - 612

317 - 406

194 - 240

946 - 1210

659 - 845

1670 - 2070

178 - 248

455 - 568

1290 - 1870

310 - 414

121 - 161

450 - 667

__99_1__ ~8-1110

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010821996

EPA 60108 21996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 60108 21996

EPA 6010B 21996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996 -shy

782

402

344 2350

444

1650

416

537

374

219

1080

756

1900

212

505

1590

360

140

555

980

446

211

190

850

202

972

166

224

159

965

495

325

732

103

224

969

203

672

319

446

KSOO021

KSOO021

KSOOO21

KSOOO21

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOOO21

KSoo021

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

EPA 60108 21996 WP204

_- ---- shy1030

1040

1075

jcadmium

[chromium

Lampad

jJglL

jJglL

IJgIL

Acceptable

Acceptable

Acceptable

439

534

843

427

541

754

364 - 485

471 612

659 - 845

EPA 6010C 2000

EPA 6010C 2000

EPA 6010C 2000

416

537

756

166

224

325

KSOOO21

KSOOO21

KSOO021

WP204

WP204

WP204

e All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 Pof13 ~

DMRQA32 Final Report ERA AWaters Company

NPoes Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 middot0706112 City of Nevada WWTP 16517 South 1338 Road Nevad MO 84m 417-448middot2761

Analyte Code Analyte Units Performanu

Evaluation Reported

Value Assigned

Value Acceptance

Lim Method DeSCription Study Mesn

Study Stndard DevIlItion

USEPA Lab Code Study

wp rce Metal (cetil586J Aluminum EPA 2008 55 19981000 KS00021 WP204 iAcceptable 778 782 446IJglL 800 619middot932 Antimony EPA 2008 55 19981005 KSOOO21Acceptable 211 WP204413 402IJglL 404 286middot499 Arsenic EPA 2008 55 19981010 Acceptable 190 KS00021 WP204370 347 289 - 408 3441J91L ~rium1015 EPA 2008 55 1998 850 KSOOO21 WP204Acceptable 2350IJglL 2360 2360 2050 - 2660 Betylhum EPA 2008 55 19981020 WP204KS00021gil Acceptable 444 202431 454 386 - 513 cadmium EPA 2008 55 19981030 KS00021Acceptable 166 WP204gil 416 427 416364 middot485 Chromium EPA 2008 55 19981040 224 KS00021Acceptable 541 537 WP204IJglL 551 471 - 612

Cobah EPA 2008 55 19981050 KS00021 WP204Acceptable 374 159IJglL 377 362 317 - 406

Copper EPA 2008 5519981055 KS00021Acceptable 965 WP204IJglL 221 217 219194middot240 Iron EPA 2008 55 19981070 gIL 1080 495 KS00021 WP204Acceptable 10701040 946 - 1210

ead EPA 2008 5519981075 gIL KSOO021 WP204Acceptable 756 325760 754 659- 845

EPA 2008 55 19981090 ~nese KS00021gIL Acceptable 1900 732 WP2041940 1860 1670middot2070

EPA 2008 55 1998~enum1100 KSOOO21gIL Acceptable 103 WP204213 214 212178middot248 Nickel EPA 2008 5519981105 gIL 224 KSOO021 WP204Acceptable 505512 507 455 - 568

1140 Selenium EPA 2008 55 1998giL 1590 KS00021Acceptable 1620 969 WP2041600 1290middot1870

EPA 2008 551998I 1150 ~lIver KS00021Acceptable WP204322 361 310-414 360 203IJgIL 1165 Thallium EPA 2008 551998 319 KSOO021Acceptable 557 555 WP204538 450middot6671JgL

1185 Vanadium Nol Accepteble EPA 2008 551998 KS00021446 WP204991 980IJglL 1440 868middot1110

EPA 2008 5519981190 Zinc KS00021giL Acceptable 977 462 WP204993 975 _838middot 11~0 - - bull- -~

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 _ of13 ~

DMRQA32 Final Report ERA A Waters Company

NPOES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP SupelVlsor Study Dates 03119112 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 84772 417-448middot2761

Analyta Analyt8Code Unite Performence Reported AIIIUned

Evaluation Value Value Acceplll nee

LImite IiMthod Oeerlpllon

Study USEPALabStudyMn Standard Study DevIation

Code i

WP Trce Metals (Clltti 586J 1000 [Aluminum IlglL Acceptable 800 778 619-932 EPA 8020A 1998 782 446 KSOOO21 WP204 I

1005 [Antimony IlglL Acceptable 404 413 286-499 EPA 8020A 1998 402 211 KSOO021 WP204

1010 iAraenk IlglL Acceptable 370 347 289 - 408 EPA 802011 1998 344 190 KSOOO21 WP204

1015 ~lium 1l91L Acceptable 2360 2360 2050 - 2660 EPA 8020A 1998 2350 850 KS00021 WP204

1020 Seryffium IlgIL Acceptable 431 454 386 - 513 EPA 8020A 1998 444 202 KSOOO21 WP204

1030 ~mium IlgIL Acceptable 416 427 364 - 485 EPA 6020A 1998 416 166 KSOOO21 WP204

1040 Chromium IlQIL Acceptable 551 541 471 - 612 EPA 6020A 1998 537 224 KSOO021 WP204

1050 Cabalaquo IlQIL Acceptable 377 362 317 - 406 EPA 8020A 1998 374 159 KSOOO21 WP204

1055 Copper 1l91L Acceptable 221 217 194middot240 EPA 8020A 1998 219 965 KSOO021 WP204

1070 lroo 1l91L Acceptable 1040 1070 9Mi-1210 EPA 602011 1998 1080 495 KSOOO21 WP204

1075 ~ad IlglL Acceptable 760 754 659 - 845 EPA 6020A 1998 756 325 KSOOO21 WP204

1090 Manganese IlgIL Acceptable 1940 1860 1670 - 2070 EPA 602011 1998 1900 732 KSOO021 WP204

1100 MolytxIenum IlglL Acceptable 213 214 178-248 EPA 6020A 1998 212 103 KSOOO21 WP204

1105 Nickel IlgL Acceptable 512 507 455 - 568 EPA 602011 1998 505 224 KSOOO21 WP204

1140 Selenium IlglL Acceptable 1600 1620 1290 - 1870 EPA 8020A 1998 1590 969 KSOO021 WP204

1150 Silver 1l9L Acceptable 322 361 310 - 414 EPA 8020A 1998 360 203 KSOO021 WP204

1165 Thatlium 1l9L Acceptable 538 557 450 - 667 EPA 8020A 1998 555 319 KSOO021 WP204

1185 Vanadium IlQL Not Acceptable 1440 991 868-1110 EPA 8020A 1998 980 446 KSOO021 WP204

1190 Zinc IJgL Acceptable 993 975 838 -1120 EPA 8020A 1998 977 462 KSOO021 WP204

EPA 2451 3 1994

EPA 747011 1 1994

SM3500Cr 0 18th ED 1992

KS00021 WP204

KS00021 WP204

KSOO021 WP204

All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 13~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 031912 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448~2761

AII~ Code Ane~ Unltll Performnce

evaluation Reported

1Ilue Aalilned

1Ilue ~ptenc

Umltll Method Deecrtptloll Study Men Study

Stanclllrd Oevilltion

USEPA Leb Coda Study

WP Hexvent Chromium (ttl aN) 1045 HellllY81ent Chromium IJQL ---1 Aclteptable 1 580 1 606 1 494 712 1 EPA 7196A 1 19921 6Q4 ~4 I KSOOO21 WP204 J

EPA 1801 2 1993 672 0483 KSOOO21 WP204

SM2130B 18th ED 672 0483 KSOO021 WP2041992

SM21308 online 672 0483 KSOO021 WP204

EPA9012A 0836 00962 KSOO021 WP204

SM4500CN E 18th 0836 00962 KSOO021 WP204ED 1992

SM4500CN E online I 0836 00962 KSOO021 WP204

EPA 4201 1978 0491 0101 KSOO021 WP204

EPA 9066 1986 0491 0101 KSOO021 WP204

SM4500CI E 18th ED I 0850 00673 KSOO021 WP2041992

ISM4500CI E online 0850 00673 KSOO021 WP204

SM4500Ct G 18th ED I 0850 00673 KSOO021 WP2041992

e All analy1es are included in ERAs A2LA accreditation Lab Code 1539middot01 Pag1Oof13

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 03119112 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

Anltya Code Anltya UnMa Performanee

EVlluation Reported

Vllue Anlgned

Vllue Acceptance

Umltll Method Oeecrlptlon Study Meln Study

Satndlrd DevIation

USEPA lab Code

Study

WP Totll Reldulll ChIorlfHIlc 587J 1940 ITotal Residual Chlorine

-shy I mgll I Acceptable I 945 I 0822 I 0594 - 103 LSM4500CI CO onNne I 0850 - 00673 KSOOO21 WP204

ISM4500f~218th EO I 134 159 KSOOO21 WP204

SM4SOOCI E online KSOOO21 WP204

ISM4~~18th Eol 134 159 KSOO021 WP204

SM4500CI G onMne I 134 159 KSOOO21 WP204

CNI Level TDlaI Residual Chlorine

Level T alai Residual Chlorine

Level Total Residual Chlorine

jlglL Acceptable 140 138 780 _198

Ievel TDIal Residual Chlorine

uolL

jlgL

IlnlL

Acceptable 138 138 780 -198

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 P oI

ERA A Waters Company

Study DMRQA-32

NPDES Permit M00089109

Laboratory Name City of Nevada WWTP

It 120113

DMRQA32 Final Report ERA A Waters Company

NPDES Permitll MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dales 031912 middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Analyte rlS End Point Code Performance Repolllld Anlgned evaluation Value Value

Acceptance Method O crlptlonLimite

Study USEPAlIIbStudy StMldard Code

Study DevIatIon

-- -shyDMRQA FathNd minnow (Tut Code 13) (cat WETOO2) 48Hr Acute Non-Renewal 25 C MHSF Poraum chloride

~- IlC50 Acceptable 512 456 I 239 - 674 I EPA 2000 456 109 KSOOO21-(------oP4RQA32

DMRQA Fathead minnow (Test Code 15) (cat WET004) Today Short temI ChroniC Dally Renewal MHSF Potalum chlol1de

0808

0810

0756

IC25 (ON) Growth

NOEC (ON) Growth

NOEC Survival

Acceptable

Acceptable

-- Acceptable

389

25

25

355

250

250

175 - 535

125 - 500

125 - SOO

EPA 1000 2002

EPA 1000 2002

EPA 1000 2002 -shy

355 900 KSOO021

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32

DMRQA Cerlodaphna dubla (Tut Code 19) (cat WETOOB) 48Hr Acute Renewal 25 C MHSF Potlllum chlorlde

[Os ILC50 Acceptable 442 342 I 179middot504 I EPA 2002 342 810 - LIltSOOO21 [ DMRciA3iJ

DMRQA Cerlodflphnla dubla (Tet Code 21) (cat WET010) Today Short term Chronic Dally Renewal MHSF Potlllum chloride

0767

0768

0766

IC25 Raproduction

NOEC ReproductIOn

NOEC Survival -~ -shy

Acceptable

Acceptable

Acceptable

283

25

25

259

250

250

123 - 395

125 - 500

125middot500

EPA 1002 2002

EPA 10022002

EPA 10022002-_ __ __ shy

259 679 KSOOO21

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32shyDMRQA Daphnia pulax (Tet Code 38) (ea WET015) 48Hr Acute Non-Renewal 25 C MHSF Potassium chloride

[0794 ILC50 I Acceptable I 565 525 I 232middot818 I EPA 2021 525 147~r-KSoo021 -r OMRQAi2---]

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 13of13 ~

AWaters Company

Pennittee Name City of Nevada WWTP Pennit Number MOO089109 EPA Lab Code KSOOO21

WET OrganismsITest ConditionsEnd Points Checklist

DMRQA Study 32 La bull Graded Result

Analyte Number Organisms I Conditions End Points Test

Required Acceptable

Not Accepblble (ComtctIYe

Action Required)

Fathead minnow (Test Code 13) 0754 48Hrbull Acute Non-Renewal 25middot C MHSF lC50

EPA 2000 0 lEI 0 Fathead minnow (Test Code 14) 0755 48Hrbull Acute Non-Renewal 25middot C 20 DMW LC50

0 0 0 Fathead minnow (Test Code 15) 0808 7 -day Short Ierm Chronic Daily Renewal MHSF IC25 (ON) Growth

EPA 1000 0 lEI 0 0810 7 -day Short term Chronic Daily Renewal MHSF NOEC (ON) Growth

EPA 1000 0 lEI 0 0756 7-day Short term Chronic Daily Renewal MHSF NOEC Survival

EPA 1000 0 IRI 0 Fathead minnow (Test Code 18) 0812 7 -day Short term Chronic Daily Renewal 20 DMW IC25 (ON) Growth

0 0 0 0814 7-day Short Ierm Chronic Daily Renewal 20 DMW NOEC (ON) Growth

0 0 0 0759 7-day Short term Chronic Daily Renewal 20 DMW NOEC Survival

0 0 0 CerIodaphnle dubla (Test Code 19) 0764 48Hr Acute Renewal 25middot C MHSF LCSO

EPA 2002 0 IXI 0 CerIodaphnla dubla (Test Code 20) 0765 48Hr Acute ReneWal 25- C 20 DMW LCSO

0 0 0 CerIodaphnla dubla (Tast Code 21) 0767

0768

0766

7-day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF

IC25 Reproduction

NOEC Reproduction

NOEC Survival

0

0

IXI

[8]

0

0 EPA 1002 0 lEI 0

CerIodaphnla dubla (Tn Code 22) one 7-day Short term Chronic Daily Renewal 20 DMW IC25 Reproduction

0771 7-day Short term Chronic Daily Renewal 20 DMW NOEC Reproduction 0 0 0

0769 7 -day Short term Chronic Daily Renewal 20 DMW NOEC Survival 0 0 0

0 0 0 Daphnia magna (Test Code 32) 0788 48Hr Acute Non-Renewal 25deg C MHSF LCSO

0 0 0

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 072712

WWTP Supervisor Study Dates 0311912 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-44a-2761

AIllIyte Code

Analyle Unlt$ Performance Evaluation

Reported Value

Aulgned Value

Aeptance Umlb

Method Ducriptlon Study Mean Study

Standard Deviation

USEPALab Code

Study

WP MlnetII (ca 51111 1575 EhIoride mgll Acceptable 482 489 414 - 569 EPA 9056 1994 494 215 KSOOO21 WP204

WP Hrd (cttI 580

1960

1035

1085

1550

1755

lion-Filterable Residue (TSS)

Calcium

Magnesium

Clkium Hardneas as CaCD3

olal Hardneaa as CaC03

mgIl

mgIl

mgIl

mgIl

mgIl

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

440

448

105

112

155

439

448

103

112

154

334 - 508

399middot509

876-118

998 127

136 - 176

S12540D 18th ED 1992

EPA 2007 44 1994

EPA 2007 441994

EPA 2007 44 1994

EPA 200744 1994

428

449

104

113

155

276

200

0622

472

574

KSOOO21

KS00021

KS00021

KSOOO21

KSOOO21

WP204

WP204

WP204

WP204

WP204 I

~ _ _ ___ __n ___

1960

1035

1085

1550

1755

Non-Filterable Residue (TSS)

plclum

Magnesium

Clkium HlIIdneas 88 CaC03

Tolal Hardness as CeC03

mgIl

mgIl

mgl

mgL

mgl

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

440

44B

105

112

155

439

448

103

112

154

334middot508

399middot509

876-118

998 - 127

136-176

SM2540D online

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

428

449

104

113

155

276

200

0622

472

574

KSOOO21

KS00021

KS00021

KSOOO21

KSOOO21

WP204

WP204

WP204

WP204

WP204

_ _ --- -_ --shy1550

1755

plcium Hardness as CaC03

Total Hardness as CaC03 --shy -shy

mgl

mgl --shy _ _shy

Acceptable

Acceptable

112

155

112

154

998 127

136middot176 --shy

SM2340B 18th ED 1992

SM2340B 18th ED 1992

113

155

472

574

KSOOO21

KS00021

WP204

WP204

All anafytes are included in ERAs A2LA accreditation lab Code 1539-01 I

SM2340B online WP204

SM2340B online WP204

SM2540D 21st ED DMRQA322005

SM4500H B 18th ED WP2041992

ot13 ~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 07127112

WWTP Supervisor Study Dates 03119112middot07106112 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Anatyte Coct AnaIyW Unit Performance

EV1Iluatlon Reported

Value Aliligned

Value Acceptance

Limits Method Deacrlpllon Study n

Study Stllndllrd DevIation

USEPALab Code

Study

WP pH caft 5711

1900 jpH SU Acceptable 633 631 611middot651 SM4500H+ a online 629 00470 KSOOO21 WP204

WPSlmpjbull Nutrients (caft 584)

1515 Ammoniaaa N

1820 Nitrate + Nitrite as N

1810 Nitrate as N

1870 jor1ho-Phosphate as P

su

SU

SU

mLlL

mUL

mgl

mgl

mgll

mgll

mgIl

I Acceetable 633 631

Acceptable 633 631

Acceptable 731 723

Acceptable 330 279

Acceptable 330 279

Acceptable 514 529

Acceptable 121 109

Acceptable 426 435

Acceptable 426 435

Acceptable 394 40l~

I 611 - 651 I EPA 9040621995 I

611 bull 651 I EPA 9040C 2002 I 703743 ISM4500~~ 21s1 ED

I 227 - 355 SM2540F 18th ED 1992

I 227middot355 SM2540F online

I 385 _ 6 75 ISM4500NH3 021st ED 2005

808 -136

354middot507

339 - 526

337 - 484

EPA 3501 2 1993

EPA 3532 2 1993

EPA 3532 2 1993

EPA365121993

629 00470

629 00470

727 00644

298 230

298 230

530 0467

110 0839

431 0214

431 0212

412 0204

KSOOO21

KSOOO21

MOOO982

KSOOO21

KSOOO21

MOOO982

KSOOO21

KSOOO21

KSOOO21

KSOOO21

WP204

WP204

OMRQA32

WP204

WP204

OMRQA32

WP204

WP204

WP204

WP204

EPA 3000 21 1993 KS00021

EPA 3000 21 1993 KS00021

EPA 3512 21993 KSOOO21 EPA 3654 1974 KSO0021

All analytes are included in ERAs A2LA accreditation Lab Code 1539-01

WP204

WP204

WP204

WP204

13 ~_

---

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 072712

WWTP Supervisor Study Dates 0311912middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Al1IIiyte Code

Anltyte Units Perforll1llnCll Evaluation

Reported Valul

Asalgned Value

Ac~ptanc Llmltll Mlthod D bullbullcrlpllon Study MIn

Study Sblndard DevIation

USEPAub Code Study

DIIRQA Demand (ClIf1 57aJ

1530 roo mgll Acceptable 815 904 457-135 514521082111 ED 2005

913 168 MOOO982 DMRQA32

_

EPA 3532 2 1993 KSO0021 WP204

EPA 3000 21 1993 KSOOO21 WP204

EPA 9056 1994 KS00021 WP204

r _ __

1530

1555

1565

IBOD

C800

COD

mgIl

mgll

mgIl

Acceptable

Acceptable

Acceptable

322

259

529

323

279

521

161 - 466

125 - 433

353 - 646

5M5210B 18th ED 1992

51452108 18th ED 1992

514522001811 ED 1992

319

295

519

530

490

542

KSOO021

KSOO021

KSOO021

WP204

WP204

WP204

WP Demand leaf1 571) 5M5210B online KSOO0211530 soo 319 530Acceptable 322 323 161 - 486 WP204mgll 5M5210B online KSOO021279 125middot433 295 490 WP2041555 Feoo mgl Acceptable 259

51452200 online KSOO021519 542 WP2041565 icoo Acceptable 521 353 - 648 mgll 529

EPA 4104 2 1993 KSOO021 WP204

EPA 1664A 1999 KSOO021 WP204

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 ~

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 - 0706112 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

AlUliyW Code

Anetytw Unlta Performance Evaluation

Reported Valua

Aaalgned Value

ACQplence Llmlta

Method DelCription Study Mean Study

Standard Deviation

USEPA Lab Code Study

WP TlIICe Metallea 586j

1000 AlUminum J91L Acceptable 772 778 619middot932 EPA 2007441994 782 446 KSOOO21 WP204

1005 Anllmony JgL Acceptable 416 413 286 - 499 EPA 2007 441994 402 211 KSOO021 WP204

1010 Araenic Jgl Acceptable 350 347 289 - 408 EPA 2007 441994 344 190 KSOOO21 WP204

1015 Barium JgL Acceptable 2350 2360 2050 - 2660 EPA 2007441994 2350 850 KSOOO21 WP204

1020 ~elytijum J91L Acceptable 462 454 386 - 513 EPA 2007 44 1994 444 202 KSOOO21 WP204

1025 BClron J91L Acceptable 1560 1660 1350 - 1930 EPA 2007 44 1994 1650 972 KSOO021 WP204

1030 centadmlum J9l Acceptable 439 427 364 -485 EPA 2007 44 1994 416 166 KSOOO21 WP204

1040 Chromium J91L Acceptable 534 541 471 - 612 EPA 2007 441994 537 224 KSOOO21 WP204

1050 Cobalt JglL Acceptable 397 362 317-406 EPA 2007 44 1994 374 159 KSOOO21 WP204

1055 Copper JgIL Acceptable 223 217 194 - 240 EPA 2007 441994 219 965 KSOOO21 WP204

1070 Iron JgIL Acceptable 1070 1070 946 - 1210 EPA 200744 1994 1080 495 KSOOO21 WP204

1075 Lead J9IL Acceptable 843 754 659middot845 EPA 2007 441994 756 325 KS00021 WP204

1090 ~nese 1J91L Acceptable 1930 1860 1670 - 2070 EPA 2007 441994 1900 732 KSOOO21 WP204

1100 Molybdenum JglL Acceptable 226 214 178 - 248 EPA 2007 44 1994 212 103 KSOOO21 WP204

1105 Nlckal Jell Acceptable 557 507 455 - 568 EPA 2007 44 1994 505 224 KSOOO21 WP204

1140 Selenium Jgl Acceptable 1600 1620 1290middot 1870 EPA 200144 1994 1590 969 KSOOO21 WP204

1150 SiMlr IJgL Acceptable 366 361 310 -414 EPA 2001 441994 360 203 KSOOO21 WP204

1160 Strontium 1JgL Acceptable 143 141 121 - 161 EPA 2001 44 1994 140 672 KSOOO21 WP204

1165 Thallium J9IL Not Acceptable 669 557 450 - 667 EPA 20074 41994 555 319 KSOOO21 WP204

1185 Vanadium JgL Acceptable 966 991 868-1110 EPA 200744 1994 980 446 KSOOO21 WP204

EPA 2007 44 1994 WP204

All analytes are included in ERAs A2LA accreditation Lab Gode 1539-01 _ of13 ~II

DMRQA32 Final Report ERA AWaters Company

NPoes Permit MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Illued 072712

WWTP Supervisor Study Dates 031912 middot070612 City of Neyada WWTP 16517 South 1338 Road Neyada MO 64772 417-448middot2761

Analyte Code

Analyte Unttll Performance Evaluation

Reported Value

Assigned Vllue

Accaptllnca Limb

Method DseMptlon Study Mean Study

Standard Devtatlon

USEPAub Code

Study

WP TRee _1 (calf 58B)

1000

1005

1010

1015

1020

1025

1030

1040

1050

1055

1070

1075

1090

1100

1105

1140

1150

1160

1165

1185

Aluminum

Antimony

Anlenic

Barium

Beryl~um

~on Cadmium

Chromium

Cobalt

Copper

Iron

fLead Manganese

Molybdenum

Nickel

Selenium

Silver

Strontium

Thallium

Vanedium

IJgIL

1J91L

1J91L

IJgIL

IJgIL

IJgIL

IJglL

IJglL

IJgIL

IJgIL

jJgL

IJglL

1J9L

IJglL

IJglL

1J91L

IJglL

IJgIL

jJgL

Jl9L_ _

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Not Acceptable

A~tatgt1ft

772

416

350

2350

462

1560

439

534

397

223

1070

843

1930

226

557

1600

366

143

669

966

778

413

347

2360

454

1660

427

541

362

217

1070

754

1860

214

507

1620

361

141

557

619middot932

286 -499

289 - 408

2050 - 2660

386 - 513

1350middot1930

364 - 485

471 - 612

317 - 406

194 - 240

946 - 1210

659 - 845

1670 - 2070

178 - 248

455 - 568

1290 - 1870

310 - 414

121 - 161

450 - 667

__99_1__ ~8-1110

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010821996

EPA 60108 21996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 60108 21996

EPA 6010B 21996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996 -shy

782

402

344 2350

444

1650

416

537

374

219

1080

756

1900

212

505

1590

360

140

555

980

446

211

190

850

202

972

166

224

159

965

495

325

732

103

224

969

203

672

319

446

KSOO021

KSOO021

KSOOO21

KSOOO21

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOOO21

KSoo021

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

EPA 60108 21996 WP204

_- ---- shy1030

1040

1075

jcadmium

[chromium

Lampad

jJglL

jJglL

IJgIL

Acceptable

Acceptable

Acceptable

439

534

843

427

541

754

364 - 485

471 612

659 - 845

EPA 6010C 2000

EPA 6010C 2000

EPA 6010C 2000

416

537

756

166

224

325

KSOOO21

KSOOO21

KSOO021

WP204

WP204

WP204

e All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 Pof13 ~

DMRQA32 Final Report ERA AWaters Company

NPoes Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 middot0706112 City of Nevada WWTP 16517 South 1338 Road Nevad MO 84m 417-448middot2761

Analyte Code Analyte Units Performanu

Evaluation Reported

Value Assigned

Value Acceptance

Lim Method DeSCription Study Mesn

Study Stndard DevIlItion

USEPA Lab Code Study

wp rce Metal (cetil586J Aluminum EPA 2008 55 19981000 KS00021 WP204 iAcceptable 778 782 446IJglL 800 619middot932 Antimony EPA 2008 55 19981005 KSOOO21Acceptable 211 WP204413 402IJglL 404 286middot499 Arsenic EPA 2008 55 19981010 Acceptable 190 KS00021 WP204370 347 289 - 408 3441J91L ~rium1015 EPA 2008 55 1998 850 KSOOO21 WP204Acceptable 2350IJglL 2360 2360 2050 - 2660 Betylhum EPA 2008 55 19981020 WP204KS00021gil Acceptable 444 202431 454 386 - 513 cadmium EPA 2008 55 19981030 KS00021Acceptable 166 WP204gil 416 427 416364 middot485 Chromium EPA 2008 55 19981040 224 KS00021Acceptable 541 537 WP204IJglL 551 471 - 612

Cobah EPA 2008 55 19981050 KS00021 WP204Acceptable 374 159IJglL 377 362 317 - 406

Copper EPA 2008 5519981055 KS00021Acceptable 965 WP204IJglL 221 217 219194middot240 Iron EPA 2008 55 19981070 gIL 1080 495 KS00021 WP204Acceptable 10701040 946 - 1210

ead EPA 2008 5519981075 gIL KSOO021 WP204Acceptable 756 325760 754 659- 845

EPA 2008 55 19981090 ~nese KS00021gIL Acceptable 1900 732 WP2041940 1860 1670middot2070

EPA 2008 55 1998~enum1100 KSOOO21gIL Acceptable 103 WP204213 214 212178middot248 Nickel EPA 2008 5519981105 gIL 224 KSOO021 WP204Acceptable 505512 507 455 - 568

1140 Selenium EPA 2008 55 1998giL 1590 KS00021Acceptable 1620 969 WP2041600 1290middot1870

EPA 2008 551998I 1150 ~lIver KS00021Acceptable WP204322 361 310-414 360 203IJgIL 1165 Thallium EPA 2008 551998 319 KSOO021Acceptable 557 555 WP204538 450middot6671JgL

1185 Vanadium Nol Accepteble EPA 2008 551998 KS00021446 WP204991 980IJglL 1440 868middot1110

EPA 2008 5519981190 Zinc KS00021giL Acceptable 977 462 WP204993 975 _838middot 11~0 - - bull- -~

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 _ of13 ~

DMRQA32 Final Report ERA A Waters Company

NPOES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP SupelVlsor Study Dates 03119112 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 84772 417-448middot2761

Analyta Analyt8Code Unite Performence Reported AIIIUned

Evaluation Value Value Acceplll nee

LImite IiMthod Oeerlpllon

Study USEPALabStudyMn Standard Study DevIation

Code i

WP Trce Metals (Clltti 586J 1000 [Aluminum IlglL Acceptable 800 778 619-932 EPA 8020A 1998 782 446 KSOOO21 WP204 I

1005 [Antimony IlglL Acceptable 404 413 286-499 EPA 8020A 1998 402 211 KSOO021 WP204

1010 iAraenk IlglL Acceptable 370 347 289 - 408 EPA 802011 1998 344 190 KSOOO21 WP204

1015 ~lium 1l91L Acceptable 2360 2360 2050 - 2660 EPA 8020A 1998 2350 850 KS00021 WP204

1020 Seryffium IlgIL Acceptable 431 454 386 - 513 EPA 8020A 1998 444 202 KSOOO21 WP204

1030 ~mium IlgIL Acceptable 416 427 364 - 485 EPA 6020A 1998 416 166 KSOOO21 WP204

1040 Chromium IlQIL Acceptable 551 541 471 - 612 EPA 6020A 1998 537 224 KSOO021 WP204

1050 Cabalaquo IlQIL Acceptable 377 362 317 - 406 EPA 8020A 1998 374 159 KSOOO21 WP204

1055 Copper 1l91L Acceptable 221 217 194middot240 EPA 8020A 1998 219 965 KSOO021 WP204

1070 lroo 1l91L Acceptable 1040 1070 9Mi-1210 EPA 602011 1998 1080 495 KSOOO21 WP204

1075 ~ad IlglL Acceptable 760 754 659 - 845 EPA 6020A 1998 756 325 KSOOO21 WP204

1090 Manganese IlgIL Acceptable 1940 1860 1670 - 2070 EPA 602011 1998 1900 732 KSOO021 WP204

1100 MolytxIenum IlglL Acceptable 213 214 178-248 EPA 6020A 1998 212 103 KSOOO21 WP204

1105 Nickel IlgL Acceptable 512 507 455 - 568 EPA 602011 1998 505 224 KSOOO21 WP204

1140 Selenium IlglL Acceptable 1600 1620 1290 - 1870 EPA 8020A 1998 1590 969 KSOO021 WP204

1150 Silver 1l9L Acceptable 322 361 310 - 414 EPA 8020A 1998 360 203 KSOO021 WP204

1165 Thatlium 1l9L Acceptable 538 557 450 - 667 EPA 8020A 1998 555 319 KSOO021 WP204

1185 Vanadium IlQL Not Acceptable 1440 991 868-1110 EPA 8020A 1998 980 446 KSOO021 WP204

1190 Zinc IJgL Acceptable 993 975 838 -1120 EPA 8020A 1998 977 462 KSOO021 WP204

EPA 2451 3 1994

EPA 747011 1 1994

SM3500Cr 0 18th ED 1992

KS00021 WP204

KS00021 WP204

KSOO021 WP204

All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 13~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 031912 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448~2761

AII~ Code Ane~ Unltll Performnce

evaluation Reported

1Ilue Aalilned

1Ilue ~ptenc

Umltll Method Deecrtptloll Study Men Study

Stanclllrd Oevilltion

USEPA Leb Coda Study

WP Hexvent Chromium (ttl aN) 1045 HellllY81ent Chromium IJQL ---1 Aclteptable 1 580 1 606 1 494 712 1 EPA 7196A 1 19921 6Q4 ~4 I KSOOO21 WP204 J

EPA 1801 2 1993 672 0483 KSOOO21 WP204

SM2130B 18th ED 672 0483 KSOO021 WP2041992

SM21308 online 672 0483 KSOO021 WP204

EPA9012A 0836 00962 KSOO021 WP204

SM4500CN E 18th 0836 00962 KSOO021 WP204ED 1992

SM4500CN E online I 0836 00962 KSOO021 WP204

EPA 4201 1978 0491 0101 KSOO021 WP204

EPA 9066 1986 0491 0101 KSOO021 WP204

SM4500CI E 18th ED I 0850 00673 KSOO021 WP2041992

ISM4500CI E online 0850 00673 KSOO021 WP204

SM4500Ct G 18th ED I 0850 00673 KSOO021 WP2041992

e All analy1es are included in ERAs A2LA accreditation Lab Code 1539middot01 Pag1Oof13

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 03119112 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

Anltya Code Anltya UnMa Performanee

EVlluation Reported

Vllue Anlgned

Vllue Acceptance

Umltll Method Oeecrlptlon Study Meln Study

Satndlrd DevIation

USEPA lab Code

Study

WP Totll Reldulll ChIorlfHIlc 587J 1940 ITotal Residual Chlorine

-shy I mgll I Acceptable I 945 I 0822 I 0594 - 103 LSM4500CI CO onNne I 0850 - 00673 KSOOO21 WP204

ISM4500f~218th EO I 134 159 KSOOO21 WP204

SM4SOOCI E online KSOOO21 WP204

ISM4~~18th Eol 134 159 KSOO021 WP204

SM4500CI G onMne I 134 159 KSOOO21 WP204

CNI Level TDlaI Residual Chlorine

Level T alai Residual Chlorine

Level Total Residual Chlorine

jlglL Acceptable 140 138 780 _198

Ievel TDIal Residual Chlorine

uolL

jlgL

IlnlL

Acceptable 138 138 780 -198

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 P oI

ERA A Waters Company

Study DMRQA-32

NPDES Permit M00089109

Laboratory Name City of Nevada WWTP

It 120113

DMRQA32 Final Report ERA A Waters Company

NPDES Permitll MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dales 031912 middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Analyte rlS End Point Code Performance Repolllld Anlgned evaluation Value Value

Acceptance Method O crlptlonLimite

Study USEPAlIIbStudy StMldard Code

Study DevIatIon

-- -shyDMRQA FathNd minnow (Tut Code 13) (cat WETOO2) 48Hr Acute Non-Renewal 25 C MHSF Poraum chloride

~- IlC50 Acceptable 512 456 I 239 - 674 I EPA 2000 456 109 KSOOO21-(------oP4RQA32

DMRQA Fathead minnow (Test Code 15) (cat WET004) Today Short temI ChroniC Dally Renewal MHSF Potalum chlol1de

0808

0810

0756

IC25 (ON) Growth

NOEC (ON) Growth

NOEC Survival

Acceptable

Acceptable

-- Acceptable

389

25

25

355

250

250

175 - 535

125 - 500

125 - SOO

EPA 1000 2002

EPA 1000 2002

EPA 1000 2002 -shy

355 900 KSOO021

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32

DMRQA Cerlodaphna dubla (Tut Code 19) (cat WETOOB) 48Hr Acute Renewal 25 C MHSF Potlllum chlorlde

[Os ILC50 Acceptable 442 342 I 179middot504 I EPA 2002 342 810 - LIltSOOO21 [ DMRciA3iJ

DMRQA Cerlodflphnla dubla (Tet Code 21) (cat WET010) Today Short term Chronic Dally Renewal MHSF Potlllum chloride

0767

0768

0766

IC25 Raproduction

NOEC ReproductIOn

NOEC Survival -~ -shy

Acceptable

Acceptable

Acceptable

283

25

25

259

250

250

123 - 395

125 - 500

125middot500

EPA 1002 2002

EPA 10022002

EPA 10022002-_ __ __ shy

259 679 KSOOO21

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32shyDMRQA Daphnia pulax (Tet Code 38) (ea WET015) 48Hr Acute Non-Renewal 25 C MHSF Potassium chloride

[0794 ILC50 I Acceptable I 565 525 I 232middot818 I EPA 2021 525 147~r-KSoo021 -r OMRQAi2---]

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 13of13 ~

AWaters Company

Pennittee Name City of Nevada WWTP Pennit Number MOO089109 EPA Lab Code KSOOO21

WET OrganismsITest ConditionsEnd Points Checklist

DMRQA Study 32 La bull Graded Result

Analyte Number Organisms I Conditions End Points Test

Required Acceptable

Not Accepblble (ComtctIYe

Action Required)

Fathead minnow (Test Code 13) 0754 48Hrbull Acute Non-Renewal 25middot C MHSF lC50

EPA 2000 0 lEI 0 Fathead minnow (Test Code 14) 0755 48Hrbull Acute Non-Renewal 25middot C 20 DMW LC50

0 0 0 Fathead minnow (Test Code 15) 0808 7 -day Short Ierm Chronic Daily Renewal MHSF IC25 (ON) Growth

EPA 1000 0 lEI 0 0810 7 -day Short term Chronic Daily Renewal MHSF NOEC (ON) Growth

EPA 1000 0 lEI 0 0756 7-day Short term Chronic Daily Renewal MHSF NOEC Survival

EPA 1000 0 IRI 0 Fathead minnow (Test Code 18) 0812 7 -day Short term Chronic Daily Renewal 20 DMW IC25 (ON) Growth

0 0 0 0814 7-day Short Ierm Chronic Daily Renewal 20 DMW NOEC (ON) Growth

0 0 0 0759 7-day Short term Chronic Daily Renewal 20 DMW NOEC Survival

0 0 0 CerIodaphnle dubla (Test Code 19) 0764 48Hr Acute Renewal 25middot C MHSF LCSO

EPA 2002 0 IXI 0 CerIodaphnla dubla (Test Code 20) 0765 48Hr Acute ReneWal 25- C 20 DMW LCSO

0 0 0 CerIodaphnla dubla (Tast Code 21) 0767

0768

0766

7-day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF

IC25 Reproduction

NOEC Reproduction

NOEC Survival

0

0

IXI

[8]

0

0 EPA 1002 0 lEI 0

CerIodaphnla dubla (Tn Code 22) one 7-day Short term Chronic Daily Renewal 20 DMW IC25 Reproduction

0771 7-day Short term Chronic Daily Renewal 20 DMW NOEC Reproduction 0 0 0

0769 7 -day Short term Chronic Daily Renewal 20 DMW NOEC Survival 0 0 0

0 0 0 Daphnia magna (Test Code 32) 0788 48Hr Acute Non-Renewal 25deg C MHSF LCSO

0 0 0

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

DMRQA32 Final Report ERA A Waters Company

NPDES Permit MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 07127112

WWTP Supervisor Study Dates 03119112middot07106112 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Anatyte Coct AnaIyW Unit Performance

EV1Iluatlon Reported

Value Aliligned

Value Acceptance

Limits Method Deacrlpllon Study n

Study Stllndllrd DevIation

USEPALab Code

Study

WP pH caft 5711

1900 jpH SU Acceptable 633 631 611middot651 SM4500H+ a online 629 00470 KSOOO21 WP204

WPSlmpjbull Nutrients (caft 584)

1515 Ammoniaaa N

1820 Nitrate + Nitrite as N

1810 Nitrate as N

1870 jor1ho-Phosphate as P

su

SU

SU

mLlL

mUL

mgl

mgl

mgll

mgll

mgIl

I Acceetable 633 631

Acceptable 633 631

Acceptable 731 723

Acceptable 330 279

Acceptable 330 279

Acceptable 514 529

Acceptable 121 109

Acceptable 426 435

Acceptable 426 435

Acceptable 394 40l~

I 611 - 651 I EPA 9040621995 I

611 bull 651 I EPA 9040C 2002 I 703743 ISM4500~~ 21s1 ED

I 227 - 355 SM2540F 18th ED 1992

I 227middot355 SM2540F online

I 385 _ 6 75 ISM4500NH3 021st ED 2005

808 -136

354middot507

339 - 526

337 - 484

EPA 3501 2 1993

EPA 3532 2 1993

EPA 3532 2 1993

EPA365121993

629 00470

629 00470

727 00644

298 230

298 230

530 0467

110 0839

431 0214

431 0212

412 0204

KSOOO21

KSOOO21

MOOO982

KSOOO21

KSOOO21

MOOO982

KSOOO21

KSOOO21

KSOOO21

KSOOO21

WP204

WP204

OMRQA32

WP204

WP204

OMRQA32

WP204

WP204

WP204

WP204

EPA 3000 21 1993 KS00021

EPA 3000 21 1993 KS00021

EPA 3512 21993 KSOOO21 EPA 3654 1974 KSO0021

All analytes are included in ERAs A2LA accreditation Lab Code 1539-01

WP204

WP204

WP204

WP204

13 ~_

---

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 072712

WWTP Supervisor Study Dates 0311912middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Al1IIiyte Code

Anltyte Units Perforll1llnCll Evaluation

Reported Valul

Asalgned Value

Ac~ptanc Llmltll Mlthod D bullbullcrlpllon Study MIn

Study Sblndard DevIation

USEPAub Code Study

DIIRQA Demand (ClIf1 57aJ

1530 roo mgll Acceptable 815 904 457-135 514521082111 ED 2005

913 168 MOOO982 DMRQA32

_

EPA 3532 2 1993 KSO0021 WP204

EPA 3000 21 1993 KSOOO21 WP204

EPA 9056 1994 KS00021 WP204

r _ __

1530

1555

1565

IBOD

C800

COD

mgIl

mgll

mgIl

Acceptable

Acceptable

Acceptable

322

259

529

323

279

521

161 - 466

125 - 433

353 - 646

5M5210B 18th ED 1992

51452108 18th ED 1992

514522001811 ED 1992

319

295

519

530

490

542

KSOO021

KSOO021

KSOO021

WP204

WP204

WP204

WP Demand leaf1 571) 5M5210B online KSOO0211530 soo 319 530Acceptable 322 323 161 - 486 WP204mgll 5M5210B online KSOO021279 125middot433 295 490 WP2041555 Feoo mgl Acceptable 259

51452200 online KSOO021519 542 WP2041565 icoo Acceptable 521 353 - 648 mgll 529

EPA 4104 2 1993 KSOO021 WP204

EPA 1664A 1999 KSOO021 WP204

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 ~

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 - 0706112 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

AlUliyW Code

Anetytw Unlta Performance Evaluation

Reported Valua

Aaalgned Value

ACQplence Llmlta

Method DelCription Study Mean Study

Standard Deviation

USEPA Lab Code Study

WP TlIICe Metallea 586j

1000 AlUminum J91L Acceptable 772 778 619middot932 EPA 2007441994 782 446 KSOOO21 WP204

1005 Anllmony JgL Acceptable 416 413 286 - 499 EPA 2007 441994 402 211 KSOO021 WP204

1010 Araenic Jgl Acceptable 350 347 289 - 408 EPA 2007 441994 344 190 KSOOO21 WP204

1015 Barium JgL Acceptable 2350 2360 2050 - 2660 EPA 2007441994 2350 850 KSOOO21 WP204

1020 ~elytijum J91L Acceptable 462 454 386 - 513 EPA 2007 44 1994 444 202 KSOOO21 WP204

1025 BClron J91L Acceptable 1560 1660 1350 - 1930 EPA 2007 44 1994 1650 972 KSOO021 WP204

1030 centadmlum J9l Acceptable 439 427 364 -485 EPA 2007 44 1994 416 166 KSOOO21 WP204

1040 Chromium J91L Acceptable 534 541 471 - 612 EPA 2007 441994 537 224 KSOOO21 WP204

1050 Cobalt JglL Acceptable 397 362 317-406 EPA 2007 44 1994 374 159 KSOOO21 WP204

1055 Copper JgIL Acceptable 223 217 194 - 240 EPA 2007 441994 219 965 KSOOO21 WP204

1070 Iron JgIL Acceptable 1070 1070 946 - 1210 EPA 200744 1994 1080 495 KSOOO21 WP204

1075 Lead J9IL Acceptable 843 754 659middot845 EPA 2007 441994 756 325 KS00021 WP204

1090 ~nese 1J91L Acceptable 1930 1860 1670 - 2070 EPA 2007 441994 1900 732 KSOOO21 WP204

1100 Molybdenum JglL Acceptable 226 214 178 - 248 EPA 2007 44 1994 212 103 KSOOO21 WP204

1105 Nlckal Jell Acceptable 557 507 455 - 568 EPA 2007 44 1994 505 224 KSOOO21 WP204

1140 Selenium Jgl Acceptable 1600 1620 1290middot 1870 EPA 200144 1994 1590 969 KSOOO21 WP204

1150 SiMlr IJgL Acceptable 366 361 310 -414 EPA 2001 441994 360 203 KSOOO21 WP204

1160 Strontium 1JgL Acceptable 143 141 121 - 161 EPA 2001 44 1994 140 672 KSOOO21 WP204

1165 Thallium J9IL Not Acceptable 669 557 450 - 667 EPA 20074 41994 555 319 KSOOO21 WP204

1185 Vanadium JgL Acceptable 966 991 868-1110 EPA 200744 1994 980 446 KSOOO21 WP204

EPA 2007 44 1994 WP204

All analytes are included in ERAs A2LA accreditation Lab Gode 1539-01 _ of13 ~II

DMRQA32 Final Report ERA AWaters Company

NPoes Permit MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Illued 072712

WWTP Supervisor Study Dates 031912 middot070612 City of Neyada WWTP 16517 South 1338 Road Neyada MO 64772 417-448middot2761

Analyte Code

Analyte Unttll Performance Evaluation

Reported Value

Assigned Vllue

Accaptllnca Limb

Method DseMptlon Study Mean Study

Standard Devtatlon

USEPAub Code

Study

WP TRee _1 (calf 58B)

1000

1005

1010

1015

1020

1025

1030

1040

1050

1055

1070

1075

1090

1100

1105

1140

1150

1160

1165

1185

Aluminum

Antimony

Anlenic

Barium

Beryl~um

~on Cadmium

Chromium

Cobalt

Copper

Iron

fLead Manganese

Molybdenum

Nickel

Selenium

Silver

Strontium

Thallium

Vanedium

IJgIL

1J91L

1J91L

IJgIL

IJgIL

IJgIL

IJglL

IJglL

IJgIL

IJgIL

jJgL

IJglL

1J9L

IJglL

IJglL

1J91L

IJglL

IJgIL

jJgL

Jl9L_ _

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Not Acceptable

A~tatgt1ft

772

416

350

2350

462

1560

439

534

397

223

1070

843

1930

226

557

1600

366

143

669

966

778

413

347

2360

454

1660

427

541

362

217

1070

754

1860

214

507

1620

361

141

557

619middot932

286 -499

289 - 408

2050 - 2660

386 - 513

1350middot1930

364 - 485

471 - 612

317 - 406

194 - 240

946 - 1210

659 - 845

1670 - 2070

178 - 248

455 - 568

1290 - 1870

310 - 414

121 - 161

450 - 667

__99_1__ ~8-1110

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010821996

EPA 60108 21996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 60108 21996

EPA 6010B 21996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996 -shy

782

402

344 2350

444

1650

416

537

374

219

1080

756

1900

212

505

1590

360

140

555

980

446

211

190

850

202

972

166

224

159

965

495

325

732

103

224

969

203

672

319

446

KSOO021

KSOO021

KSOOO21

KSOOO21

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOOO21

KSoo021

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

EPA 60108 21996 WP204

_- ---- shy1030

1040

1075

jcadmium

[chromium

Lampad

jJglL

jJglL

IJgIL

Acceptable

Acceptable

Acceptable

439

534

843

427

541

754

364 - 485

471 612

659 - 845

EPA 6010C 2000

EPA 6010C 2000

EPA 6010C 2000

416

537

756

166

224

325

KSOOO21

KSOOO21

KSOO021

WP204

WP204

WP204

e All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 Pof13 ~

DMRQA32 Final Report ERA AWaters Company

NPoes Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 middot0706112 City of Nevada WWTP 16517 South 1338 Road Nevad MO 84m 417-448middot2761

Analyte Code Analyte Units Performanu

Evaluation Reported

Value Assigned

Value Acceptance

Lim Method DeSCription Study Mesn

Study Stndard DevIlItion

USEPA Lab Code Study

wp rce Metal (cetil586J Aluminum EPA 2008 55 19981000 KS00021 WP204 iAcceptable 778 782 446IJglL 800 619middot932 Antimony EPA 2008 55 19981005 KSOOO21Acceptable 211 WP204413 402IJglL 404 286middot499 Arsenic EPA 2008 55 19981010 Acceptable 190 KS00021 WP204370 347 289 - 408 3441J91L ~rium1015 EPA 2008 55 1998 850 KSOOO21 WP204Acceptable 2350IJglL 2360 2360 2050 - 2660 Betylhum EPA 2008 55 19981020 WP204KS00021gil Acceptable 444 202431 454 386 - 513 cadmium EPA 2008 55 19981030 KS00021Acceptable 166 WP204gil 416 427 416364 middot485 Chromium EPA 2008 55 19981040 224 KS00021Acceptable 541 537 WP204IJglL 551 471 - 612

Cobah EPA 2008 55 19981050 KS00021 WP204Acceptable 374 159IJglL 377 362 317 - 406

Copper EPA 2008 5519981055 KS00021Acceptable 965 WP204IJglL 221 217 219194middot240 Iron EPA 2008 55 19981070 gIL 1080 495 KS00021 WP204Acceptable 10701040 946 - 1210

ead EPA 2008 5519981075 gIL KSOO021 WP204Acceptable 756 325760 754 659- 845

EPA 2008 55 19981090 ~nese KS00021gIL Acceptable 1900 732 WP2041940 1860 1670middot2070

EPA 2008 55 1998~enum1100 KSOOO21gIL Acceptable 103 WP204213 214 212178middot248 Nickel EPA 2008 5519981105 gIL 224 KSOO021 WP204Acceptable 505512 507 455 - 568

1140 Selenium EPA 2008 55 1998giL 1590 KS00021Acceptable 1620 969 WP2041600 1290middot1870

EPA 2008 551998I 1150 ~lIver KS00021Acceptable WP204322 361 310-414 360 203IJgIL 1165 Thallium EPA 2008 551998 319 KSOO021Acceptable 557 555 WP204538 450middot6671JgL

1185 Vanadium Nol Accepteble EPA 2008 551998 KS00021446 WP204991 980IJglL 1440 868middot1110

EPA 2008 5519981190 Zinc KS00021giL Acceptable 977 462 WP204993 975 _838middot 11~0 - - bull- -~

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 _ of13 ~

DMRQA32 Final Report ERA A Waters Company

NPOES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP SupelVlsor Study Dates 03119112 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 84772 417-448middot2761

Analyta Analyt8Code Unite Performence Reported AIIIUned

Evaluation Value Value Acceplll nee

LImite IiMthod Oeerlpllon

Study USEPALabStudyMn Standard Study DevIation

Code i

WP Trce Metals (Clltti 586J 1000 [Aluminum IlglL Acceptable 800 778 619-932 EPA 8020A 1998 782 446 KSOOO21 WP204 I

1005 [Antimony IlglL Acceptable 404 413 286-499 EPA 8020A 1998 402 211 KSOO021 WP204

1010 iAraenk IlglL Acceptable 370 347 289 - 408 EPA 802011 1998 344 190 KSOOO21 WP204

1015 ~lium 1l91L Acceptable 2360 2360 2050 - 2660 EPA 8020A 1998 2350 850 KS00021 WP204

1020 Seryffium IlgIL Acceptable 431 454 386 - 513 EPA 8020A 1998 444 202 KSOOO21 WP204

1030 ~mium IlgIL Acceptable 416 427 364 - 485 EPA 6020A 1998 416 166 KSOOO21 WP204

1040 Chromium IlQIL Acceptable 551 541 471 - 612 EPA 6020A 1998 537 224 KSOO021 WP204

1050 Cabalaquo IlQIL Acceptable 377 362 317 - 406 EPA 8020A 1998 374 159 KSOOO21 WP204

1055 Copper 1l91L Acceptable 221 217 194middot240 EPA 8020A 1998 219 965 KSOO021 WP204

1070 lroo 1l91L Acceptable 1040 1070 9Mi-1210 EPA 602011 1998 1080 495 KSOOO21 WP204

1075 ~ad IlglL Acceptable 760 754 659 - 845 EPA 6020A 1998 756 325 KSOOO21 WP204

1090 Manganese IlgIL Acceptable 1940 1860 1670 - 2070 EPA 602011 1998 1900 732 KSOO021 WP204

1100 MolytxIenum IlglL Acceptable 213 214 178-248 EPA 6020A 1998 212 103 KSOOO21 WP204

1105 Nickel IlgL Acceptable 512 507 455 - 568 EPA 602011 1998 505 224 KSOOO21 WP204

1140 Selenium IlglL Acceptable 1600 1620 1290 - 1870 EPA 8020A 1998 1590 969 KSOO021 WP204

1150 Silver 1l9L Acceptable 322 361 310 - 414 EPA 8020A 1998 360 203 KSOO021 WP204

1165 Thatlium 1l9L Acceptable 538 557 450 - 667 EPA 8020A 1998 555 319 KSOO021 WP204

1185 Vanadium IlQL Not Acceptable 1440 991 868-1110 EPA 8020A 1998 980 446 KSOO021 WP204

1190 Zinc IJgL Acceptable 993 975 838 -1120 EPA 8020A 1998 977 462 KSOO021 WP204

EPA 2451 3 1994

EPA 747011 1 1994

SM3500Cr 0 18th ED 1992

KS00021 WP204

KS00021 WP204

KSOO021 WP204

All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 13~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 031912 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448~2761

AII~ Code Ane~ Unltll Performnce

evaluation Reported

1Ilue Aalilned

1Ilue ~ptenc

Umltll Method Deecrtptloll Study Men Study

Stanclllrd Oevilltion

USEPA Leb Coda Study

WP Hexvent Chromium (ttl aN) 1045 HellllY81ent Chromium IJQL ---1 Aclteptable 1 580 1 606 1 494 712 1 EPA 7196A 1 19921 6Q4 ~4 I KSOOO21 WP204 J

EPA 1801 2 1993 672 0483 KSOOO21 WP204

SM2130B 18th ED 672 0483 KSOO021 WP2041992

SM21308 online 672 0483 KSOO021 WP204

EPA9012A 0836 00962 KSOO021 WP204

SM4500CN E 18th 0836 00962 KSOO021 WP204ED 1992

SM4500CN E online I 0836 00962 KSOO021 WP204

EPA 4201 1978 0491 0101 KSOO021 WP204

EPA 9066 1986 0491 0101 KSOO021 WP204

SM4500CI E 18th ED I 0850 00673 KSOO021 WP2041992

ISM4500CI E online 0850 00673 KSOO021 WP204

SM4500Ct G 18th ED I 0850 00673 KSOO021 WP2041992

e All analy1es are included in ERAs A2LA accreditation Lab Code 1539middot01 Pag1Oof13

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 03119112 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

Anltya Code Anltya UnMa Performanee

EVlluation Reported

Vllue Anlgned

Vllue Acceptance

Umltll Method Oeecrlptlon Study Meln Study

Satndlrd DevIation

USEPA lab Code

Study

WP Totll Reldulll ChIorlfHIlc 587J 1940 ITotal Residual Chlorine

-shy I mgll I Acceptable I 945 I 0822 I 0594 - 103 LSM4500CI CO onNne I 0850 - 00673 KSOOO21 WP204

ISM4500f~218th EO I 134 159 KSOOO21 WP204

SM4SOOCI E online KSOOO21 WP204

ISM4~~18th Eol 134 159 KSOO021 WP204

SM4500CI G onMne I 134 159 KSOOO21 WP204

CNI Level TDlaI Residual Chlorine

Level T alai Residual Chlorine

Level Total Residual Chlorine

jlglL Acceptable 140 138 780 _198

Ievel TDIal Residual Chlorine

uolL

jlgL

IlnlL

Acceptable 138 138 780 -198

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 P oI

ERA A Waters Company

Study DMRQA-32

NPDES Permit M00089109

Laboratory Name City of Nevada WWTP

It 120113

DMRQA32 Final Report ERA A Waters Company

NPDES Permitll MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dales 031912 middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Analyte rlS End Point Code Performance Repolllld Anlgned evaluation Value Value

Acceptance Method O crlptlonLimite

Study USEPAlIIbStudy StMldard Code

Study DevIatIon

-- -shyDMRQA FathNd minnow (Tut Code 13) (cat WETOO2) 48Hr Acute Non-Renewal 25 C MHSF Poraum chloride

~- IlC50 Acceptable 512 456 I 239 - 674 I EPA 2000 456 109 KSOOO21-(------oP4RQA32

DMRQA Fathead minnow (Test Code 15) (cat WET004) Today Short temI ChroniC Dally Renewal MHSF Potalum chlol1de

0808

0810

0756

IC25 (ON) Growth

NOEC (ON) Growth

NOEC Survival

Acceptable

Acceptable

-- Acceptable

389

25

25

355

250

250

175 - 535

125 - 500

125 - SOO

EPA 1000 2002

EPA 1000 2002

EPA 1000 2002 -shy

355 900 KSOO021

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32

DMRQA Cerlodaphna dubla (Tut Code 19) (cat WETOOB) 48Hr Acute Renewal 25 C MHSF Potlllum chlorlde

[Os ILC50 Acceptable 442 342 I 179middot504 I EPA 2002 342 810 - LIltSOOO21 [ DMRciA3iJ

DMRQA Cerlodflphnla dubla (Tet Code 21) (cat WET010) Today Short term Chronic Dally Renewal MHSF Potlllum chloride

0767

0768

0766

IC25 Raproduction

NOEC ReproductIOn

NOEC Survival -~ -shy

Acceptable

Acceptable

Acceptable

283

25

25

259

250

250

123 - 395

125 - 500

125middot500

EPA 1002 2002

EPA 10022002

EPA 10022002-_ __ __ shy

259 679 KSOOO21

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32shyDMRQA Daphnia pulax (Tet Code 38) (ea WET015) 48Hr Acute Non-Renewal 25 C MHSF Potassium chloride

[0794 ILC50 I Acceptable I 565 525 I 232middot818 I EPA 2021 525 147~r-KSoo021 -r OMRQAi2---]

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 13of13 ~

AWaters Company

Pennittee Name City of Nevada WWTP Pennit Number MOO089109 EPA Lab Code KSOOO21

WET OrganismsITest ConditionsEnd Points Checklist

DMRQA Study 32 La bull Graded Result

Analyte Number Organisms I Conditions End Points Test

Required Acceptable

Not Accepblble (ComtctIYe

Action Required)

Fathead minnow (Test Code 13) 0754 48Hrbull Acute Non-Renewal 25middot C MHSF lC50

EPA 2000 0 lEI 0 Fathead minnow (Test Code 14) 0755 48Hrbull Acute Non-Renewal 25middot C 20 DMW LC50

0 0 0 Fathead minnow (Test Code 15) 0808 7 -day Short Ierm Chronic Daily Renewal MHSF IC25 (ON) Growth

EPA 1000 0 lEI 0 0810 7 -day Short term Chronic Daily Renewal MHSF NOEC (ON) Growth

EPA 1000 0 lEI 0 0756 7-day Short term Chronic Daily Renewal MHSF NOEC Survival

EPA 1000 0 IRI 0 Fathead minnow (Test Code 18) 0812 7 -day Short term Chronic Daily Renewal 20 DMW IC25 (ON) Growth

0 0 0 0814 7-day Short Ierm Chronic Daily Renewal 20 DMW NOEC (ON) Growth

0 0 0 0759 7-day Short term Chronic Daily Renewal 20 DMW NOEC Survival

0 0 0 CerIodaphnle dubla (Test Code 19) 0764 48Hr Acute Renewal 25middot C MHSF LCSO

EPA 2002 0 IXI 0 CerIodaphnla dubla (Test Code 20) 0765 48Hr Acute ReneWal 25- C 20 DMW LCSO

0 0 0 CerIodaphnla dubla (Tast Code 21) 0767

0768

0766

7-day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF

IC25 Reproduction

NOEC Reproduction

NOEC Survival

0

0

IXI

[8]

0

0 EPA 1002 0 lEI 0

CerIodaphnla dubla (Tn Code 22) one 7-day Short term Chronic Daily Renewal 20 DMW IC25 Reproduction

0771 7-day Short term Chronic Daily Renewal 20 DMW NOEC Reproduction 0 0 0

0769 7 -day Short term Chronic Daily Renewal 20 DMW NOEC Survival 0 0 0

0 0 0 Daphnia magna (Test Code 32) 0788 48Hr Acute Non-Renewal 25deg C MHSF LCSO

0 0 0

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

---

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 072712

WWTP Supervisor Study Dates 0311912middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Al1IIiyte Code

Anltyte Units Perforll1llnCll Evaluation

Reported Valul

Asalgned Value

Ac~ptanc Llmltll Mlthod D bullbullcrlpllon Study MIn

Study Sblndard DevIation

USEPAub Code Study

DIIRQA Demand (ClIf1 57aJ

1530 roo mgll Acceptable 815 904 457-135 514521082111 ED 2005

913 168 MOOO982 DMRQA32

_

EPA 3532 2 1993 KSO0021 WP204

EPA 3000 21 1993 KSOOO21 WP204

EPA 9056 1994 KS00021 WP204

r _ __

1530

1555

1565

IBOD

C800

COD

mgIl

mgll

mgIl

Acceptable

Acceptable

Acceptable

322

259

529

323

279

521

161 - 466

125 - 433

353 - 646

5M5210B 18th ED 1992

51452108 18th ED 1992

514522001811 ED 1992

319

295

519

530

490

542

KSOO021

KSOO021

KSOO021

WP204

WP204

WP204

WP Demand leaf1 571) 5M5210B online KSOO0211530 soo 319 530Acceptable 322 323 161 - 486 WP204mgll 5M5210B online KSOO021279 125middot433 295 490 WP2041555 Feoo mgl Acceptable 259

51452200 online KSOO021519 542 WP2041565 icoo Acceptable 521 353 - 648 mgll 529

EPA 4104 2 1993 KSOO021 WP204

EPA 1664A 1999 KSOO021 WP204

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 ~

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 - 0706112 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

AlUliyW Code

Anetytw Unlta Performance Evaluation

Reported Valua

Aaalgned Value

ACQplence Llmlta

Method DelCription Study Mean Study

Standard Deviation

USEPA Lab Code Study

WP TlIICe Metallea 586j

1000 AlUminum J91L Acceptable 772 778 619middot932 EPA 2007441994 782 446 KSOOO21 WP204

1005 Anllmony JgL Acceptable 416 413 286 - 499 EPA 2007 441994 402 211 KSOO021 WP204

1010 Araenic Jgl Acceptable 350 347 289 - 408 EPA 2007 441994 344 190 KSOOO21 WP204

1015 Barium JgL Acceptable 2350 2360 2050 - 2660 EPA 2007441994 2350 850 KSOOO21 WP204

1020 ~elytijum J91L Acceptable 462 454 386 - 513 EPA 2007 44 1994 444 202 KSOOO21 WP204

1025 BClron J91L Acceptable 1560 1660 1350 - 1930 EPA 2007 44 1994 1650 972 KSOO021 WP204

1030 centadmlum J9l Acceptable 439 427 364 -485 EPA 2007 44 1994 416 166 KSOOO21 WP204

1040 Chromium J91L Acceptable 534 541 471 - 612 EPA 2007 441994 537 224 KSOOO21 WP204

1050 Cobalt JglL Acceptable 397 362 317-406 EPA 2007 44 1994 374 159 KSOOO21 WP204

1055 Copper JgIL Acceptable 223 217 194 - 240 EPA 2007 441994 219 965 KSOOO21 WP204

1070 Iron JgIL Acceptable 1070 1070 946 - 1210 EPA 200744 1994 1080 495 KSOOO21 WP204

1075 Lead J9IL Acceptable 843 754 659middot845 EPA 2007 441994 756 325 KS00021 WP204

1090 ~nese 1J91L Acceptable 1930 1860 1670 - 2070 EPA 2007 441994 1900 732 KSOOO21 WP204

1100 Molybdenum JglL Acceptable 226 214 178 - 248 EPA 2007 44 1994 212 103 KSOOO21 WP204

1105 Nlckal Jell Acceptable 557 507 455 - 568 EPA 2007 44 1994 505 224 KSOOO21 WP204

1140 Selenium Jgl Acceptable 1600 1620 1290middot 1870 EPA 200144 1994 1590 969 KSOOO21 WP204

1150 SiMlr IJgL Acceptable 366 361 310 -414 EPA 2001 441994 360 203 KSOOO21 WP204

1160 Strontium 1JgL Acceptable 143 141 121 - 161 EPA 2001 44 1994 140 672 KSOOO21 WP204

1165 Thallium J9IL Not Acceptable 669 557 450 - 667 EPA 20074 41994 555 319 KSOOO21 WP204

1185 Vanadium JgL Acceptable 966 991 868-1110 EPA 200744 1994 980 446 KSOOO21 WP204

EPA 2007 44 1994 WP204

All analytes are included in ERAs A2LA accreditation Lab Gode 1539-01 _ of13 ~II

DMRQA32 Final Report ERA AWaters Company

NPoes Permit MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Illued 072712

WWTP Supervisor Study Dates 031912 middot070612 City of Neyada WWTP 16517 South 1338 Road Neyada MO 64772 417-448middot2761

Analyte Code

Analyte Unttll Performance Evaluation

Reported Value

Assigned Vllue

Accaptllnca Limb

Method DseMptlon Study Mean Study

Standard Devtatlon

USEPAub Code

Study

WP TRee _1 (calf 58B)

1000

1005

1010

1015

1020

1025

1030

1040

1050

1055

1070

1075

1090

1100

1105

1140

1150

1160

1165

1185

Aluminum

Antimony

Anlenic

Barium

Beryl~um

~on Cadmium

Chromium

Cobalt

Copper

Iron

fLead Manganese

Molybdenum

Nickel

Selenium

Silver

Strontium

Thallium

Vanedium

IJgIL

1J91L

1J91L

IJgIL

IJgIL

IJgIL

IJglL

IJglL

IJgIL

IJgIL

jJgL

IJglL

1J9L

IJglL

IJglL

1J91L

IJglL

IJgIL

jJgL

Jl9L_ _

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Not Acceptable

A~tatgt1ft

772

416

350

2350

462

1560

439

534

397

223

1070

843

1930

226

557

1600

366

143

669

966

778

413

347

2360

454

1660

427

541

362

217

1070

754

1860

214

507

1620

361

141

557

619middot932

286 -499

289 - 408

2050 - 2660

386 - 513

1350middot1930

364 - 485

471 - 612

317 - 406

194 - 240

946 - 1210

659 - 845

1670 - 2070

178 - 248

455 - 568

1290 - 1870

310 - 414

121 - 161

450 - 667

__99_1__ ~8-1110

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010821996

EPA 60108 21996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 60108 21996

EPA 6010B 21996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996 -shy

782

402

344 2350

444

1650

416

537

374

219

1080

756

1900

212

505

1590

360

140

555

980

446

211

190

850

202

972

166

224

159

965

495

325

732

103

224

969

203

672

319

446

KSOO021

KSOO021

KSOOO21

KSOOO21

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOOO21

KSoo021

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

EPA 60108 21996 WP204

_- ---- shy1030

1040

1075

jcadmium

[chromium

Lampad

jJglL

jJglL

IJgIL

Acceptable

Acceptable

Acceptable

439

534

843

427

541

754

364 - 485

471 612

659 - 845

EPA 6010C 2000

EPA 6010C 2000

EPA 6010C 2000

416

537

756

166

224

325

KSOOO21

KSOOO21

KSOO021

WP204

WP204

WP204

e All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 Pof13 ~

DMRQA32 Final Report ERA AWaters Company

NPoes Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 middot0706112 City of Nevada WWTP 16517 South 1338 Road Nevad MO 84m 417-448middot2761

Analyte Code Analyte Units Performanu

Evaluation Reported

Value Assigned

Value Acceptance

Lim Method DeSCription Study Mesn

Study Stndard DevIlItion

USEPA Lab Code Study

wp rce Metal (cetil586J Aluminum EPA 2008 55 19981000 KS00021 WP204 iAcceptable 778 782 446IJglL 800 619middot932 Antimony EPA 2008 55 19981005 KSOOO21Acceptable 211 WP204413 402IJglL 404 286middot499 Arsenic EPA 2008 55 19981010 Acceptable 190 KS00021 WP204370 347 289 - 408 3441J91L ~rium1015 EPA 2008 55 1998 850 KSOOO21 WP204Acceptable 2350IJglL 2360 2360 2050 - 2660 Betylhum EPA 2008 55 19981020 WP204KS00021gil Acceptable 444 202431 454 386 - 513 cadmium EPA 2008 55 19981030 KS00021Acceptable 166 WP204gil 416 427 416364 middot485 Chromium EPA 2008 55 19981040 224 KS00021Acceptable 541 537 WP204IJglL 551 471 - 612

Cobah EPA 2008 55 19981050 KS00021 WP204Acceptable 374 159IJglL 377 362 317 - 406

Copper EPA 2008 5519981055 KS00021Acceptable 965 WP204IJglL 221 217 219194middot240 Iron EPA 2008 55 19981070 gIL 1080 495 KS00021 WP204Acceptable 10701040 946 - 1210

ead EPA 2008 5519981075 gIL KSOO021 WP204Acceptable 756 325760 754 659- 845

EPA 2008 55 19981090 ~nese KS00021gIL Acceptable 1900 732 WP2041940 1860 1670middot2070

EPA 2008 55 1998~enum1100 KSOOO21gIL Acceptable 103 WP204213 214 212178middot248 Nickel EPA 2008 5519981105 gIL 224 KSOO021 WP204Acceptable 505512 507 455 - 568

1140 Selenium EPA 2008 55 1998giL 1590 KS00021Acceptable 1620 969 WP2041600 1290middot1870

EPA 2008 551998I 1150 ~lIver KS00021Acceptable WP204322 361 310-414 360 203IJgIL 1165 Thallium EPA 2008 551998 319 KSOO021Acceptable 557 555 WP204538 450middot6671JgL

1185 Vanadium Nol Accepteble EPA 2008 551998 KS00021446 WP204991 980IJglL 1440 868middot1110

EPA 2008 5519981190 Zinc KS00021giL Acceptable 977 462 WP204993 975 _838middot 11~0 - - bull- -~

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 _ of13 ~

DMRQA32 Final Report ERA A Waters Company

NPOES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP SupelVlsor Study Dates 03119112 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 84772 417-448middot2761

Analyta Analyt8Code Unite Performence Reported AIIIUned

Evaluation Value Value Acceplll nee

LImite IiMthod Oeerlpllon

Study USEPALabStudyMn Standard Study DevIation

Code i

WP Trce Metals (Clltti 586J 1000 [Aluminum IlglL Acceptable 800 778 619-932 EPA 8020A 1998 782 446 KSOOO21 WP204 I

1005 [Antimony IlglL Acceptable 404 413 286-499 EPA 8020A 1998 402 211 KSOO021 WP204

1010 iAraenk IlglL Acceptable 370 347 289 - 408 EPA 802011 1998 344 190 KSOOO21 WP204

1015 ~lium 1l91L Acceptable 2360 2360 2050 - 2660 EPA 8020A 1998 2350 850 KS00021 WP204

1020 Seryffium IlgIL Acceptable 431 454 386 - 513 EPA 8020A 1998 444 202 KSOOO21 WP204

1030 ~mium IlgIL Acceptable 416 427 364 - 485 EPA 6020A 1998 416 166 KSOOO21 WP204

1040 Chromium IlQIL Acceptable 551 541 471 - 612 EPA 6020A 1998 537 224 KSOO021 WP204

1050 Cabalaquo IlQIL Acceptable 377 362 317 - 406 EPA 8020A 1998 374 159 KSOOO21 WP204

1055 Copper 1l91L Acceptable 221 217 194middot240 EPA 8020A 1998 219 965 KSOO021 WP204

1070 lroo 1l91L Acceptable 1040 1070 9Mi-1210 EPA 602011 1998 1080 495 KSOOO21 WP204

1075 ~ad IlglL Acceptable 760 754 659 - 845 EPA 6020A 1998 756 325 KSOOO21 WP204

1090 Manganese IlgIL Acceptable 1940 1860 1670 - 2070 EPA 602011 1998 1900 732 KSOO021 WP204

1100 MolytxIenum IlglL Acceptable 213 214 178-248 EPA 6020A 1998 212 103 KSOOO21 WP204

1105 Nickel IlgL Acceptable 512 507 455 - 568 EPA 602011 1998 505 224 KSOOO21 WP204

1140 Selenium IlglL Acceptable 1600 1620 1290 - 1870 EPA 8020A 1998 1590 969 KSOO021 WP204

1150 Silver 1l9L Acceptable 322 361 310 - 414 EPA 8020A 1998 360 203 KSOO021 WP204

1165 Thatlium 1l9L Acceptable 538 557 450 - 667 EPA 8020A 1998 555 319 KSOO021 WP204

1185 Vanadium IlQL Not Acceptable 1440 991 868-1110 EPA 8020A 1998 980 446 KSOO021 WP204

1190 Zinc IJgL Acceptable 993 975 838 -1120 EPA 8020A 1998 977 462 KSOO021 WP204

EPA 2451 3 1994

EPA 747011 1 1994

SM3500Cr 0 18th ED 1992

KS00021 WP204

KS00021 WP204

KSOO021 WP204

All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 13~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 031912 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448~2761

AII~ Code Ane~ Unltll Performnce

evaluation Reported

1Ilue Aalilned

1Ilue ~ptenc

Umltll Method Deecrtptloll Study Men Study

Stanclllrd Oevilltion

USEPA Leb Coda Study

WP Hexvent Chromium (ttl aN) 1045 HellllY81ent Chromium IJQL ---1 Aclteptable 1 580 1 606 1 494 712 1 EPA 7196A 1 19921 6Q4 ~4 I KSOOO21 WP204 J

EPA 1801 2 1993 672 0483 KSOOO21 WP204

SM2130B 18th ED 672 0483 KSOO021 WP2041992

SM21308 online 672 0483 KSOO021 WP204

EPA9012A 0836 00962 KSOO021 WP204

SM4500CN E 18th 0836 00962 KSOO021 WP204ED 1992

SM4500CN E online I 0836 00962 KSOO021 WP204

EPA 4201 1978 0491 0101 KSOO021 WP204

EPA 9066 1986 0491 0101 KSOO021 WP204

SM4500CI E 18th ED I 0850 00673 KSOO021 WP2041992

ISM4500CI E online 0850 00673 KSOO021 WP204

SM4500Ct G 18th ED I 0850 00673 KSOO021 WP2041992

e All analy1es are included in ERAs A2LA accreditation Lab Code 1539middot01 Pag1Oof13

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 03119112 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

Anltya Code Anltya UnMa Performanee

EVlluation Reported

Vllue Anlgned

Vllue Acceptance

Umltll Method Oeecrlptlon Study Meln Study

Satndlrd DevIation

USEPA lab Code

Study

WP Totll Reldulll ChIorlfHIlc 587J 1940 ITotal Residual Chlorine

-shy I mgll I Acceptable I 945 I 0822 I 0594 - 103 LSM4500CI CO onNne I 0850 - 00673 KSOOO21 WP204

ISM4500f~218th EO I 134 159 KSOOO21 WP204

SM4SOOCI E online KSOOO21 WP204

ISM4~~18th Eol 134 159 KSOO021 WP204

SM4500CI G onMne I 134 159 KSOOO21 WP204

CNI Level TDlaI Residual Chlorine

Level T alai Residual Chlorine

Level Total Residual Chlorine

jlglL Acceptable 140 138 780 _198

Ievel TDIal Residual Chlorine

uolL

jlgL

IlnlL

Acceptable 138 138 780 -198

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 P oI

ERA A Waters Company

Study DMRQA-32

NPDES Permit M00089109

Laboratory Name City of Nevada WWTP

It 120113

DMRQA32 Final Report ERA A Waters Company

NPDES Permitll MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dales 031912 middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Analyte rlS End Point Code Performance Repolllld Anlgned evaluation Value Value

Acceptance Method O crlptlonLimite

Study USEPAlIIbStudy StMldard Code

Study DevIatIon

-- -shyDMRQA FathNd minnow (Tut Code 13) (cat WETOO2) 48Hr Acute Non-Renewal 25 C MHSF Poraum chloride

~- IlC50 Acceptable 512 456 I 239 - 674 I EPA 2000 456 109 KSOOO21-(------oP4RQA32

DMRQA Fathead minnow (Test Code 15) (cat WET004) Today Short temI ChroniC Dally Renewal MHSF Potalum chlol1de

0808

0810

0756

IC25 (ON) Growth

NOEC (ON) Growth

NOEC Survival

Acceptable

Acceptable

-- Acceptable

389

25

25

355

250

250

175 - 535

125 - 500

125 - SOO

EPA 1000 2002

EPA 1000 2002

EPA 1000 2002 -shy

355 900 KSOO021

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32

DMRQA Cerlodaphna dubla (Tut Code 19) (cat WETOOB) 48Hr Acute Renewal 25 C MHSF Potlllum chlorlde

[Os ILC50 Acceptable 442 342 I 179middot504 I EPA 2002 342 810 - LIltSOOO21 [ DMRciA3iJ

DMRQA Cerlodflphnla dubla (Tet Code 21) (cat WET010) Today Short term Chronic Dally Renewal MHSF Potlllum chloride

0767

0768

0766

IC25 Raproduction

NOEC ReproductIOn

NOEC Survival -~ -shy

Acceptable

Acceptable

Acceptable

283

25

25

259

250

250

123 - 395

125 - 500

125middot500

EPA 1002 2002

EPA 10022002

EPA 10022002-_ __ __ shy

259 679 KSOOO21

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32shyDMRQA Daphnia pulax (Tet Code 38) (ea WET015) 48Hr Acute Non-Renewal 25 C MHSF Potassium chloride

[0794 ILC50 I Acceptable I 565 525 I 232middot818 I EPA 2021 525 147~r-KSoo021 -r OMRQAi2---]

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 13of13 ~

AWaters Company

Pennittee Name City of Nevada WWTP Pennit Number MOO089109 EPA Lab Code KSOOO21

WET OrganismsITest ConditionsEnd Points Checklist

DMRQA Study 32 La bull Graded Result

Analyte Number Organisms I Conditions End Points Test

Required Acceptable

Not Accepblble (ComtctIYe

Action Required)

Fathead minnow (Test Code 13) 0754 48Hrbull Acute Non-Renewal 25middot C MHSF lC50

EPA 2000 0 lEI 0 Fathead minnow (Test Code 14) 0755 48Hrbull Acute Non-Renewal 25middot C 20 DMW LC50

0 0 0 Fathead minnow (Test Code 15) 0808 7 -day Short Ierm Chronic Daily Renewal MHSF IC25 (ON) Growth

EPA 1000 0 lEI 0 0810 7 -day Short term Chronic Daily Renewal MHSF NOEC (ON) Growth

EPA 1000 0 lEI 0 0756 7-day Short term Chronic Daily Renewal MHSF NOEC Survival

EPA 1000 0 IRI 0 Fathead minnow (Test Code 18) 0812 7 -day Short term Chronic Daily Renewal 20 DMW IC25 (ON) Growth

0 0 0 0814 7-day Short Ierm Chronic Daily Renewal 20 DMW NOEC (ON) Growth

0 0 0 0759 7-day Short term Chronic Daily Renewal 20 DMW NOEC Survival

0 0 0 CerIodaphnle dubla (Test Code 19) 0764 48Hr Acute Renewal 25middot C MHSF LCSO

EPA 2002 0 IXI 0 CerIodaphnla dubla (Test Code 20) 0765 48Hr Acute ReneWal 25- C 20 DMW LCSO

0 0 0 CerIodaphnla dubla (Tast Code 21) 0767

0768

0766

7-day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF

IC25 Reproduction

NOEC Reproduction

NOEC Survival

0

0

IXI

[8]

0

0 EPA 1002 0 lEI 0

CerIodaphnla dubla (Tn Code 22) one 7-day Short term Chronic Daily Renewal 20 DMW IC25 Reproduction

0771 7-day Short term Chronic Daily Renewal 20 DMW NOEC Reproduction 0 0 0

0769 7 -day Short term Chronic Daily Renewal 20 DMW NOEC Survival 0 0 0

0 0 0 Daphnia magna (Test Code 32) 0788 48Hr Acute Non-Renewal 25deg C MHSF LCSO

0 0 0

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 - 0706112 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

AlUliyW Code

Anetytw Unlta Performance Evaluation

Reported Valua

Aaalgned Value

ACQplence Llmlta

Method DelCription Study Mean Study

Standard Deviation

USEPA Lab Code Study

WP TlIICe Metallea 586j

1000 AlUminum J91L Acceptable 772 778 619middot932 EPA 2007441994 782 446 KSOOO21 WP204

1005 Anllmony JgL Acceptable 416 413 286 - 499 EPA 2007 441994 402 211 KSOO021 WP204

1010 Araenic Jgl Acceptable 350 347 289 - 408 EPA 2007 441994 344 190 KSOOO21 WP204

1015 Barium JgL Acceptable 2350 2360 2050 - 2660 EPA 2007441994 2350 850 KSOOO21 WP204

1020 ~elytijum J91L Acceptable 462 454 386 - 513 EPA 2007 44 1994 444 202 KSOOO21 WP204

1025 BClron J91L Acceptable 1560 1660 1350 - 1930 EPA 2007 44 1994 1650 972 KSOO021 WP204

1030 centadmlum J9l Acceptable 439 427 364 -485 EPA 2007 44 1994 416 166 KSOOO21 WP204

1040 Chromium J91L Acceptable 534 541 471 - 612 EPA 2007 441994 537 224 KSOOO21 WP204

1050 Cobalt JglL Acceptable 397 362 317-406 EPA 2007 44 1994 374 159 KSOOO21 WP204

1055 Copper JgIL Acceptable 223 217 194 - 240 EPA 2007 441994 219 965 KSOOO21 WP204

1070 Iron JgIL Acceptable 1070 1070 946 - 1210 EPA 200744 1994 1080 495 KSOOO21 WP204

1075 Lead J9IL Acceptable 843 754 659middot845 EPA 2007 441994 756 325 KS00021 WP204

1090 ~nese 1J91L Acceptable 1930 1860 1670 - 2070 EPA 2007 441994 1900 732 KSOOO21 WP204

1100 Molybdenum JglL Acceptable 226 214 178 - 248 EPA 2007 44 1994 212 103 KSOOO21 WP204

1105 Nlckal Jell Acceptable 557 507 455 - 568 EPA 2007 44 1994 505 224 KSOOO21 WP204

1140 Selenium Jgl Acceptable 1600 1620 1290middot 1870 EPA 200144 1994 1590 969 KSOOO21 WP204

1150 SiMlr IJgL Acceptable 366 361 310 -414 EPA 2001 441994 360 203 KSOOO21 WP204

1160 Strontium 1JgL Acceptable 143 141 121 - 161 EPA 2001 44 1994 140 672 KSOOO21 WP204

1165 Thallium J9IL Not Acceptable 669 557 450 - 667 EPA 20074 41994 555 319 KSOOO21 WP204

1185 Vanadium JgL Acceptable 966 991 868-1110 EPA 200744 1994 980 446 KSOOO21 WP204

EPA 2007 44 1994 WP204

All analytes are included in ERAs A2LA accreditation Lab Gode 1539-01 _ of13 ~II

DMRQA32 Final Report ERA AWaters Company

NPoes Permit MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Illued 072712

WWTP Supervisor Study Dates 031912 middot070612 City of Neyada WWTP 16517 South 1338 Road Neyada MO 64772 417-448middot2761

Analyte Code

Analyte Unttll Performance Evaluation

Reported Value

Assigned Vllue

Accaptllnca Limb

Method DseMptlon Study Mean Study

Standard Devtatlon

USEPAub Code

Study

WP TRee _1 (calf 58B)

1000

1005

1010

1015

1020

1025

1030

1040

1050

1055

1070

1075

1090

1100

1105

1140

1150

1160

1165

1185

Aluminum

Antimony

Anlenic

Barium

Beryl~um

~on Cadmium

Chromium

Cobalt

Copper

Iron

fLead Manganese

Molybdenum

Nickel

Selenium

Silver

Strontium

Thallium

Vanedium

IJgIL

1J91L

1J91L

IJgIL

IJgIL

IJgIL

IJglL

IJglL

IJgIL

IJgIL

jJgL

IJglL

1J9L

IJglL

IJglL

1J91L

IJglL

IJgIL

jJgL

Jl9L_ _

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Not Acceptable

A~tatgt1ft

772

416

350

2350

462

1560

439

534

397

223

1070

843

1930

226

557

1600

366

143

669

966

778

413

347

2360

454

1660

427

541

362

217

1070

754

1860

214

507

1620

361

141

557

619middot932

286 -499

289 - 408

2050 - 2660

386 - 513

1350middot1930

364 - 485

471 - 612

317 - 406

194 - 240

946 - 1210

659 - 845

1670 - 2070

178 - 248

455 - 568

1290 - 1870

310 - 414

121 - 161

450 - 667

__99_1__ ~8-1110

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010821996

EPA 60108 21996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 60108 21996

EPA 6010B 21996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996 -shy

782

402

344 2350

444

1650

416

537

374

219

1080

756

1900

212

505

1590

360

140

555

980

446

211

190

850

202

972

166

224

159

965

495

325

732

103

224

969

203

672

319

446

KSOO021

KSOO021

KSOOO21

KSOOO21

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOOO21

KSoo021

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

EPA 60108 21996 WP204

_- ---- shy1030

1040

1075

jcadmium

[chromium

Lampad

jJglL

jJglL

IJgIL

Acceptable

Acceptable

Acceptable

439

534

843

427

541

754

364 - 485

471 612

659 - 845

EPA 6010C 2000

EPA 6010C 2000

EPA 6010C 2000

416

537

756

166

224

325

KSOOO21

KSOOO21

KSOO021

WP204

WP204

WP204

e All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 Pof13 ~

DMRQA32 Final Report ERA AWaters Company

NPoes Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 middot0706112 City of Nevada WWTP 16517 South 1338 Road Nevad MO 84m 417-448middot2761

Analyte Code Analyte Units Performanu

Evaluation Reported

Value Assigned

Value Acceptance

Lim Method DeSCription Study Mesn

Study Stndard DevIlItion

USEPA Lab Code Study

wp rce Metal (cetil586J Aluminum EPA 2008 55 19981000 KS00021 WP204 iAcceptable 778 782 446IJglL 800 619middot932 Antimony EPA 2008 55 19981005 KSOOO21Acceptable 211 WP204413 402IJglL 404 286middot499 Arsenic EPA 2008 55 19981010 Acceptable 190 KS00021 WP204370 347 289 - 408 3441J91L ~rium1015 EPA 2008 55 1998 850 KSOOO21 WP204Acceptable 2350IJglL 2360 2360 2050 - 2660 Betylhum EPA 2008 55 19981020 WP204KS00021gil Acceptable 444 202431 454 386 - 513 cadmium EPA 2008 55 19981030 KS00021Acceptable 166 WP204gil 416 427 416364 middot485 Chromium EPA 2008 55 19981040 224 KS00021Acceptable 541 537 WP204IJglL 551 471 - 612

Cobah EPA 2008 55 19981050 KS00021 WP204Acceptable 374 159IJglL 377 362 317 - 406

Copper EPA 2008 5519981055 KS00021Acceptable 965 WP204IJglL 221 217 219194middot240 Iron EPA 2008 55 19981070 gIL 1080 495 KS00021 WP204Acceptable 10701040 946 - 1210

ead EPA 2008 5519981075 gIL KSOO021 WP204Acceptable 756 325760 754 659- 845

EPA 2008 55 19981090 ~nese KS00021gIL Acceptable 1900 732 WP2041940 1860 1670middot2070

EPA 2008 55 1998~enum1100 KSOOO21gIL Acceptable 103 WP204213 214 212178middot248 Nickel EPA 2008 5519981105 gIL 224 KSOO021 WP204Acceptable 505512 507 455 - 568

1140 Selenium EPA 2008 55 1998giL 1590 KS00021Acceptable 1620 969 WP2041600 1290middot1870

EPA 2008 551998I 1150 ~lIver KS00021Acceptable WP204322 361 310-414 360 203IJgIL 1165 Thallium EPA 2008 551998 319 KSOO021Acceptable 557 555 WP204538 450middot6671JgL

1185 Vanadium Nol Accepteble EPA 2008 551998 KS00021446 WP204991 980IJglL 1440 868middot1110

EPA 2008 5519981190 Zinc KS00021giL Acceptable 977 462 WP204993 975 _838middot 11~0 - - bull- -~

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 _ of13 ~

DMRQA32 Final Report ERA A Waters Company

NPOES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP SupelVlsor Study Dates 03119112 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 84772 417-448middot2761

Analyta Analyt8Code Unite Performence Reported AIIIUned

Evaluation Value Value Acceplll nee

LImite IiMthod Oeerlpllon

Study USEPALabStudyMn Standard Study DevIation

Code i

WP Trce Metals (Clltti 586J 1000 [Aluminum IlglL Acceptable 800 778 619-932 EPA 8020A 1998 782 446 KSOOO21 WP204 I

1005 [Antimony IlglL Acceptable 404 413 286-499 EPA 8020A 1998 402 211 KSOO021 WP204

1010 iAraenk IlglL Acceptable 370 347 289 - 408 EPA 802011 1998 344 190 KSOOO21 WP204

1015 ~lium 1l91L Acceptable 2360 2360 2050 - 2660 EPA 8020A 1998 2350 850 KS00021 WP204

1020 Seryffium IlgIL Acceptable 431 454 386 - 513 EPA 8020A 1998 444 202 KSOOO21 WP204

1030 ~mium IlgIL Acceptable 416 427 364 - 485 EPA 6020A 1998 416 166 KSOOO21 WP204

1040 Chromium IlQIL Acceptable 551 541 471 - 612 EPA 6020A 1998 537 224 KSOO021 WP204

1050 Cabalaquo IlQIL Acceptable 377 362 317 - 406 EPA 8020A 1998 374 159 KSOOO21 WP204

1055 Copper 1l91L Acceptable 221 217 194middot240 EPA 8020A 1998 219 965 KSOO021 WP204

1070 lroo 1l91L Acceptable 1040 1070 9Mi-1210 EPA 602011 1998 1080 495 KSOOO21 WP204

1075 ~ad IlglL Acceptable 760 754 659 - 845 EPA 6020A 1998 756 325 KSOOO21 WP204

1090 Manganese IlgIL Acceptable 1940 1860 1670 - 2070 EPA 602011 1998 1900 732 KSOO021 WP204

1100 MolytxIenum IlglL Acceptable 213 214 178-248 EPA 6020A 1998 212 103 KSOOO21 WP204

1105 Nickel IlgL Acceptable 512 507 455 - 568 EPA 602011 1998 505 224 KSOOO21 WP204

1140 Selenium IlglL Acceptable 1600 1620 1290 - 1870 EPA 8020A 1998 1590 969 KSOO021 WP204

1150 Silver 1l9L Acceptable 322 361 310 - 414 EPA 8020A 1998 360 203 KSOO021 WP204

1165 Thatlium 1l9L Acceptable 538 557 450 - 667 EPA 8020A 1998 555 319 KSOO021 WP204

1185 Vanadium IlQL Not Acceptable 1440 991 868-1110 EPA 8020A 1998 980 446 KSOO021 WP204

1190 Zinc IJgL Acceptable 993 975 838 -1120 EPA 8020A 1998 977 462 KSOO021 WP204

EPA 2451 3 1994

EPA 747011 1 1994

SM3500Cr 0 18th ED 1992

KS00021 WP204

KS00021 WP204

KSOO021 WP204

All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 13~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 031912 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448~2761

AII~ Code Ane~ Unltll Performnce

evaluation Reported

1Ilue Aalilned

1Ilue ~ptenc

Umltll Method Deecrtptloll Study Men Study

Stanclllrd Oevilltion

USEPA Leb Coda Study

WP Hexvent Chromium (ttl aN) 1045 HellllY81ent Chromium IJQL ---1 Aclteptable 1 580 1 606 1 494 712 1 EPA 7196A 1 19921 6Q4 ~4 I KSOOO21 WP204 J

EPA 1801 2 1993 672 0483 KSOOO21 WP204

SM2130B 18th ED 672 0483 KSOO021 WP2041992

SM21308 online 672 0483 KSOO021 WP204

EPA9012A 0836 00962 KSOO021 WP204

SM4500CN E 18th 0836 00962 KSOO021 WP204ED 1992

SM4500CN E online I 0836 00962 KSOO021 WP204

EPA 4201 1978 0491 0101 KSOO021 WP204

EPA 9066 1986 0491 0101 KSOO021 WP204

SM4500CI E 18th ED I 0850 00673 KSOO021 WP2041992

ISM4500CI E online 0850 00673 KSOO021 WP204

SM4500Ct G 18th ED I 0850 00673 KSOO021 WP2041992

e All analy1es are included in ERAs A2LA accreditation Lab Code 1539middot01 Pag1Oof13

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 03119112 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

Anltya Code Anltya UnMa Performanee

EVlluation Reported

Vllue Anlgned

Vllue Acceptance

Umltll Method Oeecrlptlon Study Meln Study

Satndlrd DevIation

USEPA lab Code

Study

WP Totll Reldulll ChIorlfHIlc 587J 1940 ITotal Residual Chlorine

-shy I mgll I Acceptable I 945 I 0822 I 0594 - 103 LSM4500CI CO onNne I 0850 - 00673 KSOOO21 WP204

ISM4500f~218th EO I 134 159 KSOOO21 WP204

SM4SOOCI E online KSOOO21 WP204

ISM4~~18th Eol 134 159 KSOO021 WP204

SM4500CI G onMne I 134 159 KSOOO21 WP204

CNI Level TDlaI Residual Chlorine

Level T alai Residual Chlorine

Level Total Residual Chlorine

jlglL Acceptable 140 138 780 _198

Ievel TDIal Residual Chlorine

uolL

jlgL

IlnlL

Acceptable 138 138 780 -198

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 P oI

ERA A Waters Company

Study DMRQA-32

NPDES Permit M00089109

Laboratory Name City of Nevada WWTP

It 120113

DMRQA32 Final Report ERA A Waters Company

NPDES Permitll MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dales 031912 middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Analyte rlS End Point Code Performance Repolllld Anlgned evaluation Value Value

Acceptance Method O crlptlonLimite

Study USEPAlIIbStudy StMldard Code

Study DevIatIon

-- -shyDMRQA FathNd minnow (Tut Code 13) (cat WETOO2) 48Hr Acute Non-Renewal 25 C MHSF Poraum chloride

~- IlC50 Acceptable 512 456 I 239 - 674 I EPA 2000 456 109 KSOOO21-(------oP4RQA32

DMRQA Fathead minnow (Test Code 15) (cat WET004) Today Short temI ChroniC Dally Renewal MHSF Potalum chlol1de

0808

0810

0756

IC25 (ON) Growth

NOEC (ON) Growth

NOEC Survival

Acceptable

Acceptable

-- Acceptable

389

25

25

355

250

250

175 - 535

125 - 500

125 - SOO

EPA 1000 2002

EPA 1000 2002

EPA 1000 2002 -shy

355 900 KSOO021

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32

DMRQA Cerlodaphna dubla (Tut Code 19) (cat WETOOB) 48Hr Acute Renewal 25 C MHSF Potlllum chlorlde

[Os ILC50 Acceptable 442 342 I 179middot504 I EPA 2002 342 810 - LIltSOOO21 [ DMRciA3iJ

DMRQA Cerlodflphnla dubla (Tet Code 21) (cat WET010) Today Short term Chronic Dally Renewal MHSF Potlllum chloride

0767

0768

0766

IC25 Raproduction

NOEC ReproductIOn

NOEC Survival -~ -shy

Acceptable

Acceptable

Acceptable

283

25

25

259

250

250

123 - 395

125 - 500

125middot500

EPA 1002 2002

EPA 10022002

EPA 10022002-_ __ __ shy

259 679 KSOOO21

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32shyDMRQA Daphnia pulax (Tet Code 38) (ea WET015) 48Hr Acute Non-Renewal 25 C MHSF Potassium chloride

[0794 ILC50 I Acceptable I 565 525 I 232middot818 I EPA 2021 525 147~r-KSoo021 -r OMRQAi2---]

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 13of13 ~

AWaters Company

Pennittee Name City of Nevada WWTP Pennit Number MOO089109 EPA Lab Code KSOOO21

WET OrganismsITest ConditionsEnd Points Checklist

DMRQA Study 32 La bull Graded Result

Analyte Number Organisms I Conditions End Points Test

Required Acceptable

Not Accepblble (ComtctIYe

Action Required)

Fathead minnow (Test Code 13) 0754 48Hrbull Acute Non-Renewal 25middot C MHSF lC50

EPA 2000 0 lEI 0 Fathead minnow (Test Code 14) 0755 48Hrbull Acute Non-Renewal 25middot C 20 DMW LC50

0 0 0 Fathead minnow (Test Code 15) 0808 7 -day Short Ierm Chronic Daily Renewal MHSF IC25 (ON) Growth

EPA 1000 0 lEI 0 0810 7 -day Short term Chronic Daily Renewal MHSF NOEC (ON) Growth

EPA 1000 0 lEI 0 0756 7-day Short term Chronic Daily Renewal MHSF NOEC Survival

EPA 1000 0 IRI 0 Fathead minnow (Test Code 18) 0812 7 -day Short term Chronic Daily Renewal 20 DMW IC25 (ON) Growth

0 0 0 0814 7-day Short Ierm Chronic Daily Renewal 20 DMW NOEC (ON) Growth

0 0 0 0759 7-day Short term Chronic Daily Renewal 20 DMW NOEC Survival

0 0 0 CerIodaphnle dubla (Test Code 19) 0764 48Hr Acute Renewal 25middot C MHSF LCSO

EPA 2002 0 IXI 0 CerIodaphnla dubla (Test Code 20) 0765 48Hr Acute ReneWal 25- C 20 DMW LCSO

0 0 0 CerIodaphnla dubla (Tast Code 21) 0767

0768

0766

7-day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF

IC25 Reproduction

NOEC Reproduction

NOEC Survival

0

0

IXI

[8]

0

0 EPA 1002 0 lEI 0

CerIodaphnla dubla (Tn Code 22) one 7-day Short term Chronic Daily Renewal 20 DMW IC25 Reproduction

0771 7-day Short term Chronic Daily Renewal 20 DMW NOEC Reproduction 0 0 0

0769 7 -day Short term Chronic Daily Renewal 20 DMW NOEC Survival 0 0 0

0 0 0 Daphnia magna (Test Code 32) 0788 48Hr Acute Non-Renewal 25deg C MHSF LCSO

0 0 0

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

DMRQA32 Final Report ERA AWaters Company

NPoes Permit MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Illued 072712

WWTP Supervisor Study Dates 031912 middot070612 City of Neyada WWTP 16517 South 1338 Road Neyada MO 64772 417-448middot2761

Analyte Code

Analyte Unttll Performance Evaluation

Reported Value

Assigned Vllue

Accaptllnca Limb

Method DseMptlon Study Mean Study

Standard Devtatlon

USEPAub Code

Study

WP TRee _1 (calf 58B)

1000

1005

1010

1015

1020

1025

1030

1040

1050

1055

1070

1075

1090

1100

1105

1140

1150

1160

1165

1185

Aluminum

Antimony

Anlenic

Barium

Beryl~um

~on Cadmium

Chromium

Cobalt

Copper

Iron

fLead Manganese

Molybdenum

Nickel

Selenium

Silver

Strontium

Thallium

Vanedium

IJgIL

1J91L

1J91L

IJgIL

IJgIL

IJgIL

IJglL

IJglL

IJgIL

IJgIL

jJgL

IJglL

1J9L

IJglL

IJglL

1J91L

IJglL

IJgIL

jJgL

Jl9L_ _

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Not Acceptable

A~tatgt1ft

772

416

350

2350

462

1560

439

534

397

223

1070

843

1930

226

557

1600

366

143

669

966

778

413

347

2360

454

1660

427

541

362

217

1070

754

1860

214

507

1620

361

141

557

619middot932

286 -499

289 - 408

2050 - 2660

386 - 513

1350middot1930

364 - 485

471 - 612

317 - 406

194 - 240

946 - 1210

659 - 845

1670 - 2070

178 - 248

455 - 568

1290 - 1870

310 - 414

121 - 161

450 - 667

__99_1__ ~8-1110

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010821996

EPA 60108 21996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 60108 21996

EPA 6010B 21996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996

EPA 60108 2 1996

EPA 6010B 2 1996

EPA 6010B 2 1996 -shy

782

402

344 2350

444

1650

416

537

374

219

1080

756

1900

212

505

1590

360

140

555

980

446

211

190

850

202

972

166

224

159

965

495

325

732

103

224

969

203

672

319

446

KSOO021

KSOO021

KSOOO21

KSOOO21

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOO021

KSOOO21

KSOOO21

KSoo021

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

WP204

EPA 60108 21996 WP204

_- ---- shy1030

1040

1075

jcadmium

[chromium

Lampad

jJglL

jJglL

IJgIL

Acceptable

Acceptable

Acceptable

439

534

843

427

541

754

364 - 485

471 612

659 - 845

EPA 6010C 2000

EPA 6010C 2000

EPA 6010C 2000

416

537

756

166

224

325

KSOOO21

KSOOO21

KSOO021

WP204

WP204

WP204

e All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 Pof13 ~

DMRQA32 Final Report ERA AWaters Company

NPoes Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 middot0706112 City of Nevada WWTP 16517 South 1338 Road Nevad MO 84m 417-448middot2761

Analyte Code Analyte Units Performanu

Evaluation Reported

Value Assigned

Value Acceptance

Lim Method DeSCription Study Mesn

Study Stndard DevIlItion

USEPA Lab Code Study

wp rce Metal (cetil586J Aluminum EPA 2008 55 19981000 KS00021 WP204 iAcceptable 778 782 446IJglL 800 619middot932 Antimony EPA 2008 55 19981005 KSOOO21Acceptable 211 WP204413 402IJglL 404 286middot499 Arsenic EPA 2008 55 19981010 Acceptable 190 KS00021 WP204370 347 289 - 408 3441J91L ~rium1015 EPA 2008 55 1998 850 KSOOO21 WP204Acceptable 2350IJglL 2360 2360 2050 - 2660 Betylhum EPA 2008 55 19981020 WP204KS00021gil Acceptable 444 202431 454 386 - 513 cadmium EPA 2008 55 19981030 KS00021Acceptable 166 WP204gil 416 427 416364 middot485 Chromium EPA 2008 55 19981040 224 KS00021Acceptable 541 537 WP204IJglL 551 471 - 612

Cobah EPA 2008 55 19981050 KS00021 WP204Acceptable 374 159IJglL 377 362 317 - 406

Copper EPA 2008 5519981055 KS00021Acceptable 965 WP204IJglL 221 217 219194middot240 Iron EPA 2008 55 19981070 gIL 1080 495 KS00021 WP204Acceptable 10701040 946 - 1210

ead EPA 2008 5519981075 gIL KSOO021 WP204Acceptable 756 325760 754 659- 845

EPA 2008 55 19981090 ~nese KS00021gIL Acceptable 1900 732 WP2041940 1860 1670middot2070

EPA 2008 55 1998~enum1100 KSOOO21gIL Acceptable 103 WP204213 214 212178middot248 Nickel EPA 2008 5519981105 gIL 224 KSOO021 WP204Acceptable 505512 507 455 - 568

1140 Selenium EPA 2008 55 1998giL 1590 KS00021Acceptable 1620 969 WP2041600 1290middot1870

EPA 2008 551998I 1150 ~lIver KS00021Acceptable WP204322 361 310-414 360 203IJgIL 1165 Thallium EPA 2008 551998 319 KSOO021Acceptable 557 555 WP204538 450middot6671JgL

1185 Vanadium Nol Accepteble EPA 2008 551998 KS00021446 WP204991 980IJglL 1440 868middot1110

EPA 2008 5519981190 Zinc KS00021giL Acceptable 977 462 WP204993 975 _838middot 11~0 - - bull- -~

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 _ of13 ~

DMRQA32 Final Report ERA A Waters Company

NPOES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP SupelVlsor Study Dates 03119112 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 84772 417-448middot2761

Analyta Analyt8Code Unite Performence Reported AIIIUned

Evaluation Value Value Acceplll nee

LImite IiMthod Oeerlpllon

Study USEPALabStudyMn Standard Study DevIation

Code i

WP Trce Metals (Clltti 586J 1000 [Aluminum IlglL Acceptable 800 778 619-932 EPA 8020A 1998 782 446 KSOOO21 WP204 I

1005 [Antimony IlglL Acceptable 404 413 286-499 EPA 8020A 1998 402 211 KSOO021 WP204

1010 iAraenk IlglL Acceptable 370 347 289 - 408 EPA 802011 1998 344 190 KSOOO21 WP204

1015 ~lium 1l91L Acceptable 2360 2360 2050 - 2660 EPA 8020A 1998 2350 850 KS00021 WP204

1020 Seryffium IlgIL Acceptable 431 454 386 - 513 EPA 8020A 1998 444 202 KSOOO21 WP204

1030 ~mium IlgIL Acceptable 416 427 364 - 485 EPA 6020A 1998 416 166 KSOOO21 WP204

1040 Chromium IlQIL Acceptable 551 541 471 - 612 EPA 6020A 1998 537 224 KSOO021 WP204

1050 Cabalaquo IlQIL Acceptable 377 362 317 - 406 EPA 8020A 1998 374 159 KSOOO21 WP204

1055 Copper 1l91L Acceptable 221 217 194middot240 EPA 8020A 1998 219 965 KSOO021 WP204

1070 lroo 1l91L Acceptable 1040 1070 9Mi-1210 EPA 602011 1998 1080 495 KSOOO21 WP204

1075 ~ad IlglL Acceptable 760 754 659 - 845 EPA 6020A 1998 756 325 KSOOO21 WP204

1090 Manganese IlgIL Acceptable 1940 1860 1670 - 2070 EPA 602011 1998 1900 732 KSOO021 WP204

1100 MolytxIenum IlglL Acceptable 213 214 178-248 EPA 6020A 1998 212 103 KSOOO21 WP204

1105 Nickel IlgL Acceptable 512 507 455 - 568 EPA 602011 1998 505 224 KSOOO21 WP204

1140 Selenium IlglL Acceptable 1600 1620 1290 - 1870 EPA 8020A 1998 1590 969 KSOO021 WP204

1150 Silver 1l9L Acceptable 322 361 310 - 414 EPA 8020A 1998 360 203 KSOO021 WP204

1165 Thatlium 1l9L Acceptable 538 557 450 - 667 EPA 8020A 1998 555 319 KSOO021 WP204

1185 Vanadium IlQL Not Acceptable 1440 991 868-1110 EPA 8020A 1998 980 446 KSOO021 WP204

1190 Zinc IJgL Acceptable 993 975 838 -1120 EPA 8020A 1998 977 462 KSOO021 WP204

EPA 2451 3 1994

EPA 747011 1 1994

SM3500Cr 0 18th ED 1992

KS00021 WP204

KS00021 WP204

KSOO021 WP204

All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 13~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 031912 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448~2761

AII~ Code Ane~ Unltll Performnce

evaluation Reported

1Ilue Aalilned

1Ilue ~ptenc

Umltll Method Deecrtptloll Study Men Study

Stanclllrd Oevilltion

USEPA Leb Coda Study

WP Hexvent Chromium (ttl aN) 1045 HellllY81ent Chromium IJQL ---1 Aclteptable 1 580 1 606 1 494 712 1 EPA 7196A 1 19921 6Q4 ~4 I KSOOO21 WP204 J

EPA 1801 2 1993 672 0483 KSOOO21 WP204

SM2130B 18th ED 672 0483 KSOO021 WP2041992

SM21308 online 672 0483 KSOO021 WP204

EPA9012A 0836 00962 KSOO021 WP204

SM4500CN E 18th 0836 00962 KSOO021 WP204ED 1992

SM4500CN E online I 0836 00962 KSOO021 WP204

EPA 4201 1978 0491 0101 KSOO021 WP204

EPA 9066 1986 0491 0101 KSOO021 WP204

SM4500CI E 18th ED I 0850 00673 KSOO021 WP2041992

ISM4500CI E online 0850 00673 KSOO021 WP204

SM4500Ct G 18th ED I 0850 00673 KSOO021 WP2041992

e All analy1es are included in ERAs A2LA accreditation Lab Code 1539middot01 Pag1Oof13

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 03119112 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

Anltya Code Anltya UnMa Performanee

EVlluation Reported

Vllue Anlgned

Vllue Acceptance

Umltll Method Oeecrlptlon Study Meln Study

Satndlrd DevIation

USEPA lab Code

Study

WP Totll Reldulll ChIorlfHIlc 587J 1940 ITotal Residual Chlorine

-shy I mgll I Acceptable I 945 I 0822 I 0594 - 103 LSM4500CI CO onNne I 0850 - 00673 KSOOO21 WP204

ISM4500f~218th EO I 134 159 KSOOO21 WP204

SM4SOOCI E online KSOOO21 WP204

ISM4~~18th Eol 134 159 KSOO021 WP204

SM4500CI G onMne I 134 159 KSOOO21 WP204

CNI Level TDlaI Residual Chlorine

Level T alai Residual Chlorine

Level Total Residual Chlorine

jlglL Acceptable 140 138 780 _198

Ievel TDIal Residual Chlorine

uolL

jlgL

IlnlL

Acceptable 138 138 780 -198

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 P oI

ERA A Waters Company

Study DMRQA-32

NPDES Permit M00089109

Laboratory Name City of Nevada WWTP

It 120113

DMRQA32 Final Report ERA A Waters Company

NPDES Permitll MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dales 031912 middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Analyte rlS End Point Code Performance Repolllld Anlgned evaluation Value Value

Acceptance Method O crlptlonLimite

Study USEPAlIIbStudy StMldard Code

Study DevIatIon

-- -shyDMRQA FathNd minnow (Tut Code 13) (cat WETOO2) 48Hr Acute Non-Renewal 25 C MHSF Poraum chloride

~- IlC50 Acceptable 512 456 I 239 - 674 I EPA 2000 456 109 KSOOO21-(------oP4RQA32

DMRQA Fathead minnow (Test Code 15) (cat WET004) Today Short temI ChroniC Dally Renewal MHSF Potalum chlol1de

0808

0810

0756

IC25 (ON) Growth

NOEC (ON) Growth

NOEC Survival

Acceptable

Acceptable

-- Acceptable

389

25

25

355

250

250

175 - 535

125 - 500

125 - SOO

EPA 1000 2002

EPA 1000 2002

EPA 1000 2002 -shy

355 900 KSOO021

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32

DMRQA Cerlodaphna dubla (Tut Code 19) (cat WETOOB) 48Hr Acute Renewal 25 C MHSF Potlllum chlorlde

[Os ILC50 Acceptable 442 342 I 179middot504 I EPA 2002 342 810 - LIltSOOO21 [ DMRciA3iJ

DMRQA Cerlodflphnla dubla (Tet Code 21) (cat WET010) Today Short term Chronic Dally Renewal MHSF Potlllum chloride

0767

0768

0766

IC25 Raproduction

NOEC ReproductIOn

NOEC Survival -~ -shy

Acceptable

Acceptable

Acceptable

283

25

25

259

250

250

123 - 395

125 - 500

125middot500

EPA 1002 2002

EPA 10022002

EPA 10022002-_ __ __ shy

259 679 KSOOO21

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32shyDMRQA Daphnia pulax (Tet Code 38) (ea WET015) 48Hr Acute Non-Renewal 25 C MHSF Potassium chloride

[0794 ILC50 I Acceptable I 565 525 I 232middot818 I EPA 2021 525 147~r-KSoo021 -r OMRQAi2---]

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 13of13 ~

AWaters Company

Pennittee Name City of Nevada WWTP Pennit Number MOO089109 EPA Lab Code KSOOO21

WET OrganismsITest ConditionsEnd Points Checklist

DMRQA Study 32 La bull Graded Result

Analyte Number Organisms I Conditions End Points Test

Required Acceptable

Not Accepblble (ComtctIYe

Action Required)

Fathead minnow (Test Code 13) 0754 48Hrbull Acute Non-Renewal 25middot C MHSF lC50

EPA 2000 0 lEI 0 Fathead minnow (Test Code 14) 0755 48Hrbull Acute Non-Renewal 25middot C 20 DMW LC50

0 0 0 Fathead minnow (Test Code 15) 0808 7 -day Short Ierm Chronic Daily Renewal MHSF IC25 (ON) Growth

EPA 1000 0 lEI 0 0810 7 -day Short term Chronic Daily Renewal MHSF NOEC (ON) Growth

EPA 1000 0 lEI 0 0756 7-day Short term Chronic Daily Renewal MHSF NOEC Survival

EPA 1000 0 IRI 0 Fathead minnow (Test Code 18) 0812 7 -day Short term Chronic Daily Renewal 20 DMW IC25 (ON) Growth

0 0 0 0814 7-day Short Ierm Chronic Daily Renewal 20 DMW NOEC (ON) Growth

0 0 0 0759 7-day Short term Chronic Daily Renewal 20 DMW NOEC Survival

0 0 0 CerIodaphnle dubla (Test Code 19) 0764 48Hr Acute Renewal 25middot C MHSF LCSO

EPA 2002 0 IXI 0 CerIodaphnla dubla (Test Code 20) 0765 48Hr Acute ReneWal 25- C 20 DMW LCSO

0 0 0 CerIodaphnla dubla (Tast Code 21) 0767

0768

0766

7-day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF

IC25 Reproduction

NOEC Reproduction

NOEC Survival

0

0

IXI

[8]

0

0 EPA 1002 0 lEI 0

CerIodaphnla dubla (Tn Code 22) one 7-day Short term Chronic Daily Renewal 20 DMW IC25 Reproduction

0771 7-day Short term Chronic Daily Renewal 20 DMW NOEC Reproduction 0 0 0

0769 7 -day Short term Chronic Daily Renewal 20 DMW NOEC Survival 0 0 0

0 0 0 Daphnia magna (Test Code 32) 0788 48Hr Acute Non-Renewal 25deg C MHSF LCSO

0 0 0

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

DMRQA32 Final Report ERA AWaters Company

NPoes Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0727112

WWTP Supervisor Study Dates 0311912 middot0706112 City of Nevada WWTP 16517 South 1338 Road Nevad MO 84m 417-448middot2761

Analyte Code Analyte Units Performanu

Evaluation Reported

Value Assigned

Value Acceptance

Lim Method DeSCription Study Mesn

Study Stndard DevIlItion

USEPA Lab Code Study

wp rce Metal (cetil586J Aluminum EPA 2008 55 19981000 KS00021 WP204 iAcceptable 778 782 446IJglL 800 619middot932 Antimony EPA 2008 55 19981005 KSOOO21Acceptable 211 WP204413 402IJglL 404 286middot499 Arsenic EPA 2008 55 19981010 Acceptable 190 KS00021 WP204370 347 289 - 408 3441J91L ~rium1015 EPA 2008 55 1998 850 KSOOO21 WP204Acceptable 2350IJglL 2360 2360 2050 - 2660 Betylhum EPA 2008 55 19981020 WP204KS00021gil Acceptable 444 202431 454 386 - 513 cadmium EPA 2008 55 19981030 KS00021Acceptable 166 WP204gil 416 427 416364 middot485 Chromium EPA 2008 55 19981040 224 KS00021Acceptable 541 537 WP204IJglL 551 471 - 612

Cobah EPA 2008 55 19981050 KS00021 WP204Acceptable 374 159IJglL 377 362 317 - 406

Copper EPA 2008 5519981055 KS00021Acceptable 965 WP204IJglL 221 217 219194middot240 Iron EPA 2008 55 19981070 gIL 1080 495 KS00021 WP204Acceptable 10701040 946 - 1210

ead EPA 2008 5519981075 gIL KSOO021 WP204Acceptable 756 325760 754 659- 845

EPA 2008 55 19981090 ~nese KS00021gIL Acceptable 1900 732 WP2041940 1860 1670middot2070

EPA 2008 55 1998~enum1100 KSOOO21gIL Acceptable 103 WP204213 214 212178middot248 Nickel EPA 2008 5519981105 gIL 224 KSOO021 WP204Acceptable 505512 507 455 - 568

1140 Selenium EPA 2008 55 1998giL 1590 KS00021Acceptable 1620 969 WP2041600 1290middot1870

EPA 2008 551998I 1150 ~lIver KS00021Acceptable WP204322 361 310-414 360 203IJgIL 1165 Thallium EPA 2008 551998 319 KSOO021Acceptable 557 555 WP204538 450middot6671JgL

1185 Vanadium Nol Accepteble EPA 2008 551998 KS00021446 WP204991 980IJglL 1440 868middot1110

EPA 2008 5519981190 Zinc KS00021giL Acceptable 977 462 WP204993 975 _838middot 11~0 - - bull- -~

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 _ of13 ~

DMRQA32 Final Report ERA A Waters Company

NPOES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP SupelVlsor Study Dates 03119112 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 84772 417-448middot2761

Analyta Analyt8Code Unite Performence Reported AIIIUned

Evaluation Value Value Acceplll nee

LImite IiMthod Oeerlpllon

Study USEPALabStudyMn Standard Study DevIation

Code i

WP Trce Metals (Clltti 586J 1000 [Aluminum IlglL Acceptable 800 778 619-932 EPA 8020A 1998 782 446 KSOOO21 WP204 I

1005 [Antimony IlglL Acceptable 404 413 286-499 EPA 8020A 1998 402 211 KSOO021 WP204

1010 iAraenk IlglL Acceptable 370 347 289 - 408 EPA 802011 1998 344 190 KSOOO21 WP204

1015 ~lium 1l91L Acceptable 2360 2360 2050 - 2660 EPA 8020A 1998 2350 850 KS00021 WP204

1020 Seryffium IlgIL Acceptable 431 454 386 - 513 EPA 8020A 1998 444 202 KSOOO21 WP204

1030 ~mium IlgIL Acceptable 416 427 364 - 485 EPA 6020A 1998 416 166 KSOOO21 WP204

1040 Chromium IlQIL Acceptable 551 541 471 - 612 EPA 6020A 1998 537 224 KSOO021 WP204

1050 Cabalaquo IlQIL Acceptable 377 362 317 - 406 EPA 8020A 1998 374 159 KSOOO21 WP204

1055 Copper 1l91L Acceptable 221 217 194middot240 EPA 8020A 1998 219 965 KSOO021 WP204

1070 lroo 1l91L Acceptable 1040 1070 9Mi-1210 EPA 602011 1998 1080 495 KSOOO21 WP204

1075 ~ad IlglL Acceptable 760 754 659 - 845 EPA 6020A 1998 756 325 KSOOO21 WP204

1090 Manganese IlgIL Acceptable 1940 1860 1670 - 2070 EPA 602011 1998 1900 732 KSOO021 WP204

1100 MolytxIenum IlglL Acceptable 213 214 178-248 EPA 6020A 1998 212 103 KSOOO21 WP204

1105 Nickel IlgL Acceptable 512 507 455 - 568 EPA 602011 1998 505 224 KSOOO21 WP204

1140 Selenium IlglL Acceptable 1600 1620 1290 - 1870 EPA 8020A 1998 1590 969 KSOO021 WP204

1150 Silver 1l9L Acceptable 322 361 310 - 414 EPA 8020A 1998 360 203 KSOO021 WP204

1165 Thatlium 1l9L Acceptable 538 557 450 - 667 EPA 8020A 1998 555 319 KSOO021 WP204

1185 Vanadium IlQL Not Acceptable 1440 991 868-1110 EPA 8020A 1998 980 446 KSOO021 WP204

1190 Zinc IJgL Acceptable 993 975 838 -1120 EPA 8020A 1998 977 462 KSOO021 WP204

EPA 2451 3 1994

EPA 747011 1 1994

SM3500Cr 0 18th ED 1992

KS00021 WP204

KS00021 WP204

KSOO021 WP204

All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 13~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 031912 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448~2761

AII~ Code Ane~ Unltll Performnce

evaluation Reported

1Ilue Aalilned

1Ilue ~ptenc

Umltll Method Deecrtptloll Study Men Study

Stanclllrd Oevilltion

USEPA Leb Coda Study

WP Hexvent Chromium (ttl aN) 1045 HellllY81ent Chromium IJQL ---1 Aclteptable 1 580 1 606 1 494 712 1 EPA 7196A 1 19921 6Q4 ~4 I KSOOO21 WP204 J

EPA 1801 2 1993 672 0483 KSOOO21 WP204

SM2130B 18th ED 672 0483 KSOO021 WP2041992

SM21308 online 672 0483 KSOO021 WP204

EPA9012A 0836 00962 KSOO021 WP204

SM4500CN E 18th 0836 00962 KSOO021 WP204ED 1992

SM4500CN E online I 0836 00962 KSOO021 WP204

EPA 4201 1978 0491 0101 KSOO021 WP204

EPA 9066 1986 0491 0101 KSOO021 WP204

SM4500CI E 18th ED I 0850 00673 KSOO021 WP2041992

ISM4500CI E online 0850 00673 KSOO021 WP204

SM4500Ct G 18th ED I 0850 00673 KSOO021 WP2041992

e All analy1es are included in ERAs A2LA accreditation Lab Code 1539middot01 Pag1Oof13

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 03119112 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

Anltya Code Anltya UnMa Performanee

EVlluation Reported

Vllue Anlgned

Vllue Acceptance

Umltll Method Oeecrlptlon Study Meln Study

Satndlrd DevIation

USEPA lab Code

Study

WP Totll Reldulll ChIorlfHIlc 587J 1940 ITotal Residual Chlorine

-shy I mgll I Acceptable I 945 I 0822 I 0594 - 103 LSM4500CI CO onNne I 0850 - 00673 KSOOO21 WP204

ISM4500f~218th EO I 134 159 KSOOO21 WP204

SM4SOOCI E online KSOOO21 WP204

ISM4~~18th Eol 134 159 KSOO021 WP204

SM4500CI G onMne I 134 159 KSOOO21 WP204

CNI Level TDlaI Residual Chlorine

Level T alai Residual Chlorine

Level Total Residual Chlorine

jlglL Acceptable 140 138 780 _198

Ievel TDIal Residual Chlorine

uolL

jlgL

IlnlL

Acceptable 138 138 780 -198

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 P oI

ERA A Waters Company

Study DMRQA-32

NPDES Permit M00089109

Laboratory Name City of Nevada WWTP

It 120113

DMRQA32 Final Report ERA A Waters Company

NPDES Permitll MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dales 031912 middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Analyte rlS End Point Code Performance Repolllld Anlgned evaluation Value Value

Acceptance Method O crlptlonLimite

Study USEPAlIIbStudy StMldard Code

Study DevIatIon

-- -shyDMRQA FathNd minnow (Tut Code 13) (cat WETOO2) 48Hr Acute Non-Renewal 25 C MHSF Poraum chloride

~- IlC50 Acceptable 512 456 I 239 - 674 I EPA 2000 456 109 KSOOO21-(------oP4RQA32

DMRQA Fathead minnow (Test Code 15) (cat WET004) Today Short temI ChroniC Dally Renewal MHSF Potalum chlol1de

0808

0810

0756

IC25 (ON) Growth

NOEC (ON) Growth

NOEC Survival

Acceptable

Acceptable

-- Acceptable

389

25

25

355

250

250

175 - 535

125 - 500

125 - SOO

EPA 1000 2002

EPA 1000 2002

EPA 1000 2002 -shy

355 900 KSOO021

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32

DMRQA Cerlodaphna dubla (Tut Code 19) (cat WETOOB) 48Hr Acute Renewal 25 C MHSF Potlllum chlorlde

[Os ILC50 Acceptable 442 342 I 179middot504 I EPA 2002 342 810 - LIltSOOO21 [ DMRciA3iJ

DMRQA Cerlodflphnla dubla (Tet Code 21) (cat WET010) Today Short term Chronic Dally Renewal MHSF Potlllum chloride

0767

0768

0766

IC25 Raproduction

NOEC ReproductIOn

NOEC Survival -~ -shy

Acceptable

Acceptable

Acceptable

283

25

25

259

250

250

123 - 395

125 - 500

125middot500

EPA 1002 2002

EPA 10022002

EPA 10022002-_ __ __ shy

259 679 KSOOO21

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32shyDMRQA Daphnia pulax (Tet Code 38) (ea WET015) 48Hr Acute Non-Renewal 25 C MHSF Potassium chloride

[0794 ILC50 I Acceptable I 565 525 I 232middot818 I EPA 2021 525 147~r-KSoo021 -r OMRQAi2---]

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 13of13 ~

AWaters Company

Pennittee Name City of Nevada WWTP Pennit Number MOO089109 EPA Lab Code KSOOO21

WET OrganismsITest ConditionsEnd Points Checklist

DMRQA Study 32 La bull Graded Result

Analyte Number Organisms I Conditions End Points Test

Required Acceptable

Not Accepblble (ComtctIYe

Action Required)

Fathead minnow (Test Code 13) 0754 48Hrbull Acute Non-Renewal 25middot C MHSF lC50

EPA 2000 0 lEI 0 Fathead minnow (Test Code 14) 0755 48Hrbull Acute Non-Renewal 25middot C 20 DMW LC50

0 0 0 Fathead minnow (Test Code 15) 0808 7 -day Short Ierm Chronic Daily Renewal MHSF IC25 (ON) Growth

EPA 1000 0 lEI 0 0810 7 -day Short term Chronic Daily Renewal MHSF NOEC (ON) Growth

EPA 1000 0 lEI 0 0756 7-day Short term Chronic Daily Renewal MHSF NOEC Survival

EPA 1000 0 IRI 0 Fathead minnow (Test Code 18) 0812 7 -day Short term Chronic Daily Renewal 20 DMW IC25 (ON) Growth

0 0 0 0814 7-day Short Ierm Chronic Daily Renewal 20 DMW NOEC (ON) Growth

0 0 0 0759 7-day Short term Chronic Daily Renewal 20 DMW NOEC Survival

0 0 0 CerIodaphnle dubla (Test Code 19) 0764 48Hr Acute Renewal 25middot C MHSF LCSO

EPA 2002 0 IXI 0 CerIodaphnla dubla (Test Code 20) 0765 48Hr Acute ReneWal 25- C 20 DMW LCSO

0 0 0 CerIodaphnla dubla (Tast Code 21) 0767

0768

0766

7-day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF

IC25 Reproduction

NOEC Reproduction

NOEC Survival

0

0

IXI

[8]

0

0 EPA 1002 0 lEI 0

CerIodaphnla dubla (Tn Code 22) one 7-day Short term Chronic Daily Renewal 20 DMW IC25 Reproduction

0771 7-day Short term Chronic Daily Renewal 20 DMW NOEC Reproduction 0 0 0

0769 7 -day Short term Chronic Daily Renewal 20 DMW NOEC Survival 0 0 0

0 0 0 Daphnia magna (Test Code 32) 0788 48Hr Acute Non-Renewal 25deg C MHSF LCSO

0 0 0

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

DMRQA32 Final Report ERA A Waters Company

NPOES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP SupelVlsor Study Dates 03119112 - 070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 84772 417-448middot2761

Analyta Analyt8Code Unite Performence Reported AIIIUned

Evaluation Value Value Acceplll nee

LImite IiMthod Oeerlpllon

Study USEPALabStudyMn Standard Study DevIation

Code i

WP Trce Metals (Clltti 586J 1000 [Aluminum IlglL Acceptable 800 778 619-932 EPA 8020A 1998 782 446 KSOOO21 WP204 I

1005 [Antimony IlglL Acceptable 404 413 286-499 EPA 8020A 1998 402 211 KSOO021 WP204

1010 iAraenk IlglL Acceptable 370 347 289 - 408 EPA 802011 1998 344 190 KSOOO21 WP204

1015 ~lium 1l91L Acceptable 2360 2360 2050 - 2660 EPA 8020A 1998 2350 850 KS00021 WP204

1020 Seryffium IlgIL Acceptable 431 454 386 - 513 EPA 8020A 1998 444 202 KSOOO21 WP204

1030 ~mium IlgIL Acceptable 416 427 364 - 485 EPA 6020A 1998 416 166 KSOOO21 WP204

1040 Chromium IlQIL Acceptable 551 541 471 - 612 EPA 6020A 1998 537 224 KSOO021 WP204

1050 Cabalaquo IlQIL Acceptable 377 362 317 - 406 EPA 8020A 1998 374 159 KSOOO21 WP204

1055 Copper 1l91L Acceptable 221 217 194middot240 EPA 8020A 1998 219 965 KSOO021 WP204

1070 lroo 1l91L Acceptable 1040 1070 9Mi-1210 EPA 602011 1998 1080 495 KSOOO21 WP204

1075 ~ad IlglL Acceptable 760 754 659 - 845 EPA 6020A 1998 756 325 KSOOO21 WP204

1090 Manganese IlgIL Acceptable 1940 1860 1670 - 2070 EPA 602011 1998 1900 732 KSOO021 WP204

1100 MolytxIenum IlglL Acceptable 213 214 178-248 EPA 6020A 1998 212 103 KSOOO21 WP204

1105 Nickel IlgL Acceptable 512 507 455 - 568 EPA 602011 1998 505 224 KSOOO21 WP204

1140 Selenium IlglL Acceptable 1600 1620 1290 - 1870 EPA 8020A 1998 1590 969 KSOO021 WP204

1150 Silver 1l9L Acceptable 322 361 310 - 414 EPA 8020A 1998 360 203 KSOO021 WP204

1165 Thatlium 1l9L Acceptable 538 557 450 - 667 EPA 8020A 1998 555 319 KSOO021 WP204

1185 Vanadium IlQL Not Acceptable 1440 991 868-1110 EPA 8020A 1998 980 446 KSOO021 WP204

1190 Zinc IJgL Acceptable 993 975 838 -1120 EPA 8020A 1998 977 462 KSOO021 WP204

EPA 2451 3 1994

EPA 747011 1 1994

SM3500Cr 0 18th ED 1992

KS00021 WP204

KS00021 WP204

KSOO021 WP204

All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 13~

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 031912 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448~2761

AII~ Code Ane~ Unltll Performnce

evaluation Reported

1Ilue Aalilned

1Ilue ~ptenc

Umltll Method Deecrtptloll Study Men Study

Stanclllrd Oevilltion

USEPA Leb Coda Study

WP Hexvent Chromium (ttl aN) 1045 HellllY81ent Chromium IJQL ---1 Aclteptable 1 580 1 606 1 494 712 1 EPA 7196A 1 19921 6Q4 ~4 I KSOOO21 WP204 J

EPA 1801 2 1993 672 0483 KSOOO21 WP204

SM2130B 18th ED 672 0483 KSOO021 WP2041992

SM21308 online 672 0483 KSOO021 WP204

EPA9012A 0836 00962 KSOO021 WP204

SM4500CN E 18th 0836 00962 KSOO021 WP204ED 1992

SM4500CN E online I 0836 00962 KSOO021 WP204

EPA 4201 1978 0491 0101 KSOO021 WP204

EPA 9066 1986 0491 0101 KSOO021 WP204

SM4500CI E 18th ED I 0850 00673 KSOO021 WP2041992

ISM4500CI E online 0850 00673 KSOO021 WP204

SM4500Ct G 18th ED I 0850 00673 KSOO021 WP2041992

e All analy1es are included in ERAs A2LA accreditation Lab Code 1539middot01 Pag1Oof13

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 03119112 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

Anltya Code Anltya UnMa Performanee

EVlluation Reported

Vllue Anlgned

Vllue Acceptance

Umltll Method Oeecrlptlon Study Meln Study

Satndlrd DevIation

USEPA lab Code

Study

WP Totll Reldulll ChIorlfHIlc 587J 1940 ITotal Residual Chlorine

-shy I mgll I Acceptable I 945 I 0822 I 0594 - 103 LSM4500CI CO onNne I 0850 - 00673 KSOOO21 WP204

ISM4500f~218th EO I 134 159 KSOOO21 WP204

SM4SOOCI E online KSOOO21 WP204

ISM4~~18th Eol 134 159 KSOO021 WP204

SM4500CI G onMne I 134 159 KSOOO21 WP204

CNI Level TDlaI Residual Chlorine

Level T alai Residual Chlorine

Level Total Residual Chlorine

jlglL Acceptable 140 138 780 _198

Ievel TDIal Residual Chlorine

uolL

jlgL

IlnlL

Acceptable 138 138 780 -198

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 P oI

ERA A Waters Company

Study DMRQA-32

NPDES Permit M00089109

Laboratory Name City of Nevada WWTP

It 120113

DMRQA32 Final Report ERA A Waters Company

NPDES Permitll MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dales 031912 middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Analyte rlS End Point Code Performance Repolllld Anlgned evaluation Value Value

Acceptance Method O crlptlonLimite

Study USEPAlIIbStudy StMldard Code

Study DevIatIon

-- -shyDMRQA FathNd minnow (Tut Code 13) (cat WETOO2) 48Hr Acute Non-Renewal 25 C MHSF Poraum chloride

~- IlC50 Acceptable 512 456 I 239 - 674 I EPA 2000 456 109 KSOOO21-(------oP4RQA32

DMRQA Fathead minnow (Test Code 15) (cat WET004) Today Short temI ChroniC Dally Renewal MHSF Potalum chlol1de

0808

0810

0756

IC25 (ON) Growth

NOEC (ON) Growth

NOEC Survival

Acceptable

Acceptable

-- Acceptable

389

25

25

355

250

250

175 - 535

125 - 500

125 - SOO

EPA 1000 2002

EPA 1000 2002

EPA 1000 2002 -shy

355 900 KSOO021

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32

DMRQA Cerlodaphna dubla (Tut Code 19) (cat WETOOB) 48Hr Acute Renewal 25 C MHSF Potlllum chlorlde

[Os ILC50 Acceptable 442 342 I 179middot504 I EPA 2002 342 810 - LIltSOOO21 [ DMRciA3iJ

DMRQA Cerlodflphnla dubla (Tet Code 21) (cat WET010) Today Short term Chronic Dally Renewal MHSF Potlllum chloride

0767

0768

0766

IC25 Raproduction

NOEC ReproductIOn

NOEC Survival -~ -shy

Acceptable

Acceptable

Acceptable

283

25

25

259

250

250

123 - 395

125 - 500

125middot500

EPA 1002 2002

EPA 10022002

EPA 10022002-_ __ __ shy

259 679 KSOOO21

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32shyDMRQA Daphnia pulax (Tet Code 38) (ea WET015) 48Hr Acute Non-Renewal 25 C MHSF Potassium chloride

[0794 ILC50 I Acceptable I 565 525 I 232middot818 I EPA 2021 525 147~r-KSoo021 -r OMRQAi2---]

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 13of13 ~

AWaters Company

Pennittee Name City of Nevada WWTP Pennit Number MOO089109 EPA Lab Code KSOOO21

WET OrganismsITest ConditionsEnd Points Checklist

DMRQA Study 32 La bull Graded Result

Analyte Number Organisms I Conditions End Points Test

Required Acceptable

Not Accepblble (ComtctIYe

Action Required)

Fathead minnow (Test Code 13) 0754 48Hrbull Acute Non-Renewal 25middot C MHSF lC50

EPA 2000 0 lEI 0 Fathead minnow (Test Code 14) 0755 48Hrbull Acute Non-Renewal 25middot C 20 DMW LC50

0 0 0 Fathead minnow (Test Code 15) 0808 7 -day Short Ierm Chronic Daily Renewal MHSF IC25 (ON) Growth

EPA 1000 0 lEI 0 0810 7 -day Short term Chronic Daily Renewal MHSF NOEC (ON) Growth

EPA 1000 0 lEI 0 0756 7-day Short term Chronic Daily Renewal MHSF NOEC Survival

EPA 1000 0 IRI 0 Fathead minnow (Test Code 18) 0812 7 -day Short term Chronic Daily Renewal 20 DMW IC25 (ON) Growth

0 0 0 0814 7-day Short Ierm Chronic Daily Renewal 20 DMW NOEC (ON) Growth

0 0 0 0759 7-day Short term Chronic Daily Renewal 20 DMW NOEC Survival

0 0 0 CerIodaphnle dubla (Test Code 19) 0764 48Hr Acute Renewal 25middot C MHSF LCSO

EPA 2002 0 IXI 0 CerIodaphnla dubla (Test Code 20) 0765 48Hr Acute ReneWal 25- C 20 DMW LCSO

0 0 0 CerIodaphnla dubla (Tast Code 21) 0767

0768

0766

7-day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF

IC25 Reproduction

NOEC Reproduction

NOEC Survival

0

0

IXI

[8]

0

0 EPA 1002 0 lEI 0

CerIodaphnla dubla (Tn Code 22) one 7-day Short term Chronic Daily Renewal 20 DMW IC25 Reproduction

0771 7-day Short term Chronic Daily Renewal 20 DMW NOEC Reproduction 0 0 0

0769 7 -day Short term Chronic Daily Renewal 20 DMW NOEC Survival 0 0 0

0 0 0 Daphnia magna (Test Code 32) 0788 48Hr Acute Non-Renewal 25deg C MHSF LCSO

0 0 0

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

DMRQA32 Final Report ERA A Waters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 031912 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448~2761

AII~ Code Ane~ Unltll Performnce

evaluation Reported

1Ilue Aalilned

1Ilue ~ptenc

Umltll Method Deecrtptloll Study Men Study

Stanclllrd Oevilltion

USEPA Leb Coda Study

WP Hexvent Chromium (ttl aN) 1045 HellllY81ent Chromium IJQL ---1 Aclteptable 1 580 1 606 1 494 712 1 EPA 7196A 1 19921 6Q4 ~4 I KSOOO21 WP204 J

EPA 1801 2 1993 672 0483 KSOOO21 WP204

SM2130B 18th ED 672 0483 KSOO021 WP2041992

SM21308 online 672 0483 KSOO021 WP204

EPA9012A 0836 00962 KSOO021 WP204

SM4500CN E 18th 0836 00962 KSOO021 WP204ED 1992

SM4500CN E online I 0836 00962 KSOO021 WP204

EPA 4201 1978 0491 0101 KSOO021 WP204

EPA 9066 1986 0491 0101 KSOO021 WP204

SM4500CI E 18th ED I 0850 00673 KSOO021 WP2041992

ISM4500CI E online 0850 00673 KSOO021 WP204

SM4500Ct G 18th ED I 0850 00673 KSOO021 WP2041992

e All analy1es are included in ERAs A2LA accreditation Lab Code 1539middot01 Pag1Oof13

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 03119112 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

Anltya Code Anltya UnMa Performanee

EVlluation Reported

Vllue Anlgned

Vllue Acceptance

Umltll Method Oeecrlptlon Study Meln Study

Satndlrd DevIation

USEPA lab Code

Study

WP Totll Reldulll ChIorlfHIlc 587J 1940 ITotal Residual Chlorine

-shy I mgll I Acceptable I 945 I 0822 I 0594 - 103 LSM4500CI CO onNne I 0850 - 00673 KSOOO21 WP204

ISM4500f~218th EO I 134 159 KSOOO21 WP204

SM4SOOCI E online KSOOO21 WP204

ISM4~~18th Eol 134 159 KSOO021 WP204

SM4500CI G onMne I 134 159 KSOOO21 WP204

CNI Level TDlaI Residual Chlorine

Level T alai Residual Chlorine

Level Total Residual Chlorine

jlglL Acceptable 140 138 780 _198

Ievel TDIal Residual Chlorine

uolL

jlgL

IlnlL

Acceptable 138 138 780 -198

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 P oI

ERA A Waters Company

Study DMRQA-32

NPDES Permit M00089109

Laboratory Name City of Nevada WWTP

It 120113

DMRQA32 Final Report ERA A Waters Company

NPDES Permitll MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dales 031912 middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Analyte rlS End Point Code Performance Repolllld Anlgned evaluation Value Value

Acceptance Method O crlptlonLimite

Study USEPAlIIbStudy StMldard Code

Study DevIatIon

-- -shyDMRQA FathNd minnow (Tut Code 13) (cat WETOO2) 48Hr Acute Non-Renewal 25 C MHSF Poraum chloride

~- IlC50 Acceptable 512 456 I 239 - 674 I EPA 2000 456 109 KSOOO21-(------oP4RQA32

DMRQA Fathead minnow (Test Code 15) (cat WET004) Today Short temI ChroniC Dally Renewal MHSF Potalum chlol1de

0808

0810

0756

IC25 (ON) Growth

NOEC (ON) Growth

NOEC Survival

Acceptable

Acceptable

-- Acceptable

389

25

25

355

250

250

175 - 535

125 - 500

125 - SOO

EPA 1000 2002

EPA 1000 2002

EPA 1000 2002 -shy

355 900 KSOO021

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32

DMRQA Cerlodaphna dubla (Tut Code 19) (cat WETOOB) 48Hr Acute Renewal 25 C MHSF Potlllum chlorlde

[Os ILC50 Acceptable 442 342 I 179middot504 I EPA 2002 342 810 - LIltSOOO21 [ DMRciA3iJ

DMRQA Cerlodflphnla dubla (Tet Code 21) (cat WET010) Today Short term Chronic Dally Renewal MHSF Potlllum chloride

0767

0768

0766

IC25 Raproduction

NOEC ReproductIOn

NOEC Survival -~ -shy

Acceptable

Acceptable

Acceptable

283

25

25

259

250

250

123 - 395

125 - 500

125middot500

EPA 1002 2002

EPA 10022002

EPA 10022002-_ __ __ shy

259 679 KSOOO21

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32shyDMRQA Daphnia pulax (Tet Code 38) (ea WET015) 48Hr Acute Non-Renewal 25 C MHSF Potassium chloride

[0794 ILC50 I Acceptable I 565 525 I 232middot818 I EPA 2021 525 147~r-KSoo021 -r OMRQAi2---]

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 13of13 ~

AWaters Company

Pennittee Name City of Nevada WWTP Pennit Number MOO089109 EPA Lab Code KSOOO21

WET OrganismsITest ConditionsEnd Points Checklist

DMRQA Study 32 La bull Graded Result

Analyte Number Organisms I Conditions End Points Test

Required Acceptable

Not Accepblble (ComtctIYe

Action Required)

Fathead minnow (Test Code 13) 0754 48Hrbull Acute Non-Renewal 25middot C MHSF lC50

EPA 2000 0 lEI 0 Fathead minnow (Test Code 14) 0755 48Hrbull Acute Non-Renewal 25middot C 20 DMW LC50

0 0 0 Fathead minnow (Test Code 15) 0808 7 -day Short Ierm Chronic Daily Renewal MHSF IC25 (ON) Growth

EPA 1000 0 lEI 0 0810 7 -day Short term Chronic Daily Renewal MHSF NOEC (ON) Growth

EPA 1000 0 lEI 0 0756 7-day Short term Chronic Daily Renewal MHSF NOEC Survival

EPA 1000 0 IRI 0 Fathead minnow (Test Code 18) 0812 7 -day Short term Chronic Daily Renewal 20 DMW IC25 (ON) Growth

0 0 0 0814 7-day Short Ierm Chronic Daily Renewal 20 DMW NOEC (ON) Growth

0 0 0 0759 7-day Short term Chronic Daily Renewal 20 DMW NOEC Survival

0 0 0 CerIodaphnle dubla (Test Code 19) 0764 48Hr Acute Renewal 25middot C MHSF LCSO

EPA 2002 0 IXI 0 CerIodaphnla dubla (Test Code 20) 0765 48Hr Acute ReneWal 25- C 20 DMW LCSO

0 0 0 CerIodaphnla dubla (Tast Code 21) 0767

0768

0766

7-day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF

IC25 Reproduction

NOEC Reproduction

NOEC Survival

0

0

IXI

[8]

0

0 EPA 1002 0 lEI 0

CerIodaphnla dubla (Tn Code 22) one 7-day Short term Chronic Daily Renewal 20 DMW IC25 Reproduction

0771 7-day Short term Chronic Daily Renewal 20 DMW NOEC Reproduction 0 0 0

0769 7 -day Short term Chronic Daily Renewal 20 DMW NOEC Survival 0 0 0

0 0 0 Daphnia magna (Test Code 32) 0788 48Hr Acute Non-Renewal 25deg C MHSF LCSO

0 0 0

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

DMRQA32 Final Report ERA AWaters Company

NPDES Permit M00089109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dates 03119112 - 0710612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417 -448middot2761

Anltya Code Anltya UnMa Performanee

EVlluation Reported

Vllue Anlgned

Vllue Acceptance

Umltll Method Oeecrlptlon Study Meln Study

Satndlrd DevIation

USEPA lab Code

Study

WP Totll Reldulll ChIorlfHIlc 587J 1940 ITotal Residual Chlorine

-shy I mgll I Acceptable I 945 I 0822 I 0594 - 103 LSM4500CI CO onNne I 0850 - 00673 KSOOO21 WP204

ISM4500f~218th EO I 134 159 KSOOO21 WP204

SM4SOOCI E online KSOOO21 WP204

ISM4~~18th Eol 134 159 KSOO021 WP204

SM4500CI G onMne I 134 159 KSOOO21 WP204

CNI Level TDlaI Residual Chlorine

Level T alai Residual Chlorine

Level Total Residual Chlorine

jlglL Acceptable 140 138 780 _198

Ievel TDIal Residual Chlorine

uolL

jlgL

IlnlL

Acceptable 138 138 780 -198

It All analytes are included in ERAs A2LA accreditation Lab Code 1539-01 P oI

ERA A Waters Company

Study DMRQA-32

NPDES Permit M00089109

Laboratory Name City of Nevada WWTP

It 120113

DMRQA32 Final Report ERA A Waters Company

NPDES Permitll MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dales 031912 middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Analyte rlS End Point Code Performance Repolllld Anlgned evaluation Value Value

Acceptance Method O crlptlonLimite

Study USEPAlIIbStudy StMldard Code

Study DevIatIon

-- -shyDMRQA FathNd minnow (Tut Code 13) (cat WETOO2) 48Hr Acute Non-Renewal 25 C MHSF Poraum chloride

~- IlC50 Acceptable 512 456 I 239 - 674 I EPA 2000 456 109 KSOOO21-(------oP4RQA32

DMRQA Fathead minnow (Test Code 15) (cat WET004) Today Short temI ChroniC Dally Renewal MHSF Potalum chlol1de

0808

0810

0756

IC25 (ON) Growth

NOEC (ON) Growth

NOEC Survival

Acceptable

Acceptable

-- Acceptable

389

25

25

355

250

250

175 - 535

125 - 500

125 - SOO

EPA 1000 2002

EPA 1000 2002

EPA 1000 2002 -shy

355 900 KSOO021

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32

DMRQA Cerlodaphna dubla (Tut Code 19) (cat WETOOB) 48Hr Acute Renewal 25 C MHSF Potlllum chlorlde

[Os ILC50 Acceptable 442 342 I 179middot504 I EPA 2002 342 810 - LIltSOOO21 [ DMRciA3iJ

DMRQA Cerlodflphnla dubla (Tet Code 21) (cat WET010) Today Short term Chronic Dally Renewal MHSF Potlllum chloride

0767

0768

0766

IC25 Raproduction

NOEC ReproductIOn

NOEC Survival -~ -shy

Acceptable

Acceptable

Acceptable

283

25

25

259

250

250

123 - 395

125 - 500

125middot500

EPA 1002 2002

EPA 10022002

EPA 10022002-_ __ __ shy

259 679 KSOOO21

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32shyDMRQA Daphnia pulax (Tet Code 38) (ea WET015) 48Hr Acute Non-Renewal 25 C MHSF Potassium chloride

[0794 ILC50 I Acceptable I 565 525 I 232middot818 I EPA 2021 525 147~r-KSoo021 -r OMRQAi2---]

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 13of13 ~

AWaters Company

Pennittee Name City of Nevada WWTP Pennit Number MOO089109 EPA Lab Code KSOOO21

WET OrganismsITest ConditionsEnd Points Checklist

DMRQA Study 32 La bull Graded Result

Analyte Number Organisms I Conditions End Points Test

Required Acceptable

Not Accepblble (ComtctIYe

Action Required)

Fathead minnow (Test Code 13) 0754 48Hrbull Acute Non-Renewal 25middot C MHSF lC50

EPA 2000 0 lEI 0 Fathead minnow (Test Code 14) 0755 48Hrbull Acute Non-Renewal 25middot C 20 DMW LC50

0 0 0 Fathead minnow (Test Code 15) 0808 7 -day Short Ierm Chronic Daily Renewal MHSF IC25 (ON) Growth

EPA 1000 0 lEI 0 0810 7 -day Short term Chronic Daily Renewal MHSF NOEC (ON) Growth

EPA 1000 0 lEI 0 0756 7-day Short term Chronic Daily Renewal MHSF NOEC Survival

EPA 1000 0 IRI 0 Fathead minnow (Test Code 18) 0812 7 -day Short term Chronic Daily Renewal 20 DMW IC25 (ON) Growth

0 0 0 0814 7-day Short Ierm Chronic Daily Renewal 20 DMW NOEC (ON) Growth

0 0 0 0759 7-day Short term Chronic Daily Renewal 20 DMW NOEC Survival

0 0 0 CerIodaphnle dubla (Test Code 19) 0764 48Hr Acute Renewal 25middot C MHSF LCSO

EPA 2002 0 IXI 0 CerIodaphnla dubla (Test Code 20) 0765 48Hr Acute ReneWal 25- C 20 DMW LCSO

0 0 0 CerIodaphnla dubla (Tast Code 21) 0767

0768

0766

7-day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF

IC25 Reproduction

NOEC Reproduction

NOEC Survival

0

0

IXI

[8]

0

0 EPA 1002 0 lEI 0

CerIodaphnla dubla (Tn Code 22) one 7-day Short term Chronic Daily Renewal 20 DMW IC25 Reproduction

0771 7-day Short term Chronic Daily Renewal 20 DMW NOEC Reproduction 0 0 0

0769 7 -day Short term Chronic Daily Renewal 20 DMW NOEC Survival 0 0 0

0 0 0 Daphnia magna (Test Code 32) 0788 48Hr Acute Non-Renewal 25deg C MHSF LCSO

0 0 0

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

ERA A Waters Company

Study DMRQA-32

NPDES Permit M00089109

Laboratory Name City of Nevada WWTP

It 120113

DMRQA32 Final Report ERA A Waters Company

NPDES Permitll MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dales 031912 middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Analyte rlS End Point Code Performance Repolllld Anlgned evaluation Value Value

Acceptance Method O crlptlonLimite

Study USEPAlIIbStudy StMldard Code

Study DevIatIon

-- -shyDMRQA FathNd minnow (Tut Code 13) (cat WETOO2) 48Hr Acute Non-Renewal 25 C MHSF Poraum chloride

~- IlC50 Acceptable 512 456 I 239 - 674 I EPA 2000 456 109 KSOOO21-(------oP4RQA32

DMRQA Fathead minnow (Test Code 15) (cat WET004) Today Short temI ChroniC Dally Renewal MHSF Potalum chlol1de

0808

0810

0756

IC25 (ON) Growth

NOEC (ON) Growth

NOEC Survival

Acceptable

Acceptable

-- Acceptable

389

25

25

355

250

250

175 - 535

125 - 500

125 - SOO

EPA 1000 2002

EPA 1000 2002

EPA 1000 2002 -shy

355 900 KSOO021

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32

DMRQA Cerlodaphna dubla (Tut Code 19) (cat WETOOB) 48Hr Acute Renewal 25 C MHSF Potlllum chlorlde

[Os ILC50 Acceptable 442 342 I 179middot504 I EPA 2002 342 810 - LIltSOOO21 [ DMRciA3iJ

DMRQA Cerlodflphnla dubla (Tet Code 21) (cat WET010) Today Short term Chronic Dally Renewal MHSF Potlllum chloride

0767

0768

0766

IC25 Raproduction

NOEC ReproductIOn

NOEC Survival -~ -shy

Acceptable

Acceptable

Acceptable

283

25

25

259

250

250

123 - 395

125 - 500

125middot500

EPA 1002 2002

EPA 10022002

EPA 10022002-_ __ __ shy

259 679 KSOOO21

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32shyDMRQA Daphnia pulax (Tet Code 38) (ea WET015) 48Hr Acute Non-Renewal 25 C MHSF Potassium chloride

[0794 ILC50 I Acceptable I 565 525 I 232middot818 I EPA 2021 525 147~r-KSoo021 -r OMRQAi2---]

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 13of13 ~

AWaters Company

Pennittee Name City of Nevada WWTP Pennit Number MOO089109 EPA Lab Code KSOOO21

WET OrganismsITest ConditionsEnd Points Checklist

DMRQA Study 32 La bull Graded Result

Analyte Number Organisms I Conditions End Points Test

Required Acceptable

Not Accepblble (ComtctIYe

Action Required)

Fathead minnow (Test Code 13) 0754 48Hrbull Acute Non-Renewal 25middot C MHSF lC50

EPA 2000 0 lEI 0 Fathead minnow (Test Code 14) 0755 48Hrbull Acute Non-Renewal 25middot C 20 DMW LC50

0 0 0 Fathead minnow (Test Code 15) 0808 7 -day Short Ierm Chronic Daily Renewal MHSF IC25 (ON) Growth

EPA 1000 0 lEI 0 0810 7 -day Short term Chronic Daily Renewal MHSF NOEC (ON) Growth

EPA 1000 0 lEI 0 0756 7-day Short term Chronic Daily Renewal MHSF NOEC Survival

EPA 1000 0 IRI 0 Fathead minnow (Test Code 18) 0812 7 -day Short term Chronic Daily Renewal 20 DMW IC25 (ON) Growth

0 0 0 0814 7-day Short Ierm Chronic Daily Renewal 20 DMW NOEC (ON) Growth

0 0 0 0759 7-day Short term Chronic Daily Renewal 20 DMW NOEC Survival

0 0 0 CerIodaphnle dubla (Test Code 19) 0764 48Hr Acute Renewal 25middot C MHSF LCSO

EPA 2002 0 IXI 0 CerIodaphnla dubla (Test Code 20) 0765 48Hr Acute ReneWal 25- C 20 DMW LCSO

0 0 0 CerIodaphnla dubla (Tast Code 21) 0767

0768

0766

7-day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF

IC25 Reproduction

NOEC Reproduction

NOEC Survival

0

0

IXI

[8]

0

0 EPA 1002 0 lEI 0

CerIodaphnla dubla (Tn Code 22) one 7-day Short term Chronic Daily Renewal 20 DMW IC25 Reproduction

0771 7-day Short term Chronic Daily Renewal 20 DMW NOEC Reproduction 0 0 0

0769 7 -day Short term Chronic Daily Renewal 20 DMW NOEC Survival 0 0 0

0 0 0 Daphnia magna (Test Code 32) 0788 48Hr Acute Non-Renewal 25deg C MHSF LCSO

0 0 0

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

DMRQA32 Final Report ERA A Waters Company

NPDES Permitll MOOO89109 ERA Customer Number C480901 Permit Holder Mark Mendenhall Report Issued 0712712

WWTP Supervisor Study Dales 031912 middot070612 City of Nevada WWTP 16517 South 1338 Road Nevada MO 64772 417-448middot2761

Analyte rlS End Point Code Performance Repolllld Anlgned evaluation Value Value

Acceptance Method O crlptlonLimite

Study USEPAlIIbStudy StMldard Code

Study DevIatIon

-- -shyDMRQA FathNd minnow (Tut Code 13) (cat WETOO2) 48Hr Acute Non-Renewal 25 C MHSF Poraum chloride

~- IlC50 Acceptable 512 456 I 239 - 674 I EPA 2000 456 109 KSOOO21-(------oP4RQA32

DMRQA Fathead minnow (Test Code 15) (cat WET004) Today Short temI ChroniC Dally Renewal MHSF Potalum chlol1de

0808

0810

0756

IC25 (ON) Growth

NOEC (ON) Growth

NOEC Survival

Acceptable

Acceptable

-- Acceptable

389

25

25

355

250

250

175 - 535

125 - 500

125 - SOO

EPA 1000 2002

EPA 1000 2002

EPA 1000 2002 -shy

355 900 KSOO021

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32

DMRQA Cerlodaphna dubla (Tut Code 19) (cat WETOOB) 48Hr Acute Renewal 25 C MHSF Potlllum chlorlde

[Os ILC50 Acceptable 442 342 I 179middot504 I EPA 2002 342 810 - LIltSOOO21 [ DMRciA3iJ

DMRQA Cerlodflphnla dubla (Tet Code 21) (cat WET010) Today Short term Chronic Dally Renewal MHSF Potlllum chloride

0767

0768

0766

IC25 Raproduction

NOEC ReproductIOn

NOEC Survival -~ -shy

Acceptable

Acceptable

Acceptable

283

25

25

259

250

250

123 - 395

125 - 500

125middot500

EPA 1002 2002

EPA 10022002

EPA 10022002-_ __ __ shy

259 679 KSOOO21

KSOOO21

KSOOO21

DMRQA32

DMRQA32

DMRQA32shyDMRQA Daphnia pulax (Tet Code 38) (ea WET015) 48Hr Acute Non-Renewal 25 C MHSF Potassium chloride

[0794 ILC50 I Acceptable I 565 525 I 232middot818 I EPA 2021 525 147~r-KSoo021 -r OMRQAi2---]

e All analytes are included in ERAs A2LA accreditation lab Code 1539-01 13of13 ~

AWaters Company

Pennittee Name City of Nevada WWTP Pennit Number MOO089109 EPA Lab Code KSOOO21

WET OrganismsITest ConditionsEnd Points Checklist

DMRQA Study 32 La bull Graded Result

Analyte Number Organisms I Conditions End Points Test

Required Acceptable

Not Accepblble (ComtctIYe

Action Required)

Fathead minnow (Test Code 13) 0754 48Hrbull Acute Non-Renewal 25middot C MHSF lC50

EPA 2000 0 lEI 0 Fathead minnow (Test Code 14) 0755 48Hrbull Acute Non-Renewal 25middot C 20 DMW LC50

0 0 0 Fathead minnow (Test Code 15) 0808 7 -day Short Ierm Chronic Daily Renewal MHSF IC25 (ON) Growth

EPA 1000 0 lEI 0 0810 7 -day Short term Chronic Daily Renewal MHSF NOEC (ON) Growth

EPA 1000 0 lEI 0 0756 7-day Short term Chronic Daily Renewal MHSF NOEC Survival

EPA 1000 0 IRI 0 Fathead minnow (Test Code 18) 0812 7 -day Short term Chronic Daily Renewal 20 DMW IC25 (ON) Growth

0 0 0 0814 7-day Short Ierm Chronic Daily Renewal 20 DMW NOEC (ON) Growth

0 0 0 0759 7-day Short term Chronic Daily Renewal 20 DMW NOEC Survival

0 0 0 CerIodaphnle dubla (Test Code 19) 0764 48Hr Acute Renewal 25middot C MHSF LCSO

EPA 2002 0 IXI 0 CerIodaphnla dubla (Test Code 20) 0765 48Hr Acute ReneWal 25- C 20 DMW LCSO

0 0 0 CerIodaphnla dubla (Tast Code 21) 0767

0768

0766

7-day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF

IC25 Reproduction

NOEC Reproduction

NOEC Survival

0

0

IXI

[8]

0

0 EPA 1002 0 lEI 0

CerIodaphnla dubla (Tn Code 22) one 7-day Short term Chronic Daily Renewal 20 DMW IC25 Reproduction

0771 7-day Short term Chronic Daily Renewal 20 DMW NOEC Reproduction 0 0 0

0769 7 -day Short term Chronic Daily Renewal 20 DMW NOEC Survival 0 0 0

0 0 0 Daphnia magna (Test Code 32) 0788 48Hr Acute Non-Renewal 25deg C MHSF LCSO

0 0 0

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

AWaters Company

Pennittee Name City of Nevada WWTP Pennit Number MOO089109 EPA Lab Code KSOOO21

WET OrganismsITest ConditionsEnd Points Checklist

DMRQA Study 32 La bull Graded Result

Analyte Number Organisms I Conditions End Points Test

Required Acceptable

Not Accepblble (ComtctIYe

Action Required)

Fathead minnow (Test Code 13) 0754 48Hrbull Acute Non-Renewal 25middot C MHSF lC50

EPA 2000 0 lEI 0 Fathead minnow (Test Code 14) 0755 48Hrbull Acute Non-Renewal 25middot C 20 DMW LC50

0 0 0 Fathead minnow (Test Code 15) 0808 7 -day Short Ierm Chronic Daily Renewal MHSF IC25 (ON) Growth

EPA 1000 0 lEI 0 0810 7 -day Short term Chronic Daily Renewal MHSF NOEC (ON) Growth

EPA 1000 0 lEI 0 0756 7-day Short term Chronic Daily Renewal MHSF NOEC Survival

EPA 1000 0 IRI 0 Fathead minnow (Test Code 18) 0812 7 -day Short term Chronic Daily Renewal 20 DMW IC25 (ON) Growth

0 0 0 0814 7-day Short Ierm Chronic Daily Renewal 20 DMW NOEC (ON) Growth

0 0 0 0759 7-day Short term Chronic Daily Renewal 20 DMW NOEC Survival

0 0 0 CerIodaphnle dubla (Test Code 19) 0764 48Hr Acute Renewal 25middot C MHSF LCSO

EPA 2002 0 IXI 0 CerIodaphnla dubla (Test Code 20) 0765 48Hr Acute ReneWal 25- C 20 DMW LCSO

0 0 0 CerIodaphnla dubla (Tast Code 21) 0767

0768

0766

7-day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF EPA 1002

7 -day Short term Chronic Daily Renewal MHSF

IC25 Reproduction

NOEC Reproduction

NOEC Survival

0

0

IXI

[8]

0

0 EPA 1002 0 lEI 0

CerIodaphnla dubla (Tn Code 22) one 7-day Short term Chronic Daily Renewal 20 DMW IC25 Reproduction

0771 7-day Short term Chronic Daily Renewal 20 DMW NOEC Reproduction 0 0 0

0769 7 -day Short term Chronic Daily Renewal 20 DMW NOEC Survival 0 0 0

0 0 0 Daphnia magna (Test Code 32) 0788 48Hr Acute Non-Renewal 25deg C MHSF LCSO

0 0 0

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

A Waters Company

Permittee Name City of Nevada WWfP Permit Number M00089109 EPA Lab Code KSOOO21

WET OrganismsfTest ConditionsEnd Points Checklist

Laboratorys GIIIdIKI Rault

Not Acceptable Analyte Number

Organisms I Condition EndPoints Test Required

Acceptable (ComIctIve Actton

RequlnKl)

Daphnia pulex (Test Code 38) 0794 48Hrbull Acute Non-Renewal 25middot C MHSF lCSO

EPA 2021 0 IBl 0 MysId (Teat Code 42) 0798 48Hr Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Inland Sltverside (Teat Code 45) 0825 7~y Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0826 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0824 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 IIysId (Test Code 043) 0816 7 -day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0 0 0 0818 7-day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth

0 0 0 0799 7~y Short term Chronic Daily Renewal 40 FSW NOEC Survival

0 0 0 Inland sllwtrside (Tet Code 44) 0803 48Hrbull Acute Non-Renewal 25deg C 40 FSW lCSO

0 0 0 Sheepahead minnow (Test Code 46) 0804 4BHr Acute Non-Renewal 25 C 40 fSW LC50

0 0 0 Sheepahead minnow (Tnt Code 47) 0820 7-day Short term Chronic Daily Renewal 40 FSW IC25 (ON) Growth

0822 7 -day Short term Chronic Daily Renewal 40 FSW NOEC (ON) Growth 0 0 0

0805 7-day Short term Chronic Daily Renewal 40 FSW NOEC Survival 0 0 0

0 0 0

PrInt Name Date

IUse a separate checklist for EACH lab usedSignaturelT1tle

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

~ERA A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab COde KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded Result

I Not AcceptableAnalyte Test I Method Test Required Acceptable (Corrective Action Required)

MI

Potanlum EPA6010B 0 IX 0 EPA 2007 0 IX 0 Sulfate EPA 3000 0 IXJ 0 EPA 9056 0 1KI 0 ConducUvlty at 2SmiddotC EPA9050A 0 1KI 0 SM2510B 0 1KI 0 Fluoride EPA 3000 0 IXJ 0 EPA 9056 0 IXJ 0 Sodium EPA 2007 0 IXJ 0 EPA6010B 0 IXJ 0 Total Dluolved Sollde at 18OC SM2540C 0 IXJ 0 Total Solids at 105degC SM2540B 0 IXJ 0 Chloride EPA 9056 0 IXJ 0 EPA 3000 0 IXJ 0 SM45OOCI-E 0 IXJ 0 Alkalinity a CaC03 SM23206 0 IXJ 0

Hardneg

Nonfllterable Residue (TSS) SM2540D 0 IXJ 0Calcium EPA 2007 0 IXJ 0EPA6010B 0 1KI 0Magnesium EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0Calcium Hardness a CaC03 EPA 2007 0 IXJ 0SM2340B 0 IXJ 0EPA6010B 0 IXJ 0Total Hardn as CaC03 SM2340B 0 IXJ 0EPA 2007 0 IXJ 0EPA6010B 0 IXJ 0

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

A Waters (ompan~

Pennittee Name City of Nevada WlNTP PennH Number MOO089109 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (COmtCtIve ActIon Required)

gH

Test Required AcceptableAnalyte Tes f Method

pH EPA9040B 0 1amp1 0 EPA9040C 0 1amp1 0 SM4500H+ B 0 1amp1 0

SetQaable Solids

Settleable Solids SM2540F 0 1amp1 0

SoIIda Concentrate Non-fllterabie Residue (TSS) Total DIHoIved SolIds at 1809C Total Solids at 1059C

~ Non-fllterabie Residue (TSS) Total Dissolved Sollde at 180degC Total SoIIde at 10SOC

llroM Nutrients

Nitrate 18 N EPA 3532 0 1amp1 0 EPA 3000 0 1amp1 0 ortho-Phosphale as P EPA 3651 0 1amp1 0 AmmonlaasN EPA 3501 0 IampI 0 Nitrate + NHrIte 18 N EPA 3532 0 IRI 0EPA 3000 0 IRI 0

ComplelNutrenbi

Total phosphorus 18 P EPA 3654 0 IRI 0Total tQeldahl Nitrogen EPA 3512 0 IRI 0

lIIIdIt Nitrite as N EPA 3000 0 IRI 0EPA 3532 0 IRI 0EPA 9056 0 1amp1 0

QmnIm1 COD SM5220D 0 IRI 0

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO0891 09 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Teat I Method Teat Required

Laboratorys Graded Result

Acceptable 1 Not Acceptable (Corrective Action Required)

EPA 4104 D [EJ D CBOO SM5210B 0 [EJ 0 BOD SM5210B D [EJ D TOC

OJI II GnIaae Concentrate

n-Hexane Extractable Materlal(OampG) (Grav)

0i1ampGreiH

n-Hexane Extractable Materlal(OampG) (IR) n-Hexane Extractable Material(OampG) (Grav) EPA 1664A D [EJ 0

T1Jct Metals Aluminum EPA 2007 D [EJ D EPA 60108 D [EJ 0 EPA 2008 D [EJ D EPA6020A D [EJ D Arsenic EPA 2008 D [EJ D EPA6020A D [EJ D EPA6010B 0 00 0 EPA 2007 D [EJ 0 Lead EPA6010C 0 [EJ D EPA 2008 D [EJ D EPA6010B D [EJ D EPA6020A D [EJ D EPA 2007 D [EJ D Manganese EPA6020A D [EJ D EPA6010B EPA 2007 EPA 2008 Thallium

D D D

[EJ D [EJ D [EJ D

EPA6010B D D [EJEPA 2008 EPA 2007

D 0

[EJ D D [EJ

EPA6020A Zinc

D 00 D EPA 2008 D [EJ D

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

A Waters Company

Permittee Name City of Nevada WWTP Permit Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Analyte Test I Method Test Required

Laboratory Graded Result

Acceptable I Not Acceptable (Corrective ActIon Required)

EPA6020A 0 IRI 0 EPA 2007 0 IRI 0 EPA6010B 0 00 0 Antimony EPA 2008 0 IRI 0 EPA6020A 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 00 0 Beryllium EPA 2007 0 IRI 0 EPA6020A 0 IRI 0 EPA 2008 0 00 0 EPA6010B 0 IRI 0 Chromium EPA6010B 0 IRI 0 EPA6010C 0 IRI 0 EPA 6020A 0 00 0 EPA 2007 0 IRI 0 EPA 2008 0 IRI 0 Copper EPA 2008 0 IRI 0 EPA6010B 0 IRI 0 EPA 2007 0 1B1 0 EPA6020A 0 1B1 0 Nickel EPA6020A 0 1B1 0 EPA 2007 0 00 0 EPA6010B 0 00 0 EPA 2008 0 1B1 0 Barium EPA 2008 0 1B1 0 EPA6010B 0 1B1 0 EPA 2007 EPA6020A Boron

0 0

00 0 1B1 0

EPA 2007 EPA6010B Cadmium

0 0

00 0 1B1 0

EPA 2008 EPA6010B EPA 2007 EPA6010C EPA6020A Iron

0 0 0 0 0

IX 0 IRI 0 [BJ 0 [BJ 0 [BJ 0

EPA 2008 0 [BJ 0

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

A Waters Company

Permittee Name City of Nevada WWTP Penni Number MOO089109 EPA Lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratorys Graded Result

I Not Acceptable (Corrective ActIon Required)

EPA 2007

Test Required Analyle Test I Method Acceptable

0 lEI 0 EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 Molybdenum EPA6010B 0 lEI 0 EPA6020A 0 lEI 0 EPA 2008 0 00 0 EPA 2007 0 00 0 Vanadum EPA 2007 0 00 0 EPA6010B 0 00 0 EPA6020A 0 0 IBJ EPA 2008 0 0 lEI Cobalt EPA6020A 0 lEI 0 EPA6010B 0 lEI 0 EPA 2007 0 lEI 0 EPA 2008 0 00 0 Selenium EPA6010B 0 lEI 0 EPA6020A 0 00 0 EPA 2008 0 00 0 EPA 2007 0 lEI 0 Silver EPA 2008 0 lEI 0 EPA6020A 0 00 0 EPA6010B 0 00 0 EPA 2007 0 00 0 strontium EPA 2007 0 00 0 EPA 6010B 0 lEI 0

MIndur Mercury EPA 2451 0 lEI 0EPA 7470A 0 lEI 0

LowmiddotLay1 Mercury

Low Level Mercury

HaXllValel CbllllDllim Hexavalent Chromium EPA 7196A 0 lEI 0SM3500CrD 0 lEI 0

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

QERA A Waters Companj

Permittee Name City of Nevada WWTP Permit Number M000891 09 EPA lab Code KSOOO21

ChemistryMicrobiology Analyte Checklist

WP Study 204

Laboratory Graded RbullbulluH

Analyta Tnt f Method Tnt Required Acceptable I Not Acceptable (Corrective Action Required)

TurbIdity Turbidity SM2130B 0 [8] 0 EPA 1801 0 [8] 0

Total Cyanide

Cyanide total EPA9012A 0 [8] 0 SM4500CN E 0 [8] 0

IIltAI fMngllGa 4-AAP

Phenolics total EPA 9066 0 [8] 0 EPA 4201 0 [8] 0

I~IBlI~ICbkWDI Total Residual Chlortne SM4500CIG 0 [8] 0 SM4500CIE 0 [8] 0

LIMuvaJ Total Resklual Cblszd[JI Low Level Total Reldual Chtorine SM4500cIG 0 [8] 0 SM4500CIE 0 [8] 0

tYastaWIdBTIl g11m[JIJ MIcrobEl1I

Total Coliform (MF) Fecal Collfonns (MF) Ecoll (MF) Total Coliform (MPH) Fecal CoIlfonns (MPN) Ecoli (MPH)

Print Name Date

Use a separate checklist for EACH lab usedSignalurelTltle

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

A Waters Company

EPA Lab Code M000982Permittee Name City of Nevada WWTP Permit Number MOO089109

ChemistryMicrobiology Analyte Checklist OMRQA Study 32

Analyte Teat I Method

MI1s

Sulfate Total Diaaolved Solids at 180C Chloride Potaulum SodIum Fluoride AlkaHnlty aa CaC03 Total Solids at 10SC Conductivity at 2SC

Tet Requlntd

Labonltoty Graded Resu

Acceptable I Not Acceptable (Corrective Action Requlntd)

HardntU Non-Flltarable Residue (TSS) SM2540D Calcium Magnesium Calcium Hardness aa CaC03 Total Hardn aa CaC03

0 [amp] 0

RII pH SM4500H+B 0 lBl 0

Settlteblt Solids

Settleable SoHds

Sob Concentrate Non-Flltarable Residue (TSS) Total DIssolVed SOlids at 180middotC Total Solids at 10SC

hIIdI Non-Fllterable Residue (TSS) Total Diaaolved Sollda at 180C Total Solids at 10S-C

Simple Nutrients

AmmonlaaaN SM4500NH30 ortho-Phosphate aa P Nltrateaa N Nitrate + NItrtte aa N

0 IX 0

Complex Nutrients

Totallqeldahl Nitrogen Total phosphorus aa P

tmdta Nltrtteas N

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

ERAAWaters Company

Permittee Name City of Nevada WNTP Permit Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist

DMRQA Study 32

Analyt_ Teat I Method Teat Required

Laboratorys Graded Result

AceeptabIe I Not Acceptable (ComIcIiYe Action Required)

IlImiDd COD BOD SM5210B CBOD TOC

[J IX] [J

ilIll Grease Cgognlratlt

n-+lnane Extractable Material(OampG) (Grav)

011 I Gntau n-Hexane Extractable Meterial(OampG) (Gnrv) n-Hexane Extractable Materlal(OampG) (IR)

Tract MtIaIt Cadmium Laed Silver Vanadium Boron Selenium Thallium Barium Copper Iron Aluminum Molybdenum Zinc Antimony Chromium Nickel SlronUum Cobalt Araenlc Beryllium Mangane

IIAmIu Mercury

Low-lrntl Mercury Low Level Mercury

ltluvallDl Cbromium Hexavalent Chromium

TUJbIdky Tutbidtty

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

A Waters Compaoy

Permittee Name City of Nevada WWTP Permtt Number M00089109 EPA Lab Code M000982

ChemistryMicrobiology Analyte Checklist DMRQA Study 32

Analyle Test I Method Test Required

Laboratorys Graded Result

Acceptable I Not Acceptable (CometIVe ActIon RequlnKl)

Total Cyanide

Cyanide total

IotallblnoIIcs (4-Ayraquol

Phenolics total

Tobil RMJduaI ~blorllHl Total Residual Chlorine

Law-level T obIl BuIilUilI CbklllDl Low Level Total Residual Chlortne

WIlttYlIIBTII kgHform MicrobE Total Collforms eMF) Fecal Coliform (MF) Ecoll (MF) Total CoIlforms (MPN) Fecal CoIIforms (MPN) Ecoll(MPN)

Print Name Date

SignaturelTitle fUse a separate checklist for EACH lab used

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom

II Waters Company

DMRQA 32 Corrective Action Guidelines

Permit Holders

Upon reviewing your enclosed DMR-QA 32 final report you may notice that some analyte results have been evaluated as Not Acceptable For these analytes the USEPAs DMR-QA 32 announcement letter directs permit holders to consult with the laboratory and investigate any discrepancies or Not Acceptable evaluations reported by the PT Provider Permittees must identify and report to the state OMR-QA coordinator causes and system changes to correct the discrepancies and avoid their reoccurrence The corrective action report must be sent to the coordinator before October 5 2012 This means that for all Not Acceptable evaluations the laboratory must conduct an investigation identify the probtem and implement adequate corrective actions Your state may also require the laboratory to analyze a remedial QC or PT Sample as a demonstration that the corrective action implemented was successful ERA has contacted all state and regional coordinators and determined the type of remedial samples that they recommend or require

If any of your Not Acceptable results originated from your in-house laboratory an order form is enclosed listing the standards that you should order and analyze Your in-house laboratory will need to conduct its investigation and then analyze the listed standards to ensure that the identified problem has been corrected The corrective action report and if applicable the results of the analysis will then need to be forwarded to your OMR-QA coordinator by October 52012

You may receive an order form for both your in-house standards that have analytes evaluated as Not Acceptable as well as a list of standards that your outside or contract laboratory(ies) have with Not Acceptable evaluations Some agencies require corrective action on a case by case basis If you have a Not Acceptable evaluation but there is not an order form or a list of standards for your in-house or outside laboratories ERA recommends that you contact your DMR-QA Coordinator for their corrective action requirements if any

The standards listed in the attachments are based on general guidance given to us by the state or regional coordinators If you have any questions about your specific corrective action requirements please contact your state or regional coordinator directly

If you have any questions or to place an order please contact ERAs Customer Service Group at 1-888-372-0122

16341 Tabte MountalnPkwy GotdenCO 80403 Il 800-372-0122 II fax (303)421-0159 WWWIIRIqccom