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Roma, 31 Maggio 2018

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Page 1: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Roma, 31 Maggio 2018

Page 2: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Industry Mission & Vision

• Generate value for our Shareholders and our Clients being

partner of choice when competences, innovation, materials

and technologies have a critical role with a special focus on

Steel, Manufacturing, Space and Defense industries

• Create value and competitiveness throughout the entire life

cycle of projects, from R&D to end-of–life

• Be the key player in the technological transfer from

research up to the best innovative solutions for any

industrial application

Page 3: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Concept Design

Detail Design

System Specification

Procurement & Construction

Commi-ssioning

Through-Life

Management

Life

Extension

Early Stage Topics

Product/Process life cycle Cross topics

Intelligence &

Feasibility Analysis

Materials, Product & Process Innovation

Material Performance, & Condition assessement

Specialised engineering services (Development Support Services)

Programme

planning support

(Decision Support

Services)

Safety Assessment &

Compliance

Security &

Cybersecurity

Product / Process

Sustainability

Life Cycle

Assessment

Innovation &

Business strategy

Training & E-

learning Solutions

On site engineering and inspection services

INDUSTRY - Value proposition

Page 4: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Innovation drivers analysis

Ideas generation

landscape analysis

Conceptual design

Market strategy

FEATURED PROJECT – INTELLIGENCE AND BUSINESS ANALYSIS FOR ADDITIVE MANUFACTURING

Client: MIMETE (FOMAS GROUP)

Scope of work: Market Analysis and business plan, selection of more suitable production technology.

A new industrial initiative has been launched to manufacture metallic powders by gas atomization.

Contract value : xxx k€

Duration: 3 months

New opportunities regarding the alloy design, process and product development, participation in funded projects (Domestic an EU)

Innovation & Business

Strategy

Page 5: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Design for AM

Page 6: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Development of the metal alloy

The alloy design and the alloys development is necessary to define the best chemical

composition for AM processes.

This will lead to a new proprietary alloy, very suitable for AM technologies.

This alloy design and development will be focused on aluminum alloys.

The commercial Al alloys actually available for AM processes have limited mechanical

properties as shown in the Figure below (Metal AM - Metal powders – the raw materials).

The market needs an increase of mechanical behavior for high demanding applications

and this goal can be achieved by a proper new alloy design.

Page 7: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Material Renishaw EOS SLM

Solutions 3DS Sisma

Concept

Laser Applications

Stainless

steel 316L

316L, CX,

GP1, PH1

316L, 15-5, 17-4PH

316L, 17-4 PH 316L 316L, 17-4

PH,91RW

Food,

biomedical,

consumer

Ni-alloys In625, In718 In625, In718

In625,

In718,In939,

Hastelloy X

In718 Type not

specified In625, In718

Energy,

motorsport

Al-alloy AlSi10Mg AlSi10Mg

AlSi12,

AlSi10Mg,

AlSi7Mg,AlSi9

Cu3,AlMg4.5M

n0.4

AlSi12 AlSi12,

AlSi10Mg

AlSi12,

AlSi10Mg

Lightweight,

aerospace,

aviation

CoCr-alloy CoCrMo CoCrMo CoCrMo CoCrMo CoCrMo CoCrW Dental,

biomedical

Ti-alloys Ti6Al4V Ti6Al4V, CP Ti

Ti6Al4V,

Ti6Al7Nb, CP

Ti

Ti6Al4V, CP Ti Ti6Al4V Ti6Al4V, CP Ti

Biomedical,

lightweight,

aerospace

Tool steel Maraging

18Ni300

Maraging

18Ni300

H13, Maraging

18Ni300

Maraging

18Ni300

Maraging

18Ni300

Maraging

18Ni300

Tooling,

aerospace,

automotive

Cu-alloys Bronze Bronze Energy, heat

exchange

Precious Type not

specified Au, Pt, Ag

Jewellery,

design

Materials available as declared by the manufacturers’ websites (last access on 26/09/2017).

SLM – Material availability

Page 8: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Metal powder properties

Different production methods

lead to extremely

different morphologies,

shapes and particle sizes.

Some examples:

a) Iron - reducing chemically,

b) Copper - electrolytic reduction,

c) Aluminum - grinding,

d) Iron - Water atomization,

e) Nickel base - Gas atomization.

Page 9: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Electrolytic copper

850 ppm O2

3.7 g/cc

< 200 ppm O2

4.9 g/cc

Atomized copper

2200 ppm O2

< 400 ppm O2

Copper

Page 10: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Tech

no

logy

Gas Atomization (GA) Plasma Atomization (PA) Water Atomization (WA)

Cu

rre

nt

stat

us

Raw materials: Fe-alloys,

selected scrap, bars

Size: 5 - 2200 kg/batch

Productivity: 350 kg/h; 1-950

ton/year

Alloys: Steel, Ni and Co

alloys, Al and Ti alloys

Powders for (AM, Coating,

MIM etc.)

Raw materials: bars (filo,

polveri)

Productivity: 6 kg/h (30

t/year)

Alloys: All, mainly for Ti

Raw materials: Fe-

alloys, selected scrap,

bars

Productivity: 30 t/h

Materiali

Alloys: Steel, Cu, for

pressing, sintering,

MIM,etc

Atomization technologies

Page 11: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

VACUUM INDUCTION

MELTING

VACUUM INDUCTION GAS

ATOMISATION

Pilot Plant for powder manufacturing

Page 12: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Numerical modelling

Lab & full scale testing

Factory acceptance test

Long tradition in full scale test

Featured project – SAFE

TRANSPORTATION OF CO2

Client: Oil Company

Location: ASIA

Scope of work:

• Development of guidelines for safe transportation of CO2 by

pipeline

• Modelling by FEA CFD

• Laboratory testing

• Final validation by full scale testing in on-shore and off-shore

conditions

• Contract: confidential

• Duration: 24 months

Integrity Assessment

Page 13: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Design Options for

Transporting Gas from Remote Areas

Overall gas demand pushing for long distance gas transmission pipelines:

from Mid-Asia to East China-Korea and to Europe

in North America from Alaska to Canadian-USA market

Higher steel grade

(same WT)

Higher internal

pressure

Higher flow rate

Conveying large gas quantity by high diameter (≥36”) and HP (>100 bar)

Avoiding excessive increase of WT by using HSS pipes (X80 and beyond)

Page 14: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Integrity Management

Environmental Assisted Cracking susceptibility

INTEGRITY MANAGEMENT

in overall life cycle of long pipelines involves the

following items among others:

Pipeline and girth welds resistance under strain based conditions

Fracture propagation control & arrest

Page 15: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Potential

Strain-Based Scenarios

Example of Potential Onshore Hazards

Fault crossings

Example of Potential Offshore Hazards

Ice gouging Global-local buckling Reel Laying

Landslide crossing

Axial displ./load by

thermal expansion

Axial displ./load by

thermal expansion

Soil subsidence

Page 16: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Strain demand vs. Strain Capacity

example of ground movement

Strain Demand

- Pipeline route

- Geo-morphology

- Seasonal parameters

- Project specific parameters

Strain Capacity

- Pipe geometry

- Material properties

- Pressure, Temperature

- Weld characteristics Source: ExxonMobil

Page 17: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Strain Capacity Evaluation:

Numerical Approach

Tearing

Element switching-off,

pipe rupture by proprietary

damage model

Advanced finite element modeling of local buckling & pipe wall tearing

Without internal pressure

With internal pressure (hoop stress = 50% SMYS)

no internal pressure

with internal pressure

Page 18: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Material Behavior Improvement

Y/T ratio too basic parameter. Need to establish material requirements in

terms of local tangent modulus( Y/T, Rt0.5/Rt1.0, Rt1.0/Rt1.5, etc…)

Page 19: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Strain Capacity Evaluation:

Experimental Approach

Full-Scale testing for line pipe

deformability evaluation

Full-Scale testing facilities – onshore pipelines

Page 20: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Gas majors requirements to top producers

Tensile properties

The requirements for the tensile tests are limited to:

Range of Yield and Tensile properties in transversal direction

Yield to Tensile ratio

Total elongation

Grade Delivery

conds.

Y, Rt0.5

MPa

T, Rm

MPa

Rt0.5/Rm Elong.

AF %

min. max. min. max. max.

L245 or B R,N,Q,M 245 450 415 655 0.93

refers to

table 7 of

ISO3183:

2012

standard

L290 or X42 R,N,Q,M 290 495 415 655 0.93

L320 or X46 N,Q,M 320 525 435 655 0.93

L360 or X52 N,Q,M 360 530 460 760 0.93

L390 or X56 N,Q,M 390 545 490 760 0.93

L415 or X60 N,Q,M 415 565 520 760 0.93

L450 or X65 Q,M 450 600 535 760 0.93

L485 or X70 Q,M 485 635 570 760 0.93

L555 or X80 Q,M 555 705 625 825 0.93

L625 or X90 M 625 775 695 915 0.95

L625 or X90 Q 625 775 695 915 0.97

L690 or X100 M 690 840 760 990 0.97

L690 or X100 Q 690 840 760 990 0.97

L830 or X120 M 830 1050 915 1145 0.99

Wide min-max ranges:

Y range>150MPa

(even 200MPa)

Additional requirements limit

the range to 100 or 120MPa to

limit the “actual” production

grade

Page 21: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Gas majors requirements to top producers

Tensile properties – strain based design

Additional requirements for strain based design application:

high strain capacity to meet higher strain demand to pipeline

SBD not fully included in standards, but several specs already established

Longitudinal direction usually the most severe: laying, bending, ground movements

Limits for strain hardening and ductility

in transverse and axial direction

min. uniform el

min. value of work hardening coefficient

Shape of stress-strain curve (Round House)

Step-wise stress ratios specs

(Rt1.0 / Rt0.5, Rt1.5 / Rt1.0, Rm / Rt1.5, etc.)

LOW LEVEL

HIGH LEVEL

Page 22: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Deep knowledge of metallurgy and steel making

Multidisciplinary approach

New products development

Existing process optimization & new process development

Advance control and monitoring systems (industry 4.0)

Reduce environmental footprint

FEATURED PROJECT - NEW PRODUCTION TECHNOLOGY

OF GRAIN ORIENTED ELECTRICAL STEEL

Clients: Steel makers

Location: Scope of Work:

• Design and development of a new production method to manufacture Grain Oriented Electrical Steel (GOES), the specialty flat steel grades used to build the electric transformer

cores.

• The new production technology has been designed through the entire processing route from the steel making to the finished strips.

Contract Values: 2000k€ Duration: 24+ months

Product Development

Page 23: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

AL

Mg

SS

TWIP

New Steel Families

AL Aluminum Alloys

Mg Magnesium Alloys

SS Stainless Steels Tensile strength (MPa)

Page 24: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

218 Kg – 100 % HSS with 85 % UHSS- 81 parts

Page 25: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Stirring Gas

(bath agitation)

Prereduced and preheated iron ore

Foamy slag

Dense slag layer

Reduction Zone

Top gas

Primary O2+ Coal

(coal gasification) Flux (slag formation)

Hot Metal

Tertiary Oxygen (postcombustion)

Fine Iron ore

Secondary Oxygen (postcombustion)

Slag

CleanSMelt®

Technology

View of 25,000 tpy Pilot

Plant

(ILVA Taranto Steelworks)

Reactor height 14 m

Smelter diameter 2 m

Feeder diameter 1.2 m

Production/Process Main Figures

1 – Reactor’s tower 30 m height for

a production of : 100 kt/y

2 – Productivity ~ 14 t/h

3 – Coal (Fines/No–coking) 680 kg/t

Pig Iron Production

Page 26: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

EAF / AOD Integrated Process Control System

OUTPUT / INPUT

EAF Charge

Maximum EAF temperature,

target AOD tapping temperature,

electric energy consumption,……

Steel and slag composition

Steel temperature

Steel and slag weight

Off Gas, powders

INPUT

OUTPUT

Integrated modellisation of the

EAF and AOD process and

raw materials charge

Steel temperature,

slag composition and weight,…..

INPUT

The objective function could

also be addressed to:

• energy reduction,

• productivity,

• Slag control,

• CO2 emission …

Optimisation model able to

minimise the objective function

(typically raw materials charge

cost)

Page 27: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

0,5

1,0

1,5

2,0

2,5

3,0

3,5

0 5 10 15 20 25 30 35

tem po (m in)

Co

nc

en

tra

zio

ne

di

idr

og

en

o (

pp

m)

so lo g a s

g a s + stirring 'c o nc o rde '

g a s + stirring 'disc o rde '

Gas only

Gas + EMS “equiversus

Gas + EMS “opposite

Time (min)

Co

ncentr

atio

n o

f hydro

gen (p

pm

)

gas only

Gas+EMS

‘equiversu

s’

Gas+EMS

‘opposite’

Results:

Lower Hydrogen content

(forging steels)

Lower inclusional content

(steel for pipes)

Industrial purpose:

Improving of degassing

efficiency

Improving steel cleanliness Activities:

Numerical and physical models

coupled with laboratory and

industrial tests for operating

practices set-up and

identification of new technical

solutions

0

10

20

30

40

50

60

70

80

90

100

Prim a del vuoto D opo vuoto D opo aggiunte F ine tra ttam ento Paniera

Ma

ssa

di

inc

lusi

on

i (%

)

In tervento C SM

Situazione d i riferim ento

After CSM activities

Before CSM activities

Before Vacuum After Vacuum CaSi addition End of treatment Pony Ladle

Vacuum Degassing Process

Page 28: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Thin Slab Casting Technology at TKAST

Stainless, Electrical and Carbon Steel

Determination of steel grades, strip

formats and rolling program length to be

processed in mix rolling mode

Mill pacing

Identification of process instabilities and

determination of the plant modification

necessary for enabling mix rolling

Mould design

Fluid-dynamics:

tundish optimisation

nozzle geometry

EMBR management

Casting powders

Refractory life

Roll riders

Roll cooling

Reheating control

Descaling strategies

Page 29: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Tundish design

optimisation (shape,

positioning of dams and

weirs) is made with use of

numerical and physical

models

1:1 T-type tundish water

model at CSM

Laboratories

CC3 TKAST thermal

simulation (Temp in

K)

CC2 grid for

numerical

simulation

Page 30: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

This document is property of Centro Sviluppo Materiali SpA

Any use, even if partial, should be agreed with Centro Sviluppo Materiali SpA

Y

Z

X

linea 1

linea 2

linea 3

linea 4

Deformation of the mould during casting

Page 31: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

This document is property of Centro Sviluppo Materiali SpA

Any use, even if partial, should be agreed with Centro Sviluppo Materiali SpA

E ffect on flow in m ould centerplane

no brake

brake

E ffect on flow in m ould centerplane

no brake

E ffect on flow in m ould centerplane

no brake

brakebrake

Applicatio

n of EMBR

in thin

slab

casting

Page 32: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Level 3 t

ools

: quality

2C

ast

ladleHeat

ladleView

Blowing

SOP

tundishView

Internal geometry

Temperature

pattern

Internal

quality

Inclusion

scenario

inclusionV

iew

castView

mouldView

powderView

Internal

quality

taperView refractoryLab

refractoryLab refractoryLab

Inclusion

engineering

In-mould process

evolution Superheat

control

serv

ices

quality2Cast complements different on-line and off-line tools to Know-Why and

Know-Where inclusions (future possible defects) are or can be generated.

Page 33: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

A high cooling rate (>50°C/s) and a low

coiling temperature (<490°C) were

identified as reference for the design of

industrial trials to produce high strength

strips (YS > 700 MPa) with a Bainitic

microstructure

0 20 40 60 80400

500

600

700

800

900

Tem

pera

ture

(°C

)

ROT Length (m)

Calc 3.0 mm

Exp 3.0 mm

Calc 4.0 mm

Exp 4.0 mm

0 10 20 30 40 50 60 70 800

200

400

600

800

1000

T (

°C)

ROT length (m)

Page 34: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

Model predictions vs. experimental

results

2.0 mm thick strip

12% MA, 88%Ferrite

0 2 4 6 8 10 12 14 16 18 200.0

0.2

0.4

0.6

0.8

1.0

MA

Ferrite

Volu

me fra

ction

time (s)

Page 35: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

35

Sample 001 (3.0 mm)

TFR = 890 °C CT = 500 °C

YS = 661 MPa, UTS =740 MPa

Subgrain size = 0.78 µm

Sample 003 (2.5 mm)

TFR = 895 °C CT =469°C

YS = 777 MPa UTS = 816 MPa

Subgrain size= 0.64 µm

Effect of CT

Page 36: Presentazione di PowerPointfigi.ing.uniroma1.it/sites/default/files/allegati... · 2018-07-10 · ISO3183: 2012 standard L290 or X42 R,N,Q,M 290 495 415 655 0.93 L320 or X46 N,Q,M

JEOL JEM-3200FS

Scanning/Transmission Electron Microscope

• Accelerating voltage: 300kV

• Resolution (point to point): 0.19nm

• Spot Size: 4 nm TEM mode

• Spot Size: 1 nm STEM mode

• Electron gun: Field Emission Gun

• Annular Dark Field detector

• In-column Energy Filter

• On axis CCD camera: 2k x 2k

The content of this document is confidential and is reserved for the Customer only

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Wheel disc produced using the 3.0 mm thick strips by I.S.P. process

Fatigue tests were passed

0

0.1

0.2

0.3

0.4

0.5

0.6

0.7

0.8

-0.5 -0.3 -0.1 0.1 0.3 0.5

1

3.0 mm

2.0 mm

Car seat side made with 3.0 mm thick

strip by I.S.P. process

0

0.1

0.2

0.3

0.4

0.5

-0.3 -0.2 -0.1 0 0.1 0.2 0.3

2

1

• Forming Limit Diagram was performed (strip 2.0 mm)

• Bending tests through 180° were passed

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06/06/2018

Evento:

N°38

Servizi forniti dal CSM:

• Caratterizzazione del materiale come Tensile

test a freddo e a caldo, Forming Limit Curve,

Attrito, Rugosità, Limiting Drawing Ratio, Hole

expansion etc.

• Stampaggio di componenti semi-industriali

• Stampaggio a freddo e a caldo (PHS)

• Lettura delle deformazioni con sistema

automatico

• Calibrazione della Simulazione numerica

attraverso il confronto con la sperimentazione

• Processo di stampaggio progettato con la

simulazione numerica

• Progettazione stampi

• Simulazione delle performance in servizio dei

componenti

• Ottimizzazione dei rivestimenti

The content of this document is confidential and is reserved for the Customer only

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Erichsen press (60 ton):

•Formability test (Erichsen,

LDR, Fukui)

•Forming Limit Diagram

Strip Draw Test

FORMING LAB

SMG press 250 ton

Hydroforming test for tubes and

sheets

Automatic strain

analysis (CAMSYS-

ASAME)

The content of this document is confidential and is reserved for the Customer only

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06/06/2018

Evento:

N°40

Si è simulata solo metà della vasca vista la sua simmetria diagonale. Si riporta

la mappa degli spessori finali dopo la simulazione numerica. Il minimo è di

0,62 mm.

The content of this document is confidential and is reserved for the Customer only

Simulazione Numerica del materiale attuale

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06/06/2018

Evento:

N°41

FeE355

DP 600

FeE355

Intervento CSM:

• Definizione della miglior soluzione in termini di

materiali, geometrie, processo produttivo (Roll

Forming, Hydroforming), con l’unico dato di

ingresso della progettazione preliminare.

• Prototyping of the bumper beam by hydroforming

DESIGN OF A NEW SOLUTION FOR

THE REAR BUMPER BEAM

The content of this document is confidential and is reserved for the Customer only

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Problem:

Real time prediction of the metallurgical

and mechanical properties of hot rolled

steel product

Approach:

Physical models for time-temperature grain size deformation and Austenite evolution

(ausView)

Physical models for phase transformation

(phaseView)

Physical models for precipitation of

titanium, niobium and vanadium carbides

and aluminium nitrides (preciView)

Neural network model for prediction of the

final tensile properties (UTS, YS,

Elongation)

Benefits:

On-line material qualification along the

product length

Reduction of the number of mechanical

tests

Process optimization to reach the target

goals

Off-line simulation of new plant

configuration.

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Deep Know How and wide Experience in steel making

processes

Multidisciplinary approach with on site support

Process modeling

Pilot plants able to reproduce the industrial transformations

FEATURED PROJECT – PROCESS IMPROVEMENT FOR NEW AUTOMOTIVE STEEL GRADE

Clients: Steel maker

Location: JAPAN

Scope of Work:

• Technological support and assistance for process optimization of the reheating & descaling along the Hot Strip Mill at Tahara Works and of pickling line at Okayama Works

• Pilot scale reheating & descaling simulations, laboratory pickling and metallographic investigations

Contract Values: Confidential Duration: 15 months

Process innovation

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Conventional / Thin Slab / Strip Casting

Technologies

Run out table cooling

Minimill Thin-Slab Casting – 1 to 2 Mt/a

– 200 to 400 m 4-6 m/minute

50-60mm thick Holding furnace

Finisher

300-400 m

1-10mm thick

Coiler

20-40 metric ton coil

Integrated “Conventional” Slab Casting – 3 to 5 Mt/a

– 500 to 800 m

200-300 mm thick

20-40 metric ton coil

1-2m/minute

Gas cutter

Cooling

Reheat furnace

Rougher Coil box Finisher

1-10mm thick

Coiler

500-800 m

Run out table cooling

Strip Casting – 0.5 Mt/a

– < 100 m 15-150 m/minute

Scale Control Chamber

20-40 metric ton coil

0.7 - 1.8 mm thick

60 m

Mill

Coiler

Run out table cooling

Total capital

expenditure will be a

factor 4 to 8 lower

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Layout Pre Industrial Plant Krefeld

2000 ------> 2001

F Pre Industrial Plant Krefeld

Ladle Turret

18 tonsTundish

Casting Frame

2-Coiler System(----> 3 ladles/sequence)

In-Line Hot Rolling

Stand

RecoilingCoiler

(1 ladle)

shearInductive Heating

90 tons Ladle

F : 1500 mmL : 1130 ----> 1450 mm

Casting Speed : 15 / 140 m/min

Strip Thickness : 1.5 / 4.5 mm

Nominal Productivity : 400 kt/year

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Deep know-how in materials and Fracture

mechanics

Extensive laboratory capabilities and on-purpose

procedures

Standard and fit-for-purpose materials testing &

qualification

FEATURED PROJECT - MATERIAL QUALIFICATION AND ENGINEERING (ECA) FOR UPSTREAM GAS WELLS (Egypt)

Clients: Pipe maker, Oil Company

Location: EUROPE AND BRASIL

Scope of Work: • Very challenging off-shore project with no platform over the well and remotely controlled (around 300 km

length pipelines) and sour content of the reservoir gas. • High safety level must be ensured, particularly against corrosion related phenomena. • RINA was asked to assess corrosion, stress corrosion and mechanical resistance of metallic materials in

the very complex scenario trough special testing and highly specialized studies. • RINA was the reference provider for high reliability analysis and special procedure for high end testing

level. • Final results allow the Client to safely and reliably develop the giant Egypt field.

Contract Values: Confidential Duration: 24- months

Materials Selection & Qualification

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Corrosion and welding knowledge

Material design

Steel making process

Waste management

Featured project – EUROFUSION (ITER)

Client: ENEA

Location: ITALY

• Scope of work: This study aims to develop innovative materials and

welding processes for a new fusion power plant.

• Evaluate existing and emerging steel melting technology for the

specific issues of recycling of steel grades planned for the DEMO

plant.

Contract value: confidential

Duration: 36 months

Specialized engineering service

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Laser Hybrid concept

implemented in the project

Pipeline multi-pass girth welding in downhill 5G

position (two opposite welding heads, each going

from 12h to 6h position)

Narrow gap preparation

Welding from external side only

Root pass welding LB-GMAW

Groove filling GMAW, fully weaved passes

Expected advantages

Avoidance of copper backing system

Enhanced productivity compared to current

process (GMAW) capability

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Target Weld Properties

Mechanical properties

Min Service T: +0°C

σy WM (AWM): min. 655 MPa (18% OM)

Charpy V-notch toughness: 40J avg (32J min)

@ +0°C

CTOD: min 0.20 mm @ +0 °C

Integrity

Conformance to ISO 13847 after RT, UT, VT

(NDT according to relevant ISO and ASME

BPVC Sec. V standards)

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Activities

First modification of the orbital ‘bug & band’ GMAW system (PROTEUS equipment)

Bevel design, LB-GMAW process development in 5G downhill position

Welding consumable testing, first joint properties

Weld integrity on trial complete weldments (180° + 180°), NDT

Investigation on tolerance of step and gap

Modification of a new improved orbital GMAW system (TSA PASSO equipment)

Process refinement, ultimate productivity investigation in 5G downhill

WPS qualification on complete welds, NDT, further consumable testing

Prototype pipes (7) complete girth welds production (testing process robustness on full-

scale situation)

Design of the welds mechanical testing matrix, specimen production

Small scale welds mechanical testing, metallographic investigations

Welds curved Wide Plate mechanical testing (full-scale)

Drafting specification for an industrial system

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Weld speed

Root travel speed: 3.0 m/min (compared to

~1.2 m/min for GMAW on Cu backing)

Good tolerable gap <1.5 mm, step <3.0 mm

LB-GMAW heat input: ~ 0.20 kJ/mm

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Process repeatability & robustness

No. 7 prototypal pipes fully welded during an uninterrupted welding session

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Power sources

(LB-GMAW, GMAW)

Nd:YAG (diode pumped) Laser Resonator, rated 4.4 kW (1.06 mm wavelength, optical

fiber transmission possible)

Laser beam optical fiber transmission (f=600mm); collimation lens: f=200 mm,

focusing lens: f=120 or 160 mm; focused spot diameter ~0.4 mm

GMA CV inverter, rated 420 A, no pulsed arc usage (spray arc usage)

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Cross fertilization between different market sectors

Expertise in steel making and refinery processes

Patent and Pilot plant for Real scale proof assessment

Financial support from EU Funded project

Waste valorization

FEATURED PROJECT – USE OF ENI’S BEST RESIDUAL IN STEEL

MAKING

Client: Oil Company Steel Maker

Location: ITALY

Scope of Work:

• Business plan validation

• Define treatment process for making ENI’s BEST residual suitable for steel

making EAF.

• Identification of potential steel makers for industrial trials • On site support for ENI and Steel maker

•Contract: confidential

•Duration: 24 months

Circular Economy

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RIN

A C

onsu

ltin

g a

ppro

ach f

or

a s

ust

ain

able

steel

pro

ducti

on

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Material performances FFS, ECA, Creep Assessment

Failure analysis on material and complex component

Root Cause Analysis, Mechanical, Electrical, Corrosion,

metallurgy competences

Fit for Purpose Testing to reproduce real operating condition

FMECA

FEATURED PROJECT – ROUTE CAUSE ANALISYS

ON ELECTRICAL TERMINAL

Client: Confidential

Location: ITALY

Scope of Work:

• Failure Analysis

• Fit For Purpose Testing to reproduce the failure scenario and

environment conditions

•Contract Values: Confidential

•Duration: 3 months

Material Performance &

Condition assessement

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Pin N. 56

as received

N

N

Hinge axis

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Pin end N. 56

Female seat lateral marks

N

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Tensile specimens (appearance after tests)

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N°60

Sample “B” Fig. 1 - FT 1 Zona Centrale Fig. 2 - FT 2 frattura intergranulare

Fig. 3 - FT 3 dettaglio di Fig. 2 Fig. 4 - FT 4 dettaglio di Fig. 3

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https://www.rina.org/en/careers/working-in-rina