Prepared For: NER BUREAU OF WASTOE SITE CLEANUP …QCS = Quality Control Sample (external to lab) acceptance limits as per method or Interlaboratory proficiency study . RDL = Reporting

Report Print Date: 1/29/2007 MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION Page 1 of 24 DIVISION OF ENVIRONMENTAL ANALYSIS WILLIAM X. WALL EXPERIMENT STATION

EPA#: MA00019

Analysis Report for Login Batch: 2006491

Prepared For: NERO BUREAU OF WASTE SITE CLEANUP Project Name: SDMS DocID 273519 Contact: Paul Giddings Project Coordinator

Sample Lab ID#: 2006491-001 Site: Sutton Brook Matrix: GW Collect Date: 12/19/2006 10:30 AM

Sample Field ID#: DEP-1 Locator: Collector: Giddings, P Receive Date: 12/19/2006 12:20 PM

Analvte/Compound Result Units MDL RDL Method Analysis Date Status

Surrogate Acceptance Criteria

Dibromofluoromethane 99 % Recovery 70 -130 EPA 8260B 12/19/2007 1:00 PM Approved

Toluene-d8 103 % Recovery 7 0 - 1 3 0 EPA8260B 12/19/2007 1:00 PM Approved

4-bromofluorobenzene 84 % Recovery 7 0 - 1 3 0 EPA 8260B 12/19/2007 1:00 PM Approved

Dichlorodifluoromethane ND ug/L 0.27 20 EPA 8260B 12/19/2007 1:00 PM Approved

Chloromethane ND ug/L 0.32 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

Vinyl chloride ND ug/L 0.23 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

Dromomethane ND ug/L 0.46 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

Chloroethane ND ug/L 0.17 2.0 EPA8260B 12/19/2007 1:00 PM Approved

Acetone 22 M, J ug/L 10 50 EPA8260B 12/19/2007 1:00 PM Approved

Trichlorofluoromethane ND ug/L 0.44 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

1.1-Dichloroethcne ND ug/L 0.49 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Carbon disulfide ND ug/L 0.52 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

Melhylene chloride 3.8 J ug/L 0.24 2 0 EPA 8260B 12/19/2007 1 :00 PM Approved

Freon-113 ND ug/L 0.46 2.0 EPA8260B 12/19/2007 1:00 PM Approved

trans- 1 .2-Dicnloroethene ND ug/L 0 30 2.0 EPA 8260B 12/19/2007 1 :00 PM Approved

Melhyl-t-butyl ether 4.2 J ug/L 0.32 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

1.1-Dichloroelhanc ND ug/L 0.49 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

MEK ND ug/L 4.G 20 EPA8260B 12/19/2007 100 PM Approved

Chlorobromomethane ND ug/L 0.44 20 EPA8260B 12/19/2007 1:00 PM Approved

2.2-Dichloropro[ianc NU ug'L 0.52 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

cis- 1 .2-nichloroethene ND ug'L 0.43 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

Chloroform ND ug/L 0.41 2.0 EPA8260B 12/19/2007 1:00 PM Approved

1 ,1 ,1-Tnchloroeltiano ND ug'L 0.37 20 EPA 8260B 12/19/2007 1 00 PM Approved

Carbon telrachlonde ND ug'L 0.25 2.0 EPA8260B 12/19/2007 1:00 PM Approved

Some vials contain large amount of silt/soil.

ND = Analyzed for, but not detected above MDL (equiv. U) B = Analyte detected in sample, and in LB, LRB, LRB = Laboratory Reagent Blank

Estimated Value: and/or trip blank or no trip blank was collected LB = Laboratory Blank (equiv. Method Blank)

M = Analyte concentration > MDL but < RDL H = USEPA holding time exceeded J = Other QC criteria not met (see comments)

NA = Not applicable

N = GC/MS non-target tentatively identified compound (TIC) - no standard available for quantitation

R = Data rejected due to severe QC, quantitation and/or qualitative ID deficiencies

MDL = Method Detection Limit

LFB = Laboratory Fortified Blank (equiv. LCS) LFM = Laboratory Fortified Sample Matrix (equiv. MS) QCS = Quality Control Sample (external to lab) acceptance limits as per method or interlaboratory proficiency study

RDL = Reporting Detection Limit (equiv. MRL)


EPA#:MA00019


Prepared For: NERO BUREAU OF WASTE SITE CLEANUP Project Name:

Contact: Paul Giddings Project Coordinator:

Sample Lab ID*: 2006491-001 Site: Sutton Brook Matrix: GW Collect Date: 12/19/2006 10:30 AM

Sample Field ID*: DEP-1 Locator: Collector: Giddings. P Receive Date: 12/19/2006 12:20 PM

Analvte/Compound Result Units MDL RDL Method Analysis Date Status 1 , 1 -Dichloropropene ND ug/L 0.23 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

Benzene 0.47 M, J ug/L 0.32 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

1,2-Dichloroethane ND ug/L 0.34 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

Trichloroethene 1.4 M,J ug/L 0.20 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

1 ,2-Dichloropropane ND ug/L 0.27 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Dibromomethane ND ug/L 0.32 2.0 EPA8260B 12/19/2007 1:00 PM Approved

Bromodichloromethane ND ug/L 0.22 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

cis-1 ,3-Dichloropropene ND ug/L 0.40 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

MIBK ND ug/L 2.1 20 EPA8260B 12/19/2007 1 :00 PM Approved

Toluene 8.0 J ug/L 0.29 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

trans-1 ,3-Dichloropropene ND ug/L 0.44 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

1,1,2-Trichloroethane ND ug/L 0.24 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

TetrachlotDethene ND ug/L 0.30 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved


Dibromochloromethane ND ug/L 0.30 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

1 ,2-Dibromoethane ND ug/L 0.30 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

Chlorobenzene ND ug/L 0.22 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

1,1,1 ,2-Tetrachloroethane ND ug/L 0.27 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Ethylbenzene 0.51 M, J ug/L 0.17 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

p,m-xylene 1.4 M,J ug/L 0.49 4.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

o-Xylene 0.49 M, J ug/L 0.27 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Styrene ND ug/L 0.16 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

Bromoform ND ug/L 0.35 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Isopropylbenzene ND ug/L 0.20 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Bromobenzene ND ug/L 0.22 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved


ND = Analyzed for, but not detected above MDL (equlv. U) B = Analyte detected In sample, and In LB, LRB, LRB = Laboratory Reagent Blank

Estimated Value: and/or trip blank or no trip blank was collected LB = Laboratory Blank (equlv. Method Blank)


NA = Not applicable

N = GC/MS non-target tentatively Identified compound (TIC) no standard available for quantltatlon

R " Data rejected due to severe QC, quantltatlon and/or qualitative ID deficiencies


LFB = Laboratory Fortified Blank (equlv. LCS) LFM = Laboratory Fortified Sample Matrix (equiv. MS) QCS = Quality Control Sample (external to lab) acceptance limits as per method or Interlaboratory proficiency study

RDL = Reporting Detection Limit (equlv. MRL)


EPA#:MA00019


Prepared For: NERO BUREAU OF WASTE SITE CLEANUP Project Name: Contact: Paul Giddings Project Coordinator:

Sample Lab ID*: 2006491-001 Site: Button Brook Matrix: GW Collect Date: 12/19/2006 10:30 AM

Sample Field ID#: DEP-1 Locator: Collector: Giddings. P Receive Date: 12/19/2006 12:20 PM


1 ,1 ,2,2-Tetrachloroethane ND ug/L 0.26 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

1 ,2,3-Trichloropropane ND ug/L 0.37 2.0 EPA 8260B 12/19/2007 1 00PM Approved

n-Propyl benzene ND ug/L 0.14 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

2-Chlorotoluene ND ug/L 0.070 2.0 EPA 8260B 12/19/2007 100 PM Approved

4-Chlorotoluene ND ug/L 0.33 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

1 ,3,5-Trimethylbenzene ND ug/L 0.13 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

tert-Butylbenzene ND ug/L 0.18 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

1 ,2,4-Trimethylbenzene 0.33 M, J ug/L 0.14 2.0 EPA 8260B 12/19/2007 :00 PM Approved

sec-Butylbenzene ND ug/L 0.17 2.0 EPA 8260B 12/19/2007 :00 PM Approved

1 ,3-Dichlorobenzene ND ug/L 0.18 2.0 EPA 8260B 12/19/2007 :00 PM Approved

4-lsopropyltoluene ND ug/L 0.27 2.0 EPA 8260B 12/19/2007 :00 PM Approved



n-Butylbenzene ND ug/L 0.17 2.0 EPA 8260B 12/19/2007 00 PM Approved

1 ,2-Dibromo-3-chloropropane ND ug/L 0.75 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

1 ,2,4-Trichlorobenzene ND ug/L 0.52 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

Hexachlorobutadiene ND ug/L 0.84 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

Naphthalene ND ug/L 0.52 2.0 EPA 8260B 12/19/2007 1•00 PM Approved

1 ,2,3-Trichlorobenzene ND ug/L 0.27 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

J = Duplicate vial, analyzed but not reported, had much lower or ND concentrations of analytes detected in the sample reported above. Variable collection procedures


Sample Field ID*: DEP-2 Locator: Collector: Giddings, P Receive Date: 12/19/2006 12:20PM



ND = Analyzed for, but not detected above MDL (equiv. U) B = Analyte detected In sample, and in LB, LRB, LRB = Laboratory Reagent Blank and/or trip blank or no trip blank was collected LB = Laboratory Blank (equiv. Method Blank) Estimated Value:

LFB = Laboratory Fortified Blank (equiv. LCS) M = Analyte concentration > MDL but < RDL N = GC/MS non-target tentatively identified compound H = USEPA holding time exceeded (TIC) - no standard available for quantitation LFM = Laboratory Fortified Sample Matrix (equiv. MS)

QCS = Quality Control Sample (external to lab) J > •• Other QC criteria not met (see comments) R = Data rejected due to severe QC, quantitation acceptance limits as per method or interlaboratory and/or qualitative ID deficiencies

NA • Not applicable proficiency study MDL = Method Detection Limit RDL = Reporting Detection Limit (equiv. MRL)

I


EPA*:MA00019



Sample Lab ID* 2006491-002 Site: Sutton Brook Matrix: GW

Sample Field ID*: DEP-2 Locator: Collector: Giddings, P

Analvte/Compound Result Units MDL RDL Method

Surrogate Acceptance Criteria Dibromofluoromethane 98 % Recovery 70-130 EPA 8260B

Toluene-d8 96 % Recovery 70-130 EPA 8260B

4-bromofluorobenzene 99 % Recovery 70-130 EPA 8260B

Dichlorodifluoromethane ND ug/L 0.27 2.0 EPA8260B

Chloromethane ND ug/L 0.32 2.0 EPA8260B

Vinyl chloride ND ug/L 0.23 2.0 EPA8260B

Bromomethane ND ug/L 0.46 2.0 EPA8260B Chloroethane ND ug/L 0.17 2.0 EPA8260B

Acetone 16M ug/L 10 50 EPA8260B

Trichlorofluoromethane ND ug/L 0.44 2.0 EPA8260B

1,1-Dichloroethene ND ug/L 0.49 2.0 EPA8260B

Carbon bisulfide ND ug/L 0.52 2.0 EPA 8260B

Methylene chloride ND ug/L 0.24 2.0 EPA8260B

Freon-113 ND ug/L 0.46 2.0 EPA8260B

trans-1 ,2-Dichloroethene ND ug/L 0.30 2.0 EPA 8260B

Methyl-t-butyl ether ND ug/L 0.32 2.0 EPA 8260B 1,1-Dichloroethane ND ug/L 0.49 2.0 EPA 8260B

MEK ND ug/L 4.6 20 EPA8260B

Chlorobromomethane ND ug/L 0.44 2.0 EPA8260B

2,2-Dichloropropane ND ug/L 0.52 2.0 EPA 8260B

cis-1 ,2-Dichloroethene ND ug/L 0.43 2.0 EPA8260B

Chloroform 0.43 M ug/L 0.41 2.0 EPA8260B

1,1,1 -Tri chloroethane ND ug/L 0.37 2.0 EPA8260B Carbon tetrachloride ND ug/L 0.25 2.0 EPA 8260B


ND = Analyzed for, but not detected above MDL (equlv. U) B = Analyte detected In sample, and In LB, LRB, LRB

Collect Date: 12/19/2006 10:35 AM

Receive Date: 12/19/2006 12:20 PM

Analysis Date Status

1 2/1 9/2007 1 :00 PM Approved 1 2/1 9/2007 1 :00 PM Approved

1 2/1 9/2007 1 :00 PM Approved

1 2/1 9/2007 1 :00 PM Approved

1 2/1 9/2007 1 :00 PM Approved

1 2/1 9/2007 1 :00 PM Approved

12/19/2007 1 :00 PM Approved

1 2/1 9/2007 1 :00 PM Approved

1 2/1 9/2007 1 :00 PM Approved

1 2/1 9/2007 1 :00 PM Approved

1 2/1 9/2007 1 :00 PM Approved

1 2/1 9/2007 1 :00 PM Approved

1 2/1 9/2007 1 :00 PM Approved

1 2/1 9/2007 1 :00 PM Approved

1 2/1 9/2007 1 :00 PM Approved



1 2/1 9/2007 1 :00 PM Approved


1 2/1 9/2007 1 :00 PM Approved

1 2/1 9/2007 1 :00 PM Approved

= Laboratory Reagent Blank



NA = Not applicable

N = GC/MS non-target tentatively Identified compound (TIC) - no standard available for quantltatlon

R = Data rejected due to severe QC, quantltatlon and/or qualitative ID deficiencies


LFB = Laboratory Fortified Blank (equiv. LCS) LFM = Laboratory Fortified Sample Matrix (equiv. MS) QCS = Quality Control Sample (external to lab) acceptance limits as per method or Interlaboratory proficiency study



EPA*:MA00019




Sample Field ID*: DEP-2 Locator: Collector: Giddings, P Receive Date: 12/19/2006 12:20 PM


1,1-Dichloropropene ND ug/L 0.23 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Benzene ND ug/L 0.32 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

1 ,2-Dichloroethane ND ug/L 0.34 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

Trichloroethene ND ug/L 0.20 2.0 EPA 8260B 12/19/2007 1:00 PM Approved


Dibromomethane ND ug/L 0.32 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved



MIBK ND ug/L 2.1 20 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

Toluene ND ug/L 0.29 2.0 EPA8260B 12/19/2007 1 :00 PM Approved

trans- 1 ,3-Dichloropropene ND ug/L 0.44 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

1 , 1 ,2-Trichloroethane ND ug/L 0.24 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

Tetrachloroethene 1.6M ug/L 0.30 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved


Dibromochloromethane ND ug/L 0.30 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

1 ,2-Dibromoethane ND ug/L 0.30 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Chlorobenzene ND ug/L 0.22 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

1,1,1 ,2-Tetrachloroethane ND ug/L 0.27 2.0 EPA 8260B 12/19/2007 1 :00 PM Approved

Ethylbenzene ND ug/L 0.17 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

p,m-xylene ND ug/L 0.49 4.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

o-Xylene ND ug/L 0.27 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Styrene ND ug/L 0.16 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Bromoform ND ug/L 0.35 2.0 EPA8260B 12/19/2007 1 :00 PM Approved

Isopropyl benzene ND ug/L 0.20 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved



ND = Analyzed for, but not detected above MDL (equlv. U) B = Analyte detected in sample, and In LB, LRB, LRB = Laboratory Reagent Blank



NA = Not applicable

N = GC/MS non-target tentatively Identified compound (TIC) - no standard available for quantitation



LFB = Laboratory Fortified Blank (equiv. LCS) LFM = Laboratory Fortified Sample Matrix (equlv. MS) QCS = Quality Control Sample (external to lab) acceptance limits as per method or Interlaboratory proficiency study



EPA#:MA00019



Sample Lab ID* 2006491-002 SHe: Sutton Brook Matrix: GW Collect Date: 12/19/2006 10:35 AM Sample Field ID*: DEP-2 Locator: Collector: Giddings, P Receive Date: 12/19/2006 12:20PM

Analvte/Compound Result Units MDL RDL Method Analysis Date Status 1 ,1 ,2,2-Tetrachloroethane ND ug/L 0.26 2.0 EPA 8260B 12/19/2007 1:OOPM Approved 1 ,2,3-Trichloropropane ND ug/L 0.37 2.0 EPA 8260B 12/19/2007 1:00 PM Approved n-Propyl benzene ND ug/L 0.14 2.0 EPA 8260B 12/19/2007 1:OOPM Approved 2-Chlorotoluene ND ug/L 0.070 2.0 EPA 8260B 12/19/2007 1:OOPM Approved 4-Chlorotoluene ND ug/L 0.33 2.0 EPA 8260B 12/19/2007 1:OOPM Approved 1 ,3,5-Trimethylbenzene ND ug/L 0.13 2.0 EPA 8260B 12/19/2007 1:OOPM Approved tert-Butyl benzene ND ug/L 0.18 2.0 EPA 8260B 12/19/2007 1:OOPM Approved 1 ,2,4-Trimethylbenzene 0.37 M ug/L 0.14 2.0 EPA 8260B 12/19/2007 1:OOPM Approved sec-Butylbenzene ND ug/L 0.17 2.0 EPA 8260B 12/19/2007 1:OOPM Approved 1 ,3-Dlchlorobenzene ND ug/L 0.18 2.0 EPA 8260B 12/19/2007 1:OOPM Approved 4-lsopropyltoluene ND ug/L 0.27 2.0 EPA 8260B 12/19/2007 1:OOPM Approved 1 ,4-Dichlorobenzene ND ug/L 0.28 2.0 EPA 8260B 12/19/2007 1:OOPM Approved 1 ,2-DJchlorobenzene ND ug/L 0.29 2.0 EPA 8260B 12/19/2007 1:OOPM Approved n-Butylbenzene ND ug/L 0.17 2.0 EPA 8260B 12/19/2007 1:OOPM Approved 1 ,2-Dibromo-3-chloropropane ND ug/L 0.75 2.0 EPA 8260B 12/19/2007 1:OOPM Approved 1 ,2,4-Trichlorobenzene ND ug/L 0.52 2.0 EPA 8260B 12/19/2007 1:OOPM Approved Hexachlorobutadiene ND ug/L 0.84 2.0 EPA 8260B 12/19/2007 1:OOPM Approved Naphthalene ND ug/L 0.52 2.0 EPA 8260B 12/19/2007 1:OOPM Approved 1 ,2,3-Trichlorobenzene ND ug/L 0.27 2.0 EPA 8260B 12/19/2007 1:OOPM Approved

N = Ethyl methyl benzene, dlethyl benzene, dimethyl benzene, nonen-1-ol.

Sample Lab ID*: 2006491-003 Site: Sutton Brook Matrix: GW Collect Date : 12/19/2006 10:40 AM Sample Field ID*: DEP-2D Locator: Collector: Giddings,P Receive Date: 12/19/2006 12:20 PM



ND = Analyzed for, but not detected above MDL (equlv. U) B = Analyte detected in sample, and In LB, LRB, LRB = Laboratory Reagent Blank and/or trip blank or no trip blank was collected LB = Laboratory Blank (equlv. Method Blank) Estimated Value:

M = Analyte concentration > MDL but < RDL N = GC/MS non-target tentatively Identified compound LFB = Laboratory Fortified Blank (equiv. LCS) H = USEPA holding time exceeded (TIC) - no standard available for quantltatlon LFM = Laboratory Fortified Sample Matrix (equlv. MS)

QCS = Quality Control Sample (external to lab) J = Other QC criteria not met (see comments) R = Data rejected due to severe QC, quantltatlon acceptance limits as per method or Interlaboratory and/or qualitative ID deficiencies

NA = Not applicable proficiency study MDL = Method Detection Limit RDL = Reporting Detection Limit (equlv. MRL)


EPA*:MA00019




Sample Field ID*: DEP-2D Locator: Collector: Giddings, P Receive Date: 12/19/2006 12:20 PM


Surrogate Acceptance Criteria Dibromofluoromethane 0.0 % Recovery 70- 130 EPA 8260B 12/19/2007 1 00 PM Approved

Not Analyzed. Toluene-d8 0.0 % Recovery 70- 130 EPA 8260B 12/19/2007 1 00 PM Approved

Not Analyzed. 4-bromofluorobenzene 0.0 % Recovery 70- 130 EPA 8260B 12/19/2007 1:00 PM Approved

Not Analyzed. Dichlorodifluoromethane NAJ ug/L 0.27 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

Chloromethane NAJ ug/L 0.32 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

Vinyl chloride NAJ ug/L 0.23 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

Bromomethane NAJ ug/L 0.46 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

Chloroethane NAJ ug/L 0.17 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

Acetone NAJ ug/L 10 50 EPA 8260B 12/19/2007 1 00 PM Approved

Trichlorofluoromethane NAJ ug/L 0.44 2.0 EPA 8260B 12/19/2007 1 00PM Approved

1,1-Dichloroethene NAJ ug/L 0.49 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

Carbon disulfide NAJ ug/L 0.52 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

Methylene chloride NAJ ug/L 0.24 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

Freon-113 NAJ ug/L 0.46 2.0 EPA 8260B 12/19/2007 1•00 PM Approved

trans- 1 ,2-Dichloroethene NAJ ug/L 0.30 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

Methyl-t-butyl ether NAJ ug/L 0.32 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

1,1-Dichloroethane NAJ ug/L 0.49 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

MEK NAJ ug/L 4.6 20 EPA 8260B 12/19/2007 1 00 PM Approved

Chlorobromomethane NAJ ug/L 0.44 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

2,2-Dichloropropane NAJ ug/L 0.52 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

cis-1 ,2-Dichloroethene NAJ ug/L 0.43 2.0 EPA 8260B 12/19/2007 1 00 PM Approved


ND = Analyzed for, but not detected above MDL (equlv. U) B = Analyte detected in sample, and in LB, LRB, LRB = Laboratory Reagent Blank



NA = Not applicable

N = GC/MS non-target tentatively Identified compound (TIC) - no standard available for quantitation



LFB = Laboratory Fortified Blank (equlv. LCS) LFM = Laboratory Fortified Sample Matrix (equlv. MS) QCS = Quality Control Sample (external to lab) acceptance limits as per method or Interlaboratory proficiency study


Report Print Date: 1 /29/2007 MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION Page 8 of 24 DIVISION OF ENVIRONMENTAL ANALYSIS WILLIAM X. WALL EXPERIMENT STATION

EPA*: MA00019



Sample Lab ID*: 2006491-003 Site: Sutton Brook Matrix: GW Collect Date: 12/19/2006 10:40 AM Sample Field ID*: DEP-2D Locator: Collector: Giddings, P Receive Date: 12/19/2006 12:20 PM

Analvte/Compound Result Units MDL RDL Method Analysis Date Status Chloroform NAJ ug/L 0.41 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved 1,1.1 -Trichloroethane NAJ ug/L 0.37 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved Carbon tetrachloride NAJ ug/L 0.25 2.0 EPA 8260B 12/19/2007 1 :00 PM Approved 1 , 1 -Dichloropropene NAJ ug/L 0.23 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved Benzene NAJ ug/L 0.32 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved 1 ,2-Dichloroethane NAJ ug/L 0.34 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved Trichloroethene NAJ ug/L 0.20 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved 1 ,2-Dichloropropane NAJ ug/L 0.27 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved Dibromomethane NAJ ug/L 0.32 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved Bromodichloromethane NAJ ug/L 0.22 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved cis-1 ,3-Dichloropropene NAJ ug/L 0.40 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved MIBK NAJ ug/L 2.1 20 EPA8260B 12/19/2007 1 :00 PM Approved Toluene NAJ ug/L 0.29 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

trans-1 ,3-Dichloropropene NAJ ug/L 0.44 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved 1 ,1 ,2-Trichloroethane NAJ ug/L 0.24 2.0 EPA8260B 12/19/2007 1 :00 PM Approved Tetrachloroethene NAJ ug/L 0.30 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

1 ,3-Dichloropropane NAJ ug/L 0.14 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved Dibromochloromethane NAJ ug/L 0.30 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved 1 ,2-Dibrornoethane NAJ ug/L 0.30 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved Chlorobenzene NAJ ug/L 0.22 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved 1,1,1 ,2-Tetrachloroethane NAJ ug/L 0.27 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved Ethylbenzene NAJ ug/L 0.17 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved p,m-xylene NAJ ug/L 0.49 4.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved o-Xylene NAJ ug/L 0.27 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

Styrene NAJ ug/L 0.16 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved


ND = Analyzed for, but not detected above MDL (equlv. U) B = Analyte detected In sample, and in LB, LRB, LRB = Laboratory Reagent Blank and/or trip blank or no trip blank was collected LB = Laboratory Blank (equlv. Method Blank) Estimated Value:

M = Analyte concentration > MDL but < RDL N = GC/MS non-target tentatively identified compound LFB = Laboratory Fortified Blank (equiv. LCS) H = USEPA holding time exceeded (TIC) - no standard available for quantitation LFM = Laboratory Fortified Sample Matrix (equiv. MS) J = Other QC criteria not met (see comments) QCS = Quality Control Sample (external to lab) R = Data rejected due to severe QC, quantitation

acceptance limits as per method or interlaboratory and/or qualitative ID deficiencies NA = Not applicable proficiency study

MDL = Method Detection Limit RDL = Reporting Detection Limit (equlv. MRL)


EPA#:MA00019




Sample Field ID*: DEP-2D Locator: Collector: Giddings, P Receive Date: 12/19/2006 12:20 PM


Bromoform NAJ ug/L 0.35 2.0 EPA 8260B 12/19/2007 1 00PM Approved

Isopropylbenzene NAJ ug/L 0.20 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

Bromobenzene NAJ ug/L 0.22 2.0 EPA 8260B 12/19/2007 1 00PM Approved

1 ,1 ,2,2-Tetrachloroethane NAJ ug/L 0.26 2.0 EPA 8260B 12/19/2007 100PM Approved

1 ,2,3-Trichloropropane NAJ ug/L 0.37 2.0 EPA 8260B 12/19/2007 1 00PM Approved

n-Propylbenzene NAJ ug/L 0.14 2.0 EPA 8260B 12/19/2007 1 00PM Approved

2-Chlorotoluene NAJ ug/L 0.070 2.0 EPA 8260B 12/19/2007 100PM Approved

4-Chlorotoluene NAJ ug/L 0.33 2.0 EPA 8260B 12/19/2007 1 00PM Approved

1 ,3,5-Trimethylbenzene NAJ ug/L 0.13 2.0 EPA 8260B 12/19/2007 1 00PM Approved

tert-Butylbenzene NAJ ug/L 0.18 2.0 EPA 8260B 12/19/2007 1 00PM Approved

1 ,2,4-Trimethylbenzene NAJ ug/L 2.0 0.14 EPA 8260B 12/19/2007 1 00PM Approved

0.17 EPA 8260B 12/19/2007 1:OOPM Approved sec-Butylbenzene NAJ ug/L 2.0

1 ,3-Dichlorobenzene NAJ ug/L 0.18 2.0 EPA 8260B 12/19/2007 1 00PM Approved

4-lsopropyltoluene NAJ ug/L 0.27 2.0 EPA 8260B 12/19/2007 1:OOPM Approved

NAJ ug/L 0.28 2.0 EPA 8260B 12/19/2007 1:OOPM Approved 1 ,4-Dichlorobenzene 12/19/2007 1:OOPM Approved 1 ,2-Dichlorobenzene NAJ ug/L 0.29 2.0 EPA 8260B

n-Butylbenzene NAJ ug/L 0.17 2.0 EPA 8260B 12/19/2007 1 00PM Approved

1 ,2-Dibromo-3-chloropropane NAJ ug/L 0.75 2.0 EPA 8260B 12/19/2007 1 00PM Approved

1 ,2,4-Trichlorobenzene NAJ ug/L 0.52 2.0 EPA 8260B 12/19/2007 1 00PM Approved

ug/L 0.84 2.0 EPA 8260B 12/19/2007 1 00PM Approved Hexachlorobutadiene NAJ

Naphthalene NAJ ug/L 0.52 2.0 EPA 8260B 12/19/2007 1 00PM Approved

1 ,2,3-Trichlorobenzene NAJ ug/L 0.27 2.0 EPA 8260B 12/19/2007 1:OOPM Approved

J = Sample could not be analyzed due to a large amount of silt/soil In vials.


ND = Analyzed for, but not detected above MDL (equiv. U) B = Analyte detected in sample, and in LB, LRB, LRB = Laboratory Reagent Blank and/or trip blank or no trip blank was collected LB = Laboratory Blank (equlv. Method Blank) Estimated Value:

LFB = Laboratory Fortified Blank (equlv. LCS) M = Analyte concentration > MDL but < RDL N = GC/MS non-target tentatively Identified compound LFM = Laboratory Fortified Sample Matrix (equiv. MS) H = USEPA holding time exceeded (TIC) - no standard available for quantitation QCS = Quality Control Sample (external to lab) J = Other QC criteria not met (see comments) R = Data rejected due to severe QC, quantitation acceptance limits as per method or inter laboratory

and/or qualitative ID deficiencies NA = Not applicable proficiency study

MDL = Method Detection Limit RDL = Reporting Detection Limit (equlv. MRL)


EPA*: MA00019







Dibromofluoromethane 106 % Recovery 70-130 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Toluene-cIS 90 % Recovery 70-130 EPA 8260B 12/19/2007 1 :00 PM Approved

4-bromofluorobenzene 88 % Recovery 70-130 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Dichlorodifluoromethane ND ug/L 0.27 2.0 EPA 8260B l27l 9/2007 1 :00 PM Approved

Chloromethane ND ug/L 0.32 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Vinyl chloride ND ug/L 0.23 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

Bromomethane ND ug/L 0.46 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Chloroe thane ND ug/L 0.17 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Acetone ND ug/L 10 50 EPA8260B 12/19/2007 :OOPM Approved

Trichlorofluoromethane ND ug/L 0.44 2.0 EPA8260B 12/19/2007 :OOPM Approved

1,1-Dichloroethene ND ug/L 0.49 2.0 EPA 8260B 12/19/2007 :OOPM Approved

Carbon disulfide ND ug/L 0.52 2.0 EPA8260B 12/19/2007 :OOPM Approved

Methylene chloride ND ug/L 0.24 2.0 EPA 8260B 12/19/2007 :OOPM Approved

Freon-113 ND ug/L 0.46 2.0 EPA 8260B 12/19/2007 :OOPM Approved

trans-1 ,2-Dichloroethene ND ug/L 0.30 2.0 EPA 8260B 12/19/2007 :OOPM Approved

Methyl-t-butyl ether ND ug/L 0.32 2.0 EPA 8260B 12/19/2007 :OOPM Approved

1,1-Dichloroethane ND ug/L 0.49 2.0 EPA 8260B 12/19/2007 :OOPM Approved

MEK ND ug/L 4.6 20 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

Chlorobromomethane ND ug/L 0.44 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

2,2-Dichloropropane ND ug/L 0.52 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

cis-1 ,2-Dichloroethene ND ug/L 0.43 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Chloroform ND ug/L 0.41 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

1.1,1 -Trichloroethane ND ug/L 0.37 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

Carbon tetrachloride ND ug/L 0.25 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved


ND = Analyzed for, but not detected above MDL (equlv. U) B = Analyte detected In sample, and In LB, LRB, LRB = Laboratory Reagent Blank


M = Analyte concentration > MDL but < RDL H = USEPA holding time exceeded J = Other QC criteria not met (see comments]

NA = Not applicable




LFB = Laboratory Fortified Blank (equiv. LCS) LFM = Laboratory Fortified Sample Matrix (equlv. MS) QCS = Quality Control Sample (external to lab) acceptance limits as per method or interlaboratory proficiency study



EPA#:MA00019






1 , 1 -Dichloropropene ND ug/L 0.23 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

Benzene ND ug/L 0.32 2.0 EPA 8260B 12/1 9/20071. -00PM Approved

1 ,2-Dichloroethane ND ug/L 0.34 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

Trichloroethene ND ug/L 0.20 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

1 ,2-Dichloropropane ND ug/L 0.27 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

Dibromomethane ND ug/L 0.32 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

Bromodichloromethane ND ug/L 0.22 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

cis-1 ,3-Dichloropropene ND ug/L 0.40 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

MIBK ND ug/L 2.1 20 EPA 8260B 12/19/2007 1:00 PM Approved

Toluene ND ug/L 0.29 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

trans-1 ,3-Dichloropropene ND ug/L 0.44 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

1,1,2-Trichloroethane ND ug/L 0.24 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

Tetrachloroethene ND ug/L 0.30 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

1 ,3-Dichloropropane ND ug/L 0.14 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

Dibromochloromethane ND ug/L 0.30 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

1 ,2-Dibromoethane ND ug/L 0.30 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

Chlorobenzene ND ug/L 0.22 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

1,1,1 ,2-Tetrachloroethane ND ug/L 0.27 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

Ethylbenzene ND ug/L 0.17 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

p,m-xylene ND ug/L 0.49 4.0 EPA 8260B 12/19/2007 1:00 PM Approved

o-Xylene ND ug/L 0.27 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

Styrene ND ug/L 0.16 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

Bromoform ND ug/L 0.35 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

Isopropylbenzene ND ug/L 0.20 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

Bromobenzene ND ug/L 0.22 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved


ND = Analyzed for, but not detected above MDL (equlv. U) B = Analyte detected in sample, and in LB, LRB, LRB = Laboratory Reagent Blank



NA = Not applicable




LFB Laboratory Fortified Blank (equlv. LCS) LFM = Laboratory Fortified Sample Matrix (equiv. MS) QCS = Quality Control Sample (external to lab) acceptance limits as per method or Interlaboratory proficiency study



EPA#:MA00019




Sample Field ID*: DEP-3 Locator: Collector: Giddings,P Receive Date: 12/19/2006 12:20 PM


1 , 1 ,2,2-Tetrachloroethane ND ug/L 0.26 2.0 EPA 8260B 12/19/2007 1.-OOPM Approved

1 ,2,3-Trichloropropane ND ug/L 0.37 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

n-Propylbenzene ND ug/L 0.14 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved



1 ,3,5-Trimethylbenzene ND ug/L 0.13 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

tert-Butylbenzene ND ug/L 0.18 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

1 ,2,4-Trimethylbenzene ND ug/L 0.14 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved

sec-Butylbenzene ND ug/L 0.17 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

1 ,3-Dichlorobenzene ND ug/L 0.18 2.0 EPA 8260B 12/19/2007 1:00 PM Approved 4-lsopropyltoluene ND ug/L 0.27 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

1 ,4-Dichlorobenzene ND ug/L 0.28 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

1 ,2-Dichlorobenzene ND ug/L 0.29 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

n-Butylbenzene ND ug/L 0.17 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

1 ,2-Dibromo-3-chloropropane ND ug/L 0.75 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved


Hexachlorobutadiene ND ug/L 0.84 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

Naphthalene ND ug/L 0.52 2.0 EPA 8260B 12/1 9/2007 1:00 PM Approved


N = Methyl pentene, hexanal, heptanal, cyclootyl alcohol, nonanal, several other unidentified small peaks.

Sample Lab ID*: 2006491-005 Site: Sutton Brook Matrix: TB Collect Date: 12/19/2006

Sample Field ID#: Trip Blank Locator- Collector: Giddings,P Receive Date: 12/19/2006 12:20PM

Analvte/Compound Units MDL RDL Method Analysis Date Status


ND = Analyzed for, but not detected above MDL (equfv. U) B = Analyte detected In sample, and in LB, LRB, LRB = Laboratory Reagent Blank and/or trip blank or no trip blank was collected LB = Laboratory Blank (equlv. Method Blank) Estimated Value:

M = Analyte concentration > MDL but < RDL N = GC/MS non-target tentatively Identified compound LFB = Laboratory Fortified Blank (equiv. LCS)

H = USEPA holding time exceeded (TIC) - no standard available for quantitatlon LFM = Laboratory Fortified Sample Matrix (equlv. MS) QCS = Quality Control Sample (external to lab) J = Other QC criteria not met (see comments) R B Data rejected due to severe QC, quantitatlon acceptance limits as per method or Interlaboratory and/or qualitative ID deficiencies



EPA#:MA00019




Sample Lab ID*: 2006491-005 Site: Sutton Brook Matrix: TB Collect Date: 12/19/2006

Sample Field ID*: Trip Blank Locator: Collector: Giddings , P Receive Date: 12/19/2006 12:20 PM



Dibromofluoromethane 98 % Recovery 70-130 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Toluene-d8 96 % Recovery 70-130 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

4-bromofluorobenzene 88 % Recovery 70-130 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Dichlorodifluoromethane ND "ug/L 0.27 2.0 EPA8260B ~~ 12/19/2007 1:00 PM Approved

Chloromethane ND ug/L 0.32 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Vinyl chloride ND ug/L 0.23 2.0 EPA 8260B 12/19/2007 1 :00 PM Approved

Bromomethane ND ug/L 0.46 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Chloroethane ND ug/L 0.17 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Acetone ND ug/L 10 50 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

Trichlorofluoromethane ND ug/L 0.44 2.0 EPA 8260B 12/19/2007 1 :00 PM Approved

1,1-Dichloroethene ND ug/L 0.49 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Carbon disulfide ND ug/L 0.52 2.0 EPA 8260B 12/19/2007 1:00 PM Approved

Methylene chloride ND ug/L 0.24 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Freon-113 ND ug/L 0.46 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

trans-1 ,2-Dichloroethene ND ug/L 0.30 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Methyl-t-butyl ether ND ug/L 0.32 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

1,1-Dichloroethane ND ug/L 0.49 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

MEK ND ug/L 4.6 20 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Chlorobromomethane ND ug/L 0.44 2.0 EPA8260B 12/19/2007 1 :00 PM Approved

2,2-Dichloropropane ND ug/L 0.52 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

cis-1 ,2-Dichloroethene ND ug/L 0.43 2.0 EPA 8260B 12/19/2007 1 :00 PM Approved

Chloroform 4.6 ug/L 0.41 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

1,1,1 -Trichloroethane ND ug/L 0.37 2.0 EPA8260B 12/19/2007 1 :00 PM Approved

Carbon tetrachloride ND ug/L 0.25 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved


ND = Analyzed for, but not detected above MDL (equiv. U) B = Analyte detected In sample, and In LB, LRB, LRB = Laboratory Reagent Blank and/or trip blank or no trip blank was collected LB = Laboratory Blank (equlv. Method Blank) Estimated Value:

LFB = Laboratory Fortified Blank (equlv. LCS) M = Analyte concentration > MDL but < RDL N = GC/MS non-target tentatively Identified compound LFM = Laboratory Fortified Sample Matrix (equlv. MS) H = USEPA holding time exceeded (TIC) - no standard available for quantltation QCS = Quality Control Sample (external to lab) J = Other QC criteria not met (see comments) R = Data rejected due to severe QC, quantltation acceptance limits as per method or Interlaboratory and/or qualitative ID deficiencies



EPA#:MA00019



Sample Lab ID*: 2006491-005 Site: Button Brook Matrix: TB Collect Date: 12/19/2006

Sample Field ID*: Trip Blank Locator: Collector: Giddings, P Receive Date: 12/19/2006 12:20 PM

Analvte/Comoound Result Units MDL RDL Method Analysis Date Status

1 , 1 -Dichloropropene ND ug/L 0.23 2.0 EPA8260B 12/1 9/2007 1:00 PM Approved

Benzene ND ug/L 0.32 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

1 ,2-Dichloroethane ND ug/L 0.34 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

Trichloroethene ND ug/L 0.20 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

1 ,2-Dichloropropane ND ug/L 0.27 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

Dibromomethane ND ug/L 0.32 2,0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved



MIBK ND ug/L 2.1 20 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

Toluene ND ug/L 0.29 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

trans-1 ,3-Dichloropropene ND ug/L 0.44 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

1 ,1 ,2-Trichloroethane ND ug/L 0.24 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Tetrachloroethene ND ug/L 0.30 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved


Dibromochlorom ethane ND ug/L 0.30 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

1 ,2-Dibromoethane ND ug/L 0.30 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Chloro benzene ND ug/L 0.22 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

1,1,1 ,2-Tetrachloroethane ND ug/L 0.27 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Ethylbenzene ND ug/L 0.17 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

p,m-xylene ND ug/L 0.49 4.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

o-Xylene ND ug/L 0.27 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved

Styrene ND ug/L 0.16 2.0 EPA 8260B 12/19/2007 1 :00 PM Approved

Bromoform 0.43 M ug/L 0.35 2.0 EPA8260B 1 2/1 9/2007 1 :00 PM Approved

I sopropylbenzene ND ug/L 0.20 2.0 EPA 8260B 1 2/1 9/2007 1 :00 PM Approved



ND = Analyzed for, but not detected above MDL (equiv. U) B = Analyte detected In sample, and in LB, LRB, LRB = Laboratory Reagent Blank



NA = Not applicable

N = GC/MS non-target tentatively identified compound (TIC) - no standard available for quantitatlon



LFB = Laboratory Fortified Blank (equiv. LCS) LFM = Laboratory Fortified Sample Matrix (equiv. MS) QCS = Quality Control Sample (external to lab) acceptance limits as per method or interlaboratory proficiency study


Report Print Date: 1 /29/2007 MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION Page 15 of 24 DIVISION OF ENVIRONMENTAL ANALYSIS WILLIAM X. WALL EXPERIMENT STATION

EPA*:MA00019




Sample Lab ID* 2006491-005 Site: Sutton Brook Matrix: TB Collect Date: 12/19/2006

Sample Field ID*: Trip Blank Locator: Collector: Giddings,P Receive Date: 12/19/2006 12:20PM

Analvte/Compound Result Units MDL RDL Method Analysis Date Status 1 ,1 ,2,2-Tetrachloroethane ND ug/L 0.26 2.0 EPA 8260B 12/19/2007 1 00PM Approved

1 ,2,3-Trichloropropane ND ug/L 0.37 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

n-Propylbenzene ND ug/L 0.14 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

2-Chlorotoluene ND ug/L 0.070 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

4-Chlorotoluene ND ug/L 0.33 2.0 EPA 8260B 12/19/2007 1 00 PM Approved 1 ,3,5-Trimethylbenzene ND ug/L 0.13 2.0 EPA 8260B 12/19/2007 100PM Approved

tert-Butylbenzene ND ug/L 0.18 2.0 EPA 8260B 12/19/2007 1 00 PM Approved 1 ,2,4-Trimethyl benzene ND ug/L 0.14 2.0 EPA 8260B 12/19/2007 1 00 PM Approved sec-Butylbenzene ND ug/L 0.17 2.0 EPA 8260B 12/19/2007 100PM Approved

1 ,3-Dichlorobenzene ND ug/L 0.18 2.0 EPA 8260B 12/19/2007 1:0p PM Approved 4-lsopropyltoluene ND ug/L 0.27 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

1 ,4-Dichlorobenzene ND ug/L 0.28 2.0 EPA 8260B 12/19/2007 100 PM Approved

1 ,2-Dichlorobenzene ND ug/L 0.29 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

n-Butyl benzene ND ug/L 0.17 2.0 EPA 8260B 12/19/2007 100 PM Approved

1 ,2-Dibromo-3-chloropropane ND ug/L 0.75 2.0 EPA 8260B 12/19/2007 100 PM Approved


Hexachlorobutadiene ND ug/L 0.84 2.0 EPA 8260B 12/19/2007 1 00 PM Approved

Naphthalene ND ug/L 0.52 2.0 EPA 8260B 12/19/2007 100 PM Approved


Quality Control Data

Analvte/Compound QCType Result Units Acceptance Criteria Method Spike Cone. Spike Units Analysis Date


ND = Analyzed for, but not detected above MDL (equlv. U) B = Analyte detected In sample, and in LB, LRB, LRB = Laboratory Reagent Blank



NA = Not applicable

N = GC/MS non-target tentatively identified compound (TIC) no standard available for quantltation



LFB = Laboratory Fortified Blank (equiv. LCS) LFM = Laboratory Fortified Sample Matrix (equlv. MS) QCS = Quality Control Sample (external to lab) acceptance limits as per method or interlaboratory proficiency study



EPA#:MA00019





Surrogate Dibromofluoromethane LCS 76 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:OOPM

Toluene-d8 LCS 76 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:OOPM

4-bromofluorobenzene LCS 73 % Recovery 70 - 130 EPA 8260B 10 ug/L 12/19/2007 1:OOPM

Dichlorodifluoromethane LCS 107 % Recovery 70- 130 EPA8260B 10 ug/L 12/19/2007 1 00PM

Chloromethane LCS 95 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 100PM

Vinyl chloride LCS 107 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 100PM

Bromomethane LCS 77 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1 00PM

Chloroethane LCS 79 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 100PM

Acetone LCS 112 % Recovery 70- 130 EPA 8260B 250 ug/L 12/19/2007 100PM

Trichlorofluoromethane LCS 112 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 100PM

1,1-Dichloroethene LCS 95 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 100PM

Carbon disulfide LCS 77 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1 00PM

Methylene chloride LCS 124 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1 00PM

Freon-113 LCS 103 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

trans-1,2-Dichloroethene LCS 109 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 100PM

Methyl-t-butyl ether LCS 114 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1 00PM

1,1-Dichloroethane LCS 111 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1 00PM

MEK LCS 109 % Recovery 70- 130 EPA 8260B 100 ug/L 12/19/2007 100PM

Chlorobromomethane LCS 111 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 100PM

2,2-Dichloropropane LCS 106 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1 00PM

cis-1,2-Dichloroethene LCS 99 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 100PM

Chloroform LCS 111 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 100PM

1,1,1 -Trichloroethane LCS 112 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 100PM

Carbon tetrachloride LCS 113 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

1,1 -Dichloropropene LCS 106 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:OOPM


ND = Analyzed for, but not detected above MDL (equiv. U) B a Analyte detected In sample, and In LB, LRB, LRB = Laboratory Reagent Blank and/or trip blank or no trip blank was collected LB = Laboratory Blank (equlv. Method Blank) Estimated Value:

LFB = Laboratory Fortified Blank (equiv. LCS) M = Analyte concentration > MDL but < RDL N a GC/MS non-target tentatively Identified compound LFM = Laboratory Fortified Sample Matrix (equiv. MS) H = USEPA holding time exceeded (TIC) - no standard available for quantltatlon QCS = Quality Control Sample (external to lab) J = Other QC criteria not met (see comments) R a Data rejected due to severe QC, quantltation acceptance limits as per method or Inter laboratory and/or qualitative ID deficiencies



EPA#:MA00019





Benzene LCS 118 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

1,2-Dichloroethane LCS 110 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

Trichloroethene LCS 116 % Recovery 70 - 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

1,2-Dichloropropane LCS 116 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

Dibromomethane LCS 118 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

Bromodichloromethane LCS 102 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

cis-1,3-Dichloropropene LCS 103 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

MIBK LCS 104 % Recovery 70- 130 EPA 8260B 100 ug/L 12/19/2007 1:00 PM

Toluene LCS 96 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

trans-1,3-Dichloropropene LCS 106 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

1,1,2-Trichloroethane LCS 114 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

Tetrachloroethene LCS 104 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

1,3-Dichloropropane LCS 111 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

Dibromochloromethane LCS 113 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

1,2-Dibromoethane LCS 108 % Recovery 70 - 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

Chlorobenzene LCS 101 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

1,1.1,2-Tetrachloroethane LCS 107 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

Ethylbenzene LCS 103 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

p,m-xylene LCS 107 % Recovery 70-130 EPA 8260B 20 ug/L 12/19/2007 1:00 PM

o-Xylene LCS 97 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

Styrene LCS 91 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

Bromoform LCS 99 % Recovery 70 - 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

Isopropylbenzene LCS 98 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

Bromobenzene LCS 97 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

1,1,2,2-Tetrachloroethane LCS 97 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

1,2,3-Trichloropropane LCS 81 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

Some vials contain largea lount of silt/soil,

ND = Analyzed for, but not elected above MDL (equlv. U) B = Analyte detected in sample, and In LB, LRB, LRB = Laboratory Reagent Blank and/or trip blank or no trip blank was collected LB = Laboratory Blank (equiv. Method Blank) Estimated Value:

M = Analyte concentratic > MDL but < RDL N = GC/MS non-target tentatively identified compound LFB = Laboratory Fortified Blank (equiv. LCS)

H = USEPA holding time exceeded (TIC) - no standard available for quantitation LFM = Laboratory Fortified Sample Matrix (equiv. MS) QCS = Quality Control Sample (external to lab) J = Other QC criteria not met (see comments) R = Data rejected due to severe QC, quantitation acceptance limits as per method or interlaboratory and/or qualitative ID deficiencies



EPA#:MA00019





n-Propylbenzene LCS 95 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

2-Chlorotoluene LCS 95 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

4-Chlorotoluene LCS 99 % Recovery 70-130 EPA 8260B 10 ug/L 12/1 9/2007 1:00 PM

1 ,3,5-Trimethylbenzene LCS 94 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

tert-Butylbenzene LCS 101 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

1 ,2,4-Trimethylbenzene LCS 97 % Recovery 70-130 EPA 8260B 10 ug/L 12/1 9/2007 1:00 PM

sec-Butyl benzene LCS 96 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

1 ,3-Dichlorobenzene LCS 90 % Recovery 70- 130 EPA 8260B 10 ug/L 12/1 9/2007 1:00 PM

4-lsopropyltoluene LCS 96 % Recovery 70- 130 EPA 8260B 10 ug/L 12/1 9/2007 1:00 PM



n-Butyl benzene LCS 119 % Recovery 70- 130 EPA 8260B 10 ug/L 12/1 9/2007 1:00 PM

1 ,2-Dibromo-3-chloropropane LCS 124 % Recovery 70- 130 EPA 8260B 10 ug/L 12/1 9/2007 1:00 PM

1 ,2,4-Trichlorobenzene LCS 111 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

Hexachlorobutadiene LCS 70 % Recovery 70-130 EPA 8260B 10 ug/L 12/1 9/2007 1:00 PM

Naphthalene LCS 112 % Recovery 70-130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

1 ,2,3-Trichlorobenzene LCS 76 % Recovery 70- 130 EPA 8260B 10 ug/L 12/1 9/2007 1:00 PM

Surrogate Dibromofluoromethane Method Blank 105 % Recovery 70- 130 EPA 8260B 10 ug/L 12/19/2007 1:00 PM

Toluene-d8 Method Blank 101 % Recovery 70- 130 EPA 8260B 10 ug/L 12/1 9/2007 1:00 PM

4-bromofluorobenzene Method Blank 106 % Recovery 70- 130 EPA 8260B 10 ug/L 12/1 9/2007 1:00 PM

Dichlorodifluoromethane Method Blank ND ug/L ND EPA8260B NA 12/1 9/2007 1:00 PM

Chloromethane Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 1:00 PM

Vinyl chloride Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 1:00 PM

Bromomethane Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 1:00 PM

Chloroethane Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 1:00 PM


ND = Analyzed for, but not detected above MDL (equiv. U) B = Analyte detected In sample, and In LB, LRB, LRB = Laboratory Reagent Blank and/or trip blank or no trip blank was collected LB = Laboratory Blank (equlv. Method Blank) Estimated Value:

M = Analyte concentration > MDL but < RDL N = GC/MS non-target tentatively identified compound LFB = Laboratory Fortified Blank (equiv. LCS)

H = USEPA holding time exceeded (TIC) - no standard available for quantltation LFM = Laboratory Fortified Sample Matrix (equiv. MS) QCS - Quality Control Sample (external to lab) J = Other QC criteria not met (see comments) R = Data rejected due to severe QC, quantitation acceptance limits as per method or interlaboratory and/or qualitative ID deficiencies



EPA ft: MA00019



r ' Quality Control Data

Analvte/Compound QCType Result Units Acceptance Criteria Method

Acetone Method Blank ND ug/L ND EPA 82608

Trichlorofluoromethane Method Blank ND ug/L ND EPA 8260B

1,1-Dichloroethene Method Blank ND ug/L ND EPA 8260B

Carbon disulfide Method Blank ND ug/L ND EPA 8260B

Methylene chloride Method Blank ND ug/L ND EPA 8260B

Freon-113 Method Blank ND ug/L ND EPA 8260B

trans-1 ,2-Dichloroethene Method Blank ND ug/L ND EPA 8260B

Methyl-t-butyl ether Method Blank ND ug/L ND EPA 8260B

1,1-Dichloroethane Method Blank ND ug/L ND EPA 8260B

MEK Method Blank ND ug/L ND EPA 8260B

Chlorobromomethane Method Blank ND ug/L ND EPA 8260B

2,2-Dichloropropane Method Blank ND ug/L ND EPA 8260B

cis-1 ,2-Dichloroethene Method Blank ND ug/L ND EPA 8260B

Chloroform Method Blank ND ug/L ND EPA 8260B

1,1,1 -Trichloroethane Method Blank ND ug/L ND EPA 8260B

Carbon tetrachloride Method Blank ND ug/L ND EPA 8260B

1,1-Dichloropropene Method Blank ND ug/L ND EPA 8260B

Benzene Method Blank ND ug/L ND EPA 8260B

1 ,2-Dichloroethane Method Blank ND ug/L ND EPA 8260B

Trichloroethene Method Blank ND ug/L ND EPA 8260B

1 ,2-Dichloropropane Method Blank ND ug/L ND EPA 8260B

Dibromomethane Method Blank ND ug/L ND EPA 8260B

Bromodichloromethane Method Blank ND ug/L ND EPA 8260B

cis-1 ,3-Dichloropropene Method Blank ND ug/L ND EPA 8260B

MIBK Method Blank ND ug/L ND EPA 8260B

Toluene Method Blank ND ug/L ND EPA 8260B


ND = Analyzed for, but not detected above MDL (equlv. U) B = Analyte detected in sample, and In LB, LRB,

Spike Cone. Spike Units Analysis Date

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

LRB = Laboratory Reagent Blank

Estimated Value: M = Analyte concentration > MDL but < RDL H = USEPA holding time exceeded J = Other QC criteria not met (see comments)

NA = Not applicable

and/or trip blank or no trip blank was collected N = GC/MS non-target tentatively identified compound

(TIC) - no standard available for quantitation R = Data rejected due to severe QC, quantitation

and/or qualitative ID deficiencies MDL = Method Detection Limit

LB = Laboratory Blank (equiv. Method Blank) LFB = Laboratory Fortified Blank (equlv. LCS) LFM = Laboratory Fortified Sample Matrix (equiv. MS) QCS = Quality Control Sample (external to lab) acceptance limits as per method or interlaboratory proficiency study



EPA#:MA00019





trans-1,3-Dichloropropene Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 1:00 PM

1,1,2-Trichloroethane Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 1:00 PM

Tetrachloroethene Method Blank ND ug/L ND EPA 8260B NA 12/1 9/2007 1:00 PM

1,3-Dichloropropane Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 1:00 PM

Dibromochloromethane Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 1:00 PM

1,2-Dibromoethane Method Blank ND ug/L ND EPA 8260B NA 12/1 9/2007 1:00 PM

Chlorobenzene Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 1:00 PM

1,1,1,2-Tetrachloroethane Method Blank ND ug/L ND EPA 8260B NA 12/1 9/2007 1:00 PM

Ethylbenzene Method Blank ND ug/L ND EPA 8260B NA 12/1 9/2007 1:00 PM

p,m-xylene Method Blank ND ug/L ND EPA 8260B NA 12/1 9/2007 1:00 PM

o-Xylene Method Blank ND ug/L ND EPA 8260B NA 12/1 9/2007 1:00 PM

Styrene Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 1:00 PM

Bromoform Method Blank ND ug/L ND EPA 8260B NA 12/1 9/2007 1:00 PM

Isopropylbenzene Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 :OOPM

Bromobenzene Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 :OOPM

1,1,2,2-Tetrachloroethane Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 :OOPM

1,2,3-Trichloropropane Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 :OOPM

n-Propylbenzene Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 :OOPM

2-Chlorotoluene Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 :OOPM

4-Chlorotoluene Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 :OOPM

1,3,5-Trimethylbenzene Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 :OOPM

tert-Butylbenzene Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 :OOPM

1,2,4-Trimethylbenzene Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 :OOPM

sec-Butylbenzene Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 :OOPM

1,3-Dichlorobenzene Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 :OOPM

4-lsopropyltoluene Method Blank ND ug/L ND EPA 8260B NA 12/19/2007 :OOPM


ND = Analyzed for, but not detected above MDL (equiv. U) B = Analyte detected in sample, and in LB, LRB, LRB = Laboratory Reagent Blank and/or trip blank or no trip blank was collected LB = Laboratory Blank (equiv. Method Blank) Estimated Value:

M = Analyte concentration > MDL but < RDL N = GC/MS non-target tentatively Identified compound LFB = Laboratory Fortified Blank (equiv. LCS)

H • USEPA holding time exceeded (TIC) - no standard available for quantltatlon LFM = Laboratory Fortified Sample Matrix (equiv. MS) QCS = Quality Control Sample (external to lab) J = Other QC criteria not met (see comments) R = Data rejected due to severe QC, quantltatlon acceptance limits as per method or Interlaboratory and/or qualitative ID deficiencies

NA = Not applicable proficiency study MDL = Method Detection Limit RDL = Reporting Detection Limit (equiv. MRL)


EPA*:MA00019


Prepared For: NERO BUREAU OF WASTE SITE CLEANUP Project Name: Contact: Paul Giddings

Analvte/Compound

1 ,4-Dichlorobenzene

1 ,2-Dichlorobenzene

n-Butyl benzene

1 ,2-Dibromo-3-chloropropane

1 ,2,4-Trichlorobenzene

Hexachlorobutadiene

Naphthalene

1 ,2,3-Trichlorobenzene

Surrogate

Dibromofluoromethane

Toluene-d8

4-bromofluorobenzene

Dichlorodifluoromethane

Chloromethane

Vinyl chloride

Bromomethane

Chloroe thane

Acetone

QCType Result Method Blank ND

Method Blank ND

Method Blank ND

Method Blank ND

Method Blank ND

Method Blank ND

Method Blank ND

Method Blank ND

SampDUP 130

Samp DUP 95

SampDUP 115

Samp DUP 0.0

Samp DUP 0.0

Samp DUP 0.0

Samp DUP 0.0

Samp DUP 0.0

Samp DUP 82 Duplicate result Is acceptable because result Is <MDL.

Trichlorofluorom ethane

1,1-Dichloroethene

Carbon disulfide

Methylene chloride

Freon-113

trans-1 ,2-Dichloroethene

Methyl-t-butyl ether

Samp DUP 0.0

Samp DUP 0.0

Samp DUP 0.0

Samp DUP 0.0

Samp DUP 0.0

Samp DUP 0.0

Samp DUP 0.0


ND = Analyzed for, but not detected above MDL (equlv. U)

Estimated Value: M = Analyte concentration > MDL but < RDL H = USEPA holding time exceeded J = Other QC criteria not met (see comments)

NA = Not applicable

Project Coordinator:


Spike Cone. Spike Units Analysis Date

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/19/2007 1:00 PM

10 ug/L 12/19/2007 1:00 PM

10 ug/L 12/19/2007 1:00 PM

10 ug/L 12/19/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

LRB = Laboratory Reagent Blank LB = Laboratory Blank (equlv. Method Blank) LFB = Laboratory Fortified Blank (equlv. LCS) LFM = Laboratory Fortified Sample Matrix (equlv. MS) QCS = Quality Control Sample (external to lab) acceptance limits as per method or Interlaboratory proficiency study

Units

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

% Recovery

% Recovery

% Recovery

RPD

RPD

RPD

RPD

RPD

RPD

RPD

RPD

RPD

RPD

RPD

RPD

RPD

Acceptance Criteria

ND

ND

ND

ND

ND

ND

ND

ND

70-130

70-130

70- 130

0-20

0-20

0-20

0 -20

0-20

0-20

0-20

0-20

0 -20

0-20

0 -20

0 -20

0-20

Method

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

EPA 8260B

B = Analyte detected in sample, and In LB, LRB, and/or trip blank or no trip blank was collected

N = GC/MS non-target tentatively Identified compound (TIC) - no standard available for quantitatlon

R = Data rejected due to severe QC, quantitatlon and/or qualitative ID deficiencies

MDL = Method Detection Limit RDL = Reporting Detection Limit (equiv. MRL)

Report Print Date: 112912007 MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION Page 22 of 24 DIVISION OF ENVIRONMENTAL ANALYSIS WILLIAM X. WALL EXPERIMENT STATION

EPA#:MA00019




Analvte/Compound QC Type Result Units Acceptance Criteria Method

1,1-Dichloroethane Samp DUP 0.0 RPD 0 - 20 EPA 8260B

MEK Samp DUP 0.0 RPD 0 - 20 EPA 8260B

Chlorobromomethane Samp DUP 0.0 RPD 0 - 20 EPA 8260B

2,2-Dichloropropane Samp DUP 0.0 RPD 0 - 20 EPA 8260B

cis-1,2-Dichloroethene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

Chloroform Samp DUP 200 RPD 0 - 20 EPA 8260B Duplicate result is acceptable because result is <RDL.

1,1,1-Trichloroethane Samp DUP 0.0 RPD 0 - 20 EPA 8260B

Carbon tetrachloride Samp DUP 0.0 RPD 0 - 20 EPA 8260B

1,1-Dichloropropene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

Benzene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

1,2-Dichloroethane Samp DUP 0.0 RPD 0 - 20 EPA 8260B

Trichloroethene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

1 ,2-Dichloropropane Samp DUP 0.0 RPD 0 - 20 EPA 8260B

Dibromomethane Samp DUP 0.0 RPD 0 - 20 EPA 8260B

Bromodichloromethane Samp DUP 0.0 RPD 0 - 20 EPA 8260B

cis-1,3-Dichloropropene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

MIBK Samp DUP 0.0 RPD 0 - 20 EPA 8260B

Toluene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

trans-1 ,3-Dichloropropene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

1,1,2-Trichloroethane Samp DUP 0.0 RPD 0 - 20 EPA 8260B

Tetrachloroethene Samp DUP 200 RPD 0 - 20 EPA 8260B Duplicate result Is acceptable because result is <RDL.

1 ,3-Dichloropropane Samp DUP 0.0 RPD 0 - 20 EPA 8260B

Dibromochloromethane Samp DUP 0.0 RPD 0 - 20 EPA 8260B

1 ,2-Dibromoethane Samp DUP 0.0 RPD 0 - 20 EPA 8260B


VD = Analyzed for, but not detected above MDL (equiv. U) B = Analyte detected In sample, and in LB, LRB,

Spike Cone. Spike Units Analysis Date NA 12/19/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/19/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/1 9/2007 1:00 PM

NA 12/19/2007 1:00 PM




MA = Not applicable

N = GC/MS non-target tentatively identified compound (TIC) no standard available for quantitatlon



LFB = Laboratory Fortified Blank (equiv. LCS) LFM = Laboratory Fortified Sample Matrix (equiv. MS) QCS = Quality Control Sample (external to lab) acceptance limits as per method or Interlaboratory proficiency study

-\ RDL = Reporting Detection Limit (equiv. MRL)

Report Print Date: 1/29/2007 MASSACHUSETTS DEPARTMENT OF ENVIRONMENTAL PROTECTION Page 23 of 24 DIVISION OF ENVIRONMENTAL ANALYSIS WJLLIAM X. WALL EXPERIMENT STATION

EPA ft: MA00019


ASTE SITE CLEANUP Project Name:

Project Coordinator:


Analvte/Compound QCType Resu lit Units Acceptance Criteria Method

Chlorobenzene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

1,1,1 ,2-Tetrachloroethane Samp DUP 0.0 RPD 0 - 20 EPA 8260B

Ethylbenzene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

p,m-xylene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

o-Xylene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

Styrene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

Bromoform Samp DUP 0.0 RPD 0 - 20 EPA 8260B

Isopropyl benzene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

Bromobenzene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

1 , 1 ,2,2-Tetracnloroethane Samp DUP 0.0 RPD 0 - 20 EPA 8260B

1 ,2,3-Trichloropropane Samp DUP 0.0 RPD 0 - 20 EPA 8260B

n-Propylbenzene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

2-Chlorotoluene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

4-Chlorotoluene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

1 ,3,5-Trimethylbenzene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

tert-Butylbenzene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

1,2,4-Trimethylbenzene Samp DUP 200 RPD 0 - 20 EPA 8260B Duplicate result Is acceptable because result is <RDL.

sec-Butyl benzene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

1 ,3-Dichlorobenzene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

4-lsopropyltoluene Samp DUP 0.0 RPD 0 - 20 EPA 8260B



n-Butylbenzene Samp DUP 0.0 RPD 0 - 20 EPA 8260B

1 ,2-Dibromo-3-chloropropane Samp DUP 0.0 RPD 0 - 20 EPA 8260B

1 ,2,4-Trichlorobenzene Samp DUP 0.0 RPD 0 - 20 EPA 8260B


ND = Analyzed for, but not detected above MDL (equlv. U) B = Analyte detected in sample, and In LB, LRB,

Spike Cone. Spike UnitsNA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA

NA


Analysis Date 12/1 9/2007 1:00 PM 12/1 9/2007 1:00 PM

12/1 9/2007 1:00 PM

12/1 9/2007 1:00 PM

12/1 9/2007 1:00 PM

12/1 9/2007 1:00 PM 12/1 9/2007 1:00 PM

12/1 9/2007 1:00 PM

12/1 9/2007 1:00 PM

12/1 9/20071. -00PM

12/1 9/2007 1:00 PM

12/1 9/2007 1:00 PM

12/1 9/2007 1:00 PM

12/1 9/2007 1:00 PM

12/1 9/2007 1:00 PM

12/1 9/2007 1:00 PM

12/19/2007 1:00 PM

12/19/2007 1:00 PM

12/1 9/2007 1:00 PM

12/1 9/2007 1:00 PM

12/1 9/2007 1:00 PM

12/1 9/2007 1:00 PM

12/1 9/2007 1:00 PM

12/19/2007 1:00 PM

12/1 9/2007 1:00 PM



NA = Not applicable

N = GC/MS non-target tentatively identified compound (TIC) - no standard available for quantitatlon



LFB = Laboratory Fortified Blank (equiv. LCS) LFM = Laboratory Fortified Sample Matrix (equiv. MS) QCS = Quality Control Sample (external to lab) acceptance limits as per method or Intel-laboratory proficiency study



EPA#:MA00019






Hexachlorobutadiene Samp DUP 0.0 RPD 0-20 EPA 8260B NA 12/19/2007 1:00 PM

Naphthalene Samp DUP 0.0 RPD 0 -2 0 EPA 8260B NA 12/19/2007 1:00 PM

1,2,3-Trichlorobenzene Samp DUP 0.0 RPD 0-20 EPA 8260B NA 12/19/2007 1:00 PM

Sample Lab ID#: 2006491-002

Approved*: .^/wees 1/29/2007

*QA Level 1 and 2 Completed - QA/QC documentation, raw analytical data, and Chaln-of-Custody/Sample Tracking Form are available upon request.


ND = Analyzed for, but not detected above MDL (equlv. U) B = Analyte detected In sample, and in LB, LRB, and/or trip blank or no trip blank was collected Estimated Value:

M = Analyte concentration > MDL but < RDL N = GC/MS non-target tentatively Identified compound H = USEPA holding time exceeded (TIC) - no standard available for quantltatlon J = Other QC criteria not met (see comments) R = Data rejected due to severe QC, quantltation

and/or qualitative ID deficiencies NA = Not applicable

MDL = Method Detection Limit RDL = Reporting Detection Limit (equiv. MRL)

LRB = Laboratory Reagent Blank LB = Laboratory Blank (equiv. Method Blank) LFB = Laboratory Fortified Blank (equlv. LCS) LFM = Laboratory Fortified Sample Matrix (equiv. MS) QCS = Quality Control Sample (external to lab) acceptance limits as per method or Interlaboratory proficiency study

Documents

Prepared For: NER BUREAU OF WASTOE SITE CLEANUP …QCS = Quality Control Sample (external to lab) acceptance limits as per method or Interlaboratory proficiency study . RDL = Reporting