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Preparation, Characterization of TiO Nanoparticles by ...docsdrive.com/pdfs/medwelljournals/jeasci/2018/10364-10374.pdf · 35 30 25 20 15 10 5 0 Percentage 0 20 40 60 80 100 0.00

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Page 1: Preparation, Characterization of TiO Nanoparticles by ...docsdrive.com/pdfs/medwelljournals/jeasci/2018/10364-10374.pdf · 35 30 25 20 15 10 5 0 Percentage 0 20 40 60 80 100 0.00
Page 2: Preparation, Characterization of TiO Nanoparticles by ...docsdrive.com/pdfs/medwelljournals/jeasci/2018/10364-10374.pdf · 35 30 25 20 15 10 5 0 Percentage 0 20 40 60 80 100 0.00
Page 3: Preparation, Characterization of TiO Nanoparticles by ...docsdrive.com/pdfs/medwelljournals/jeasci/2018/10364-10374.pdf · 35 30 25 20 15 10 5 0 Percentage 0 20 40 60 80 100 0.00

20

15

10

5

0

Perc

enta

ge

0 20 40 60 80 100 120 140

Diameter (nm)

11.12 0.00 1546.73

1031.16

515.58 0.00 0.00

511.79

1023.57

1535.36

nm

2000

1500

1000

500

0

nm

0 500 1000 1500 2000

11.12 10.00 8.00 6.00 4.00 2.00 0

nm

…/197.csm CSPM title Topography Pixels = (408, 405) Size (2062 and 2047 nm)

(a) (b)

(c)

nm

nm

nm

Perc

enta

ge 30

25 20 15 10 5 0

0 40 80 120 160 Diameter (nm)

3.11 nm -0.02 1516.48

1010.98 505.49 nm

0.00 0.00 514.94

1544.82 1029.88

2000

1500

1000

500

0

nm

0 500 1000 1500 2000 nm

3.00

2.50

2.00

1.50

1.00

0.50

0

nm

…/200.csm CSPM title Topography Pixels = (428, 436) Size = (2022 and 2060 m)

(a) (b)

(c)

nm

Page 4: Preparation, Characterization of TiO Nanoparticles by ...docsdrive.com/pdfs/medwelljournals/jeasci/2018/10364-10374.pdf · 35 30 25 20 15 10 5 0 Percentage 0 20 40 60 80 100 0.00

35 30 25 20 15 10 5 0

Perc

enta

ge

0 20 40 60 80 100 Diameter (nm)

(a)

33.91 -0.17

nm

1503.49 1002.32

501.16 nm 0.00 0.00

511.71 1023.43

1535.14

nm

(b) 2000

1500

1000

500

0

nm

(c) 33.91 30.00 25.00 20.00 15.00 10.00 5.00 0

200…/-csm CSPM title Topography Pixels = (380.388) Size = (2005 and 2047 nm)

700

600

500

400

300

200

100

0

Cou

nts

(a)

10 20 30 40 50 60 70 80 Values

101

004

300

280

260

240

220

200

180

160

140

120

100

800

600

400

200 0

Cou

nts

20 30 40 50 60 70 80 Values

(b) 101A

110 R 101 R

004 A

111 R 112 A

200 A

105 A 211 A 204 A

TiO2

15000

10000

5000

0 10 20 30 40 50 60 70

Copper (Cu)

(a)

Val

ues

1300

1200

1100

1000

900

800

700

600

500

400

300

200

100

0

Cou

nts

20 30 40 50 60 70 80 Values

(b)

Page 5: Preparation, Characterization of TiO Nanoparticles by ...docsdrive.com/pdfs/medwelljournals/jeasci/2018/10364-10374.pdf · 35 30 25 20 15 10 5 0 Percentage 0 20 40 60 80 100 0.00

3500

3000

2500

2000

1500

1000

500

0 0 5 10 15

keV

Val

ues

TiLα 0 Kα

200 nm

(a) (b) TiKα

60 nm

3500

3000

2500

2000

1500

1000

500

0

TiKα

TiLα 0 Kα

200 nm

0 5 10 15 keV

Val

ues

(a) (b)

80 nm

Page 6: Preparation, Characterization of TiO Nanoparticles by ...docsdrive.com/pdfs/medwelljournals/jeasci/2018/10364-10374.pdf · 35 30 25 20 15 10 5 0 Percentage 0 20 40 60 80 100 0.00

o a

o

C -C(D%) ×100%

3000

2500

2000

1500

1000

500

0

TiKα

0 5 10 15 keV

Val

ues

200 nm

(a) (b)

40 nm

60

50

40

30

20

10

0

Val

ues

0 50 100

Time (min)

Page 7: Preparation, Characterization of TiO Nanoparticles by ...docsdrive.com/pdfs/medwelljournals/jeasci/2018/10364-10374.pdf · 35 30 25 20 15 10 5 0 Percentage 0 20 40 60 80 100 0.00
Page 8: Preparation, Characterization of TiO Nanoparticles by ...docsdrive.com/pdfs/medwelljournals/jeasci/2018/10364-10374.pdf · 35 30 25 20 15 10 5 0 Percentage 0 20 40 60 80 100 0.00
Page 9: Preparation, Characterization of TiO Nanoparticles by ...docsdrive.com/pdfs/medwelljournals/jeasci/2018/10364-10374.pdf · 35 30 25 20 15 10 5 0 Percentage 0 20 40 60 80 100 0.00
Page 10: Preparation, Characterization of TiO Nanoparticles by ...docsdrive.com/pdfs/medwelljournals/jeasci/2018/10364-10374.pdf · 35 30 25 20 15 10 5 0 Percentage 0 20 40 60 80 100 0.00
Page 11: Preparation, Characterization of TiO Nanoparticles by ...docsdrive.com/pdfs/medwelljournals/jeasci/2018/10364-10374.pdf · 35 30 25 20 15 10 5 0 Percentage 0 20 40 60 80 100 0.00