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    mal and Cryogenic Testing

    ms Development

    penter

    StateUniversity Los Angeles

    ulsion Laboratory

    o Urquiza Ph.D., P.E.

    ct:

    model, fabricate, setup, conduct and analyze thermal and cryogenic test results for several current JPL projects.

    tra Compact Imaging Spectroscopy (UCIS):

    y the eective thermal conductance of a data cable to enable optimization of tactical cryocooler use in future systems.

    rborne scanning MultiSPectral Infrared instrument (AirMSPI):

    nd run a test to determine whether normal operating thermal stresses on a silica lter will result in epoxy failure and delamination of

    rs within the silica lter.

    ars Atmospheric Trace Molecule Occultation Spectrometer (MATMOS):

    interface parts in Solidworks for the physical connection between the radiator, thermal strap and load; and created a LabVIEW data

    ion graphical user interface for the test data characterizing the cooling system thermal performance.

    Sounding Oceanographic Lagrangian Observer Thermal RECharging (SOLO TREC):

    nduct testing of the accumulator portion of the power generation subsystem for the SOLO TREC Submersible that derives its power from

    nging thermoclines of sea water. Tasks include implementing improvements to the power generation subsystem, to increase reliability

    ime.

    ce to NASA:

    one of the projects will be going into space any time soon, both AirMSPI and SOLO TREC will be utilized on active NASA missions in the

    ure. During this internship MATMOS lost its funding when NASA pulled out of the European Space Agencys ExoMars Trace Gas Orbiter

    ated to launch in 2016. But the technology is good and the results of the thermal vacuum test should help to sell the technology for

    rojects. UCIS is still in its infancy, but could very well end up on a future rover, or utilizing a small space on a satellite to conduct

    ents.

    e:

    engineer it was my goal to quickly set up and conduct tests pertaining to the performance of parts and systems under working

    ons. I will discuss each of my projects individually to better illustrate my work.

    Methods:

    S project ts many applications, from an airborne or ground based spectroscopy instrument to future applications in a small space on

    rcial satellites or a rover on other planets or moons. In the current conguration it was found that there was a heat leak that required a

    tactical cryocooler to maintain the desired temperature of 150K. This means there was an unaccounted for heat source.

    etermined that this was probably through the data cable that communicates to the exterior instruments. UCIS is currently used in the

    here in places like Death Valley, so it is safe to say there is at least a 150K temperature dierence between the ends of the cable. UCIS is

    d as an inexpensive alternative to past por table Spectrometers, therefore a pre made cable was used, this while saving cost meant it

    ot be designed for the specic application and properties sought.

    an un-quantied amount of copper being used sandwiched with Kapton, a polyamide that is stable at a large range of temperatures

    s not outgas in a vacuum. This precludes the ability to calculate the conductance based on pure material properties and necessitates a

    he working conditions to get an overall conductance of the complete cable. This will allow the right sizing of the tactical cryocooler in

    re to keep cost and power consumption down.

    Target Focus

    odeling the cable in Solidworks, I designed a test that would give me the eective conductance of the cable. Conductance is the

    t of heat (watts) over temperature drop (kelvin), therefore, I had to nd a way to accurately measure the heat rate input in watts and the

    ature on either end of the strap. We are only interested in the conductance so the other forms of heat transfer need to be negated as

    possible. To negate the eects of convection, the mean free path between particles in the surrounding has to be greater than the size

    st chamber. To achieve this, a vacuum chamber at 10^-6 Torr will give a mean free path between particles much greater than the whole

    chamber. To minimize radiation, a Multi-Layer Insulation (MLI) blanket is used so the vast majority of radiation heat is returned to the

    is also used to block any view of the cold sensor end of the assembly. This way we can assume that the applied watts are going into and

    the data cable.

    uce the temperature dierence between the two ends, a cryocooler is used on the sensor end of the cable. It can reach temperatures as

    0K so heat lift must be provided. To accomplish this, four 25W heaters are used each at 50ohms. The heaters are on two dierent circuits

    ater in parallel, cutting the resistance to 25ohms per circuit, using a 50V power supply this gives a maximum of 100W of heat per circuit.

    heat lift to maintain temperatures so much higher than the 40K the cold head is designed for.

    h thermal modeling in Solidworks, I determined that in order to get a fairly even temperature distribution on the sensor end of the cable,

    quarter inch piece of 6061 aluminum would be sucient. For each of the three data out plates a 5W heater would suce on a three

    piece of 6061 aluminum. In all cases, a one eighth piece of 6061 aluminum is used as a compression backing using indium to increase

    mal connection then they are compression t securely together.

    Computer Models

    ee data out cables are then hung from manganin wires. At Cryogenic temperatures which are 150K or below, silicon diodes provide the

    mperature reading using phosphor bronze wires to minimize heat leak. By curve tting the resistance change across the diode as a

    n of temperature, curves have been developed to get temperature readings. By applying a known current, then reading the voltage

    he diode, the resistance can be determined, (R=V/I) input that into the cur ve function and an accurate temperature reading is generated.

    ecting the diodes to a Lakeshore temperature reader these temperatures are read constantly with the right curves applied. By placing

    on diode at each of the edges of the kapton/copper cable the temperatures can be monitored. After the sensor end is stabilized at

    nd the data out ends at 300K. The voltage is read across the resistance heaters and also from either side of an installed shunt resistor of

    ute known resistance. The actual current can be determined for each heater by dividing the voltage over the shunt by its known

    ce. By squaring the current and multiplying by the resistance of the heaters the power can be determined. By adding up these powers in

    iding by the temperature dierence the eective conductance is determined.

    Test Setup

    time I set up the experiment and measured the resistance of each of the data out heater circuits, I found that there was an increase of

    ce of 9ohms from the manganin wire. This would not be a lot except that the 5W heaters I had on hand were only 25ohms of resistance.

    the stage for large joule heating losses through the manganin wire that would be impossible to accurately predict if it was going into

    e or not. So 500ohm resistors were ordered to be over-nighted.

    ings are as follows

    ctive Conductance is:

    K) Conductance

    009897

    010112525

    012046678

    009959191

    owing data shows the results from the eective conductance test. The heater power (W) is calculated by P=I^2 R using the current

    y reading the voltage across a shunt resistor than dividing that by the known resistance of the shunt. The heaters are at 300K roughly

    mperature where there resistances should be the same as measured at room temperature.

    data and graphs:

    150k data point this is the data from two dierent days and also hours apart.

    ductance and total power through the strap vary only slightly supporting the integrity of the data. The dierence in conductance of the

    st stabilized readings is = 7.36x10^-4(mW/K)

    erence in total heat is = 0.599(mW)

    g readings periodically it was possible to check the convergence of the change in temperature on zero.

    a denite convergence but not at zero, looking at the sensor plate there is a slight temperature increase that is tapering o as shown.

    e sensor plate stabilized the data out ends of the cable should converge towards zero.

    ctive conductance at the time of data collection for this period changed by 2.09x10^-4(W/K) or 0.046% therefore even without total

    ation this is fairly accurate. The total power also changed by 2.76x10^-4(W) or 0.0038%, unless a greater accuracy then that is desired

    nt is good.

    170K:

    For this data point the temperature change over time converged nicely towards zero leading me to believe it was a good data point. Unfortunatelyas demonstrated by the up oscillations of the data that the transient eects had not subsided making this an outlying data point.

    180K

    For this data point the temperature change over time converged nicely towards zero conrming the accuracy of the data.

    Airborne scanning MultiSPectral Infrared instrument (AirMSPI):

    This project utilizes a specially made silica lter. The lters are on layers between the silica glass. The whole thing is epoxied together using an

    epoxy with a similar clarity and refractive index as the silica. It was found through calculations that, due to the dierence in coecients of thermalexpansion thermal stresses would form. The operating temperature of the sensor is 200K at that temperature using the listed specications for the

    epoxy and silica there was a chance that the lter would delaminate. These specications where for properties at room temperature and probablyhave an unspecied factor of safety, therefore a test would let us know for sure if delamination would occur under operating conditions.

    Test SetupI created the through ports into the vacuum chamber, cables and connections for the heaters and the silicon diodes. I also tested the system for

    control because we wanted only to test the ability of the lter to handle the thermal stress of the operating temperatures not that of an abrupt

    temperature change. After an eective dry run, the lter was incorporated and I ran the test again with a slow cool down and warm up.

    Test Setup

    After plotting the results of the temperatures over time the lter was sent to be checked with an electron microscope. It did not delaminate, thebest case for everyone involved.

    Test Results

    Using the same setup we also categorized the conductance of a exible strap made of pyrolytic graphite sheet (PGS). Conductance is temperature

    dependent and also is inuenced by the temperature dierence. It was necessary to test the strap at dierent stabilized temperatures using thedierence of the two ends of the strap as the normalizing factor, then applying a heat load to the bottom to create a larger temperature dierence

    and taking the measurement after stabilization of temperature occurred again.

    Test Setup

    Mars Atmospheric Trace Molecule Occultation Spectrometer (MATMOS):

    Project Components

    The purpose of this test is to determine if the empirical results match the calculated results of a passive cooler designed for MATMOS. By using amulti stage passive cooler that radiates to cold space, the change in temperature between any two sides of a stage limited to maximize conduc-

    tance, this is a state of the art cooler that needs no external power. The polished surfaces are to reect the heat from the planet and the higheredge is extra insurance that the sun never shines directly on the cooling manifold if there is a wobble in the orbit of the satellite.

    I modeled the exible straps and their connectors and modied the cold head attachment above. Also interfaced with six Lakeshore devices of fourto eight channels reading silicon diodes placed strategically throughout the test system , sixty channels from an Agilent reading thermocouple

    temperatures and voltages across the heaters and shunt resistors. Using these I programed the data writing virtual instrument to calculate thepowers and the current for eight heater circuits. This LabVIEW project was my focus for a LabVIEW course that culminated in me passing the

    Certied LabVIEW associate developers (CLAD) exam o ered on lab.

    Sounding Oceanographic Lagrangian Observer Thermal RECharging (SOLO TREC):

    The Solo Trec completed a successful year and half o the coast of Hawaii of continuous dives measuring the salinity down to 500m of the oceanthen transmitting the data on each resur face three times a day. This generation will utilize wing-like structures to direct the dives covering more

    area and providing a much higher resolution study of the oceans salinity than the current thirty thousand probes being utilized for this function.With an improved power generation subsystem t his generation should prove extremely eective. It uses phase changing materials (PCM)

    formulated for various freezing points down to the four degrees Celsius found at ve hundred meter depths. The freezing and melting of thematerials pushes on a exible membrane, in return pushing hydraulic uid through a one way valve into an accumulator. The accumulator consists

    of a contained piston with nitrogen on one side and the hydraulic uid on the other. The hydraulic uid compresses the nitrogen up to 3000psi,

    when the vehicle needs power it releases some of the built up pressurized hydraulic uid to drive a generator, the hydraulic uid then travels intoan unpressurized reservoir waiting to be pulled into the PCM tube to start the cycle again.

    An increase in eciency for this generation comes from the use of open cell aluminum foam cylinders touching the outer walls of the vehicle. Byboring a hole through the center and placing the membrane containing the PCM in the center, there is a better heat transfer from the ocean to the

    PCM. Being the PCM only changes volume by 10% its increase pushes into the open cells of the foam further increasing the area of contact for heattransfer and displacing the hydraulic uid. One issue with this well t hought out system is the leak of nitrogen in the accumulator across the piston

    into the hydraulic uid over time. The nitrogen being compressible would decrease the eciency of the whole system. To determine the impactthis phenomena may have, a power generation subsystem was built using a pump instead of the PCM to build up pressure. By running this

    through thousands of repetitions we can measure the amount of nitrogen that leaks into the hydraulic uid.

    Testing Rig

    My part was to maintain the testing system and to install the motor and pump to simulate the PCMs. To make this work properly, the right pump

    and motor needed to be used. The rst two pumps blew o rings and leaked, the next motor was not strong enough to get up to the pressuresneeded. The third pump used a dierent viscosity of hydraulic uid meaning the system needed to be drained, cleaned and relled with a

    homogeneous viscosity of hydraulic uid, in case the viscosity played a part in the nitrogen leak rate. The working system is at the momentrunning well thanks to the hard work of all involved. The nitrogen leak appears to be minimal.

    Acknowledgements:

    I would like to thank Jose Rodrigues for his direction and expertise. Dean Johnson for his ever smiling demeanor and coee brewing. Jack Johnsonfor his enthusiasm and fantastic projects. Scott Leland for his help and wealth of information and stories. Russ Sugimura for his camaraderie and

    technical writing help. Howard Tseng and Jason Kempenaar for their friendship and in depth knowledge of the thermal world. ArthurNa-Nakornpanom for his stories and insights on OCO2, Dr. Helen Boussalis for the opportunities and support that has opened so many doors for

    me. Jenny Tieu for her belief and dedication in nding me a mentor. My family for their enthusiasm and supporting me through all the ext ra hours.

    And a special thanks to my mentor Eugenio (Keno) Urquiza for his guidance and personal tutelage, may his new endeavor be extremely successful.Also to the Space Grant and everyone involved in the NASA URC program, especially those at Space Center who have helped guide and push myknowledge and research skills.

    0

    0.002

    0.004

    0.006

    0.008

    0.01

    0.012

    0.014

    1 45 1 50 1 55 1 60 1 65 1 70 1 75 1 80 1 85

    Conductance(W/K)

    ColdEndTemperature (K)

    Conductance W/K

    0

    0.2

    0.4

    0.6

    0.8

    1

    1.2

    1.4

    1.6

    1.8

    1 45 1 50 1 55 1 60 1 65 1 70 1 75 1 80 1 85

    AppliedHeatWarmEn

    d(W)

    ColdEndTemperature (K)

    Watts

    Experience:

    Flora:

    Fauna:

    Thermal and Cryogenic Testing Systems Development

    SPACE Center; NASA-URC

    Kalind Carpenter

    Graduate Student in Mechanical Engineering

    California State University, Los Angeles

    Jet Propulsion Laboratory

    Program: Minority Student Programs; Education Office

    JPL Mentors:Eugenio Urquiza

    This work is supported by the NASA University Research Center (URC) Grant No. URC NCC NNX08BA44A in

    collaboration with Jet Propulsion Laboratory. Special thanks to our SPACE Center Director, Dr. Helen Boussalis.

    Heat Leak:

    Temp (K) Watts

    150 1.483956593

    160 1.437933664

    170 1.565345354

    180 1.200082555

    http://instrumentsystems.jpl.nasa.gov/projects/matmos/

    http://www.greencleaningideas.com/2010/05/nasas-solo-trec-robotic-diver-gets-powered-by-changing-ocean-temperatures/