PHASE II ENVIRONMENTAL SITE ASSESSMENT SUMTER …

PHASE II ENVIRONMENTAL SITE ASSESSMENT

SUMTER AIRPORT PROPERTY2945 AIRPORT ROAD

SUMTER, SCSITE ID # 43-04382

Prepared For:

Sumter County13 E. Canal StreetSumter, SC 29150

Prepared By:

Emerald, Inc.P.O. Box 3050

2520 Tahoe DriveSumter, South Carolina 29151

Report Date: January 29, 2010

Signature Page

This document entitled “Phase II Environmental Site Assessment Report”, has been

prepared for Sumter County to describe investigative activities initiated at the Sumter

County Airport located in Sumter, South Carolina. It has been prepared in accordance with

accepted quality control practices.

Emerald, Inc.

Ronny L. Lowder, CHMM, REPAPresident

Phase II Environmental Site Assessment ReportSumter County Airport

2945 Airport RoadSumter, South Carolina

TABLE OF CONTENTS

Section Page

1.0 Executive Summary. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

2.0 Introduction & Scope of Work. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

3.0 Regional & Site Specific Geology.. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

4.0 Site Activities. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

4.1 Soil & Groundwaer Assessment. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

4.2 Analytical.. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5

5.0 Results & Conclusions. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

6.0 Appendices.. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21

A) Field Screening Log & Water Well Records

B) Laboratory Analytical Results

C) SCDHEC Monitoring Well Approval No. 3745

1.0 Executive Summary

Emerald, Inc. has conducted a Phase II Environmental Site Assessment (Phase II

ESA) on the Sumter County Airport site at the request of Sumter County. Such Phase II

ESA was conducted in three areas of concern which were discovered to contain

Recognized Environmental Conditions (RECs) in Phase I Environmental Site Assessments

conducted in 2005 and 2008. The three areas of concern are located on the eastern side

of the airport property, and are designated as Area 1, Area 2, and Area 3 as seen on the

site map labeled Figure 1. Area 1 is associated with a former pesticides storage and

mixing area as part of an aerial spraying service; Area 2 is associated with a former solid

waste dump from hurricane debris deposited on the site in 1989 and 1990; and, Area 3 is

associated with a former railroad line that crossed the site but is no longer present.

The purpose of the Phase II ESA was to conduct soil and groundwater sampling in

the three areas of concern, and to have the samples analyzed by an independent

laboratory for Chemicals of Concern (CoCs) that would have been associated with the prior

use of each area. Such was conducted in December 2009, and the analytical results found

that each area has been impacted by CoCs in either the soil or groundwater, or both. In

Area 1, the analytical results found Toxaphene, an organochlorine pesticide, at a level 4.5

times the acceptable limit in soil, and 318 times the Maximum Contaminant Level (MCL)

in drinking water. Toxaphene is listed as possibly causing kidney, liver and thyroid

problems as well as an increased risk for cancer. Area 2 results found low levels of

petroleum and paint solvents in both the soil and groundwater, none of which are above

acceptable limits for such CoCs. Area 3 found levels of Total Petroleum Hydrocarbons

(TPH) in the soil. TPH is an indicator of the possible presence of used oils and creosote,

1

both used by railroad companies in the past.

The results of this Phase II ESA have found the presence of CoCs in each area;

however, the extent of the CoCs have not been determined in this initial assessment.

Additional assessment should be conducted to determine the horizontal and vertical extent

of the CoCs, the possible impact to nearby wetlands, and the risk to human health and the

environment that each area poses with regards to occupancy and development.

2.0 Introduction & Scope of Work

The Sumter County Airport (subject site) is located in a rural area in Sumter County,

north of the City of Sumter. Specifically, the site is located in an area bounded by Hill

Road on the north and west, Queen Chapel Road on the east, and W. Brewington Road

on the south. The site consists of approximately 730.15 acres of developed and

undeveloped land. Figure 2 contains an USGS topographic map showing the location of

the Sumter County Airport and the surrounding land.

In 2005 and 2008, Emerald, Inc. personnel conducted a Phase I ESA on the

Sumter Airport site. The Phase I ESA report found RECs due to the past usage of portions

of the site as an aerial spraying service where pesticides and herbicides were mixed and

stored, designated as Area 1; an area east of Area 1 where storm debris and solid waste

were deposited in 1989 and 1990 plus years after, designated as Area 2; and, an area east

of Area 2 where a former railroad line ran North-South through the property as seen on the

topographic map in Figure 2, designated as Area 3. A Phase II ESA was recommended

for the site to determine if there had been any adverse impact to the soil and/or

groundwater at the site during the time of usage for each area of concern. Specifically,

Area 1 may have been impacted by pesticides; Area 2 where white goods and empty paint

2

cans were observed in the Phase I ESA reports, may have been impacted by petroleum

products, paint products and possibly PCBs; and Area 3 may have been impacted by

waste oils used for vegetation control, and creosote used as a preservative for wooden

crossties.

A Phase II ESA was approved by Sumter County in November 2009, and SCDHEC

issued Temporary Monitoring Well Approval No. 3745 (copy in Appendix C) for the

collection of groundwater samples beneath the site. The Phase II ESA included soil and

groundwater sampling in the limited area of the three areas of concern. This report entitled

“Phase II Environmental Site Assessment” covers the findings of this assessment.

3.0 Regional & Site Specific Geology

The Sumter Airport site is located within the northern section of Sumter County.

Sumter County is part of the Atlantic Coastal Plain Physiographic Province of South

Carolina. This province is characterized by rolling or undulating areas along with broad

flats or nearly level areas.

The subject site is in an area dominated by sandy soils as characteristic of the

province. Continuous soil borings were conducted in the areas of concern from the ground

surface to the shallow aquifer which was typically found between 9 and 10 feet below land

surface (BLS). The soil structure was found to be silty sands and sandy clays from just

beneath the surface to the boring termination.

4.0 Site Activities

Emerald, Inc. personnel conducted the Phase II ESA at the Sumter County Airport

site to determine if any prior releases had occurred at the site during the uses as described

for each area in Section 2.0 above. Field activities required to generate site-specific

3

information for the subject site are described in detail within this section.

4.1 Soil & Groundwater Assessment

On December 3 and 4 , 2009, Emerald, Inc. personnel, using Geoprobe®rd th

equipment operated by a South Carolina licensed well driller from VERCO, conducted 10

borings in Area 1 as shown on the site map in Figure 3. Continuous soil sampling was

conducted from just below the surface to a depth of approximately 9 feet BLS for each

boring labeled B-1 through B-10. Soil screening was conducted at 4 to 5 foot intervals by

field personnel who placed a portion of the soil sample into a plastic, sealable baggie for

field screening using a Photo-ionization Detector (PID) to screen for the presence of

Volatile Organic Compounds (VOCs). All data was recorded in the Field Screening Log

as found in Appendix A including sample identification as to boring number, soil

descriptions, depth and PID readings. Surficial soil samples from 0 to 5 feet were selected

for laboratory analysis at each boring location unless otherwise noted in the field log.

Each labeled soil sample was then packed into glass jar containers as provided by the

laboratory for placement into the field ice chest, and shipment to the independent

laboratory.

After collection of soil samples at each boring location, the direct push equipment

was advanced to the shallow groundwater table in order to collect a sample of the

groundwater. At a depth of approximately 14 feet BLS, a stainless steel screen was

exposed for the collection of a groundwater sample using a peristaltic pump and plastic

tubing (new tubing used at each collection point). Field personnel collected groundwater

samples and placed such in preserved glass vials and bottles as provided by the

laboratory, labeled and placed in the field ice chest for overnight shipment to the

4

independent laboratory.

This same procedure was used for the collection of soil and groundwater samples

in each of the two remaining areas as seen on the area maps labeled Figure 4 (Area 2)

and Figure 5 (Area 3). In Area 1, a water sample was collected from an abandoned water

supply well labeled “PW”.

4.2 Soil & Groundwater Analytical

The soil and groundwater samples were packed in ice and shipped via overnight

carrier to the Test America laboratory in Nashville, Tennessee, along with the properly

completed chain of custody. Each soil and groundwater sample collected from Area 1 was

tested for Pesticides as per EPA Method 8081B. Table 1 shows the analytical results for

each sample, and the actual lab sheets can be found in Appendix B. As Table 1 shows,

each pesticide soil result is compared to the EPA Region 9 Preliminary Remediation Goals

(PRGs) using the Industrial Soil standard (December 2009). All of the pesticide analytical

results may not have a comparative PRG. Table 2 shows the groundwater analytical

results for each boring as compared to the individual Maximum Contaminant Level (MCL)

for Drinking Water. Not all pesticides are listed on the MCL list and are so designated.

5

Table IArea 1 - Soil Analytical Data for Pesticides

Sumter AirportSite ID #43-04382

Sample Date: 12/03/09

Pesticide PRG B-1-S B-2-S B-3-S B-4-S B-5-S

Aldrin 0.10 ND ND ND ND ND

delta-BHC * ND ND ND ND ND

alpha-BHC * ND ND ND ND ND

beta-BHC * ND ND ND ND ND

gamma-BHC (Lindane) * ND ND ND ND ND

alpha-Chlordane * 0.0197 0.00521 ND ND ND

gamma-Chlordane * ND ND ND ND ND

Chlordane 6.50 ND ND ND ND ND

4,4'-DDD 7.20 0.125 0.00489 ND ND ND

4,4'-DDE 5.10 0.0230 0.00782 0.00466 ND 0.00819

4,4'-DDT 7.00 0.0592 0.0228 0.00499 0.00666 0.0164

Dieldrin 0.11 0.0592 0.00521 0.00300 ND ND

Endosulfan I 3700 0.0625 ND ND ND ND

Endosulfan II * 0.253 0.0147 0.00632 ND 0.00361

Endosulfan Sulfate * ND ND 0.0123 ND ND

Endrin 180 0.293 ND ND ND ND

Endrin aldehyde * 0.201 0.00489 0.0233 ND 0.00295

Endrin ketone * ND ND ND ND ND

Heptachlor 0.38 ND ND ND ND ND

Heptachlor epoxide 0.19 ND ND ND ND ND

Methoxychlor 3100 0.839 0.0153 0.0163 ND ND

Toxaphene 1.60 7.23 0.317 0.398 0.132 0.211

Notes: All units mg/kg, ND - Not Detected, * - Not on PRG List

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Table I - Cont’dArea 1 - Soil Analytical Data for Pesticides



Pesticide PRG B-6-S B-7-S B-8-S B-9-S B-10-S

Aldrin 0.10 ND ND ND ND ND

delta-BHC * ND ND ND ND ND

alpha-BHC * ND ND ND ND ND

beta-BHC * ND ND ND ND ND


alpha-Chlordane * ND 0.972 ND ND ND

gamma-Chlordane * ND 1.23 ND ND ND


4,4'-DDD 7.20 ND 5.51 ND ND ND

4,4'-DDE 5.10 0.00232 ND ND ND ND

4,4'-DDT 7.00 0.00299 ND ND ND ND

Dieldrin 0.11 ND ND ND ND ND

Endosulfan I 3700 ND ND ND ND ND

Endosulfan II * ND 9.72 ND ND ND

Endosulfan Sulfate * ND ND ND ND ND

Endrin 180 ND ND ND ND ND

Endrin aldehyde * ND 9.08 ND ND ND



Heptachlor epoxide 0.19 ND 0.713 ND ND ND

Methoxychlor 3100 ND 33.7 0.0821 0.0392 ND

Toxaphene 1.60 0.192 342 0.744 0.426 0.178


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Table 2Area 1 - Groundwater Analytical Data for Pesticides



Pesticide MCL B-1-GW B-2-GW B-3-GW B-4-GW B-5-GW

Aldrin * 5.40 ND ND ND ND

delta-BHC * 3.80 ND ND ND ND

alpha-BHC * 3.60 5.00 ND ND ND

beta-BHC * 5.80 ND ND ND ND


alpha-Chlordane * ND 6.00 ND 0.100 ND

gamma-Chlordane * ND 16.0 ND ND ND


4,4'-DDD * 5.0 ND ND ND ND

4,4'-DDE * ND ND ND ND ND

4,4'-DDT * 3.40 25.0 ND ND ND

Dieldrin * 2.60 ND ND 0.280 ND

Endosulfan I * ND 11.0 ND 0.200 ND

Endosulfan II * ND 10.0 ND 0.860 ND

Endosulfan Sulfate * ND ND ND ND ND

Endrin 2.0 ND ND ND 0.910 ND

Endrin aldehyde * ND ND ND 0.290 ND



Heptachlor epoxide 0.2 ND ND ND ND ND

Methoxychlor 40.0 2.20 ND ND ND ND

Toxaphene 3.0 142 954 181 20.0 ND

Notes: All units ug/L, ND - Not Detected, * - Not on MCL List

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Table 2 - Cont’dArea 1 - Groundwater Analytical Data for Pesticides



Pesticide MCL B-6-GW B-7-GW B-8-GW B-9-GW B-10-GW SAP-PW

Aldrin * ND ND ND ND ND ND

delta-BHC * ND ND ND ND ND ND

alpha-BHC * ND ND ND ND ND ND

beta-BHC * ND ND ND ND ND ND

gamma-BHC (Lindane) * ND ND ND ND ND ND

alpha-Chlordane * ND ND ND ND ND ND

gamma-Chlordane * ND ND ND ND ND ND

Chlordane 2.0 ND ND ND ND ND ND

4,4'-DDD * ND ND ND ND ND ND

4,4'-DDE * ND ND ND ND ND ND

4,4'-DDT * ND ND ND ND ND ND

Dieldrin * ND ND ND ND ND ND

Endosulfan I * ND ND ND ND ND ND

Endosulfan II * ND ND ND ND ND ND

Endosulfan Sulfate * ND ND ND ND ND ND

Endrin 2.0 ND ND ND ND ND ND

Endrin aldehyde * ND ND ND ND ND ND

Endrin ketone * ND ND ND ND ND ND

Heptachlor 0.4 ND ND ND ND ND ND

Heptachlor epoxide 0.2 ND ND ND ND ND ND

Methoxychlor 40.0 ND ND ND ND ND ND

Toxaphene 3.0 ND 213 4.07 16.3 9.08 ND


9

Area 2 contained soil and groundwater samples labeled B-11 through B-15. Each

soil and groundwater sample was submitted to the independent laboratory to test for

Volatile Organic Compounds (VOCs) using EPA Method 8260. VOCs may be found in

petroleum materials such as gasoline, heating oil, diesel fuel, and paint solvents. VOCs

would also indicate the presence of PCBs from white goods, etc. Table 3 shows the

analytical for each soil sample, and Table 4 shows the analytical results for each

groundwater sample from Area 2. Each soil result is also compared to the EPA Region 9

PRGs for soil, as appropriate, and the groundwater results are compared to the MCLs for

Drinking Water.

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Table 3Area 2 - Soil Analytical Data for VOCs



Contaminant PRG B-11-S B-12-S B-13-S B-14-S B-15-S

Acetone 630000 ND ND 0.0851 0.0190 ND

Benzene 5.40 ND ND ND ND ND

Bromobenzene 1800 ND ND ND ND ND

Bromochloromethane * ND ND ND ND ND

Bromodichloromethane 1.40 ND ND ND ND ND

Bromoform 220.0 ND ND ND ND ND

Bromomethane 32.0 ND ND ND ND ND

2-Butanone * ND ND ND ND ND

sec-Butylbenzene * ND ND ND ND ND

n-Butylbenzene * ND ND ND ND ND

tert-Butylbenzene * ND ND ND ND ND

Carbon disulfide 3700.0 ND ND ND ND ND

Carbon Tetrachloride 1.20 ND ND ND ND ND

Chlorobenzene 1400.0 ND ND ND ND ND

Chlorodibromomethane * ND ND ND ND ND

Chloroethane * ND ND ND ND ND

Chloroform 1.50 ND ND 0.000814 0.000748 0.000712

Chloromethane 500 ND ND ND ND ND

2-Chlorotoluene * ND ND ND ND ND


1,2 Dibromo-3-chloropropane 0.07 ND ND ND ND ND

1,2-Dibromoethane (EDB) 0.17 ND ND ND ND ND

Dibromomethane 110.0 ND ND ND ND ND

1,4-Dichlorobenzene 12.0 ND ND ND ND ND

1,3-Dichlorobenzene * ND ND ND ND ND


Dichlorodifluoromethane 780 ND ND ND ND ND

1,1-Dichloroethane 17.0 ND ND ND ND ND


cis-1,2-Dichloroethene * ND ND ND ND ND

1,1-Dichloroethene * ND ND ND ND ND

trans-1,2-Dichloroethene * ND ND ND ND ND


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Table 3 - Cont’dArea 2 - Soil Analytical Data for VOCs




1,3-Dichloropropane 20000 ND ND ND ND ND

1,2-Dichloropropane 4.50 ND ND ND ND ND

2,2-Dichloropropane * ND ND ND ND ND

cis-1,3-Dichloropropene * ND ND ND ND ND

trans-1,3-Dichloropropene * ND ND ND ND ND

1,1-Dichloropropene * ND ND ND ND ND

Ethlybenzene 27.0 ND ND ND ND ND

Hexachlorobutadiene 22.0 ND ND ND ND ND

2-Hexanone 1400.0 ND ND ND ND ND

Isopropylbenzene * ND ND ND ND ND

p-Isopropyltoluene * ND ND ND ND ND

Methyl tert-Butyl Ether 220.0 ND ND ND ND ND

Methylene Chloride 53.0 ND ND ND ND ND

4-Methyl-2-pentanone * ND ND ND ND ND

Naphthalene * ND ND ND ND ND

n-Propylbenzene * ND ND ND ND ND

Styrene 36000 ND ND ND ND ND

1,1,1,2-Tetrachloroethane 9.3 ND ND ND ND ND

1,1,2,2-Tetrachlorethane 2.8 ND ND ND ND ND

Tetrachloroethene * ND ND ND ND ND

Toluene 45000 ND ND ND 0.000204 ND

1,2,3-Trichlorobenzene 490.0 ND ND ND ND ND


1,1,2-Trichloroethane 5.30 ND ND ND ND ND

1,1,1-Trichloroethane 38000 ND ND ND ND ND

Trichloroethene * ND ND ND ND ND

Trichlorofluormethane 3400 ND ND ND ND ND

1,2,3-Trichloropropane 0.10 ND ND ND ND ND

1,3,5-Trimethylbenzene 10000 ND ND ND ND ND

1,2,4-Trimethylbenzene 260.0 ND ND ND ND ND

Vinyl Chloride 1.7 ND ND ND ND ND

Xylenes, total * ND ND ND ND ND


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Table 4Area 2 - Groundwater Analytical Data for VOCs



Contaminant MCL B-11-GW B-12-GW B-13-GW B-14-GW B-15-GW

Acetone * ND ND ND ND ND

Benzene 5.0 3.97 ND ND ND ND

Bromobenzene * ND ND ND ND ND


Bromodichloromethane * ND ND ND ND ND

Bromoform * ND ND ND ND ND

Bromomethane * ND ND ND ND ND


sec-Butylbenzene * ND 0.380 ND ND ND

n-Butylbenzene * ND 0.880 ND ND ND


Carbon disulfide * ND ND ND ND ND


Chlorobenzene 100.0 1.01 0.530 ND ND ND



Chloroform * ND ND ND ND ND

Chloromethane * ND 0.880 ND ND ND




1,2-Dibromoethane(EDB) * 1.77 ND ND ND ND

Dibromomethane * ND ND ND ND ND


1,3-Dichlorobenzene * 0.810 ND ND ND ND


Dichlorodifluoromethane * ND ND ND ND ND

1,1-Dichloroethane * ND ND ND ND ND






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Table 4 - Cont’dArea 2 - Groundwater Analytical Data for VOCs










Ethlybenzene 700.0 ND 5.19 0.550 ND ND

Hexachlorobutadiene * ND ND ND ND ND

2-Hexanone * ND ND ND ND ND

Isopropylbenzene * 1.02 1.30 ND ND ND


Methyl tert-Butyl Ether * 1.74 ND ND ND ND

Methylene Chloride * ND ND ND ND ND


Naphthalene * ND ND ND ND ND

n-Propylbenzene * ND 5.89 0.430 ND ND

Styrene 100.0 ND ND ND ND ND

1,1,1,2-Tetrachloroethane * ND ND ND ND ND

1,1,2,2-Tetrachlorethane * ND ND ND ND ND

Tetrachloroethene * ND 0.340 ND ND ND

Toluene 1000.0 ND 0.600 ND ND ND

1,2,3-Trichlorobenzene * ND ND ND ND ND





Trichlorofluormethane * ND ND ND ND ND

1,2,3-Trichloropropane * ND ND ND ND ND

1,3,5-Trimethylbenzene * 10.9 11.4 1.09 ND ND

1,2,4-Trimethylbenzene * 15.6 36.4 2.75 0.350 0.490


Xylenes, total 10000 18.6 31.8 3.28 ND ND


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Area 3 contained soil and groundwater samples labeled B-16 through B-20.

Each soil sample was submitted to the independent laboratory to test for Total

Petroleum Hydrocarbons - Diesel Range Organics (TPH-DRO) using EPA Method

8015 and VOCs, as would possibly be found in waste oils, and also would provide

an indicator of the presence of creosote. Table 5 contains the analytical results for

each soil sample. Each groundwater sample collected in Area 3 was submitted for

VOC analysis only. Table 6 contains the analytical results for each groundwater

sample. Each soil result is also compared to the EPA Region 9 PRGs for soil, as

appropriate, and the groundwater results are compared to the MCLs for Drinking

Water.

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Table 5Area 3 - Soil Analytical Data for VOCs & TPH-DRO




Acetone 630000 0.434 0.0179 0.113 0.135 0.0195


Bromobenzene 1800 ND ND ND ND ND


Bromodichloromethane 1.40 ND ND ND ND ND

Bromoform 220.0 ND ND ND ND ND

Bromomethane 32.0 ND ND ND ND ND





Carbon disulfide 3700.0 ND ND ND ND ND





Chloroform 1.50 0.00103 0.000664 0.00162 0.00106 0.00202

Chloromethane 500 ND ND ND ND ND




1,2-Dibromoethane (EDB) 0.17 ND ND ND ND ND

Dibromomethane 110.0 ND ND ND ND ND




Dichlorodifluoromethane 780 ND ND ND ND ND







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Table 5 - Cont’dArea 3 - Soil Analytical Data for VOCs & TPH-DRO




1,3-Dichloropropane 20000 ND ND ND ND ND







Hexachlorobutadiene 22.0 ND ND ND ND ND

2-Hexanone 1400.0 ND ND ND ND ND

Isopropylbenzene * ND ND 0.00355 ND ND

p-Isopropyltoluene * ND ND 0.00366 ND ND

Methyl tert-Butyl Ether 220.0 ND ND ND ND ND

Methylene Chloride 53.0 ND ND ND ND ND

4-Methyl-2-pentanone * 0.0191 ND ND ND ND

Naphthalene * ND ND 0.00461 ND ND


Styrene 36000 ND ND ND ND ND

1,1,1,2-Tetrachloroethane 9.3 ND ND ND ND ND

1,1,2,2-Tetrachlorethane 2.8 ND ND ND ND ND

Tetrachloroethene * ND ND ND ND ND

Toluene 45000 0.00170 ND 0.000649 ND 0.000392




1,1,1-Trichloroethane 38000 ND ND ND ND ND


Trichlorofluormethane 3400 ND ND ND ND ND

1,2,3-Trichloropropane 0.10 ND ND ND ND ND

1,3,5-Trimethylbenzene 10000 ND ND ND ND ND

1,2,4-Trimethylbenzene 260.0 ND ND ND ND ND


Xylenes, total * ND ND ND ND ND

Diesel (TPH-DRO) * 4.08 9.01 54.0 15.8 3.90

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Table 6Area 3 - Groundwater Analytical Data for VOCs & TPH-DRO




Acetone * ND ND ND ND ND


Bromobenzene * ND ND ND ND ND


Bromodichloromethane * ND ND ND ND ND

Bromoform * ND ND ND ND ND

Bromomethane * ND ND ND ND ND





Carbon disulfide * ND ND ND ND ND





Chloroform * ND ND ND ND ND

Chloromethane * 0.420 0.440 ND ND ND




1,2-Dibromoethane(EDB) * ND ND ND ND ND

Dibromomethane * ND ND ND ND ND




Dichlorodifluoromethane * ND ND ND ND ND

1,1-Dichloroethane * ND ND ND ND ND






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Table 6 - Cont’dArea 3 - Groundwater Analytical Data for VOCs & TPH-DRO











Hexachlorobutadiene * ND ND ND ND ND

2-Hexanone * ND ND ND ND ND

Isopropylbenzene * ND ND ND ND ND


Methyl tert-Butyl Ether * ND ND ND ND ND

Methylene Chloride * ND ND ND ND ND


Naphthalene * 5.17 ND ND ND ND


Styrene 100.0 ND ND ND ND ND

1,1,1,2-Tetrachloroethane * ND ND ND ND ND

1,1,2,2-Tetrachlorethane * ND ND ND ND ND

Tetrachloroethene * ND 0.660 0.380 ND ND

Toluene 1000.0 ND ND ND ND ND

1,2,3-Trichlorobenzene * ND ND ND ND ND





Trichlorofluormethane * ND ND ND ND ND

1,2,3-Trichloropropane * ND ND ND ND ND

1,3,5-Trimethylbenzene * ND ND ND ND ND

1,2,4-Trimethylbenzene * ND ND ND ND ND


Xylenes, total 10000 ND ND ND ND ND

Diesel (TPH-DRO) NT NT NT NT NT NT

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Notes: All units ug/L, ND - Not Detected, * - Not on MCL List, NT - Not Tested

5.0 Results & Conclusions

At the request of Sumter County, Emerald, Inc. conducted a Phase II ESA on a

limited portion of the Sumter Airport property located at 2945 Airport Road in Sumter, South

Carolina. The assessment was limited to the three areas of concern as found in Phase I

ESAs conducted on the site. Specifically, such areas are labeled Areas 1 through 3 as

seen on the site map in Figure 1. Each area was associated with past usages as described

in this report.

The Phase II ESA was conducted in December 2009, and the analytical results

found that each area has been impacted by CoCs in either the soil and groundwater, or

both. In Area 1, the analytical results found Toxaphene, a pesticide, at a level 4.5 times the

acceptable limit in soil, and 318 times the MCL for Toxaphene in drinking water.

Toxaphene is listed as possibly causing kidney, liver and thyroid problems as well as an

increased risk for cancer. Area 2 results found low levels of petroleum and paint solvents

in both the soil and groundwater, none of which are above acceptable limits for such CoCs.

Area 3 found levels of TPH-DRO in the soil. TPH-DRO is an indicator of the possible

presence of waste oils and creosote, both used by railroad companies in the past.

The results of the Phase II ESA have found the presence of CoCs in each area;

however, the extent of the CoCs have not been determined in this initial assessment.

Additional assessment should be conducted to determine the horizontal and vertical extent

of the CoCs, the possible impact to nearby wetlands, and the risk to human health and the

environment that each area poses with regards to occupancy and development.

20

6.0 Appendices

A) Field Screening Logs & Water Well Records

B) Laboratory Analytical Results

C) SCDHEC Temporary Monitoring Well Approval

21

2960 Foster Creighton Road Nashville, TN 37204 * 800-765-0980 * Fax 615-726-3404

December 17, 2009

Client:

Attn:

Work Order:

Project Name:

Project Nbr:

Date Received:

Emerald, Inc.

SAP-1

NSL0939

12/08/09

Sumter, SC 29151

Emerald, Inc. (8583)P. O. Box 3050

Robbin Brown P/O Nbr:

3:33:54PM

SAMPLE IDENTIFICATION LAB NUMBER COLLECTION DATE AND TIME

NSL0939-01B-1-S 12/03/09 15:44

NSL0939-02B-1-GW 12/03/09 15:55

NSL0939-03B-2-S 12/03/09 14:03

NSL0939-04B-2-GW 12/03/09 14:10

NSL0939-05B-3-S 12/03/09 13:40

NSL0939-06B-3-GW 12/03/09 14:00

NSL0939-07B-4-S 12/03/09 11:11

NSL0939-08B-4-GW 12/03/09 11:30

NSL0939-09B-5-S 12/03/09 10:45

NSL0939-10B-5-GW 12/03/09 11:00

NSL0939-11B-6-S 12/03/09 10:14

NSL0939-12B-6-GW 12/03/09 10:30

NSL0939-13B-7-S 12/03/09 16:05

NSL0939-14B-7-GW 12/03/09 16:15

NSL0939-15B-8-S 12/03/09 14:50

NSL0939-16B-8-GW 12/03/09 15:00

NSL0939-17B-9-S 12/03/09 14:27

NSL0939-18B-9-GW 12/03/09 14:40

NSL0939-19B-10-S 12/03/09 15:18

NSL0939-20B-10-GW 12/03/09 15:25

NSL0939-21SAP-PW 12/03/09 16:40

An executed copy of the chain of custody, the project quality control data, and the sample receipt form are also included as an addendum

to this report. If you have any questions relating to this analytical report, please contact your Laboratory Project Manager at

1-800-765-0980. Any opinions, if expressed, are outside the scope of the Laboratory's accreditation.

This material is intended only for the use of the individual(s) or entity to whom it is addressed, and may contain information that is

privileged and confidential. If you are not the intended recipient, or the employee or agent responsible for delivering this material to the

intended recipient, you are hereby notified that any dissemination, distribution, or copying of this material is strictly prohibited. If you

have received this material in error, please notify us immediately at 615-726-0177.

South Carolina Certification Number: 84009001

These results relate only to the items tested. This report shall not be reproduced except in full and with permission of the laboratory.

Report Approved By:

The Chain(s) of Custody, 5 pages, are included and are an integral part of this report.

Estimated uncertainty is available upon request.This report has been electronically signed.

All solids results are reported in wet weight unless specifically stated.

Page 1 of 24


Client

Attn

Emerald, Inc. (8583)

P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:

Project Number: SAP-1

12/08/09 08:00

NSL0939

Cathy Gartner

Project Management

Page 2 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

ANALYTICAL REPORT

Analyte FlagResult Units

Dilution

FactorMRL Method Analyst Batch

Analysis

Date/Time

Sample ID: NSL0939-01 (B-1-S - Soil) Sampled: 12/03/09 15:44

Organochlorine Pesticides by EPA Method 8081A

Aldrin 91217330.0168ND 12/15/09 20:0510mg/kg SW846 8081A jlf

delta-BHC 91217330.0168ND 12/15/09 20:0510mg/kg SW846 8081A jlf

alpha-BHC 91217330.0168ND 12/15/09 20:0510mg/kg SW846 8081A jlf

beta-BHC 91217330.0326ND 12/15/09 20:0510mg/kg SW846 8081A jlf

gamma-BHC (Lindane) 91217330.0168ND 12/15/09 20:0510mg/kg SW846 8081A jlf

alpha-Chlordane 91217330.01680.0197 12/15/09 20:0510mg/kg SW846 8081A jlf

gamma-Chlordane 91217330.0168ND 12/15/09 20:0510mg/kg SW846 8081A jlf

Chlordane 91217330.658ND 12/15/09 20:0510mg/kg SW846 8081A jlf

4,4'-DDD 91217330.01680.125 12/15/09 20:0510mg/kg SW846 8081A jlf

4,4'-DDE 91217330.01680.0230 12/15/09 20:0510mg/kg SW846 8081A jlf

4,4'-DDT 91217330.01680.0592 12/15/09 20:0510mg/kg SW846 8081A jlf

Dieldrin 91217330.01680.0592 12/15/09 20:0510mg/kg SW846 8081A jlf

Endosulfan I 91217330.01680.0625 12/15/09 20:0510mg/kg SW846 8081A jlf

Endosulfan II 91217330.01680.253 12/15/09 20:0510mg/kg SW846 8081A jlf

Endosulfan sulfate 91217330.0168ND 12/15/09 20:0510mg/kg SW846 8081A jlf

Endrin 91217330.01680.293 12/15/09 20:0510mg/kg SW846 8081A jlf

Endrin aldehyde 91217330.01680.201 12/15/09 20:0510mg/kg SW846 8081A jlf

Endrin ketone 91217330.0168ND 12/15/09 20:0510mg/kg SW846 8081A jlf

Heptachlor 91217330.0168ND 12/15/09 20:0510mg/kg SW846 8081A jlf

Heptachlor epoxide 91217330.0168ND 12/15/09 20:0510mg/kg SW846 8081A jlf

Methoxychlor 91217330.1630.839 12/16/09 14:4550mg/kg SW846 8081A jlf

Toxaphene 91217330.6587.23 12/15/09 13:3710mg/kg SW846 8081A jlf

Surr: Tetrachloro-meta-xylene (22-150%) 40 % 12/15/09 20:05 SW846 8081A jlf 9121733

Surr: Decachlorobiphenyl (25-150%) 140 % 12/15/09 20:05 SW846 8081A jlf 9121733

Sample ID: NSL0939-02 (B-1-GW - Ground Water) Sampled: 12/03/09 15:55


Aldrin R10 91217391.005.40 12/14/09 15:5920ug/L SW846 8081A jlf

delta-BHC R10 91217391.003.80 12/14/09 15:5920ug/L SW846 8081A jlf

alpha-BHC R10 91217391.003.60 12/14/09 15:5920ug/L SW846 8081A jlf

beta-BHC 91217391.005.80 12/14/09 15:5920ug/L SW846 8081A jlf

gamma-BHC (Lindane) 91217391.00ND 12/14/09 15:5920ug/L SW846 8081A jlf

alpha-Chlordane 91217391.00ND 12/14/09 15:5920ug/L SW846 8081A jlf

gamma-Chlordane 91217391.00ND 12/14/09 15:5920ug/L SW846 8081A jlf

Chlordane 912173960.0ND 12/14/09 15:5920ug/L SW846 8081A jlf

4,4'-DDD 91217391.005.00 12/14/09 15:5920ug/L SW846 8081A jlf

4,4'-DDE 91217391.00ND 12/14/09 15:5920ug/L SW846 8081A jlf

4,4'-DDT 91217391.003.40 12/14/09 15:5920ug/L SW846 8081A jlf

Dieldrin 91217391.002.60 12/14/09 15:5920ug/L SW846 8081A jlf

Endosulfan I 91217391.00ND 12/14/09 15:5920ug/L SW846 8081A jlf

Endosulfan II 91217391.00ND 12/14/09 15:5920ug/L SW846 8081A jlf

Endosulfan sulfate 91217391.00ND 12/14/09 15:5920ug/L SW846 8081A jlf

Endrin 91217391.00ND 12/14/09 15:5920ug/L SW846 8081A jlf

Endrin aldehyde 91217391.00ND 12/14/09 15:5920ug/L SW846 8081A jlf

Endrin ketone 91217391.00ND 12/14/09 15:5920ug/L SW846 8081A jlf

Heptachlor 91217391.00ND 12/14/09 15:5920ug/L SW846 8081A jlf

Heptachlor epoxide 91217391.00ND 12/14/09 15:5920ug/L SW846 8081A jlf

Page 3 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

ANALYTICAL REPORT


Dilution


Analysis

Date/Time

Sample ID: NSL0939-02 (B-1-GW - Ground Water) - cont. Sampled: 12/03/09 15:55

Organochlorine Pesticides by EPA Method 8081A - cont.

Methoxychlor R10 91217391.002.20 12/14/09 15:5920ug/L SW846 8081A jlf

Toxaphene 912173940.0142 12/15/09 12:3320ug/L SW846 8081A jlf

Surr: Tetrachloro-meta-xylene (38-150%) 1780 % ZX 12/14/09 15:59 SW846 8081A jlf 9121739












4,4'-DDD 91217330.001660.00489 12/14/09 23:551mg/kg SW846 8081A jlf

4,4'-DDE 91217330.001660.00782 12/14/09 23:551mg/kg SW846 8081A jlf

4,4'-DDT R10 91217330.001660.0228 12/14/09 23:551mg/kg SW846 8081A jlf


Endosulfan I 91217330.00166ND 12/14/09 23:551mg/kg SW846 8081A jlf



Endrin 91217330.00166ND 12/14/09 23:551mg/kg SW846 8081A jlf

Endrin aldehyde R10 91217330.001660.00489 12/14/09 23:551mg/kg SW846 8081A jlf








Page 4 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

ANALYTICAL REPORT


Dilution


Analysis

Date/Time



Aldrin 91217395.00ND 12/14/09 14:56100ug/L SW846 8081A jlf

delta-BHC 91217395.00ND 12/14/09 14:56100ug/L SW846 8081A jlf

alpha-BHC 91217395.005.00 12/14/09 14:56100ug/L SW846 8081A jlf

beta-BHC 91217395.00ND 12/14/09 14:56100ug/L SW846 8081A jlf


alpha-Chlordane 91217395.006.00 12/14/09 14:56100ug/L SW846 8081A jlf

gamma-Chlordane 91217395.0016.0 12/14/09 14:56100ug/L SW846 8081A jlf

Chlordane 9121739300ND 12/14/09 14:56100ug/L SW846 8081A jlf

4,4'-DDD 91217395.00ND 12/14/09 14:56100ug/L SW846 8081A jlf

4,4'-DDE 91217395.00ND 12/14/09 14:56100ug/L SW846 8081A jlf

4,4'-DDT R1 91217395.0025.0 12/14/09 14:56100ug/L SW846 8081A jlf

Dieldrin 91217395.00ND 12/14/09 14:56100ug/L SW846 8081A jlf

Endosulfan I 91217395.0011.0 12/14/09 14:56100ug/L SW846 8081A jlf

Endosulfan II 91217395.0010.0 12/14/09 14:56100ug/L SW846 8081A jlf







Methoxychlor 91217395.00ND 12/14/09 14:56100ug/L SW846 8081A jlf

Toxaphene 9121739200954 12/15/09 12:49100ug/L SW846 8081A jlf


Surr: Decachlorobiphenyl (10-141%) * ZX 12/14/09 14:56 SW846 8081A jlf 9121739








alpha-Chlordane 91217330.00170ND 12/15/09 00:071mg/kg SW846 8081A jlf



4,4'-DDD 91217330.00170ND 12/15/09 00:071mg/kg SW846 8081A jlf

4,4'-DDE 91217330.001700.00466 12/15/09 00:071mg/kg SW846 8081A jlf

4,4'-DDT R10 91217330.001700.00499 12/15/09 00:071mg/kg SW846 8081A jlf




Endosulfan sulfate 91217330.001700.0123 12/15/09 00:071mg/kg SW846 8081A jlf


Endrin aldehyde R10 91217330.001700.0233 12/15/09 00:071mg/kg SW846 8081A jlf




Page 5 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

ANALYTICAL REPORT


Dilution


Analysis

Date/Time

Sample ID: NSL0939-05 (B-3-S - Soil) - cont. Sampled: 12/03/09 13:40








Aldrin RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

delta-BHC RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

alpha-BHC RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

beta-BHC RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

gamma-BHC (Lindane) RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

alpha-Chlordane RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

gamma-Chlordane RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

Chlordane RL1 9121739150ND 12/14/09 15:0950ug/L SW846 8081A jlf

4,4'-DDD RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

4,4'-DDE RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

4,4'-DDT RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

Dieldrin RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

Endosulfan I RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

Endosulfan II RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

Endosulfan sulfate RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

Endrin RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

Endrin aldehyde RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

Endrin ketone RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

Heptachlor RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

Heptachlor epoxide RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf

Methoxychlor RL1 91217392.50ND 12/14/09 15:0950ug/L SW846 8081A jlf


Surr: Tetrachloro-meta-xylene (38-150%) * Z3 12/14/09 15:09 SW846 8081A jlf 9121739

Surr: Decachlorobiphenyl (10-141%) * Z3 12/14/09 15:09 SW846 8081A jlf 9121739

Page 6 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

ANALYTICAL REPORT


Dilution


Analysis

Date/Time












4,4'-DDE 91217330.00170ND 12/15/09 00:201mg/kg SW846 8081A jlf

4,4'-DDT 91217330.001700.00666 12/15/09 00:201mg/kg SW846 8081A jlf

Dieldrin 91217330.00170ND 12/15/09 00:201mg/kg SW846 8081A jlf


Endosulfan II 91217330.00170ND 12/15/09 00:201mg/kg SW846 8081A jlf



Endrin aldehyde 91217330.00170ND 12/15/09 00:201mg/kg SW846 8081A jlf




Methoxychlor 91217330.00330ND 12/15/09 00:201mg/kg SW846 8081A jlf








alpha-BHC 91217390.0500ND 12/14/09 13:531ug/L SW846 8081A jlf



alpha-Chlordane 91217390.05000.100 12/14/09 13:531ug/L SW846 8081A jlf



4,4'-DDD 91217390.0500ND 12/14/09 13:531ug/L SW846 8081A jlf

4,4'-DDE 91217390.0500ND 12/14/09 13:531ug/L SW846 8081A jlf

4,4'-DDT 91217390.0500ND 12/14/09 13:531ug/L SW846 8081A jlf

Dieldrin 91217390.05000.280 12/14/09 13:531ug/L SW846 8081A jlf

Endosulfan I 91217390.05000.200 12/14/09 13:531ug/L SW846 8081A jlf

Endosulfan II 91217390.05000.860 12/14/09 13:531ug/L SW846 8081A jlf


Endrin 91217390.05000.910 12/14/09 13:531ug/L SW846 8081A jlf

Endrin aldehyde 91217390.05000.290 12/14/09 13:531ug/L SW846 8081A jlf




Page 7 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

ANALYTICAL REPORT


Dilution


Analysis

Date/Time




Toxaphene 91217392.0020.0 12/14/09 21:471ug/L SW846 8081A jlf














4,4'-DDE 91217330.001670.00819 12/15/09 00:321mg/kg SW846 8081A jlf

4,4'-DDT R10 91217330.001670.0164 12/15/09 00:321mg/kg SW846 8081A jlf














Page 8 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

ANALYTICAL REPORT


Dilution


Analysis

Date/Time











4,4'-DDD 91217390.0500ND 12/14/09 14:181ug/L SW846 8081A jlf

4,4'-DDE 91217390.0500ND 12/14/09 14:181ug/L SW846 8081A jlf

4,4'-DDT 91217390.0500ND 12/14/09 14:181ug/L SW846 8081A jlf











Toxaphene 91217392.00ND 12/14/09 14:181ug/L SW846 8081A jlf














4,4'-DDE R10 91217330.001690.00232 12/15/09 00:451mg/kg SW846 8081A jlf

4,4'-DDT R10 91217330.001690.00299 12/15/09 00:451mg/kg SW846 8081A jlf










Page 9 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

ANALYTICAL REPORT


Dilution


Analysis

Date/Time

















4,4'-DDD 91217390.0500ND 12/12/09 16:401ug/L SW846 8081A jlf

4,4'-DDE 91217390.0500ND 12/12/09 16:401ug/L SW846 8081A jlf

4,4'-DDT 91217390.0500ND 12/12/09 16:401ug/L SW846 8081A jlf














Page 10 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

ANALYTICAL REPORT


Dilution


Analysis

Date/Time









gamma-Chlordane 91217330.1651.23 12/15/09 20:18100mg/kg SW846 8081A jlf


4,4'-DDD 91217331.655.51 12/16/09 11:331000mg/kg SW846 8081A jlf


4,4'-DDT 91217331.65ND 12/16/09 11:331000mg/kg SW846 8081A jlf









Heptachlor epoxide 91217330.1650.713 12/15/09 20:18100mg/kg SW846 8081A jlf


Toxaphene 912173332.4342 12/17/09 12:18500mg/kg SW846 8081A jlf












Chlordane RL1 9121739150ND 12/14/09 15:2150ug/L SW846 8081A jlf













Page 11 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

ANALYTICAL REPORT


Dilution


Analysis

Date/Time

































Page 12 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

ANALYTICAL REPORT


Dilution


Analysis

Date/Time











4,4'-DDD 91217390.0500ND 12/14/09 14:061ug/L SW846 8081A jlf

4,4'-DDE 91217390.0500ND 12/14/09 14:061ug/L SW846 8081A jlf

4,4'-DDT 91217390.0500ND 12/14/09 14:061ug/L SW846 8081A jlf




































Page 13 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

ANALYTICAL REPORT


Dilution


Analysis

Date/Time
















Chlordane RL1 912173930.0ND 12/14/09 15:3410ug/L SW846 8081A jlf

















Page 14 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

ANALYTICAL REPORT


Dilution


Analysis

Date/Time




































Chlordane RL1 912173915.0ND 12/14/09 15:465ug/L SW846 8081A jlf













Page 15 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

ANALYTICAL REPORT


Dilution


Analysis

Date/Time







Sample ID: NSL0939-21 (SAP-PW - Ground Water) Sampled: 12/03/09 16:40










4,4'-DDD 91217390.0500ND 12/12/09 17:431ug/L SW846 8081A jlf

4,4'-DDE 91217390.0500ND 12/12/09 17:431ug/L SW846 8081A jlf

4,4'-DDT 91217390.0500ND 12/12/09 17:431ug/L SW846 8081A jlf














Page 16 of 24


Client

Attn


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Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

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Received:


12/08/09 08:00

NSL0939

SAMPLE EXTRACTION DATA

Parameter

Wt/Vol

Extracted Extracted Vol Date Analyst

Extraction

MethodLab NumberBatch

Organochlorine Pesticides by EPA Method 8081A 30.41 EPA 3550BAJF12/11/09 15:209121733SW846 8081A NSL0939-01 10.00

30.41 EPA 3550BAJF12/11/09 15:209121733SW846 8081A NSL0939-01RE1 10.00




500.00 EPA 3510CJJR12/10/09 11:249121739SW846 8081A NSL0939-02 5.00

500.00 EPA 3510CJJR12/10/09 11:249121739SW846 8081A NSL0939-02RE1 5.00




30.69 EPA 3550BAJF12/11/09 15:209121733SW846 8081A NSL0939-03 10.00



500.00 EPA 3510CJJR12/10/09 11:249121739SW846 8081A NSL0939-04 5.00





30.04 EPA 3550BAJF12/11/09 15:209121733SW846 8081A NSL0939-05 10.00


500.00 EPA 3510CJJR12/10/09 11:249121739SW846 8081A NSL0939-06 5.00




30.04 EPA 3550BAJF12/11/09 15:209121733SW846 8081A NSL0939-07 10.00


500.00 EPA 3510CJJR12/10/09 11:249121739SW846 8081A NSL0939-08 5.00



30.51 EPA 3550BAJF12/11/09 15:209121733SW846 8081A NSL0939-09 10.00


500.00 EPA 3510CJJR12/10/09 11:249121739SW846 8081A NSL0939-10 5.00


30.15 EPA 3550BAJF12/11/09 15:209121733SW846 8081A NSL0939-11 10.00


500.00 EPA 3510CJJR12/10/09 11:249121739SW846 8081A NSL0939-12 5.00

30.85 EPA 3550BAJF12/11/09 15:209121733SW846 8081A NSL0939-13 10.00






500.00 EPA 3510CJJR12/10/09 11:249121739SW846 8081A NSL0939-14 5.00


Page 17 of 24


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Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

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Received:


12/08/09 08:00

NSL0939


Parameter

Wt/Vol


Extraction




30.46 EPA 3550BAJF12/11/09 15:209121733SW846 8081A NSL0939-15 10.00




500.00 EPA 3510CJJR12/10/09 11:249121739SW846 8081A NSL0939-16 5.00



30.61 EPA 3550BAJF12/11/09 15:209121733SW846 8081A NSL0939-17 10.00




500.00 EPA 3510CJJR12/10/09 11:249121739SW846 8081A NSL0939-18 5.00




30.18 EPA 3550BAJF12/11/09 15:209121733SW846 8081A NSL0939-19 10.00



500.00 EPA 3510CJJR12/10/09 11:249121739SW846 8081A NSL0939-20 5.00




500.00 EPA 3510CJJR12/10/09 11:249121739SW846 8081A NSL0939-21 5.00

Page 18 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

PROJECT QUALITY CONTROL DATABlank

Blank Value Units Q.C. BatchAnalyte Lab NumberQ Analyzed Date/Time


9121733-BLK1mg/kg 9121733<0.000500 9121733-BLK1 12/14/09 22:40Aldrin

mg/kg 9121733<0.000400 9121733-BLK1 12/14/09 22:40delta-BHC

mg/kg 9121733<0.000400 9121733-BLK1 12/14/09 22:40alpha-BHC

mg/kg 9121733<0.00110 9121733-BLK1 12/14/09 22:40beta-BHC

mg/kg 9121733<0.000400 9121733-BLK1 12/14/09 22:40gamma-BHC (Lindane)

mg/kg 9121733<0.000400 9121733-BLK1 12/14/09 22:40alpha-Chlordane

mg/kg 9121733<0.000400 9121733-BLK1 12/14/09 22:40gamma-Chlordane

mg/kg 9121733<0.0167 9121733-BLK1 12/14/09 22:40Chlordane

mg/kg 9121733<0.000600 9121733-BLK1 12/14/09 22:404,4'-DDD

mg/kg 9121733<0.000400 9121733-BLK1 12/14/09 22:404,4'-DDE

mg/kg 9121733<0.000400 9121733-BLK1 12/14/09 22:404,4'-DDT

mg/kg 9121733<0.000400 9121733-BLK1 12/14/09 22:40Dieldrin

mg/kg 9121733<0.000400 9121733-BLK1 12/14/09 22:40Endosulfan I

mg/kg 9121733<0.000500 9121733-BLK1 12/14/09 22:40Endosulfan II

mg/kg 9121733<0.000400 9121733-BLK1 12/14/09 22:40Endosulfan sulfate

mg/kg 9121733<0.000500 9121733-BLK1 12/14/09 22:40Endrin

mg/kg 9121733<0.000800 9121733-BLK1 12/14/09 22:40Endrin aldehyde

mg/kg 9121733<0.000700 9121733-BLK1 12/14/09 22:40Endrin ketone

mg/kg 9121733<0.000500 9121733-BLK1 12/14/09 22:40Heptachlor

mg/kg 9121733<0.000500 9121733-BLK1 12/14/09 22:40Heptachlor epoxide

mg/kg 9121733<0.000600 9121733-BLK1 12/14/09 22:40Methoxychlor

mg/kg 9121733<0.0167 9121733-BLK1 12/14/09 22:40Toxaphene

9121733 9121733-BLK1 12/14/09 22:4094%Surrogate: Tetrachloro-meta-xylene

9121733 9121733-BLK1 12/14/09 22:40102%Surrogate: Decachlorobiphenyl

9121739-BLK1ug/L 9121739<0.0100 9121739-BLK1 12/12/09 13:57Aldrin

ug/L 9121739<0.00900 9121739-BLK1 12/12/09 13:57delta-BHC

ug/L 9121739<0.0130 9121739-BLK1 12/12/09 13:57alpha-BHC

ug/L 9121739<0.0220 9121739-BLK1 12/12/09 13:57beta-BHC

ug/L 9121739<0.0320 9121739-BLK1 12/12/09 13:57gamma-BHC (Lindane)

ug/L 9121739<0.0130 9121739-BLK1 12/12/09 13:57alpha-Chlordane

ug/L 9121739<0.0270 9121739-BLK1 12/12/09 13:57gamma-Chlordane

ug/L 9121739<0.300 9121739-BLK1 12/12/09 13:57Chlordane

ug/L 9121739<0.0160 9121739-BLK1 12/12/09 13:574,4'-DDD

ug/L 9121739<0.00900 9121739-BLK1 12/12/09 13:574,4'-DDE

ug/L 9121739<0.0110 9121739-BLK1 12/12/09 13:574,4'-DDT

ug/L 9121739<0.0250 9121739-BLK1 12/12/09 13:57Dieldrin

ug/L 9121739<0.0100 9121739-BLK1 12/12/09 13:57Endosulfan I

ug/L 9121739<0.0140 9121739-BLK1 12/12/09 13:57Endosulfan II

ug/L 9121739<0.0150 9121739-BLK1 12/12/09 13:57Endosulfan sulfate

Page 19 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

PROJECT QUALITY CONTROL DATABlank - Cont.



9121739-BLK1ug/L 9121739<0.0210 9121739-BLK1 12/12/09 13:57Endrin

ug/L 9121739<0.0160 9121739-BLK1 12/12/09 13:57Endrin aldehyde

ug/L 9121739<0.0120 9121739-BLK1 12/12/09 13:57Endrin ketone

ug/L 9121739<0.0120 9121739-BLK1 12/12/09 13:57Heptachlor

ug/L 9121739<0.0230 9121739-BLK1 12/12/09 13:57Heptachlor epoxide

ug/L 9121739<0.0210 9121739-BLK1 12/12/09 13:57Methoxychlor

ug/L 9121739<0.500 9121739-BLK1 12/12/09 13:57Toxaphene

9121739 9121739-BLK1 12/12/09 13:5779%Surrogate: Tetrachloro-meta-xylene

9121739 9121739-BLK1 12/12/09 13:5781%Surrogate: Decachlorobiphenyl

Page 20 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

PROJECT QUALITY CONTROL DATA

LCS

Analyte UnitsKnown Val. Analyzed Val % Rec. BatchQ

Target

Range

Analyzed

Date/Time


9121733-BS143 - 150 91217330.0167 0.0133 80% mg/kg 12/14/09 22:52Aldrin

34 - 147 91217330.0167 0.0130 78% mg/kg 12/14/09 22:52delta-BHC

47 - 142 91217330.0167 0.0120 72% mg/kg 12/14/09 22:52alpha-BHC

52 - 148 91217330.0167 0.0133 80% mg/kg 12/14/09 22:52beta-BHC

53 - 142 91217330.0167 0.0130 78% mg/kg 12/14/09 22:52gamma-BHC (Lindane)

50 - 148 91217330.0167 0.0133 80% mg/kg 12/14/09 22:52alpha-Chlordane

46 - 150 91217330.0167 0.0133 80% mg/kg 12/14/09 22:52gamma-Chlordane

47 - 150 91217330.0167 0.0147 88% mg/kg 12/14/09 22:524,4'-DDD

42 - 150 91217330.0167 0.0133 80% mg/kg 12/14/09 22:524,4'-DDE

38 - 150 91217330.0167 0.0123 74% mg/kg 12/14/09 22:524,4'-DDT

53 - 142 91217330.0167 0.0130 78% mg/kg 12/14/09 22:52Dieldrin

50 - 143 91217330.0167 0.0123 74% mg/kg 12/14/09 22:52Endosulfan I

51 - 150 91217330.0167 0.0123 74% mg/kg 12/14/09 22:52Endosulfan II

49 - 143 91217330.0167 0.0143 86% mg/kg 12/14/09 22:52Endosulfan sulfate

49 - 150 91217330.0167 0.0183 110% mg/kg 12/14/09 22:52Endrin

40 - 150 91217330.0167 0.0137 82% mg/kg 12/14/09 22:52Endrin aldehyde

55 - 139 91217330.0167 0.0127 76% mg/kg 12/14/09 22:52Endrin ketone

49 - 149 91217330.0167 0.0137 82% mg/kg 12/14/09 22:52Heptachlor

53 - 150 91217330.0167 0.0130 78% mg/kg 12/14/09 22:52Heptachlor epoxide

43 - 144 91217330.0167 0.0153 92% mg/kg 12/14/09 22:52Methoxychlor

22 - 150 91217330.0167 0.0137Surrogate: Tetrachloro-meta-xylene 82% 12/14/09 22:52

25 - 150 91217330.0167 0.0163Surrogate: Decachlorobiphenyl 98% 12/14/09 22:52

9121733-BS259 - 150 91217330.167 0.195 117% mg/kg 12/14/09 23:05Chlordane

18 - 150 91217330.333 0.312 94% mg/kg 12/14/09 23:05Toxaphene



9121739-BS135 - 135 91217391.00 0.570 57% ug/L 12/12/09 14:09Aldrin

40 - 138 91217391.00 0.670 67% ug/L 12/12/09 14:09delta-BHC

50 - 136 91217391.00 0.620 62% ug/L 12/12/09 14:09alpha-BHC

49 - 136 91217391.00 0.680 68% ug/L 12/12/09 14:09beta-BHC

49 - 141 91217391.00 0.670 67% ug/L 12/12/09 14:09gamma-BHC (Lindane)

43 - 137 91217391.00 0.650 65% ug/L 12/12/09 14:09alpha-Chlordane

44 - 134 91217391.00 0.630 63% ug/L 12/12/09 14:09gamma-Chlordane

41 - 150 91217391.00 0.680 68% ug/L 12/12/09 14:094,4'-DDD

40 - 144 91217391.00 0.650 65% ug/L 12/12/09 14:094,4'-DDE

43 - 138 91217391.00 0.670 67% ug/L 12/12/09 14:094,4'-DDT

48 - 142 91217391.00 0.640 64% ug/L 12/12/09 14:09Dieldrin

Page 21 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939


LCS - Cont.


Target

Range

Analyzed

Date/Time


9121739-BS146 - 139 91217391.00 0.620 62% ug/L 12/12/09 14:09Endosulfan I

48 - 141 91217391.00 0.620 62% ug/L 12/12/09 14:09Endosulfan II

40 - 146 91217391.00 0.680 68% ug/L 12/12/09 14:09Endosulfan sulfate

48 - 149 91217391.00 0.960 96% ug/L 12/12/09 14:09Endrin

30 - 150 91217391.00 0.650 65% ug/L 12/12/09 14:09Endrin aldehyde

48 - 140 91217391.00 0.590 59% ug/L 12/12/09 14:09Endrin ketone

32 - 137 91217391.00 0.660 66% ug/L 12/12/09 14:09Heptachlor

47 - 141 91217391.00 0.660 66% ug/L 12/12/09 14:09Heptachlor epoxide

44 - 139 91217391.00 0.800 80% ug/L 12/12/09 14:09Methoxychlor



9121739-BS256 - 152 912173910.0 11.0 109% ug/L 12/12/09 14:22Chlordane

32 - 140 912173920.0 18.6 93% ug/L 12/12/09 14:22Toxaphene



Page 22 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

CERTIFICATION SUMMARY

Method Matrix

TestAmerica Nashville

AIHA Nelac South Carolina

Soil N/A XSW846 8081A

Water N/A XSW846 8081A

Page 23 of 24


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

Emerald, Inc.

Received:


12/08/09 08:00

NSL0939

DATA QUALIFIERS AND DEFINITIONS

R1 The RPD between the primary and confirmatory analysis exceeded 40%. Per method 8000B, the higher value was reported.

R10 The RPD between the primary and confirmatory analysis exceeded 40%. Per method 8000B, the lower value was reported due to

apparent chromatographic problems.RL1 Reporting limit raised due to sample matrix effects.

Z3 The sample required a dilution due to the nature of the sample matrix. Because of this dilution, the surrogate spike concentration

in the sample was reduced to a level where the recovery calculation does not provide useful information.ZX Due to sample matrix effects, the surrogate recovery was outside the acceptance limits.

ND Not detected at the reporting limit (or method detection limit if shown)

METHOD MODIFICATION NOTES

Page 24 of 24


December 17, 2009

Client:

Attn:

Work Order:

Project Name:

Project Nbr:

Date Received:

SAP-2

[none]

NSL0913

12/08/09

Sumter, SC 29151



1:59:06PM


NSL0913-01B-11-S 12/04/09 08:49

NSL0913-02B-11-GW 12/04/09 08:55

NSL0913-03B-12-S 12/04/09 09:06

NSL0913-04B-12-GW 12/04/09 09:15

NSL0913-05B-13-S 12/04/09 09:30

NSL0913-06B-13-GW 12/04/09 09:40

NSL0913-07B-14-S 12/04/09 09:50

NSL0913-08B-14-GW 12/04/09 10:06

NSL0913-09B-15-S 12/04/09 10:22

NSL0913-10B-15-GW 12/04/09 10:30










Report Approved By:

Cathy Gartner

Project Management




Page 1 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:

Project Number: [none]

12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis

Date/TimeFlag MRLDilution

Factor MethodUnits BatchMDL


General Chemistry Parameters

91224890.50080.6 12/15/09 08:461 SW-846% 0.500% Dry Solids

Volatile Organic Compounds by EPA Method 8260B

RL1 91217111.15ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.574Acetone

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154Benzene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154Bromobenzene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0234Bromochloromethane

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.00918Bromodichloromethane

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154Bromoform

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0147Bromomethane

RL1 91217111.15ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.3902-Butanone

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154sec-Butylbenzene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154n-Butylbenzene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154tert-Butylbenzene

RL1 91217110.115ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154Carbon disulfide

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154Carbon Tetrachloride

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154Chlorobenzene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.00872Chlorodibromomethane

RL1 91217110.115ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.00964Chloroethane

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154Chloroform

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0230Chloromethane

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.01542-Chlorotoluene


RL1 91217110.115ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.07811,2-Dibromo-3-chloropropane

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.01191,2-Dibromoethane (EDB)

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154Dibromomethane

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.01651,4-Dichlorobenzene



RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0367Dichlorodifluoromethane

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.01541,1-Dichloroethane


RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154cis-1,2-Dichloroethene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.01541,1-Dichloroethene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154trans-1,2-Dichloroethene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.01031,3-Dichloropropane



RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154cis-1,3-Dichloropropene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154trans-1,3-Dichloropropene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.01541,1-Dichloropropene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154Ethylbenzene

RL1 91217110.115ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0145Hexachlorobutadiene

RL1 91217111.15ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.3902-Hexanone

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154Isopropylbenzene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154p-Isopropyltoluene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154Methyl tert-Butyl Ether

RL1 91217110.230ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0459Methylene Chloride

Page 2 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis




Volatile Organic Compounds by EPA Method 8260B - cont.

RL1 91217111.15ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.06664-Methyl-2-pentanone

RL1 91217110.115ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0390Naphthalene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154n-Propylbenzene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154Styrene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.01541,1,1,2-Tetrachloroethane


RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.00918Tetrachloroethene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.00918Toluene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.02111,2,3-Trichlorobenzene


RL1 91217110.115ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.02551,1,2-Trichloroethane


RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0191Trichloroethene

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0154Trichlorofluoromethane

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.02361,2,3-Trichloropropane

RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.009181,3,5-Trimethylbenzene


RL1 91217110.0459ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0188Vinyl chloride

RL1 91217110.115ND 12/14/09 02:2350 SW846 8260Bmg/kg dry 0.0298Xylenes, total

Surr: 1,2-Dichloroethane-d4 (67-138%) 114 % 12/14/09 02:23 SW846 8260B 912171150Surr: Dibromofluoromethane (75-125%) 105 % 12/14/09 02:23 SW846 8260B 912171150Surr: Toluene-d8 (76-129%) 114 % 12/14/09 02:23 SW846 8260B 912171150Surr: 4-Bromofluorobenzene (67-147%) 110 % 12/14/09 02:23 SW846 8260B 912171150

Page 3 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis





912161650.0ND 12/10/09 00:341 SW846 8260Bug/L 25.0Acetone

91216161.003.97 12/10/09 00:341 SW846 8260Bug/L 0.410Benzene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.360Bromobenzene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.470Bromochloromethane

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.270Bromodichloromethane

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.430Bromoform

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.300Bromomethane

912161650.0ND 12/10/09 00:341 SW846 8260Bug/L 2.102-Butanone

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.360sec-Butylbenzene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.310n-Butylbenzene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.380tert-Butylbenzene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.360Carbon disulfide

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.330Carbon Tetrachloride

91216161.001.01 12/10/09 00:341 SW846 8260Bug/L 0.220Chlorobenzene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.260Chlorodibromomethane

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.460Chloroethane

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.250Chloroform

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.390Chloromethane

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.5102-Chlorotoluene


91216165.00ND 12/10/09 00:341 SW846 8260Bug/L 0.8601,2-Dibromo-3-chloropropane

91216161.001.77 12/10/09 00:341 SW846 8260Bug/L 0.4601,2-Dibromoethane (EDB)

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.410Dibromomethane

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.4301,4-Dichlorobenzene

J 91216161.000.810 12/10/09 00:341 SW846 8260Bug/L 0.3201,3-Dichlorobenzene


91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.190Dichlorodifluoromethane

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.3401,1-Dichloroethane


91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.330cis-1,2-Dichloroethene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.2201,1-Dichloroethene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.330trans-1,2-Dichloroethene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.2701,3-Dichloropropane



91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.330cis-1,3-Dichloropropene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.330trans-1,3-Dichloropropene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.2601,1-Dichloropropene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.350Ethylbenzene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.790Hexachlorobutadiene

912161650.0ND 12/10/09 00:341 SW846 8260Bug/L 1.402-Hexanone

91216161.001.02 12/10/09 00:341 SW846 8260Bug/L 0.400Isopropylbenzene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.330p-Isopropyltoluene

91216161.001.74 12/10/09 00:341 SW846 8260Bug/L 0.320Methyl tert-Butyl Ether

91216165.00ND 12/10/09 00:341 SW846 8260Bug/L 0.480Methylene Chloride

912161610.0ND 12/10/09 00:341 SW846 8260Bug/L 1.404-Methyl-2-pentanone

91216165.00ND 12/10/09 00:341 SW846 8260Bug/L 0.380Naphthalene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.390n-Propylbenzene

Page 4 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis





91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.260Styrene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.2001,1,1,2-Tetrachloroethane


91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.320Tetrachloroethene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.350Toluene

L 91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.2701,2,3-Trichlorobenzene


91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.3201,1,2-Trichloroethane


91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.260Trichloroethene

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.220Trichlorofluoromethane

91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.4701,2,3-Trichloropropane

91216161.0010.9 12/10/09 00:341 SW846 8260Bug/L 0.3601,3,5-Trimethylbenzene


91216161.00ND 12/10/09 00:341 SW846 8260Bug/L 0.220Vinyl chloride

91216163.0018.6 12/10/09 00:341 SW846 8260Bug/L 0.730Xylenes, total


Page 5 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis





91224890.50084.1 12/15/09 08:461 SW-846% 0.500% Dry Solids


RL1 91217111.64ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.820Acetone

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220Benzene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220Bromobenzene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0335Bromochloromethane

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0131Bromodichloromethane

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220Bromoform

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0210Bromomethane

RL1 91217111.64ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.5582-Butanone

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220sec-Butylbenzene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220n-Butylbenzene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220tert-Butylbenzene

RL1 91217110.164ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220Carbon disulfide

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220Carbon Tetrachloride

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220Chlorobenzene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0125Chlorodibromomethane

RL1 91217110.164ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0138Chloroethane

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220Chloroform

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0328Chloromethane



RL1 91217110.164ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.1121,2-Dibromo-3-chloropropane

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.01711,2-Dibromoethane (EDB)

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220Dibromomethane




RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0525Dichlorodifluoromethane



RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220cis-1,2-Dichloroethene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.02201,1-Dichloroethene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220trans-1,2-Dichloroethene




RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220cis-1,3-Dichloropropene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220trans-1,3-Dichloropropene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.02201,1-Dichloropropene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220Ethylbenzene

RL1 91217110.164ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0207Hexachlorobutadiene

RL1 91217111.64ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.5582-Hexanone

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220Isopropylbenzene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220p-Isopropyltoluene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220Methyl tert-Butyl Ether

RL1 91217110.328ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0656Methylene Chloride

Page 6 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis





RL1 91217111.64ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.09524-Methyl-2-pentanone

RL1 91217110.164ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0558Naphthalene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220n-Propylbenzene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220Styrene



RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0131Tetrachloroethene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0131Toluene





RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0272Trichloroethene

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0220Trichlorofluoromethane

RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.03381,2,3-Trichloropropane



RL1 91217110.0656ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0269Vinyl chloride

RL1 91217110.164ND 12/14/09 02:5150 SW846 8260Bmg/kg dry 0.0427Xylenes, total


Page 7 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis






91216161.00ND 12/10/09 01:021 SW846 8260Bug/L 0.410Benzene







J 91216161.000.380 12/10/09 01:021 SW846 8260Bug/L 0.360sec-Butylbenzene

J 91216161.000.880 12/10/09 01:021 SW846 8260Bug/L 0.310n-Butylbenzene




J 91216161.000.530 12/10/09 01:021 SW846 8260Bug/L 0.220Chlorobenzene




J 91216161.000.880 12/10/09 01:021 SW846 8260Bug/L 0.390Chloromethane




91216161.00ND 12/10/09 01:021 SW846 8260Bug/L 0.4601,2-Dibromoethane (EDB)

















91216161.005.19 12/10/09 01:021 SW846 8260Bug/L 0.350Ethylbenzene



91216161.001.30 12/10/09 01:021 SW846 8260Bug/L 0.400Isopropylbenzene


91216161.00ND 12/10/09 01:021 SW846 8260Bug/L 0.320Methyl tert-Butyl Ether




91216161.005.89 12/10/09 01:021 SW846 8260Bug/L 0.390n-Propylbenzene

Page 8 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis








J 91216161.000.340 12/10/09 01:021 SW846 8260Bug/L 0.320Tetrachloroethene

J 91216161.000.600 12/10/09 01:021 SW846 8260Bug/L 0.350Toluene













Page 9 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis





91224890.50087.2 12/15/09 08:461 SW-846% 0.500% Dry Solids


91211620.04790.0851 12/14/09 15:011 SW846 8260Bmg/kg dry 0.0239Acetone

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641Benzene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641Bromobenzene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000976Bromochloromethane

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000383Bromodichloromethane

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641Bromoform

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000613Bromomethane

91211620.0479ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.01632-Butanone

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641sec-Butylbenzene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641n-Butylbenzene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641tert-Butylbenzene

91211620.00479ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641Carbon disulfide

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641Carbon Tetrachloride

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641Chlorobenzene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000364Chlorodibromomethane

91211620.00479ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000402Chloroethane

J, B 91211620.001910.000814 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641Chloroform

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000957Chloromethane

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.0006412-Chlorotoluene


91211620.00479ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.003251,2-Dibromo-3-chloropropane

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.0004981,2-Dibromoethane (EDB)

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641Dibromomethane

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.0006891,4-Dichlorobenzene



91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.00153Dichlorodifluoromethane

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.0006411,1-Dichloroethane


91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641cis-1,2-Dichloroethene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.0006411,1-Dichloroethene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641trans-1,2-Dichloroethene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.0004311,3-Dichloropropane



91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641cis-1,3-Dichloropropene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641trans-1,3-Dichloropropene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.0006411,1-Dichloropropene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641Ethylbenzene

91211620.00479ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000603Hexachlorobutadiene

91211620.0479ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.01632-Hexanone

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641Isopropylbenzene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641p-Isopropyltoluene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641Methyl tert-Butyl Ether

91211620.00957ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.00191Methylene Chloride

Page 10 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis





91211620.0479ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.002784-Methyl-2-pentanone

91211620.00479ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.00163Naphthalene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641n-Propylbenzene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641Styrene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.0006411,1,1,2-Tetrachloroethane


91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000383Tetrachloroethene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000383Toluene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.0008811,2,3-Trichlorobenzene


91211620.00479ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.001061,1,2-Trichloroethane


91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000795Trichloroethene

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000641Trichlorofluoromethane

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.0009861,2,3-Trichloropropane

91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.0003831,3,5-Trimethylbenzene


91211620.00191ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.000785Vinyl chloride

91211620.00479ND 12/14/09 15:011 SW846 8260Bmg/kg dry 0.00124Xylenes, total


Page 11 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis


















91216161.00ND 12/10/09 01:291 SW846 8260Bug/L 0.220Chlorobenzene

























J 91216161.000.550 12/10/09 01:291 SW846 8260Bug/L 0.350Ethylbenzene



91216161.00ND 12/10/09 01:291 SW846 8260Bug/L 0.400Isopropylbenzene






J 91216161.000.430 12/10/09 01:291 SW846 8260Bug/L 0.390n-Propylbenzene

Page 12 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis






















Page 13 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis





91224890.50085.0 12/15/09 08:461 SW-846% 0.500% Dry Solids


J 91222340.02430.0190 12/12/09 22:451 SW846 8260Bmg/kg dry 0.0121Acetone
















J, B 91222340.0009710.000748 12/12/09 22:451 SW846 8260Bmg/kg dry 0.000325Chloroform





























Page 14 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis












J 91222340.0009710.000204 12/12/09 22:451 SW846 8260Bmg/kg dry 0.000194Toluene













Page 15 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis





















































Page 16 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis

















91216161.00ND 12/10/09 01:571 SW846 8260Bug/L 0.3601,3,5-Trimethylbenzene

J 91216161.000.350 12/10/09 01:571 SW846 8260Bug/L 0.3201,2,4-Trimethylbenzene


91216163.00ND 12/10/09 01:571 SW846 8260Bug/L 0.730Xylenes, total


Page 17 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis





91224890.50080.9 12/15/09 08:461 SW-846% 0.500% Dry Solids


91211620.0494ND 12/14/09 15:321 SW846 8260Bmg/kg dry 0.0247Acetone
















B, J 91211620.001980.000712 12/14/09 15:321 SW846 8260Bmg/kg dry 0.000663Chloroform





























Page 18 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis












91211620.00198ND 12/14/09 15:321 SW846 8260Bmg/kg dry 0.000396Toluene













Page 19 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis





















































Page 20 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

ANALYTICAL REPORT

Analyte Result

Analysis

















91216161.00ND 12/10/09 02:241 SW846 8260Bug/L 0.3601,3,5-Trimethylbenzene

J 91216161.000.490 12/10/09 02:241 SW846 8260Bug/L 0.3201,2,4-Trimethylbenzene


91216163.00ND 12/10/09 02:241 SW846 8260Bug/L 0.730Xylenes, total


Page 21 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


Parameter

Wt/Vol


Extraction


Volatile Organic Compounds by EPA Method 8260B 11.91 EPA 5035JRL12/04/09 08:499122234SW846 8260B NSL0913-01 5.00

12.55 EPA 5035JRL12/04/09 08:499121162SW846 8260B NSL0913-01RE1 5.00

13.51 EPA 5035JRL12/04/09 08:499121711SW846 8260B NSL0913-01RE2 5.00

9.21 EPA 5035JRL12/04/09 09:069122234SW846 8260B NSL0913-03 5.00

9.49 EPA 5035JRL12/04/09 09:069121162SW846 8260B NSL0913-03RE1 5.00

9.06 EPA 5035JRL12/04/09 09:069121711SW846 8260B NSL0913-03RE2 5.00

5.33 EPA 5035JRL12/04/09 09:309122234SW846 8260B NSL0913-05 5.00

5.99 EPA 5035JRL12/04/09 09:309121162SW846 8260B NSL0913-05RE1 5.00

12.11 EPA 5035JRL12/04/09 09:509122234SW846 8260B NSL0913-07 5.00

6.35 EPA 5035JRL12/04/09 10:229122234SW846 8260B NSL0913-09 5.00

6.25 EPA 5035JRL12/04/09 10:229121162SW846 8260B NSL0913-09RE1 5.00

Page 22 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913




9121162-BLK1mg/kg wet 9121162<0.0250 9121162-BLK1 12/14/09 13:29Acetone

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29Benzene

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29Bromobenzene

mg/kg wet 9121162<0.00102 9121162-BLK1 12/14/09 13:29Bromochloromethane

mg/kg wet 9121162<0.000400 9121162-BLK1 12/14/09 13:29Bromodichloromethane

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29Bromoform

mg/kg wet 9121162<0.000640 9121162-BLK1 12/14/09 13:29Bromomethane

mg/kg wet 9121162<0.0170 9121162-BLK1 12/14/09 13:292-Butanone

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29sec-Butylbenzene

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29n-Butylbenzene

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29tert-Butylbenzene

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29Carbon disulfide

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29Carbon Tetrachloride

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29Chlorobenzene

mg/kg wet 9121162<0.000380 9121162-BLK1 12/14/09 13:29Chlorodibromomethane

mg/kg wet 9121162<0.000420 9121162-BLK1 12/14/09 13:29Chloroethane

mg/kg wet 91211620.00499 9121162-BLK1 12/14/09 13:29Chloroform

mg/kg wet 9121162<0.00100 9121162-BLK1 12/14/09 13:29Chloromethane

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:292-Chlorotoluene


mg/kg wet 9121162<0.00340 9121162-BLK1 12/14/09 13:291,2-Dibromo-3-chloropropane

mg/kg wet 9121162<0.000520 9121162-BLK1 12/14/09 13:291,2-Dibromoethane (EDB)

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29Dibromomethane

mg/kg wet 9121162<0.000720 9121162-BLK1 12/14/09 13:291,4-Dichlorobenzene



mg/kg wet 9121162<0.00160 9121162-BLK1 12/14/09 13:29Dichlorodifluoromethane

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:291,1-Dichloroethane


mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29cis-1,2-Dichloroethene

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:291,1-Dichloroethene

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29trans-1,2-Dichloroethene

mg/kg wet 9121162<0.000450 9121162-BLK1 12/14/09 13:291,3-Dichloropropane



mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29cis-1,3-Dichloropropene

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29trans-1,3-Dichloropropene

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:291,1-Dichloropropene

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29Ethylbenzene

mg/kg wet 9121162<0.000630 9121162-BLK1 12/14/09 13:29Hexachlorobutadiene

mg/kg wet 9121162<0.0170 9121162-BLK1 12/14/09 13:292-Hexanone

Page 23 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913




9121162-BLK1mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29Isopropylbenzene

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29p-Isopropyltoluene

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29Methyl tert-Butyl Ether

mg/kg wet 91211620.00302 9121162-BLK1J 12/14/09 13:29Methylene Chloride

mg/kg wet 9121162<0.00290 9121162-BLK1 12/14/09 13:294-Methyl-2-pentanone

mg/kg wet 9121162<0.00170 9121162-BLK1 12/14/09 13:29Naphthalene

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29n-Propylbenzene

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29Styrene

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:291,1,1,2-Tetrachloroethane


mg/kg wet 91211620.000680 9121162-BLK1J 12/14/09 13:29Tetrachloroethene

mg/kg wet 9121162<0.000400 9121162-BLK1 12/14/09 13:29Toluene

mg/kg wet 9121162<0.000920 9121162-BLK1 12/14/09 13:291,2,3-Trichlorobenzene


mg/kg wet 9121162<0.00111 9121162-BLK1 12/14/09 13:291,1,2-Trichloroethane


mg/kg wet 9121162<0.000830 9121162-BLK1 12/14/09 13:29Trichloroethene

mg/kg wet 9121162<0.000670 9121162-BLK1 12/14/09 13:29Trichlorofluoromethane

mg/kg wet 9121162<0.00103 9121162-BLK1 12/14/09 13:291,2,3-Trichloropropane

mg/kg wet 9121162<0.000400 9121162-BLK1 12/14/09 13:291,3,5-Trimethylbenzene


mg/kg wet 9121162<0.000820 9121162-BLK1 12/14/09 13:29Vinyl chloride

mg/kg wet 9121162<0.00130 9121162-BLK1 12/14/09 13:29Xylenes, total

9121162 9121162-BLK1 12/14/09 13:2992%Surrogate: 1,2-Dichloroethane-d4

9121162 9121162-BLK1 12/14/09 13:2996%Surrogate: Dibromofluoromethane

9121162 9121162-BLK1 12/14/09 13:29104%Surrogate: Toluene-d8

9121162 9121162-BLK1 12/14/09 13:2994%Surrogate: 4-Bromofluorobenzene

9121616-BLK1ug/L 9121616<25.0 9121616-BLK1 12/09/09 17:16Acetone

ug/L 9121616<0.410 9121616-BLK1 12/09/09 17:16Benzene

ug/L 9121616<0.360 9121616-BLK1 12/09/09 17:16Bromobenzene

ug/L 9121616<0.470 9121616-BLK1 12/09/09 17:16Bromochloromethane

ug/L 9121616<0.270 9121616-BLK1 12/09/09 17:16Bromodichloromethane

ug/L 9121616<0.430 9121616-BLK1 12/09/09 17:16Bromoform

ug/L 9121616<0.300 9121616-BLK1 12/09/09 17:16Bromomethane

ug/L 9121616<2.10 9121616-BLK1 12/09/09 17:162-Butanone

ug/L 9121616<0.360 9121616-BLK1 12/09/09 17:16sec-Butylbenzene

ug/L 9121616<0.310 9121616-BLK1 12/09/09 17:16n-Butylbenzene

ug/L 9121616<0.380 9121616-BLK1 12/09/09 17:16tert-Butylbenzene

ug/L 9121616<0.360 9121616-BLK1 12/09/09 17:16Carbon disulfide

Page 24 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913




9121616-BLK1ug/L 9121616<0.330 9121616-BLK1 12/09/09 17:16Carbon Tetrachloride

ug/L 9121616<0.220 9121616-BLK1 12/09/09 17:16Chlorobenzene

ug/L 9121616<0.260 9121616-BLK1 12/09/09 17:16Chlorodibromomethane

ug/L 9121616<0.460 9121616-BLK1 12/09/09 17:16Chloroethane

ug/L 9121616<0.250 9121616-BLK1 12/09/09 17:16Chloroform

ug/L 9121616<0.390 9121616-BLK1 12/09/09 17:16Chloromethane

ug/L 9121616<0.510 9121616-BLK1 12/09/09 17:162-Chlorotoluene


ug/L 9121616<0.860 9121616-BLK1 12/09/09 17:161,2-Dibromo-3-chloropropane

ug/L 9121616<0.460 9121616-BLK1 12/09/09 17:161,2-Dibromoethane (EDB)

ug/L 9121616<0.410 9121616-BLK1 12/09/09 17:16Dibromomethane

ug/L 9121616<0.430 9121616-BLK1 12/09/09 17:161,4-Dichlorobenzene



ug/L 9121616<0.190 9121616-BLK1 12/09/09 17:16Dichlorodifluoromethane

ug/L 9121616<0.340 9121616-BLK1 12/09/09 17:161,1-Dichloroethane


ug/L 9121616<0.330 9121616-BLK1 12/09/09 17:16cis-1,2-Dichloroethene

ug/L 9121616<0.220 9121616-BLK1 12/09/09 17:161,1-Dichloroethene

ug/L 9121616<0.330 9121616-BLK1 12/09/09 17:16trans-1,2-Dichloroethene

ug/L 9121616<0.270 9121616-BLK1 12/09/09 17:161,3-Dichloropropane



ug/L 9121616<0.330 9121616-BLK1 12/09/09 17:16cis-1,3-Dichloropropene

ug/L 9121616<0.330 9121616-BLK1 12/09/09 17:16trans-1,3-Dichloropropene

ug/L 9121616<0.260 9121616-BLK1 12/09/09 17:161,1-Dichloropropene

ug/L 9121616<0.350 9121616-BLK1 12/09/09 17:16Ethylbenzene

ug/L 91216162.41 9121616-BLK1 12/09/09 17:16Hexachlorobutadiene

ug/L 9121616<1.40 9121616-BLK1 12/09/09 17:162-Hexanone

ug/L 9121616<0.400 9121616-BLK1 12/09/09 17:16Isopropylbenzene

ug/L 9121616<0.330 9121616-BLK1 12/09/09 17:16p-Isopropyltoluene

ug/L 9121616<0.320 9121616-BLK1 12/09/09 17:16Methyl tert-Butyl Ether

ug/L 9121616<0.480 9121616-BLK1 12/09/09 17:16Methylene Chloride

ug/L 9121616<1.40 9121616-BLK1 12/09/09 17:164-Methyl-2-pentanone

ug/L 9121616<0.380 9121616-BLK1 12/09/09 17:16Naphthalene

ug/L 9121616<0.390 9121616-BLK1 12/09/09 17:16n-Propylbenzene

ug/L 9121616<0.260 9121616-BLK1 12/09/09 17:16Styrene

ug/L 9121616<0.200 9121616-BLK1 12/09/09 17:161,1,1,2-Tetrachloroethane


ug/L 9121616<0.320 9121616-BLK1 12/09/09 17:16Tetrachloroethene

ug/L 9121616<0.350 9121616-BLK1 12/09/09 17:16Toluene

Page 25 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913




9121616-BLK1ug/L 91216162.30 9121616-BLK1 12/09/09 17:161,2,3-Trichlorobenzene

ug/L 91216160.640 9121616-BLK1J 12/09/09 17:161,2,4-Trichlorobenzene

ug/L 9121616<0.320 9121616-BLK1 12/09/09 17:161,1,2-Trichloroethane


ug/L 9121616<0.260 9121616-BLK1 12/09/09 17:16Trichloroethene

ug/L 9121616<0.220 9121616-BLK1 12/09/09 17:16Trichlorofluoromethane

ug/L 9121616<0.470 9121616-BLK1 12/09/09 17:161,2,3-Trichloropropane

ug/L 9121616<0.360 9121616-BLK1 12/09/09 17:161,3,5-Trimethylbenzene


ug/L 9121616<0.220 9121616-BLK1 12/09/09 17:16Vinyl chloride

ug/L 9121616<0.330 9121616-BLK1 12/09/09 17:16o-Xylene

ug/L 9121616<0.400 9121616-BLK1 12/09/09 17:16m,p-Xylene

ug/L 9121616<0.730 9121616-BLK1 12/09/09 17:16Xylenes, total





















mg/kg wet 9121711<0.000670 9121711-BLK1 12/13/09 20:27Chloroform






Page 26 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913




9121711-BLK1mg/kg wet 9121711<0.000670 9121711-BLK1 12/13/09 20:27Dibromomethane



















mg/kg wet 9121711<0.000670 9121711-BLK1 12/13/09 20:27Isopropylbenzene



mg/kg wet 9121711<0.00200 9121711-BLK1 12/13/09 20:27Methylene Chloride







mg/kg wet 9121711<0.000400 9121711-BLK1 12/13/09 20:27Tetrachloroethene












Page 27 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913




9121711-BLK1mg/kg wet 9121711<0.00130 9121711-BLK1 12/13/09 20:27Xylenes, total





















mg/kg wet 91222340.00306 9122234-BLK1B 12/12/09 16:25Chloroform


















Page 28 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913




9122234-BLK1mg/kg wet 9122234<0.000780 9122234-BLK1 12/12/09 16:252,2-Dichloropropane


































Page 29 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


Duplicate

Analyte UnitsOrig. Val. Duplicate RPD Batch

Sample

DuplicatedQ

Analyzed

Date/TimeLimit % Rec.


9122489-DUP1%41.7 18.5 20 9122489 NSL0632-02 12/15/09 08:46% Dry Solids 77

Page 30 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


LCS


Target

Range

Analyzed

Date/Time


9121162-BS160 - 150 9121162250 284 114% ug/kg 12/14/09 11:57Acetone

78 - 126 912116250.0 52.6 105% ug/kg 12/14/09 11:57Benzene

79 - 126 912116250.0 51.1 102% ug/kg 12/14/09 11:57Bromobenzene

78 - 126 912116250.0 52.2 104% ug/kg 12/14/09 11:57Bromochloromethane

75 - 129 912116250.0 51.8 104% ug/kg 12/14/09 11:57Bromodichloromethane

74 - 133 912116250.0 48.0 96% ug/kg 12/14/09 11:57Bromoform

50 - 150 912116250.0 50.4 101% ug/kg 12/14/09 11:57Bromomethane

68 - 149 9121162250 306 122% ug/kg 12/14/09 11:572-Butanone

76 - 135 912116250.0 55.3 111% ug/kg 12/14/09 11:57sec-Butylbenzene

73 - 143 912116250.0 55.6 111% ug/kg 12/14/09 11:57n-Butylbenzene

80 - 129 912116250.0 53.3 107% ug/kg 12/14/09 11:57tert-Butylbenzene

80 - 132 912116250.0 54.3 109% ug/kg 12/14/09 11:57Carbon disulfide

70 - 138 912116250.0 48.3 97% ug/kg 12/14/09 11:57Carbon Tetrachloride

80 - 123 912116250.0 53.2 106% ug/kg 12/14/09 11:57Chlorobenzene

80 - 127 912116250.0 47.8 96% ug/kg 12/14/09 11:57Chlorodibromomethane

55 - 150 912116250.0 50.8 102% ug/kg 12/14/09 11:57Chloroethane

70 - 127 912116250.0 45.8 92%B ug/kg 12/14/09 11:57Chloroform

36 - 137 912116250.0 44.9 90% ug/kg 12/14/09 11:57Chloromethane

80 - 130 912116250.0 53.1 106% ug/kg 12/14/09 11:572-Chlorotoluene


62 - 150 912116250.0 52.3 105% ug/kg 12/14/09 11:571,2-Dibromo-3-chloropropane

80 - 131 912116250.0 53.5 107% ug/kg 12/14/09 11:571,2-Dibromoethane (EDB)

78 - 128 912116250.0 50.8 102% ug/kg 12/14/09 11:57Dibromomethane

80 - 129 912116250.0 55.3 111% ug/kg 12/14/09 11:571,4-Dichlorobenzene



30 - 150 912116250.0 34.1 68% ug/kg 12/14/09 11:57Dichlorodifluoromethane

71 - 126 912116250.0 51.8 104% ug/kg 12/14/09 11:571,1-Dichloroethane


75 - 126 912116250.0 50.2 100% ug/kg 12/14/09 11:57cis-1,2-Dichloroethene

70 - 125 912116250.0 52.6 105% ug/kg 12/14/09 11:571,1-Dichloroethene

73 - 128 912116250.0 49.2 98% ug/kg 12/14/09 11:57trans-1,2-Dichloroethene

79 - 128 912116250.0 52.9 106% ug/kg 12/14/09 11:571,3-Dichloropropane



74 - 136 912116250.0 57.4 115% ug/kg 12/14/09 11:57cis-1,3-Dichloropropene

73 - 128 912116250.0 54.8 110% ug/kg 12/14/09 11:57trans-1,3-Dichloropropene

78 - 125 912116250.0 49.8 100% ug/kg 12/14/09 11:571,1-Dichloropropene

79 - 130 912116250.0 53.2 106% ug/kg 12/14/09 11:57Ethylbenzene

75 - 150 912116250.0 54.5 109% ug/kg 12/14/09 11:57Hexachlorobutadiene

65 - 150 9121162250 302 121% ug/kg 12/14/09 11:572-Hexanone

Page 31 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


LCS - Cont.


Target

Range

Analyzed

Date/Time


9121162-BS165 - 121 912116250.0 52.8 106% ug/kg 12/14/09 11:57Isopropylbenzene

76 - 133 912116250.0 53.5 107% ug/kg 12/14/09 11:57p-Isopropyltoluene

70 - 128 912116250.0 45.6 91% ug/kg 12/14/09 11:57Methyl tert-Butyl Ether

69 - 140 912116250.0 53.6 107% ug/kg 12/14/09 11:57Methylene Chloride

67 - 147 9121162250 294 118% ug/kg 12/14/09 11:574-Methyl-2-pentanone

72 - 150 912116250.0 58.9 118% ug/kg 12/14/09 11:57Naphthalene

76 - 133 912116250.0 54.7 109% ug/kg 12/14/09 11:57n-Propylbenzene

80 - 140 912116250.0 56.4 113% ug/kg 12/14/09 11:57Styrene

80 - 132 912116250.0 55.3 111% ug/kg 12/14/09 11:571,1,1,2-Tetrachloroethane


76 - 130 912116250.0 51.6 103% ug/kg 12/14/09 11:57Tetrachloroethene

76 - 126 912116250.0 54.8 110% ug/kg 12/14/09 11:57Toluene

75 - 150 912116250.0 57.1 114% ug/kg 12/14/09 11:571,2,3-Trichlorobenzene


73 - 133 912116250.0 53.3 107% ug/kg 12/14/09 11:571,1,2-Trichloroethane


79 - 129 912116250.0 51.4 103% ug/kg 12/14/09 11:57Trichloroethene

52 - 148 912116250.0 42.0 84% ug/kg 12/14/09 11:57Trichlorofluoromethane

70 - 125 912116250.0 49.7 99% ug/kg 12/14/09 11:571,2,3-Trichloropropane

80 - 134 912116250.0 53.1 106% ug/kg 12/14/09 11:571,3,5-Trimethylbenzene


53 - 142 912116250.0 47.8 96% ug/kg 12/14/09 11:57Vinyl chloride

80 - 130 9121162150 151 101% ug/kg 12/14/09 11:57Xylenes, total

67 - 138 912116250.0 46.2Surrogate: 1,2-Dichloroethane-d4 92% 12/14/09 11:57

75 - 125 912116250.0 47.5Surrogate: Dibromofluoromethane 95% 12/14/09 11:57

76 - 129 912116250.0 50.8Surrogate: Toluene-d8 102% 12/14/09 11:57

67 - 147 912116250.0 48.2Surrogate: 4-Bromofluorobenzene 96% 12/14/09 11:57

9121616-BS156 - 150 9121616250 338 135% ug/L 12/09/09 15:27Acetone

80 - 121 912161650.0 51.7 103% ug/L 12/09/09 15:27Benzene

72 - 130 912161650.0 47.7 95% ug/L 12/09/09 15:27Bromobenzene

73 - 137 912161650.0 54.4 109% ug/L 12/09/09 15:27Bromochloromethane

75 - 131 912161650.0 59.2 118% ug/L 12/09/09 15:27Bromodichloromethane

65 - 140 912161650.0 51.5 103% ug/L 12/09/09 15:27Bromoform

50 - 150 912161650.0 57.8 116% ug/L 12/09/09 15:27Bromomethane

70 - 144 9121616250 303 121% ug/L 12/09/09 15:272-Butanone

72 - 140 912161650.0 51.8 104% ug/L 12/09/09 15:27sec-Butylbenzene

68 - 140 912161650.0 52.4 105% ug/L 12/09/09 15:27n-Butylbenzene

76 - 135 912161650.0 51.5 103% ug/L 12/09/09 15:27tert-Butylbenzene

74 - 137 912161650.0 53.2 106% ug/L 12/09/09 15:27Carbon disulfide

Page 32 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


LCS - Cont.


Target

Range

Analyzed

Date/Time


9121616-BS171 - 137 912161650.0 63.1 126% ug/L 12/09/09 15:27Carbon Tetrachloride

80 - 121 912161650.0 50.4 101% ug/L 12/09/09 15:27Chlorobenzene

68 - 137 912161650.0 53.1 106% ug/L 12/09/09 15:27Chlorodibromomethane

50 - 146 912161650.0 50.8 102% ug/L 12/09/09 15:27Chloroethane

73 - 131 912161650.0 61.4 123% ug/L 12/09/09 15:27Chloroform

30 - 132 912161650.0 53.8 108% ug/L 12/09/09 15:27Chloromethane

74 - 135 912161650.0 48.2 96% ug/L 12/09/09 15:272-Chlorotoluene


56 - 145 912161650.0 49.3 99% ug/L 12/09/09 15:271,2-Dibromo-3-chloropropane

80 - 135 912161650.0 55.3 111% ug/L 12/09/09 15:271,2-Dibromoethane (EDB)

78 - 133 912161650.0 60.0 120% ug/L 12/09/09 15:27Dibromomethane

80 - 120 912161650.0 48.0 96% ug/L 12/09/09 15:271,4-Dichlorobenzene



30 - 132 912161650.0 42.7 85% ug/L 12/09/09 15:27Dichlorodifluoromethane

75 - 125 912161650.0 55.3 111% ug/L 12/09/09 15:271,1-Dichloroethane


71 - 132 912161650.0 59.0 118% ug/L 12/09/09 15:27cis-1,2-Dichloroethene

73 - 125 912161650.0 54.8 110% ug/L 12/09/09 15:271,1-Dichloroethene

77 - 125 912161650.0 57.7 115% ug/L 12/09/09 15:27trans-1,2-Dichloroethene

76 - 125 912161650.0 53.2 106% ug/L 12/09/09 15:271,3-Dichloropropane



70 - 140 912161650.0 50.6 101% ug/L 12/09/09 15:27cis-1,3-Dichloropropene

62 - 139 912161650.0 52.7 105% ug/L 12/09/09 15:27trans-1,3-Dichloropropene

78 - 126 912161650.0 56.1 112% ug/L 12/09/09 15:271,1-Dichloropropene

78 - 133 912161650.0 52.4 105% ug/L 12/09/09 15:27Ethylbenzene

70 - 150 912161650.0 62.8 126%B ug/L 12/09/09 15:27Hexachlorobutadiene

60 - 150 9121616250 305 122% ug/L 12/09/09 15:272-Hexanone

69 - 120 912161650.0 53.6 107% ug/L 12/09/09 15:27Isopropylbenzene

72 - 134 912161650.0 50.9 102% ug/L 12/09/09 15:27p-Isopropyltoluene

76 - 120 912161650.0 55.1 110% ug/L 12/09/09 15:27Methyl tert-Butyl Ether

80 - 133 912161650.0 56.4 113% ug/L 12/09/09 15:27Methylene Chloride

62 - 146 9121616250 266 107% ug/L 12/09/09 15:274-Methyl-2-pentanone

71 - 139 912161650.0 60.4 121% ug/L 12/09/09 15:27Naphthalene

70 - 143 912161650.0 49.1 98% ug/L 12/09/09 15:27n-Propylbenzene

80 - 136 912161650.0 52.9 106% ug/L 12/09/09 15:27Styrene

80 - 130 912161650.0 57.9 116% ug/L 12/09/09 15:271,1,1,2-Tetrachloroethane


77 - 131 912161650.0 52.6 105% ug/L 12/09/09 15:27Tetrachloroethene

78 - 125 912161650.0 47.5 95% ug/L 12/09/09 15:27Toluene

Page 33 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


LCS - Cont.


Target

Range

Analyzed

Date/Time


9121616-BS171 - 138 912161650.0 77.3 155%L, B ug/L 12/09/09 15:271,2,3-Trichlorobenzene

74 - 136 912161650.0 65.9 132% ug/L 12/09/09 15:271,2,4-Trichlorobenzene

80 - 123 912161650.0 53.3 107% ug/L 12/09/09 15:271,1,2-Trichloroethane


74 - 139 912161650.0 55.6 111% ug/L 12/09/09 15:27Trichloroethene

60 - 133 912161650.0 55.0 110% ug/L 12/09/09 15:27Trichlorofluoromethane

64 - 127 912161650.0 46.1 92% ug/L 12/09/09 15:271,2,3-Trichloropropane

75 - 134 912161650.0 51.0 102% ug/L 12/09/09 15:271,3,5-Trimethylbenzene


60 - 122 912161650.0 50.5 101% ug/L 12/09/09 15:27Vinyl chloride

66 - 150 912161650.0 51.6 103% ug/L 12/09/09 15:27o-Xylene

78 - 132 9121616100 104 104% ug/L 12/09/09 15:27m,p-Xylene

78 - 134 9121616150 155 103% ug/L 12/09/09 15:27Xylenes, total





9121711-BS160 - 150 9121711250 313 125% ug/kg 12/13/09 18:11Acetone

78 - 126 912171150.0 51.3 103% ug/kg 12/13/09 18:11Benzene




74 - 133 912171150.0 50.2 100% ug/kg 12/13/09 18:11Bromoform


68 - 149 9121711250 280 112% ug/kg 12/13/09 18:112-Butanone









70 - 127 912171150.0 51.2 102% ug/kg 12/13/09 18:11Chloroform






Page 34 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


LCS - Cont.


Target

Range

Analyzed

Date/Time


9121711-BS178 - 128 912171150.0 53.3 107% ug/kg 12/13/09 18:11Dibromomethane


















65 - 150 9121711250 278 111% ug/kg 12/13/09 18:112-Hexanone

65 - 121 912171150.0 53.1 106% ug/kg 12/13/09 18:11Isopropylbenzene







80 - 140 912171150.0 52.9 106% ug/kg 12/13/09 18:11Styrene



76 - 130 912171150.0 53.0 106%MNR ug/kg 12/13/09 18:11Tetrachloroethene

76 - 126 912171150.0 53.3 107% ug/kg 12/13/09 18:11Toluene





79 - 129 912171150.0 53.9 108%MNR ug/kg 12/13/09 18:11Trichloroethene






Page 35 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


LCS - Cont.


Target

Range

Analyzed

Date/Time


9121711-BS180 - 130 9121711150 166 111% ug/kg 12/13/09 18:11Xylenes, total





9122234-BS160 - 150 9122234250 221 89% ug/kg 12/12/09 14:26Acetone

78 - 126 912223450.0 45.8 92% ug/kg 12/12/09 14:26Benzene




74 - 133 912223450.0 44.8 90% ug/kg 12/12/09 14:26Bromoform


68 - 149 9122234250 244 98% ug/kg 12/12/09 14:262-Butanone



























Page 36 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


LCS - Cont.


Target

Range

Analyzed

Date/Time


9122234-BS160 - 139 912223450.0 46.0 92% ug/kg 12/12/09 14:262,2-Dichloropropane






65 - 150 9122234250 257 103% ug/kg 12/12/09 14:262-Hexanone








80 - 140 912223450.0 55.7 111% ug/kg 12/12/09 14:26Styrene




76 - 126 912223450.0 49.4 99% ug/kg 12/12/09 14:26Toluene
















Page 37 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

Orig. Val. UnitsAnalyte

Sample

DuplicatedBatchRPDDuplicate

LCS Dup


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121162-BSD1309 8 50 9121162 250 124%ug/kg 60 - 150 12/14/09 12:28Acetone

52.4 0.5 50 9121162 50.0 105%ug/kg 78 - 126 12/14/09 12:28Benzene

49.6 3 50 9121162 50.0 99%ug/kg 79 - 126 12/14/09 12:28Bromobenzene

52.6 0.7 50 9121162 50.0 105%ug/kg 78 - 126 12/14/09 12:28Bromochloromethane

52.7 2 50 9121162 50.0 105%ug/kg 75 - 129 12/14/09 12:28Bromodichloromethane

47.6 0.9 43 9121162 50.0 95%ug/kg 74 - 133 12/14/09 12:28Bromoform

51.6 2 46 9121162 50.0 103%ug/kg 50 - 150 12/14/09 12:28Bromomethane

302 1 50 9121162 250 121%ug/kg 68 - 149 12/14/09 12:282-Butanone

54.2 2 50 9121162 50.0 108%ug/kg 76 - 135 12/14/09 12:28sec-Butylbenzene

55.1 1 50 9121162 50.0 110%ug/kg 73 - 143 12/14/09 12:28n-Butylbenzene

52.4 2 50 9121162 50.0 105%ug/kg 80 - 129 12/14/09 12:28tert-Butylbenzene

54.6 0.6 48 9121162 50.0 109%ug/kg 80 - 132 12/14/09 12:28Carbon disulfide

47.5 2 44 9121162 50.0 95%ug/kg 70 - 138 12/14/09 12:28Carbon Tetrachloride

52.6 1 50 9121162 50.0 105%ug/kg 80 - 123 12/14/09 12:28Chlorobenzene

48.8 2 48 9121162 50.0 98%ug/kg 80 - 127 12/14/09 12:28Chlorodibromomethane

51.7 2 50 9121162 50.0 103%ug/kg 55 - 150 12/14/09 12:28Chloroethane

46.0 0.4 50 9121162B 50.0 92%ug/kg 70 - 127 12/14/09 12:28Chloroform

44.5 0.8 44 9121162 50.0 89%ug/kg 36 - 137 12/14/09 12:28Chloromethane

52.1 2 50 9121162 50.0 104%ug/kg 80 - 130 12/14/09 12:282-Chlorotoluene


51.4 2 45 9121162 50.0 103%ug/kg 62 - 150 12/14/09 12:281,2-Dibromo-3-chloropropane

54.0 0.9 45 9121162 50.0 108%ug/kg 80 - 131 12/14/09 12:281,2-Dibromoethane (EDB)

52.0 2 50 9121162 50.0 104%ug/kg 78 - 128 12/14/09 12:28Dibromomethane

53.3 4 50 9121162 50.0 107%ug/kg 80 - 129 12/14/09 12:281,4-Dichlorobenzene



33.1 3 50 9121162 50.0 66%ug/kg 30 - 150 12/14/09 12:28Dichlorodifluoromethane

52.0 0.3 50 9121162 50.0 104%ug/kg 71 - 126 12/14/09 12:281,1-Dichloroethane


50.3 0.3 50 9121162 50.0 101%ug/kg 75 - 126 12/14/09 12:28cis-1,2-Dichloroethene

52.2 0.7 50 9121162 50.0 104%ug/kg 70 - 125 12/14/09 12:281,1-Dichloroethene

48.2 2 40 9121162 50.0 96%ug/kg 73 - 128 12/14/09 12:28trans-1,2-Dichloroethene

52.6 0.5 42 9121162 50.0 105%ug/kg 79 - 128 12/14/09 12:281,3-Dichloropropane


44.7 1 39 9121162 50.0 89%ug/kg 60 - 139 12/14/09 12:282,2-Dichloropropane

57.2 0.5 50 9121162 50.0 114%ug/kg 74 - 136 12/14/09 12:28cis-1,3-Dichloropropene

53.8 2 48 9121162 50.0 108%ug/kg 73 - 128 12/14/09 12:28trans-1,3-Dichloropropene

49.3 1 50 9121162 50.0 99%ug/kg 78 - 125 12/14/09 12:281,1-Dichloropropene

52.1 2 50 9121162 50.0 104%ug/kg 79 - 130 12/14/09 12:28Ethylbenzene

53.9 1 50 9121162 50.0 108%ug/kg 75 - 150 12/14/09 12:28Hexachlorobutadiene

300 0.8 50 9121162 250 120%ug/kg 65 - 150 12/14/09 12:282-Hexanone

Page 38 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


Sample


LCS Dup - Cont.


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121162-BSD151.4 3 50 9121162 50.0 103%ug/kg 65 - 121 12/14/09 12:28Isopropylbenzene

52.5 2 50 9121162 50.0 105%ug/kg 76 - 133 12/14/09 12:28p-Isopropyltoluene

46.2 1 50 9121162 50.0 92%ug/kg 70 - 128 12/14/09 12:28Methyl tert-Butyl Ether

55.1 3 50 9121162 50.0 110%ug/kg 69 - 140 12/14/09 12:28Methylene Chloride

292 0.7 45 9121162 250 117%ug/kg 67 - 147 12/14/09 12:284-Methyl-2-pentanone

58.7 0.4 50 9121162 50.0 117%ug/kg 72 - 150 12/14/09 12:28Naphthalene

53.2 3 50 9121162 50.0 106%ug/kg 76 - 133 12/14/09 12:28n-Propylbenzene

56.1 0.5 50 9121162 50.0 112%ug/kg 80 - 140 12/14/09 12:28Styrene

54.1 2 50 9121162 50.0 108%ug/kg 80 - 132 12/14/09 12:281,1,1,2-Tetrachloroethane


50.6 2 50 9121162 50.0 101%ug/kg 76 - 130 12/14/09 12:28Tetrachloroethene

54.0 1 50 9121162 50.0 108%ug/kg 76 - 126 12/14/09 12:28Toluene

56.3 1 50 9121162 50.0 113%ug/kg 75 - 150 12/14/09 12:281,2,3-Trichlorobenzene


53.9 1 50 9121162 50.0 108%ug/kg 73 - 133 12/14/09 12:281,1,2-Trichloroethane

45.0 0.3 41 9121162 50.0 90%ug/kg 70 - 132 12/14/09 12:281,1,1-Trichloroethane

51.9 0.9 50 9121162 50.0 104%ug/kg 79 - 129 12/14/09 12:28Trichloroethene

41.2 2 47 9121162 50.0 82%ug/kg 52 - 148 12/14/09 12:28Trichlorofluoromethane

55.2 10 47 9121162 50.0 110%ug/kg 70 - 125 12/14/09 12:281,2,3-Trichloropropane

52.1 2 50 9121162 50.0 104%ug/kg 80 - 134 12/14/09 12:281,3,5-Trimethylbenzene


48.5 1 39 9121162 50.0 97%ug/kg 53 - 142 12/14/09 12:28Vinyl chloride

149 1 50 9121162 150 99%ug/kg 80 - 130 12/14/09 12:28Xylenes, total

46.7 9121162 50.0 93%Surrogate: 1,2-Dichloroethane-d4 ug/kg 67 - 138 12/14/09 12:28

47.8 9121162 50.0 96%Surrogate: Dibromofluoromethane ug/kg 75 - 125 12/14/09 12:28

50.5 9121162 50.0 101%Surrogate: Toluene-d8 ug/kg 76 - 129 12/14/09 12:28

48.0 9121162 50.0 96%Surrogate: 4-Bromofluorobenzene ug/kg 67 - 147 12/14/09 12:28

9121616-BSD1352 4 31 9121616 250 141%ug/L 56 - 150 12/09/09 15:54Acetone

51.8 0.3 12 9121616 50.0 104%ug/L 80 - 121 12/09/09 15:54Benzene

49.0 3 23 9121616 50.0 98%ug/L 72 - 130 12/09/09 15:54Bromobenzene

56.0 3 32 9121616 50.0 112%ug/L 73 - 137 12/09/09 15:54Bromochloromethane

60.8 3 13 9121616 50.0 122%ug/L 75 - 131 12/09/09 15:54Bromodichloromethane

53.3 3 18 9121616 50.0 107%ug/L 65 - 140 12/09/09 15:54Bromoform

58.1 0.4 50 9121616 50.0 116%ug/L 50 - 150 12/09/09 15:54Bromomethane

311 3 37 9121616 250 124%ug/L 70 - 144 12/09/09 15:542-Butanone

53.4 3 21 9121616 50.0 107%ug/L 72 - 140 12/09/09 15:54sec-Butylbenzene

54.5 4 11 9121616 50.0 109%ug/L 68 - 140 12/09/09 15:54n-Butylbenzene

53.0 3 20 9121616 50.0 106%ug/L 76 - 135 12/09/09 15:54tert-Butylbenzene

54.2 2 28 9121616 50.0 108%ug/L 74 - 137 12/09/09 15:54Carbon disulfide

Page 39 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


Sample


LCS Dup - Cont.


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121616-BSD163.7 1 26 9121616 50.0 127%ug/L 71 - 137 12/09/09 15:54Carbon Tetrachloride

51.3 2 11 9121616 50.0 103%ug/L 80 - 121 12/09/09 15:54Chlorobenzene

54.5 3 16 9121616 50.0 109%ug/L 68 - 137 12/09/09 15:54Chlorodibromomethane

51.2 0.7 35 9121616 50.0 102%ug/L 50 - 146 12/09/09 15:54Chloroethane

62.1 1 32 9121616 50.0 124%ug/L 73 - 131 12/09/09 15:54Chloroform

55.2 2 34 9121616 50.0 110%ug/L 30 - 132 12/09/09 15:54Chloromethane

49.7 3 22 9121616 50.0 99%ug/L 74 - 135 12/09/09 15:542-Chlorotoluene


50.4 2 21 9121616 50.0 101%ug/L 56 - 145 12/09/09 15:541,2-Dibromo-3-chloropropane

56.7 2 10 9121616 50.0 113%ug/L 80 - 135 12/09/09 15:541,2-Dibromoethane (EDB)

61.7 3 11 9121616 50.0 123%ug/L 78 - 133 12/09/09 15:54Dibromomethane

49.4 3 10 9121616 50.0 99%ug/L 80 - 120 12/09/09 15:541,4-Dichlorobenzene



43.2 1 32 9121616 50.0 86%ug/L 30 - 132 12/09/09 15:54Dichlorodifluoromethane

56.0 1 34 9121616 50.0 112%ug/L 75 - 125 12/09/09 15:541,1-Dichloroethane


59.2 0.4 32 9121616 50.0 118%ug/L 71 - 132 12/09/09 15:54cis-1,2-Dichloroethene

55.2 0.8 31 9121616 50.0 110%ug/L 73 - 125 12/09/09 15:541,1-Dichloroethene

58.8 2 32 9121616 50.0 118%ug/L 77 - 125 12/09/09 15:54trans-1,2-Dichloroethene

54.2 2 20 9121616 50.0 108%ug/L 76 - 125 12/09/09 15:541,3-Dichloropropane



51.1 0.9 35 9121616 50.0 102%ug/L 70 - 140 12/09/09 15:54cis-1,3-Dichloropropene

55.2 5 26 9121616 50.0 110%ug/L 62 - 139 12/09/09 15:54trans-1,3-Dichloropropene

57.1 2 18 9121616 50.0 114%ug/L 78 - 126 12/09/09 15:541,1-Dichloropropene

53.4 2 12 9121616 50.0 107%ug/L 78 - 133 12/09/09 15:54Ethylbenzene

66.1 5 21 9121616B 50.0 132%ug/L 70 - 150 12/09/09 15:54Hexachlorobutadiene

316 4 20 9121616 250 127%ug/L 60 - 150 12/09/09 15:542-Hexanone

54.1 0.9 15 9121616 50.0 108%ug/L 69 - 120 12/09/09 15:54Isopropylbenzene

52.5 3 18 9121616 50.0 105%ug/L 72 - 134 12/09/09 15:54p-Isopropyltoluene

57.2 4 32 9121616 50.0 114%ug/L 76 - 120 12/09/09 15:54Methyl tert-Butyl Ether

57.1 1 36 9121616 50.0 114%ug/L 80 - 133 12/09/09 15:54Methylene Chloride

273 3 35 9121616 250 109%ug/L 62 - 146 12/09/09 15:544-Methyl-2-pentanone

65.8 9 30 9121616 50.0 132%ug/L 71 - 139 12/09/09 15:54Naphthalene

50.2 2 23 9121616 50.0 100%ug/L 70 - 143 12/09/09 15:54n-Propylbenzene

53.7 1 29 9121616 50.0 107%ug/L 80 - 136 12/09/09 15:54Styrene

58.8 1 11 9121616 50.0 118%ug/L 80 - 130 12/09/09 15:541,1,1,2-Tetrachloroethane


53.2 1 16 9121616 50.0 106%ug/L 77 - 131 12/09/09 15:54Tetrachloroethene

47.6 0.2 35 9121616 50.0 95%ug/L 78 - 125 12/09/09 15:54Toluene

Page 40 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


Sample


LCS Dup - Cont.


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121616-BSD185.7 10 28 9121616L, B 50.0 171%ug/L 71 - 138 12/09/09 15:541,2,3-Trichlorobenzene

70.3 6 23 9121616L 50.0 141%ug/L 74 - 136 12/09/09 15:541,2,4-Trichlorobenzene

55.1 3 21 9121616 50.0 110%ug/L 80 - 123 12/09/09 15:541,1,2-Trichloroethane


57.3 3 11 9121616 50.0 115%ug/L 74 - 139 12/09/09 15:54Trichloroethene

55.8 1 33 9121616 50.0 112%ug/L 60 - 133 12/09/09 15:54Trichlorofluoromethane

47.6 3 25 9121616 50.0 95%ug/L 64 - 127 12/09/09 15:541,2,3-Trichloropropane

52.3 3 21 9121616 50.0 105%ug/L 75 - 134 12/09/09 15:541,3,5-Trimethylbenzene


50.9 0.9 32 9121616 50.0 102%ug/L 60 - 122 12/09/09 15:54Vinyl chloride

52.2 1 27 9121616 50.0 104%ug/L 66 - 150 12/09/09 15:54o-Xylene

105 0.9 16 9121616 100 105%ug/L 78 - 132 12/09/09 15:54m,p-Xylene

157 1 18 9121616 150 104%ug/L 78 - 134 12/09/09 15:54Xylenes, total

29.5 9121616 25.0 118%Surrogate: 1,2-Dichloroethane-d4 ug/L 63 - 140 12/09/09 15:54

27.4 9121616 25.0 109%Surrogate: Dibromofluoromethane ug/L 73 - 131 12/09/09 15:54

22.9 9121616 25.0 92%Surrogate: Toluene-d8 ug/L 80 - 120 12/09/09 15:54

24.1 9121616 25.0 96%Surrogate: 4-Bromofluorobenzene ug/L 79 - 125 12/09/09 15:54

9121711-BSD1307 2 50 9121711 250 123%ug/kg 60 - 150 12/13/09 18:38Acetone

50.9 0.7 50 9121711 50.0 102%ug/kg 78 - 126 12/13/09 18:38Benzene




50.8 1 43 9121711 50.0 102%ug/kg 74 - 133 12/13/09 18:38Bromoform


284 1 50 9121711 250 113%ug/kg 68 - 149 12/13/09 18:382-Butanone

54.4 0.7 50 9121711 50.0 109%ug/kg 76 - 135 12/13/09 18:38sec-Butylbenzene


55.0 0.9 50 9121711 50.0 110%ug/kg 80 - 129 12/13/09 18:38tert-Butylbenzene


51.2 0.2 44 9121711 50.0 102%ug/kg 70 - 138 12/13/09 18:38Carbon Tetrachloride

52.4 0.4 50 9121711 50.0 105%ug/kg 80 - 123 12/13/09 18:38Chlorobenzene

51.3 0.2 48 9121711 50.0 103%ug/kg 80 - 127 12/13/09 18:38Chlorodibromomethane

50.4 0.9 50 9121711 50.0 101%ug/kg 55 - 150 12/13/09 18:38Chloroethane

51.0 0.4 50 9121711 50.0 102%ug/kg 70 - 127 12/13/09 18:38Chloroform


57.9 0.8 50 9121711 50.0 116%ug/kg 80 - 130 12/13/09 18:382-Chlorotoluene




Page 41 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


Sample


LCS Dup - Cont.


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121711-BSD153.2 0.3 50 9121711 50.0 106%ug/kg 78 - 128 12/13/09 18:38Dibromomethane

50.8 0.3 50 9121711 50.0 102%ug/kg 80 - 129 12/13/09 18:381,4-Dichlorobenzene




50.4 1 50 9121711 50.0 101%ug/kg 71 - 126 12/13/09 18:381,1-Dichloroethane


51.0 1 50 9121711 50.0 102%ug/kg 75 - 126 12/13/09 18:38cis-1,2-Dichloroethene

52.3 2 50 9121711 50.0 105%ug/kg 70 - 125 12/13/09 18:381,1-Dichloroethene

51.2 0.4 40 9121711 50.0 102%ug/kg 73 - 128 12/13/09 18:38trans-1,2-Dichloroethene




57.9 2 50 9121711 50.0 116%ug/kg 74 - 136 12/13/09 18:38cis-1,3-Dichloropropene


52.3 0.3 50 9121711 50.0 105%ug/kg 78 - 125 12/13/09 18:381,1-Dichloropropene

56.8 0.9 50 9121711 50.0 114%ug/kg 79 - 130 12/13/09 18:38Ethylbenzene


272 2 50 9121711 250 109%ug/kg 65 - 150 12/13/09 18:382-Hexanone

52.6 1 50 9121711 50.0 105%ug/kg 65 - 121 12/13/09 18:38Isopropylbenzene




296 1 45 9121711 250 118%ug/kg 67 - 147 12/13/09 18:384-Methyl-2-pentanone

68.8 6 50 9121711 50.0 138%ug/kg 72 - 150 12/13/09 18:38Naphthalene

58.8 0.4 50 9121711 50.0 118%ug/kg 76 - 133 12/13/09 18:38n-Propylbenzene

52.3 1 50 9121711 50.0 105%ug/kg 80 - 140 12/13/09 18:38Styrene




52.4 2 50 9121711 50.0 105%ug/kg 76 - 126 12/13/09 18:38Toluene





52.1 3 50 9121711 50.0 104%ug/kg 79 - 129 12/13/09 18:38Trichloroethene




54.6 0.5 50 9121711 50.0 109%ug/kg 80 - 132 12/13/09 18:381,2,4-Trimethylbenzene

50.5 0.8 39 9121711 50.0 101%ug/kg 53 - 142 12/13/09 18:38Vinyl chloride

Page 42 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


Sample


LCS Dup - Cont.


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121711-BSD1164 1 50 9121711 150 109%ug/kg 80 - 130 12/13/09 18:38Xylenes, total





9122234-BSD1239 8 50 9122234 250 96%ug/kg 60 - 150 12/12/09 14:55Acetone

46.1 0.6 50 9122234 50.0 92%ug/kg 78 - 126 12/12/09 14:55Benzene

47.5 0.1 50 9122234 50.0 95%ug/kg 79 - 126 12/12/09 14:55Bromobenzene

47.5 1 50 9122234 50.0 95%ug/kg 78 - 126 12/12/09 14:55Bromochloromethane


46.7 4 43 9122234 50.0 93%ug/kg 74 - 133 12/12/09 14:55Bromoform


257 5 50 9122234 250 103%ug/kg 68 - 149 12/12/09 14:552-Butanone




48.3 3 48 9122234 50.0 97%ug/kg 80 - 132 12/12/09 14:55Carbon disulfide





44.7 1 50 9122234B 50.0 89%ug/kg 70 - 127 12/12/09 14:55Chloroform

49.0 2 44 9122234 50.0 98%ug/kg 36 - 137 12/12/09 14:55Chloromethane




53.6 2 45 9122234 50.0 107%ug/kg 80 - 131 12/12/09 14:551,2-Dibromoethane (EDB)

47.0 1 50 9122234 50.0 94%ug/kg 78 - 128 12/12/09 14:55Dibromomethane












Page 43 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


Sample


LCS Dup - Cont.


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9122234-BSD146.0 0.02 39 9122234 50.0 92%ug/kg 60 - 139 12/12/09 14:552,2-Dichloropropane






276 7 50 9122234 250 111%ug/kg 65 - 150 12/12/09 14:552-Hexanone




48.7 0.2 50 9122234 50.0 97%ug/kg 69 - 140 12/12/09 14:55Methylene Chloride




54.6 2 50 9122234 50.0 109%ug/kg 80 - 140 12/12/09 14:55Styrene

50.5 0.6 50 9122234 50.0 101%ug/kg 80 - 132 12/12/09 14:551,1,1,2-Tetrachloroethane



48.4 2 50 9122234 50.0 97%ug/kg 76 - 126 12/12/09 14:55Toluene


53.8 0.5 50 9122234 50.0 108%ug/kg 64 - 150 12/12/09 14:551,2,4-Trichlorobenzene




43.5 0.7 47 9122234 50.0 87%ug/kg 52 - 148 12/12/09 14:55Trichlorofluoromethane










Page 44 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

Analyte Units


Orig. Val. MS Val Spike Conc % Rec.

Target

Range

Matrix Spike

Q

Analyzed

Date/Time

Sample

SpikedBatch


9121162-MS1316 250 NSL1304-04 123%8.53 912116229 - 181ug/kg 12/14/09 22:09Acetone

42.5 50.0 NSL1304-04 85%ND 912116242 - 141ug/kg 12/14/09 22:09Benzene

41.6 50.0 NSL1304-04 83%ND 912116219 - 154ug/kg 12/14/09 22:09Bromobenzene

46.6 50.0 NSL1304-04 93%ND 912116241 - 146ug/kg 12/14/09 22:09Bromochloromethane

44.8 50.0 NSL1304-04 90%ND 912116232 - 155ug/kg 12/14/09 22:09Bromodichloromethane

42.9 50.0 NSL1304-04 86%ND 912116210 - 155ug/kg 12/14/09 22:09Bromoform

40.6 50.0 NSL1304-04 81%ND 912116210 - 199ug/kg 12/14/09 22:09Bromomethane

297 250 NSL1304-04 119%ND 912116238 - 161ug/kg 12/14/09 22:092-Butanone

44.3 50.0 NSL1304-04 89%ND 912116210 - 170ug/kg 12/14/09 22:09sec-Butylbenzene

45.6 50.0 NSL1304-04 91%ND 912116210 - 183ug/kg 12/14/09 22:09n-Butylbenzene

42.1 50.0 NSL1304-04 84%ND 912116211 - 165ug/kg 12/14/09 22:09tert-Butylbenzene

40.4 50.0 NSL1304-04 81%ND 912116250 - 136ug/kg 12/14/09 22:09Carbon disulfide

38.6 50.0 NSL1304-04 77%ND 912116230 - 159ug/kg 12/14/09 22:09Carbon Tetrachloride

45.3 50.0 NSL1304-04 91%ND 912116225 - 151ug/kg 12/14/09 22:09Chlorobenzene

43.0 50.0 NSL1304-04 86%ND 912116227 - 150ug/kg 12/14/09 22:09Chlorodibromomethane

39.4 50.0 NSL1304-04 79%ND 912116215 - 197ug/kg 12/14/09 22:09Chloroethane

44.2 50.0 NSL1304-04B 78%5.41 912116233 - 148ug/kg 12/14/09 22:09Chloroform

36.4 50.0 NSL1304-04 73%ND 912116210 - 166ug/kg 12/14/09 22:09Chloromethane

43.5 50.0 NSL1304-04 87%ND 912116225 - 166ug/kg 12/14/09 22:092-Chlorotoluene


47.6 50.0 NSL1304-04 95%ND 912116210 - 167ug/kg 12/14/09 22:091,2-Dibromo-3-chloropropane

50.7 50.0 NSL1304-04 101%ND 912116230 - 155ug/kg 12/14/09 22:091,2-Dibromoethane (EDB)

48.8 50.0 NSL1304-04 98%ND 912116230 - 149ug/kg 12/14/09 22:09Dibromomethane

46.5 50.0 NSL1304-04 93%ND 912116210 - 170ug/kg 12/14/09 22:091,4-Dichlorobenzene



26.1 50.0 NSL1304-04 52%ND 912116210 - 188ug/kg 12/14/09 22:09Dichlorodifluoromethane

41.5 50.0 NSL1304-04 83%ND 912116251 - 135ug/kg 12/14/09 22:091,1-Dichloroethane


41.0 50.0 NSL1304-04 82%ND 912116232 - 150ug/kg 12/14/09 22:09cis-1,2-Dichloroethene

38.8 50.0 NSL1304-04 78%ND 912116246 - 141ug/kg 12/14/09 22:091,1-Dichloroethene

40.3 50.0 NSL1304-04 81%ND 912116241 - 146ug/kg 12/14/09 22:09trans-1,2-Dichloroethene

48.5 50.0 NSL1304-04 97%ND 912116235 - 148ug/kg 12/14/09 22:091,3-Dichloropropane



44.2 50.0 NSL1304-04 88%ND 912116223 - 152ug/kg 12/14/09 22:09cis-1,3-Dichloropropene

46.3 50.0 NSL1304-04 93%ND 912116224 - 151ug/kg 12/14/09 22:09trans-1,3-Dichloropropene

Page 45 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

Analyte Units



Target

Range

Matrix Spike - Cont.

Q

Analyzed

Date/Time

Sample

SpikedBatch


9121162-MS138.7 50.0 NSL1304-04 77%ND 912116240 - 151ug/kg 12/14/09 22:091,1-Dichloropropene

43.6 50.0 NSL1304-04 87%ND 912116221 - 165ug/kg 12/14/09 22:09Ethylbenzene

45.9 50.0 NSL1304-04 92%ND 912116210 - 173ug/kg 12/14/09 22:09Hexachlorobutadiene

303 250 NSL1304-04 121%ND 912116213 - 174ug/kg 12/14/09 22:092-Hexanone

42.8 50.0 NSL1304-04 86%ND 912116220 - 139ug/kg 12/14/09 22:09Isopropylbenzene

43.6 50.0 NSL1304-04 87%ND 912116210 - 164ug/kg 12/14/09 22:09p-Isopropyltoluene

40.2 50.0 NSL1304-04 80%ND 912116234 - 154ug/kg 12/14/09 22:09Methyl tert-Butyl Ether

50.6 50.0 NSL1304-04 90%5.75 912116236 - 163ug/kg 12/14/09 22:09Methylene Chloride

272 250 NSL1304-04 109%ND 912116219 - 176ug/kg 12/14/09 22:094-Methyl-2-pentanone

46.7 50.0 NSL1304-04 93%ND 912116210 - 160ug/kg 12/14/09 22:09Naphthalene

44.5 50.0 NSL1304-04 89%ND 912116216 - 174ug/kg 12/14/09 22:09n-Propylbenzene

29.3 50.0 NSL1304-04 59%ND 912116210 - 177ug/kg 12/14/09 22:09Styrene

47.1 50.0 NSL1304-04 94%ND 912116231 - 150ug/kg 12/14/09 22:091,1,1,2-Tetrachloroethane


45.8 50.0 NSL1304-04 81%5.10 912116233 - 155ug/kg 12/14/09 22:09Tetrachloroethene

46.5 50.0 NSL1304-04 93%ND 912116245 - 145ug/kg 12/14/09 22:09Toluene

47.0 50.0 NSL1304-04 94%ND 912116210 - 182ug/kg 12/14/09 22:091,2,3-Trichlorobenzene


50.4 50.0 NSL1304-04 101%ND 912116243 - 145ug/kg 12/14/09 22:091,1,2-Trichloroethane


40.8 50.0 NSL1304-04 82%ND 912116239 - 150ug/kg 12/14/09 22:09Trichloroethene

33.3 50.0 NSL1304-04 67%ND 912116225 - 174ug/kg 12/14/09 22:09Trichlorofluoromethane

52.9 50.0 NSL1304-04 106%ND 912116210 - 152ug/kg 12/14/09 22:091,2,3-Trichloropropane

43.4 50.0 NSL1304-04 87%ND 912116238 - 148ug/kg 12/14/09 22:091,3,5-Trimethylbenzene


35.0 50.0 NSL1304-04 70%ND 912116232 - 163ug/kg 12/14/09 22:09Vinyl chloride

128 150 NSL1304-04 85%ND 912116231 - 159ug/kg 12/14/09 22:09Xylenes, total

49.4 50.0 NSL1304-04 Surrogate: 1,2-Dichloroethane-d4 99% 912116267 - 138ug/kg 12/14/09 22:09

49.6 50.0 NSL1304-04 Surrogate: Dibromofluoromethane 99% 912116275 - 125ug/kg 12/14/09 22:09

56.3 50.0 NSL1304-04 Surrogate: Toluene-d8 113% 912116276 - 129ug/kg 12/14/09 22:09

46.3 50.0 NSL1304-04 Surrogate: 4-Bromofluorobenzene 93% 912116267 - 147ug/kg 12/14/09 22:09

9121616-MS1271 250 NSL0918-01 109%ND 912161656 - 150ug/L 12/10/09 09:22Acetone

55.8 50.0 NSL0918-01 112%ND 912161665 - 151ug/L 12/10/09 09:22Benzene

48.9 50.0 NSL0918-01 98%ND 912161669 - 142ug/L 12/10/09 09:22Bromobenzene

60.2 50.0 NSL0918-01 120%ND 912161664 - 154ug/L 12/10/09 09:22Bromochloromethane

Page 46 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

Analyte Units



Target

Range


Q

Analyzed

Date/Time

Sample

SpikedBatch


9121616-MS167.0 50.0 NSL0918-01 134%ND 912161675 - 138ug/L 12/10/09 09:22Bromodichloromethane

58.1 50.0 NSL0918-01 116%ND 912161655 - 153ug/L 12/10/09 09:22Bromoform

55.3 50.0 NSL0918-01 111%ND 912161613 - 176ug/L 12/10/09 09:22Bromomethane

295 250 NSL0918-01 118%ND 912161645 - 164ug/L 12/10/09 09:222-Butanone

55.5 50.0 NSL0918-01 111%ND 912161668 - 159ug/L 12/10/09 09:22sec-Butylbenzene

57.4 50.0 NSL0918-01 115%ND 912161667 - 151ug/L 12/10/09 09:22n-Butylbenzene

55.1 50.0 NSL0918-01 110%ND 912161673 - 153ug/L 12/10/09 09:22tert-Butylbenzene

62.1 50.0 NSL0918-01 119%2.47 912161633 - 187ug/L 12/10/09 09:22Carbon disulfide

79.8 50.0 NSL0918-01M7 160%ND 912161664 - 157ug/L 12/10/09 09:22Carbon Tetrachloride

55.1 50.0 NSL0918-01 110%ND 912161678 - 136ug/L 12/10/09 09:22Chlorobenzene

60.0 50.0 NSL0918-01 120%ND 912161664 - 145ug/L 12/10/09 09:22Chlorodibromomethane

53.4 50.0 NSL0918-01 107%ND 912161648 - 159ug/L 12/10/09 09:22Chloroethane

70.5 50.0 NSL0918-01 141%ND 912161672 - 145ug/L 12/10/09 09:22Chloroform

51.0 50.0 NSL0918-01 102%ND 912161610 - 194ug/L 12/10/09 09:22Chloromethane

51.2 50.0 NSL0918-01 102%ND 912161666 - 155ug/L 12/10/09 09:222-Chlorotoluene


43.3 50.0 NSL0918-01 87%ND 912161649 - 162ug/L 12/10/09 09:221,2-Dibromo-3-chloropropane

59.2 50.0 NSL0918-01 118%ND 912161670 - 152ug/L 12/10/09 09:221,2-Dibromoethane (EDB)

67.1 50.0 NSL0918-01 134%ND 912161675 - 141ug/L 12/10/09 09:22Dibromomethane

50.5 50.0 NSL0918-01 101%ND 912161675 - 135ug/L 12/10/09 09:221,4-Dichlorobenzene



45.1 50.0 NSL0918-01 90%ND 912161623 - 159ug/L 12/10/09 09:22Dichlorodifluoromethane

61.1 50.0 NSL0918-01 122%ND 912161664 - 154ug/L 12/10/09 09:221,1-Dichloroethane

78.4 50.0 NSL0918-01M7 157%ND 912161672 - 137ug/L 12/10/09 09:221,2-Dichloroethane

66.3 50.0 NSL0918-01 133%ND 912161657 - 154ug/L 12/10/09 09:22cis-1,2-Dichloroethene

60.6 50.0 NSL0918-01 121%ND 912161634 - 151ug/L 12/10/09 09:221,1-Dichloroethene

64.7 50.0 NSL0918-01 129%ND 912161657 - 157ug/L 12/10/09 09:22trans-1,2-Dichloroethene

57.3 50.0 NSL0918-01 115%ND 912161671 - 137ug/L 12/10/09 09:221,3-Dichloropropane



56.3 50.0 NSL0918-01 113%ND 912161656 - 156ug/L 12/10/09 09:22cis-1,3-Dichloropropene

60.9 50.0 NSL0918-01 122%ND 912161647 - 157ug/L 12/10/09 09:22trans-1,3-Dichloropropene

65.5 50.0 NSL0918-01 131%ND 912161670 - 155ug/L 12/10/09 09:221,1-Dichloropropene

58.8 50.0 NSL0918-01 118%ND 912161668 - 157ug/L 12/10/09 09:22Ethylbenzene

59.8 50.0 NSL0918-01B 120%ND 912161647 - 173ug/L 12/10/09 09:22Hexachlorobutadiene

312 250 NSL0918-01 125%ND 912161657 - 154ug/L 12/10/09 09:222-Hexanone

Page 47 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

Analyte Units



Target

Range


Q

Analyzed

Date/Time

Sample

SpikedBatch


9121616-MS161.8 50.0 NSL0918-01 124%ND 912161669 - 139ug/L 12/10/09 09:22Isopropylbenzene

54.7 50.0 NSL0918-01 109%ND 912161669 - 151ug/L 12/10/09 09:22p-Isopropyltoluene

54.2 50.0 NSL0918-01 108%ND 912161656 - 152ug/L 12/10/09 09:22Methyl tert-Butyl Ether

59.1 50.0 NSL0918-01 118%ND 912161671 - 136ug/L 12/10/09 09:22Methylene Chloride

292 250 NSL0918-01 117%ND 912161662 - 159ug/L 12/10/09 09:224-Methyl-2-pentanone

36.4 50.0 NSL0918-01 73%ND 912161656 - 161ug/L 12/10/09 09:22Naphthalene

52.2 50.0 NSL0918-01 104%ND 912161661 - 167ug/L 12/10/09 09:22n-Propylbenzene

59.3 50.0 NSL0918-01 119%ND 912161669 - 150ug/L 12/10/09 09:22Styrene

65.4 50.0 NSL0918-01 131%ND 912161680 - 140ug/L 12/10/09 09:221,1,1,2-Tetrachloroethane


62.9 50.0 NSL0918-01 120%3.00 912161663 - 155ug/L 12/10/09 09:22Tetrachloroethene

54.2 50.0 NSL0918-01 108%ND 912161661 - 153ug/L 12/10/09 09:22Toluene

41.4 50.0 NSL0918-01B 83%ND 912161657 - 155ug/L 12/10/09 09:221,2,3-Trichlorobenzene

51.9 50.0 NSL0918-01 104%ND 912161664 - 147ug/L 12/10/09 09:221,2,4-Trichlorobenzene

57.7 50.0 NSL0918-01 115%ND 912161674 - 138ug/L 12/10/09 09:221,1,2-Trichloroethane


68.7 50.0 NSL0918-01 124%6.88 912161674 - 139ug/L 12/10/09 09:22Trichloroethene

66.4 50.0 NSL0918-01 133%ND 912161653 - 149ug/L 12/10/09 09:22Trichlorofluoromethane

46.7 50.0 NSL0918-01 93%ND 912161649 - 148ug/L 12/10/09 09:221,2,3-Trichloropropane

54.1 50.0 NSL0918-01 108%ND 912161667 - 151ug/L 12/10/09 09:221,3,5-Trimethylbenzene


51.9 50.0 NSL0918-01 104%ND 912161653 - 137ug/L 12/10/09 09:22Vinyl chloride

59.1 50.0 NSL0918-01 118%ND 912161662 - 167ug/L 12/10/09 09:22o-Xylene

119 100 NSL0918-01 119%ND 912161669 - 155ug/L 12/10/09 09:22m,p-Xylene

178 150 NSL0918-01 118%ND 912161668 - 158ug/L 12/10/09 09:22Xylenes, total

32.6 25.0 NSL0918-01 Surrogate: 1,2-Dichloroethane-d4 130% 912161663 - 140ug/L 12/10/09 09:22

29.0 25.0 NSL0918-01 Surrogate: Dibromofluoromethane 116% 912161673 - 131ug/L 12/10/09 09:22

23.9 25.0 NSL0918-01 Surrogate: Toluene-d8 96% 912161680 - 120ug/L 12/10/09 09:22

22.9 25.0 NSL0918-01 Surrogate: 4-Bromofluorobenzene 91% 912161679 - 125ug/L 12/10/09 09:22

9121711-MS112700 12500 NSL1079-01 102%ND 912171129 - 181mg/kg wet 12/14/09 07:24Acetone

2380 2500 NSL1079-01 95%ND 912171142 - 141mg/kg wet 12/14/09 07:24Benzene

2630 2500 NSL1079-01 105%ND 912171119 - 154mg/kg wet 12/14/09 07:24Bromobenzene

2250 2500 NSL1079-01 90%ND 912171141 - 146mg/kg wet 12/14/09 07:24Bromochloromethane

2460 2500 NSL1079-01 99%ND 912171132 - 155mg/kg wet 12/14/09 07:24Bromodichloromethane

2550 2500 NSL1079-01 102%ND 912171110 - 155mg/kg wet 12/14/09 07:24Bromoform

Page 48 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

Analyte Units



Target

Range


Q

Analyzed

Date/Time

Sample

SpikedBatch


9121711-MS12370 2500 NSL1079-01 95%ND 912171110 - 199mg/kg wet 12/14/09 07:24Bromomethane

12300 12500 NSL1079-01 98%ND 912171138 - 161mg/kg wet 12/14/09 07:242-Butanone

2700 2500 NSL1079-01 108%ND 912171110 - 170mg/kg wet 12/14/09 07:24sec-Butylbenzene

2690 2500 NSL1079-01 108%ND 912171110 - 183mg/kg wet 12/14/09 07:24n-Butylbenzene

2670 2500 NSL1079-01 107%ND 912171111 - 165mg/kg wet 12/14/09 07:24tert-Butylbenzene

2300 2500 NSL1079-01 92%ND 912171150 - 136mg/kg wet 12/14/09 07:24Carbon disulfide

2590 2500 NSL1079-01 104%ND 912171130 - 159mg/kg wet 12/14/09 07:24Carbon Tetrachloride

2560 2500 NSL1079-01 102%ND 912171125 - 151mg/kg wet 12/14/09 07:24Chlorobenzene

2620 2500 NSL1079-01 105%ND 912171127 - 150mg/kg wet 12/14/09 07:24Chlorodibromomethane

2200 2500 NSL1079-01 88%ND 912171115 - 197mg/kg wet 12/14/09 07:24Chloroethane

2440 2500 NSL1079-01 98%ND 912171133 - 148mg/kg wet 12/14/09 07:24Chloroform

1840 2500 NSL1079-01 73%ND 912171110 - 166mg/kg wet 12/14/09 07:24Chloromethane

2800 2500 NSL1079-01 112%ND 912171125 - 166mg/kg wet 12/14/09 07:242-Chlorotoluene


2630 2500 NSL1079-01 105%ND 912171110 - 167mg/kg wet 12/14/09 07:241,2-Dibromo-3-chloropropane

2790 2500 NSL1079-01 112%ND 912171130 - 155mg/kg wet 12/14/09 07:241,2-Dibromoethane (EDB)

2410 2500 NSL1079-01 96%ND 912171130 - 149mg/kg wet 12/14/09 07:24Dibromomethane

2610 2500 NSL1079-01 100%122 912171110 - 170mg/kg wet 12/14/09 07:241,4-Dichlorobenzene

2700 2500 NSL1079-01 108%ND 912171110 - 173mg/kg wet 12/14/09 07:241,3-Dichlorobenzene

2810 2500 NSL1079-01 110%52.5 912171110 - 168mg/kg wet 12/14/09 07:241,2-Dichlorobenzene

1240 2500 NSL1079-01 50%ND 912171110 - 188mg/kg wet 12/14/09 07:24Dichlorodifluoromethane

2370 2500 NSL1079-01 95%ND 912171151 - 135mg/kg wet 12/14/09 07:241,1-Dichloroethane


3360 2500 NSL1079-01 112%548 912171132 - 150mg/kg wet 12/14/09 07:24cis-1,2-Dichloroethene

2570 2500 NSL1079-01 103%ND 912171146 - 141mg/kg wet 12/14/09 07:241,1-Dichloroethene

2450 2500 NSL1079-01 98%ND 912171141 - 146mg/kg wet 12/14/09 07:24trans-1,2-Dichloroethene

1140 2500 NSL1079-01 46%ND 912171135 - 148mg/kg wet 12/14/09 07:241,3-Dichloropropane



2780 2500 NSL1079-01 111%ND 912171123 - 152mg/kg wet 12/14/09 07:24cis-1,3-Dichloropropene

2380 2500 NSL1079-01 95%ND 912171124 - 151mg/kg wet 12/14/09 07:24trans-1,3-Dichloropropene

2530 2500 NSL1079-01 101%ND 912171140 - 151mg/kg wet 12/14/09 07:241,1-Dichloropropene

2870 2500 NSL1079-01 115%ND 912171121 - 165mg/kg wet 12/14/09 07:24Ethylbenzene

4020 2500 NSL1079-01 161%ND 912171110 - 173mg/kg wet 12/14/09 07:24Hexachlorobutadiene

8190 12500 NSL1079-01 66%ND 912171113 - 174mg/kg wet 12/14/09 07:242-Hexanone

2660 2500 NSL1079-01 106%ND 912171120 - 139mg/kg wet 12/14/09 07:24Isopropylbenzene

2570 2500 NSL1079-01 103%ND 912171110 - 164mg/kg wet 12/14/09 07:24p-Isopropyltoluene

Page 49 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

Analyte Units



Target

Range


Q

Analyzed

Date/Time

Sample

SpikedBatch


9121711-MS12400 2500 NSL1079-01 96%ND 912171134 - 154mg/kg wet 12/14/09 07:24Methyl tert-Butyl Ether

2340 2500 NSL1079-01 94%ND 912171136 - 163mg/kg wet 12/14/09 07:24Methylene Chloride

13700 12500 NSL1079-01 110%ND 912171119 - 176mg/kg wet 12/14/09 07:244-Methyl-2-pentanone

3400 2500 NSL1079-01 136%ND 912171110 - 160mg/kg wet 12/14/09 07:24Naphthalene

2870 2500 NSL1079-01 115%ND 912171116 - 174mg/kg wet 12/14/09 07:24n-Propylbenzene

2560 2500 NSL1079-01 102%ND 912171110 - 177mg/kg wet 12/14/09 07:24Styrene

2780 2500 NSL1079-01 111%ND 912171131 - 150mg/kg wet 12/14/09 07:241,1,1,2-Tetrachloroethane


2680 2500 NSL1079-01 107%ND 912171145 - 145mg/kg wet 12/14/09 07:24Toluene

3740 2500 NSL1079-01 150%ND 912171110 - 182mg/kg wet 12/14/09 07:241,2,3-Trichlorobenzene

4430 2500 NSL1079-01 140%930 912171110 - 175mg/kg wet 12/14/09 07:241,2,4-Trichlorobenzene

2630 2500 NSL1079-01 105%ND 912171143 - 145mg/kg wet 12/14/09 07:241,1,2-Trichloroethane


2130 2500 NSL1079-01 85%ND 912171125 - 174mg/kg wet 12/14/09 07:24Trichlorofluoromethane

2440 2500 NSL1079-01 98%ND 912171110 - 152mg/kg wet 12/14/09 07:241,2,3-Trichloropropane

2570 2500 NSL1079-01 103%ND 912171138 - 148mg/kg wet 12/14/09 07:241,3,5-Trimethylbenzene


2090 2500 NSL1079-01 83%ND 912171132 - 163mg/kg wet 12/14/09 07:24Vinyl chloride

8390 7500 NSL1079-01 110%113 912171131 - 159mg/kg wet 12/14/09 07:24Xylenes, total






52.7 50.0 NSL1340-04 105%0.338 912223442 - 141ug/kg 12/12/09 23:44Benzene





62.0 50.0 NSL1340-04 123%0.687 912223410 - 199ug/kg 12/12/09 23:44Bromomethane

308 250 NSL1340-04 120%7.87 912223438 - 161ug/kg 12/12/09 23:442-Butanone

53.2 50.0 NSL1340-04 106%ND 912223410 - 170ug/kg 12/12/09 23:44sec-Butylbenzene




Page 50 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

Analyte Units



Target

Range


Q

Analyzed

Date/Time

Sample

SpikedBatch


9122234-MS155.1 50.0 NSL1340-04 110%ND 912223430 - 159ug/kg 12/12/09 23:44Carbon Tetrachloride

























46.9 50.0 NSL1340-04 94%ND 912223440 - 151ug/kg 12/12/09 23:441,1-Dichloropropene








282 250 NSL1340-04 113%ND 912223419 - 176ug/kg 12/12/09 23:444-Methyl-2-pentanone



2.44 50.0 NSL1340-04M8 5%ND 912223410 - 177ug/kg 12/12/09 23:44Styrene

Page 51 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913

Analyte Units



Target

Range


Q

Analyzed

Date/Time

Sample

SpikedBatch


9122234-MS157.1 50.0 NSL1340-04 114%ND 912223431 - 150ug/kg 12/12/09 23:441,1,1,2-Tetrachloroethane



51.6 50.0 NSL1340-04 102%0.464 912223445 - 145ug/kg 12/12/09 23:44Toluene




55.8 50.0 NSL1340-04 110%0.513 912223439 - 148ug/kg 12/12/09 23:441,1,1-Trichloroethane







174 150 NSL1340-04 115%0.261 912223431 - 159ug/kg 12/12/09 23:44Xylenes, total





Page 52 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


Sample


Matrix Spike Dup


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121162-MSD19.23 309 2 50 9121162 NSL1304-04 250 120%ug/kg 29 - 181 12/14/09 22:40Acetone

ND 50.8 18 50 9121162 NSL1304-04 50.0 102%ug/kg 42 - 141 12/14/09 22:40Benzene

ND 49.2 17 50 9121162 NSL1304-04 50.0 98%ug/kg 19 - 154 12/14/09 22:40Bromobenzene

ND 49.0 5 50 9121162 NSL1304-04 50.0 98%ug/kg 41 - 146 12/14/09 22:40Bromochloromethane

ND 50.9 13 50 9121162 NSL1304-04 50.0 102%ug/kg 32 - 155 12/14/09 22:40Bromodichloromethane

ND 46.4 8 43 9121162 NSL1304-04 50.0 93%ug/kg 10 - 155 12/14/09 22:40Bromoform

ND 45.2 11 46 9121162 NSL1304-04 50.0 90%ug/kg 10 - 199 12/14/09 22:40Bromomethane

ND 279 6 50 9121162 NSL1304-04 250 112%ug/kg 38 - 161 12/14/09 22:402-Butanone

ND 54.0 20 50 9121162 NSL1304-04 50.0 108%ug/kg 10 - 170 12/14/09 22:40sec-Butylbenzene

ND 54.8 18 50 9121162 NSL1304-04 50.0 110%ug/kg 10 - 183 12/14/09 22:40n-Butylbenzene

ND 51.1 19 50 9121162 NSL1304-04 50.0 102%ug/kg 11 - 165 12/14/09 22:40tert-Butylbenzene

ND 51.3 24 48 9121162 NSL1304-04 50.0 103%ug/kg 50 - 136 12/14/09 22:40Carbon disulfide

ND 47.6 21 44 9121162 NSL1304-04 50.0 95%ug/kg 30 - 159 12/14/09 22:40Carbon Tetrachloride

ND 53.3 16 50 9121162 NSL1304-04 50.0 107%ug/kg 25 - 151 12/14/09 22:40Chlorobenzene

ND 47.3 9 48 9121162 NSL1304-04 50.0 95%ug/kg 27 - 150 12/14/09 22:40Chlorodibromomethane

ND 48.5 21 50 9121162 NSL1304-04 50.0 97%ug/kg 15 - 197 12/14/09 22:40Chloroethane

5.86 50.1 12 50 9121162 NSL1304-04B 50.0 88%ug/kg 33 - 148 12/14/09 22:40Chloroform

ND 43.1 17 44 9121162 NSL1304-04 50.0 86%ug/kg 10 - 166 12/14/09 22:40Chloromethane

ND 51.3 16 50 9121162 NSL1304-04 50.0 103%ug/kg 25 - 166 12/14/09 22:402-Chlorotoluene


ND 47.2 0.9 45 9121162 NSL1304-04 50.0 94%ug/kg 10 - 167 12/14/09 22:401,2-Dibromo-3-chloropropane

ND 52.8 4 45 9121162 NSL1304-04 50.0 106%ug/kg 30 - 155 12/14/09 22:401,2-Dibromoethane (EDB)

ND 48.2 1 50 9121162 NSL1304-04 50.0 96%ug/kg 30 - 149 12/14/09 22:40Dibromomethane

ND 52.3 12 50 9121162 NSL1304-04 50.0 105%ug/kg 10 - 170 12/14/09 22:401,4-Dichlorobenzene



ND 30.7 16 50 9121162 NSL1304-04 50.0 61%ug/kg 10 - 188 12/14/09 22:40Dichlorodifluoromethane

ND 50.2 19 50 9121162 NSL1304-04 50.0 100%ug/kg 51 - 135 12/14/09 22:401,1-Dichloroethane


ND 49.0 18 50 9121162 NSL1304-04 50.0 98%ug/kg 32 - 150 12/14/09 22:40cis-1,2-Dichloroethene

ND 50.0 25 50 9121162 NSL1304-04 50.0 100%ug/kg 46 - 141 12/14/09 22:401,1-Dichloroethene

ND 48.6 19 40 9121162 NSL1304-04 50.0 97%ug/kg 41 - 146 12/14/09 22:40trans-1,2-Dichloroethene

ND 51.8 7 42 9121162 NSL1304-04 50.0 104%ug/kg 35 - 148 12/14/09 22:401,3-Dichloropropane



ND 51.1 14 50 9121162 NSL1304-04 50.0 102%ug/kg 23 - 152 12/14/09 22:40cis-1,3-Dichloropropene

ND 52.1 12 48 9121162 NSL1304-04 50.0 104%ug/kg 24 - 151 12/14/09 22:40trans-1,3-Dichloropropene

ND 48.7 23 50 9121162 NSL1304-04 50.0 97%ug/kg 40 - 151 12/14/09 22:401,1-Dichloropropene

ND 52.6 19 50 9121162 NSL1304-04 50.0 105%ug/kg 21 - 165 12/14/09 22:40Ethylbenzene

ND 53.0 15 50 9121162 NSL1304-04 50.0 106%ug/kg 10 - 173 12/14/09 22:40Hexachlorobutadiene

ND 288 5 50 9121162 NSL1304-04 250 115%ug/kg 13 - 174 12/14/09 22:402-Hexanone

Page 53 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


Sample


Matrix Spike Dup - Cont.


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121162-MSD1ND 52.7 21 50 9121162 NSL1304-04 50.0 105%ug/kg 20 - 139 12/14/09 22:40Isopropylbenzene

ND 52.0 18 50 9121162 NSL1304-04 50.0 104%ug/kg 10 - 164 12/14/09 22:40p-Isopropyltoluene

ND 42.5 6 50 9121162 NSL1304-04 50.0 85%ug/kg 34 - 154 12/14/09 22:40Methyl tert-Butyl Ether

6.22 56.4 11 50 9121162 NSL1304-04 50.0 100%ug/kg 36 - 163 12/14/09 22:40Methylene Chloride

ND 258 5 45 9121162 NSL1304-04 250 103%ug/kg 19 - 176 12/14/09 22:404-Methyl-2-pentanone

ND 51.0 9 50 9121162 NSL1304-04 50.0 102%ug/kg 10 - 160 12/14/09 22:40Naphthalene

ND 52.3 16 50 9121162 NSL1304-04 50.0 105%ug/kg 16 - 174 12/14/09 22:40n-Propylbenzene

ND 38.0 26 50 9121162 NSL1304-04 50.0 76%ug/kg 10 - 177 12/14/09 22:40Styrene

ND 54.0 14 50 9121162 NSL1304-04 50.0 108%ug/kg 31 - 150 12/14/09 22:401,1,1,2-Tetrachloroethane

ND 55.1 0.9 45 9121162 NSL1304-04 50.0 110%ug/kg 27 - 163 12/14/09 22:401,1,2,2-Tetrachloroethane

5.52 58.0 24 50 9121162 NSL1304-04 50.0 105%ug/kg 33 - 155 12/14/09 22:40Tetrachloroethene

ND 55.6 18 50 9121162 NSL1304-04 50.0 111%ug/kg 45 - 145 12/14/09 22:40Toluene

ND 52.4 11 50 9121162 NSL1304-04 50.0 105%ug/kg 10 - 182 12/14/09 22:401,2,3-Trichlorobenzene


ND 54.4 8 50 9121162 NSL1304-04 50.0 109%ug/kg 43 - 145 12/14/09 22:401,1,2-Trichloroethane


ND 51.1 22 50 9121162 NSL1304-04 50.0 102%ug/kg 39 - 150 12/14/09 22:40Trichloroethene

ND 41.1 21 47 9121162 NSL1304-04 50.0 82%ug/kg 25 - 174 12/14/09 22:40Trichlorofluoromethane

ND 48.6 8 47 9121162 NSL1304-04 50.0 97%ug/kg 10 - 152 12/14/09 22:401,2,3-Trichloropropane

ND 51.5 17 50 9121162 NSL1304-04 50.0 103%ug/kg 38 - 148 12/14/09 22:401,3,5-Trimethylbenzene


ND 45.8 27 39 9121162 NSL1304-04 50.0 92%ug/kg 32 - 163 12/14/09 22:40Vinyl chloride

ND 154 19 50 9121162 NSL1304-04 150 103%ug/kg 31 - 159 12/14/09 22:40Xylenes, total

45.6 9121162 NSL1304-04 50.0 91%Surrogate: 1,2-Dichloroethane-d4 ug/kg 67 - 138 12/14/09 22:40

47.5 9121162 NSL1304-04 50.0 95%Surrogate: Dibromofluoromethane ug/kg 75 - 125 12/14/09 22:40

56.3 9121162 NSL1304-04 50.0 113%Surrogate: Toluene-d8 ug/kg 76 - 129 12/14/09 22:40

45.8 9121162 NSL1304-04 50.0 92%Surrogate: 4-Bromofluorobenzene ug/kg 67 - 147 12/14/09 22:40

9121616-MSD1ND 298 9 31 9121616 NSL0918-01 250 119%ug/L 56 - 150 12/10/09 09:49Acetone

ND 59.3 6 12 9121616 NSL0918-01 50.0 119%ug/L 65 - 151 12/10/09 09:49Benzene

ND 51.6 5 23 9121616 NSL0918-01 50.0 103%ug/L 69 - 142 12/10/09 09:49Bromobenzene

ND 62.7 4 32 9121616 NSL0918-01 50.0 125%ug/L 64 - 154 12/10/09 09:49Bromochloromethane

ND 70.5 5 13 9121616 NSL0918-01M7 50.0 141%ug/L 75 - 138 12/10/09 09:49Bromodichloromethane

ND 61.5 6 18 9121616 NSL0918-01 50.0 123%ug/L 55 - 153 12/10/09 09:49Bromoform

ND 64.3 15 50 9121616 NSL0918-01 50.0 129%ug/L 13 - 176 12/10/09 09:49Bromomethane

ND 325 10 37 9121616 NSL0918-01 250 130%ug/L 45 - 164 12/10/09 09:492-Butanone

ND 58.1 5 21 9121616 NSL0918-01 50.0 116%ug/L 68 - 159 12/10/09 09:49sec-Butylbenzene

ND 59.8 4 11 9121616 NSL0918-01 50.0 120%ug/L 67 - 151 12/10/09 09:49n-Butylbenzene

ND 57.4 4 20 9121616 NSL0918-01 50.0 115%ug/L 73 - 153 12/10/09 09:49tert-Butylbenzene

2.47 66.8 7 28 9121616 NSL0918-01 50.0 129%ug/L 33 - 187 12/10/09 09:49Carbon disulfide

Page 54 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


Sample




Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121616-MSD1ND 82.8 4 26 9121616 NSL0918-01M7 50.0 166%ug/L 64 - 157 12/10/09 09:49Carbon Tetrachloride

ND 57.5 4 11 9121616 NSL0918-01 50.0 115%ug/L 78 - 136 12/10/09 09:49Chlorobenzene

ND 62.4 4 16 9121616 NSL0918-01 50.0 125%ug/L 64 - 145 12/10/09 09:49Chlorodibromomethane

ND 57.4 7 35 9121616 NSL0918-01 50.0 115%ug/L 48 - 159 12/10/09 09:49Chloroethane

ND 73.9 5 32 9121616 NSL0918-01M7 50.0 148%ug/L 72 - 145 12/10/09 09:49Chloroform

ND 56.2 10 34 9121616 NSL0918-01 50.0 112%ug/L 10 - 194 12/10/09 09:49Chloromethane

ND 53.2 4 22 9121616 NSL0918-01 50.0 106%ug/L 66 - 155 12/10/09 09:492-Chlorotoluene


ND 53.5 21 21 9121616 NSL0918-01 50.0 107%ug/L 49 - 162 12/10/09 09:491,2-Dibromo-3-chloropropane

ND 63.1 6 10 9121616 NSL0918-01 50.0 126%ug/L 70 - 152 12/10/09 09:491,2-Dibromoethane (EDB)

ND 69.2 3 11 9121616 NSL0918-01 50.0 138%ug/L 75 - 141 12/10/09 09:49Dibromomethane

ND 53.3 5 10 9121616 NSL0918-01 50.0 107%ug/L 75 - 135 12/10/09 09:491,4-Dichlorobenzene



ND 47.9 6 32 9121616 NSL0918-01 50.0 96%ug/L 23 - 159 12/10/09 09:49Dichlorodifluoromethane

ND 64.8 6 34 9121616 NSL0918-01 50.0 130%ug/L 64 - 154 12/10/09 09:491,1-Dichloroethane

ND 80.0 2 25 9121616 NSL0918-01M7 50.0 160%ug/L 72 - 137 12/10/09 09:491,2-Dichloroethane

ND 69.8 5 32 9121616 NSL0918-01 50.0 140%ug/L 57 - 154 12/10/09 09:49cis-1,2-Dichloroethene

ND 66.9 10 31 9121616 NSL0918-01 50.0 134%ug/L 34 - 151 12/10/09 09:491,1-Dichloroethene

ND 69.3 7 32 9121616 NSL0918-01 50.0 139%ug/L 57 - 157 12/10/09 09:49trans-1,2-Dichloroethene

ND 61.1 6 20 9121616 NSL0918-01 50.0 122%ug/L 71 - 137 12/10/09 09:491,3-Dichloropropane



ND 60.6 7 35 9121616 NSL0918-01 50.0 121%ug/L 56 - 156 12/10/09 09:49cis-1,3-Dichloropropene

ND 64.9 6 26 9121616 NSL0918-01 50.0 130%ug/L 47 - 157 12/10/09 09:49trans-1,3-Dichloropropene

ND 68.7 5 18 9121616 NSL0918-01 50.0 137%ug/L 70 - 155 12/10/09 09:491,1-Dichloropropene

ND 61.6 5 12 9121616 NSL0918-01 50.0 123%ug/L 68 - 157 12/10/09 09:49Ethylbenzene

ND 69.5 15 21 9121616 NSL0918-01B 50.0 139%ug/L 47 - 173 12/10/09 09:49Hexachlorobutadiene

ND 337 8 20 9121616 NSL0918-01 250 135%ug/L 57 - 154 12/10/09 09:492-Hexanone

ND 64.4 4 15 9121616 NSL0918-01 50.0 129%ug/L 69 - 139 12/10/09 09:49Isopropylbenzene

ND 57.6 5 18 9121616 NSL0918-01 50.0 115%ug/L 69 - 151 12/10/09 09:49p-Isopropyltoluene

ND 60.3 11 32 9121616 NSL0918-01 50.0 121%ug/L 56 - 152 12/10/09 09:49Methyl tert-Butyl Ether

ND 63.4 7 36 9121616 NSL0918-01 50.0 127%ug/L 71 - 136 12/10/09 09:49Methylene Chloride

ND 315 7 35 9121616 NSL0918-01 250 126%ug/L 62 - 159 12/10/09 09:494-Methyl-2-pentanone

ND 65.6 57 30 9121616 NSL0918-01R2 50.0 131%ug/L 56 - 161 12/10/09 09:49Naphthalene

ND 54.6 4 23 9121616 NSL0918-01 50.0 109%ug/L 61 - 167 12/10/09 09:49n-Propylbenzene

ND 61.3 3 29 9121616 NSL0918-01 50.0 123%ug/L 69 - 150 12/10/09 09:49Styrene

ND 68.3 4 11 9121616 NSL0918-01 50.0 137%ug/L 80 - 140 12/10/09 09:491,1,1,2-Tetrachloroethane


3.00 67.0 6 16 9121616 NSL0918-01 50.0 128%ug/L 63 - 155 12/10/09 09:49Tetrachloroethene

ND 57.6 6 35 9121616 NSL0918-01 50.0 115%ug/L 61 - 153 12/10/09 09:49Toluene

Page 55 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


Sample




Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121616-MSD1ND 82.6 66 28 9121616 NSL0918-01R2, M7, 50.0 165%ug/L 57 - 155 12/10/09 09:491,2,3-Trichlorobenzene

ND 72.7 33 23 9121616 NSL0918-01R2 50.0 145%ug/L 64 - 147 12/10/09 09:491,2,4-Trichlorobenzene

ND 58.6 2 21 9121616 NSL0918-01 50.0 117%ug/L 74 - 138 12/10/09 09:491,1,2-Trichloroethane


6.88 72.6 6 11 9121616 NSL0918-01 50.0 131%ug/L 74 - 139 12/10/09 09:49Trichloroethene

ND 70.0 5 33 9121616 NSL0918-01 50.0 140%ug/L 53 - 149 12/10/09 09:49Trichlorofluoromethane

ND 49.7 6 25 9121616 NSL0918-01 50.0 99%ug/L 49 - 148 12/10/09 09:491,2,3-Trichloropropane

ND 56.5 4 21 9121616 NSL0918-01 50.0 113%ug/L 67 - 151 12/10/09 09:491,3,5-Trimethylbenzene


ND 57.3 10 32 9121616 NSL0918-01 50.0 115%ug/L 53 - 137 12/10/09 09:49Vinyl chloride

ND 61.5 4 27 9121616 NSL0918-01 50.0 123%ug/L 62 - 167 12/10/09 09:49o-Xylene

ND 124 5 16 9121616 NSL0918-01 100 124%ug/L 69 - 155 12/10/09 09:49m,p-Xylene

ND 186 4 18 9121616 NSL0918-01 150 124%ug/L 68 - 158 12/10/09 09:49Xylenes, total

32.6 9121616 NSL0918-01 25.0 131%Surrogate: 1,2-Dichloroethane-d4 ug/L 63 - 140 12/10/09 09:49

28.9 9121616 NSL0918-01 25.0 115%Surrogate: Dibromofluoromethane ug/L 73 - 131 12/10/09 09:49

24.1 9121616 NSL0918-01 25.0 96%Surrogate: Toluene-d8 ug/L 80 - 120 12/10/09 09:49

23.1 9121616 NSL0918-01 25.0 92%Surrogate: 4-Bromofluorobenzene ug/L 79 - 125 12/10/09 09:49

9121711-MSD1ND 12700 0.3 50 9121711 NSL1079-01 12500 102%mg/kg wet 29 - 181 12/14/09 07:52Acetone

ND 2410 2 50 9121711 NSL1079-01 2500 97%mg/kg wet 42 - 141 12/14/09 07:52Benzene

ND 2720 3 50 9121711 NSL1079-01 2500 109%mg/kg wet 19 - 154 12/14/09 07:52Bromobenzene

ND 2320 3 50 9121711 NSL1079-01 2500 93%mg/kg wet 41 - 146 12/14/09 07:52Bromochloromethane

ND 2490 1 50 9121711 NSL1079-01 2500 100%mg/kg wet 32 - 155 12/14/09 07:52Bromodichloromethane

ND 2590 1 43 9121711 NSL1079-01 2500 104%mg/kg wet 10 - 155 12/14/09 07:52Bromoform

ND 2400 1 46 9121711 NSL1079-01 2500 96%mg/kg wet 10 - 199 12/14/09 07:52Bromomethane

ND 12700 3 50 9121711 NSL1079-01 12500 101%mg/kg wet 38 - 161 12/14/09 07:522-Butanone

ND 2790 3 50 9121711 NSL1079-01 2500 111%mg/kg wet 10 - 170 12/14/09 07:52sec-Butylbenzene

ND 2790 4 50 9121711 NSL1079-01 2500 112%mg/kg wet 10 - 183 12/14/09 07:52n-Butylbenzene

ND 2740 3 50 9121711 NSL1079-01 2500 110%mg/kg wet 11 - 165 12/14/09 07:52tert-Butylbenzene

ND 2370 3 48 9121711 NSL1079-01 2500 95%mg/kg wet 50 - 136 12/14/09 07:52Carbon disulfide

ND 2580 0.3 44 9121711 NSL1079-01 2500 103%mg/kg wet 30 - 159 12/14/09 07:52Carbon Tetrachloride

ND 2580 1 50 9121711 NSL1079-01 2500 103%mg/kg wet 25 - 151 12/14/09 07:52Chlorobenzene

ND 2640 0.7 48 9121711 NSL1079-01 2500 106%mg/kg wet 27 - 150 12/14/09 07:52Chlorodibromomethane

ND 2270 3 50 9121711 NSL1079-01 2500 91%mg/kg wet 15 - 197 12/14/09 07:52Chloroethane

ND 2470 1 50 9121711 NSL1079-01 2500 99%mg/kg wet 33 - 148 12/14/09 07:52Chloroform

ND 1800 2 44 9121711 NSL1079-01 2500 72%mg/kg wet 10 - 166 12/14/09 07:52Chloromethane

ND 2880 3 50 9121711 NSL1079-01 2500 115%mg/kg wet 25 - 166 12/14/09 07:522-Chlorotoluene


ND 2730 4 45 9121711 NSL1079-01 2500 109%mg/kg wet 10 - 167 12/14/09 07:521,2-Dibromo-3-chloropropane

ND 2850 2 45 9121711 NSL1079-01 2500 114%mg/kg wet 30 - 155 12/14/09 07:521,2-Dibromoethane (EDB)

Page 56 of 61


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-2

Received:


12/08/09 16:00

NSL0913


Sample




Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121711-MSD1ND 2460 2 50 9121711 NSL1079-01 2500 99%mg/kg wet 30 - 149 12/14/09 07:52Dibromomethane

122 2690 3 50 9121711 NSL1079-01 2500 103%mg/kg wet 10 - 170 12/14/09 07:521,4-Dichlorobenzene

ND 2800 4 50 9121711 NSL1079-01 2500 112%mg/kg wet 10 - 173 12/14/09 07:521,3-Dichlorobenzene

52.5 2910 4 50 9121711 NSL1079-01 2500 114%mg/kg wet 10 - 168 12/14/09 07:521,2-Dichlorobenzene

ND 1220 2 50 9121711 NSL1079-01 2500 49%mg/kg wet 10 - 188 12/14/09 07:52Dichlorodifluoromethane

ND 2440 3 50 9121711 NSL1079-01 2500 97%mg/kg wet 51 - 135 12/14/09 07:521,1-Dichloroethane


548 3420 2 50 9121711 NSL1079-01 2500 115%mg/kg wet 32 - 150 12/14/09 07:52cis-1,2-Dichloroethene

ND 2610 2 50 9121711 NSL1079-01 2500 105%mg/kg wet 46 - 141 12/14/09 07:521,1-Dichloroethene

ND 2490 2 40 9121711 NSL1079-01 2500 100%mg/kg wet 41 - 146 12/14/09 07:52trans-1,2-Dichloroethene

ND 1120 2 42 9121711 NSL1079-01 2500 45%mg/kg wet 35 - 148 12/14/09 07:521,3-Dichloropropane



ND 2860 3 50 9121711 NSL1079-01 2500 114%mg/kg wet 23 - 152 12/14/09 07:52cis-1,3-Dichloropropene

ND 2410 1 48 9121711 NSL1079-01 2500 96%mg/kg wet 24 - 151 12/14/09 07:52trans-1,3-Dichloropropene

ND 2560 1 50 9121711 NSL1079-01 2500 103%mg/kg wet 40 - 151 12/14/09 07:521,1-Dichloropropene

ND 2880 0.3 50 9121711 NSL1079-01 2500 115%mg/kg wet 21 - 165 12/14/09 07:52Ethylbenzene

ND 4190 4 50 9121711 NSL1079-01 2500 168%mg/kg wet 10 - 173 12/14/09 07:52Hexachlorobutadiene

ND 10900 28 50 9121711 NSL1079-01 12500 87%mg/kg wet 13 - 174 12/14/09 07:522-Hexanone

ND 2670 0.2 50 9121711 NSL1079-01 2500 107%mg/kg wet 20 - 139 12/14/09 07:52Isopropylbenzene

ND 2680 4 50 9121711 NSL1079-01 2500 107%mg/kg wet 10 - 164 12/14/09 07:52p-Isopropyltoluene

ND 2530 5 50 9121711 NSL1079-01 2500 101%mg/kg wet 34 - 154 12/14/09 07:52Methyl tert-Butyl Ether

ND 2430 4 50 9121711 NSL1079-01 2500 97%mg/kg wet 36 - 163 12/14/09 07:52Methylene Chloride

ND 14200 4 45 9121711 NSL1079-01 12500 114%mg/kg wet 19 - 176 12/14/09 07:524-Methyl-2-pentanone

ND 3390 0.1 50 9121711 NSL1079-01 2500 136%mg/kg wet 10 - 160 12/14/09 07:52Naphthalene

ND 2950 3 50 9121711 NSL1079-01 2500 118%mg/kg wet 16 - 174 12/14/09 07:52n-Propylbenzene

ND 2590 1 50 9121711 NSL1079-01 2500 104%mg/kg wet 10 - 177 12/14/09 07:52Styrene

ND 2840 2 50 9121711 NSL1079-01 2500 113%mg/kg wet 31 - 150 12/14/09 07:521,1,1,2-Tetrachloroethane


ND 2680 0.09 50 9121711 NSL1079-01 2500 107%mg/kg wet 45 - 145 12/14/09 07:52Toluene

ND 3830 2 50 9121711 NSL1079-01 2500 153%mg/kg wet 10 - 182 12/14/09 07:521,2,3-Trichlorobenzene

930 5100 14 50 9121711 NSL1079-01 2500 167%mg/kg wet 10 - 175 12/14/09 07:521,2,4-Trichlorobenzene

ND 2710 3 50 9121711 NSL1079-01 2500 108%mg/kg wet 43 - 145 12/14/09 07:521,1,2-Trichloroethane

ND 2530 0.2 41 9121711 NSL1079-01 2500 101%mg/kg wet 39 - 148 12/14/09 07:521,1,1-Trichloroethane

ND 2140 0.4 47 9121711 NSL1079-01 2500 85%mg/kg wet 25 - 174 12/14/09 07:52Trichlorofluoromethane

ND 2540 4 47 9121711 NSL1079-01 2500 102%mg/kg wet 10 - 152 12/14/09 07:521,2,3-Trichloropropane

ND 2660 3 50 9121711 NSL1079-01 2500 106%mg/kg wet 38 - 148 12/14/09 07:521,3,5-Trimethylbenzene


ND 2150 3 39 9121711 NSL1079-01 2500 86%mg/kg wet 32 - 163 12/14/09 07:52Vinyl chloride

113 8410 0.2 50 9121711 NSL1079-01 7500 111%mg/kg wet 31 - 159 12/14/09 07:52Xylenes, total


Page 57 of 61


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Sample




Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121711-MSD125.9 9121711 NSL1079-01 25.0 104%Surrogate: Dibromofluoromethane ug/kg 75 - 125 12/14/09 07:52



9122234-MSD169.6 34.5 169 50 9122234 NSL1340-04R2, M8 250 -14%ug/kg 29 - 181 12/13/09 00:13Acetone

0.338 48.9 7 50 9122234 NSL1340-04 50.0 97%ug/kg 42 - 141 12/13/09 00:13Benzene

ND 48.8 0.1 50 9122234 NSL1340-04 50.0 98%ug/kg 19 - 154 12/13/09 00:13Bromobenzene



ND 42.8 0.7 43 9122234 NSL1340-04 50.0 86%ug/kg 10 - 155 12/13/09 00:13Bromoform

0.687 59.5 4 46 9122234 NSL1340-04 50.0 118%ug/kg 10 - 199 12/13/09 00:13Bromomethane

7.87 276 11 50 9122234 NSL1340-04 250 107%ug/kg 38 - 161 12/13/09 00:132-Butanone












ND 49.2 0.9 50 9122234 NSL1340-04 50.0 98%ug/kg 19 - 163 12/13/09 00:134-Chlorotoluene

ND 44.4 3 45 9122234 NSL1340-04 50.0 89%ug/kg 10 - 167 12/13/09 00:131,2-Dibromo-3-chloropropane
















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Sample




Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9122234-MSD1ND 51.6 1 48 9122234 NSL1340-04 50.0 103%ug/kg 24 - 151 12/13/09 00:13trans-1,3-Dichloropropene


ND 56.1 0.5 50 9122234 NSL1340-04 50.0 112%ug/kg 21 - 165 12/13/09 00:13Ethylbenzene



ND 50.5 0.7 50 9122234 NSL1340-04 50.0 101%ug/kg 20 - 139 12/13/09 00:13Isopropylbenzene







ND 2.44 0 50 9122234 NSL1340-04M8 50.0 5%ug/kg 10 - 177 12/13/09 00:13Styrene




0.464 54.5 5 50 9122234 NSL1340-04 50.0 108%ug/kg 45 - 145 12/13/09 00:13Toluene




0.513 50.4 10 41 9122234 NSL1340-04 50.0 100%ug/kg 39 - 148 12/13/09 00:131,1,1-Trichloroethane







0.261 170 2 50 9122234 NSL1340-04 150 113%ug/kg 31 - 159 12/13/09 00:13Xylenes, total





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Method Matrix



Soil XN/A XSW846 8260B

Water XN/A XSW846 8260B

SoilSW-846

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B Analyte was detected in the associated Method Blank.

J Analyte detected at a level less than the Reporting Limit (RL) and greater than or equal to the Method Detection Limit (MDL).

Concentrations within this range are estimated.L Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was above the acceptance limits. Analyte not

detected, data not impacted.M7 The MS and/or MSD were above the acceptance limits. See Blank Spike (LCS).

M8 The MS and/or MSD were below the acceptance limits. See Blank Spike (LCS).

MNR No results were reported for the MS/MSD. The sample used for the MS/MSD required dilution due to the sample matrix.

Because of this, the spike compounds were diluted below the detection limit.R2 The RPD exceeded the acceptance limit.

RL1 Reporting limit raised due to sample matrix effects.



Page 61 of 61


December 17, 2009

Client:

Attn:

Work Order:

Project Name:

Project Nbr:

Date Received:

SAP-3

[none]

NSL0906

12/08/09

Sumter, SC 29151



2:36:50PM


NSL0906-01B-16-S 12/04/09 12:00

NSL0906-02B-16-GW 12/04/09 12:10

NSL0906-03B-17-S 12/04/09 13:10

NSL0906-04B-17-GW 12/04/09 13:15

NSL0906-05B-18-S 12/04/09 13:25

NSL0906-06B-18-GW 12/04/09 13:30

NSL0906-07B-19-S 12/04/09 13:55

NSL0906-08B-19-GW 12/04/09 14:00

NSL0906-09B-20-S 12/04/09 14:20

NSL0906-10B-20-GW 12/04/09 14:30










Report Approved By:

Cathy Gartner

Project Management




Page 1 of 56


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Robbin Brown

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NSL0906

ANALYTICAL REPORT

Analyte Result

Analysis


Factor MethodUnits Analyst BatchMDL



% Dry Solids 91224890.50091.0 12/15/09 08:461 SW-846% DEA0.500


Acetone 91224290.05470.434 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.0274

Benzene 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

Bromobenzene RL1 91217110.106ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0354

Bromochloromethane 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.00112

Bromodichloromethane 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000438

Bromoform 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

Bromomethane 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000700

2-Butanone 91224290.0547ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.0186

sec-Butylbenzene RL1 91217110.106ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0354

n-Butylbenzene RL1 91217110.106ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0354

tert-Butylbenzene RL1 91217110.106ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0354

Carbon disulfide 91224290.00547ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

Carbon Tetrachloride 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

Chlorobenzene 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

Chlorodibromomethane 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000416

Chloroethane 91224290.00547ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000460

Chloroform J, B 91224290.002190.00103 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

Chloromethane 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.00109

2-Chlorotoluene RL1 91217110.106ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0354

4-Chlorotoluene RL1 91217110.106ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0354

1,2-Dibromo-3-chloropropane RL1 91217110.264ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.180

1,2-Dibromoethane (EDB) 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000569

Dibromomethane 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

1,4-Dichlorobenzene RL1 91217110.106ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0380



Dichlorodifluoromethane 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.00175

1,1-Dichloroethane 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733


cis-1,2-Dichloroethene 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

1,1-Dichloroethene 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

trans-1,2-Dichloroethene 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

1,3-Dichloropropane 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000493



cis-1,3-Dichloropropene 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

trans-1,3-Dichloropropene 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

Page 2 of 56


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Robbin Brown

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ANALYTICAL REPORT

Analyte Result

Analysis





1,1-Dichloropropene 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

Ethylbenzene 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

Hexachlorobutadiene RL1 91217110.264ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0333

2-Hexanone 91224290.0547ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.0186

Isopropylbenzene 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

p-Isopropyltoluene RL1 91217110.106ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0354

Methyl tert-Butyl Ether 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

Methylene Chloride 91224290.0109ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.00219

4-Methyl-2-pentanone J 91224290.05470.0191 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.00317

Naphthalene RL1 91217110.264ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0898

n-Propylbenzene RL1 91217110.106ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0354

Styrene 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

1,1,1,2-Tetrachloroethane 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

1,1,2,2-Tetrachloroethane RL1 91217110.106ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0354

Tetrachloroethene 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000438

Toluene J 91224290.002190.00170 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000438

1,2,3-Trichlorobenzene RL1 91217110.106ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0486

1,2,4-Trichlorobenzene RL1 91217110.106ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0539

1,1,2-Trichloroethane 91224290.00547ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.00121


Trichloroethene 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000908

Trichlorofluoromethane 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000733

1,2,3-Trichloropropane RL1 91217110.106ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0544

1,3,5-Trimethylbenzene RL1 91217110.106ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0211

1,2,4-Trimethylbenzene RL1 91217110.106ND 12/14/09 00:3450 SW846 8260Bmg/kg dry JJP0.0222

Vinyl chloride 91224290.00219ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.000898

Xylenes, total 91224290.00547ND 12/13/09 17:161 SW846 8260Bmg/kg dry KxC0.00142

Surr: 1,2-Dichloroethane-d4 (67-138%) 85 % 12/13/09 17:16 SW846 8260B KxC 91224291

Surr: 1,2-Dichloroethane-d4 (67-138%) 110 % 12/14/09 00:34 SW846 8260B JJP 912171150

Surr: Dibromofluoromethane (75-125%) 96 % 12/13/09 17:16 SW846 8260B KxC 91224291

Surr: Dibromofluoromethane (75-125%) 103 % 12/14/09 00:34 SW846 8260B JJP 912171150

Surr: Toluene-d8 (76-129%) 103 % 12/13/09 17:16 SW846 8260B KxC 91224291

Surr: Toluene-d8 (76-129%) 112 % 12/14/09 00:34 SW846 8260B JJP 912171150

Surr: 4-Bromofluorobenzene (67-147%) 112 % 12/13/09 17:16 SW846 8260B KxC 91224291

Surr: 4-Bromofluorobenzene (67-147%) 110 % 12/14/09 00:34 SW846 8260B JJP 912171150

Extractable Petroleum Hydrocarbons

Diesel J, QP6 91217274.364.08 12/15/09 03:531 TPH-D/Fingermg/kg dry mrb2.18

Surr: o-Terphenyl (29-141%) 77 % 12/15/09 03:53 TPH-D/Finger mrb 91217271

Page 3 of 56


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Robbin Brown

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NSL0906

ANALYTICAL REPORT

Analyte Result

Analysis





Acetone 912161650.0ND 12/09/09 22:171 SW846 8260Bug/L JJP25.0

Benzene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.410

Bromobenzene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.360

Bromochloromethane 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.470

Bromodichloromethane 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.270

Bromoform 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.430

Bromomethane 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.300

2-Butanone 912161650.0ND 12/09/09 22:171 SW846 8260Bug/L JJP2.10

sec-Butylbenzene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.360

n-Butylbenzene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.310

tert-Butylbenzene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.380

Carbon disulfide 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.360

Carbon Tetrachloride 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.330

Chlorobenzene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.220

Chlorodibromomethane 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.260

Chloroethane 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.460

Chloroform 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.250

Chloromethane J 91216161.000.420 12/09/09 22:171 SW846 8260Bug/L JJP0.390

2-Chlorotoluene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.510


1,2-Dibromo-3-chloropropane 91216165.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.860

1,2-Dibromoethane (EDB) 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.460

Dibromomethane 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.410

1,4-Dichlorobenzene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.430



Dichlorodifluoromethane 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.190

1,1-Dichloroethane 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.340


cis-1,2-Dichloroethene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.330

1,1-Dichloroethene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.220

trans-1,2-Dichloroethene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.330

1,3-Dichloropropane 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.270



cis-1,3-Dichloropropene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.330

trans-1,3-Dichloropropene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.330

1,1-Dichloropropene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.260

Ethylbenzene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.350

Page 4 of 56


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Robbin Brown

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Received:


12/08/09 08:00

NSL0906

ANALYTICAL REPORT

Analyte Result

Analysis





Hexachlorobutadiene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.790

2-Hexanone 912161650.0ND 12/09/09 22:171 SW846 8260Bug/L JJP1.40

Isopropylbenzene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.400

p-Isopropyltoluene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.330

Methyl tert-Butyl Ether 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.320

Methylene Chloride 91216165.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.480

4-Methyl-2-pentanone 912161610.0ND 12/09/09 22:171 SW846 8260Bug/L JJP1.40

Naphthalene 91216165.005.17 12/09/09 22:171 SW846 8260Bug/L JJP0.380

n-Propylbenzene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.390

Styrene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.260

1,1,1,2-Tetrachloroethane 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.200


Tetrachloroethene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.320

Toluene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.350

1,2,3-Trichlorobenzene L 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.270


1,1,2-Trichloroethane 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.320


Trichloroethene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.260

Trichlorofluoromethane 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.220

1,2,3-Trichloropropane 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.470

1,3,5-Trimethylbenzene 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.360


Vinyl chloride 91216161.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.220

Xylenes, total 91216163.00ND 12/09/09 22:171 SW846 8260Bug/L JJP0.730





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Robbin Brown

Project Name:

Work Order:

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Received:


12/08/09 08:00

NSL0906

ANALYTICAL REPORT

Analyte Result

Analysis





% Dry Solids 91224890.50082.4 12/15/09 08:461 SW-846% DEA0.500


Acetone J 91224290.02700.0179 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.0135


Bromobenzene 91224290.00108ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.000362






sec-Butylbenzene 91224290.00108ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.000362

n-Butylbenzene 91224290.00108ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.000362

tert-Butylbenzene 91224290.00108ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.000362








2-Chlorotoluene 91224290.00108ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.000362


1,2-Dibromo-3-chloropropane 91224290.00270ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.00184



1,4-Dichlorobenzene 91224290.00108ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.000389














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Analysis







Hexachlorobutadiene 91224290.00270ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.000340



p-Isopropyltoluene 91224290.00108ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.000362



4-Methyl-2-pentanone 91224290.0270ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.00157

Naphthalene 91224290.00270ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.000918

n-Propylbenzene 91224290.00108ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.000362





Toluene 91224290.00108ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.000216

1,2,3-Trichlorobenzene 91224290.00108ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.000497






1,2,3-Trichloropropane 91224290.00108ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.000556

1,3,5-Trimethylbenzene 91224290.00108ND 12/13/09 17:471 SW846 8260Bmg/kg dry KxC0.000216









Diesel QP6 91217274.799.01 12/15/09 04:101 TPH-D/Fingermg/kg dry mrb2.40






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Chloromethane J 91216161.000.440 12/09/09 22:451 SW846 8260Bug/L JJP0.390
























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Naphthalene 91216165.00ND 12/09/09 22:451 SW846 8260Bug/L JJP0.380





Tetrachloroethene J 91216161.000.660 12/09/09 22:451 SW846 8260Bug/L JJP0.320



















% Dry Solids 91224890.50080.4 12/15/09 08:461 SW-846% DEA0.500









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Isopropylbenzene 91222340.002280.00355 12/12/09 19:501 SW846 8260Bmg/kg dry KxC0.000763

p-Isopropyltoluene 91222340.002280.00366 12/12/09 19:501 SW846 8260Bmg/kg dry KxC0.000763




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Naphthalene J 91222340.005690.00461 12/12/09 19:501 SW846 8260Bmg/kg dry KxC0.00194






































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Chloromethane 91216161.00ND 12/09/09 23:121 SW846 8260Bug/L JJP0.390

































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Analysis






Tetrachloroethene J 91216161.000.380 12/09/09 23:121 SW846 8260Bug/L JJP0.320



















% Dry Solids 91224890.50083.4 12/15/09 08:461 SW-846% DEA0.500


















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Toluene 91224290.00216ND 12/13/09 18:171 SW846 8260Bmg/kg dry KxC0.000431



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% Dry Solids 91224890.50084.1 12/15/09 08:461 SW-846% DEA0.500


Acetone J 91224290.02390.0195 12/13/09 18:481 SW846 8260Bmg/kg dry KxC0.0119
















Chloroform B 91224290.0009560.00202 12/13/09 18:481 SW846 8260Bmg/kg dry KxC0.000320









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Diesel J, QP6 91217274.733.90 12/15/09 05:021 TPH-D/Fingermg/kg dry mrb2.37

































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Parameter

Wt/Vol


Extraction


Extractable Petroleum Hydrocarbons 25.18 EPA 3550BHLB12/12/09 11:409121727TPH-D/Finger NSL0906-01 1.00

25.31 EPA 3550BHLB12/12/09 11:409121727TPH-D/Finger NSL0906-03 1.00




Volatile Organic Compounds by EPA Method 8260B 4.68 EPA 5035CHH12/04/09 12:009122234SW846 8260B NSL0906-01 5.00

5.02 EPA 5035CHH12/04/09 12:009122429SW846 8260B NSL0906-01RE1 5.00

5.20 EPA 5035CHH12/04/09 12:009121711SW846 8260B NSL0906-01RE2 5.00

10.67 EPA 5035CHH12/04/09 13:109122234SW846 8260B NSL0906-03 5.00

11.24 EPA 5035CHH12/04/09 13:109122429SW846 8260B NSL0906-03RE1 5.00

5.46 EPA 5035CHH12/04/09 13:259122234SW846 8260B NSL0906-05 5.00

6.71 EPA 5035CHH12/04/09 13:559122234SW846 8260B NSL0906-07 5.00

5.56 EPA 5035CHH12/04/09 13:559122429SW846 8260B NSL0906-07RE1 5.00

12.96 EPA 5035CHH12/04/09 14:209122234SW846 8260B NSL0906-09 5.00

12.44 EPA 5035CHH12/04/09 14:209122429SW846 8260B NSL0906-09RE1 5.00

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9121616-BLK1ug/L 9121616<25.0 9121616-BLK1 12/09/09 17:16Acetone

ug/L 9121616<0.410 9121616-BLK1 12/09/09 17:16Benzene

ug/L 9121616<0.360 9121616-BLK1 12/09/09 17:16Bromobenzene

ug/L 9121616<0.470 9121616-BLK1 12/09/09 17:16Bromochloromethane

ug/L 9121616<0.270 9121616-BLK1 12/09/09 17:16Bromodichloromethane

ug/L 9121616<0.430 9121616-BLK1 12/09/09 17:16Bromoform

ug/L 9121616<0.300 9121616-BLK1 12/09/09 17:16Bromomethane

ug/L 9121616<2.10 9121616-BLK1 12/09/09 17:162-Butanone

ug/L 9121616<0.360 9121616-BLK1 12/09/09 17:16sec-Butylbenzene

ug/L 9121616<0.310 9121616-BLK1 12/09/09 17:16n-Butylbenzene

ug/L 9121616<0.380 9121616-BLK1 12/09/09 17:16tert-Butylbenzene

ug/L 9121616<0.360 9121616-BLK1 12/09/09 17:16Carbon disulfide

ug/L 9121616<0.330 9121616-BLK1 12/09/09 17:16Carbon Tetrachloride

ug/L 9121616<0.220 9121616-BLK1 12/09/09 17:16Chlorobenzene

ug/L 9121616<0.260 9121616-BLK1 12/09/09 17:16Chlorodibromomethane

ug/L 9121616<0.460 9121616-BLK1 12/09/09 17:16Chloroethane

ug/L 9121616<0.250 9121616-BLK1 12/09/09 17:16Chloroform

ug/L 9121616<0.390 9121616-BLK1 12/09/09 17:16Chloromethane



ug/L 9121616<0.860 9121616-BLK1 12/09/09 17:161,2-Dibromo-3-chloropropane

ug/L 9121616<0.460 9121616-BLK1 12/09/09 17:161,2-Dibromoethane (EDB)

ug/L 9121616<0.410 9121616-BLK1 12/09/09 17:16Dibromomethane




ug/L 9121616<0.190 9121616-BLK1 12/09/09 17:16Dichlorodifluoromethane



ug/L 9121616<0.330 9121616-BLK1 12/09/09 17:16cis-1,2-Dichloroethene

ug/L 9121616<0.220 9121616-BLK1 12/09/09 17:161,1-Dichloroethene

ug/L 9121616<0.330 9121616-BLK1 12/09/09 17:16trans-1,2-Dichloroethene




ug/L 9121616<0.330 9121616-BLK1 12/09/09 17:16cis-1,3-Dichloropropene

ug/L 9121616<0.330 9121616-BLK1 12/09/09 17:16trans-1,3-Dichloropropene

ug/L 9121616<0.260 9121616-BLK1 12/09/09 17:161,1-Dichloropropene

ug/L 9121616<0.350 9121616-BLK1 12/09/09 17:16Ethylbenzene

ug/L 91216162.41 9121616-BLK1 12/09/09 17:16Hexachlorobutadiene

ug/L 9121616<1.40 9121616-BLK1 12/09/09 17:162-Hexanone

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9121616-BLK1ug/L 9121616<0.400 9121616-BLK1 12/09/09 17:16Isopropylbenzene

ug/L 9121616<0.330 9121616-BLK1 12/09/09 17:16p-Isopropyltoluene

ug/L 9121616<0.320 9121616-BLK1 12/09/09 17:16Methyl tert-Butyl Ether

ug/L 9121616<0.480 9121616-BLK1 12/09/09 17:16Methylene Chloride

ug/L 9121616<1.40 9121616-BLK1 12/09/09 17:164-Methyl-2-pentanone

ug/L 9121616<0.380 9121616-BLK1 12/09/09 17:16Naphthalene

ug/L 9121616<0.390 9121616-BLK1 12/09/09 17:16n-Propylbenzene

ug/L 9121616<0.260 9121616-BLK1 12/09/09 17:16Styrene



ug/L 9121616<0.320 9121616-BLK1 12/09/09 17:16Tetrachloroethene

ug/L 9121616<0.350 9121616-BLK1 12/09/09 17:16Toluene

ug/L 91216162.30 9121616-BLK1 12/09/09 17:161,2,3-Trichlorobenzene

ug/L 91216160.640 9121616-BLK1J 12/09/09 17:161,2,4-Trichlorobenzene



ug/L 9121616<0.260 9121616-BLK1 12/09/09 17:16Trichloroethene

ug/L 9121616<0.220 9121616-BLK1 12/09/09 17:16Trichlorofluoromethane

ug/L 9121616<0.470 9121616-BLK1 12/09/09 17:161,2,3-Trichloropropane



ug/L 9121616<0.220 9121616-BLK1 12/09/09 17:16Vinyl chloride

ug/L 9121616<0.330 9121616-BLK1 12/09/09 17:16o-Xylene

ug/L 9121616<0.400 9121616-BLK1 12/09/09 17:16m,p-Xylene

ug/L 9121616<0.730 9121616-BLK1 12/09/09 17:16Xylenes, total















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9121711-BLK1mg/kg wet 9121711<0.000670 9121711-BLK1 12/13/09 20:27tert-Butylbenzene






mg/kg wet 9121711<0.000670 9121711-BLK1 12/13/09 20:27Chloroform



































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9121711-BLK1mg/kg wet 9121711<0.000400 9121711-BLK1 12/13/09 20:27Tetrachloroethene

































mg/kg wet 91222340.00306 9122234-BLK1B 12/12/09 16:25Chloroform






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9122234-BLK1mg/kg wet 9122234<0.000670 9122234-BLK1 12/12/09 16:25Dibromomethane









































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9122234-BLK1mg/kg wet 9122234<0.00130 9122234-BLK1 12/12/09 16:25Xylenes, total





















mg/kg wet 91224290.00241 9122429-BLK1 12/13/09 13:41Chloroform


















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9122429-BLK1mg/kg wet 9122429<0.000780 9122429-BLK1 12/13/09 13:412,2-Dichloropropane



































9121727-BLK1mg/kg wet 9121727<2.00 9121727-BLK1 12/14/09 11:15Diesel

9121727 9121727-BLK1 12/14/09 11:1579%Surrogate: o-Terphenyl

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Duplicate

Analyte UnitsOrig. Val. Duplicate RPD Batch

Sample

DuplicatedQ

Analyzed

Date/TimeLimit % Rec.


9122489-DUP1%41.7 18.5 20 9122489 NSL0632-02 12/15/09 08:46% Dry Solids 77

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LCS


Target

Range

Analyzed

Date/Time


9121616-BS156 - 150 9121616250 338 135% ug/L 12/09/09 15:27Acetone

80 - 121 912161650.0 51.7 103% ug/L 12/09/09 15:27Benzene

72 - 130 912161650.0 47.7 95% ug/L 12/09/09 15:27Bromobenzene

73 - 137 912161650.0 54.4 109% ug/L 12/09/09 15:27Bromochloromethane

75 - 131 912161650.0 59.2 118% ug/L 12/09/09 15:27Bromodichloromethane

65 - 140 912161650.0 51.5 103% ug/L 12/09/09 15:27Bromoform

50 - 150 912161650.0 57.8 116% ug/L 12/09/09 15:27Bromomethane

70 - 144 9121616250 303 121% ug/L 12/09/09 15:272-Butanone

72 - 140 912161650.0 51.8 104% ug/L 12/09/09 15:27sec-Butylbenzene

68 - 140 912161650.0 52.4 105% ug/L 12/09/09 15:27n-Butylbenzene

76 - 135 912161650.0 51.5 103% ug/L 12/09/09 15:27tert-Butylbenzene

74 - 137 912161650.0 53.2 106% ug/L 12/09/09 15:27Carbon disulfide

71 - 137 912161650.0 63.1 126% ug/L 12/09/09 15:27Carbon Tetrachloride

80 - 121 912161650.0 50.4 101% ug/L 12/09/09 15:27Chlorobenzene

68 - 137 912161650.0 53.1 106% ug/L 12/09/09 15:27Chlorodibromomethane

50 - 146 912161650.0 50.8 102% ug/L 12/09/09 15:27Chloroethane

73 - 131 912161650.0 61.4 123% ug/L 12/09/09 15:27Chloroform

30 - 132 912161650.0 53.8 108% ug/L 12/09/09 15:27Chloromethane



56 - 145 912161650.0 49.3 99% ug/L 12/09/09 15:271,2-Dibromo-3-chloropropane

80 - 135 912161650.0 55.3 111% ug/L 12/09/09 15:271,2-Dibromoethane (EDB)

78 - 133 912161650.0 60.0 120% ug/L 12/09/09 15:27Dibromomethane




30 - 132 912161650.0 42.7 85% ug/L 12/09/09 15:27Dichlorodifluoromethane



71 - 132 912161650.0 59.0 118% ug/L 12/09/09 15:27cis-1,2-Dichloroethene

73 - 125 912161650.0 54.8 110% ug/L 12/09/09 15:271,1-Dichloroethene

77 - 125 912161650.0 57.7 115% ug/L 12/09/09 15:27trans-1,2-Dichloroethene




70 - 140 912161650.0 50.6 101% ug/L 12/09/09 15:27cis-1,3-Dichloropropene

62 - 139 912161650.0 52.7 105% ug/L 12/09/09 15:27trans-1,3-Dichloropropene

78 - 126 912161650.0 56.1 112% ug/L 12/09/09 15:271,1-Dichloropropene

78 - 133 912161650.0 52.4 105% ug/L 12/09/09 15:27Ethylbenzene

70 - 150 912161650.0 62.8 126%B ug/L 12/09/09 15:27Hexachlorobutadiene

60 - 150 9121616250 305 122% ug/L 12/09/09 15:272-Hexanone

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LCS - Cont.


Target

Range

Analyzed

Date/Time


9121616-BS169 - 120 912161650.0 53.6 107% ug/L 12/09/09 15:27Isopropylbenzene

72 - 134 912161650.0 50.9 102% ug/L 12/09/09 15:27p-Isopropyltoluene

76 - 120 912161650.0 55.1 110% ug/L 12/09/09 15:27Methyl tert-Butyl Ether

80 - 133 912161650.0 56.4 113% ug/L 12/09/09 15:27Methylene Chloride

62 - 146 9121616250 266 107% ug/L 12/09/09 15:274-Methyl-2-pentanone

71 - 139 912161650.0 60.4 121% ug/L 12/09/09 15:27Naphthalene

70 - 143 912161650.0 49.1 98% ug/L 12/09/09 15:27n-Propylbenzene

80 - 136 912161650.0 52.9 106% ug/L 12/09/09 15:27Styrene



77 - 131 912161650.0 52.6 105% ug/L 12/09/09 15:27Tetrachloroethene

78 - 125 912161650.0 47.5 95% ug/L 12/09/09 15:27Toluene

71 - 138 912161650.0 77.3 155%L, B ug/L 12/09/09 15:271,2,3-Trichlorobenzene

74 - 136 912161650.0 65.9 132% ug/L 12/09/09 15:271,2,4-Trichlorobenzene



74 - 139 912161650.0 55.6 111% ug/L 12/09/09 15:27Trichloroethene

60 - 133 912161650.0 55.0 110% ug/L 12/09/09 15:27Trichlorofluoromethane

64 - 127 912161650.0 46.1 92% ug/L 12/09/09 15:271,2,3-Trichloropropane



60 - 122 912161650.0 50.5 101% ug/L 12/09/09 15:27Vinyl chloride

66 - 150 912161650.0 51.6 103% ug/L 12/09/09 15:27o-Xylene

78 - 132 9121616100 104 104% ug/L 12/09/09 15:27m,p-Xylene

78 - 134 9121616150 155 103% ug/L 12/09/09 15:27Xylenes, total





9121711-BS160 - 150 9121711250 313 125% ug/kg 12/13/09 18:11Acetone

78 - 126 912171150.0 51.3 103% ug/kg 12/13/09 18:11Benzene




74 - 133 912171150.0 50.2 100% ug/kg 12/13/09 18:11Bromoform


68 - 149 9121711250 280 112% ug/kg 12/13/09 18:112-Butanone



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LCS - Cont.


Target

Range

Analyzed

Date/Time


9121711-BS180 - 129 912171150.0 54.5 109% ug/kg 12/13/09 18:11tert-Butylbenzene






70 - 127 912171150.0 51.2 102% ug/kg 12/13/09 18:11Chloroform
























65 - 150 9121711250 278 111% ug/kg 12/13/09 18:112-Hexanone








80 - 140 912171150.0 52.9 106% ug/kg 12/13/09 18:11Styrene



Page 32 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


LCS - Cont.


Target

Range

Analyzed

Date/Time


9121711-BS176 - 130 912171150.0 53.0 106%MNR ug/kg 12/13/09 18:11Tetrachloroethene

76 - 126 912171150.0 53.3 107% ug/kg 12/13/09 18:11Toluene





79 - 129 912171150.0 53.9 108%MNR ug/kg 12/13/09 18:11Trichloroethene











9122234-BS160 - 150 9122234250 221 89% ug/kg 12/12/09 14:26Acetone

78 - 126 912223450.0 45.8 92% ug/kg 12/12/09 14:26Benzene




74 - 133 912223450.0 44.8 90% ug/kg 12/12/09 14:26Bromoform


68 - 149 9122234250 244 98% ug/kg 12/12/09 14:262-Butanone















Page 33 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


LCS - Cont.


Target

Range

Analyzed

Date/Time


9122234-BS178 - 128 912223450.0 46.5 93% ug/kg 12/12/09 14:26Dibromomethane


















65 - 150 9122234250 257 103% ug/kg 12/12/09 14:262-Hexanone








80 - 140 912223450.0 55.7 111% ug/kg 12/12/09 14:26Styrene




76 - 126 912223450.0 49.4 99% ug/kg 12/12/09 14:26Toluene











Page 34 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


LCS - Cont.


Target

Range

Analyzed

Date/Time


9122234-BS180 - 130 9122234150 175 117% ug/kg 12/12/09 14:26Xylenes, total





9122429-BS160 - 150 9122429250 281 112% ug/kg 12/13/09 12:09Acetone

78 - 126 912242950.0 52.1 104% ug/kg 12/13/09 12:09Benzene




74 - 133 912242950.0 46.3 93% ug/kg 12/13/09 12:09Bromoform


68 - 149 9122429250 282 113% ug/kg 12/13/09 12:092-Butanone



























Page 35 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


LCS - Cont.


Target

Range

Analyzed

Date/Time


9122429-BS160 - 139 912242950.0 42.1 84% ug/kg 12/13/09 12:092,2-Dichloropropane






65 - 150 9122429250 287 115% ug/kg 12/13/09 12:092-Hexanone








80 - 140 912242950.0 57.4 115% ug/kg 12/13/09 12:09Styrene




76 - 126 912242950.0 53.7 107% ug/kg 12/13/09 12:09Toluene

















9121727-BS155 - 123 912172740.0 37.7 94% mg/kg wet 12/15/09 02:44Diesel

29 - 141 91217270.800 0.818Surrogate: o-Terphenyl 102% 12/15/09 02:44

Page 36 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


Sample


LCS Dup


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121616-BSD1352 4 31 9121616 250 141%ug/L 56 - 150 12/09/09 15:54Acetone

51.8 0.3 12 9121616 50.0 104%ug/L 80 - 121 12/09/09 15:54Benzene

49.0 3 23 9121616 50.0 98%ug/L 72 - 130 12/09/09 15:54Bromobenzene

56.0 3 32 9121616 50.0 112%ug/L 73 - 137 12/09/09 15:54Bromochloromethane

60.8 3 13 9121616 50.0 122%ug/L 75 - 131 12/09/09 15:54Bromodichloromethane

53.3 3 18 9121616 50.0 107%ug/L 65 - 140 12/09/09 15:54Bromoform

58.1 0.4 50 9121616 50.0 116%ug/L 50 - 150 12/09/09 15:54Bromomethane

311 3 37 9121616 250 124%ug/L 70 - 144 12/09/09 15:542-Butanone

53.4 3 21 9121616 50.0 107%ug/L 72 - 140 12/09/09 15:54sec-Butylbenzene

54.5 4 11 9121616 50.0 109%ug/L 68 - 140 12/09/09 15:54n-Butylbenzene

53.0 3 20 9121616 50.0 106%ug/L 76 - 135 12/09/09 15:54tert-Butylbenzene

54.2 2 28 9121616 50.0 108%ug/L 74 - 137 12/09/09 15:54Carbon disulfide

63.7 1 26 9121616 50.0 127%ug/L 71 - 137 12/09/09 15:54Carbon Tetrachloride

51.3 2 11 9121616 50.0 103%ug/L 80 - 121 12/09/09 15:54Chlorobenzene

54.5 3 16 9121616 50.0 109%ug/L 68 - 137 12/09/09 15:54Chlorodibromomethane

51.2 0.7 35 9121616 50.0 102%ug/L 50 - 146 12/09/09 15:54Chloroethane

62.1 1 32 9121616 50.0 124%ug/L 73 - 131 12/09/09 15:54Chloroform

55.2 2 34 9121616 50.0 110%ug/L 30 - 132 12/09/09 15:54Chloromethane



50.4 2 21 9121616 50.0 101%ug/L 56 - 145 12/09/09 15:541,2-Dibromo-3-chloropropane

56.7 2 10 9121616 50.0 113%ug/L 80 - 135 12/09/09 15:541,2-Dibromoethane (EDB)

61.7 3 11 9121616 50.0 123%ug/L 78 - 133 12/09/09 15:54Dibromomethane




43.2 1 32 9121616 50.0 86%ug/L 30 - 132 12/09/09 15:54Dichlorodifluoromethane



59.2 0.4 32 9121616 50.0 118%ug/L 71 - 132 12/09/09 15:54cis-1,2-Dichloroethene

55.2 0.8 31 9121616 50.0 110%ug/L 73 - 125 12/09/09 15:541,1-Dichloroethene

58.8 2 32 9121616 50.0 118%ug/L 77 - 125 12/09/09 15:54trans-1,2-Dichloroethene




51.1 0.9 35 9121616 50.0 102%ug/L 70 - 140 12/09/09 15:54cis-1,3-Dichloropropene

55.2 5 26 9121616 50.0 110%ug/L 62 - 139 12/09/09 15:54trans-1,3-Dichloropropene

57.1 2 18 9121616 50.0 114%ug/L 78 - 126 12/09/09 15:541,1-Dichloropropene

53.4 2 12 9121616 50.0 107%ug/L 78 - 133 12/09/09 15:54Ethylbenzene

66.1 5 21 9121616B 50.0 132%ug/L 70 - 150 12/09/09 15:54Hexachlorobutadiene

316 4 20 9121616 250 127%ug/L 60 - 150 12/09/09 15:542-Hexanone

Page 37 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


Sample


LCS Dup - Cont.


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121616-BSD154.1 0.9 15 9121616 50.0 108%ug/L 69 - 120 12/09/09 15:54Isopropylbenzene

52.5 3 18 9121616 50.0 105%ug/L 72 - 134 12/09/09 15:54p-Isopropyltoluene

57.2 4 32 9121616 50.0 114%ug/L 76 - 120 12/09/09 15:54Methyl tert-Butyl Ether

57.1 1 36 9121616 50.0 114%ug/L 80 - 133 12/09/09 15:54Methylene Chloride

273 3 35 9121616 250 109%ug/L 62 - 146 12/09/09 15:544-Methyl-2-pentanone

65.8 9 30 9121616 50.0 132%ug/L 71 - 139 12/09/09 15:54Naphthalene

50.2 2 23 9121616 50.0 100%ug/L 70 - 143 12/09/09 15:54n-Propylbenzene

53.7 1 29 9121616 50.0 107%ug/L 80 - 136 12/09/09 15:54Styrene



53.2 1 16 9121616 50.0 106%ug/L 77 - 131 12/09/09 15:54Tetrachloroethene

47.6 0.2 35 9121616 50.0 95%ug/L 78 - 125 12/09/09 15:54Toluene

85.7 10 28 9121616L, B 50.0 171%ug/L 71 - 138 12/09/09 15:541,2,3-Trichlorobenzene

70.3 6 23 9121616L 50.0 141%ug/L 74 - 136 12/09/09 15:541,2,4-Trichlorobenzene



57.3 3 11 9121616 50.0 115%ug/L 74 - 139 12/09/09 15:54Trichloroethene

55.8 1 33 9121616 50.0 112%ug/L 60 - 133 12/09/09 15:54Trichlorofluoromethane

47.6 3 25 9121616 50.0 95%ug/L 64 - 127 12/09/09 15:541,2,3-Trichloropropane



50.9 0.9 32 9121616 50.0 102%ug/L 60 - 122 12/09/09 15:54Vinyl chloride

52.2 1 27 9121616 50.0 104%ug/L 66 - 150 12/09/09 15:54o-Xylene

105 0.9 16 9121616 100 105%ug/L 78 - 132 12/09/09 15:54m,p-Xylene

157 1 18 9121616 150 104%ug/L 78 - 134 12/09/09 15:54Xylenes, total

29.5 9121616 25.0 118%Surrogate: 1,2-Dichloroethane-d4 ug/L 63 - 140 12/09/09 15:54

27.4 9121616 25.0 109%Surrogate: Dibromofluoromethane ug/L 73 - 131 12/09/09 15:54

22.9 9121616 25.0 92%Surrogate: Toluene-d8 ug/L 80 - 120 12/09/09 15:54

24.1 9121616 25.0 96%Surrogate: 4-Bromofluorobenzene ug/L 79 - 125 12/09/09 15:54

9121711-BSD1307 2 50 9121711 250 123%ug/kg 60 - 150 12/13/09 18:38Acetone

50.9 0.7 50 9121711 50.0 102%ug/kg 78 - 126 12/13/09 18:38Benzene




50.8 1 43 9121711 50.0 102%ug/kg 74 - 133 12/13/09 18:38Bromoform


284 1 50 9121711 250 113%ug/kg 68 - 149 12/13/09 18:382-Butanone

54.4 0.7 50 9121711 50.0 109%ug/kg 76 - 135 12/13/09 18:38sec-Butylbenzene


Page 38 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


Sample


LCS Dup - Cont.


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121711-BSD155.0 0.9 50 9121711 50.0 110%ug/kg 80 - 129 12/13/09 18:38tert-Butylbenzene


51.2 0.2 44 9121711 50.0 102%ug/kg 70 - 138 12/13/09 18:38Carbon Tetrachloride

52.4 0.4 50 9121711 50.0 105%ug/kg 80 - 123 12/13/09 18:38Chlorobenzene

51.3 0.2 48 9121711 50.0 103%ug/kg 80 - 127 12/13/09 18:38Chlorodibromomethane

50.4 0.9 50 9121711 50.0 101%ug/kg 55 - 150 12/13/09 18:38Chloroethane

51.0 0.4 50 9121711 50.0 102%ug/kg 70 - 127 12/13/09 18:38Chloroform


57.9 0.8 50 9121711 50.0 116%ug/kg 80 - 130 12/13/09 18:382-Chlorotoluene




53.2 0.3 50 9121711 50.0 106%ug/kg 78 - 128 12/13/09 18:38Dibromomethane








52.3 2 50 9121711 50.0 105%ug/kg 70 - 125 12/13/09 18:381,1-Dichloroethene

51.2 0.4 40 9121711 50.0 102%ug/kg 73 - 128 12/13/09 18:38trans-1,2-Dichloroethene






52.3 0.3 50 9121711 50.0 105%ug/kg 78 - 125 12/13/09 18:381,1-Dichloropropene

56.8 0.9 50 9121711 50.0 114%ug/kg 79 - 130 12/13/09 18:38Ethylbenzene


272 2 50 9121711 250 109%ug/kg 65 - 150 12/13/09 18:382-Hexanone







58.8 0.4 50 9121711 50.0 118%ug/kg 76 - 133 12/13/09 18:38n-Propylbenzene

52.3 1 50 9121711 50.0 105%ug/kg 80 - 140 12/13/09 18:38Styrene



Page 39 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


Sample


LCS Dup - Cont.


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121711-BSD152.0 2 50 9121711 50.0 104%ug/kg 76 - 130 12/13/09 18:38Tetrachloroethene

52.4 2 50 9121711 50.0 105%ug/kg 76 - 126 12/13/09 18:38Toluene





52.1 3 50 9121711 50.0 104%ug/kg 79 - 129 12/13/09 18:38Trichloroethene




54.6 0.5 50 9121711 50.0 109%ug/kg 80 - 132 12/13/09 18:381,2,4-Trimethylbenzene

50.5 0.8 39 9121711 50.0 101%ug/kg 53 - 142 12/13/09 18:38Vinyl chloride






9122234-BSD1239 8 50 9122234 250 96%ug/kg 60 - 150 12/12/09 14:55Acetone

46.1 0.6 50 9122234 50.0 92%ug/kg 78 - 126 12/12/09 14:55Benzene

47.5 0.1 50 9122234 50.0 95%ug/kg 79 - 126 12/12/09 14:55Bromobenzene

47.5 1 50 9122234 50.0 95%ug/kg 78 - 126 12/12/09 14:55Bromochloromethane


46.7 4 43 9122234 50.0 93%ug/kg 74 - 133 12/12/09 14:55Bromoform


257 5 50 9122234 250 103%ug/kg 68 - 149 12/12/09 14:552-Butanone




48.3 3 48 9122234 50.0 97%ug/kg 80 - 132 12/12/09 14:55Carbon disulfide





44.7 1 50 9122234B 50.0 89%ug/kg 70 - 127 12/12/09 14:55Chloroform

49.0 2 44 9122234 50.0 98%ug/kg 36 - 137 12/12/09 14:55Chloromethane




53.6 2 45 9122234 50.0 107%ug/kg 80 - 131 12/12/09 14:551,2-Dibromoethane (EDB)

Page 40 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


Sample


LCS Dup - Cont.


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9122234-BSD147.0 1 50 9122234 50.0 94%ug/kg 78 - 128 12/12/09 14:55Dibromomethane


















276 7 50 9122234 250 111%ug/kg 65 - 150 12/12/09 14:552-Hexanone




48.7 0.2 50 9122234 50.0 97%ug/kg 69 - 140 12/12/09 14:55Methylene Chloride




54.6 2 50 9122234 50.0 109%ug/kg 80 - 140 12/12/09 14:55Styrene

50.5 0.6 50 9122234 50.0 101%ug/kg 80 - 132 12/12/09 14:551,1,1,2-Tetrachloroethane



48.4 2 50 9122234 50.0 97%ug/kg 76 - 126 12/12/09 14:55Toluene


53.8 0.5 50 9122234 50.0 108%ug/kg 64 - 150 12/12/09 14:551,2,4-Trichlorobenzene




43.5 0.7 47 9122234 50.0 87%ug/kg 52 - 148 12/12/09 14:55Trichlorofluoromethane





Page 41 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


Sample


LCS Dup - Cont.


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9122234-BSD1168 4 50 9122234 150 112%ug/kg 80 - 130 12/12/09 14:55Xylenes, total





Page 42 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906

Analyte Units



Target

Range

Matrix Spike

Q

Analyzed

Date/Time

Sample

SpikedBatch


9121616-MS1271 250 NSL0918-01 109%ND 912161656 - 150ug/L 12/10/09 09:22Acetone

55.8 50.0 NSL0918-01 112%ND 912161665 - 151ug/L 12/10/09 09:22Benzene

48.9 50.0 NSL0918-01 98%ND 912161669 - 142ug/L 12/10/09 09:22Bromobenzene

60.2 50.0 NSL0918-01 120%ND 912161664 - 154ug/L 12/10/09 09:22Bromochloromethane

67.0 50.0 NSL0918-01 134%ND 912161675 - 138ug/L 12/10/09 09:22Bromodichloromethane

58.1 50.0 NSL0918-01 116%ND 912161655 - 153ug/L 12/10/09 09:22Bromoform

55.3 50.0 NSL0918-01 111%ND 912161613 - 176ug/L 12/10/09 09:22Bromomethane

295 250 NSL0918-01 118%ND 912161645 - 164ug/L 12/10/09 09:222-Butanone

55.5 50.0 NSL0918-01 111%ND 912161668 - 159ug/L 12/10/09 09:22sec-Butylbenzene

57.4 50.0 NSL0918-01 115%ND 912161667 - 151ug/L 12/10/09 09:22n-Butylbenzene

55.1 50.0 NSL0918-01 110%ND 912161673 - 153ug/L 12/10/09 09:22tert-Butylbenzene

62.1 50.0 NSL0918-01 119%2.47 912161633 - 187ug/L 12/10/09 09:22Carbon disulfide

79.8 50.0 NSL0918-01M7 160%ND 912161664 - 157ug/L 12/10/09 09:22Carbon Tetrachloride

55.1 50.0 NSL0918-01 110%ND 912161678 - 136ug/L 12/10/09 09:22Chlorobenzene

60.0 50.0 NSL0918-01 120%ND 912161664 - 145ug/L 12/10/09 09:22Chlorodibromomethane

53.4 50.0 NSL0918-01 107%ND 912161648 - 159ug/L 12/10/09 09:22Chloroethane

70.5 50.0 NSL0918-01 141%ND 912161672 - 145ug/L 12/10/09 09:22Chloroform

51.0 50.0 NSL0918-01 102%ND 912161610 - 194ug/L 12/10/09 09:22Chloromethane



43.3 50.0 NSL0918-01 87%ND 912161649 - 162ug/L 12/10/09 09:221,2-Dibromo-3-chloropropane

59.2 50.0 NSL0918-01 118%ND 912161670 - 152ug/L 12/10/09 09:221,2-Dibromoethane (EDB)

67.1 50.0 NSL0918-01 134%ND 912161675 - 141ug/L 12/10/09 09:22Dibromomethane




45.1 50.0 NSL0918-01 90%ND 912161623 - 159ug/L 12/10/09 09:22Dichlorodifluoromethane

61.1 50.0 NSL0918-01 122%ND 912161664 - 154ug/L 12/10/09 09:221,1-Dichloroethane

78.4 50.0 NSL0918-01M7 157%ND 912161672 - 137ug/L 12/10/09 09:221,2-Dichloroethane

66.3 50.0 NSL0918-01 133%ND 912161657 - 154ug/L 12/10/09 09:22cis-1,2-Dichloroethene

60.6 50.0 NSL0918-01 121%ND 912161634 - 151ug/L 12/10/09 09:221,1-Dichloroethene

64.7 50.0 NSL0918-01 129%ND 912161657 - 157ug/L 12/10/09 09:22trans-1,2-Dichloroethene




56.3 50.0 NSL0918-01 113%ND 912161656 - 156ug/L 12/10/09 09:22cis-1,3-Dichloropropene

60.9 50.0 NSL0918-01 122%ND 912161647 - 157ug/L 12/10/09 09:22trans-1,3-Dichloropropene

Page 43 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906

Analyte Units



Target

Range


Q

Analyzed

Date/Time

Sample

SpikedBatch


9121616-MS165.5 50.0 NSL0918-01 131%ND 912161670 - 155ug/L 12/10/09 09:221,1-Dichloropropene

58.8 50.0 NSL0918-01 118%ND 912161668 - 157ug/L 12/10/09 09:22Ethylbenzene

59.8 50.0 NSL0918-01B 120%ND 912161647 - 173ug/L 12/10/09 09:22Hexachlorobutadiene

312 250 NSL0918-01 125%ND 912161657 - 154ug/L 12/10/09 09:222-Hexanone

61.8 50.0 NSL0918-01 124%ND 912161669 - 139ug/L 12/10/09 09:22Isopropylbenzene

54.7 50.0 NSL0918-01 109%ND 912161669 - 151ug/L 12/10/09 09:22p-Isopropyltoluene

54.2 50.0 NSL0918-01 108%ND 912161656 - 152ug/L 12/10/09 09:22Methyl tert-Butyl Ether

59.1 50.0 NSL0918-01 118%ND 912161671 - 136ug/L 12/10/09 09:22Methylene Chloride

292 250 NSL0918-01 117%ND 912161662 - 159ug/L 12/10/09 09:224-Methyl-2-pentanone

36.4 50.0 NSL0918-01 73%ND 912161656 - 161ug/L 12/10/09 09:22Naphthalene

52.2 50.0 NSL0918-01 104%ND 912161661 - 167ug/L 12/10/09 09:22n-Propylbenzene

59.3 50.0 NSL0918-01 119%ND 912161669 - 150ug/L 12/10/09 09:22Styrene



62.9 50.0 NSL0918-01 120%3.00 912161663 - 155ug/L 12/10/09 09:22Tetrachloroethene

54.2 50.0 NSL0918-01 108%ND 912161661 - 153ug/L 12/10/09 09:22Toluene

41.4 50.0 NSL0918-01B 83%ND 912161657 - 155ug/L 12/10/09 09:221,2,3-Trichlorobenzene

51.9 50.0 NSL0918-01 104%ND 912161664 - 147ug/L 12/10/09 09:221,2,4-Trichlorobenzene



68.7 50.0 NSL0918-01 124%6.88 912161674 - 139ug/L 12/10/09 09:22Trichloroethene

66.4 50.0 NSL0918-01 133%ND 912161653 - 149ug/L 12/10/09 09:22Trichlorofluoromethane

46.7 50.0 NSL0918-01 93%ND 912161649 - 148ug/L 12/10/09 09:221,2,3-Trichloropropane



51.9 50.0 NSL0918-01 104%ND 912161653 - 137ug/L 12/10/09 09:22Vinyl chloride

59.1 50.0 NSL0918-01 118%ND 912161662 - 167ug/L 12/10/09 09:22o-Xylene

119 100 NSL0918-01 119%ND 912161669 - 155ug/L 12/10/09 09:22m,p-Xylene

178 150 NSL0918-01 118%ND 912161668 - 158ug/L 12/10/09 09:22Xylenes, total

32.6 25.0 NSL0918-01 Surrogate: 1,2-Dichloroethane-d4 130% 912161663 - 140ug/L 12/10/09 09:22

29.0 25.0 NSL0918-01 Surrogate: Dibromofluoromethane 116% 912161673 - 131ug/L 12/10/09 09:22

23.9 25.0 NSL0918-01 Surrogate: Toluene-d8 96% 912161680 - 120ug/L 12/10/09 09:22

22.9 25.0 NSL0918-01 Surrogate: 4-Bromofluorobenzene 91% 912161679 - 125ug/L 12/10/09 09:22

9121711-MS112700 12500 NSL1079-01 102%ND 912171129 - 181mg/kg wet 12/14/09 07:24Acetone

2380 2500 NSL1079-01 95%ND 912171142 - 141mg/kg wet 12/14/09 07:24Benzene

Page 44 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906

Analyte Units



Target

Range


Q

Analyzed

Date/Time

Sample

SpikedBatch


9121711-MS12630 2500 NSL1079-01 105%ND 912171119 - 154mg/kg wet 12/14/09 07:24Bromobenzene

2250 2500 NSL1079-01 90%ND 912171141 - 146mg/kg wet 12/14/09 07:24Bromochloromethane

2460 2500 NSL1079-01 99%ND 912171132 - 155mg/kg wet 12/14/09 07:24Bromodichloromethane

2550 2500 NSL1079-01 102%ND 912171110 - 155mg/kg wet 12/14/09 07:24Bromoform

2370 2500 NSL1079-01 95%ND 912171110 - 199mg/kg wet 12/14/09 07:24Bromomethane

12300 12500 NSL1079-01 98%ND 912171138 - 161mg/kg wet 12/14/09 07:242-Butanone

2700 2500 NSL1079-01 108%ND 912171110 - 170mg/kg wet 12/14/09 07:24sec-Butylbenzene

2690 2500 NSL1079-01 108%ND 912171110 - 183mg/kg wet 12/14/09 07:24n-Butylbenzene

2670 2500 NSL1079-01 107%ND 912171111 - 165mg/kg wet 12/14/09 07:24tert-Butylbenzene

2300 2500 NSL1079-01 92%ND 912171150 - 136mg/kg wet 12/14/09 07:24Carbon disulfide

2590 2500 NSL1079-01 104%ND 912171130 - 159mg/kg wet 12/14/09 07:24Carbon Tetrachloride

2560 2500 NSL1079-01 102%ND 912171125 - 151mg/kg wet 12/14/09 07:24Chlorobenzene

2620 2500 NSL1079-01 105%ND 912171127 - 150mg/kg wet 12/14/09 07:24Chlorodibromomethane

2200 2500 NSL1079-01 88%ND 912171115 - 197mg/kg wet 12/14/09 07:24Chloroethane

2440 2500 NSL1079-01 98%ND 912171133 - 148mg/kg wet 12/14/09 07:24Chloroform

1840 2500 NSL1079-01 73%ND 912171110 - 166mg/kg wet 12/14/09 07:24Chloromethane



2630 2500 NSL1079-01 105%ND 912171110 - 167mg/kg wet 12/14/09 07:241,2-Dibromo-3-chloropropane

2790 2500 NSL1079-01 112%ND 912171130 - 155mg/kg wet 12/14/09 07:241,2-Dibromoethane (EDB)

2410 2500 NSL1079-01 96%ND 912171130 - 149mg/kg wet 12/14/09 07:24Dibromomethane

2610 2500 NSL1079-01 100%122 912171110 - 170mg/kg wet 12/14/09 07:241,4-Dichlorobenzene

2700 2500 NSL1079-01 108%ND 912171110 - 173mg/kg wet 12/14/09 07:241,3-Dichlorobenzene

2810 2500 NSL1079-01 110%52.5 912171110 - 168mg/kg wet 12/14/09 07:241,2-Dichlorobenzene

1240 2500 NSL1079-01 50%ND 912171110 - 188mg/kg wet 12/14/09 07:24Dichlorodifluoromethane



3360 2500 NSL1079-01 112%548 912171132 - 150mg/kg wet 12/14/09 07:24cis-1,2-Dichloroethene

2570 2500 NSL1079-01 103%ND 912171146 - 141mg/kg wet 12/14/09 07:241,1-Dichloroethene

2450 2500 NSL1079-01 98%ND 912171141 - 146mg/kg wet 12/14/09 07:24trans-1,2-Dichloroethene




2780 2500 NSL1079-01 111%ND 912171123 - 152mg/kg wet 12/14/09 07:24cis-1,3-Dichloropropene

2380 2500 NSL1079-01 95%ND 912171124 - 151mg/kg wet 12/14/09 07:24trans-1,3-Dichloropropene

2530 2500 NSL1079-01 101%ND 912171140 - 151mg/kg wet 12/14/09 07:241,1-Dichloropropene

2870 2500 NSL1079-01 115%ND 912171121 - 165mg/kg wet 12/14/09 07:24Ethylbenzene

Page 45 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906

Analyte Units



Target

Range


Q

Analyzed

Date/Time

Sample

SpikedBatch


9121711-MS14020 2500 NSL1079-01 161%ND 912171110 - 173mg/kg wet 12/14/09 07:24Hexachlorobutadiene

8190 12500 NSL1079-01 66%ND 912171113 - 174mg/kg wet 12/14/09 07:242-Hexanone

2660 2500 NSL1079-01 106%ND 912171120 - 139mg/kg wet 12/14/09 07:24Isopropylbenzene

2570 2500 NSL1079-01 103%ND 912171110 - 164mg/kg wet 12/14/09 07:24p-Isopropyltoluene

2400 2500 NSL1079-01 96%ND 912171134 - 154mg/kg wet 12/14/09 07:24Methyl tert-Butyl Ether

2340 2500 NSL1079-01 94%ND 912171136 - 163mg/kg wet 12/14/09 07:24Methylene Chloride

13700 12500 NSL1079-01 110%ND 912171119 - 176mg/kg wet 12/14/09 07:244-Methyl-2-pentanone

3400 2500 NSL1079-01 136%ND 912171110 - 160mg/kg wet 12/14/09 07:24Naphthalene

2870 2500 NSL1079-01 115%ND 912171116 - 174mg/kg wet 12/14/09 07:24n-Propylbenzene

2560 2500 NSL1079-01 102%ND 912171110 - 177mg/kg wet 12/14/09 07:24Styrene



2680 2500 NSL1079-01 107%ND 912171145 - 145mg/kg wet 12/14/09 07:24Toluene

3740 2500 NSL1079-01 150%ND 912171110 - 182mg/kg wet 12/14/09 07:241,2,3-Trichlorobenzene

4430 2500 NSL1079-01 140%930 912171110 - 175mg/kg wet 12/14/09 07:241,2,4-Trichlorobenzene



2130 2500 NSL1079-01 85%ND 912171125 - 174mg/kg wet 12/14/09 07:24Trichlorofluoromethane

2440 2500 NSL1079-01 98%ND 912171110 - 152mg/kg wet 12/14/09 07:241,2,3-Trichloropropane



2090 2500 NSL1079-01 83%ND 912171132 - 163mg/kg wet 12/14/09 07:24Vinyl chloride

8390 7500 NSL1079-01 110%113 912171131 - 159mg/kg wet 12/14/09 07:24Xylenes, total






52.7 50.0 NSL1340-04 105%0.338 912223442 - 141ug/kg 12/12/09 23:44Benzene





62.0 50.0 NSL1340-04 123%0.687 912223410 - 199ug/kg 12/12/09 23:44Bromomethane

308 250 NSL1340-04 120%7.87 912223438 - 161ug/kg 12/12/09 23:442-Butanone

Page 46 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906

Analyte Units



Target

Range


Q

Analyzed

Date/Time

Sample

SpikedBatch


9122234-MS153.2 50.0 NSL1340-04 106%ND 912223410 - 170ug/kg 12/12/09 23:44sec-Butylbenzene




55.1 50.0 NSL1340-04 110%ND 912223430 - 159ug/kg 12/12/09 23:44Carbon Tetrachloride

























46.9 50.0 NSL1340-04 94%ND 912223440 - 151ug/kg 12/12/09 23:441,1-Dichloropropene








Page 47 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906

Analyte Units



Target

Range


Q

Analyzed

Date/Time

Sample

SpikedBatch


9122234-MS1282 250 NSL1340-04 113%ND 912223419 - 176ug/kg 12/12/09 23:444-Methyl-2-pentanone



2.44 50.0 NSL1340-04M8 5%ND 912223410 - 177ug/kg 12/12/09 23:44Styrene




51.6 50.0 NSL1340-04 102%0.464 912223445 - 145ug/kg 12/12/09 23:44Toluene




55.8 50.0 NSL1340-04 110%0.513 912223439 - 148ug/kg 12/12/09 23:441,1,1-Trichloroethane







174 150 NSL1340-04 115%0.261 912223431 - 159ug/kg 12/12/09 23:44Xylenes, total






9121727-MS142.6 46.0 NSL1053-01 93%ND 912172710 - 154mg/kg dry 12/15/09 03:01Diesel

0.890 0.919 NSL1053-01 Surrogate: o-Terphenyl 97% 912172729 - 141mg/kg dry 12/15/09 03:01

Page 48 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


Sample


Matrix Spike Dup


Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121616-MSD1ND 298 9 31 9121616 NSL0918-01 250 119%ug/L 56 - 150 12/10/09 09:49Acetone

ND 59.3 6 12 9121616 NSL0918-01 50.0 119%ug/L 65 - 151 12/10/09 09:49Benzene

ND 51.6 5 23 9121616 NSL0918-01 50.0 103%ug/L 69 - 142 12/10/09 09:49Bromobenzene

ND 62.7 4 32 9121616 NSL0918-01 50.0 125%ug/L 64 - 154 12/10/09 09:49Bromochloromethane

ND 70.5 5 13 9121616 NSL0918-01M7 50.0 141%ug/L 75 - 138 12/10/09 09:49Bromodichloromethane

ND 61.5 6 18 9121616 NSL0918-01 50.0 123%ug/L 55 - 153 12/10/09 09:49Bromoform

ND 64.3 15 50 9121616 NSL0918-01 50.0 129%ug/L 13 - 176 12/10/09 09:49Bromomethane

ND 325 10 37 9121616 NSL0918-01 250 130%ug/L 45 - 164 12/10/09 09:492-Butanone

ND 58.1 5 21 9121616 NSL0918-01 50.0 116%ug/L 68 - 159 12/10/09 09:49sec-Butylbenzene

ND 59.8 4 11 9121616 NSL0918-01 50.0 120%ug/L 67 - 151 12/10/09 09:49n-Butylbenzene

ND 57.4 4 20 9121616 NSL0918-01 50.0 115%ug/L 73 - 153 12/10/09 09:49tert-Butylbenzene

2.47 66.8 7 28 9121616 NSL0918-01 50.0 129%ug/L 33 - 187 12/10/09 09:49Carbon disulfide

ND 82.8 4 26 9121616 NSL0918-01M7 50.0 166%ug/L 64 - 157 12/10/09 09:49Carbon Tetrachloride

ND 57.5 4 11 9121616 NSL0918-01 50.0 115%ug/L 78 - 136 12/10/09 09:49Chlorobenzene

ND 62.4 4 16 9121616 NSL0918-01 50.0 125%ug/L 64 - 145 12/10/09 09:49Chlorodibromomethane

ND 57.4 7 35 9121616 NSL0918-01 50.0 115%ug/L 48 - 159 12/10/09 09:49Chloroethane

ND 73.9 5 32 9121616 NSL0918-01M7 50.0 148%ug/L 72 - 145 12/10/09 09:49Chloroform

ND 56.2 10 34 9121616 NSL0918-01 50.0 112%ug/L 10 - 194 12/10/09 09:49Chloromethane



ND 53.5 21 21 9121616 NSL0918-01 50.0 107%ug/L 49 - 162 12/10/09 09:491,2-Dibromo-3-chloropropane

ND 63.1 6 10 9121616 NSL0918-01 50.0 126%ug/L 70 - 152 12/10/09 09:491,2-Dibromoethane (EDB)

ND 69.2 3 11 9121616 NSL0918-01 50.0 138%ug/L 75 - 141 12/10/09 09:49Dibromomethane




ND 47.9 6 32 9121616 NSL0918-01 50.0 96%ug/L 23 - 159 12/10/09 09:49Dichlorodifluoromethane

ND 64.8 6 34 9121616 NSL0918-01 50.0 130%ug/L 64 - 154 12/10/09 09:491,1-Dichloroethane

ND 80.0 2 25 9121616 NSL0918-01M7 50.0 160%ug/L 72 - 137 12/10/09 09:491,2-Dichloroethane

ND 69.8 5 32 9121616 NSL0918-01 50.0 140%ug/L 57 - 154 12/10/09 09:49cis-1,2-Dichloroethene

ND 66.9 10 31 9121616 NSL0918-01 50.0 134%ug/L 34 - 151 12/10/09 09:491,1-Dichloroethene

ND 69.3 7 32 9121616 NSL0918-01 50.0 139%ug/L 57 - 157 12/10/09 09:49trans-1,2-Dichloroethene




ND 60.6 7 35 9121616 NSL0918-01 50.0 121%ug/L 56 - 156 12/10/09 09:49cis-1,3-Dichloropropene

ND 64.9 6 26 9121616 NSL0918-01 50.0 130%ug/L 47 - 157 12/10/09 09:49trans-1,3-Dichloropropene

ND 68.7 5 18 9121616 NSL0918-01 50.0 137%ug/L 70 - 155 12/10/09 09:491,1-Dichloropropene

ND 61.6 5 12 9121616 NSL0918-01 50.0 123%ug/L 68 - 157 12/10/09 09:49Ethylbenzene

ND 69.5 15 21 9121616 NSL0918-01B 50.0 139%ug/L 47 - 173 12/10/09 09:49Hexachlorobutadiene

ND 337 8 20 9121616 NSL0918-01 250 135%ug/L 57 - 154 12/10/09 09:492-Hexanone

Page 49 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


Sample




Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121616-MSD1ND 64.4 4 15 9121616 NSL0918-01 50.0 129%ug/L 69 - 139 12/10/09 09:49Isopropylbenzene

ND 57.6 5 18 9121616 NSL0918-01 50.0 115%ug/L 69 - 151 12/10/09 09:49p-Isopropyltoluene

ND 60.3 11 32 9121616 NSL0918-01 50.0 121%ug/L 56 - 152 12/10/09 09:49Methyl tert-Butyl Ether

ND 63.4 7 36 9121616 NSL0918-01 50.0 127%ug/L 71 - 136 12/10/09 09:49Methylene Chloride

ND 315 7 35 9121616 NSL0918-01 250 126%ug/L 62 - 159 12/10/09 09:494-Methyl-2-pentanone

ND 65.6 57 30 9121616 NSL0918-01R2 50.0 131%ug/L 56 - 161 12/10/09 09:49Naphthalene

ND 54.6 4 23 9121616 NSL0918-01 50.0 109%ug/L 61 - 167 12/10/09 09:49n-Propylbenzene

ND 61.3 3 29 9121616 NSL0918-01 50.0 123%ug/L 69 - 150 12/10/09 09:49Styrene



3.00 67.0 6 16 9121616 NSL0918-01 50.0 128%ug/L 63 - 155 12/10/09 09:49Tetrachloroethene

ND 57.6 6 35 9121616 NSL0918-01 50.0 115%ug/L 61 - 153 12/10/09 09:49Toluene

ND 82.6 66 28 9121616 NSL0918-01R2, M7, 50.0 165%ug/L 57 - 155 12/10/09 09:491,2,3-Trichlorobenzene

ND 72.7 33 23 9121616 NSL0918-01R2 50.0 145%ug/L 64 - 147 12/10/09 09:491,2,4-Trichlorobenzene



6.88 72.6 6 11 9121616 NSL0918-01 50.0 131%ug/L 74 - 139 12/10/09 09:49Trichloroethene

ND 70.0 5 33 9121616 NSL0918-01 50.0 140%ug/L 53 - 149 12/10/09 09:49Trichlorofluoromethane

ND 49.7 6 25 9121616 NSL0918-01 50.0 99%ug/L 49 - 148 12/10/09 09:491,2,3-Trichloropropane



ND 57.3 10 32 9121616 NSL0918-01 50.0 115%ug/L 53 - 137 12/10/09 09:49Vinyl chloride

ND 61.5 4 27 9121616 NSL0918-01 50.0 123%ug/L 62 - 167 12/10/09 09:49o-Xylene

ND 124 5 16 9121616 NSL0918-01 100 124%ug/L 69 - 155 12/10/09 09:49m,p-Xylene

ND 186 4 18 9121616 NSL0918-01 150 124%ug/L 68 - 158 12/10/09 09:49Xylenes, total

32.6 9121616 NSL0918-01 25.0 131%Surrogate: 1,2-Dichloroethane-d4 ug/L 63 - 140 12/10/09 09:49

28.9 9121616 NSL0918-01 25.0 115%Surrogate: Dibromofluoromethane ug/L 73 - 131 12/10/09 09:49

24.1 9121616 NSL0918-01 25.0 96%Surrogate: Toluene-d8 ug/L 80 - 120 12/10/09 09:49

23.1 9121616 NSL0918-01 25.0 92%Surrogate: 4-Bromofluorobenzene ug/L 79 - 125 12/10/09 09:49

9121711-MSD1ND 12700 0.3 50 9121711 NSL1079-01 12500 102%mg/kg wet 29 - 181 12/14/09 07:52Acetone

ND 2410 2 50 9121711 NSL1079-01 2500 97%mg/kg wet 42 - 141 12/14/09 07:52Benzene

ND 2720 3 50 9121711 NSL1079-01 2500 109%mg/kg wet 19 - 154 12/14/09 07:52Bromobenzene

ND 2320 3 50 9121711 NSL1079-01 2500 93%mg/kg wet 41 - 146 12/14/09 07:52Bromochloromethane

ND 2490 1 50 9121711 NSL1079-01 2500 100%mg/kg wet 32 - 155 12/14/09 07:52Bromodichloromethane

ND 2590 1 43 9121711 NSL1079-01 2500 104%mg/kg wet 10 - 155 12/14/09 07:52Bromoform

ND 2400 1 46 9121711 NSL1079-01 2500 96%mg/kg wet 10 - 199 12/14/09 07:52Bromomethane

ND 12700 3 50 9121711 NSL1079-01 12500 101%mg/kg wet 38 - 161 12/14/09 07:522-Butanone

ND 2790 3 50 9121711 NSL1079-01 2500 111%mg/kg wet 10 - 170 12/14/09 07:52sec-Butylbenzene

ND 2790 4 50 9121711 NSL1079-01 2500 112%mg/kg wet 10 - 183 12/14/09 07:52n-Butylbenzene

Page 50 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


Sample




Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121711-MSD1ND 2740 3 50 9121711 NSL1079-01 2500 110%mg/kg wet 11 - 165 12/14/09 07:52tert-Butylbenzene

ND 2370 3 48 9121711 NSL1079-01 2500 95%mg/kg wet 50 - 136 12/14/09 07:52Carbon disulfide

ND 2580 0.3 44 9121711 NSL1079-01 2500 103%mg/kg wet 30 - 159 12/14/09 07:52Carbon Tetrachloride

ND 2580 1 50 9121711 NSL1079-01 2500 103%mg/kg wet 25 - 151 12/14/09 07:52Chlorobenzene

ND 2640 0.7 48 9121711 NSL1079-01 2500 106%mg/kg wet 27 - 150 12/14/09 07:52Chlorodibromomethane

ND 2270 3 50 9121711 NSL1079-01 2500 91%mg/kg wet 15 - 197 12/14/09 07:52Chloroethane

ND 2470 1 50 9121711 NSL1079-01 2500 99%mg/kg wet 33 - 148 12/14/09 07:52Chloroform

ND 1800 2 44 9121711 NSL1079-01 2500 72%mg/kg wet 10 - 166 12/14/09 07:52Chloromethane



ND 2730 4 45 9121711 NSL1079-01 2500 109%mg/kg wet 10 - 167 12/14/09 07:521,2-Dibromo-3-chloropropane

ND 2850 2 45 9121711 NSL1079-01 2500 114%mg/kg wet 30 - 155 12/14/09 07:521,2-Dibromoethane (EDB)

ND 2460 2 50 9121711 NSL1079-01 2500 99%mg/kg wet 30 - 149 12/14/09 07:52Dibromomethane

122 2690 3 50 9121711 NSL1079-01 2500 103%mg/kg wet 10 - 170 12/14/09 07:521,4-Dichlorobenzene

ND 2800 4 50 9121711 NSL1079-01 2500 112%mg/kg wet 10 - 173 12/14/09 07:521,3-Dichlorobenzene

52.5 2910 4 50 9121711 NSL1079-01 2500 114%mg/kg wet 10 - 168 12/14/09 07:521,2-Dichlorobenzene

ND 1220 2 50 9121711 NSL1079-01 2500 49%mg/kg wet 10 - 188 12/14/09 07:52Dichlorodifluoromethane



548 3420 2 50 9121711 NSL1079-01 2500 115%mg/kg wet 32 - 150 12/14/09 07:52cis-1,2-Dichloroethene

ND 2610 2 50 9121711 NSL1079-01 2500 105%mg/kg wet 46 - 141 12/14/09 07:521,1-Dichloroethene

ND 2490 2 40 9121711 NSL1079-01 2500 100%mg/kg wet 41 - 146 12/14/09 07:52trans-1,2-Dichloroethene




ND 2860 3 50 9121711 NSL1079-01 2500 114%mg/kg wet 23 - 152 12/14/09 07:52cis-1,3-Dichloropropene

ND 2410 1 48 9121711 NSL1079-01 2500 96%mg/kg wet 24 - 151 12/14/09 07:52trans-1,3-Dichloropropene

ND 2560 1 50 9121711 NSL1079-01 2500 103%mg/kg wet 40 - 151 12/14/09 07:521,1-Dichloropropene

ND 2880 0.3 50 9121711 NSL1079-01 2500 115%mg/kg wet 21 - 165 12/14/09 07:52Ethylbenzene

ND 4190 4 50 9121711 NSL1079-01 2500 168%mg/kg wet 10 - 173 12/14/09 07:52Hexachlorobutadiene

ND 10900 28 50 9121711 NSL1079-01 12500 87%mg/kg wet 13 - 174 12/14/09 07:522-Hexanone

ND 2670 0.2 50 9121711 NSL1079-01 2500 107%mg/kg wet 20 - 139 12/14/09 07:52Isopropylbenzene

ND 2680 4 50 9121711 NSL1079-01 2500 107%mg/kg wet 10 - 164 12/14/09 07:52p-Isopropyltoluene

ND 2530 5 50 9121711 NSL1079-01 2500 101%mg/kg wet 34 - 154 12/14/09 07:52Methyl tert-Butyl Ether

ND 2430 4 50 9121711 NSL1079-01 2500 97%mg/kg wet 36 - 163 12/14/09 07:52Methylene Chloride

ND 14200 4 45 9121711 NSL1079-01 12500 114%mg/kg wet 19 - 176 12/14/09 07:524-Methyl-2-pentanone

ND 3390 0.1 50 9121711 NSL1079-01 2500 136%mg/kg wet 10 - 160 12/14/09 07:52Naphthalene

ND 2950 3 50 9121711 NSL1079-01 2500 118%mg/kg wet 16 - 174 12/14/09 07:52n-Propylbenzene

ND 2590 1 50 9121711 NSL1079-01 2500 104%mg/kg wet 10 - 177 12/14/09 07:52Styrene



Page 51 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


Sample




Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9121711-MSD1ND 2680 0.09 50 9121711 NSL1079-01 2500 107%mg/kg wet 45 - 145 12/14/09 07:52Toluene

ND 3830 2 50 9121711 NSL1079-01 2500 153%mg/kg wet 10 - 182 12/14/09 07:521,2,3-Trichlorobenzene

930 5100 14 50 9121711 NSL1079-01 2500 167%mg/kg wet 10 - 175 12/14/09 07:521,2,4-Trichlorobenzene

ND 2710 3 50 9121711 NSL1079-01 2500 108%mg/kg wet 43 - 145 12/14/09 07:521,1,2-Trichloroethane

ND 2530 0.2 41 9121711 NSL1079-01 2500 101%mg/kg wet 39 - 148 12/14/09 07:521,1,1-Trichloroethane

ND 2140 0.4 47 9121711 NSL1079-01 2500 85%mg/kg wet 25 - 174 12/14/09 07:52Trichlorofluoromethane

ND 2540 4 47 9121711 NSL1079-01 2500 102%mg/kg wet 10 - 152 12/14/09 07:521,2,3-Trichloropropane



ND 2150 3 39 9121711 NSL1079-01 2500 86%mg/kg wet 32 - 163 12/14/09 07:52Vinyl chloride

113 8410 0.2 50 9121711 NSL1079-01 7500 111%mg/kg wet 31 - 159 12/14/09 07:52Xylenes, total





9122234-MSD169.6 34.5 169 50 9122234 NSL1340-04R2, M8 250 -14%ug/kg 29 - 181 12/13/09 00:13Acetone

0.338 48.9 7 50 9122234 NSL1340-04 50.0 97%ug/kg 42 - 141 12/13/09 00:13Benzene

ND 48.8 0.1 50 9122234 NSL1340-04 50.0 98%ug/kg 19 - 154 12/13/09 00:13Bromobenzene



ND 42.8 0.7 43 9122234 NSL1340-04 50.0 86%ug/kg 10 - 155 12/13/09 00:13Bromoform

0.687 59.5 4 46 9122234 NSL1340-04 50.0 118%ug/kg 10 - 199 12/13/09 00:13Bromomethane

7.87 276 11 50 9122234 NSL1340-04 250 107%ug/kg 38 - 161 12/13/09 00:132-Butanone












ND 49.2 0.9 50 9122234 NSL1340-04 50.0 98%ug/kg 19 - 163 12/13/09 00:134-Chlorotoluene

ND 44.4 3 45 9122234 NSL1340-04 50.0 89%ug/kg 10 - 167 12/13/09 00:131,2-Dibromo-3-chloropropane




Page 52 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


Sample




Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9122234-MSD1ND 45.1 1 50 9122234 NSL1340-04 50.0 90%ug/kg 10 - 173 12/13/09 00:131,3-Dichlorobenzene












ND 51.6 1 48 9122234 NSL1340-04 50.0 103%ug/kg 24 - 151 12/13/09 00:13trans-1,3-Dichloropropene


ND 56.1 0.5 50 9122234 NSL1340-04 50.0 112%ug/kg 21 - 165 12/13/09 00:13Ethylbenzene



ND 50.5 0.7 50 9122234 NSL1340-04 50.0 101%ug/kg 20 - 139 12/13/09 00:13Isopropylbenzene







ND 2.44 0 50 9122234 NSL1340-04M8 50.0 5%ug/kg 10 - 177 12/13/09 00:13Styrene




0.464 54.5 5 50 9122234 NSL1340-04 50.0 108%ug/kg 45 - 145 12/13/09 00:13Toluene




0.513 50.4 10 41 9122234 NSL1340-04 50.0 100%ug/kg 39 - 148 12/13/09 00:131,1,1-Trichloroethane







0.261 170 2 50 9122234 NSL1340-04 150 113%ug/kg 31 - 159 12/13/09 00:13Xylenes, total


Page 53 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


Sample




Q

Spike

Conc % Rec.

Target

Range

Analyzed

Date/TimeLimit


9122234-MSD147.8 9122234 NSL1340-04 50.0 96%Surrogate: Dibromofluoromethane ug/kg 75 - 125 12/13/09 00:13




9121727-MSD1ND 35.8 17 48 9121727 NSL1053-01 45.4 79%mg/kg dry 10 - 154 12/15/09 03:18Diesel

0.826 9121727 NSL1053-01 0.908 91%Surrogate: o-Terphenyl mg/kg dry 29 - 141 12/15/09 03:18

Page 54 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


Method Matrix



Soil XN/A XSW846 8260B

Water XN/A XSW846 8260B

SoilSW-846

SoilTPH-D/Finger

Page 55 of 56


Client

Attn


P. O. Box 3050

Sumter, SC 29151

Robbin Brown

Project Name:

Work Order:

SAP-3

Received:


12/08/09 08:00

NSL0906


B Analyte was detected in the associated Method Blank.

J Analyte detected at a level less than the Reporting Limit (RL) and greater than or equal to the Method Detection Limit (MDL).

Concentrations within this range are estimated.L Laboratory Control Sample and/or Laboratory Control Sample Duplicate recovery was above the acceptance limits. Analyte not

detected, data not impacted.M7 The MS and/or MSD were above the acceptance limits. See Blank Spike (LCS).

M8 The MS and/or MSD were below the acceptance limits. See Blank Spike (LCS).

MNR No results were reported for the MS/MSD. The sample used for the MS/MSD required dilution due to the sample matrix.

Because of this, the spike compounds were diluted below the detection limit.QP6 The contamination did not match any standards in our library.

R2 The RPD exceeded the acceptance limit.

RL1 Reporting limit raised due to sample matrix effects.



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PHASE II ENVIRONMENTAL SITE ASSESSMENT SUMTER …