Perseverance Mill, Albion Street, Padiham Supplementary ... · Supplementary Stockpile Investigation Further to the completion of our recent Ground Investigation works and interpretive

Ref – QY14-1 –January 2014 – Prepared by A Edgar

Environmental Engineering Partnership Limited trading as E3P Registered in England No: 08725262 Registered Office: Heliport Business Park, Liverpool Road, Eccles, Salford, M30 7RU

E3P Heliport Business Park

Liverpool Road Eccles

Manchester M30 7RU

Manchester / London / Edinburgh

[email protected] http://www.E3P.co.uk

Ref: 11-360-L2 Date: 13th December 2016 Alan Johnston Partnerships 4th Floor 1 Dale Street Liverpool L2 2ET BY Email (KennyO'[email protected])

Perseverance Mill, Albion Street, Padiham Supplementary Stockpile Investigation Further to the completion of our recent Ground Investigation works and interpretive Geo-Environmental Report (October 2016), E3P has undertaken a supplementary intrusive investigation of stockpiles currently on-site. Exploratory fieldwork was completed on the 18th November 2016 comprising 15 No. mechanically excavated trial pits within four stockpiles of demolition materials on the subject site. Exploratory hole locations were advanced to collect samples to enable the completion of a Tier 1 assessment to determine chemical suitability of materials and appropriate placement on the site to ensure no risk to the identified receptors. A snapshot of the exploratory hole locations and stockpiles is shown below in Figure 1.1: Figure 1.1 Exploratory hole and stockpile locations

A

B

C

D

Perseverance Mill Alan Johnston Partnership December 2016

The fieldworks are summarised in Table 1.1 below: Table 1.1 Summary of Fieldwork

POTENTIAL SOURCE / RATIONALE LOCATION HOLE TYPE MAXIMUM DEPTH

(M BGL)

Investigation of Stockpile A to examine the nature of material and gain environmental samples.

SP201

SP207

SP208

Mechanically

Excavated Trial

Pit

1.50

Investigation of Stockpile B to examine the nature of material and gain environmental samples.

SP202

SP209

SP210

2.00

Investigation of Stockpile C to examine the nature of material and gain environmental samples.

SP203

SP211

SP212

SP213

SP214

SP215

4.00

Investigation of Stockpile D to examine the nature of material and gain environmental samples.

SP204

SP205

SP206

3.00

The sampling locations are illustrated in Drawing 11-360-005 attached to this letter. The ground conditions encountered are indicated on the logs attached to this letter. Summary of Ground Conditions Made Ground was encountered within all exploratory hole locations to depths of between 1.00m and 4.00m. Made Ground within Stockpile A and B generally consisted of brown very gravelly sand or sandy gravel, where gravel consisted of brick, wood, concrete, metal, plastic, insulation and asbestos sheeting. Stockpile C consisted of a brown slightly clayey gravelly sand with brick, wood, plastic, sandstone, polystyrene and cement bonded asbestos sheeting. Within Stockpile D the Made Ground consisted of slightly clayey sandy gravel with cobbles, gravel is brick, plastic, wood, concrete, metal and sandstone. Human Health Risk Assessment Samples retrieved from the stockpiled materials have been submitted to I2 Analytical Laboratory for analysis of speciated PAHs, heavy metals and asbestos identification and quantification. A Tier 1 Human Health Risk Assessment has been completed using the chemical analysis results and comparing to the Tier 1 screening values for the protection of human health in a residential setting. The results of this comparison are summarised within Table 1.2 overleaf.


Table 1.2 Summary of Inorganic and Hydrocarbon Toxicity Assessment for a Residential End Use

DETERMINANT UNIT GAC N MC LOC.

OF EX PATH-WAY

ASSESSMENT

Arsenic mg/kg 37 12 50 SP215 0.5 1 Further Action

Cadmium mg/kg 17 12 2.1 N/A 1 No Further Action

Chromium (VI) mg/kg 910 12 54 N/A 1 No Further Action

Lead mg/kg 200 12 3700

SP201 1.00 SP207 0.50 SP208 1.00 SP210 1.50 SP211 1.00 SP212 1.80 SP213 1.00 SP214 2.00 SP215 0.50

1 Further Action

Mercury mg/kg 11 12 0.7 N/A 2 No Further Action

Nickel mg/kg 180 12 93 N/A 1 No Further Action

Selenium mg/kg 250 12 <1.0 N/A 1 No Further Action

Copper mg/kg 2400 12 700 N/A 1 No Further Action

Zinc mg/kg 3700 12 1200 N/A 1 No Further Action

Cyanide - Total mg/kg 791 12 - - 1 -

Phenols - Total. mg/kg 210 12 - - 1 -

Asbestos Fibres NFD 12 detected All locations Further Action

Naphthalene mg/kg 2.3 12 1.7 N/A 2 No Further Action

Acenaphthylene mg/kg 170 12 0.59 N/A 3 No Further Action

Acenaphthene mg/kg 210 12 1.7 N/A 1 No Further Action

Fluorene mg/kg 170 12 1.6 N/A 1 No Further Action

Phenanthrene mg/kg 95 12 11 N/A 3 No Further Action

Anthracene mg/kg 2400 12 2.6 N/A 3 No Further Action

Fluoranthene mg/kg 280 12 14 N/A 3 No Further Action

Pyrene mg/kg 620 12 12 N/A 3 No Further Action

Benzo(a)Anthracene mg/kg 7.2 12 7.8 SP212 1.80 3 Further Action

Chrysene mg/kg 15 12 5.9 N/A 3 No Further Action

Benzo(b)Fluoranthene mg/kg 2.6 12 8.3

SP205 0.50 SP206 1.00 SP212 1.80 SP213 1.00 SP214 2.00 SP215 0.50

3 Further Action

Benzo(k)Fluoranthene mg/kg 77 12 3.3 N/A No Further Action

Benzo(a)Pyrene** mg/kg 2.2 12 6.5

SP205 0.50 SP206 1.00 SP212 1.80 SP213 1.00 SP215 0.50

3 Further Action

Indeno(123-cd)Pyrene mg/kg 27 12 2.7 N/A 3 No Further Action

Dibenzo(a,h)Anthracene mg/kg 0.24

12

0.74

SP205 0.50 SP206 1.00 SP212 1.80 SP213 1.00 SP214 2.00 SP215 0.50

3 Further Action

Benzo(ghi)Perylene mg/kg 320 12 3.3 N/A 3 No Further Action


Notes Main Exposure Pathways: 1 = Soil Ingestion, 2 = Vapour Inhalation (indoor), 3 = Dermal Contact & Ingestion, 4 = Dust Inhalation. Abbreviations: GAC = General Assessment Criteria, n = number of samples, MC = Maximum Concentration; Loc of Ex = Location of Exceedance; NFD = No Fibres Detected * The Tier 1 GAC for the hydrocarbon fraction is derived from the CIEH assessment for petroleum hydrocarbons Criteria Working Group (CWG) for both aliphatic and aromatic compounds. E3P has utilised the Tier 1 values for aliphatic compounds for the volatile and semi volatile fractions (C5-C12) and the Tier 1 values for aromatic compound for the non-volatile fractions (C12-C35). The comparison of a total (aliphatic/aromatic) compounds to an individual fraction is considered to be a conservative approach and satisfactory for the protection of human health.

Referring to Table 1.2, the results of this direct comparison indicate that the data exceeds the preliminary Tier 1 risk assessment screening criteria for a residential end use for the following contaminants:

Arsenic Lead Asbestos Benzo(a)Anthracene Benzo(b)Fluoranthene Benzo(a)Pyrene Dibenzo(a,h)Anthracene

Asbestos fibres, insulation lagging and cement type materials were identified within all samples sent for testing in the form of chrysotile, amosite and crocidolite. Quantification analysis was undertaken on all samples, identifying a maximum of 1.43% at SP201 within Stockpile A. Only one sample was identified to comprise trace fibres (<0.001%) with all other samples exceeding this. No elevated Naphthalene were identified within the stockpiles, however there were exceedances of Benzo(a)Anthracene, Benzo(b)Fluoranthene, Benzo(a)Pyrene, Dibenzo(a,h)Anthracene with SP205, SP206, SP212, SP213, SP214 and SP215, in addition to arsenic and lead. The elevated concentrations of heavy metals and PAHs have a primary exposure pathway of dermal contact, soil ingestion. As such, should this material be used on site it should be placed below a 600mm cover system comprising 150mm topsoil and 450mm subsoil. Upon installation, these elevated concentrations will pose no unacceptable risk to the future site users. Given the presence of asbestos (Chrysotile, Amosite, Crocidolite) within all samples, a suitably detailed remediation strategy will be required to document the safe handling, management and placement of all Made Ground to ensure that no unacceptable degree of risk is presented to construction workers or future site occupants. It is considered that the risks to construction workers during the development phase can be mitigated through the use of appropriate health and safety controls, PPE and good site hygiene. E3P has produced as asbestos specific CSM which identifies the locations that asbestos impacted soils may be placed in a residential setting to ensure there is no unacceptable level of risk to the future site users, included below as Figure 1.2 overleaf:


Figure 1.2 Asbestos Conceptual Site Model

Asbestos Quantification has identified 11 out of the 12 samples tested to have asbestos levels above 0.001%. Therefore, should this impacted material be kept on-site, it should be placed beneath proposed plots which are intended for vibro ground improvement to a depth of >1.00mbgl (thus soils are not being further disturbed) and below gardens at >1.00m bgl. These asbestos impacted materials will require careful and regulatory approved handling using dust suppression and HSG248 asbestos in air monitoring by way of validation to confirm there have been no asbestos fibre release to the air. There are no materials present on site within stockpiles that are chemically suitable for use as the topsoil or subsoil element of the cover system, therefore any topsoil or subsoil will require importing with the appropriate quality checks. I trust that the above information is sufficient at this time and if you require anything further please do not hesitate to contact me. Yours sincerely, For and on behalf of E3P Ltd

Stephanie Cox Associate Director


Appendix I-Drawings


Appendix II-Exploratory Hole Logs

Trial Pit LogTrialpit No

SP201Sheet 1 of 1

Project Name: Perseverance Mill

Project No.11360

Co-ords:Level:

- Date18/11/2016

Location:

Client:

Albion Street, Padiham

Alan Johnston Partnership LLP

Dimensions (m):

Depth1.50

Scale1:25

LoggedR. Hodnett

Remarks:

Stability:

Complete.

Samples and In Situ Testing

Depth Type ResultsDepth

(m)

1.50

Level(m) Legend Stratum Description

MADE GROUND: Brown very gravelly fine to coarse sand with cobbles. Gravel is fine to coarse angular to sub-rounded of brick, wood, concrete, metal, plastic and insulation.

End of pit at 1.50 m

1

2

3

4

5

1.00 ES


SP202Sheet 1 of 1


Project No.11360

Co-ords:Level:

- Date18/11/2016

Location:

Client:



Dimensions (m):

Depth1.00

Scale1:25

LoggedR. Hodnett

Remarks:

Stability:

Complete.



(m)

1.00


MADE GROUND: Brown very gravelly fine to coarse sand with cobbles. Gravel is fine to coarse angular to sub-rounded of brick, wood, concrete, metal, plastic and insulation.

End of pit at 1.00 m 1

2

3

4

5


SP203Sheet 1 of 1


Project No.11360

Co-ords:Level:

- Date18/11/2016

Location:

Client:



Dimensions (m):

Depth2.50

Scale1:25

LoggedR. Hodnett

Remarks:

Stability:

Complete.



(m)

2.50


MADE GROUND: Brown gravelly sand. Gravel is fine to coarse angular to sub-rounded of asbestos, brick, plastic, concrete, sandstone, wood and glass.


1

2

3

4

5


SP204Sheet 1 of 1


Project No.11360

Co-ords:Level:

- Date18/11/2016

Location:

Client:



Dimensions (m):

Depth1.50

Scale1:25

LoggedR. Hodnett

Remarks:

Stability:

Complete.



(m)

1.50


MADE GROUND: Brown slightly clayey sandy gravel with cobbles. Gravel is fine to coarse angular to sub-rounded of brick, plastic, wood, concrete, metal and sandstone.


1

2

3

4

5

1.00 ES


SP205Sheet 1 of 1


Project No.11360

Co-ords:Level:

- Date18/11/2016

Location:

Client:



Dimensions (m):

Depth3.00

Scale1:25

LoggedR. Hodnett

Remarks:

Stability:

Complete.



(m)

3.00




1

2

3

4

5

0.50 ES


SP206Sheet 1 of 1


Project No.11360

Co-ords:Level:

- Date18/11/2016

Location:

Client:



Dimensions (m):

Depth2.00

Scale1:25

LoggedR. Hodnett

Remarks:

Stability:

Complete.



(m)

2.00




1

2

3

4

5

1.00 ES


SP207Sheet 1 of 1


Project No.11360

Co-ords:Level:

- Date18/11/2016

Location:

Client:



Dimensions (m):

Depth1.50

Scale1:25

LoggedR. Hodnett

Remarks:

Stability:

Complete.



(m)

1.50


MADE GROUND: Brown very sandy gravel with cobbles and boulders. Gravel is fine to coarse angular to sub-rounded of brick, asbestos sheeting, plastic, metal, concrete and metal.


1

2

3

4

5

0.50 ES


SP208Sheet 1 of 1


Project No.11360

Co-ords:Level:

- Date18/11/2016

Location:

Client:



Dimensions (m):

Depth1.50

Scale1:25

LoggedR. Hodnett

Remarks:

Stability:

Complete.



(m)

1.50


MADE GROUND: Brown sandy gravel with cobbles and boulders of concrete. Gravel is fine to coarse angular to sub-rounded of brick, asbestos sheeting, wood, plastic, metal and slate.


1

2

3

4

5

1.00 ES


SP209Sheet 1 of 1


Project No.11360

Co-ords:Level:

- Date18/11/2016

Location:

Client:



Dimensions (m):

Depth1.00

Scale1:25

LoggedR. Hodnett

Remarks:

Stability:

Complete.



(m)

1.00


MADE GROUND: Grey brown sandy gravel. Gravel is fine to coarse angular to sub-rounded of asbestos sheeting, plastic, brick and sandstone.


2

3

4

5


SP210Sheet 1 of 1


Project No.11360

Co-ords:Level:

- Date18/11/2016

Location:

Client:



Dimensions (m):

Depth2.00

Scale1:25

LoggedR. Hodnett

Remarks:

Stability:

Complete.



(m)

2.00


MADE GROUND: Grey brown sandy gravel. Gravel is fine to coarse angular to sub-rounded of asbestos sheeting, plastic, brick and sandstone.


1

2

3

4

5

1.50 ES


SP211Sheet 1 of 1


Project No.11360

Co-ords:Level:

- Date18/11/2016

Location:

Client:



Dimensions (m):

Depth2.00

Scale1:25

LoggedR. Hodnett

Remarks:

Stability:

Complete.



(m)

2.00


MADE GROUND: Brown slightly clayey very gravelly medium to coarse sand with cobbles of brick and concrete. Gravel is fine to coarse angular to sub-rounded of slate, metal, asbestos, brick, wood and plastic.


1

2

3

4

5

1.00 ES


SP212Sheet 1 of 1


Project No.11360

Co-ords:Level:

- Date18/11/2016

Location:

Client:



Dimensions (m):

Depth2.00

Scale1:25

LoggedR. Hodnett

Remarks:

Stability:

Complete.



(m)

2.00




1

2

3

4

5

1.80 ES


SP213Sheet 1 of 1


Project No.11360

Co-ords:Level:

- Date18/11/2016

Location:

Client:



Dimensions (m):

Depth2.00

Scale1:25

LoggedR. Hodnett

Remarks:

Stability:

Complete.



(m)

2.00




1

2

3

4

5

1.00 ES


SP214Sheet 1 of 1


Project No.11360

Co-ords:Level:

- Date18/11/2016

Location:

Client:



Dimensions (m):

Depth4.00

Scale1:25

LoggedR. Hodnett

Remarks:

Stability:

Complete.



(m)

4.00


MADE GROUND: Brown very gravelly fine to coarse sand. Gravel is fine to coarse angular to sub-rounded of brick, wood, plastic, sandstone and polystyrene.


1

2

3

4

5

2.00 ES


SP215Sheet 1 of 1


Project No.11360

Co-ords:Level:

- Date18/11/2016

Location:

Client:



Dimensions (m):

Depth1.00

Scale1:25

LoggedR. Hodnett

Remarks:

Stability:

Complete.



(m)

1.00


MADE GROUND: Brown very gravelly fine to coarse sand. Gravel is fine to coarse angular to sub-rounded of brick, wood, plastic, sandstone and polystyrene.


2

3

4

5

0.50 ES


Appendix III-Chemical Testing Results

This certificate should not be reproduced, except in full, without the express permission of the laboratory. The results included within the report are representative of the samples submitted for analysis.

Iss No 16-33631-1 Perseverance Mill, Padiham 11-360

Page 1 of 7

Analytical Report Number: 16-33631

Project / Site name: Perseverance Mill, Padiham

Your Order No: 11360-4905-NS

Lab Sample Number 662795 662796 662797 662798 662799

Sample Reference SP201 SP204 SP205 SP206 SP207

Sample Number None Supplied None Supplied None Supplied None Supplied None Supplied

Depth (m) 1.00 1.00 0.50 1.00 0.50

Date Sampled 18/11/2016 18/11/2016 18/11/2016 18/11/2016 18/11/2016

Time Taken None Supplied None Supplied None Supplied None Supplied None Supplied

Analytical Parameter

(Soil Analysis)

Un

its

Lim

it of

de

tectio

n

Accre

dita

tion

Sta

tus

Stone Content % 0.1 NONE < 0.1 < 0.1 < 0.1 < 0.1 < 0.1

Moisture Content % N/A NONE 22 19 15 16 24

Total mass of sample received kg 0.001 NONE 0.52 0.59 0.57 0.56 0.54

Asbestos in Soil Screen / Identification Name Type N/A ISO 17025Chrysotile &

Amosite

Chrysotile &

Amosite &

Crocidolite

Chrysotile &

Amosite

Chrysotile &

Crocidolite

Chrysotile &

Amosite &

Crocidolite

Asbestos in Soil Type N/A ISO 17025 Detected Detected Detected Detected Detected

Asbestos Quantification (Stage 2) % 0.001 ISO 17025 1.434 0.009 0.001 < 0.001 0.017

Asbestos Quantification Total % 0.001 ISO 17025 1.43 0.009 0.001 < 0.001 0.017

Speciated PAHs

Naphthalene mg/kg 0.05 MCERTS < 0.05 < 0.05 0.54 1.7 < 0.05

Acenaphthylene mg/kg 0.1 MCERTS < 0.10 < 0.10 < 0.10 < 0.10 < 0.10

Acenaphthene mg/kg 0.1 MCERTS 0.31 0.42 0.96 1.7 < 0.10

Fluorene mg/kg 0.1 MCERTS 0.25 0.27 0.78 1.6 < 0.10

Phenanthrene mg/kg 0.1 MCERTS 2.3 2.8 7.1 11 0.79

Anthracene mg/kg 0.1 MCERTS 0.37 0.53 1.1 2.4 0.13

Fluoranthene mg/kg 0.1 MCERTS 3.3 4.0 11 13 0.97

Pyrene mg/kg 0.1 MCERTS 2.7 3.4 8.6 10 0.78

Benzo(a)anthracene mg/kg 0.1 MCERTS 1.4 1.7 4.6 5.3 0.48

Chrysene mg/kg 0.05 MCERTS 1.3 1.5 3.9 4.3 0.43

Benzo(b)fluoranthene mg/kg 0.1 MCERTS 1.5 2.0 5.5 5.1 0.48

Benzo(k)fluoranthene mg/kg 0.1 MCERTS 0.93 0.96 2.0 2.5 0.33

Benzo(a)pyrene mg/kg 0.1 MCERTS 1.0 1.5 3.7 3.3 0.32

Indeno(1,2,3-cd)pyrene mg/kg 0.1 MCERTS 0.48 0.67 1.4 1.6 < 0.10

Dibenz(a,h)anthracene mg/kg 0.1 MCERTS < 0.10 < 0.10 0.46 0.37 < 0.10

Benzo(ghi)perylene mg/kg 0.05 MCERTS 0.68 0.80 1.8 2.0 < 0.05

Total PAH

Speciated Total EPA-16 PAHs mg/kg 1.6 MCERTS 16.5 20.4 53.1 66.2 4.71

Heavy Metals / Metalloids

Arsenic (aqua regia extractable) mg/kg 1 MCERTS 12 12 13 11 15

Barium (aqua regia extractable) mg/kg 1 MCERTS 520 310 200 190 640

Beryllium (aqua regia extractable) mg/kg 0.06 MCERTS 0.84 1.0 0.63 0.69 0.81

Boron (water soluble) mg/kg 0.2 MCERTS 1.7 2.2 2.0 1.4 3.4

Cadmium (aqua regia extractable) mg/kg 0.2 MCERTS 0.6 0.5 0.4 0.4 0.4

Chromium (aqua regia extractable) mg/kg 1 MCERTS 29 41 23 23 25

Copper (aqua regia extractable) mg/kg 1 MCERTS 60 62 50 53 68

Lead (aqua regia extractable) mg/kg 1 MCERTS 220 130 100 100 230

Mercury (aqua regia extractable) mg/kg 0.3 MCERTS < 0.3 < 0.3 < 0.3 < 0.3 0.4

Nickel (aqua regia extractable) mg/kg 1 MCERTS 29 33 27 25 35

Selenium (aqua regia extractable) mg/kg 1 MCERTS < 1.0 < 1.0 < 1.0 < 1.0 < 1.0

Vanadium (aqua regia extractable) mg/kg 1 MCERTS 33 36 60 39 34

Zinc (aqua regia extractable) mg/kg 1 MCERTS 530 220 170 160 760



Page 2 of 7




Lab Sample Number

Sample Reference

Sample Number

Depth (m)

Date Sampled

Time Taken


(Soil Analysis)

Un

its

Lim

it of

de

tectio

n

Accre

dita

tion

Sta

tus

Stone Content % 0.1 NONE

Moisture Content % N/A NONE

Total mass of sample received kg 0.001 NONE

Asbestos in Soil Screen / Identification Name Type N/A ISO 17025

Asbestos in Soil Type N/A ISO 17025

Asbestos Quantification (Stage 2) % 0.001 ISO 17025

Asbestos Quantification Total % 0.001 ISO 17025

Speciated PAHs

Naphthalene mg/kg 0.05 MCERTS

Acenaphthylene mg/kg 0.1 MCERTS

Acenaphthene mg/kg 0.1 MCERTS

Fluorene mg/kg 0.1 MCERTS

Phenanthrene mg/kg 0.1 MCERTS

Anthracene mg/kg 0.1 MCERTS

Fluoranthene mg/kg 0.1 MCERTS

Pyrene mg/kg 0.1 MCERTS

Benzo(a)anthracene mg/kg 0.1 MCERTS

Chrysene mg/kg 0.05 MCERTS

Benzo(b)fluoranthene mg/kg 0.1 MCERTS

Benzo(k)fluoranthene mg/kg 0.1 MCERTS

Benzo(a)pyrene mg/kg 0.1 MCERTS

Indeno(1,2,3-cd)pyrene mg/kg 0.1 MCERTS

Dibenz(a,h)anthracene mg/kg 0.1 MCERTS

Benzo(ghi)perylene mg/kg 0.05 MCERTS

Total PAH

Speciated Total EPA-16 PAHs mg/kg 1.6 MCERTS


Arsenic (aqua regia extractable) mg/kg 1 MCERTS

Barium (aqua regia extractable) mg/kg 1 MCERTS

Beryllium (aqua regia extractable) mg/kg 0.06 MCERTS

Boron (water soluble) mg/kg 0.2 MCERTS

Cadmium (aqua regia extractable) mg/kg 0.2 MCERTS

Chromium (aqua regia extractable) mg/kg 1 MCERTS

Copper (aqua regia extractable) mg/kg 1 MCERTS

Lead (aqua regia extractable) mg/kg 1 MCERTS

Mercury (aqua regia extractable) mg/kg 0.3 MCERTS

Nickel (aqua regia extractable) mg/kg 1 MCERTS

Selenium (aqua regia extractable) mg/kg 1 MCERTS

Vanadium (aqua regia extractable) mg/kg 1 MCERTS

Zinc (aqua regia extractable) mg/kg 1 MCERTS

662800 662801 662802 662803 662804

SP208 SP210 SP211 SP212 SP213

None Supplied None Supplied None Supplied None Supplied None Supplied

1.00 1.50 1.00 1.80 1.00

18/11/2016 18/11/2016 18/11/2016 18/11/2016 18/11/2016

None Supplied None Supplied None Supplied None Supplied None Supplied

< 0.1 < 0.1 < 0.1 < 0.1 < 0.1

21 32 31 25 25

0.47 0.36 0.46 0.45 0.48

Chrysotile

Chrysotile,

Amosite,

Crocidolite

Chrysotile,

AmositeChrysotile

Chrysotile &

Amosite

Detected Detected Detected Detected Detected

0.168 1.275 0.064 0.021 0.033

0.168 1.28 0.064 0.021 0.033

< 0.05 < 0.05 < 0.05 < 0.05 < 0.05

< 0.10 < 0.10 < 0.10 0.59 < 0.10

< 0.10 < 0.10 < 0.10 0.30 0.62

< 0.10 < 0.10 < 0.10 0.45 0.49

0.44 0.72 0.79 6.0 6.3

< 0.10 0.20 0.24 2.6 1.6

0.67 1.1 2.0 14 12

0.64 0.97 1.9 12 10

0.39 0.55 1.1 7.8 5.9

0.34 0.52 0.97 5.9 4.6

0.49 0.73 1.4 8.3 7.5

0.24 0.36 0.63 3.3 2.4

0.27 0.41 0.98 6.5 4.8

< 0.10 0.31 0.50 2.7 2.0

< 0.10 < 0.10 < 0.10 0.74 0.67

< 0.05 0.37 0.62 3.3 2.9

3.48 6.22 11.2 74.7 61.8

13 8.9 18 13 11

480 450 380 390 410

1.2 0.63 0.55 0.65 0.57

2.7 5.3 8.4 5.3 7.2

0.9 0.9 0.9 1.1 0.7

27 27 26 54 34

85 95 300 160 170

480 300 490 490 750

< 0.3 0.5 0.6 0.6 < 0.3

38 34 32 47 42

< 1.0 < 1.0 < 1.0 < 1.0 < 1.0

31 25 26 29 31

320 1100 810 530 540



Page 3 of 7




Lab Sample Number

Sample Reference

Sample Number

Depth (m)

Date Sampled

Time Taken


(Soil Analysis)

Un

its

Lim

it of

de

tectio

n

Accre

dita

tion

Sta

tus

Stone Content % 0.1 NONE

Moisture Content % N/A NONE

Total mass of sample received kg 0.001 NONE

Asbestos in Soil Screen / Identification Name Type N/A ISO 17025

Asbestos in Soil Type N/A ISO 17025

Asbestos Quantification (Stage 2) % 0.001 ISO 17025

Asbestos Quantification Total % 0.001 ISO 17025

Speciated PAHs

Naphthalene mg/kg 0.05 MCERTS

Acenaphthylene mg/kg 0.1 MCERTS

Acenaphthene mg/kg 0.1 MCERTS

Fluorene mg/kg 0.1 MCERTS

Phenanthrene mg/kg 0.1 MCERTS

Anthracene mg/kg 0.1 MCERTS

Fluoranthene mg/kg 0.1 MCERTS

Pyrene mg/kg 0.1 MCERTS

Benzo(a)anthracene mg/kg 0.1 MCERTS

Chrysene mg/kg 0.05 MCERTS

Benzo(b)fluoranthene mg/kg 0.1 MCERTS

Benzo(k)fluoranthene mg/kg 0.1 MCERTS

Benzo(a)pyrene mg/kg 0.1 MCERTS

Indeno(1,2,3-cd)pyrene mg/kg 0.1 MCERTS

Dibenz(a,h)anthracene mg/kg 0.1 MCERTS

Benzo(ghi)perylene mg/kg 0.05 MCERTS

Total PAH

Speciated Total EPA-16 PAHs mg/kg 1.6 MCERTS


Arsenic (aqua regia extractable) mg/kg 1 MCERTS

Barium (aqua regia extractable) mg/kg 1 MCERTS

Beryllium (aqua regia extractable) mg/kg 0.06 MCERTS

Boron (water soluble) mg/kg 0.2 MCERTS

Cadmium (aqua regia extractable) mg/kg 0.2 MCERTS

Chromium (aqua regia extractable) mg/kg 1 MCERTS

Copper (aqua regia extractable) mg/kg 1 MCERTS

Lead (aqua regia extractable) mg/kg 1 MCERTS

Mercury (aqua regia extractable) mg/kg 0.3 MCERTS

Nickel (aqua regia extractable) mg/kg 1 MCERTS

Selenium (aqua regia extractable) mg/kg 1 MCERTS

Vanadium (aqua regia extractable) mg/kg 1 MCERTS

Zinc (aqua regia extractable) mg/kg 1 MCERTS

662805 662806

SP214 SP215

None Supplied None Supplied

2.00 0.50

18/11/2016 18/11/2016

None Supplied None Supplied

< 0.1 < 0.1

27 20

0.45 0.44

Chrysotile &

AmositeChrysotile

Detected Detected

0.256 0.019

0.256 0.019

< 0.05 < 0.05

< 0.10 < 0.10

< 0.10 < 0.10

< 0.10 < 0.10

0.89 2.0

0.27 0.66

3.0 7.6

3.2 7.1

2.2 4.3

1.9 3.5

3.6 6.1

1.1 1.7

2.1 3.5

1.2 2.1

0.37 0.57

1.6 2.6

21.2 41.7

17 50

190 67

0.37 0.42

4.4 8.1

1.1 2.1

28 32

300 700

3700 1300

0.7 0.6

56 93

< 1.0 < 1.0

21 24

900 1200



Page 4 of 7

16-33631

Perseverance Mill, Padiham

11360-4905-NS

Methods:

Qualitative Analysis

Sample

NumberSample ID

Sample

Depth

(m)

Sample

Weight

(g)

Asbestos Containing

Material Types Detected

(ACM)

PLM Results

Asbestos by hand

picking/weighing

(%)

Total %

Asbestos in

Sample

662795 SP201 1.00 114Hard/ Cement Type Material

& Insulation Lagging

Chrysotile &

Amosite1.434 1.43

662796 SP204 1.00 104Loose Fibres & Insulation

Lagging

Chrysotile &

Amosite &

Crocidolite

0.009 0.009

662797 SP205 0.50 120 Loose FibresChrysotile &

Amosite0.001 0.001

662798 SP206 1.00 125 Loose FibresChrysotile &

Crocidolite< 0.001 < 0.001

662799 SP207 0.50 127Insulation Lagging & Hard/

Cement Type Material

Chrysotile &

Amosite &

Crocidolite

0.017 0.017

662800 SP208 1.00 108Insulation Lagging & Hard/

Cement Type MaterialChrysotile 0.168 0.168

662801 SP210 1.50 85

Insulation lagging, Insulation

Board/Tile, Hard/Cement

type material

Chrysotile,

Amosite,

Crocidolite

1.275 1.28

662802 SP211 1.00 111Insulation lagging, Loose

fibres

Chrysotile,

Amosite0.064 0.064

662803 SP212 1.80 100Loose Fibres & Insulation

LaggingChrysotile 0.021 0.021

662804 SP213 1.00 122Insulation Lagging & Loose

Fibres

Chrysotile &

Amosite0.033 0.033


Fibres

Chrysotile &

Amosite0.256 0.256


FibresChrysotile 0.019 0.019

The analysis was carried out using our documented in-house method A006 based on HSE Contract Research Report No: 83/1996:

Development and Validation of an analytical method to determine the amount of asbestos in soils and loose aggregates (Davies et al, 1996)

and HSG 248. Our method includes initial examination of the entire representative sample, then fractionation and detailed analysis of each

fraction, with quantification by hand picking and weighing.

The limit of detection (reporting limit) of this method is 0.001 %.

The method has been validated using samples of at least 100 g, results for samples smaller than this should be interpreted with caution.

Both Qualitative and Quantitative Analyses are UKAS accredited.

Opinions and interpretations expressed herein are outside the scope of UKAS accreditation.

Analytical Report Number:

Project / Site name:

Your Order No:

Certificate of Analysis - Asbestos Quantification

The samples were analysed qualitatively for asbestos by polarising light and dispersion staining as described by the Health and Safety

Executive in HSG 248.

Quantitative Analysis



Page 5 of 7

Analytical Report Number : 16-33631


Lab Sample

Number

Sample

Reference

Sample

NumberDepth (m) Sample Description *

662795 SP201 None Supplied 1.00 Brown loam and gravel with vegetation.

662796 SP204 None Supplied 1.00 Brown loam and clay with gravel and vegetation.



662799 SP207 None Supplied 0.50 Brown loam and gravel with vegetation.

662800 SP208 None Supplied 1.00 Brown loam and gravel.

662801 SP210 None Supplied 1.50 Brown loam and clay with vegetation.

662802 SP211 None Supplied 1.00 Brown loam and clay with vegetation.





* These descriptions are only intended to act as a cross check if sample identities are questioned. The major constituent of the sample is intended to act with respect to MCERTS

validation. The laboratory is accredited for sand, clay and loam (MCERTS) soil types. Data for unaccredited types of solid should be interpreted with care.

Stone content of a sample is calculated as the % weight of the stones not passing a 10 mm sieve. Results are not corrected for stone content.



Page 6 of 7

Analytical Report Number : 16-33631


Water matrix abbreviations: Surface Water (SW) Potable Water (PW) Ground Water (GW)

Analytical Test Name Analytical Method Description Analytical Method ReferenceMethod

number

Wet / Dry

Analysis

Accreditation

Status

Asbestos identification in soil Asbestos Identification with the use of polarised

light microscopy in conjunction with disperion

staining techniques.

In house method based on HSG 248 A001-PL D ISO 17025

Asbestos Quantification - Gravimetric Asbestos quantification by gravimetric method - in

ouse method based on references.

HSE Report No: 83/1996, HSG 248, HSG

264 & SCA Blue Book (draft).

A006-PL D ISO 17025

Boron, water soluble, in soil Determination of water soluble boron in soil by hot

water extract followed by ICP-OES.

In-house method based on Second Site

Properties version 3

L038-PL D MCERTS

D.O. for Gravimetric Quant if

Screen/ID positive

Dependent option for Gravimetric Quant if

Screen/ID positive scheduled.

In house asbestos methods A001 & A006. A006-PL D NONE

Metals in soil by ICP-OES Determination of metals in soil by aqua-regia

digestion followed by ICP-OES.

In-house method based on MEWAM 2006

Methods for the Determination of Metals in

Soil.

L038-PL D MCERTS

Moisture Content Moisture content, determined gravimetrically. In-house method based on BS1377 Part 3,

1990, Chemical and Electrochemical Tests

L019-UK/PL W NONE

Speciated EPA-16 PAHs in soil Determination of PAH compounds in soil by

extraction in dichloromethane and hexane followed

by GC-MS with the use of surrogate and internal

standards.

In-house method based on USEPA 8270 L064-PL D MCERTS

Stones content of soil Standard preparation for all samples unless

otherwise detailed. Gravimetric determination of

stone > 10 mm as % dry weight.

In-house method based on British Standard

Methods and MCERTS requirements.

L019-UK/PL D NONE

For method numbers ending in 'UK' analysis have been carried out in our laboratory in the United Kingdom.

For method numbers ending in 'PL' analysis have been carried out in our laboratory in Poland.

Soil analytical results are expressed on a dry weight basis. Where analysis is carried out on as-received the results obtained are multiplied by a moisture

correction factor that is determined gravimetrically using the moisture content which is carried out at a maximum of 30oC.



Page 7 of 7

Documents

Perseverance Mill, Albion Street, Padiham Supplementary ... · Supplementary Stockpile Investigation Further to the completion of our recent Ground Investigation works and interpretive