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POLLEN ENVIRONMENTAL, LLC. CHAIN OF CUSTODY /WORKORDER FORM 3536 International Street
Fairbanks, AK 99701
(907) 479-8368 Phone (907) 452-6853 Fax
CLIENT INFORMATION
Company: City of North Pole
Address: 1 25 Snowman Lane
City, State Zip: North Pole, AK 99705
Phone: 907-388-1907
Fax: 907-488-1825
Email: [email protected]
Project Name: QC PFC Monitoring
Sampled By: JEP
Samole Identification Samole Date
W ell A 10/3/2017
W ell A Dup. 10/3/2017
Field Blank 10/3/2017
Trio Blank 10/3/2017
Possible Hazard Identification:
SamoleTime
10:05 AM
10:06 AM
10:08 AM
10:05 AM
Contact Person: Requested Analysis Paul Trissel
Perservatlve Added
WWTP APDES #:
Pws 1D #: 31os7s ~ repod ,:;:$ -,pec-;a/ Send Results to ADEC: I '
,J Yes D No
Purchase Order/Charge Code:
.9.0;1-565 Cf)
u LL a..
Matrix Lab ID# Sub Lab ID#
w f£F3{851 2 X
w PEP3t8E8 2 X
w PEJ36l~'1 2 X
w P£F36~t0 2 X
Sample Condition:
D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: oc COC Seal:
Sub Lab Temoerature on arrival: oc COC Seal:
Special I nstructions/QC Requirements & Comments:
A " -" Rer)}/Jt/1'V:IM. A · '//UT,U/'"I' l
Company:f)J//{]// fAv Da1e/f!.}rqe;,r7 ~ II OOaJN') Received by: Company:
1 nqui,ed by: Company: Date & Time: Received by: Company:
relinquished by: Company: Date & Time: Received by : Company:
Accuracy, Precision, and Professional Service
COC# CONP 2017
Page l of l
□ Normal Turnaround
□ RUSH __ day(s)
Samole Comments
D Intact D Broken D Absent
D Intact D Broken D Absent
Date & Time:
Date & Time:
Date & Time:
City of North Pole WTP Report Date: 11/1/2017Attn: Paul Trissel Sample Date: 10/3/2017125 Snowman Lane Sample Time: 10:05-10:08 AMNorth Pole, AK 99705 Sampled By: Jerry PollenPhone: 907-388-1907Fax: [email protected]
Project Name: CONP WTP PFC MonitoringAnalysis: PFC'SAnalysis Method: EPA 537COC#: CONP 2017Sample Matrix: Drinking WaterPWS ID#: AK2310675
Attached are the results for analysis of your samples. This sample was analyzed by
Eurofins Eaton Analytical in South Bend, IN.
Client Sample ID: Eurofins Eaton Analytical ID:Well A PEF36857Well A Dup. PEF36858 3793430Field Blank* PEF36859 3793431Travel Blank PEF36860 3793432
*PFC reagent water added to Field Blank bottle at the time and location of Well A sample collection.
Comments: Well A sample result for PFHxS is 1.9ng/L. This result is slightly below the laboratories detection limit of 2.0ng/L, so the report indicates the result is <2.0ng/L. This is being addressed due to the detection of 2.0ng/L of PFHxS in the Well A Dup. sample.
Jerry PollenPollen Environmental, LLC - Fairbanks
CERTIFICATE OF ANALYSIS
Pollen Env ID:3793429
Pollen Environmental, LLC
LABORATORY REPORT
This report may not be reproduced, except in full, without written approval from EEA.
If you have any questions concerning this report, please do not hesitate to call us at (800) 332-4345 or (574) 233-4777.
Page 1 of 21
=::: e u rofi n s I Eaton Analytical
Revision date: 08/28/2017
STATE CERTIFICATION LIST
State Certification State Certification Alabama 40700 Missouri 880 Alaska IN00035 Montana CERT0026 Arizona AZ0432 Nebraska NE-OS-05-04
Arkansas IN00035 Nevada IN00035 California 2920 New Hampshire* 2124 Colorado IN035 New Jersey* IN598
Colorado Radiochemistry IN035 New Mexico IN00035 Connecticut PH-0132 New York* 11398 Delaware IN035 North Carolina 18700 Florida* E87775 North Dakota R-035 Georgia 929 Ohio 87775 Hawaii IN035 Oklahoma D9508 Idaho IN00035 Oregon (Primary AB)* 4074-001
Illinois* 200001 Pennsylvania* 68-00466 Illinois Microbiology 17767 Puerto Rico IN00035
Illinois Radiochemistry IN00035 Rhode Island LAO00343 Indiana Chemistry C-71-01 South Carolina 95005
Indiana Microbiology M-76-07 South Dakota IN00035 Iowa 098 Tennessee TN02973
Kansas* E-10233 Texas* T104704187-15-8Kentucky 90056 Texas/TCEQ TX207
Louisiana* LA170006 Utah* IN00035 Maine IN00035 Vermont VT-8775
Maryland 209 Virginia* 460275 Massachusetts M-IN035 Washington C837
Michigan 9926 West Virginia 9927 C Minnesota* 018-999-338 Wisconsin 999766900 Mississippi IN035 Wyoming IN035
EPA IN00035 *NELAP/TNI Recognized Accreditation Bodies
Page 2 of 21
·=- eurofins I t Analytical -:.• Ea on
Laboratory Report
Client:
Attn:
Report:
Priority:
Status:
PWS ID:
Pollen Environmental LLC
Jerry Pollen
3536 International Avenue
399812
AK2310675
Standard Written
Final
IN00035Alaska Lab ID #
Fairbanks, AK 99701
110 South Hill Street
South Bend, IN 46617
Tel: (574) 233-4777
Fax: (574) 233-8207
1 800 332 4345
*NR = The chlorine demand was not performed for this
analytical sample, at the request of the client.
EEA
ID #
Client ID Method Collected
Date / Time
Collected
By:
Received
Date / Time
3793429 PEF36857 Well A 537 10/03/17 10:05 Client 10/05/17 08:30
3793430 PEF36858 Well A Dup. 537 10/03/17 10:06 Client 10/05/17 08:30
3793431 PEF36859 FTB 537 10/03/17 10:08 Client 10/05/17 08:30
3793432 PEF36860 LTB-09/13/17 537 10/03/17 10:05 EEA 10/05/17 08:30
Sample Information
Report Summary
Note: This report was amended on 10/20/2017 to report additional compounds at the request of the client.
Note: This report was further amended on 11/01/17 to report field blank and lab blank results, at the request of the client.
Detailed quantitative results are presented on the following pages. The results presented relate only to the samples provided for
analysis.
We appreciate the opportunity to provide you with this analysis. If you have any questions concerning this report, please do not
hesitate to call Traci Chlebowski at (574) 233-4777.
Note: This report may not be reproduced, except in full, without written approval from EEA.
Client Name:
Report #:
Pollen Environmental LLC
399812
Authorized Signature Title Date
11/01/2017
Page 1 of 4
Page 3 of 21
=:~ eurofins I Eaton Analytical
Client Name: Report #: 399812Pollen Environmental LLC
Sampling Point: PWS ID:PEF36857 Well A AK2310675
EEA Methods
Analyte
ID #
Analyte Method Reg
Limit
MRL† Result Units Preparation
Date
Analyzed
Date
EEA
ID #
379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorobutanesulfonic acid (PFBS)375-73-5
379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorodecanoic acid (PFDA)335-76-2
379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluoroheptanoic acid (PFHpA)375-85-9
379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorohexanesulfonic acid (PFHxS)355-46-4
379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorohexanoic acid (PFHxA)307-24-4
379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorolauric acid (PFDoA)307-55-1
379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluoromyristic acid (PFTA)376-06-7
379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorononanoic acid (PFNA)375-95-1
379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorooctane sulfonate (PFOS)1763-23-1
379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorooctanoic acid (PFOA)335-67-1
379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluorotridecanoic acid (PFTrDA)72629-94-8
379342910/11/17 00:5310/10/17 08:00ng/L< 2.02.0---537Perfluoroundecanoic acid (PFUnA)2058-94-8
Sampling Point: PWS ID:PEF36858 Well A Dup. AK2310675
EEA Methods
Analyte
ID #
Analyte Method Reg
Limit
MRL† Result Units Preparation
Date
Analyzed
Date
EEA
ID #
379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorobutanesulfonic acid (PFBS)375-73-5
379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorodecanoic acid (PFDA)335-76-2
379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluoroheptanoic acid (PFHpA)375-85-9
379343010/11/17 01:2710/10/17 08:00ng/L2.02.0---537Perfluorohexanesulfonic acid (PFHxS)355-46-4
379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorohexanoic acid (PFHxA)307-24-4
379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorolauric acid (PFDoA)307-55-1
379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluoromyristic acid (PFTA)376-06-7
379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorononanoic acid (PFNA)375-95-1
379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorooctane sulfonate (PFOS)1763-23-1
379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorooctanoic acid (PFOA)335-67-1
379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluorotridecanoic acid (PFTrDA)72629-94-8
379343010/11/17 01:2710/10/17 08:00ng/L< 2.02.0---537Perfluoroundecanoic acid (PFUnA)2058-94-8
Page 2 of 4Page 4 of 21
Client Name: Report #: 399812Pollen Environmental LLC
Sampling Point: PWS ID:PEF36859 FTB AK2310675
EEA Methods
Analyte
ID #
Analyte Method Reg
Limit
MRL† Result Units Preparation
Date
Analyzed
Date
EEA
ID #
379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorobutanesulfonic acid (PFBS)375-73-5
379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorodecanoic acid (PFDA)335-76-2
379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluoroheptanoic acid (PFHpA)375-85-9
379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorohexanesulfonic acid (PFHxS)355-46-4
379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorohexanoic acid (PFHxA)307-24-4
379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorolauric acid (PFDoA)307-55-1
379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluoromyristic acid (PFTA)376-06-7
379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorononanoic acid (PFNA)375-95-1
379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorooctane sulfonate (PFOS)1763-23-1
379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorooctanoic acid (PFOA)335-67-1
379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluorotridecanoic acid (PFTrDA)72629-94-8
379343110/20/17 20:5810/11/17 08:20ng/L< 2.02.0---537Perfluoroundecanoic acid (PFUnA)2058-94-8
Sampling Point: PWS ID:PEF36860 LTB-09/13/17 Not Supplied
EEA Methods
Analyte
ID #
Analyte Method Reg
Limit
MRL† Result Units Preparation
Date
Analyzed
Date
EEA
ID #
379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorobutanesulfonic acid (PFBS)375-73-5
379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorodecanoic acid (PFDA)335-76-2
379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluoroheptanoic acid (PFHpA)375-85-9
379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorohexanesulfonic acid (PFHxS)355-46-4
379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorohexanoic acid (PFHxA)307-24-4
379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorolauric acid (PFDoA)307-55-1
379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluoromyristic acid (PFTA)376-06-7
379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorononanoic acid (PFNA)375-95-1
379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorooctane sulfonate (PFOS)1763-23-1
379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorooctanoic acid (PFOA)335-67-1
379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluorotridecanoic acid (PFTrDA)72629-94-8
379343210/20/17 21:1510/11/17 08:20ng/L< 2.02.0---537Perfluoroundecanoic acid (PFUnA)2058-94-8
Reg Limit Type:
Symbol:
MCL SMCL AL
* ^ !
† EEA has demonstrated it can achieve these report limits in reagent water, but can not document them in all sample matrices.
Page 3 of 4Page 5 of 21
Client Name: Report #: 399812Pollen Environmental LLC
Lab Definitions
Continuing Calibration Check Standard (CCC) / Continuing Calibration Verification (CCV) / Initial Calibration
Verification Standard (ICV) / Initial Performance Check (IPC) - is a standard containing one or more of the target
analytes that is prepared from the same standards used to calibrate the instrument. This standard is used to verify
the calibration curve at the beginning of each analytical sequence, and may also be analyzed throughout and at the
end of the sequence. The concentration of continuing standards may be varied, when prescribed by the reference
method, so that the range of the calibration curve is verified on a regular basis. CCL, CCM, and CCH are the CCC
standards at low, mid, and high concentration levels, respectively.
Internal Standards (IS) - are pure compounds with properties similar to the analytes of interest, which are added to
field samples or extracts, calibration standards, and quality control standards at a known concentration. They are
used to measure the relative responses of the analytes of interest and surrogates in the sample, calibration standard
or quality control standard.
Laboratory Duplicate (LD) - is a field sample aliquot taken from the same sample container in the laboratory and
analyzed separately using identical procedures. Analysis of laboratory duplicates provides a measure of the
precision of the laboratory procedures.
Laboratory Fortified Blank (LFB) / Laboratory Control Sample (LCS) - is an aliquot of reagent water to which
known concentrations of the analytes of interest are added. The LFB is analyzed exactly the same as the field
samples. LFBs are used to determine whether the method is in control. FBL, FBM, and FBH are the LFB samples at
low, mid, and high concentration levels, respectively.
Laboratory Method Blank (LMB) / Laboratory Reagent Blank (LRB) - is a sample of reagent water included in the
sample batch analyzed in the same way as the associated field samples. The LMB is used to determine if method
analytes or other background contamination have been introduced during the preparation or analytical procedure.
The LMB is analyzed exactly the same as the field samples.
Laboratory Trip Blank (LTB) / Field Reagent Blank (FRB) - is a sample of laboratory reagent water placed in a
sample container in the laboratory and treated as a field sample, including storage, preservation, and all analytical
procedures. The FRB/LTB container follows the collection bottles to and from the collection site, but the FRB/LTB is
not opened at any time during the trip. The FRB/LTB is primarily a travel blank used to verify that the samples were
not contaminated during shipment.
Matrix Spike Duplicate Sample (MSD) / Laboratory Fortified Sample Matrix Duplicate (LFSMD) - is a sample
aliquot taken from the same field sample source as the Matrix Spike Sample to which known quantities of the
analytes of interest are added in the laboratory. The MSD is analyzed exactly the same as the field samples.
Analysis of the MSD provides a measure of the precision of the laboratory procedures in a specific matrix. SDL,
SDM, and SDH / LFSMDL, LFSMDM, and LFSMDH are the MSD or LFSMD at low, mid, and high concentration
levels, respectively.
Matrix Spike Sample (MS) / Laboratory Fortified Sample Matrix (LFSM) - is a sample aliquot taken from field
sample source to which known quantities of the analytes of interest are added in the laboratory. The MS is analyzed
exactly the same as the field samples. The purpose is to demonstrate recovery of the analytes from a sample matrix
to determine if the specific matrix contributes bias to the analytical results. MSL, MSM, and MSH / LFSML, LFSMM,
and LFSMH are the MS or LFSM at low, mid, and high concentration levels, respectively.
Quality Control Standard (QCS) / Second Source Calibration Verification (SSCV) - is a solution containing
known concentrations of the analytes of interest prepared from a source different from the source of the calibration
standards. The solution is obtained from a second manufacturer or lot if the lot can be demonstrated by the
manufacturer as prepared independently from other lots. The QCS sample is analyzed using the same procedures
as field samples. The QCS is used as a check on the calibration standards used in the method on a routine basis.
Reporting Limit Check (RLC) / Initial Calibration Check Standard (ICCS) - is a procedural standard that is
analyzed each day to evaluate instrument performance at or below the minimum reporting limit (MRL).
Surrogate Standard (SS) / Surrogate Analyte (SUR) - is a pure compound with properties similar to the analytes of
interest, which is highly unlikely to be found in any field sample, that is added to the field samples, calibration
standards, blanks and quality control standards before sample preparation. The SS is used to evaluate the efficiency
of the sample preparation process.
Page 4 of 4Page 6 of 21
Page 7 of 21
p~C,{ S5 io-511 CN:[l(?:x)
I ~
1e 10-s,1
POLLEN ENVIRONMENTAL, LLC. 3 0°!2//--
CHAIN OF CUSTODY /WORKORDER FORM 3536 International Street
Fairbanks, AK 99701
(907) 479-8368 Phone (907) 452-6853 Fax
CLIENT INFORMATION
Company: City of North Pole
Address: 125 Snowman Lane
City, State Zip: North Pole, AK 99705
Phone: 907-388- 1907
Fax: 907-488-1825
Email: [email protected]
Project Name: QC PFC Monitoring
Sampled By : JEP
Samole,Identification Samole Date"
Well A 10/3/2017
Well A Dup. 10/3/2017
Field Blank 10/3/2017
Trip Blank 10/3/2017
,,
Possible Hazard Identification:
Samole Tim•
10:05 AM
10:06 AM
10:08 AM
10:05 AM
Contact Person:
Paul Trissel
WWTP APDES # :
pws m # : 31061s ,, report Gr:f 5pin"al Send Results to ADEC: I I
,J Yes D No
Purchase Order/Charge Code:
;J.O;'l-565
Matrix_ Lab ID# Sub Lab ID#
w lJEf 3fi!fl m~ l-/;z.q 7lf3t8E8 - 430 w
w ff3tl §1 L/3) w P€F36~to .y 43~
-3 J<lO/<pc# CONP 2017
Requested Analysis
Page 1 of 1
Perservatlve Added
D Normal Turnaround
~ . C
D RUSH --day(s) 'ii C 0 u 0 {,/) L u . .,, E LL ,
Cl.. z Samole.Comments
2 X (_t z) Ct A0 2 X {e 0 ' 2 X(r,
,-2 X{.J /,) r-:t 1, 7 ·- I -, l ,"l I
Sample Condit ion:
D Non-Hazardous D Flammable D Skin Irritant D Unknown Pollen Env Temoerature on arrival: •c (. g•c COC Seal: D I ntact D Broken D Absent
Sub Lab Temoerature on arrival: COC Seal: K intact D Broken D Absent
Special Instructions/QC Requirements &. Comments:
A ,.. A
Re'.Wl&!, TJ,tf f//4 A • 11//U ffl' {
Company:f,J // et/ &n/ Daj!J~irct-f1 ~ iJ DOa;vJ Re~ D--- Com~~ Dit)2;'"J1 OR~ Rfjfnqul,ed by: Company: Date & Time: Recel~ y: l) Company : Date & Time:
r elinquished by: Company: Date & Time: Received by: Company: Date & Time:
Accuracy, Precision, and Professional Service
Eurofins Eaton Analytical
Run LogRun ID: 235318 Method: 537
Sample SiteSample IdType Instrument ID Calibration FileAnalysis DateMatrix
CCL 3796119 FL 101017M537b-FL-PFC12.mdb10/10/2017 18:28OS
LRB 3796102 FL 101017M537b-FL-PFC12.mdb10/10/2017 19:01RW
FBL 3796103 FL 101017M537b-FL-PFC12.mdb10/10/2017 19:18RW
CCM 3796121 FL 101017M537b-FL-PFC12.mdb10/10/2017 22:39OS
FS 3793429 PEF36857 Well A FL 101017M537b-FL-PFC12.mdb10/11/2017 00:53DW
FD 3796105 PEF36857 Well A FL 101017M537b-FL-PFC12.mdb10/11/2017 01:10DW
FS 3793430 PEF36858 Well A Dup. FL 101017M537b-FL-PFC12.mdb10/11/2017 01:27DW
CCH 3796122 FL 101017M537b-FL-PFC12.mdb10/11/2017 02:34OS
0.00
Page 1 of 5 EEA Run ID 235318 / EEA Report # 399812
Page 8 of 21
=::: e u rof i n s I Eaton Analytical
QC
Su
mm
ary
Re
po
rt
EE
A
ID #
RP
DU
nit
sT
arg
et
Am
ou
nt
Clien
t ID
Meth
od
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aly
teS
am
ple
Typ
e
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it
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very
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its
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Fals
e
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3C
2537
N/A
CC
L1807790.0
0ng/L
1.0
3796119
---
---
---
50 -
150
100
1807790
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Fals
e
IS-P
FO
S-1
3C
4537
N/A
CC
L307886.0
0ng/L
1.0
3796119
---
---
---
50 -
150
100
307886
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Fals
e
SS
-PF
DA
-13C
2537
N/A
CC
L96.7
104
ng/L
1.0
3796119
---
---
---
70 -
130
97
100
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Fals
e
SS
-PF
HxA
-13C
2537
N/A
CC
L50.1
889
ng/L
1.0
3796119
---
---
---
70 -
130
100
50.0
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Fals
e
Perf
luoro
buta
nesu
lfonic
aci
d (
PF
BS
)537
2.0
CC
L2.0
892
ng/L
1.0
3796119
---
---
---
50 -
150
104
2.0
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Fals
e
Perf
luoro
deca
noic
aci
d (
PF
DA
)537
2.0
CC
L1.9
778
ng/L
1.0
3796119
---
---
---
50 -
150
99
2.0
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Fals
e
Perf
luoro
hepta
noic
aci
d (
PF
HpA
)537
2.0
CC
L2.0
459
ng/L
1.0
3796119
---
---
---
50 -
150
102
2.0
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Fals
e
Perf
luoro
hexa
nesu
lfonic
aci
d (
PF
HxS
)537
2.0
CC
L2.0
655
ng/L
1.0
3796119
---
---
---
50 -
150
103
2.0
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Fals
e
Perf
luoro
hexa
noic
aci
d (
PF
HxA
)537
2.0
CC
L2.1
321
ng/L
1.0
3796119
---
---
---
50 -
150
107
2.0
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Fals
e
Perf
luoro
lauric
aci
d (
PF
DoA
)537
2.0
CC
L2.1
143
ng/L
1.0
3796119
---
---
---
50 -
150
106
2.0
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Fals
e
Perf
luoro
myr
istic
aci
d (
PF
TA
)537
2.0
CC
L2.0
331
ng/L
1.0
3796119
---
---
---
50 -
150
102
2.0
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Fals
e
Perf
luoro
nonanoic
aci
d (
PF
NA
)537
2.0
CC
L2.0
307
ng/L
1.0
3796119
---
---
---
50 -
150
102
2.0
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Fals
e
Perf
luoro
oct
ane s
ulfo
nate
(P
FO
S)
537
2.0
CC
L2.0
940
ng/L
1.0
3796119
---
---
---
50 -
150
105
2.0
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Fals
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
CC
L2.0
614
ng/L
1.0
3796119
---
---
---
50 -
150
103
2.0
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Fals
e
Perf
luoro
trid
eca
noic
aci
d (
PF
TrD
A)
537
2.0
CC
L2.0
341
ng/L
1.0
3796119
---
---
---
50 -
150
102
2.0
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Fals
e
Perf
luoro
undeca
noic
aci
d (
PF
UnA
)537
2.0
CC
L2.0
017
ng/L
1.0
3796119
---
---
---
50 -
150
100
2.0
09/2
7/2
017 1
4:3
110/1
0/2
017 1
8:2
8
Tru
e
IS-P
FO
A-1
3C
2537
N/A
LR
B1881550.0
0ng/L
0.9
53796102
---
---
---
50 -
150
104
1807790
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:0
1
Tru
e
IS-P
FO
S-1
3C
4537
N/A
LR
B322036.0
0ng/L
0.9
53796102
---
---
---
50 -
150
105
307886
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:0
1
Tru
e
SS
-PF
DA
-13C
2537
N/A
LR
B88.5
280
ng/L
0.9
53796102
---
---
---
70 -
130
93
100
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:0
1
Tru
e
SS
-PF
HxA
-13C
2537
N/A
LR
B46.0
713
ng/L
0.9
53796102
---
---
---
70 -
130
97
50.0
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:0
1
Tru
e
Perf
luoro
buta
nesu
lfonic
aci
d (
PF
BS
)537
2.0
LR
B2.0
ng/L
0.9
53796102
---
---
---
---
---
<
10/1
0/2
017 0
8:0
010/1
0/2
017 1
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1
Tru
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Perf
luoro
deca
noic
aci
d (
PF
DA
)537
2.0
LR
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ng/L
0.9
53796102
---
---
---
---
---
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10/1
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017 0
8:0
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017 1
9:0
1
Tru
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Perf
luoro
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noic
aci
d (
PF
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)537
2.0
LR
B2.0
ng/L
0.9
53796102
---
---
---
---
---
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10/1
0/2
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017 1
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Tru
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Perf
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nesu
lfonic
aci
d (
PF
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)537
2.0
LR
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0.9
53796102
---
---
---
---
---
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10/1
0/2
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8:0
010/1
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017 1
9:0
1
Tru
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Perf
luoro
hexa
noic
aci
d (
PF
HxA
)537
2.0
LR
B2.0
ng/L
0.9
53796102
---
---
---
---
---
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10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:0
1
Tru
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Perf
luoro
lauric
aci
d (
PF
DoA
)537
2.0
LR
B2.0
ng/L
0.9
53796102
---
---
---
---
---
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10/1
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8:0
010/1
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017 1
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1
Tru
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Perf
luoro
myr
istic
aci
d (
PF
TA
)537
2.0
LR
B2.0
ng/L
0.9
53796102
---
---
---
---
---
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10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:0
1
Tru
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Perf
luoro
nonanoic
aci
d (
PF
NA
)537
2.0
LR
B2.0
ng/L
0.9
53796102
---
---
---
---
---
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10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:0
1
Tru
e
Perf
luoro
oct
ane s
ulfo
nate
(P
FO
S)
537
2.0
LR
B2.0
ng/L
0.9
53796102
---
---
---
---
---
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10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:0
1
Tru
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
LR
B2.0
ng/L
0.9
53796102
---
---
---
---
---
<
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:0
1
Tru
e
Perf
luoro
trid
eca
noic
aci
d (
PF
TrD
A)
537
2.0
LR
B2.0
ng/L
0.9
53796102
---
---
---
---
---
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10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:0
1
Tru
e
Perf
luoro
undeca
noic
aci
d (
PF
UnA
)537
2.0
LR
B2.0
ng/L
0.9
53796102
---
---
---
---
---
<
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:0
1
Fals
e
IS-P
FO
A-1
3C
2537
N/A
FB
L1883360.0
0ng/L
1.0
3796103
---
---
---
50 -
150
104
1807790
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Fals
e
IS-P
FO
S-1
3C
4537
N/A
FB
L326350.0
0ng/L
1.0
3796103
---
---
---
50 -
150
106
307886
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Fals
e
SS
-PF
DA
-13C
2537
N/A
FB
L95.4
088
ng/L
1.0
3796103
---
---
---
70 -
130
95
100
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Fals
e
SS
-PF
HxA
-13C
2537
N/A
FB
L49.0
236
ng/L
1.0
3796103
---
---
---
70 -
130
98
50.0
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Fals
e
Perf
luoro
buta
nesu
lfonic
aci
d (
PF
BS
)537
2.0
FB
L2.0
308
ng/L
1.0
3796103
---
---
---
50 -
150
102
2.0
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Fals
e
Perf
luoro
deca
noic
aci
d (
PF
DA
)537
2.0
FB
L1.9
114
ng/L
1.0
3796103
---
---
---
50 -
150
96
2.0
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Fals
e
Perf
luoro
hepta
noic
aci
d (
PF
HpA
)537
2.0
FB
L1.9
583
ng/L
1.0
3796103
---
---
---
50 -
150
98
2.0
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Fals
e
Perf
luoro
hexa
nesu
lfonic
aci
d (
PF
HxS
)537
2.0
FB
L2.0
160
ng/L
1.0
3796103
---
---
---
50 -
150
101
2.0
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Pa
ge
2 o
f 5
EE
A R
un
ID
23
53
18
/ E
EA
Re
po
rt #
39
98
12
Page 9 of 21
~ ~ ~
D D D D
□□□□--□□--□--□ □--□ □--□--□□--□--□
Sam
ple
Typ
e
EE
A
ID #
An
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Extr
acte
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Un
its
Targ
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Am
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Clien
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An
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Lim
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Reco
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Lim
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Resu
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Su
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co
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Perf
luoro
hexa
noic
aci
d (
PF
HxA
)537
2.0
FB
L1.9
700
ng/L
1.0
3796103
---
---
---
50 -
150
99
2.0
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Fals
e
Perf
luoro
lauric
aci
d (
PF
DoA
)537
2.0
FB
L1.8
624
ng/L
1.0
3796103
---
---
---
50 -
150
93
2.0
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Fals
e
Perf
luoro
myr
istic
aci
d (
PF
TA
)537
2.0
FB
L1.7
829
ng/L
1.0
3796103
---
---
---
50 -
150
89
2.0
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Fals
e
Perf
luoro
nonanoic
aci
d (
PF
NA
)537
2.0
FB
L2.0
446
ng/L
1.0
3796103
---
---
---
50 -
150
102
2.0
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Fals
e
Perf
luoro
oct
ane s
ulfo
nate
(P
FO
S)
537
2.0
FB
L2.0
019
ng/L
1.0
3796103
---
---
---
50 -
150
100
2.0
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Fals
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
FB
L2.0
259
ng/L
1.0
3796103
---
---
---
50 -
150
101
2.0
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Fals
e
Perf
luoro
trid
eca
noic
aci
d (
PF
TrD
A)
537
2.0
FB
L1.7
753
ng/L
1.0
3796103
---
---
---
50 -
150
89
2.0
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Fals
e
Perf
luoro
undeca
noic
aci
d (
PF
UnA
)537
2.0
FB
L1.8
305
ng/L
1.0
3796103
---
---
---
50 -
150
92
2.0
10/1
0/2
017 0
8:0
010/1
0/2
017 1
9:1
8
Tru
e
IS-P
FO
A-1
3C
2537
N/A
CC
M1863950.0
0ng/L
1.0
3796121
---
---
---
50 -
150
100
1863950
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Tru
e
IS-P
FO
S-1
3C
4537
N/A
CC
M321883.0
0ng/L
1.0
3796121
---
---
---
50 -
150
100
321883
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Tru
e
SS
-PF
DA
-13C
2537
N/A
CC
M98.9
344
ng/L
1.0
3796121
---
---
---
70 -
130
99
100
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Tru
e
SS
-PF
HxA
-13C
2537
N/A
CC
M50.7
913
ng/L
1.0
3796121
---
---
---
70 -
130
102
50.0
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Tru
e
Perf
luoro
buta
nesu
lfonic
aci
d (
PF
BS
)537
2.0
CC
M96.2
943
ng/L
1.0
3796121
---
---
---
70 -
130
96
100
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Tru
e
Perf
luoro
deca
noic
aci
d (
PF
DA
)537
2.0
CC
M93.3
914
ng/L
1.0
3796121
---
---
---
70 -
130
93
100
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Tru
e
Perf
luoro
hepta
noic
aci
d (
PF
HpA
)537
2.0
CC
M97.5
328
ng/L
1.0
3796121
---
---
---
70 -
130
98
100
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Tru
e
Perf
luoro
hexa
nesu
lfonic
aci
d (
PF
HxS
)537
2.0
CC
M96.7
118
ng/L
1.0
3796121
---
---
---
70 -
130
97
100
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Tru
e
Perf
luoro
hexa
noic
aci
d (
PF
HxA
)537
2.0
CC
M97.5
800
ng/L
1.0
3796121
---
---
---
70 -
130
98
100
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Tru
e
Perf
luoro
lauric
aci
d (
PF
DoA
)537
2.0
CC
M95.1
450
ng/L
1.0
3796121
---
---
---
70 -
130
95
100
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Tru
e
Perf
luoro
myr
istic
aci
d (
PF
TA
)537
2.0
CC
M95.1
706
ng/L
1.0
3796121
---
---
---
70 -
130
95
100
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Tru
e
Perf
luoro
nonanoic
aci
d (
PF
NA
)537
2.0
CC
M96.8
495
ng/L
1.0
3796121
---
---
---
70 -
130
97
100
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Tru
e
Perf
luoro
oct
ane s
ulfo
nate
(P
FO
S)
537
2.0
CC
M95.4
877
ng/L
1.0
3796121
---
---
---
70 -
130
95
100
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Tru
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
CC
M96.1
620
ng/L
1.0
3796121
---
---
---
70 -
130
96
100
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Tru
e
Perf
luoro
trid
eca
noic
aci
d (
PF
TrD
A)
537
2.0
CC
M95.3
911
ng/L
1.0
3796121
---
---
---
70 -
130
95
100
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Tru
e
Perf
luoro
undeca
noic
aci
d (
PF
UnA
)537
2.0
CC
M94.0
570
ng/L
1.0
3796121
---
---
---
70 -
130
94
100
09/2
7/2
017 1
4:3
110/1
0/2
017 2
2:3
9
Fals
e
IS-P
FO
A-1
3C
2537
N/A
FS
1839110.0
0ng/L
0.8
93793429
PE
F36857 W
ell
A--
---
-50 -
150
99
1863950
10/1
0/2
017 0
8:0
010/1
1/2
017 0
0:5
3
Fals
e
IS-P
FO
S-1
3C
4537
N/A
FS
329499.0
0ng/L
0.8
93793429
PE
F36857 W
ell
A--
---
-50 -
150
102
321883
10/1
0/2
017 0
8:0
010/1
1/2
017 0
0:5
3
Fals
e
SS
-PF
DA
-13C
2537
N/A
FS
79.4
462
ng/L
0.8
93793429
PE
F36857 W
ell
A--
---
-70 -
130
89
100
10/1
0/2
017 0
8:0
010/1
1/2
017 0
0:5
3
Fals
e
SS
-PF
HxA
-13C
2537
N/A
FS
44.4
081
ng/L
0.8
93793429
PE
F36857 W
ell
A--
---
-70 -
130
100
50.0
10/1
0/2
017 0
8:0
010/1
1/2
017 0
0:5
3
Fals
e
Perf
luoro
buta
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aci
d (
PF
BS
)537
2.0
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0.8
93793429
PE
F36857 W
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A--
---
---
---
-
<10/1
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Fals
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---
---
---
-
<10/1
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010/1
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3
Fals
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Perf
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FS
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93793429
PE
F36857 W
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A--
---
---
---
-
<10/1
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017 0
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010/1
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017 0
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3
Fals
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Perf
luoro
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)537
2.0
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93793429
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F36857 W
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A--
---
---
---
-
<10/1
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010/1
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3
Fals
e
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2.0
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93793429
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F36857 W
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---
---
---
-
<10/1
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010/1
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Fals
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Perf
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2.0
FS
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93793429
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F36857 W
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A--
---
---
---
-
<10/1
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010/1
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017 0
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3
Fals
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Perf
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d (
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2.0
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93793429
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F36857 W
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A--
---
---
---
-
<10/1
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017 0
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017 0
0:5
3
Fals
e
Perf
luoro
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aci
d (
PF
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2.0
FS
2.0
ng/L
0.8
93793429
PE
F36857 W
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---
---
---
-
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Fals
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537
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93793429
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---
---
---
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---
---
---
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F36857 W
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---
---
---
-
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8:0
010/1
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017 0
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3
Fals
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Perf
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undeca
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2.0
FS
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93793429
PE
F36857 W
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A--
---
---
---
-
<10/1
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8:0
010/1
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3
Tru
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IS-P
FO
A-1
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2537
N/A
FD
1818770.0
0ng/L
0.9
33796105
PE
F36857 W
ell
A--
---
-50 -
150
98
1863950
10/1
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Pa
ge
3 o
f 5
EE
A R
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Page 10 of 21
~ ~ ~ l R DD D D D D D
JODI
JD□
-□□--□□- -□--□ □--□ □--□--□□--□--□ □--
Sam
ple
Typ
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314181.0
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33796105
PE
F36857 W
ell
A--
---
-50 -
150
98
321883
10/1
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8:0
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2537
N/A
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82.5
730
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33796105
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F36857 W
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---
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130
89
100
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Tru
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SS
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HxA
-13C
2537
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45.7
528
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33796105
PE
F36857 W
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---
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130
98
50.0
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Tru
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2.0
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---
---
---
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Tru
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F36857 W
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---
---
---
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F36857 W
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---
---
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10/1
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Tru
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2.0
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2.0
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0.9
33796105
PE
F36857 W
ell
A--
---
---
---
-
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Tru
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Perf
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PF
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2.0
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2.0
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0.9
33796105
PE
F36857 W
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---
---
---
-
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8:0
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PF
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2.0
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33796105
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---
---
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1721760.0
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3793430
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F36858 W
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up.
---
---
50 -
150
92
1863950
10/1
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7
Fals
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298770.0
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0.9
3793430
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F36858 W
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up.
---
---
50 -
150
93
321883
10/1
0/2
017 0
8:0
010/1
1/2
017 0
1:2
7
Fals
e
SS
-PF
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2537
N/A
FS
82.0
657
ng/L
0.9
3793430
PE
F36858 W
ell
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up.
---
---
70 -
130
91
100
10/1
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017 0
8:0
010/1
1/2
017 0
1:2
7
Fals
e
SS
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2537
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FS
45.6
226
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3793430
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up.
---
---
70 -
130
101
50.0
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7
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PF
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F36858 W
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---
---
---
---
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10/1
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---
---
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---
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10/1
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---
---
---
---
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3793430
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---
---
---
---
10/1
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010/1
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1:2
7
Fals
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luoro
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PF
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F36858 W
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---
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---
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PF
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2.0
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0.9
3793430
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F36858 W
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up.
---
---
---
---
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10/1
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3793430
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F36858 W
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---
---
---
---
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10/1
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---
---
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3793430
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F36858 W
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---
---
---
---
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3793430
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---
---
---
---
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10/1
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Fals
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0.9
3793430
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F36858 W
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---
---
---
---
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10/1
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F36858 W
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---
---
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---
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10/1
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017 0
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010/1
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017 0
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Tru
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IS-P
FO
A-1
3C
2537
N/A
CC
H1744740.0
0ng/L
1.0
3796122
---
---
---
50 -
150
100
1744740
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Tru
e
IS-P
FO
S-1
3C
4537
N/A
CC
H306487.0
0ng/L
1.0
3796122
---
---
---
50 -
150
100
306487
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Tru
e
SS
-PF
DA
-13C
2537
N/A
CC
H97.8
339
ng/L
1.0
3796122
---
---
---
70 -
130
98
100
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Tru
e
SS
-PF
HxA
-13C
2537
N/A
CC
H50.3
025
ng/L
1.0
3796122
---
---
---
70 -
130
101
50.0
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Tru
e
Perf
luoro
buta
nesu
lfonic
aci
d (
PF
BS
)537
2.0
CC
H196.8
460
ng/L
1.0
3796122
---
---
---
70 -
130
98
200
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Tru
e
Perf
luoro
deca
noic
aci
d (
PF
DA
)537
2.0
CC
H196.3
350
ng/L
1.0
3796122
---
---
---
70 -
130
98
200
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Tru
e
Perf
luoro
hepta
noic
aci
d (
PF
HpA
)537
2.0
CC
H203.4
180
ng/L
1.0
3796122
---
---
---
70 -
130
102
200
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Tru
e
Perf
luoro
hexa
nesu
lfonic
aci
d (
PF
HxS
)537
2.0
CC
H201.6
560
ng/L
1.0
3796122
---
---
---
70 -
130
101
200
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Tru
e
Perf
luoro
hexa
noic
aci
d (
PF
HxA
)537
2.0
CC
H203.1
960
ng/L
1.0
3796122
---
---
---
70 -
130
102
200
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Tru
e
Perf
luoro
lauric
aci
d (
PF
DoA
)537
2.0
CC
H198.3
530
ng/L
1.0
3796122
---
---
---
70 -
130
99
200
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Pa
ge
4 o
f 5
EE
A R
un
ID
23
53
18
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EA
Re
po
rt #
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12
Page 11 of 21
D ~
□ DJ D D D
JJDI
JJD
_ DJ __ DD_ -□--□ DODD □□□□--□□--□--□ □--
Sam
ple
Typ
e
EE
A
ID #
An
aly
zed
Extr
acte
dR
PD
Un
its
Targ
et
Am
ou
nt
Clien
t ID
MR
LM
eth
od
An
aly
teD
il
Facto
r
RP
D
Lim
it
Reco
very
Lim
its
%
Reco
very
Resu
lt
Fla
gQC
Su
mm
ary
Re
po
rt (
co
nt.
)
Tru
e
Perf
luoro
myr
istic
aci
d (
PF
TA
)537
2.0
CC
H203.8
160
ng/L
1.0
3796122
---
---
---
70 -
130
102
200
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Tru
e
Perf
luoro
nonanoic
aci
d (
PF
NA
)537
2.0
CC
H201.6
340
ng/L
1.0
3796122
---
---
---
70 -
130
101
200
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Tru
e
Perf
luoro
oct
ane s
ulfo
nate
(P
FO
S)
537
2.0
CC
H200.5
660
ng/L
1.0
3796122
---
---
---
70 -
130
100
200
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Tru
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
CC
H201.7
170
ng/L
1.0
3796122
---
---
---
70 -
130
101
200
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Tru
e
Perf
luoro
trid
eca
noic
aci
d (
PF
TrD
A)
537
2.0
CC
H200.9
130
ng/L
1.0
3796122
---
---
---
70 -
130
100
200
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Tru
e
Perf
luoro
undeca
noic
aci
d (
PF
UnA
)537
2.0
CC
H198.8
460
ng/L
1.0
3796122
---
---
---
70 -
130
99
200
09/2
7/2
017 1
4:3
110/1
1/2
017 0
2:3
4
Pa
ge
5 o
f 5
EE
A R
un
ID
23
53
18
/ E
EA
Re
po
rt #
39
98
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Page 12 of 21
D
□ DJ
JJDI
JJD
- DJ - - DD -
Eurofins Eaton Analytical
Run LogRun ID: 235533 Method: 537
Sample SiteSample IdType Instrument ID Calibration FileAnalysis DateMatrix
CCL 3796835 FL 101117M537b-FL-PFC12.mdb10/11/2017 19:03OS
UQCSM 3796834 FL 101117M537b-FL-PFC12.mdb10/11/2017 19:20OS
LRB 3796817 FL 101117M537b-FL-PFC12.mdb10/11/2017 19:37RW
FBM 3796818 FL 101117M537b-FL-PFC12.mdb10/11/2017 20:11RW
0.00
Page 1 of 3 EEA Run ID 235533 / EEA Report # 399812
Page 13 of 21
=::: e u rof i n s I Eaton Analytical
QC
Su
mm
ary
Re
po
rt
EE
A
ID #
RP
DU
nit
sT
arg
et
Am
ou
nt
Clien
t ID
Meth
od
An
aly
teS
am
ple
Typ
e
Dil
Facto
r
RP
D
Lim
it
Reco
very
Lim
its
%
Reco
very
Resu
lt
Fla
g
MR
LE
xtr
acte
dA
naly
zed
Tru
e
IS-P
FO
A-1
3C
2537
N/A
CC
L1765390.0
0ng/L
1.0
3796835
---
---
---
50 -
150
100
1765390
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Tru
e
IS-P
FO
S-1
3C
4537
N/A
CC
L313002.0
0ng/L
1.0
3796835
---
---
---
50 -
150
100
313002
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Tru
e
SS
-PF
DA
-13C
2537
N/A
CC
L95.5
705
ng/L
1.0
3796835
---
---
---
70 -
130
96
100
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Tru
e
SS
-PF
HxA
-13C
2537
N/A
CC
L48.9
792
ng/L
1.0
3796835
---
---
---
70 -
130
98
50.0
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Tru
e
Perf
luoro
buta
nesu
lfonic
aci
d (
PF
BS
)537
2.0
CC
L2.0
286
ng/L
1.0
3796835
---
---
---
50 -
150
101
2.0
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Tru
e
Perf
luoro
deca
noic
aci
d (
PF
DA
)537
2.0
CC
L2.0
933
ng/L
1.0
3796835
---
---
---
50 -
150
105
2.0
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Tru
e
Perf
luoro
hepta
noic
aci
d (
PF
HpA
)537
2.0
CC
L2.0
415
ng/L
1.0
3796835
---
---
---
50 -
150
102
2.0
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Tru
e
Perf
luoro
hexa
nesu
lfonic
aci
d (
PF
HxS
)537
2.0
CC
L1.9
971
ng/L
1.0
3796835
---
---
---
50 -
150
100
2.0
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Tru
e
Perf
luoro
hexa
noic
aci
d (
PF
HxA
)537
2.0
CC
L2.1
359
ng/L
1.0
3796835
---
---
---
50 -
150
107
2.0
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Tru
e
Perf
luoro
lauric
aci
d (
PF
DoA
)537
2.0
CC
L2.1
000
ng/L
1.0
3796835
---
---
---
50 -
150
105
2.0
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Tru
e
Perf
luoro
myr
istic
aci
d (
PF
TA
)537
2.0
CC
L2.0
378
ng/L
1.0
3796835
---
---
---
50 -
150
102
2.0
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Tru
e
Perf
luoro
nonanoic
aci
d (
PF
NA
)537
2.0
CC
L2.0
415
ng/L
1.0
3796835
---
---
---
50 -
150
102
2.0
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Tru
e
Perf
luoro
oct
ane s
ulfo
nate
(P
FO
S)
537
2.0
CC
L2.0
850
ng/L
1.0
3796835
---
---
---
50 -
150
104
2.0
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Tru
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
CC
L2.0
989
ng/L
1.0
3796835
---
---
---
50 -
150
105
2.0
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Tru
e
Perf
luoro
trid
eca
noic
aci
d (
PF
TrD
A)
537
2.0
CC
L2.0
233
ng/L
1.0
3796835
---
---
---
50 -
150
101
2.0
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Tru
e
Perf
luoro
undeca
noic
aci
d (
PF
UnA
)537
2.0
CC
L2.0
212
ng/L
1.0
3796835
---
---
---
50 -
150
101
2.0
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:0
3
Fals
e
IS-P
FO
A-1
3C
2537
N/A
UQ
CS
M1711970.0
0ng/L
1.0
3796834
---
---
---
50 -
150
97
1765390
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Fals
e
IS-P
FO
S-1
3C
4537
N/A
UQ
CS
M305262.0
0ng/L
1.0
3796834
---
---
---
50 -
150
98
313002
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Fals
e
SS
-PF
DA
-13C
2537
N/A
UQ
CS
M99.7
112
ng/L
1.0
3796834
---
---
---
70 -
130
100
100
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Fals
e
SS
-PF
HxA
-13C
2537
N/A
UQ
CS
M50.5
456
ng/L
1.0
3796834
---
---
---
70 -
130
101
50.0
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Fals
e
Perf
luoro
buta
nesu
lfonic
aci
d (
PF
BS
)537
2.0
UQ
CS
M95.1
907
ng/L
1.0
3796834
---
---
---
70 -
130
95
100
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Fals
e
Perf
luoro
deca
noic
aci
d (
PF
DA
)537
2.0
UQ
CS
M84.4
468
ng/L
1.0
3796834
---
---
---
70 -
130
84
100
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Fals
e
Perf
luoro
hepta
noic
aci
d (
PF
HpA
)537
2.0
UQ
CS
M91.4
448
ng/L
1.0
3796834
---
---
---
70 -
130
91
100
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Fals
e
Perf
luoro
hexa
nesu
lfonic
aci
d (
PF
HxS
)537
2.0
UQ
CS
M92.8
937
ng/L
1.0
3796834
---
---
---
70 -
130
93
100
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Fals
e
Perf
luoro
hexa
noic
aci
d (
PF
HxA
)537
2.0
UQ
CS
M94.3
009
ng/L
1.0
3796834
---
---
---
70 -
130
94
100
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Fals
e
Perf
luoro
lauric
aci
d (
PF
DoA
)537
2.0
UQ
CS
M94.9
277
ng/L
1.0
3796834
---
---
---
70 -
130
95
100
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Fals
e
Perf
luoro
myr
istic
aci
d (
PF
TA
)537
2.0
UQ
CS
M94.8
577
ng/L
1.0
3796834
---
---
---
70 -
130
95
100
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Fals
e
Perf
luoro
nonanoic
aci
d (
PF
NA
)537
2.0
UQ
CS
M96.8
010
ng/L
1.0
3796834
---
---
---
70 -
130
97
100
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Fals
e
Perf
luoro
oct
ane s
ulfo
nate
(P
FO
S)
537
2.0
UQ
CS
M92.4
556
ng/L
1.0
3796834
---
---
---
70 -
130
92
100
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Fals
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
UQ
CS
M93.8
446
ng/L
1.0
3796834
---
---
---
70 -
130
94
100
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Fals
e
Perf
luoro
trid
eca
noic
aci
d (
PF
TrD
A)
537
2.0
UQ
CS
M95.7
611
ng/L
1.0
3796834
---
---
---
70 -
130
96
100
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Fals
e
Perf
luoro
undeca
noic
aci
d (
PF
UnA
)537
2.0
UQ
CS
M92.8
426
ng/L
1.0
3796834
---
---
---
70 -
130
93
100
10/1
1/2
017 1
2:4
010/1
1/2
017 1
9:2
0
Tru
e
IS-P
FO
A-1
3C
2537
N/A
LR
B1747310.0
0ng/L
1.0
3796817
---
---
---
50 -
150
99
1765390
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Tru
e
IS-P
FO
S-1
3C
4537
N/A
LR
B316177.0
0ng/L
1.0
3796817
---
---
---
50 -
150
101
313002
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Tru
e
SS
-PF
DA
-13C
2537
N/A
LR
B94.0
317
ng/L
1.0
3796817
---
---
---
70 -
130
94
100
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Tru
e
SS
-PF
HxA
-13C
2537
N/A
LR
B47.8
147
ng/L
1.0
3796817
---
---
---
70 -
130
96
50.0
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Tru
e
Perf
luoro
buta
nesu
lfonic
aci
d (
PF
BS
)537
2.0
LR
B2.0
ng/L
1.0
3796817
---
---
---
---
---
<
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Tru
e
Perf
luoro
deca
noic
aci
d (
PF
DA
)537
2.0
LR
B2.0
ng/L
1.0
3796817
---
---
---
---
---
<
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Tru
e
Perf
luoro
hepta
noic
aci
d (
PF
HpA
)537
2.0
LR
B2.0
ng/L
1.0
3796817
---
---
---
---
---
<
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Tru
e
Perf
luoro
hexa
nesu
lfonic
aci
d (
PF
HxS
)537
2.0
LR
B2.0
ng/L
1.0
3796817
---
---
---
---
---
<
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Pa
ge
2 o
f 3
EE
A R
un
ID
23
55
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EA
Re
po
rt #
39
98
12
Page 14 of 21
~
D DJ D DJ
□--□--□□--□--□ DODD □□□□--□□--□
Sam
ple
Typ
e
EE
A
ID #
An
aly
zed
Extr
acte
dR
PD
Un
its
Targ
et
Am
ou
nt
Clien
t ID
MR
LM
eth
od
An
aly
teD
il
Facto
r
RP
D
Lim
it
Reco
very
Lim
its
%
Reco
very
Resu
lt
Fla
gQC
Su
mm
ary
Re
po
rt (
co
nt.
)
Tru
e
Perf
luoro
hexa
noic
aci
d (
PF
HxA
)537
2.0
LR
B2.0
ng/L
1.0
3796817
---
---
---
---
---
<
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Tru
e
Perf
luoro
lauric
aci
d (
PF
DoA
)537
2.0
LR
B2.0
ng/L
1.0
3796817
---
---
---
---
---
<
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Tru
e
Perf
luoro
myr
istic
aci
d (
PF
TA
)537
2.0
LR
B2.0
ng/L
1.0
3796817
---
---
---
---
---
<
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Tru
e
Perf
luoro
nonanoic
aci
d (
PF
NA
)537
2.0
LR
B2.0
ng/L
1.0
3796817
---
---
---
---
---
<
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Tru
e
Perf
luoro
oct
ane s
ulfo
nate
(P
FO
S)
537
2.0
LR
B2.0
ng/L
1.0
3796817
---
---
---
---
---
<
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Tru
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
LR
B2.0
ng/L
1.0
3796817
---
---
---
---
---
<
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Tru
e
Perf
luoro
trid
eca
noic
aci
d (
PF
TrD
A)
537
2.0
LR
B2.0
ng/L
1.0
3796817
---
---
---
---
---
<
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Tru
e
Perf
luoro
undeca
noic
aci
d (
PF
UnA
)537
2.0
LR
B2.0
ng/L
1.0
3796817
---
---
---
---
---
<
10/1
1/2
017 0
8:2
010/1
1/2
017 1
9:3
7
Fals
e
IS-P
FO
A-1
3C
2537
N/A
FB
M1797750.0
0ng/L
1.0
3796818
---
---
---
50 -
150
102
1765390
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
Fals
e
IS-P
FO
S-1
3C
4537
N/A
FB
M327320.0
0ng/L
1.0
3796818
---
---
---
50 -
150
105
313002
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
Fals
e
SS
-PF
DA
-13C
2537
N/A
FB
M95.2
725
ng/L
1.0
3796818
---
---
---
70 -
130
95
100
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
Fals
e
SS
-PF
HxA
-13C
2537
N/A
FB
M48.6
209
ng/L
1.0
3796818
---
---
---
70 -
130
97
50.0
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
Fals
e
Perf
luoro
buta
nesu
lfonic
aci
d (
PF
BS
)537
2.0
FB
M96.9
252
ng/L
1.0
3796818
---
---
---
70 -
130
97
100
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
Fals
e
Perf
luoro
deca
noic
aci
d (
PF
DA
)537
2.0
FB
M94.6
381
ng/L
1.0
3796818
---
---
---
70 -
130
95
100
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
Fals
e
Perf
luoro
hepta
noic
aci
d (
PF
HpA
)537
2.0
FB
M96.0
855
ng/L
1.0
3796818
---
---
---
70 -
130
96
100
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
Fals
e
Perf
luoro
hexa
nesu
lfonic
aci
d (
PF
HxS
)537
2.0
FB
M97.2
930
ng/L
1.0
3796818
---
---
---
70 -
130
97
100
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
Fals
e
Perf
luoro
hexa
noic
aci
d (
PF
HxA
)537
2.0
FB
M95.9
127
ng/L
1.0
3796818
---
---
---
70 -
130
96
100
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
Fals
e
Perf
luoro
lauric
aci
d (
PF
DoA
)537
2.0
FB
M94.4
111
ng/L
1.0
3796818
---
---
---
70 -
130
94
100
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
Fals
e
Perf
luoro
myr
istic
aci
d (
PF
TA
)537
2.0
FB
M92.7
821
ng/L
1.0
3796818
---
---
---
70 -
130
93
100
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
Fals
e
Perf
luoro
nonanoic
aci
d (
PF
NA
)537
2.0
FB
M103.5
090
ng/L
1.0
3796818
---
---
---
70 -
130
104
100
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
Fals
e
Perf
luoro
oct
ane s
ulfo
nate
(P
FO
S)
537
2.0
FB
M98.5
486
ng/L
1.0
3796818
---
---
---
70 -
130
99
100
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
Fals
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
FB
M97.4
062
ng/L
1.0
3796818
---
---
---
70 -
130
97
100
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
Fals
e
Perf
luoro
trid
eca
noic
aci
d (
PF
TrD
A)
537
2.0
FB
M92.3
356
ng/L
1.0
3796818
---
---
---
70 -
130
92
100
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
Fals
e
Perf
luoro
undeca
noic
aci
d (
PF
UnA
)537
2.0
FB
M95.3
524
ng/L
1.0
3796818
---
---
---
70 -
130
95
100
10/1
1/2
017 0
8:2
010/1
1/2
017 2
0:1
1
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Page 15 of 21
D
□ DJ
JJDI
JJD
_ DJ __ DD_ -□--□ DODD DOD
Eurofins Eaton Analytical
Run LogRun ID: 235682 Method: 537
Sample SiteSample IdType Instrument ID Calibration FileAnalysis DateMatrix
CCL 3804256 FL 102017M537b-FL-PFC-Ext.mdb10/20/2017 19:34OS
LRB 3804246 FL 102017M537b-FL-PFC-Ext.mdb10/20/2017 20:08RW
FBM 3804247 FL 102017M537b-FL-PFC-Ext.mdb10/20/2017 20:41RW
FTB 3793431 PEF36859 FTB FL 102017M537b-FL-PFC-Ext.mdb10/20/2017 20:58RW
LTB 3793432 PEF36860 LTB-09/13/17 FL 102017M537b-FL-PFC-Ext.mdb10/20/2017 21:15RW
CCM 3804257 FL 102017M537b-FL-PFC-Ext.mdb10/21/2017 00:53OS
0.00
Page 1 of 4 EEA Run ID 235682 / EEA Report # 399812
Page 16 of 21
=::: e u rof i n s I Eaton Analytical
QC
Su
mm
ary
Re
po
rt
EE
A
ID #
RP
DU
nit
sT
arg
et
Am
ou
nt
Clien
t ID
Meth
od
An
aly
teS
am
ple
Typ
e
Dil
Facto
r
RP
D
Lim
it
Reco
very
Lim
its
%
Reco
very
Resu
lt
Fla
g
MR
LE
xtr
acte
dA
naly
zed
Fals
e
IS-N
MeF
OS
AA
-d3
537
N/A
CC
L783896.0
0ng/L
1.0
3804256
---
---
---
50 -
150
100
783896
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
IS-P
FO
A-1
3C
2537
N/A
CC
L1713710.0
0ng/L
1.0
3804256
---
---
---
50 -
150
100
1713710
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
IS-P
FO
S-1
3C
4537
N/A
CC
L304248.0
0ng/L
1.0
3804256
---
---
---
50 -
150
100
304248
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
IS-G
enX
-13C
3537
N/A
CC
L7251.9
9ng/L
1.0
3804256
---
---
---
50 -
150
100
7251.9
9
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
SS
-NE
tFO
SA
A-d
5537
N/A
CC
L199.0
720
ng/L
1.0
3804256
---
---
---
70 -
130
100
200
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
SS
-PF
DA
-13C
2537
N/A
CC
L99.2
622
ng/L
1.0
3804256
---
---
---
70 -
130
99
100
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
SS
-PF
HxA
-13C
2537
N/A
CC
L50.3
141
ng/L
1.0
3804256
---
---
---
70 -
130
101
50.0
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
Perf
luoro
buta
nesu
lfonic
aci
d (
PF
BS
)537
2.0
CC
L1.9
321
ng/L
1.0
3804256
---
---
---
50 -
150
97
2.0
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
Perf
luoro
deca
noic
aci
d (
PF
DA
)537
2.0
CC
L1.9
155
ng/L
1.0
3804256
---
---
---
50 -
150
96
2.0
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
Perf
luoro
hepta
noic
aci
d (
PF
HpA
)537
2.0
CC
L1.9
163
ng/L
1.0
3804256
---
---
---
50 -
150
96
2.0
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
Perf
luoro
hexa
nesu
lfonic
aci
d (
PF
HxS
)537
2.0
CC
L1.8
745
ng/L
1.0
3804256
---
---
---
50 -
150
94
2.0
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
Perf
luoro
hexa
noic
aci
d (
PF
HxA
)537
2.0
CC
L1.9
880
ng/L
1.0
3804256
---
---
---
50 -
150
99
2.0
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
Perf
luoro
lauric
aci
d (
PF
DoA
)537
2.0
CC
L1.9
489
ng/L
1.0
3804256
---
---
---
50 -
150
97
2.0
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
Perf
luoro
myr
istic
aci
d (
PF
TA
)537
2.0
CC
L2.0
377
ng/L
1.0
3804256
---
---
---
50 -
150
102
2.0
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
Perf
luoro
nonanoic
aci
d (
PF
NA
)537
2.0
CC
L1.9
359
ng/L
1.0
3804256
---
---
---
50 -
150
97
2.0
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
Perf
luoro
oct
ane s
ulfo
nate
(P
FO
S)
537
2.0
CC
L1.9
362
ng/L
1.0
3804256
---
---
---
50 -
150
97
2.0
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
CC
L1.9
621
ng/L
1.0
3804256
---
---
---
50 -
150
98
2.0
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
Perf
luoro
trid
eca
noic
aci
d (
PF
TrD
A)
537
2.0
CC
L2.0
158
ng/L
1.0
3804256
---
---
---
50 -
150
101
2.0
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Fals
e
Perf
luoro
undeca
noic
aci
d (
PF
UnA
)537
2.0
CC
L1.9
582
ng/L
1.0
3804256
---
---
---
50 -
150
98
2.0
10/2
0/2
017 1
4:1
310/2
0/2
017 1
9:3
4
Tru
e
IS-N
MeF
OS
AA
-d3
537
N/A
LR
B817541.0
0ng/L
1.0
3804246
---
---
---
50 -
150
104
783896
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:0
8
Tru
e
IS-P
FO
A-1
3C
2537
N/A
LR
B1823210.0
0ng/L
1.0
3804246
---
---
---
50 -
150
106
1713710
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:0
8
Tru
e
IS-P
FO
S-1
3C
4537
N/A
LR
B318081.0
0ng/L
1.0
3804246
---
---
---
50 -
150
105
304248
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:0
8
Tru
e
IS-G
enX
-13C
3537
N/A
LR
B7938.9
8ng/L
1.0
3804246
---
---
---
50 -
150
109
7251.9
9
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:0
8
Tru
e
SS
-NE
tFO
SA
A-d
5537
N/A
LR
B167.6
580
ng/L
1.0
3804246
---
---
---
70 -
130
84
200
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:0
8
Tru
e
SS
-PF
DA
-13C
2537
N/A
LR
B89.3
803
ng/L
1.0
3804246
---
---
---
70 -
130
89
100
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:0
8
Tru
e
SS
-PF
HxA
-13C
2537
N/A
LR
B44.8
853
ng/L
1.0
3804246
---
---
---
70 -
130
90
50.0
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:0
8
Tru
e
Perf
luoro
buta
nesu
lfonic
aci
d (
PF
BS
)537
2.0
LR
B2.0
ng/L
1.0
3804246
---
---
---
---
---
<
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:0
8
Tru
e
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noic
aci
d (
PF
DA
)537
2.0
LR
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ng/L
1.0
3804246
---
---
---
---
---
<
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:0
8
Tru
e
Perf
luoro
hepta
noic
aci
d (
PF
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)537
2.0
LR
B2.0
ng/L
1.0
3804246
---
---
---
---
---
<
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:0
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Tru
e
Perf
luoro
hexa
nesu
lfonic
aci
d (
PF
HxS
)537
2.0
LR
B2.0
ng/L
1.0
3804246
---
---
---
---
---
<
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:0
8
Tru
e
Perf
luoro
hexa
noic
aci
d (
PF
HxA
)537
2.0
LR
B2.0
ng/L
1.0
3804246
---
---
---
---
---
<
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:0
8
Tru
e
Perf
luoro
lauric
aci
d (
PF
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)537
2.0
LR
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ng/L
1.0
3804246
---
---
---
---
---
<
10/2
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017 0
8:1
110/2
0/2
017 2
0:0
8
Tru
e
Perf
luoro
myr
istic
aci
d (
PF
TA
)537
2.0
LR
B2.0
ng/L
1.0
3804246
---
---
---
---
---
<
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:0
8
Tru
e
Perf
luoro
nonanoic
aci
d (
PF
NA
)537
2.0
LR
B2.0
ng/L
1.0
3804246
---
---
---
---
---
<
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:0
8
Tru
e
Perf
luoro
oct
ane s
ulfo
nate
(P
FO
S)
537
2.0
LR
B2.0
ng/L
1.0
3804246
---
---
---
---
---
<
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:0
8
Tru
e
Perf
luoro
oct
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aci
d (
PF
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)537
2.0
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ng/L
1.0
3804246
---
---
---
---
---
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10/2
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017 0
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2.0
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ng/L
1.0
3804246
---
---
---
---
---
<
10/2
0/2
017 0
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110/2
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017 2
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PF
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)537
2.0
LR
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ng/L
1.0
3804246
---
---
---
---
---
<
10/2
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017 0
8:1
110/2
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017 2
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8
Fals
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IS-N
MeF
OS
AA
-d3
537
N/A
FB
M829611.0
0ng/L
1.0
3804247
---
---
---
50 -
150
106
783896
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
IS-P
FO
A-1
3C
2537
N/A
FB
M1814130.0
0ng/L
1.0
3804247
---
---
---
50 -
150
106
1713710
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Pa
ge
2 o
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Page 17 of 21
~ ~
D D D DJ
□□□□--□□--□--□ □--□ □--□--□□--□--□
Sam
ple
Typ
e
EE
A
ID #
An
aly
zed
Extr
acte
dR
PD
Un
its
Targ
et
Am
ou
nt
Clien
t ID
MR
LM
eth
od
An
aly
teD
il
Facto
r
RP
D
Lim
it
Reco
very
Lim
its
%
Reco
very
Resu
lt
Fla
gQC
Su
mm
ary
Re
po
rt (
co
nt.
)
Fals
e
IS-P
FO
S-1
3C
4537
N/A
FB
M322001.0
0ng/L
1.0
3804247
---
---
---
50 -
150
106
304248
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
IS-G
enX
-13C
3537
N/A
FB
M8018.2
2ng/L
1.0
3804247
---
---
---
50 -
150
111
7251.9
9
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
SS
-NE
tFO
SA
A-d
5537
N/A
FB
M176.9
200
ng/L
1.0
3804247
---
---
---
70 -
130
88
200
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
SS
-PF
DA
-13C
2537
N/A
FB
M95.9
543
ng/L
1.0
3804247
---
---
---
70 -
130
96
100
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
SS
-PF
HxA
-13C
2537
N/A
FB
M44.7
950
ng/L
1.0
3804247
---
---
---
70 -
130
90
50.0
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
Perf
luoro
buta
nesu
lfonic
aci
d (
PF
BS
)537
2.0
FB
M96.2
633
ng/L
1.0
3804247
---
---
---
70 -
130
96
100
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
Perf
luoro
deca
noic
aci
d (
PF
DA
)537
2.0
FB
M91.2
147
ng/L
1.0
3804247
---
---
---
70 -
130
91
100
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
Perf
luoro
hepta
noic
aci
d (
PF
HpA
)537
2.0
FB
M87.3
586
ng/L
1.0
3804247
---
---
---
70 -
130
87
100
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
Perf
luoro
hexa
nesu
lfonic
aci
d (
PF
HxS
)537
2.0
FB
M96.4
092
ng/L
1.0
3804247
---
---
---
70 -
130
96
100
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
Perf
luoro
hexa
noic
aci
d (
PF
HxA
)537
2.0
FB
M85.7
089
ng/L
1.0
3804247
---
---
---
70 -
130
86
100
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
Perf
luoro
lauric
aci
d (
PF
DoA
)537
2.0
FB
M92.4
863
ng/L
1.0
3804247
---
---
---
70 -
130
92
100
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
Perf
luoro
myr
istic
aci
d (
PF
TA
)537
2.0
FB
M92.7
493
ng/L
1.0
3804247
---
---
---
70 -
130
93
100
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
Perf
luoro
nonanoic
aci
d (
PF
NA
)537
2.0
FB
M94.6
323
ng/L
1.0
3804247
---
---
---
70 -
130
95
100
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
Perf
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oct
ane s
ulfo
nate
(P
FO
S)
537
2.0
FB
M95.2
310
ng/L
1.0
3804247
---
---
---
70 -
130
95
100
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
FB
M91.2
696
ng/L
1.0
3804247
---
---
---
70 -
130
91
100
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
Perf
luoro
trid
eca
noic
aci
d (
PF
TrD
A)
537
2.0
FB
M93.1
354
ng/L
1.0
3804247
---
---
---
70 -
130
93
100
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Fals
e
Perf
luoro
undeca
noic
aci
d (
PF
UnA
)537
2.0
FB
M92.8
095
ng/L
1.0
3804247
---
---
---
70 -
130
93
100
10/2
0/2
017 0
8:1
110/2
0/2
017 2
0:4
1
Tru
e
IS-N
MeF
OS
AA
-d3
537
N/A
FT
B960652.0
0ng/L
0.9
13793431
PE
F36859 F
TB
---
---
50 -
150
123
783896
10/1
1/2
017 0
8:2
010/2
0/2
017 2
0:5
8
Tru
e
IS-P
FO
A-1
3C
2537
N/A
FT
B1874550.0
0ng/L
0.9
13793431
PE
F36859 F
TB
---
---
50 -
150
109
1713710
10/1
1/2
017 0
8:2
010/2
0/2
017 2
0:5
8
Tru
e
IS-P
FO
S-1
3C
4537
N/A
FT
B328363.0
0ng/L
0.9
13793431
PE
F36859 F
TB
---
---
50 -
150
108
304248
10/1
1/2
017 0
8:2
010/2
0/2
017 2
0:5
8
Tru
e
IS-G
enX
-13C
3537
N/A
FT
B7877.3
9ng/L
0.9
13793431
PE
F36859 F
TB
---
---
50 -
150
109
7251.9
9
10/1
1/2
017 0
8:2
010/2
0/2
017 2
0:5
8
Tru
e
SS
-NE
tFO
SA
A-d
5537
N/A
FT
B206.9
500
ng/L
0.9
13793431
PE
F36859 F
TB
---
---
70 -
130
114
200
10/1
1/2
017 0
8:2
010/2
0/2
017 2
0:5
8
Tru
e
SS
-PF
DA
-13C
2537
N/A
FT
B96.1
124
ng/L
0.9
13793431
PE
F36859 F
TB
---
---
70 -
130
106
100
10/1
1/2
017 0
8:2
010/2
0/2
017 2
0:5
8
Tru
e
SS
-PF
HxA
-13C
2537
N/A
FT
B46.2
517
ng/L
0.9
13793431
PE
F36859 F
TB
---
---
70 -
130
102
50.0
10/1
1/2
017 0
8:2
010/2
0/2
017 2
0:5
8
Tru
e
Perf
luoro
buta
nesu
lfonic
aci
d (
PF
BS
)537
2.0
FT
B2.0
ng/L
0.9
13793431
PE
F36859 F
TB
---
---
---
---
<
10/1
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8:2
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Tru
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aci
d (
PF
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)537
2.0
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F36859 F
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---
---
---
---
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10/1
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d (
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F36859 F
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---
---
---
---
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10/1
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Perf
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---
---
---
---
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10/1
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F36859 F
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---
---
---
---
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10/1
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13793431
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F36859 F
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---
---
---
---
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Tru
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0.9
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F36859 F
TB
---
---
---
---
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10/1
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Tru
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2.0
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---
---
---
---
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10/1
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Tru
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FO
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537
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0.9
13793431
PE
F36859 F
TB
---
---
---
---
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10/1
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Tru
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2.0
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0.9
13793431
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TB
---
---
---
---
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10/1
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010/2
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0.9
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---
---
---
---
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10/1
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8:2
010/2
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0.9
13793431
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TB
---
---
---
---
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10/1
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017 0
8:2
010/2
0/2
017 2
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Fals
e
IS-N
MeF
OS
AA
-d3
537
N/A
LT
B954694.0
0ng/L
0.9
3793432
PE
F36860 L
TB
-09/1
3/1
7--
---
-50 -
150
122
783896
10/1
1/2
017 0
8:2
010/2
0/2
017 2
1:1
5
Fals
e
IS-P
FO
A-1
3C
2537
N/A
LT
B1897490.0
0ng/L
0.9
3793432
PE
F36860 L
TB
-09/1
3/1
7--
---
-50 -
150
111
1713710
10/1
1/2
017 0
8:2
010/2
0/2
017 2
1:1
5
Fals
e
IS-P
FO
S-1
3C
4537
N/A
LT
B323730.0
0ng/L
0.9
3793432
PE
F36860 L
TB
-09/1
3/1
7--
---
-50 -
150
106
304248
10/1
1/2
017 0
8:2
010/2
0/2
017 2
1:1
5
Fals
e
IS-G
enX
-13C
3537
N/A
LT
B8641.7
5ng/L
0.9
3793432
PE
F36860 L
TB
-09/1
3/1
7--
---
-50 -
150
119
7251.9
9
10/1
1/2
017 0
8:2
010/2
0/2
017 2
1:1
5
Fals
e
SS
-NE
tFO
SA
A-d
5537
N/A
LT
B206.6
310
ng/L
0.9
3793432
PE
F36860 L
TB
-09/1
3/1
7--
---
-70 -
130
115
200
10/1
1/2
017 0
8:2
010/2
0/2
017 2
1:1
5
Pa
ge
3 o
f 4
EE
A R
un
ID
23
56
82
/ E
EA
Re
po
rt #
39
98
12
Page 18 of 21
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An
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Fals
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2537
N/A
LT
B94.0
926
ng/L
0.9
3793432
PE
F36860 L
TB
-09/1
3/1
7--
---
-70 -
130
105
100
10/1
1/2
017 0
8:2
010/2
0/2
017 2
1:1
5
Fals
e
SS
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HxA
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2537
N/A
LT
B44.5
144
ng/L
0.9
3793432
PE
F36860 L
TB
-09/1
3/1
7--
---
-70 -
130
99
50.0
10/1
1/2
017 0
8:2
010/2
0/2
017 2
1:1
5
Fals
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Perf
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0.9
3793432
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F36860 L
TB
-09/1
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---
---
---
-
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010/2
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Fals
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Perf
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2.0
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0.9
3793432
PE
F36860 L
TB
-09/1
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7--
---
---
---
-
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017 0
8:2
010/2
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Fals
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Perf
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0.9
3793432
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F36860 L
TB
-09/1
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---
---
---
-
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017 0
8:2
010/2
0/2
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Fals
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Perf
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2.0
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0.9
3793432
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F36860 L
TB
-09/1
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7--
---
---
---
-
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8:2
010/2
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Fals
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2.0
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0.9
3793432
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F36860 L
TB
-09/1
3/1
7--
---
---
---
-
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Fals
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2.0
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0.9
3793432
PE
F36860 L
TB
-09/1
3/1
7--
---
---
---
-
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Fals
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2.0
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0.9
3793432
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F36860 L
TB
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---
---
---
-
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Fals
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3793432
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F36860 L
TB
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---
---
---
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Fals
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F36860 L
TB
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---
---
---
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Fals
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TB
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---
---
---
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Fals
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TB
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---
---
---
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0.9
3793432
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F36860 L
TB
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3/1
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---
---
---
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017 0
8:2
010/2
0/2
017 2
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Tru
e
IS-N
MeF
OS
AA
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537
N/A
CC
M818341.0
0ng/L
1.0
3804257
---
---
---
50 -
150
100
818341
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
IS-P
FO
A-1
3C
2537
N/A
CC
M1768840.0
0ng/L
1.0
3804257
---
---
---
50 -
150
100
1768840
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
IS-P
FO
S-1
3C
4537
N/A
CC
M313944.0
0ng/L
1.0
3804257
---
---
---
50 -
150
100
313944
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
IS-G
enX
-13C
3537
N/A
CC
M7563.0
4ng/L
1.0
3804257
---
---
---
50 -
150
100
7563.0
4
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
SS
-NE
tFO
SA
A-d
5537
N/A
CC
M201.8
620
ng/L
1.0
3804257
---
---
---
70 -
130
101
200
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
SS
-PF
DA
-13C
2537
N/A
CC
M98.3
485
ng/L
1.0
3804257
---
---
---
70 -
130
98
100
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
SS
-PF
HxA
-13C
2537
N/A
CC
M48.6
021
ng/L
1.0
3804257
---
---
---
70 -
130
97
50.0
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
Perf
luoro
buta
nesu
lfonic
aci
d (
PF
BS
)537
2.0
CC
M97.6
198
ng/L
1.0
3804257
---
---
---
70 -
130
98
100
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
Perf
luoro
deca
noic
aci
d (
PF
DA
)537
2.0
CC
M97.8
170
ng/L
1.0
3804257
---
---
---
70 -
130
98
100
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
Perf
luoro
hepta
noic
aci
d (
PF
HpA
)537
2.0
CC
M96.5
528
ng/L
1.0
3804257
---
---
---
70 -
130
97
100
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
Perf
luoro
hexa
nesu
lfonic
aci
d (
PF
HxS
)537
2.0
CC
M97.5
045
ng/L
1.0
3804257
---
---
---
70 -
130
98
100
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
Perf
luoro
hexa
noic
aci
d (
PF
HxA
)537
2.0
CC
M96.6
162
ng/L
1.0
3804257
---
---
---
70 -
130
97
100
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
Perf
luoro
lauric
aci
d (
PF
DoA
)537
2.0
CC
M96.2
915
ng/L
1.0
3804257
---
---
---
70 -
130
96
100
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
Perf
luoro
myr
istic
aci
d (
PF
TA
)537
2.0
CC
M98.5
777
ng/L
1.0
3804257
---
---
---
70 -
130
99
100
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
Perf
luoro
nonanoic
aci
d (
PF
NA
)537
2.0
CC
M99.4
858
ng/L
1.0
3804257
---
---
---
70 -
130
99
100
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
Perf
luoro
oct
ane s
ulfo
nate
(P
FO
S)
537
2.0
CC
M98.1
474
ng/L
1.0
3804257
---
---
---
70 -
130
98
100
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
Perf
luoro
oct
anoic
aci
d (
PF
OA
)537
2.0
CC
M98.4
584
ng/L
1.0
3804257
---
---
---
70 -
130
98
100
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
Perf
luoro
trid
eca
noic
aci
d (
PF
TrD
A)
537
2.0
CC
M99.0
507
ng/L
1.0
3804257
---
---
---
70 -
130
99
100
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Tru
e
Perf
luoro
undeca
noic
aci
d (
PF
UnA
)537
2.0
CC
M97.6
129
ng/L
1.0
3804257
---
---
---
70 -
130
98
100
10/2
0/2
017 1
4:1
310/2
1/2
017 0
0:5
3
Pa
ge
4 o
f 4
EE
A R
un
ID
23
56
82
/ E
EA
Re
po
rt #
39
98
12
Page 19 of 21
~ l R DD D D DJ
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on
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on
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MC
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id
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Page 20 of 21
END OF REPORT
Page 21 of 21