osePh · 2017-06-09 · T~ese levels equate to 0.5, 1.0,20, 5.0, 10,25 and 50 /-LgiL for water samples. A Hewlett-Packard 5890 gas chromatograph ith a 30m x 0.32mm RTX-624 micro-capillary

Nationwide Mobile Laboratories Pesticide Residue Laboratory

Chemistry Consulting

December 11 2008

Robert Martin Martin and Slagle PO Box 1023 Black Mountain NC 28711

Dear Mr Martin

Enclosed is the Technical Memorandum for VOC work recently performed at the Kuhlman Electric Corporation (KEC) facility in Crystal Springs MS Ifyou have any questions concerning this information give me a call

Sincerely

~-~~ ~osePh Kubale

Enclosure

Environmental Chemist Consulting Services Inc

2525 Advanc Road Madison WI 53718 (608) 221-8700 (608) 221-

1 889 wwweccsmobilelabcom

Technical Memorandum

Kuhlman Electric Corporation (KEC)

Crystal sprilgs Mississippi



TECHNICAL MEMORANDUM

December 11 2008

To Robert Martin Martin and Slagle

t-lFrom Joseph Ku balef ECCS v

Re Analytical Methods Volatile Organic Compounds (VOC) ~ 14-Dioxane Kuhlman Electric Corporation (KEC)middot Crystal Springs MS

Introdnction

This Technical Memorandum provides documkntation of the analytical test methods used to analyze water samples collected in November 2008 during the city well groundwater sampling event near the Kuhlman Electric Corporation (kEC) facility in Crystal Springs MS The samples were analyzed by purge and trap GCrSD for the VOCs listed below and by direct injection GCIMSDSIM for l4-Dioxane

Narrative

Waters i

Water samples were analyzed for VOCs directly by purge and trap GCIMSD and for 14shyDioxane by direct injection GCMSDSIM

The following report limits were used for watet samples The reporting limit units are in ugL

Purge an Trap GCMSD Dichlorodifluoromethane l Chloromethane Vinyl chloride 1l~Bromomethane 1 Chloroethane L Trichlorofluoromethane 10

Environmental Chemist~ Consulting Services Inc

2525 Advance Road Madison WI 53718 608 221-8700 608 221-4889 wwweccsmobilelabcom

11-Dichloroethene Methylene chloride trans-l 2-Dichloroethene 11-Dichloroethane cis-l2-Dichloroethene 22-Dichloropropane Bromochloromethane Chloroform 11 I-Trichloroethane 11-Dichloropropene Carbon tetrachloride Benzene 12-Dichloroethane Trichloroethene 12-Dichloropropane Dibromomethane Bromodichloromethane cis-I3-Dichloropropene Toluene trans-l 3-Dichloropropene 112-Trichloroethane Tetrachloroethene 13-Dichloropropane Dibromochloromethane 12-Dibromoethane Chlorobenzene 1112-Tetrachloroethane Ethyl benzene Xylenes total Styrene Bromoform Isopropylbenzene 1122-Tetrachloroethane Bromobenzene 123-Trichloropropane n-Propylbenzene 2-Chlorotoluene 135-Trimethylbenzene 4-Chlorotoluene tert-Butylbenzene 124-Trimethylbenzene sec-Butylbenzene 13-Dichlorobenzene p-Isopropyltoluene 14-Dichlorobenzene n-Butylbenzene 12-Dichlorobenzene 12-Dibromo-3 -chloropropane 135-Trichlorobenzene 124-Trichlorobenzene Hexachlorobutadiene

Purge 1Trap GCMSD 10 110 liO 10 liO 10 10 10 10 10 10 110 10 If0 EO 10 10 10 1 0 10 1 0 1 0 20 10 liO 110 10 ItO 20 1 0 20 1 0 20 10 2]0 10 10110

10 10 10 10 10 10 10 1 10 20 110 10 Ip

Purge anJi~Trap GCMSDNaphthalene 123-Trichlorooenzene 10

Direct [ection GCMSDSIM l4-Dioxane 10

A summary ofvolatile test results is provided n Table 1 A summary of l4-Dioxane results is provided in table 2 A summary ofmethod lanks and matrix spikematrix spike duplicate data is providedin Table 3 and 4 respectivelyl

In addition copies of the chain ofcustody shee~s and shipping sheets can be found in appendix A through C bull

A) Chain ofcustody sheets for samples B) FEDEX shipping label for Columbia Analytical Services Inc C) Chain of custody sheets for samplek sent to Columbia Analytical Services Inc

VOC Method sectummary

Water Samples Water samples were provided by the client to e lab in 40mL VOC vials A lOmL aliquot of the sample was withdrawn from the vial with 1 OmL Luer-Lok tradesyringe 1deg-LL of a 25-LglmL surrogate and internal standard solution was added to the sample in the 10 mL syringe The sample was then immediately lo~ded onto a Tekmar ALS 2016 autosampler with a Tekmar LSC 2000 purge and trap concentrat~r for GCMSD analysis

GCMSD Procedure I Identification of target compounds was done ~matching retention times and mass spectra of peaks found in samples to those found in a V C calibration standard using the internal standards as time reference peaks Quantitatio was performed by the internal standard technique using a seven point standard curve1nerated from 5 102050 100250 and 500 ng standards T~ese levels equate to 05 1020 50 1025 and 50 -LgiL for water samples

A Hewlett-Packard 5890 gas chromatograph ith a 30m x 032mm RTX-624 micro-capillary column interfaced to a Hewlett-Packard 5972 MSD was used The data system included a Hewlett-Packard Enviroquant chromatography workstation for data handling

I

Quality control consisted of the following items

Initial calibration with relative smiddot dard deviation less than 15 of individual response factors obtained from ana ysis of calibration standards Continuing Calibration Verificatio standards analyzed at a frequency of every ten samples or less Surrogate standard additions to sa les Blank and LCS samples analyzed e ery twenty samples or less with a minimum of one per day per matrix MSMSD samples analyzed every t enty samples or less per matrix Information documented in Logboo 150

14-Dioxane Method Summary I

Water Samples i

Water samples were provided by the client to the lab in 1 L amber bottle 200 grams of sample was transferred to the filtering apparatus spik~d with 40uL 25uglmL surrogate solution and 40uL 25ugmL spike solution (if necessary) then filtered through a 3M 2272 activated carbon disk The activated carbon disk was placed ina 3 dram vial containing 8mL methanol and sonicated for 15 minutes A 08mL aliquot ofithe sample extract was spiked with lOuL 25uglmL internal standard solution and anal middoted by direct inject GCIMSDSIM

GCIMSD Procdture Identification of the target compound was don by matching retention times quantitaion and qualifier ion relative responses to that of an au hentic standard Quantitation is accomplished by comparing the response of the major (quan itation) ion relative to an in internal standard using a seven point calibration curve These l~vels equate to 05 102550 1050 and 100 ugIL for water s~mples I

A Hewlett-Packard 5890 Series II gas chroma(ograph with a 30m x 032mm 18u film RTXshy624 micro-capillary column interfaced to a Hewlett-Packard 5972 MSD was used The data system included a Hewlett-Packard Enviroquant chromatography workstation for data handling


Initial calibration with relative srandard deviation less than 15 of individual resppnse factors obtained from an lysis of calibration standards

Continuing Calibration Verificatio standards analyzed at a frequency of every ten samples or less Surrogate standard additions to sa pIes Blank and LCS samples analyzed e ery twenty samples or less with a minimum of one per day per matrix MSIMSD samples analyzed every enty samples or less per matrix Infoqnation documented in Logbo k 196

Sample Results olatiIes- November

TABLE 1 Kuhlman Electric - Crvstal Sorinas Mississiooi - Volatiles Detected in Wat_

VOLATILES ~

Depth Date Collected Time Collected Date Analyzed Reporting Limit

ugL

W2466 CSW WAS 030 -

12-Nov-08 815

12-Nov-08

W2467 CSW WA3 030 -

12-Nov-08 820

12-Nov-08

W2468 CSW WA1 030 -

12-Nov-08 830

12-Nov-08

-

W2469 CSW WA2 030 -

12-Nov-08 841

12-Nov-08

W2470 CSW

FB 030 -

12-Nov-08 845

12-Nov-08

~ ~~

W2471 CSW WA5 025 -

12-Nov-08 905

12-Nov-08

-- - ~

W2472 CSW WA6 025 -

12-Nov-08 925

12-Nov-08

W2473 CSW TP 030 -

12-Nov-08 935

12-Nov-08

~

W2474 CSW

Duplicate

12-Nov-08 -

12-Nov-08

-~- -

Dichlorodifluoromethane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Chloromethane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Vinyl Chloride 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Bromomethane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Chloroethane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Trichlorofluoromethane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 1 1-Dichloroethene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Methylene Chloride 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 trans-12-Dichloroethene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 11-Dichloroethane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 cis-12-Dichloroethene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10

) 1__ ~~~ ~ F~ ~ ~ ~

v ~ n

~ ~9-- ~ n ~

lt ~e ~ n ~

~ n ~

~ n v 4-9-shy 4-C

Bromochloromethane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Chloroform 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 11 1-Trichloroethane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 1 1-Dichloropropene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Carbon Tetrachloride 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Benzene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 12-Dichloroethane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Trichloroethene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 12-Dichloropropane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Dibromomethane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Bromodichloromethane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 cis-13-Dichloropropene 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 Toluene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 trans-13-Dichloropropene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 112-Trichloroethane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Tetrachloroethene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 13-Dichloropropane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Dibromochloromethane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 11 lt 10 12-Dibromoethane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Chlorobenzene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 1112-Tetrachloroethane 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Ethyl Benzene 10 lt 10 lt 10 lt 10_ lt 10 lt 10 lt 10 lt 10 lt 10 lt 10

Page 1

TABLE 1 K C~ ----~IS- ~-J ~ bullbull --- _- _ - --_ ~--

W2466 W2467 W2468 W2469 W2470 W2471 W2472 W2473 W2474

CSW CSW CSW CSW CSW CSW CSW CSW CSW

WAS WA3 WA1 WA2 FB WA5 WA6 TP Duplicate

030 030 030 030 030 025 025 030

Depth - - - - - -Date Collected 12-Nov-08 12-Nov-08 12-Nov-08 12-Nov-08 12-Nov-08 12-Nov-08 12-Nov-08 12-Nov-08 12-Nov-08

Time Collected 815 820 830 841 845 905 925 935 -Date Analyzed 12-Nov-08 12-Nov-08 12-Nov-08 12-Nov-08 12-Nov-08 12-Nov-08 12-Nov-08 12-Nov-08 12-Nov-08

Reporting Limit

VOLATILES - ugL ~ ~ - shy -

Xylenes Total 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 Styrene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Bromoform 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 Isopropylbenzene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 1122-Tetrachloroethane 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 Bromobenzene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 123-Trichloropropane 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 n-Propylbenzene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 2-Chlorotoluene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 135-Trimethylbenzene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 4-Chlorotoluene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 ted-ButylberJZene 1 n C 10 lt tI

10 -lt 10- lt 10 lt 1~ ~O-- lt 10

V

124-Trimethylbenzene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 sec-Butylbenzene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 13-Dichlorobenzene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Ip-Isopropyltoluene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 14-Dichlorobenzene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 n-Butylbenzene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 1 2-Dichlorobenzene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 1 2-Dibromo-3-Chloropropane 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 lt 20 135-Trichlorobenzene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 124-Trichlorobenzene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Hexachlorobutadiene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Naphthalene 30 lt 30 lt 30 lt 30 lt 30 lt 30 lt 30 lt 30 lt 30 lt 30 123-Trichlorobenzene 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 lt 10 Surrogates Dibromofluoromethane 109 105 105 107 103 102 977 105 103 Toluene-D8 954 967 974 953 983 103 114 104 990 4-Bromofluorobenzene 922 934 924 939 920 939 968 943 914

Page 2

Table 2

Sample Results 1iDioxane- November

TABLE 2 Kuhl Electric - Crvstal S Mississiooi - 14-D Detected in Wat_

VOLATILES

1 4-Dioxane


ugL

10 lt

W2466

CSW

WAS

030

-12-Nov-08

815

13-Nov-08

10 lt

W2467

CSW

WA3

030

-12-Nov-08

820

13-Nov-08

10 lt

W2468

CSW

WA1

030

-12-Nov-08

830

13-Nov-08

10 lt

W2469

CSW

WA2

030

-12-Nov-08

841

13-Nov-08

10 lt

W2470

CSW

FB 030

-12-Nov-08

845

13-Nov-08

10 lt

W2471

CSW

WA5

025

-

12-Nov-08

905

13-Nov-08

10 lt

W2472

CSW

WA6

025

-12-Nov-08

925

13-Nov-08

-

10 lt

W2473

CSW

TP 030

-12-Nov-08

935

13-Nov-08

10 lt

W2474 I

CSW

Duplicate

12-Nov-08

-13-Nov-08

10

Surrogates 14-Dioxane-D8 831 943 888 919 953 947 885 899 948

Page 1

Tarle 3

QC Results Vol tiles- November

TAJLE 3 QC Report

Lab associated with qc salpies W2466 through W2474

Matrix

Matrix Spike

Spike uplicate Blank

W2466 W2466

Date Analyzed 111208 ~ 1112108 111208

Compound

Dichlorodifluoromethane

Chloromethane

Vinyl chloride

Bromomethane

Chloroethane

Trichlorofluoromethane

11-Dichloroethene

Methylene chloride

trans-1 2-Dichloroethene

11-Dichloroethane

cis-12-Dichloroethene

22-Dichloropropane

Bromochloromethane

Chloroform

111-Trichloroethane

1 1-Dichloropropene

Carbon tetrachloride

Benzene

12-Dichloroethane

T richloroethene

12-Dichloropropane

Dibromomethane

Bromodichloromethane

cis-13-Dichloropropene

Toluene

trans-13-Dichloropropene

112-Trichtoroethane

T etrachloroethene

13-Dichloropropane

Dibromochloromethane

12-Dibromoethane

Chlorobenzene

1112-Tetrachloroethane

Ethyl benzene

Xylenes Total

Styrene

Bromoform

Rec Rec RPD uglL

898 i 884 16 lt 10

924 878 51 lt 10

950 942 08 lt 10

956 110~4 lt 10

103 94 1 lt 10

101 970 40 lt 10

952 101 57 lt 10

978 974 04 lt 10

100 104 33

Bit106 103 25

990 1990 00

978 1978 00 lt 10

102 103 08 lt 10

100 1990 14 lt 10

104 101 29 lt 10

956 972 17 lt 10

102 1 100 22 lt 10

102 102 02 lt 10

974 994 20 lt 10

976 976 00 lt 10

960 102 57 lt 10

980 984 04 lt 10

896 906 11 lt 10

886 1890 05 lt 20

960 976 17 lt 10

866 1896 34 lt 10

988 982 06 lt 10

958

~ lt 10

930 92 04

Bit884 872

912 908 04

101 100 08 lt 10

105 105 04 lt 10

988 994 06 lt 10

988 100 14 H2

O 984 996 12 10

962 972 10 lt 20

Pa~e 1

TAaLE 3 QC Report

Lab associated with qc samples W2466 through W2474

I Matrix

Matrix SpikeI

Spike Duplicate Blank

W2466 W2466

Date Analyzed 111208 1111208 11112108

Compound Rec Rec RPD ugL

Isopropyl benzene 918 916 02 lt 10

1122-Tetrachloroethane 100 1016 16 lt 20

Bromobenzene 984 986 02 lt 10

1 23-Trichloropropane 976 102 48 lt 20

n-Propylbenzene 972 968 04 lt 10

2-Chlorotoluene 958 968 10 lt 10

Ibenzene

4-Chlorotoluene

966

978

970

984

04

06

lt 10

lt 10

tert-Butylbenzene 908 1912 04 lt 10

124-Trimethylbenzene 954 1970 17 lt 10

sec-Butyl benzene 940 946 06 lt 10

13-Dichlorobenzene 104 105 10 lt 10

bull p-Isopropyltoluene 988 102 32 lt 10

1 A-Dichlorobenzene 102 1102 08 lt 10

n-Butylbenzene 103 107 32 lt 10


12-Dibromo-3-chloropropane 988 105 59 lt 20

135-Trichlorobenzene 934 986 54 lt 10


Hexachlorobutadiene 974 962 12 lt 10

Naphthalene 872 916 49 lt 30


Page 2

Ta le4

QC Results 14-Doxane- November

TAl~LE 4 QC ~eport

Lab associated with qc samples W2466 through W24 74

Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308

Compound Rec Rec RPD Rec ugL

1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA

Chain of Custody Sheets for Samples

l

Environmental Chemistry CHAIN OF CUSTODY NQ 013774 18cS Consulting Services Inc Page I of JC(~ w~IIJ -shyC

Project Number

2525 Advance Road Madison WI 53718

Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --

Turn Around (circle one) Normal Rush

Report Due r Invoice To

Project Name JLutLl4tN euro(E~71-tt t Company flfJf1l1iJ -- SL~ [l~ Company

Project Location C jI-Yf TIk- ~ (lVJ Address Address

Sampled By (Print)

d~ ~ PO No Quote No -

Collection Total Analysis Laboratory

Sample Description Date Time Matrix Bottles Preserv Requested Comments Number

CSLJ-W4- 9- (JO JlAz~ (Jli w I 11- lLVJqy~ oJ Yl(I)~ Wltft

C~w - WA-1- 03) t tYlzo I f A f w )Jlt 1-

CSw - wA I - 030 6130 rr It(~ I WlP

C5W- MJI 2 - O]U ofil ~ t1 1 ~ w-ztf A

CSW- f3 - 010 U615 if 1 W2-t1-o

W )- () ~tS OtfOS- t It

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CSW --rf - amp110 0155 t- It Lv l ttt]

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Preservation Code ZiShedBY DateTime idBY ~ DatelTreIt 4 fllltltY

A=None B=HCL C=H2S04 1 dy-Kj a~_~ 11amp foO 7 7-- loot)

D=HN03 E=EnCore F=Methanol IRelinquished By DatelTime

~ yceived B DatelTime

G=NaOH O=Other(lndicate) j

Custody Seal PresentfAbsent IntactfNot Intact Seal 5 Receipt Temp

Temp Blank Y N (n~Shipped Via

WHITE - REPORT COpy YELLOW - LABORATORY COPY PINK - SAMPLERSUBMITTER

App ndixB

FEDEX shipping label for Co umbia Analytical Services Inc

FadhQ USA AirbUl Tracking 837784146392NumboExpress

I From IIe8se

Senders FedEx Date Account Number 22(2- 9 Senders Name -]de fLk~(pound Phone (bOf I gys-~f7

ZIP

Your Internal Billing Reference Rrst24 characters will oppeoron IIMfica

To

~~enrs S t LE Phone f O I

~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71

Address To HOlDM at Fedamp-kleetion Print IiIdEx address We cannot deUvartc POmn or pbzIP codes

Address

LiEL-SO State Uti ZIP

By usingllis Airbim you agree ID lheselVice cond_ on the back ofllli Airoill and io our current Service Guida fnciudiog terms lhet limitouriabiitv

Questions Visit our Web site at fedexcom or call1BOOGoFedElltreg 8004633339

40 Express Package Service PIICmges up to 750 Ibs Deliv81Y commitmenrmav bGlal1itm soma araas

~ FedEllt Priority Overnight FadEllt Standard Overnight 0 FadEllt First OvemightrFiXJbusimmmoming Nmbu1mass afternoon Earnestnext businass morning

deWatyw 58lact locations

FedEx 20ay 0 FadEllt Express Saver Second busfllijss dill Thild business dey

-- Fedamp Envalopol8ta Ilotaveilatne Minimum charga One-ppund nrte _---l

4b Express Freight Service Delivery com~~~trTso~

FadEx 20ay Freight o f~~~reight$ecwd buslneslJ day

Call fLllConfinnatfon

DoclBrad valus limitS5005 Packaging FedEx Envelope o FadExPak ~Olher

Includes FedExSmnIf PakFadamp Large Pak and rooEx Sturdy Pak

6 Special Handling r--~-- kirtude fedlx address in Sbonon3 -~ SAlURDAYIleIivery

O HOLD Weekday HOLD Saturdav Available ONLY 0 at FedEx Location at FadEllt LocationFadamp Prlolity Ovamiaht and FadEl 2Oayro select ZIP codas NOT 1IlIllilbla 1m Abullbullilabl ONiY fu

FadEx Rrsc Ovamillht Fedamp Priority Overnlghtand Dothis shlpme ccnmin a_ 110007 20ey I

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Mo rann 0 i~pa(Da_ ~y~9~UNl845___ ___ kg~ ShlppatsOaclaration notrequlrad DangarousGoodsioofuding Dry Ice) car-nottle shipped in FadElt packajiinsect o Cargo Aircraft Only

7 Payment BilltD lt _ ryen~ r- ~lltar~dExAectNGMCroditGltmf~obpi6W

~~g~Sc1ion o Recipient DThirdParty 0 Credit Card oCashCheck lwillDQbillad

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To1IIlPackages Total Weight Total Declared Valuet

$ 00 FadEllt Use OnlytOur liability is limited to$iOO tmess GU declare a higherwlue See back fur details

8

By sigrnng you autharUl us 10 dalivertNs shipment without obtainIng esignature and agree to indemnify and hold us hermlessfrmn any rastrlting claims

1114)a1a 10UlPartll157612copy1Q94-2OJ1 FedhPflINTEO IN USA WCSl12

App ndix C

Chain of Custody Sheets for samples s nt to Columbia Analytical Services Inc

Columbia Analytical Servicesme CHAIN OF CUSTODY

REPORT REQUIREMENTS

I Routine Report Method

Blank Surrogate as required

INVOICE INFORMATION

PO ---C777777--r--T7h--

BilITa --______ As Sb Ba Be B Ca Cd Co Cr Cu Fe Pb Mg Mn Mo Ni K Ag Na Se Sr TI Sn V Zn Hg

Ba Be B Ca Cd Co Cr Cu Fe Pb Mg Mn Mo Ni K Ag Na Se Sr TI Sn V Zn Hg

II Report Dup MS MSD as required

III Data Validation Report (includes all raw data)

TURNAROUND REQUIREMENTS ISPECIAL INSTRUCT10NSCOMM~NTS 24 hr __48 hr L (j I ~ f f

__5 Day

-=tStandard (10-15 working days) I lr r

_IV CLP Deliverable Report

V EDD

JIELINQUIJilED BY

_ ~ - ~Ij~i~~ gt gtshy gt d_M~ DatelTlme

( shy

Firm

Provide FAX Results

Requested Report Date

RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()

RELINQUISHED BY RECEIVED BY

Signature oate7Time Signature DateTrime

Printed~ame Firm Printed Name Firm Rr1Irlt1 OltI()R

Technical Memorandum

Kuhlman Electric Corporation (KEC)

Crystal sprilgs Mississippi




December 11 2008




Introdnction


Narrative

Waters i








10 10 10 10 10 10 10 1 10 20 110 10 Ip










I




Water Samples i









VOLATILES ~


ugL

W2466 CSW WAS 030 -

12-Nov-08 815

12-Nov-08

W2467 CSW WA3 030 -

12-Nov-08 820

12-Nov-08

W2468 CSW WA1 030 -

12-Nov-08 830

12-Nov-08

-

W2469 CSW WA2 030 -

12-Nov-08 841

12-Nov-08

W2470 CSW

FB 030 -

12-Nov-08 845

12-Nov-08

~ ~~

W2471 CSW WA5 025 -

12-Nov-08 905

12-Nov-08

-- - ~

W2472 CSW WA6 025 -

12-Nov-08 925

12-Nov-08

W2473 CSW TP 030 -

12-Nov-08 935

12-Nov-08

~

W2474 CSW

Duplicate

12-Nov-08 -

12-Nov-08

-~- -


) 1__ ~~~ ~ F~ ~ ~ ~

v ~ n

~ ~9-- ~ n ~

lt ~e ~ n ~

~ n ~

~ n v 4-9-shy 4-C


Page 1


W2466 W2467 W2468 W2469 W2470 W2471 W2472 W2473 W2474



030 030 030 030 030 025 025 030



Reporting Limit



10 -lt 10- lt 10 lt 1~ ~O-- lt 10

V


Page 2

Table 2



VOLATILES

1 4-Dioxane


ugL

10 lt

W2466

CSW

WAS

030

-12-Nov-08

815

13-Nov-08

10 lt

W2467

CSW

WA3

030

-12-Nov-08

820

13-Nov-08

10 lt

W2468

CSW

WA1

030

-12-Nov-08

830

13-Nov-08

10 lt

W2469

CSW

WA2

030

-12-Nov-08

841

13-Nov-08

10 lt

W2470

CSW

FB 030

-12-Nov-08

845

13-Nov-08

10 lt

W2471

CSW

WA5

025

-

12-Nov-08

905

13-Nov-08

10 lt

W2472

CSW

WA6

025

-12-Nov-08

925

13-Nov-08

-

10 lt

W2473

CSW

TP 030

-12-Nov-08

935

13-Nov-08

10 lt

W2474 I

CSW

Duplicate

12-Nov-08

-13-Nov-08

10


Page 1

Tarle 3


TAJLE 3 QC Report


Matrix

Matrix Spike


W2466 W2466

Date Analyzed 111208 ~ 1112108 111208

Compound


Chloromethane

Vinyl chloride

Bromomethane

Chloroethane


11-Dichloroethene

Methylene chloride


11-Dichloroethane


22-Dichloropropane

Bromochloromethane

Chloroform

111-Trichloroethane

1 1-Dichloropropene


Benzene

12-Dichloroethane

T richloroethene

12-Dichloropropane

Dibromomethane



Toluene


112-Trichtoroethane

T etrachloroethene

13-Dichloropropane


12-Dibromoethane

Chlorobenzene


Ethyl benzene

Xylenes Total

Styrene

Bromoform

Rec Rec RPD uglL

898 i 884 16 lt 10

924 878 51 lt 10

950 942 08 lt 10

956 110~4 lt 10

103 94 1 lt 10

101 970 40 lt 10

952 101 57 lt 10

978 974 04 lt 10

100 104 33

Bit106 103 25

990 1990 00

978 1978 00 lt 10

102 103 08 lt 10

100 1990 14 lt 10

104 101 29 lt 10

956 972 17 lt 10

102 1 100 22 lt 10

102 102 02 lt 10

974 994 20 lt 10

976 976 00 lt 10

960 102 57 lt 10

980 984 04 lt 10

896 906 11 lt 10

886 1890 05 lt 20

960 976 17 lt 10

866 1896 34 lt 10

988 982 06 lt 10

958

~ lt 10

930 92 04

Bit884 872

912 908 04

101 100 08 lt 10

105 105 04 lt 10

988 994 06 lt 10

988 100 14 H2

O 984 996 12 10

962 972 10 lt 20

Pa~e 1

TAaLE 3 QC Report


I Matrix

Matrix SpikeI


W2466 W2466

Date Analyzed 111208 1111208 11112108








Ibenzene

4-Chlorotoluene

966

978

970

984

04

06

lt 10

lt 10















Page 2

Ta le4


TAl~LE 4 QC ~eport


Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308


1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()







December 11 2008




Introdnction


Narrative

Waters i








10 10 10 10 10 10 10 1 10 20 110 10 Ip










I




Water Samples i









VOLATILES ~


ugL

W2466 CSW WAS 030 -

12-Nov-08 815

12-Nov-08

W2467 CSW WA3 030 -

12-Nov-08 820

12-Nov-08

W2468 CSW WA1 030 -

12-Nov-08 830

12-Nov-08

-

W2469 CSW WA2 030 -

12-Nov-08 841

12-Nov-08

W2470 CSW

FB 030 -

12-Nov-08 845

12-Nov-08

~ ~~

W2471 CSW WA5 025 -

12-Nov-08 905

12-Nov-08

-- - ~

W2472 CSW WA6 025 -

12-Nov-08 925

12-Nov-08

W2473 CSW TP 030 -

12-Nov-08 935

12-Nov-08

~

W2474 CSW

Duplicate

12-Nov-08 -

12-Nov-08

-~- -


) 1__ ~~~ ~ F~ ~ ~ ~

v ~ n

~ ~9-- ~ n ~

lt ~e ~ n ~

~ n ~

~ n v 4-9-shy 4-C


Page 1


W2466 W2467 W2468 W2469 W2470 W2471 W2472 W2473 W2474



030 030 030 030 030 025 025 030



Reporting Limit



10 -lt 10- lt 10 lt 1~ ~O-- lt 10

V


Page 2

Table 2



VOLATILES

1 4-Dioxane


ugL

10 lt

W2466

CSW

WAS

030

-12-Nov-08

815

13-Nov-08

10 lt

W2467

CSW

WA3

030

-12-Nov-08

820

13-Nov-08

10 lt

W2468

CSW

WA1

030

-12-Nov-08

830

13-Nov-08

10 lt

W2469

CSW

WA2

030

-12-Nov-08

841

13-Nov-08

10 lt

W2470

CSW

FB 030

-12-Nov-08

845

13-Nov-08

10 lt

W2471

CSW

WA5

025

-

12-Nov-08

905

13-Nov-08

10 lt

W2472

CSW

WA6

025

-12-Nov-08

925

13-Nov-08

-

10 lt

W2473

CSW

TP 030

-12-Nov-08

935

13-Nov-08

10 lt

W2474 I

CSW

Duplicate

12-Nov-08

-13-Nov-08

10


Page 1

Tarle 3


TAJLE 3 QC Report


Matrix

Matrix Spike


W2466 W2466

Date Analyzed 111208 ~ 1112108 111208

Compound


Chloromethane

Vinyl chloride

Bromomethane

Chloroethane


11-Dichloroethene

Methylene chloride


11-Dichloroethane


22-Dichloropropane

Bromochloromethane

Chloroform

111-Trichloroethane

1 1-Dichloropropene


Benzene

12-Dichloroethane

T richloroethene

12-Dichloropropane

Dibromomethane



Toluene


112-Trichtoroethane

T etrachloroethene

13-Dichloropropane


12-Dibromoethane

Chlorobenzene


Ethyl benzene

Xylenes Total

Styrene

Bromoform

Rec Rec RPD uglL

898 i 884 16 lt 10

924 878 51 lt 10

950 942 08 lt 10

956 110~4 lt 10

103 94 1 lt 10

101 970 40 lt 10

952 101 57 lt 10

978 974 04 lt 10

100 104 33

Bit106 103 25

990 1990 00

978 1978 00 lt 10

102 103 08 lt 10

100 1990 14 lt 10

104 101 29 lt 10

956 972 17 lt 10

102 1 100 22 lt 10

102 102 02 lt 10

974 994 20 lt 10

976 976 00 lt 10

960 102 57 lt 10

980 984 04 lt 10

896 906 11 lt 10

886 1890 05 lt 20

960 976 17 lt 10

866 1896 34 lt 10

988 982 06 lt 10

958

~ lt 10

930 92 04

Bit884 872

912 908 04

101 100 08 lt 10

105 105 04 lt 10

988 994 06 lt 10

988 100 14 H2

O 984 996 12 10

962 972 10 lt 20

Pa~e 1

TAaLE 3 QC Report


I Matrix

Matrix SpikeI


W2466 W2466

Date Analyzed 111208 1111208 11112108








Ibenzene

4-Chlorotoluene

966

978

970

984

04

06

lt 10

lt 10















Page 2

Ta le4


TAl~LE 4 QC ~eport


Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308


1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()






10 10 10 10 10 10 10 1 10 20 110 10 Ip










I




Water Samples i









VOLATILES ~


ugL

W2466 CSW WAS 030 -

12-Nov-08 815

12-Nov-08

W2467 CSW WA3 030 -

12-Nov-08 820

12-Nov-08

W2468 CSW WA1 030 -

12-Nov-08 830

12-Nov-08

-

W2469 CSW WA2 030 -

12-Nov-08 841

12-Nov-08

W2470 CSW

FB 030 -

12-Nov-08 845

12-Nov-08

~ ~~

W2471 CSW WA5 025 -

12-Nov-08 905

12-Nov-08

-- - ~

W2472 CSW WA6 025 -

12-Nov-08 925

12-Nov-08

W2473 CSW TP 030 -

12-Nov-08 935

12-Nov-08

~

W2474 CSW

Duplicate

12-Nov-08 -

12-Nov-08

-~- -


) 1__ ~~~ ~ F~ ~ ~ ~

v ~ n

~ ~9-- ~ n ~

lt ~e ~ n ~

~ n ~

~ n v 4-9-shy 4-C


Page 1


W2466 W2467 W2468 W2469 W2470 W2471 W2472 W2473 W2474



030 030 030 030 030 025 025 030



Reporting Limit



10 -lt 10- lt 10 lt 1~ ~O-- lt 10

V


Page 2

Table 2



VOLATILES

1 4-Dioxane


ugL

10 lt

W2466

CSW

WAS

030

-12-Nov-08

815

13-Nov-08

10 lt

W2467

CSW

WA3

030

-12-Nov-08

820

13-Nov-08

10 lt

W2468

CSW

WA1

030

-12-Nov-08

830

13-Nov-08

10 lt

W2469

CSW

WA2

030

-12-Nov-08

841

13-Nov-08

10 lt

W2470

CSW

FB 030

-12-Nov-08

845

13-Nov-08

10 lt

W2471

CSW

WA5

025

-

12-Nov-08

905

13-Nov-08

10 lt

W2472

CSW

WA6

025

-12-Nov-08

925

13-Nov-08

-

10 lt

W2473

CSW

TP 030

-12-Nov-08

935

13-Nov-08

10 lt

W2474 I

CSW

Duplicate

12-Nov-08

-13-Nov-08

10


Page 1

Tarle 3


TAJLE 3 QC Report


Matrix

Matrix Spike


W2466 W2466

Date Analyzed 111208 ~ 1112108 111208

Compound


Chloromethane

Vinyl chloride

Bromomethane

Chloroethane


11-Dichloroethene

Methylene chloride


11-Dichloroethane


22-Dichloropropane

Bromochloromethane

Chloroform

111-Trichloroethane

1 1-Dichloropropene


Benzene

12-Dichloroethane

T richloroethene

12-Dichloropropane

Dibromomethane



Toluene


112-Trichtoroethane

T etrachloroethene

13-Dichloropropane


12-Dibromoethane

Chlorobenzene


Ethyl benzene

Xylenes Total

Styrene

Bromoform

Rec Rec RPD uglL

898 i 884 16 lt 10

924 878 51 lt 10

950 942 08 lt 10

956 110~4 lt 10

103 94 1 lt 10

101 970 40 lt 10

952 101 57 lt 10

978 974 04 lt 10

100 104 33

Bit106 103 25

990 1990 00

978 1978 00 lt 10

102 103 08 lt 10

100 1990 14 lt 10

104 101 29 lt 10

956 972 17 lt 10

102 1 100 22 lt 10

102 102 02 lt 10

974 994 20 lt 10

976 976 00 lt 10

960 102 57 lt 10

980 984 04 lt 10

896 906 11 lt 10

886 1890 05 lt 20

960 976 17 lt 10

866 1896 34 lt 10

988 982 06 lt 10

958

~ lt 10

930 92 04

Bit884 872

912 908 04

101 100 08 lt 10

105 105 04 lt 10

988 994 06 lt 10

988 100 14 H2

O 984 996 12 10

962 972 10 lt 20

Pa~e 1

TAaLE 3 QC Report


I Matrix

Matrix SpikeI


W2466 W2466

Date Analyzed 111208 1111208 11112108








Ibenzene

4-Chlorotoluene

966

978

970

984

04

06

lt 10

lt 10















Page 2

Ta le4


TAl~LE 4 QC ~eport


Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308


1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()













I




Water Samples i









VOLATILES ~


ugL

W2466 CSW WAS 030 -

12-Nov-08 815

12-Nov-08

W2467 CSW WA3 030 -

12-Nov-08 820

12-Nov-08

W2468 CSW WA1 030 -

12-Nov-08 830

12-Nov-08

-

W2469 CSW WA2 030 -

12-Nov-08 841

12-Nov-08

W2470 CSW

FB 030 -

12-Nov-08 845

12-Nov-08

~ ~~

W2471 CSW WA5 025 -

12-Nov-08 905

12-Nov-08

-- - ~

W2472 CSW WA6 025 -

12-Nov-08 925

12-Nov-08

W2473 CSW TP 030 -

12-Nov-08 935

12-Nov-08

~

W2474 CSW

Duplicate

12-Nov-08 -

12-Nov-08

-~- -


) 1__ ~~~ ~ F~ ~ ~ ~

v ~ n

~ ~9-- ~ n ~

lt ~e ~ n ~

~ n ~

~ n v 4-9-shy 4-C


Page 1


W2466 W2467 W2468 W2469 W2470 W2471 W2472 W2473 W2474



030 030 030 030 030 025 025 030



Reporting Limit



10 -lt 10- lt 10 lt 1~ ~O-- lt 10

V


Page 2

Table 2



VOLATILES

1 4-Dioxane


ugL

10 lt

W2466

CSW

WAS

030

-12-Nov-08

815

13-Nov-08

10 lt

W2467

CSW

WA3

030

-12-Nov-08

820

13-Nov-08

10 lt

W2468

CSW

WA1

030

-12-Nov-08

830

13-Nov-08

10 lt

W2469

CSW

WA2

030

-12-Nov-08

841

13-Nov-08

10 lt

W2470

CSW

FB 030

-12-Nov-08

845

13-Nov-08

10 lt

W2471

CSW

WA5

025

-

12-Nov-08

905

13-Nov-08

10 lt

W2472

CSW

WA6

025

-12-Nov-08

925

13-Nov-08

-

10 lt

W2473

CSW

TP 030

-12-Nov-08

935

13-Nov-08

10 lt

W2474 I

CSW

Duplicate

12-Nov-08

-13-Nov-08

10


Page 1

Tarle 3


TAJLE 3 QC Report


Matrix

Matrix Spike


W2466 W2466

Date Analyzed 111208 ~ 1112108 111208

Compound


Chloromethane

Vinyl chloride

Bromomethane

Chloroethane


11-Dichloroethene

Methylene chloride


11-Dichloroethane


22-Dichloropropane

Bromochloromethane

Chloroform

111-Trichloroethane

1 1-Dichloropropene


Benzene

12-Dichloroethane

T richloroethene

12-Dichloropropane

Dibromomethane



Toluene


112-Trichtoroethane

T etrachloroethene

13-Dichloropropane


12-Dibromoethane

Chlorobenzene


Ethyl benzene

Xylenes Total

Styrene

Bromoform

Rec Rec RPD uglL

898 i 884 16 lt 10

924 878 51 lt 10

950 942 08 lt 10

956 110~4 lt 10

103 94 1 lt 10

101 970 40 lt 10

952 101 57 lt 10

978 974 04 lt 10

100 104 33

Bit106 103 25

990 1990 00

978 1978 00 lt 10

102 103 08 lt 10

100 1990 14 lt 10

104 101 29 lt 10

956 972 17 lt 10

102 1 100 22 lt 10

102 102 02 lt 10

974 994 20 lt 10

976 976 00 lt 10

960 102 57 lt 10

980 984 04 lt 10

896 906 11 lt 10

886 1890 05 lt 20

960 976 17 lt 10

866 1896 34 lt 10

988 982 06 lt 10

958

~ lt 10

930 92 04

Bit884 872

912 908 04

101 100 08 lt 10

105 105 04 lt 10

988 994 06 lt 10

988 100 14 H2

O 984 996 12 10

962 972 10 lt 20

Pa~e 1

TAaLE 3 QC Report


I Matrix

Matrix SpikeI


W2466 W2466

Date Analyzed 111208 1111208 11112108








Ibenzene

4-Chlorotoluene

966

978

970

984

04

06

lt 10

lt 10















Page 2

Ta le4


TAl~LE 4 QC ~eport


Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308


1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()





Water Samples i









VOLATILES ~


ugL

W2466 CSW WAS 030 -

12-Nov-08 815

12-Nov-08

W2467 CSW WA3 030 -

12-Nov-08 820

12-Nov-08

W2468 CSW WA1 030 -

12-Nov-08 830

12-Nov-08

-

W2469 CSW WA2 030 -

12-Nov-08 841

12-Nov-08

W2470 CSW

FB 030 -

12-Nov-08 845

12-Nov-08

~ ~~

W2471 CSW WA5 025 -

12-Nov-08 905

12-Nov-08

-- - ~

W2472 CSW WA6 025 -

12-Nov-08 925

12-Nov-08

W2473 CSW TP 030 -

12-Nov-08 935

12-Nov-08

~

W2474 CSW

Duplicate

12-Nov-08 -

12-Nov-08

-~- -


) 1__ ~~~ ~ F~ ~ ~ ~

v ~ n

~ ~9-- ~ n ~

lt ~e ~ n ~

~ n ~

~ n v 4-9-shy 4-C


Page 1


W2466 W2467 W2468 W2469 W2470 W2471 W2472 W2473 W2474



030 030 030 030 030 025 025 030



Reporting Limit



10 -lt 10- lt 10 lt 1~ ~O-- lt 10

V


Page 2

Table 2



VOLATILES

1 4-Dioxane


ugL

10 lt

W2466

CSW

WAS

030

-12-Nov-08

815

13-Nov-08

10 lt

W2467

CSW

WA3

030

-12-Nov-08

820

13-Nov-08

10 lt

W2468

CSW

WA1

030

-12-Nov-08

830

13-Nov-08

10 lt

W2469

CSW

WA2

030

-12-Nov-08

841

13-Nov-08

10 lt

W2470

CSW

FB 030

-12-Nov-08

845

13-Nov-08

10 lt

W2471

CSW

WA5

025

-

12-Nov-08

905

13-Nov-08

10 lt

W2472

CSW

WA6

025

-12-Nov-08

925

13-Nov-08

-

10 lt

W2473

CSW

TP 030

-12-Nov-08

935

13-Nov-08

10 lt

W2474 I

CSW

Duplicate

12-Nov-08

-13-Nov-08

10


Page 1

Tarle 3


TAJLE 3 QC Report


Matrix

Matrix Spike


W2466 W2466

Date Analyzed 111208 ~ 1112108 111208

Compound


Chloromethane

Vinyl chloride

Bromomethane

Chloroethane


11-Dichloroethene

Methylene chloride


11-Dichloroethane


22-Dichloropropane

Bromochloromethane

Chloroform

111-Trichloroethane

1 1-Dichloropropene


Benzene

12-Dichloroethane

T richloroethene

12-Dichloropropane

Dibromomethane



Toluene


112-Trichtoroethane

T etrachloroethene

13-Dichloropropane


12-Dibromoethane

Chlorobenzene


Ethyl benzene

Xylenes Total

Styrene

Bromoform

Rec Rec RPD uglL

898 i 884 16 lt 10

924 878 51 lt 10

950 942 08 lt 10

956 110~4 lt 10

103 94 1 lt 10

101 970 40 lt 10

952 101 57 lt 10

978 974 04 lt 10

100 104 33

Bit106 103 25

990 1990 00

978 1978 00 lt 10

102 103 08 lt 10

100 1990 14 lt 10

104 101 29 lt 10

956 972 17 lt 10

102 1 100 22 lt 10

102 102 02 lt 10

974 994 20 lt 10

976 976 00 lt 10

960 102 57 lt 10

980 984 04 lt 10

896 906 11 lt 10

886 1890 05 lt 20

960 976 17 lt 10

866 1896 34 lt 10

988 982 06 lt 10

958

~ lt 10

930 92 04

Bit884 872

912 908 04

101 100 08 lt 10

105 105 04 lt 10

988 994 06 lt 10

988 100 14 H2

O 984 996 12 10

962 972 10 lt 20

Pa~e 1

TAaLE 3 QC Report


I Matrix

Matrix SpikeI


W2466 W2466

Date Analyzed 111208 1111208 11112108








Ibenzene

4-Chlorotoluene

966

978

970

984

04

06

lt 10

lt 10















Page 2

Ta le4


TAl~LE 4 QC ~eport


Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308


1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()






VOLATILES ~


ugL

W2466 CSW WAS 030 -

12-Nov-08 815

12-Nov-08

W2467 CSW WA3 030 -

12-Nov-08 820

12-Nov-08

W2468 CSW WA1 030 -

12-Nov-08 830

12-Nov-08

-

W2469 CSW WA2 030 -

12-Nov-08 841

12-Nov-08

W2470 CSW

FB 030 -

12-Nov-08 845

12-Nov-08

~ ~~

W2471 CSW WA5 025 -

12-Nov-08 905

12-Nov-08

-- - ~

W2472 CSW WA6 025 -

12-Nov-08 925

12-Nov-08

W2473 CSW TP 030 -

12-Nov-08 935

12-Nov-08

~

W2474 CSW

Duplicate

12-Nov-08 -

12-Nov-08

-~- -


) 1__ ~~~ ~ F~ ~ ~ ~

v ~ n

~ ~9-- ~ n ~

lt ~e ~ n ~

~ n ~

~ n v 4-9-shy 4-C


Page 1


W2466 W2467 W2468 W2469 W2470 W2471 W2472 W2473 W2474



030 030 030 030 030 025 025 030



Reporting Limit



10 -lt 10- lt 10 lt 1~ ~O-- lt 10

V


Page 2

Table 2



VOLATILES

1 4-Dioxane


ugL

10 lt

W2466

CSW

WAS

030

-12-Nov-08

815

13-Nov-08

10 lt

W2467

CSW

WA3

030

-12-Nov-08

820

13-Nov-08

10 lt

W2468

CSW

WA1

030

-12-Nov-08

830

13-Nov-08

10 lt

W2469

CSW

WA2

030

-12-Nov-08

841

13-Nov-08

10 lt

W2470

CSW

FB 030

-12-Nov-08

845

13-Nov-08

10 lt

W2471

CSW

WA5

025

-

12-Nov-08

905

13-Nov-08

10 lt

W2472

CSW

WA6

025

-12-Nov-08

925

13-Nov-08

-

10 lt

W2473

CSW

TP 030

-12-Nov-08

935

13-Nov-08

10 lt

W2474 I

CSW

Duplicate

12-Nov-08

-13-Nov-08

10


Page 1

Tarle 3


TAJLE 3 QC Report


Matrix

Matrix Spike


W2466 W2466

Date Analyzed 111208 ~ 1112108 111208

Compound


Chloromethane

Vinyl chloride

Bromomethane

Chloroethane


11-Dichloroethene

Methylene chloride


11-Dichloroethane


22-Dichloropropane

Bromochloromethane

Chloroform

111-Trichloroethane

1 1-Dichloropropene


Benzene

12-Dichloroethane

T richloroethene

12-Dichloropropane

Dibromomethane



Toluene


112-Trichtoroethane

T etrachloroethene

13-Dichloropropane


12-Dibromoethane

Chlorobenzene


Ethyl benzene

Xylenes Total

Styrene

Bromoform

Rec Rec RPD uglL

898 i 884 16 lt 10

924 878 51 lt 10

950 942 08 lt 10

956 110~4 lt 10

103 94 1 lt 10

101 970 40 lt 10

952 101 57 lt 10

978 974 04 lt 10

100 104 33

Bit106 103 25

990 1990 00

978 1978 00 lt 10

102 103 08 lt 10

100 1990 14 lt 10

104 101 29 lt 10

956 972 17 lt 10

102 1 100 22 lt 10

102 102 02 lt 10

974 994 20 lt 10

976 976 00 lt 10

960 102 57 lt 10

980 984 04 lt 10

896 906 11 lt 10

886 1890 05 lt 20

960 976 17 lt 10

866 1896 34 lt 10

988 982 06 lt 10

958

~ lt 10

930 92 04

Bit884 872

912 908 04

101 100 08 lt 10

105 105 04 lt 10

988 994 06 lt 10

988 100 14 H2

O 984 996 12 10

962 972 10 lt 20

Pa~e 1

TAaLE 3 QC Report


I Matrix

Matrix SpikeI


W2466 W2466

Date Analyzed 111208 1111208 11112108








Ibenzene

4-Chlorotoluene

966

978

970

984

04

06

lt 10

lt 10















Page 2

Ta le4


TAl~LE 4 QC ~eport


Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308


1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()





VOLATILES ~


ugL

W2466 CSW WAS 030 -

12-Nov-08 815

12-Nov-08

W2467 CSW WA3 030 -

12-Nov-08 820

12-Nov-08

W2468 CSW WA1 030 -

12-Nov-08 830

12-Nov-08

-

W2469 CSW WA2 030 -

12-Nov-08 841

12-Nov-08

W2470 CSW

FB 030 -

12-Nov-08 845

12-Nov-08

~ ~~

W2471 CSW WA5 025 -

12-Nov-08 905

12-Nov-08

-- - ~

W2472 CSW WA6 025 -

12-Nov-08 925

12-Nov-08

W2473 CSW TP 030 -

12-Nov-08 935

12-Nov-08

~

W2474 CSW

Duplicate

12-Nov-08 -

12-Nov-08

-~- -


) 1__ ~~~ ~ F~ ~ ~ ~

v ~ n

~ ~9-- ~ n ~

lt ~e ~ n ~

~ n ~

~ n v 4-9-shy 4-C


Page 1


W2466 W2467 W2468 W2469 W2470 W2471 W2472 W2473 W2474



030 030 030 030 030 025 025 030



Reporting Limit



10 -lt 10- lt 10 lt 1~ ~O-- lt 10

V


Page 2

Table 2



VOLATILES

1 4-Dioxane


ugL

10 lt

W2466

CSW

WAS

030

-12-Nov-08

815

13-Nov-08

10 lt

W2467

CSW

WA3

030

-12-Nov-08

820

13-Nov-08

10 lt

W2468

CSW

WA1

030

-12-Nov-08

830

13-Nov-08

10 lt

W2469

CSW

WA2

030

-12-Nov-08

841

13-Nov-08

10 lt

W2470

CSW

FB 030

-12-Nov-08

845

13-Nov-08

10 lt

W2471

CSW

WA5

025

-

12-Nov-08

905

13-Nov-08

10 lt

W2472

CSW

WA6

025

-12-Nov-08

925

13-Nov-08

-

10 lt

W2473

CSW

TP 030

-12-Nov-08

935

13-Nov-08

10 lt

W2474 I

CSW

Duplicate

12-Nov-08

-13-Nov-08

10


Page 1

Tarle 3


TAJLE 3 QC Report


Matrix

Matrix Spike


W2466 W2466

Date Analyzed 111208 ~ 1112108 111208

Compound


Chloromethane

Vinyl chloride

Bromomethane

Chloroethane


11-Dichloroethene

Methylene chloride


11-Dichloroethane


22-Dichloropropane

Bromochloromethane

Chloroform

111-Trichloroethane

1 1-Dichloropropene


Benzene

12-Dichloroethane

T richloroethene

12-Dichloropropane

Dibromomethane



Toluene


112-Trichtoroethane

T etrachloroethene

13-Dichloropropane


12-Dibromoethane

Chlorobenzene


Ethyl benzene

Xylenes Total

Styrene

Bromoform

Rec Rec RPD uglL

898 i 884 16 lt 10

924 878 51 lt 10

950 942 08 lt 10

956 110~4 lt 10

103 94 1 lt 10

101 970 40 lt 10

952 101 57 lt 10

978 974 04 lt 10

100 104 33

Bit106 103 25

990 1990 00

978 1978 00 lt 10

102 103 08 lt 10

100 1990 14 lt 10

104 101 29 lt 10

956 972 17 lt 10

102 1 100 22 lt 10

102 102 02 lt 10

974 994 20 lt 10

976 976 00 lt 10

960 102 57 lt 10

980 984 04 lt 10

896 906 11 lt 10

886 1890 05 lt 20

960 976 17 lt 10

866 1896 34 lt 10

988 982 06 lt 10

958

~ lt 10

930 92 04

Bit884 872

912 908 04

101 100 08 lt 10

105 105 04 lt 10

988 994 06 lt 10

988 100 14 H2

O 984 996 12 10

962 972 10 lt 20

Pa~e 1

TAaLE 3 QC Report


I Matrix

Matrix SpikeI


W2466 W2466

Date Analyzed 111208 1111208 11112108








Ibenzene

4-Chlorotoluene

966

978

970

984

04

06

lt 10

lt 10















Page 2

Ta le4


TAl~LE 4 QC ~eport


Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308


1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()





W2466 W2467 W2468 W2469 W2470 W2471 W2472 W2473 W2474



030 030 030 030 030 025 025 030



Reporting Limit



10 -lt 10- lt 10 lt 1~ ~O-- lt 10

V


Page 2

Table 2



VOLATILES

1 4-Dioxane


ugL

10 lt

W2466

CSW

WAS

030

-12-Nov-08

815

13-Nov-08

10 lt

W2467

CSW

WA3

030

-12-Nov-08

820

13-Nov-08

10 lt

W2468

CSW

WA1

030

-12-Nov-08

830

13-Nov-08

10 lt

W2469

CSW

WA2

030

-12-Nov-08

841

13-Nov-08

10 lt

W2470

CSW

FB 030

-12-Nov-08

845

13-Nov-08

10 lt

W2471

CSW

WA5

025

-

12-Nov-08

905

13-Nov-08

10 lt

W2472

CSW

WA6

025

-12-Nov-08

925

13-Nov-08

-

10 lt

W2473

CSW

TP 030

-12-Nov-08

935

13-Nov-08

10 lt

W2474 I

CSW

Duplicate

12-Nov-08

-13-Nov-08

10


Page 1

Tarle 3


TAJLE 3 QC Report


Matrix

Matrix Spike


W2466 W2466

Date Analyzed 111208 ~ 1112108 111208

Compound


Chloromethane

Vinyl chloride

Bromomethane

Chloroethane


11-Dichloroethene

Methylene chloride


11-Dichloroethane


22-Dichloropropane

Bromochloromethane

Chloroform

111-Trichloroethane

1 1-Dichloropropene


Benzene

12-Dichloroethane

T richloroethene

12-Dichloropropane

Dibromomethane



Toluene


112-Trichtoroethane

T etrachloroethene

13-Dichloropropane


12-Dibromoethane

Chlorobenzene


Ethyl benzene

Xylenes Total

Styrene

Bromoform

Rec Rec RPD uglL

898 i 884 16 lt 10

924 878 51 lt 10

950 942 08 lt 10

956 110~4 lt 10

103 94 1 lt 10

101 970 40 lt 10

952 101 57 lt 10

978 974 04 lt 10

100 104 33

Bit106 103 25

990 1990 00

978 1978 00 lt 10

102 103 08 lt 10

100 1990 14 lt 10

104 101 29 lt 10

956 972 17 lt 10

102 1 100 22 lt 10

102 102 02 lt 10

974 994 20 lt 10

976 976 00 lt 10

960 102 57 lt 10

980 984 04 lt 10

896 906 11 lt 10

886 1890 05 lt 20

960 976 17 lt 10

866 1896 34 lt 10

988 982 06 lt 10

958

~ lt 10

930 92 04

Bit884 872

912 908 04

101 100 08 lt 10

105 105 04 lt 10

988 994 06 lt 10

988 100 14 H2

O 984 996 12 10

962 972 10 lt 20

Pa~e 1

TAaLE 3 QC Report


I Matrix

Matrix SpikeI


W2466 W2466

Date Analyzed 111208 1111208 11112108








Ibenzene

4-Chlorotoluene

966

978

970

984

04

06

lt 10

lt 10















Page 2

Ta le4


TAl~LE 4 QC ~eport


Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308


1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()




Table 2



VOLATILES

1 4-Dioxane


ugL

10 lt

W2466

CSW

WAS

030

-12-Nov-08

815

13-Nov-08

10 lt

W2467

CSW

WA3

030

-12-Nov-08

820

13-Nov-08

10 lt

W2468

CSW

WA1

030

-12-Nov-08

830

13-Nov-08

10 lt

W2469

CSW

WA2

030

-12-Nov-08

841

13-Nov-08

10 lt

W2470

CSW

FB 030

-12-Nov-08

845

13-Nov-08

10 lt

W2471

CSW

WA5

025

-

12-Nov-08

905

13-Nov-08

10 lt

W2472

CSW

WA6

025

-12-Nov-08

925

13-Nov-08

-

10 lt

W2473

CSW

TP 030

-12-Nov-08

935

13-Nov-08

10 lt

W2474 I

CSW

Duplicate

12-Nov-08

-13-Nov-08

10


Page 1

Tarle 3


TAJLE 3 QC Report


Matrix

Matrix Spike


W2466 W2466

Date Analyzed 111208 ~ 1112108 111208

Compound


Chloromethane

Vinyl chloride

Bromomethane

Chloroethane


11-Dichloroethene

Methylene chloride


11-Dichloroethane


22-Dichloropropane

Bromochloromethane

Chloroform

111-Trichloroethane

1 1-Dichloropropene


Benzene

12-Dichloroethane

T richloroethene

12-Dichloropropane

Dibromomethane



Toluene


112-Trichtoroethane

T etrachloroethene

13-Dichloropropane


12-Dibromoethane

Chlorobenzene


Ethyl benzene

Xylenes Total

Styrene

Bromoform

Rec Rec RPD uglL

898 i 884 16 lt 10

924 878 51 lt 10

950 942 08 lt 10

956 110~4 lt 10

103 94 1 lt 10

101 970 40 lt 10

952 101 57 lt 10

978 974 04 lt 10

100 104 33

Bit106 103 25

990 1990 00

978 1978 00 lt 10

102 103 08 lt 10

100 1990 14 lt 10

104 101 29 lt 10

956 972 17 lt 10

102 1 100 22 lt 10

102 102 02 lt 10

974 994 20 lt 10

976 976 00 lt 10

960 102 57 lt 10

980 984 04 lt 10

896 906 11 lt 10

886 1890 05 lt 20

960 976 17 lt 10

866 1896 34 lt 10

988 982 06 lt 10

958

~ lt 10

930 92 04

Bit884 872

912 908 04

101 100 08 lt 10

105 105 04 lt 10

988 994 06 lt 10

988 100 14 H2

O 984 996 12 10

962 972 10 lt 20

Pa~e 1

TAaLE 3 QC Report


I Matrix

Matrix SpikeI


W2466 W2466

Date Analyzed 111208 1111208 11112108








Ibenzene

4-Chlorotoluene

966

978

970

984

04

06

lt 10

lt 10















Page 2

Ta le4


TAl~LE 4 QC ~eport


Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308


1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()





VOLATILES

1 4-Dioxane


ugL

10 lt

W2466

CSW

WAS

030

-12-Nov-08

815

13-Nov-08

10 lt

W2467

CSW

WA3

030

-12-Nov-08

820

13-Nov-08

10 lt

W2468

CSW

WA1

030

-12-Nov-08

830

13-Nov-08

10 lt

W2469

CSW

WA2

030

-12-Nov-08

841

13-Nov-08

10 lt

W2470

CSW

FB 030

-12-Nov-08

845

13-Nov-08

10 lt

W2471

CSW

WA5

025

-

12-Nov-08

905

13-Nov-08

10 lt

W2472

CSW

WA6

025

-12-Nov-08

925

13-Nov-08

-

10 lt

W2473

CSW

TP 030

-12-Nov-08

935

13-Nov-08

10 lt

W2474 I

CSW

Duplicate

12-Nov-08

-13-Nov-08

10


Page 1

Tarle 3


TAJLE 3 QC Report


Matrix

Matrix Spike


W2466 W2466

Date Analyzed 111208 ~ 1112108 111208

Compound


Chloromethane

Vinyl chloride

Bromomethane

Chloroethane


11-Dichloroethene

Methylene chloride


11-Dichloroethane


22-Dichloropropane

Bromochloromethane

Chloroform

111-Trichloroethane

1 1-Dichloropropene


Benzene

12-Dichloroethane

T richloroethene

12-Dichloropropane

Dibromomethane



Toluene


112-Trichtoroethane

T etrachloroethene

13-Dichloropropane


12-Dibromoethane

Chlorobenzene


Ethyl benzene

Xylenes Total

Styrene

Bromoform

Rec Rec RPD uglL

898 i 884 16 lt 10

924 878 51 lt 10

950 942 08 lt 10

956 110~4 lt 10

103 94 1 lt 10

101 970 40 lt 10

952 101 57 lt 10

978 974 04 lt 10

100 104 33

Bit106 103 25

990 1990 00

978 1978 00 lt 10

102 103 08 lt 10

100 1990 14 lt 10

104 101 29 lt 10

956 972 17 lt 10

102 1 100 22 lt 10

102 102 02 lt 10

974 994 20 lt 10

976 976 00 lt 10

960 102 57 lt 10

980 984 04 lt 10

896 906 11 lt 10

886 1890 05 lt 20

960 976 17 lt 10

866 1896 34 lt 10

988 982 06 lt 10

958

~ lt 10

930 92 04

Bit884 872

912 908 04

101 100 08 lt 10

105 105 04 lt 10

988 994 06 lt 10

988 100 14 H2

O 984 996 12 10

962 972 10 lt 20

Pa~e 1

TAaLE 3 QC Report


I Matrix

Matrix SpikeI


W2466 W2466

Date Analyzed 111208 1111208 11112108








Ibenzene

4-Chlorotoluene

966

978

970

984

04

06

lt 10

lt 10















Page 2

Ta le4


TAl~LE 4 QC ~eport


Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308


1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()




Tarle 3


TAJLE 3 QC Report


Matrix

Matrix Spike


W2466 W2466

Date Analyzed 111208 ~ 1112108 111208

Compound


Chloromethane

Vinyl chloride

Bromomethane

Chloroethane


11-Dichloroethene

Methylene chloride


11-Dichloroethane


22-Dichloropropane

Bromochloromethane

Chloroform

111-Trichloroethane

1 1-Dichloropropene


Benzene

12-Dichloroethane

T richloroethene

12-Dichloropropane

Dibromomethane



Toluene


112-Trichtoroethane

T etrachloroethene

13-Dichloropropane


12-Dibromoethane

Chlorobenzene


Ethyl benzene

Xylenes Total

Styrene

Bromoform

Rec Rec RPD uglL

898 i 884 16 lt 10

924 878 51 lt 10

950 942 08 lt 10

956 110~4 lt 10

103 94 1 lt 10

101 970 40 lt 10

952 101 57 lt 10

978 974 04 lt 10

100 104 33

Bit106 103 25

990 1990 00

978 1978 00 lt 10

102 103 08 lt 10

100 1990 14 lt 10

104 101 29 lt 10

956 972 17 lt 10

102 1 100 22 lt 10

102 102 02 lt 10

974 994 20 lt 10

976 976 00 lt 10

960 102 57 lt 10

980 984 04 lt 10

896 906 11 lt 10

886 1890 05 lt 20

960 976 17 lt 10

866 1896 34 lt 10

988 982 06 lt 10

958

~ lt 10

930 92 04

Bit884 872

912 908 04

101 100 08 lt 10

105 105 04 lt 10

988 994 06 lt 10

988 100 14 H2

O 984 996 12 10

962 972 10 lt 20

Pa~e 1

TAaLE 3 QC Report


I Matrix

Matrix SpikeI


W2466 W2466

Date Analyzed 111208 1111208 11112108








Ibenzene

4-Chlorotoluene

966

978

970

984

04

06

lt 10

lt 10















Page 2

Ta le4


TAl~LE 4 QC ~eport


Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308


1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()




TAJLE 3 QC Report


Matrix

Matrix Spike


W2466 W2466

Date Analyzed 111208 ~ 1112108 111208

Compound


Chloromethane

Vinyl chloride

Bromomethane

Chloroethane


11-Dichloroethene

Methylene chloride


11-Dichloroethane


22-Dichloropropane

Bromochloromethane

Chloroform

111-Trichloroethane

1 1-Dichloropropene


Benzene

12-Dichloroethane

T richloroethene

12-Dichloropropane

Dibromomethane



Toluene


112-Trichtoroethane

T etrachloroethene

13-Dichloropropane


12-Dibromoethane

Chlorobenzene


Ethyl benzene

Xylenes Total

Styrene

Bromoform

Rec Rec RPD uglL

898 i 884 16 lt 10

924 878 51 lt 10

950 942 08 lt 10

956 110~4 lt 10

103 94 1 lt 10

101 970 40 lt 10

952 101 57 lt 10

978 974 04 lt 10

100 104 33

Bit106 103 25

990 1990 00

978 1978 00 lt 10

102 103 08 lt 10

100 1990 14 lt 10

104 101 29 lt 10

956 972 17 lt 10

102 1 100 22 lt 10

102 102 02 lt 10

974 994 20 lt 10

976 976 00 lt 10

960 102 57 lt 10

980 984 04 lt 10

896 906 11 lt 10

886 1890 05 lt 20

960 976 17 lt 10

866 1896 34 lt 10

988 982 06 lt 10

958

~ lt 10

930 92 04

Bit884 872

912 908 04

101 100 08 lt 10

105 105 04 lt 10

988 994 06 lt 10

988 100 14 H2

O 984 996 12 10

962 972 10 lt 20

Pa~e 1

TAaLE 3 QC Report


I Matrix

Matrix SpikeI


W2466 W2466

Date Analyzed 111208 1111208 11112108








Ibenzene

4-Chlorotoluene

966

978

970

984

04

06

lt 10

lt 10















Page 2

Ta le4


TAl~LE 4 QC ~eport


Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308


1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()




TAaLE 3 QC Report


I Matrix

Matrix SpikeI


W2466 W2466

Date Analyzed 111208 1111208 11112108








Ibenzene

4-Chlorotoluene

966

978

970

984

04

06

lt 10

lt 10















Page 2

Ta le4


TAl~LE 4 QC ~eport


Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308


1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()




Ta le4


TAl~LE 4 QC ~eport


Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308


1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()




TAl~LE 4 QC ~eport


Matrix

Spike

Matrix

Spike

Duplicate LCS Blank

W2466 W2466

Date Extracted

Date Analyzed

111208

111308

111208

111308

111208

111308

111208

111308


1 A-Dioxane 947 935 13 938 lt 10

Pal~e 1

App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()




App ndixA


l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()




l


Project Number


Phone 608-221-8700 FAX 608-221-4889

Mail Report To

- --





Sampled By (Print)








CSW- f3 - 010 U615 if 1 W2-t1-o


w 7yen1C~W-




---y ~~









App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()




App ndixB



I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()





I From IIe8se


ZIP


To


~mpa~L-__~~=~L_~~~ $ _~ __ __C_~_L-________-4~_______ ____~~~~~Y_71


Address





















Ex0



8



App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()




App ndix C



REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()





REPORT REQUIREMENTS



INVOICE INFORMATION

PO ---C777777--r--T7h--






__5 Day



V EDD

JIELINQUIJilED BY


( shy

Firm

Provide FAX Results


RECEIVED BY

Signature DafeTrime

Pnnfed Name Firm

IJ ~u ) ~ - ()




Documents

osePh · 2017-06-09 · T~ese levels equate to 0.5, 1.0,20, 5.0, 10,25 and 50 /-LgiL for water samples. A Hewlett-Packard 5890 gas chromatograph ith a 30m x 0.32mm RTX-624 micro-capillary