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12.
835
7.4
43 7
.240
6.6
83
2.5
00
1.3
72
-0.0
06
9.00
0.92 1.06
3.03
0.71
14 12 10 8 6 4 2 0 PPM
DATE: Mon Feb 18 04:54:36 2019
Nuts - $pdata
DMSO, F1: 400.132 F2: 1.000 SW1: 8224 OF1: 2469.5 PTS1d: 65536 EX: zg30 PW: 15.0 usec PD: 1.0 sec NA: 8 LB: 0.0
MedKoo Biosciences www.medkoo.com [email protected]
: 18 Feb 19 Injection Date Sample Name : 263707-16-0
Acq. Method : D:\METHODS\2-POS-15MIN.M Analysis Method : D:\METHODS\2-POS-15MIN.M Sample Info : Easy-Access Method: '2-POS-15MIN' Method Info : Mobile Phase : A:water(0.01%TFA) B:ACN(0.01%TFA)
GGradientTime 0 7.5 15B % 5 95 95Flow Rate :1ml/minColumn :SUNFIRE, 150*4.6mm,3.5umColumn Temperature:45C,MS POS150-1500
min*2 4 6 8 10 12 14
mAU
0100200300400
*DAD1 A, Sig=214,4 Ref=off
9.55
0
min*2 4 6 8 10 12 14
mAU
0
100
200
300
400
*DAD1 B, Sig=254,4 Ref=off
9.55
0
10.2
89 Integration Results for DAD1 A, Sig=214,4 Ref=off
RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 9.55 0.03 1291.57 565.24 100.00
Integration Results for DAD1 B, Sig=254,4 Ref=off
RetTim Width Area Height Area%|-------|--------|--------------|--------------|--------| 9.55 0.03 1240.37 548.15 98.16 10.29 0.04 23.23 8.91 1.84
Med
Koo
Bio
scie
nces
ww
w.m
edko
o.co
msa
les@
med
koo.
com
: 18 Feb 19 Injection Date Sample Name : 263707-16-0
Acq. Method : D:\METHODS\1-POS-3MIN.M Analysis Method : D:\METHODS\1-POS-3MIN.M Sample Info : Easy-Access Method: '1-POS-3MIN' Method Info : Mobile Phase : A:water(0.01%TFA) B:ACN(0.01%TFA)
Gradient:5%B for 0.2min,increase to 95%B within 1.5min,95%B for 1.5min,back to 5%Bwithin 0.01min
Flow Rate :2ml/minColumn :Sunfire, 50*4.6mm,3.5umColumn Temperature:50C
min0.5 1 1.5 2 2.5
mV
-0.1
-0.05
0
0.05
ADC1 A, ELSD
min*0.5 1 1.5 2 2.5
mAU
0
200
*DAD1 A, Sig=214,4 Ref=off
2.21
5min*0.5 1 1.5 2 2.5
mAU
0
200
*DAD1 B, Sig=254,4 Ref=off
2.21
5
min0.5 1 1.5 2 2.50
100000
200000
MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 702.
207
<<<< POSITIVE SPECTRA >>>>
1400 m/z200 400 600 800 1000 1200
05000
100001500020000250003000035000
Ret. Time: 2.21 ES-API Positive
683
.3
334
.1 3
33.1
331
.1
Med
Koo
Bio
scie
nces
ww
w.m
edko
o.co
msa
les@
med
koo.
com
