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ENGINEERING REPORT

Neptune Research Inc. - Composite Aspect · The following composite calculations have been completed to conform to the ASME-PCC2 & ISO TS 24817 standards for

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Page 1: Neptune Research Inc. - Composite Aspect · The following composite calculations have been completed to conform to the ASME-PCC2 & ISO TS 24817 standards for

ENGINEERING REPORT

Page 2: Neptune Research Inc. - Composite Aspect · The following composite calculations have been completed to conform to the ASME-PCC2 & ISO TS 24817 standards for

ENGINEERING REPORT

Document History

Revision Comments Author Date

A BIL Botas International Limited Ryan Schwarz 10.8.12

CMT Jetty Relief Vessel

DL2R-7X18 / DL2R-11 Numarali Problar ile

Bill of Materials

Item # Description Qty Required

SPHCQT Syntho-Poxy HC 1 Quart Kit 2

SUBLV2QT SubSea LV Epoxy 2qt Kit (1qt A + 1qt B) 1

XT860 Syntho- 1

VS860 Viper-Skin 8" X 60' 3

SGUV860G Sythno-Glass UV Gray 2

APPTOOLJ Applicator Toolbox w/ Jiffy Mixer 1

Operating Parameters

Design Pressure Value / measurement Unit of measure

Pipe Size 42 inch

Pipe Grade API 5L X52 API

Original wall thickness "Pipe Schedule" 9.5mm (.375) mm / inch

Maximum wall lose mm /Inch

Design Pressure 28 bar (400 PSI) bar/ psi Design Temperature 49° C (120 °F) C° / °F

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ENGINEERING REPORT

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ENGINEERING REPORT

Installation Parameters

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ENGINEERING REPORT

INTRODUCTION Date Created: 10.08.12

This document presents the design justification for a composite repair application.

42 X52 Petroleum Jetty Relief Vessel w/153mm (6 ) axial defect X 3352 mm (132 ) circumferential defect w/32% wall loss and a design pressure of 28 bar (400 psi) caused by "External Corrosion"

NRI recommends that the repair area of the pipe be sandblasted or an MBX handtool be used to create a Sa 2.5 or NACE 2 SSPC (near white metal) with a .5mm 1mm anchor pattern followed by a SSPC-SP- . The surface preparation will need to extend 177mm ( 7 ) on either side of the defect area as specified within the calculations provided. Once the surface preparation has been completed, NRI proposes the Syntho-Poxy HC a high compressive strength two-part A & B epoxy be used to fill the external corrosion pits and to profile the weld seam to match the contour of the outside diameter of the pipe. Once all anomalies have been filled with the Syntho-Poxy HC NRI recommends the Syntho-

30-60mils (0.76cm-1.5cm) around the entire circumference of pipe make sure to extend the coverage 2" (beyond both ends of the minimum composite repair length as . The epoxy should cover 100% of the defect region and extend over the existing mainline coating at both ends of the composite sleeve to ensure 100% of the repair area is protected from external corrosion. The composite sleeve will provide a load transfer median engineered to cycle and work with the pipeline.

The following composite calculations have been completed to conform to the ASME-PCC2 & ISO TS 24817 standards for nonmetallic repairs of high risk applications for piping and pipe works.

NRI's composite calculations recommend 4 layers of a 100,000 tensile/hoop strength carbon fiber composite sleeve be applied over 508mm (26") centering the defect area which is estimated to be [163 mm (6 ) in the axial length X 3362mm (132 ) in circumferential length] in the middle of the composite sleeve. The composite calculations are based on a design pressure of 28 bar (400 psi) for the API 5L X52 pipe with an original wall thickness of 9.5mm (.375 ) that has been inspected to have a minimum remaining wall thickness of 6.5 mm (.255 ). The source of the wall loss has been identified as external corrosion allowing the composite calculations to engineering the repair thickness of the composite sleeve to take into account the remaining Rstrain of the host pipe which has been identified to be 6.5mm (.255 ). The composite calculations confirm that a 4 layer 2.8mm (0.112") thick composite sleeve be installed around the total repair area to rehabilitate the structural integrity of the defect area on the API 5L X52 petroleum jetty relief vessel. The composite sleeve is engineered to arrest the external corrosion, while also providing the structural strength to meet the design pressure of 28 bar (400 psi) for a minimum of 20 years if the UV protective coating is maintained thru the life of the repair.

Please reference the following documents found within the remainder of this document: Engineered Calculations Installation Guide Quality Control Procedures

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ENGINEERING REPORT

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ENGINEERING REPORT

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ENGINEERING REPORT

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INSTALLATION GUIDE

QA/QC Material Traceability:

ISO (see ISO certificate)

t Number: located on foil pouch, above seal.

Lot # example:

1104256

Procedures to be taken in handling and storage: For ideal shelf life, store in a cool, shaded area at an ambient temperature of 72°F (23°C). Do not expose materials to

temperatures above 110°F (44°C) or below 40°F (5°C).

Viper-SkinTM is packaged within a hermetically sealed foil pouch to protect the Viper-Skin outer composite wrap from

atmospheric moisture. Because the Viper-Skin composite wrap cures when exposed to the application of water or air

humidity, care must be taken in handling the sealed bags to prevent puncturing or scuffing. If the protective foil pouch is

punctured the Viper-Skin composite wrap will be exposed to atmospheric moisture which will cause the Viper-Skin

composite wrap to cure within the foil bag.

NOTE: Do not open the bag containing Viper-Skin until you are ready to use it.

Shelf Life: NRI provides a 12 month shelf-life if Viper-Skin is stored in a cool dry place and the protective foil pouch is

free from puncture damage.

Current MSDS and Technical Datasheets available at http://neptuneresearch.com/downloads/

Day of the year product was manufactured

Internal traceability #

Year of manufacture

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INSTALLATION GUIDE

Scope

1.1. This installation guide may be used for the application of the Viper-SkinTM system for pipeline remediation to any of the following surfaces: carbon, stainless and alloy steel pipe, fittings, flanges, structural supports, for above ground, below ground, sub-sea and splash zone service.

1.2. This installation guide covers pipe and pipeline repairs for external or internal wall loss, with upper temperature limit of the cured system rated for 194oF (90oC).

1.3. Pipe and pipeline repairs for holes, cracks, leaks or fissures fall outside of the scope of this installation guide.

1.4. The PCC- Non-Metallic Composite Repair Systems for Pipelines and Pipe work: High Risk Applications Viper-Skin System for Pipeline Remediation.

1.5. The Engineer shall follow the general guidelines provided by this installation guide to ensure that the implementation of the Viper-Skin system is comprehensive and correct for the specified work.

1.6. The Engineer shall also follow any written procedures providing further details appropriate for specific types of repairs, to ensure that the implementation of the Viper-Skin system is comprehensive and correct for the specified work.

2. General Requirements

2.1. The Engineer shall comply with all written recommendations of the Manufacturer regarding the application of the Viper-Skin system, as well as regarding the completion of written reports on each repair job.

2.2. In cold weather applications, the temperature of the repair area must be brought up to 40o F (5C) prior to the application, as the resins in the epoxies, Syntho-Glass XT and Viper-Skin will not begin to cure at lower temperatures.

2.3. To obtain the material specifications and installation manual, contact NRI:

Phone: 561-683- 561-683-8366 [email protected]

3. Materials

3.1. Syntho-PoxyTMHC Epoxy Available in cartridges (Item# SPHC50mL SPHC200mL, SPHC400mL) which require a static mixing nozzle and applicator gun, or in storage cans (Item#, SPHC_1/2PT, SPHCPT, SPHCQT, SPHC1G, SPHC2G, SPHC5G)

3.1.1. The Syntho-PoxyHC epoxy is a high compressive strength [18,000psi (1,241bar)] two-part A & B epoxy, liquid epoxy resin and amine-based curing agent.

3.1.2. After cure, the Syntho-PoxyHC epoxy will provide benefits which may include sealing, load transfer and/or the creation of a uniform transition between the damaged area and the composite repair.

3.1.3. Syntho-PoxyHC epoxy is engineered for above water sealing applications.

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INSTALLATION GUIDE

3.1.4. The epoxy cartridges should be mixed using a static mixing nozzle and applicator gun, while the storage cans should be mixed using a mixing stick or jiffy mixer. Once mixed it should be dispensed into all defects and troweled in all directions to remove any air pockets that could be trapped between the pipe surface and the liquid epoxy. Once the epoxy is applied to the repair site, feather the edges of the epoxy to create a smooth transition and uniform cylindrical surface.

3.1.5. The physical specification values shall meet the values given on the datasheet for Syntho-PoxyHC.

3.2. Syntho- Available in bi-packs (Item # SUBLV_04OZ, SUBLV_08OZ, SUBLV_16OZ) or in storage cans (Item # SUBLV2QT, SUBLV2G, SUBLV10G, SUBLV100G)

3.2.1. Syntho-SubSeaLV epoxy is a non-hazardous epoxy comprised of a Kevlar® reinforced two-part resin (liquid epoxy resin and amine-based curing agent).

3.2.2. After cure, Syntho-SubSeaLV epoxy will provide benefits which may include sealing, corrosion protection, coating repair, load transfer, adhesion between substrates, and the creation of a smooth transition between the damaged area and the Syntho-Glass®XT.

3.2.3. Syntho-SubSeaLV epoxy is designed for underwater and above water sealing applications. It should be applied between 30-60mil (0.762mm) thickness.

3.2.4. The Physical Specification values shall meet the values given on the datasheet for Syntho-SubSea LV.

3.3. Syntho-Glass®XT (Item# XT215, 330, 430, 460, 615, 630, 660, 690, 830, 860, 1030, 1060, 1260)

NOTE: 1 layer of Syntho-Glass XT applied at a 20% overlap MUST be applied as the primary (first) layer directly

over the Syntho-SubSeaLV epoxy before applying the recommended number of layers of Viper-Skin. This layer

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INSTALLATION GUIDE

of Syntho-Glass

Calculator and is intended only as a barrier layer to prevent the carbon fiber in the Viper-Skin from directly

contacting the pipe surface.

3.3.1. As packaged, Syntho-Glass XT is comprised of an asymmetric bidirectional plain weave fiberglass tape that is impregnated by an uncured (liquid) polyurethane resin.

3.3.2. The resin component of Syntho-Glass XT is activated by fresh or salt water and hardens as it cures, resulting in a thermoset composite.

3.3.3. The hardening of the resin component produces a pressure-retaining fiberglass-reinforced composite sleeve, resistant to attack by petroleum products and many other chemicals, and possessing its greatest strength in the circumferential (hoop) direction of the pipe that is being repaired.

3.3.4. The physical specification values shall meet the values given on the datasheet for Syntho-Glass XT.

3.4. Viper-SkinTM (Item# VS215, 330, 430, 450, 830, 860, 1030, 1060, 1260)

3.4.1. As packaged, Viper-Skin is comprised of an asymmetric bidirectional plain weave hybrid carbon and glass fiber tape that is impregnated by an uncured (liquid) polyurethane resin.

3.4.2. The resin component of Viper-Skin is activated by fresh or salt water and hardens as it cures, resulting in a thermo set composite.

3.4.3. The hardening of the resin component produces a pressure-retaining carbon and glass fiber reinforced composite sleeve, resistant to attack by petroleum products and many other chemicals, and possessing its greatest strength in the circumferential (hoop) direction of the pipe that is being repaired.

3.4.4. The physical specification values shall meet the values given on the data sheet for Viper-Skin.

NOTE: Do not open the bag containing Viper-Skin until you are ready to use it, as the

atmospheric moisture which will cause it to cure.

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INSTALLATION GUIDE

3.5. Syntho-Glass®UV (Item# UVW520, 930, 415, 430, 450, 830, 850)

3.5.1. As packaged, Syntho-Glass UV is a bidirectional fiberglass that is impregnated with a moisture-curable, aliphatic, UV stable, liquid polyurethane resin. This final outer wrap is in addition to the

and environmental protection only.

4. General Surface Preparation Requirements

4.1. Measure the distance of the repair application to ensure the length of the surface preparation extends beyond the minimum repair length specified by NRI's composite calculator's engineered calculations. Extend surface preparation 1" (25.4mm) each side of repair area.

4.2. Remove pipe coating, loose rust, paint and other foreign matter.

4.3. Prepare surface in accordance with Sa 2.5 or NACE 2 SSPC, near white Metal.

4.4. High-pressure [3,000 to 7,000 psi (206.84 to 482.63 bar)] water blast or grit blast cleaning may be used to prepare the surface.

4.5. The clean, prepared surface shall have a 2-4 mil (0.05-0.1mm) anchor pattern.

4.6. Remove dirt, grease and oil in accordance with SSpC-SP- Measure and mark the repair area using the engineered calculations. Be sure to extend the repair length by 2" (50.8mm) on either side of the repair area and mark edges using masking tape.

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INSTALLATION GUIDE

5. Mixing and Application of Syntho-PoxyHC as Sealing Load Transfer Material

Mixing of Syntho-PoxyTMHC Epoxy Cartridge with Static Mixing Nozzle and Applicator Gun

5.1. Syntho-PoxyHC is supplied in two precisely proportioned parts: Part A, liquid epoxy resin and Part B, curing ) in 50ml, 200ml and/or 400 mil cartridges that are dispensed using a hand

held applicator gun and mixed with a static mixing nozzle. The resin and hardener are properly mixed with the static mixer to ensure the correct physical properties of the liquid epoxy. Working time is only 10 minutes. Dispense only enough liquid epoxy that you can install in 10 minutes.

5.2. Syntho-PoxyHC is supplied in two precisely proportioned parts: Part A, liquid epoxy resin and Part B, curing ) in 50ml, 200ml and/or 400 mil cartridges that are dispensed using a hand

held applicator gun and mixed with a static mixing nozzle. The resin and hardener are properly mixed with the static mixer to ensure the correct physical properties of the liquid epoxy. Working time is only 10 minutes. Dispense only enough liquid epoxy that you can install in 10 minutes.

NOTE: Ensure Syntho-PoxyHC is being dispensed from the nozzle in equal proportions, as one consistent gray

color. If white and /or black streaks remain, additional mixing is required to achieve correct physical

properties.

NOTE: Replace the mixing nozzle (Item # SPHCNOZ) after each 10 min application to ensure proper mixing of

the Syntho-Poxy HC.

Mixing of Syntho-PoxyHC Supplied in Storage Cans by Manually Mixing or with Jiffy Mixer

5.3. Add 100% of the liquid epoxy resin (Part A) and 100% of the curing agent (Part B) into a painters pail. It is essential for the installer to add all of Part A and B into the container in order to achieve proper curing.

5.4. Complete and thorough mixing of the two parts is required in order to obtain the correct curing properties; and can be achieved by stirring the two parts together until a smooth, uniform, streak-free consistency is reached. A jiffy mixer and handheld drill can be used to mix 100% of the A & B in a clean bucket.

Application of Syntho-Poxy HC

5.5. Apply mixture to clean, prepared surface by using a spatula, trowel or putty knife, working the material into all indentations to assure that no air bubbles remain.

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INSTALLATION GUIDE

5.6. Feather the application to ensure the edges of a water-tight seal.

6. Mixing and Application of Syntho-SubSea LV

6.1. Syntho-SubSea LV is supplied in two precisely proportioned parts: Part A, liquid epoxy resin and Part B, curing Syntho-SubSea LV is available in individual storage cans (Item# SUBLV2QT,

SUBLV2G, SUBLV10G), Bi-Packs (SUBLV_04OZ, SUBLV_08OZ, SUBLV_16OZ), and a 0.4 gallon cartridge (Item# SUBLV.4) which requires an applicator gun (Item# EAGM0.4G and EAGP0.4G) and static mixing nozzle (Item # EAGMXR24).

Mixing of Syntho-SubSea LV by Manually Mixing or with Jiffy Mixer

6.2. Add 100% of the liquid epoxy resin (Part A) and 100% of curing agent (Part B) into a clean plastic bucket large enough to hold the volume. It is essential for the installer to use ALL of Part A and Part B in order to achieve proper curing.

6.3. Complete and thorough mixing of the two parts is required in order to obtain the correct curing properties; and can be achieved by stirring the two parts together until a smooth, uniform, streak-free consistency is reached. A jiffy mixer and handheld drill can be used to mix 100% of the A & B in a clean bucket.

Mixing of Syntho-SubSea LV within Bi-Packs

6.4. Subsea LV bi-packs is supplied in correct proportions a plastic bi-pack which is divided by a clip. Remove clip by sliding downward off of the bi-pack. The clip can be used to begin mixing the liquid epoxy resin (Part A) and the curing agent (Part B) on a flat surface. Continue manually mixing the epoxy within the pouch until no streaks remain.

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INSTALLATION GUIDE

6.5. Complete and thorough mixing of the two parts is required in order to obtain the correct curing properties. This is achieved by mixing the two parts together until a smooth, uniform, streak-free consistency is reached.

Application of Syntho-SubSea LV

6.6. Apply mixture to clean, prepared surface by using a spatula, trowel or putty knife, working the material into all indentations to assure that no air bubbles remain.

6.7. Feather the edges of the application to ensure a water-tight seal.

6.8. Apply Syntho-SubSeaLV around entire circumference of pipe. Be sure to extend the coverage to the previously marked masking tape [+2" (50.8mm) on both sides of the minimum composite repair length (see 4.5 above) as calculator.

NOTE: inspect the Syntho-SubSeaLV coverage to ensure proper mil thickness of 30mil 60mil using a mil

gauge supplied in the applicator tool box. Make sure 100% of the pipe surface is coated to ensure no holidays

or bare steel is exposed.

6.9. Remove masking tape which was used to mark the edges of the repair area.

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INSTALLATION GUIDE

For Application of Viper-Skin on Straight Piping proceed to 7.

For Application of Viper-Skin on Elbows proceed to 8.

For Application of Viper-Skin on Tees proceed to 9.

7. Application of Viper-Skin System on Straight Piping

7.1. Application of Syntho-Glass®XT as primary layer

NOTE: 1 layer of Syntho-GlassXT MUST be applied as the primary (first) layer directly over the Syntho-

SubSea LV Epoxy. The Syntho-GlassXT shall be applied in a spiral manner using a 20% overlap before

applying the recommend number of layers of Viper-Skin.

NOTE: Do not open the bag containing Syntho-GlassXT until you are ready to use it, as the atmospheric

moisture which will cause it to cure.

In cold weather applications, the temperature of the repair area must be brought up to 40F (5C) prior to the

application of Syntho-GlassXT since its resin component will not begin to cure at lower temperatures.

7.1.1. Water shall be sprayed on each layer of Syntho-Glass XT as it is being applied, rather than immersing the roll in water before application.

7.1.2. 1 layer of Syntho-GlassXT shall be spirally wrapped around the pipe with a 20% overlap as the primary (first) layer directly over the Subsea LV Epoxy before applying the recommended number of layers of Viper-Skin.

7.1.3. Hold the end of the Syntho-GlassXT tape firmly to the surface of the pipe at the starting point. The -SubSeaLV primary layer on either

side.

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INSTALLATION GUIDE

NOTE: Ensure the total repair length of the Syntho-GlassXT 1 primary layer is within the required

. This measurement does not include the 1" (2.54cm)

of Syntho-SubSeaLV epoxy that extends beyond the starting point and ending point of the 1 primary

layer of Syntho-GlassXT and recommend number of layers of Viper-Skin composite.

7.1.4. Unroll the tape, keeping it as close to the surface of the pipe as possible. Do not use a long lead of tape. The roll of tape shall always be in an upright position, with the tape being applied from the lower edge of the roll to maintain proper pressure.

7.1.5. Apply sufficient tension by pulling on the roll of tape as the layers are being applied.

7.1.6. The Syntho-GlassXT tape shall be spirally wrapped around the pipe from right to left or from left to right. NOTE: Only 1 layer of Syntho-GlassXT applied at a 20% overlap is required before applying the recommended number of layers of Viper-Skin.

NOTE: The Viper-Skin composite must start 1" (2.54cm) inside of the same starting point of the

1primary layer of Syntho-GlassXT. The Viper-Skin composite MUST be applied in the same clockwise

direction or counter clockwise direction as the 1 primary layer of Syntho-GlassXT.

NOTE: 1 layer of Syntho-Glass XT MUST be applied at a 20% overlap as the primary (first) layer

directly over the SubSeaLV epoxy before applying the recommend number of layers of Viper-Skin.

7.2. Application of Viper-SkinTM on Straight Piping

NOTE: Do not open the bag containing Viper-Skin until you are ready to use it, as the atmospheric moisture

which will cause it to cure.

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INSTALLATION GUIDE

In cold weather applications, the temperature of the repair area must be brought up to 40F (5C) prior to the

application of Viper-Skin since its resin component will not begin to cure at lower temperatures.

7.2.1. Water shall be sprayed on each layer of Viper-Skin as it is being applied, rather than immersing the roll in water before application.

7.2.2. Each completed Viper-Skin application shall have the specified number of layers, and be the specified

towards your total repair thickness. For example: to achieve a 10 layer application, apply 5 passes using a 50% overlap.

7.2.3. Hold the end of the tape firmly to the surface of the pipe at the starting point. The starting point shall -GlassXT primary layer on both sides.

7.2.4. Begin the wrap using 100% overlap to assure complete coverage. The Viper-Skin composite MUST be applied in the same clockwise direction or counter clockwise direction as the 1 primary layer of Syntho-GlassXT.

NOTE: Ensure the total repair length of the Viper-Skin composite is applied at the required length

Syntho-GlassXT that extends beyond the starting point and ending point of the Viper-Skin composite.

7.2.5. Unroll the tape, keeping it as close to the surface of the pipe as possible. Do not use a long lead of tape. The roll of tape shall always be in an upright position, with the tape being applied from the lower edge of the roll to maintain proper pressure.

7.2.6. Apply sufficient tension by pulling on the roll of tape as the layers are being applied using a 50% overlap.

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INSTALLATION GUIDE

7.2.7. The tape shall be spirally wrapped around the pipe from right to left or left to right using a 50%

overlap. At the end of the first wrap, apply a 100% overlap before reversing the direction of the wrap and continue to apply the Viper-Skin. Do not reverse the direction of the application without completing an entire wrap along the length of the repair area.

7.2.8. The completed Viper-Skin application shall be overwrapped by four layers of compression film &

perforated using the perforator tool. The compression film may be removed when Viper-Skin has reached its initial cure time.

7.3. The Viper-Skin installation shall be ready for service when the resin has cured sufficiently to provide adhesion between layers and has reached a hardness of 80 Shore D.

7.4. For vertical installations such as Offshore Risers or Jacket Legs, Viper-Skin application shall begin at the bottom of the repair area and proceed upwards.

7.5. For sub-sea and splash zone installations, the last (outer) wrap shall be tied down or overwrapped in a manner that will ensure that the currents or wave action will not affect the adhesion of the last layer of fiberglass tape before the resin has reached its initial cure.

7.6. For sub-sea installations, open the bag of Viper-Skin underwater, at the repair site, after all cleaning is completed and all epoxies have been applied.

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INSTALLATION GUIDE

7.7. For higher impact resistance, apply additional layers of Syntho-Glass®24 over the Viper-Skin.

NOTE: For Non-Buried applications, a Viper-Skin installation must be coated with a UV-blocking and

weather resistance coating of Syntho-GlassUV, or an approved coating by NRI.

7.8. For cold weather installations, follow procedures above. However, as an additional step, after applying the final outer wrap of a compression film, then apply a heating pad over the entire repaired area since Viper-Skin

will not cure by itself at temperatures under 40ºF (5oC). )

7.9. For hot weather installations, follow procedures above. However, use ice water in the sprayer if possible, to slow down the curing and thus allow the installer sufficient working time. Furthermore, store unopened bags of Viper-Skin in a separate container in an ice chest if possible.

7.10. The installer shall follow the written procedures and software provided by the manufacturer in order to calculate the minimum number of layers of Viper-Skin required for specific types of repairs.

7.11. The Engineer shall follow the written procedures and software provided by the Manufacturer in order to calculate the minimum axial length of repair, which includes the length directly over the repair area, the overwrap length extending beyond the repair area while remaining at the same number of layers, and the taper length extending at each end beyond the overwrap region.

Warranty/Disclaimer: NRI® , Syntho-Glass®XT , Syntho-Glass®UV, and Syntho-Glass®24 are registered trademarks, and Viper-Skin , Syntho-Poxy HC, Syntho-

Subsea LV, and Syntho-Subsea are trademarks of NRI. NRI, the Manufacturer of Viper-Skin will replace at no charge to the purchaser any product proved to be

defective. Responsibility of the Manufacturer and the Distributor is limited to replacement of the product only. Neither the Manufacturer nor the Distributor shall be liable

for consequential or incidental damage or loss of any kind as they do not have any control over the conditions under which these products may be used or over the

methods of application. Users should test the product for their particular need and suitability. Users should consult with the Manufacturer or the Distributor for all

proposed repairs using the Viper-Skin system. Written procedures for specific repairs are available upon request from the Manufacturer or Distributor. All proposed repairs

to pipeline systems using the Viper-Skin system must be installed or supervised by certified technicians. Viper-Skin is not an approved coating system. Failing to coat per

standard procedures can lead to atmospheric corrosion damage. Apply protective coatings per company standards. Kevlar® is a registered trademark of E. I. du Pont

Nemours and Company.

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INSTALLATION VALIDATION PROCEDURE:

QUALITY CONTROL RECORDS

Project name or reference #: Date:

Company:

Address:

City: State: Postal Code: Country:

Contact(s):

Phone: Fax: E-mail:

** Please provide photos before, during and after application **

Pre-Installation QC Requirements Value # / Initials Project Verification

NRI Calculation ID #: Diameter of Pipe: Length of Repair: # of Viper-Skin Layers:

Initial:

Material Preparation Raw materials have been inspected to ensure proper labeling, within expiration date, proper requirements & quantities.

Initial:

Record Expiration Dates Syntho-Poxy HC Lot # & Mfg Date: Subsea LV Lot # & Mfg Date: Syntho-Glass XT Lot #(s): Viper-Skin Lot #(s):

Initial:

Surface Preparation Requirements Value # / Initials

Inspection NACE 2/ Sa 2.5/SSPC-SP- Initial: Definition: Removal of nearly all mill scale, rust, rust scale, paint, or foreign matter by the use of abrasive propelled through nozzles or by centrifugal wheels, to the degree hereafter specified. A Near-White Blast Clean Surface Finish is defined as one from which all oil, grease, dirt, mill scale, rust, corrosion products, oxides, paint or other foreign matter have been completely removed from the surface except for very light shadows, very slight streaks or slight discolorations caused by rust stain, mill scale oxides, or light, tight residues of paint or coating that may remain. At least 95 percent of each square inch of surface area shall be free of all visible residues, and the remainder shall be limited to the light discoloration mentioned above.

Page 23: Neptune Research Inc. - Composite Aspect · The following composite calculations have been completed to conform to the ASME-PCC2 & ISO TS 24817 standards for

INSTALLATION VALIDATION PROCEDURE:

QUALITY CONTROL RECORDS

Application Controls Requirements Value # / Initials

Material Preparation Raw materials have been inspected to ensure proper labeling, requirements & quantities

Initial:

Syntho-Poxy HC Putty The Syntho-Poxy HC was manually mixed until uniform in color (light grey) or mixed using the applicator gun & static mixing nozzle. The SPHC was applied within 10 minutes.

Initial:

Cured Epoxy Putty The Syntho-Poxy HC was inspected to ensure the filler material conforms to the geometry of the pipe's cylinder shape

Initial:

Subsea LV Epoxy Mixing

100% of the SubSea LV part A & B was manually mixed until uniform in color (light green) or mixed using the applicator gun & static mixing nozzle.

Initial:

Subsea LV Epoxy Application Thickness

30-60 mils of SubSea LV was applied which was within the target range of technical data requirements.

Initial:

Syntho-Glass XT Resin Activating

100% of the Syntho-Glass XT composite wrap's resin was activated using fresh water or salt water.

Initial:

Syntho-Glass XT The 1 layer of Syntho-Glass XT was applied using a 20% overlap beginning 1" (2.54cm) inside the border of the Subsea LV epoxy on both sides of the overall repair distance.

Initial:

Syntho-Glass XT 1 layer of Syntho-Glass XT was applied using a 20% overlap before applying the Viper-Skin composite.

# Layers:

Viper-Skin Resin Activating

100% of the Viper-Skin composite wrap's resin was activated using fresh water or salt water.

Initial:

Viper-Skin The starting point for the Viper-Skin composite should be 1" (2.54cm) inside the border of the 1 layer of the Syntho-Glass XT on both sides.

Initial:

Viper-Skin Correct # of layers of composite wraps were applied based on NRI's calculations. # Layers: Compression Film 100% of the outer layers of Viper-Skin were wrapped with 4 layers of

compression film and perforated every 16 layers while the resin is still tacky. Initial:

Repair Length Requirements Value # / Initials

Dimensions NOTE: 1 layer of Syntho-Glass XT MUST be applied as the primary (first) layer directly over the Subsea LV epoxy before applying the recommended number of layers of Viper Skin. The overall composite repair length MUST be within the minimum axial repair length as specified within the NRI composite calculations.

NOTE: The Subsea LV epoxy should extend 2" (5.08cm) beyond the minimum axial length of the Viper-Skin composite repair determined by NRI's composite calculations.

1 layer of Syntho-Glass XT should by applied at a 20% overlap beginning 1" (2.54cm) inside the border of the Subsea LV epoxy on both sides of the overall repair distance.

The starting point for the Viper-Skin composite should be 1" (2.54cm) inside the border of the 1 layer of the Syntho-Glass XT on both sides.

Initial:

Viper-Skin total length:

Syntho-Glass XT total length:

Subsea LV total length:

Page 24: Neptune Research Inc. - Composite Aspect · The following composite calculations have been completed to conform to the ASME-PCC2 & ISO TS 24817 standards for

INSTALLATION VALIDATION PROCEDURE:

QUALITY CONTROL RECORDS

Using a Shore D hardness tester, do the following upon completion of repair:

1. The Syntho-SubSeaTMLV Epoxy should be tested using the Shore D hardness tester after 24 hrs and should have a minimum average Shore D value of 70

a. The epoxy used for this test should be an excess amount left over from the repair and can be place on an area outside of the pipe.

b. The highest point to the epoxy should be where the pin is placed c. A minimum of 10 tests shall be done to get the average.

2. The Syntho-Glass® 1 primary layer should have a minimum average Shore D of 70 a. Testing should be performed ensuring the pin is placed on the highest point of the composite repair

to ensure proper reading b. A minimum of 10 test shall be done to get the average c. The test point shall be placed directly on a fiber and not the valley where the fibers cross as this

could result in a false low reading.

3. The Viper SkinTM outer layer should have a minimum average Shore D of 70 a. Testing should be performed ensuring the pin is placed on the highest point of the composite repair

to ensure proper reading b. A minimum of 10 test shall be done to get the average c. The test point shall be placed directly on a fiber and not the valley where the fibers cross as this

could result in a false low reading.

All test parameters and to be performed to ensure that all materials have been properly mixed and ensure complete curing profile of the Viper Skin composite repair system.

Name: Certification #:

Signature: Date:

** Please provide photos before, during and after application **

Test on Repair Requirements Value # / Initials Cure Subsea LV epoxy Hardness requirements of the epoxy meet Shore D requirements of the technical

data (see next page) Value:

Cure Viper-Skin Wrap Hardness requirements of the Viper-Skin composite wrap meet Shore D requirements of the technical data (see next page)

Value:

Composite Wrap Correct # of layers of Viper-Skin composite wraps were applied based on NRI's calculations

# Layers:

Dimensions The Viper-Skin overall repair length is within the minimum axial repair length specified within the calculations. The Subsea LV should extend 1-2 inch beyond the required Viper-Skin axial repair length.

Length:

** Please provide photos before, during and after application **