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MODIFIED TEST ASSEMBLY FOR WATER TREE STUDY ON POLYMERIC INSULATING MATERIALS CHE NURU SANIYYATI BINTI CHE MOHAMAD SHUKRI A thesis submitted in fulfilment of the requirements for the award of the degree of Master of Engineering (Electrical) Faculty of Electrical Engineering Universiti Teknologi Malaysia JULY 2014

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MODIFIED TEST ASSEMBLY FOR WATER TREE STUDY ON POLYMERIC

INSULATING MATERIALS

CHE NURU SANIYYATI BINTI CHE MOHAMAD SHUKRI

A thesis submitted in fulfilment of the

requirements for the award of the degree of

Master of Engineering (Electrical)

Faculty of Electrical Engineering

Universiti Teknologi Malaysia

JULY 2014

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iii

To my beloved father,

Che Mohd Shukri bin Che Musa

To my beloved mother,

Nik Zaleha binti Nik Abdul Rahman

To my brothers and sisters

Che Nurul Saadatina, Che Ahmad Nazimuddin, Che Ahmad Najmi and

Che Ahmad Najwan

lecturers and friends

for their encouragement, inspiration and support

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iv

ACKNOWLEDGEMENT

First of all, I would like to give my thanks to the Almighty Allah, for giving

me the strength and ability to wholeheartedly complete this project. With His

blessings, this project is finally, successfully finished.

Secondly, I would like express to my deepest gratitude and appreciation to

Dr. Yanuar Zulardiansyah Arief, Dr Zuraimy Adzis and Dr Mohd Hafizi Ahmad for

the opportunity to conduct research under their guidances and supervisions. The

completion of the present study would not have been possible without their

invaluable knowledge and unwavering support throughout the project.

Special thanks to my parents, Che Mohd Shukri bin Che Musa and Pn. Nik

Zaleha binti Nik Abdul Rahman for their invaluable help and support throughout the

year and to my significant other, Mohd Fakhruddin bin Zainal Ashirin, for putting up

with the late nights and for always providing words of encouragement.

Lastly, to all the people that have been directly or indirectly involved towards

the contribution and the realisation of this project, friends and librarians, your help

and involvement is greatly appreciated.

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ABSTRACT

Water tree is a process that causes degradation of insulation performance and

ageing of Cross-Linked Polyethylene (XLPE) underground cables. It is known as one

of the major causes of premature ageing and failure of polymeric cables. Previous

research has shown that there are different effects of ageing time on water tree growth in

different types of polymeric insulating materials where nickel and platinum have been

used as electrodes and were found to cause corrosion and reduce efficiency. Thus, in

this research, a modified test assembly using tungsten needle as an electrode to avoid

corrosion and increase efficiency was introduced. This research investigated the effects

of ageing time on water tree growth in two different types of polymeric sample namely

(XLPE) and Low-Density Polyethylene (LDPE) under high voltage stress. Using

computational simulation, the effect of voltage application and angle of tip radius against

electric field using COMSOL 4.2a was studied. In this study, the polymeric samples

were prepared using a new method known as “leaf-like” specimen method. The

experiment was based on BS IEC 61956 2001, “Methods of test for the evaluation of

water treeing in insulating materials” and BS EN 60243-1 : 1998, “Electrical strength of

insulating materials-Test methods”. Samples were exposed to high voltage injection for

150 hours and 470 hours. The simulation results show that when voltage application

increases, the electric field will increase. Besides that, a lower angle of tip radius in

polymeric sample, will result in higher electric field being produced. Experimental

results show that water tree growth is proportional to ageing time of the two polymeric

samples. However, XLPE has better water treeing resistance than LDPE because the

average length of water tree growth for LDPE is higher as compared to XLPE. This

study has shown that ageing time as the cause of water tree growth that causes

degradation in insulation performance has different effects on different types of

polymers.

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ABSTRAK

Pepohon air ialah satu proses yang menyebabkan degradasi prestasi penebat dan

penuaan Polietilen Hubung-Silang (XLPE) kabel bawah tanah. Proses ini menjadi salah

satu punca utama penuaan pramatang dan kegagalan kabel polimer. Kajian terdahulu

menunjukkan terdapat kesan yang berlainan terhadap masa penuaan kepada

pertumbuhan pepohon air dalam pelbagai jenis bahan penebat polimer dengan nikel dan

platinum digunakan sebagai elektrod didapati menyebabkan hakisan dan mengurangkan

kecekapan. Dalam kajian ini, pemasangan ujian diubah suai menggunakan tungsten

sebagai elektrod untuk mengelakkan hakisan dan meningkatkan kecekapan. Kajian ini

mengkaji kesan masa penuaan terhadap pertumbuhan pepohon air dalam dua jenis

sampel polimer iaitu (XLPE) dan Polietilen Berketumpatan-Rendah (LDPE) di bawah

tekanan voltan tinggi. Kesan aplikasi voltan dan sudut jejari hujung terhadap medan

elektrik menggunakan COMSOL 4.2a telah dikaji menggunakan simulasi pengiraan.

Dalam kajian ini, sampel polimer telah disediakan dengan kaedah spesimen "jenis

dedaun". Eksperimen ini berdasarkan BS IEC 61956 2001, "Kaedah ujian untuk

penilaian pepohon air dalam bahan-bahan penebat" dan BS EN 60243-1: 1998,

"Kekuatan elektrik bahan penebat – Kaedah ujian”. Sampel telah didedahkan kepada

suntikan voltan tinggi selama 150 jam dan 470 jam. Keputusan simulasi menunjukkan

apabila aplikasi voltan bertambah medan elektrik akan bertambah. Selain itu, jejari

hujung di dalam polimer yang bersudut lebih rendah akan menghasilkan medan elektrik

yang lebih tinggi. Keputusan eksperimen menunjukkan pertumbuhan pepohon air

berkadar terus dengan masa penuaan kedua-dua sampel polimer. Walau bagaimanapun

XLPE mempunyai rintangan pepohon air yang lebih baik daripada LDPE kerana purata

tempoh pertumbuhan pepohon air untuk LDPE adalah lebih tinggi berbanding dengan

XLPE. Kajian ini menunjukkan bahawa masa penuaan merupakan punca pertumbuhan

pepohon air yang menyebabkan kemerosotan dalam prestasi penebat yang mempunyai

kesan berbeza kepada jenis polimer yang digunakan.

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TABLE OF CONTENTS

CHAPTER TITLE PAGE

DECLARATION ii

DEDICATION iii

ACKNOWLEDGEMENT iv

ABSTRACT v

ABSTRAK vi

TABLE OF CONTENTS vii

LIST OF TABLES xii

LIST OF FIGURES xiii

LIST OF ABBREVIATIONS AND SYMBOLS xviii

LIST OF APPENDICES xxi

1 INTRODUCTION

1.1 Research background 1

1.2 Problem Statement 4

1.3 Objective of Research 5

1.4 Scope of Research 6

1.5 Significance of Research 6

1.6 Thesis Organization 7

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2 LITERATURE REVIEW

2.1 Introduction 9

2.2 Background of Water Tree 11

2.3 Types of Water Tree 11

2.3.1 Bow-Tie Tree in the insulation 12

2.3.2 Vented Tree in the insulation 13

2.4 Basic Formation of Water Tree 14

2.4.1 Water Tree Initiation and Growth

Mechanism

15

2.4.2 Ageing Conditions 18

2.4.3 Characteristics of Water Tree 18

2.4.4 Chemical, Mechanical and Thermal

Aspects

21

2.4.5 Investigation of Water Tree Using

FTIR, Micro-PIXE, and Electron

Spectroscopy

21

2.4.6 Fractal Behaviour and Analysis

During Water Tree

22

2.4.7 Effects of Water Tree on Electrical

Properties

23

2.5 Diagnostic Technique and Testing of Water Tree 25

2.5.1 Capacitance and Loss Tangent 25

2.5.2 Non-Linearity of Loss Current with

Voltage

25

2.5.3 Dielectric 26

2.5.3.1 Broadband Dielectric

Spectroscopy

26

2.5.3.2 Time Domain Dielectric

Spectroscopy

27

2.5.3.3 Dielectric Response

Measurements

27

2.5.4 Depolarization 28

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2.5.4.1 DC Leakage, Polarization and

Depolarization Currents

Response

28

2.5.4.2 Return/Recovery Voltage

Measurements

29

2.5.5 Current 29

2.5.5.1 Current Pulses during Water

Tree

30

2.5.5.2 Thermally Simulated Currents 30

2.5.6 Non-Standard Test Voltages 31

2.5.7 Time Domain Reflectometry 31

2.6 Factors Affecting Growth and Initiation of

Water Tree

32

2.6.1 Ageing Time 32

2.6.2 Electric Field 33

2.6.3 Applied Voltage 35

2.6.4 Applied Frequency 36

2.6.5 Temperature Dependent 37

2.6.6 Concentration of Solution 39

2.6.7 Types of Electrode 40

2.6.8 Types of Sample Materials 41

2.6.9 Mechanical Stress of Materials 43

3 RESEARCH METHODOLOGY

3.1 Introduction 44

3.2 Research Flowchart 45

3.3 Computational Simulation and Simulation

Procedure

47

3.3.1 Meshing Strategy 53

3.3.2 Types of Meshing 54

3.4 Sample Production Process 60

3.4.1 Raw Material Preparation 60

3.4.2 Molding Process 63

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3.4.3 Cooling Process 64

3.4.4 Finished Good Sample 65

3.5 Test Kit Assembly 67

3.5.1 Standard Test Kit Assembly

According to British Standard

67

3.5.2 Modified Test Kit Assembly 68

3.5.3 Modified Test Sample 69

3.5.3.1 Design and Sample

Preparation

69

3.5.3.2 Sample Preparation from

Pre-Casting Process

71

3.5.3.3 Needle Tip Formation 72

3.5.4 Modified Test Cell 74

3.5.5 Overall Modified Test Kit Assembly 76

3.6 Experimental Setup 77

3.6.1 Water Tree Testing Setup 78

3.6.2 Water Tree Testing Procedure 79

3.7 Dyed Water Tree in Methylene Blue 80

3.8 Water Tree Observation 81

4 RESULTS AND DISCUSSION

4.1 Introduction 82

4.2 Method of Measurement 83

4.3 Analysis Using COMSOL 4.2a Software 84

4.3.1 Electric field for Different Voltage 85

4.3.1.1 Electric Field for Voltage 3kV 86

4.3.1.2 Electric Field for Voltage 4kV 88

4.3.1.3 Electric Field for Voltage 5kV 89

4.3.1.4 Electric Field for Voltage 6kV 91

4.3.2 Analysis and Discussion for Different

Voltage against Electric Field

92

4.3.3 Electric Field for Different Angle of Tip

Radius

94

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4.3.3.1 Electric Field for Different

Angle of Tip Radius of the

Needle

95

4.3.3.2 Electric Field for Different

Angle of Tip Radius in

Polymeric Sample

97

4.3.4 Analysis and Discussion for Different

Angle of Tip Radius in Polymeric

Sample at Different Voltage against

Electric Field

109

4.4 Water Tree Results through Laboratory

Experiment

111

4.4.1 Water Tree Length of XLPE Sample

Tested for 0 Hour

112

4.4.2 Water Tree Length of XLPE Sample

Tested for 470 Hours

113

4.4.3 Water Tree Length of LDPE Sample

Tested for 0 Hour

115

4.4.4 Water Tree Length of LDPE Sample

Tested for 150 Hours

116

4.4.5 Water Tree Length of LDPE Sample

Tested for 470 Hour

117

4.5 Water Tree Analysis and Discussion For

Laboratory Experiment

118

4.5.1 Water Tree for Different Ageing Time 119

4.5.2 Water Tree for Two Different Materials 122

5 CONCLUSIONS AND RECOMMENDATION

5.1 Conclusions 124

5.2 Recommendations For Future Work 126

REFERENCES 127

Appendices A - B 136 - 143

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LIST OF TABLES

TABLE NO. TITLE PAGE

2.1 Ageing conditions 18

3.1 Summary of computational simulation. 48

3.2 Strengths and weakness of COMSOL 4.2a meshing 53

3.3 Maximum electric field for types of mesh 59

4.1 Electric field for different voltage 93

4.2 Electric field for different angle of tip radius of the

needle at different voltage 96

4.3 Electric field for different angle of tip radius in

polymeric sample at different voltage 110

4.4 Measurement water tree length data for Figure 4.23 114

4.5 Measurement water tree length data for Figure 4.25 116

4.6 Measurement water tree length data for Figure 4.26 118

4.7 Length of water tree for different ageing time (hours) 121

4.8 Average length of water tree for different ageing time

(hours) 121

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LIST OF FIGURES

FIGURE NO. TITLE PAGE

1.1 Failure category diagram of underground cable

reported by Tenaga Nasional Berhad (TNB)

Selangor for the data of 1 Sept – 31 Aug 2011

2

1.2 Typical vented trees observed in the water tree

needle electrode of XLPE cable insulation

4

2.1 Bow-tie tree in the insulation 12

2.2 Vented tree in the insulation 13

2.3 Relationship between the ageing time and water tree

length

33

2.4 Relationship between the radius curvature of the

needle and water tree length

35

2.5 Relationship between the applied voltage and water

tree length

36

2.6 Relationship between frequency and water tree

growth with different time of testing

37

2.7 Relationship between the temperature and maximum

length of water tree

39

2.8 Relationship between concentration of NaCl and

water tree length

40

2.9 Relationship between types of electrodes and water

tree length

41

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xiv

2.10 Relation between different molecular weight and

length of water tree as a function of time in LDPE

without antioxidant

42

3.1 Research flowchart 46

3.2 Simulation procedure 49

3.3 Computational modelling 50

3.4 Dimension of the sample in the simulation 50

3.5 Definitions of the sample 51

3.6 Material for NaCl solution 51

3.7 Study of electrostatics 52

3.8 Result of electric field of the simulation 52

3.9 Maximum electric field for extremely coarse 55

3.10 Maximum electric field for normal 56

3.11 Maximum electric field for finer 57

3.12 Maximum electric field for extremely fine 58

3.13 Relationship between maximum electric field and

types of mesh

59

3.14 Cleaning plate and process using release agent 61

3.15 Dimension for sample block 62

3.16 Pallets in the barrier plate 62

3.17 Molding machine 64

3.18 Cooling machine 65

3.19 Finished good sample from the machine 66

3.20 Sample that cuts into pieces 66

3.21 Standard test cell assembly 68

3.22 Configuration of leaf-like specimen with (a) schematic

diagram of top view, (b) schematic diagram of side

view

70

3.23 Tungsten wire 73

3.24 Needle tip formation process using NaOH solution and

distilled water

73

3.25 Schematic diagram for needle tip formation 74

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3.26 Schematic diagram of the modified test cell (a) acrylic

plate for box, (b) top view, (c) 3D view

75

3.27 Actual picture of overall modified test assembly 77

3.28 Setup offline monitoring systems for water tree studies

schematic diagram

78

3.29 Setup for water tree testing 79

3.30 Dyed methylene blue samples in vacuum valve 80

3.31 Metallographic microscope 81

4.1 Measurement method for water tree length 84

4.2 Overall shape of sample dimension in COMSOL 4.2a 85

4.3 Electric field in sample dimension 86

4.4 Electric field for voltage 3kV with (a) Electric field

profile at polymeric side, (b) Display of voltage setting

in COMSOL 4.2a

87

4.5 Electric field at voltage 4kV with (a) Electric field

profile at polymeric side, (b) Display of voltage setting

in COMSOL 4.2a

88

4.6 Electric field at voltage 5kV with (a) Electric field

profile at polymeric side, (b) Display of voltage setting

in COMSOL 4.2a

90

4.7 Electric field at voltage 6kV with (a) Electric field

profile at polymeric side, (b) Display of voltage setting

in COMSOL 4.2a

91

4.8 Relationship between the electric field and the voltage 94

4.9 Electric field for angle of tip radius of the needle 150 at

voltage 3 kV

95

4.10 Relationship between the electric field and the angle of

tip radius of the needle at different voltage

97

4.11 Electric field for angle of tip radius in polymeric

sample of 150 at voltage 3 kV with (a) Electric field

profile at polymeric side, (b) Display of voltage setting

in COMSOL 4.2a

98

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4.12 Electric field for angle of tip radius in polymeric

sample of 150 at voltage 6 kV with (a) Electric field

profile at polymeric side, (b) Display of voltage setting

in COMSOL 4.2a

99

4.13 Electric field for angle of tip radius in polymeric

sample of 300 at voltage 3 kV with (a) Electric field

profile at polymeric side, (b) Display of voltage setting

in COMSOL 4.2a

101

4.14 Electric field for angle of tip radius in polymeric

sample of 300 at voltage 6 kV with (a) Electric field

profile at polymeric side, (b) Display of voltage setting

in COMSOL 4.2a

102

4.15 Electric field for angle of tip radius in polymeric

sample of 450 at voltage 3 kV with (a) Electric field

profile at polymeric side, (b) Display of voltage setting

in COMSOL 4.2a

104

4.16 Electric field for angle of tip radius in polymeric

sample of 450 at voltage 6 kV with (a) Electric field

profile at polymeric side, (b) Display of voltage setting

in COMSOL 4.2a

105

4.17 Electric field for angle of tip radius in polymeric

sample of 600 at voltage 3 kV with (a) Electric field

profile at polymeric side, (b) Display of voltage setting

in COMSOL 4.2a

107

4.18 Electric field for angle of tip radius in polymeric

sample of 600 at voltage 6 kV with (a) Electric field

profile at polymeric side, (b) Display of voltage setting

in COMSOL 4.2a

108

4.19 Relationship between the electric field and the angle of

tip radius in polymeric sample at different voltage

110

4.20 Bow-tie tree 111

4.21 Vented tree 111

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4.22 No water tree detected for 0 hour 112

4.23 Water tree length of XLPE sample tested for 470 hours 113

4.24 No water tree detected for 0 hour 115

4.25 Water tree length of LDPE sample tested for 150 hours 116

4.26 Water tree length of LDPE sample tested for 470 hours 117

4.27 The growth of water tree in LDPE sample for different

ageing time

120

4.28 The growth of water tree in XLPE sample for different

ageing time

120

4.29 The growth of water tree for two different materials 123

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LIST OF ABBREVIATIONS AND SYMBOLS

XLPE - Cross-linked Polyethylene

AC - Alternating Current

DC - Direct Current

HDPE - High Density Polyethylene

RF - Radio Frequency

PE - Polyethylene

PS - Polystyrene

PVC - Polyvinyl Chloride

LDPE - Low-density Polyethylene

TEM - Transmission Electron Microscopy

SEM - Scanning Electron Microscopy

PIXE - Particle Induced X-ray Emission

FTIR - Fourier Transform Infrared Spectroscopy

PEA - Pulse Electro Acoustic

RC - Resistance Capacitance

TSC - Thermally Stimulated Current

OSW - Oscillating Wave

VLF - Very Low Frequency Wave

RVM - Return Voltage Measurement

DR - Dielectric Response

PD - Partial Discharge

TDR - Time Domain Reflectometry

NaCl - Sodium Chloride

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PT - Platinum

Cu - Copper

Al - Aluminium

Fe - Ferum

Pb - Plumbum

NaOH - Sodium Hydroxide

Ep - Electric field in the axis of the point

U - Voltage applied

r - Radius of curvature of needle tip

d - Distance between needle tip and sample

t - time

to - Parameters

m - Parameters in the range 0.2-0.9

Mw - molecular weight

P (L) - probability of finding a tree length

T - temperature

exp - exponent

L - length

Lc (t) - Characteristic tree length to the function of time

α - Shape parameter of the distribution

L (t) - Average length water tree

kV - kilo volt

cm - centimeter

mm - milimeter

h - hour

kHz - kilo hertz

Hz - hertz

MHz - mega hertz

μm - micrometer

% - percent

kV/mm - kilo volt per milimeter

oC - degree Celsius

0 degrees

β - beta

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mol/l - moles per litre

kVA - kilo volt ampere

Ω - ohm

V/m - volt per meter

g/cm3 - grams per cubic centimeter

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LIST OF APPENDICES

APPENDIX TITLE PAGE

A Safety data sheet of Methylene Blue

Solution 136

B Data sheet of Tungsten Wire 143

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CHAPTER 1

INTRODUCTION

1.1 Research Background

Water tree is a process that causes degradation of insulation performance as

well as the ageing of cross-linked polyethylene (XLPE) cables. It is also one of the

major causes of premature ageing and failure of polymeric cables [1-3]. The

reduction in cable life due to water treeing has been identified as a major problem

and the way to overcome this problem is needed [4]. This phenomenon is known as

the growth and initiation of voids and microchannels filled with water [5]. They are

two main types of water trees, namely bow-tie trees and vented trees [6]. Water trees

occur between the insulation and another substance. They are many factors that can

cause the growth of water trees. Some of them are the material variables such as

additives and different kinds of polymeric materials, mechanical stress,

environmental factors include temperature, electrical variables such as ac, dc,

frequency, and contaminations ions in water [7].

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Water tree is one of the major causes of premature ageing and failure of

extruded medium voltage of polymeric cables which do not have water-impervious

barriers. It has been a challenge until now to overcome such failures.

Figure 1.1 shows a failure category diagram of underground cable (medium

voltage 6.6kV) reported by Tenaga Nasional Berhad (TNB) Selangor for the date of

1 Sept 2010 to 31 Aug 2011. It can be seen that the majority of the cable failures is

due to water tree, which is about 16.5%. In Malaysia, according to national power

utility, Tenaga Nasional Berhad (TNB), the main cause of power cable breakdown is

suspected due to water tree in underground polymeric cable. The inconsistent and

unreliable nature comes out with the importance of research in water tree observation

in polymeric materials.

Figure 1.1 Failure category diagram of underground cable (medium voltage 6.6

kV) reported by Tenaga Nasional Berhad (TNB) Selangor for the data of 1 Sept 2010

– 31 Aug 2011

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Currently, there are some techniques for water tree detection such as a

residual charge method, return voltage method, low frequency dielectric losses

measurement, time domain reflectometry method, very low frequency voltage

withstand test, dc current method, and RF technique [1, 8-11]. Polymeric cables are

widely used in power system application as cable insulation. From economical

perspective, there is significantly reduced demand of paper-type cable and increase

of polymeric ones. The maintenance routines of cables are improved to minimize the

cost and the diagnostic testing of installed cross-linked polyethylene (XLPE) power

cable is high of interest because of the high probability of failure caused by water

treeing. For the detection of water trees in XLPE cables, various types of electrical

testing have been done as reported in [8].

Many previous studies concentrated on the mechanism of water treeing

process as there are questions that are still unanswered, such as the formulation of

tree-resistant materials and the factors that cause the tree growth. Many observations

have been made to explain the propagation of water trees which include chemical,

electrical and mechanical aspects. It is believed that there are a lot of factors that can

contribute to the growth of water trees and not only depend on single mechanism. In

the treeing process, the ionic materials in the water play the significant role [7].

Water trees are hydrophilic dendritic, tree-like features (specifically, they

appear initially to be chains of water-filled cavities which later become bushes of

microscopic channels with hydrophilic surfaces), which grow typically under wet

and electrical operating conditions and may reach lengths of the order of 1 mm

within several years. A typical feature of water tree is shown in Figure 1.2. It shows

the typical vented trees are observed in water needle electrode of XLPE cable

insulation.

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Figure 1.2 Typical vented trees observed in the water needle electrode of XLPE

cable insulation [12]

1.2 Problem Statement

The use of high water treeing resistance underground cable is important in

order to ensure the reliability of power supply. Water tree observation in polymeric

insulating materials is important to investigate the water tree occurrence mechanism.

There are different effects of ageing time on water tree growth in different types of

polymeric insulating materials. From the previous researches, the types of needle

that have been used are nickel and platinum. It is found that the use of these needles

has weaknesses such as corrosion and corona discharge. They may hinder the clarity

of water tree observation by introducing noise in the result. In addition, it was shown

that the time taken is longer using the previous method to observe the water tree.

Thus, a modified test assembly for water tree study on polymeric insulating

materials was introduced in this research. From the modified test assembly, a

tungsten needle was used as an electrode in this research because it has a very high

electrical resistance and is the most refractory metal. Tungsten needle can avoid

corrosion and increase efficiency during experimental work. The modified test

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assembly tests samples in parallel condition reducing the time taken to observe water

tree since more samples can be tested simultaneously at equal applied voltage. This

research using modified test assembly, the effect of ageing time on water tree growth

in two different types of polymeric sample namely cross-linked polyethylene (XLPE)

and low-density polyethylene (LDPE) were investigated.

1.3 Objective of Research

The objectives of the research are as follows:

1. To study the effect of voltage application and different angle of tip radius

against electric field using COMSOL 4.2a.

2. To investigate the effect of ageing time on water tree growth in two different

types of polymeric sample namely cross-linked polyethylene (XLPE) and

low-density polyethylene (LDPE).

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1.4 Scope of Research

In order to achieve the direction of research and objectives, there are several

scopes that must be outlined and these include:

Analyze previous researches regarding the water tree observation method and

application to the polymeric sample materials.

Research focuses only on two thermoplastic materials such as cross linked

polyethylene (XLPE) and low-density polyethylene (LDPE).

The conducted experiments are based on BS IEC 61956 : 2001, “Methods of

test for the evaluation of water treeing in insulating materials” and BS EN

60243-1 : 1998, “Electrical strength of insulating materials-Test methods”.

Computational simulation and analysis using COMSOL 4.2a.

1.5 Significance of Research

In this research, a new method of water tree observation by improved

methods of water tree study so called “leaf-like” method was successfully

proposed.

From computational simulation studies using COMSOL 4.2a of the improved

investigation method, it is clearly describe the voltage application is directly

proportional to the electric field and the angle of tip radius in polymeric

sample is inversely proportional to the electric field.

The use of tungsten needle can avoid corrosion and losses during the

experiment.

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Experimental data from the improved investigation method clearly shows

XLPE has better water treeing resistance than LDPE.

Experimental data clearly shows the ageing time is directly proportional to

the water tree growth.

1.6 Thesis Organization

Chapter 1: Introduction

This chapter describes the overview of this project. Besides that, the first

chapter discusses the introduction that includes the research background, problem

definition, direction of research and objective, the significance of the research and

research flowchart as well as the summary of work that has been undertaken.

Chapter 2 : Literature Review

Additional information and literature reviews related to this research, such as

the background of water tree, basic of water tree, types of water tree, diagnostic and

testing of water tree and factors affecting the growth of water tree are discussed and

highlighted in this chapter.

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Chapter 3 : Research Methodology

In Chapter 3, this chapter describes about the operation and methodology

used in this project. The main content of this chapter is a detailed discussion on

computational analysis using COMSOL 4.2a, the sample production process and test

kit assembly. This chapter also gives detailed information on how the test and

analysis will be conducted in this project, including the experimental setup and

parameter used.

Chapter 4 : Results and Discussion

The analysis of water tree using COMSOL 4.2a software will also be

presented. The experimental results of water treeing tests will be discussed

thoroughly in this chapter. After that, the water tree analysis and discussion of

laboratory experiment will be highlighted in this chapter.

Chapter 5 : Conclusion and Recommendations

Chapter 5 concludes the work based on the results and discussion obtained

from this research and suggestions on some recommendations for the future work

that can be done to improve the research in this field.

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