Mini-Labs on Chemical Changes

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    Lab Skills Focus:

    Filtration

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    magnesium + sodium magnesium + sodium

    sulfate carbonate carbonate sulfate

    Chemical Equation

    MgSO4 + Na2CO3 MgCO3(s) + Na2SO4

    Word Equation

    Clear liquid

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    When solutions of two soluble salts are mixed, a

    solid may form. This solid is called a precipitate.and the reaction is called a precipitation reaction.

    Precipitation reactions are used to make insoluble

    salts.

    In this example the soluble salts are magnesiumsulfate and sodium carbonate, and the insolublesalt formed is magnesium carbonate.

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    Law of Conservation of Mass

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    Instructions

    1. Measure 5 g of baking soda and

    put into a flask.

    2. Measure 20 mL of vinegar and carefully

    pour it into a balloon.

    3. Carefully attach the balloon to the top of the flaskwithout spilling the vinegar into the flask.

    4. Place the flask with balloon on a weighing scale andrecord the mass of the system.

    5. Tip the vinegar from the balloon into the flask andrecord your observations.

    6. Measure the mass of the system after the reaction.

    7. Pop the balloon and measure the mass again.

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    Summary

    1. Explain whether your results support

    the Law of Conservation of Mass.

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    There are times when mass might

    appear to change during a chemical

    reaction.

    If you experience this during anexperiment, be sure to remember the

    Law of Conservation of Mass.

    The change in mass must be

    accounted for in a way other than

    destroying or creating atoms.

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    Endothermic andExothermic Reactions

    (Heat Change)

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    Exothermic and Endothermic Reactions

    An energy change accompanies the forming or

    breaking of a bond between atoms in a molecule.

    O Energy is released (produces heat) when a

    bond forms

    Exothermic

    o Energy is absorbed from the surroundingsto break the bonds in a molecule

    Endothermic

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    In your notebook:

    Draw a diagram of the set-up

    Make a data table

    Make a graph Calculate temperature change as a

    function of time

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    Maximum C Minimum C = Rate of temperature change

    Total Time (sec)

    Calculating Rate of temperature change

    Temperature/T degrees C Time/sec

    Starting temperature- ex. 28

    27

    26

    25

    24

    23

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    Endothermic

    ReactionExplore Lab:

    Energy change

    Summary:

    Explain how this lab shows a chemicalreaction.

    How does the graph show that the reaction isendothermic? Explain.

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    Endothermic reaction results:

    Starts at around 25 degrees C andends at around 21 degrees C

    Happens within about 2 minutes

    http://www.youtube.com/watch?v=MyAzjSdc3Fc

    Endothermic Reaction

    http://www.youtube.com/watch?v=MyAzjSdc3Fchttp://www.youtube.com/watch?v=MyAzjSdc3Fchttp://www.youtube.com/watch?v=MyAzjSdc3Fc
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    Exothermic Reaction: Oxidation of steel wool

    1. Put 8 grams of wool into a 400 mL beaker.

    2. Add enough acetic acid to completely

    cover the wool.

    3. Swirl for 2 minutes to remove the protective coating.

    4. Pour the acetic acid into a waste beaker.

    5. Quickly cover the beaker with Parafilm.

    6. Insert a thermometer through

    the film and into the steel wool.

    7. Record the time for each degree Celsius rise and

    follow the temperature/time profile through a 5

    degree change.

    Explore Lab 2:Energy change

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    Exothermic reactions

    The reaction produces heat.

    In this reaction vinegar is used

    to remove the protective coatingfrom steel wool, allowing it torust.

    When the iron combines withoxygen, heat is released.

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    Exothermic Reaction: Oxidation of steel wool

    Summary:

    Explain how this lab shows a

    chemical reaction.

    On the same graph (endothermic), show a

    graph of temperature change as a function of

    time.

    How does the graph show that the

    reaction is exothermic? Explain.

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    Exothermic Reaction: Oxidation of steel wool

    4Fe

    + 3O2

    2Fe2O3

    4 Fe + 6 O = 4 Fe + 6 O

    4 Fe

    + ___ O2

    2 Fe2O3

    Applying the Law of Conservation of Mass:

    How many atoms of Oxygen are needed to reactwith 4 atoms of Iron to form 2 units of Iron oxide?