1
dd 469 474 479 484 489 494 499 504 0 50 100 150 Core Gamma (API) 469 474 479 484 489 494 499 504 500 600 700 800 Tool Gamma (cps) 469 474 479 484 489 494 499 504 0 5 10 15 Gamma Scanner (cps) 469 474 479 484 489 494 499 504 0 100 200 300 XRF (ppm) 469 474 479 484 489 494 499 504 0 0.005 0.01 0.015 0.02 LAS Gamma 469 474 479 484 489 494 499 504 0.5 0.7 0.9 1.1 1.3 1.5 Gamma Tool 469 474 479 484 489 494 499 504 0 1 2 3 4 K Scanner 469 474 479 484 489 494 499 504 0 0.5 1 1.5 2 2.5 XRF 469 474 479 484 489 494 499 504 0 50 100 150 200 XRF 469 474 479 484 489 494 499 504 0 10 20 30 Gamma Scanner 469 474 479 484 489 494 499 504 2.5 4.5 6.5 8.5 Gamma Tool 469 474 479 484 489 494 499 504 0 5 10 15 LAS Gamma 469 474 479 484 489 494 499 504 0 10 20 30 40 50 XRF 469 474 479 484 489 494 499 504 0 5 10 15 20 25 Gamma Scanner 469 474 479 484 489 494 499 504 2.5 3.5 4.5 5.5 6.5 7.5 Gamma Tool 469 474 479 484 489 494 499 504 0 5 10 15 20 LAS Gamma Total Gamma K U Th A B C D A CENTRE FOR APPLIED BASIN STUDIES 465 470 475 480 485 490 495 500 505 0 10 20 30 Depth (m) TOC (%) , Gas Content (scf/ton) TOC Gas Content 0 5 10 15 469 474 479 484 489 494 499 0 100 200 300 TOC (%) V, Mo (ppm) V Mo TOC Cross plots comparing different total and spectral gamma values. (A) Total gamma ray values measured by handheld gamma tool (RS350), Gamma Scanner (SGR) and calculated gamma ray from XRF tests, respectively, showing a good match with core gamma (LAS). Measurements for core gamma are taken continuously whereas reading in handheld gamma tool, XRF tests and gamma scanner are taken in discrete points. (B), (C), (D) Spectral gamma values measured by mentioned techniques plotted against original spectral gamma values from core showing a reasonable match. Facies B: Massive or normally graded bentonite beds Facies BM: Bivalve-rich mudstone, planar stratification Facies CS: Carbonate-rich silty sand- stone, common bioturbation Facies CC: Coarse-grained carbonate (limestone), heavily bioturbated Facies FC: Fine-grained carbonate (limestone), rare bioturbation Facies FS: Slightly to noncalcareous fissile shale, rare broken bivalve fragments Facies FM: Foram, bivalve-rich mudstone, rare ripples Facies SM: Speckled mudstone with finely laminated silt-sized foraminifera grains Facies MC: Massive with medium to thick parting, noncalcareous mud/claystone. Facies OM: Organic-rich, fissile mudstone 0 2 4c m Carbonate-rich sandstone Massive mudstone Muddy sandstone Sandstone Calcareous mudstone Silty mudstone Bentonite bed Missing core Limestone Organic-rich mudstone 3-27-1-25W1 10-34-1-25W1 8-29-4-29W1 2-11-4-29W1 Northwest Southeast A` A 7105.5m 2524.2m 45525.3m 380 400 420 440 460 480 500 520 540 560 360 380 400 420 440 460 480 500 520 540 560 330 380 430 480 530 325 345 365 385 405 425 445 465 485 505 525 545 Datum Base of Fish Scale Sandstone) Assiniboine Mb. Keld Mb. Belle Fourche Mb. Boyne Mb. mud siltvf fm c mud siltvf f mc mud siltvf f mc mud silt vf f m c meters GR R GR GR GR R R R Gammon Mb. Morden Mb. meters meters meters These facies are recognized based on grain size, mineralogy, fossil content etc. The mud- dominated facies with the lowest degree of biotur- bation are interpreted as being deposited below storm-wave base in a marine environment. The mud-dominated fossiliferous facies are interpreted to be deposited in a marine shelf environment above storm wave base but below fairweather wave base. These contain planar stratified Inocera- mus shell hash beds deposited by storm-induced, higher energy currents reworking the shallow shelf. The sand-dominated facies are comprised of coarse-grain carbonate grains reflect the shallow- est water facies which, together with the high degree of bioturbation, suggest deposition in a well oxygenated proximal offshore to lower shore- face setting. Facies OM is more dominant in Morden interval. Facies BM and FM are mostly covering the Keld in- terval. CC facies is occuring on top of the keld and Assiniboine members as resistant, carbonate layers. Facies MC was only detected in the upper Belle Fourche member of the Ashville formation. Facies B or bentonite beds are occuring through the whole section as thick to very thin beds. B 5 15 25 35 45 55 65 75 468 478 488 498 SiO2 (%) Depth (m) SiO2 CaCO3 5 10 15 20 25 30 35 468 478 488 498 Al2O3 (%) Depth (m) 0.00 0.40 0.80 1.20 1.60 2.00 2.40 468 478 488 498 K2O (%) Depth (m) 0 5 10 15 20 468 478 488 498 FeS2 (%) Depth (m) 0 2 4 6 8 10 12 14 16 0.03 0.08 0.13 0.18 468 478 488 498 V (ppm) Depth (m) V TOC (%) 0 10 20 30 40 50 0 0.02 0.04 0.06 0.08 468 478 488 498 Mn (ppm) Depth (m) Mn U a) b) e) f) d) c) Cross-plots of different elemental compositions vs. depth for the well 3-27-1-25W1. Miner- alogical data are generated by ED-XRF. a) Percentage of SiO2 and CaCO3 versus depth showing the reverse relationship between the two major oxides. b) Values of aluminum oxide versus depth showing the same trend as silica in plot A. c) Showing the values for po- tassium oxide. Note that this trend almost matches the aluminum and silica trends. d) Pyrite content. e) Uranium and manganese, that displays an inverse relationship between the two. f) TOC percentage plotted along vanadium content as a reducing environment indicative element (TOC data from well report provided by CBM Solutions LTD, 2002). B-fourche Assiniboine Keld Morden B-fourche Assiniboine Keld Morden B-fourche Assiniboine Keld Morden B-fourche Assiniboine Keld Morden B-fourche Assiniboine Keld Morden Carbonate Types of Occurance Total and Spectral (K, Th, U) Gamma, Geochemistry Overview and Objectives, Stratigraphic Framework Lithologs, Facies and Mineralogy Stratigraphic nomenclature for the Upper-Cretaceous formations in southwestern Manitoba (Nicolas, 2008). Typical gamma-ray and resistivity well-logs in the well 3-27-1-25W1. Cretaceous Turonian Carlile Fm. Morden Shale Favel Fm. Assiniboine Member Marco Calcarenite Cenomanian Keld Member Laurier Limestone Beds Ashville Fm. Belle Fourche Sandstone Boyne Member Geophysical well Log (gamma ray and resistivity) with stratigraphic markers for upper Ashville, Favel and Carlile Formations. Facies 1 through 10 are shown in lithology logs. Area outcrop views. (a) Keld member (Favel formation) outcrop by the Wilson river. (b) Assiniboine member (Favel formation) and its top Marco calcarenite located by the Virmilion river. Also lower part of the Morden is shown on top of the hill. c) Boyne memebr (Carlile formation) and the bentonite beds within the interval. Shale gas plays are becoming progressively more important in the energy market as gas production from conventional reservoirs decreases. With the advances in exploitation technology gas production from shale has become viable and economic. The first modern exploration of shallow shale gas in Manitoba was initiated by EOG Resources Canada Inc. in 2003. Three shallow wells were drilled in the Waskada Field and perforated in the Assiniboine Member of the Favel Formation (Figure GS-X04-1). These wells did not produce gas and were abandoned in 2006–2007 (Nicolas, 2008). Additionally, in 2006-2007 Tundra Oil and Gas Partnership drilled three wells in Cretaceous shale units; which were also abandoned (Nicolas, 2008). Based on previous studies southwestern Manitoba is a good candidate for extracting gas from shale formations at shallow depth (Nicolas and Bam- burak, 2009). However, there is need for more studies in order to find the most productive shale intervals in the area and to design the proper techniques for gas extraction. Research in this recently started project will address several of these issues to better understand the shallow shale gas potential of these units. Previous work mainly focused on outcrops, whereas this project integrates these studies with subsurface data, core and well-logs to provide a link between the surface and subsurface where the potential gas resource exists. This study is being conducted on Upper-Cretaceous formations in southwestern Manitoba including the Upper Ashville, Favel, and Carlile formations. This study examines a number of wells drilled in this area. The goal of this study is to provide information needed to improve exploration in the new and unproven unconventional shallow shale gas play. Detailed subsurface mineralogical and geochemical studies are conducted on cores from a number of wells in this area. The data presented in this work are from well 3-27-1-25W1 located in Waskada oil field. Core examination, well-log and petrographic analysis are used to investigate the sedimentary structures, grain size, ichnology and bioturbation degree, and consequently to describe the facies scheme. Six main facies are identified ranging from non-calcareous organic mudstone to highly calcar- eous, bioturbated very fine-grained sandstone representing a change from offshore fissile shale to shallow water carbonate-rich lithologies. The biotur- bation intensity varies from rare to moderate representing more distal environmental settings from relatively anoxic to oxic interfaces. Bentonite beds occur at different intervals in the wells indicating volcanic activities during deposition. It may be possible to use these bentonite beds for high resolution dating of the strata as well as for lateral stratigraphic correlations. X-ray Fluorescence, from core and powdered samples, along with X-ray Diffraction are used to identify mineral composition and elemen- tal abundances. One objective is to look at minerals with a link to their types of occurrence within these units. For example, carbonate occurs in three different forms through shale units including; laminae of carbonate foram grains within shale beds, coccolith accumulations and as calcite fiber in thin to thick well -preserved bivalves (Inoceramus) laminae. These different styles of carbonate show rela- tively similar bulk mineralogy. However, each style affects the reser- voir properties and behavior in a different way. It is crucial to conduct mineralogical studies in association with sedimentological observa- tions in order to get the most realistic interpretation, understanding and analysis. Gamma ray values are calculated based on radioactive element concentrations measured through X-ray Fluorescence as well as using a hand-held gamma ray tool (RS 230). Additionally, gamma ray values are acquired using a gamma ray core scanner (SGR). All these gamma measurements are compared with the original high resolution 1. Department of Geoscience, University of Calgary, Calgary, Alberta, 2 .Manitoba Geological Survey, Winnipeg, Manitoba Mineralogy, Sedimetology and Facies Description of a Potential Cretaceous Shale Gas Play in Western Manitoba Somayeh Hosseininejad 1 , Per Kent Pedersen 1 , Ronald James Spencer 1 , Michelle P. B. Nicolas 2 3) Calcareous Clay Clasts 2) Calcic Bivalve Fragment Beds 4) Coccolith/Siderite c d e 1cm 1cm 1cm 1cm 1cm 1cm a a b b c a b c a b 1cm FB F FB NC NC OM F 500 µm CC 500 µm 500 µm 500 µm 250 µm 1 mm 1 mm 1) Calcic Foraminifera Laminae Facies Description (A) Reducing environment associated elements (V and Mo) plotted against TOC values. vana- dium can be used as a proxy for higher TOC values (Swanson, 1961). (B) TOC values vs. gas content. Note higher concentrations of gas occures at shallower depth with relatively con- stant values of organic matter. References: Nicolas, M.P.B. 2008: Summary report on petroleum and stratigraphic investigations, southwestern Manitoba; in Report of Activities 2008, Manitoba Science, Technology, Energy and Mines, Manitoba Geological Survey, p. 171–179. Swanson, V.E. 1961: Geology and geochemistry of uranium in marine black shales, a review; United States Geological Survey Professional Paper 356-c, United States Government Printing Office, Washington. (well depth shown in metres) Study area Located at the SW corner of Manitoba, The location of the 55 km long A-A', NW-SE cross section is indicated. b c . Assiniboine Mb. Morden Mb. Marco calcarenite Keld Mb. Boyne Mb. a 1) Planctic foraminifera occuring within different intervals of the studied strata. (a) Thin to thick foram laminae within the mudstone facies. (b ) Closer microscopic view of a thin foram lamina in shale. (c), (d) and (e) Different foraminifera speices within mudstone. 2) (a) Core veiw of interlaminated Inoceramid shells hashes within dark grey calcareous mudstone. (b) Closer view of prismatic Inoceramid shells. (c) Mi- croscopic view of a red dyed shell. 3) (a) Overall thin section view of a shaly facies. (b), (c) Calcareous and noncalcareous clay clasts in shale (CC) and non-calcareous clay clasts (NC), organic material (OM), forams (F) and phosphatic fish bones (FB). 4) (a) Coccolith accumulations (pellets) in silty mudstone. (b) Siderite grain in calcareous silty.

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Page 1: Mineralogy, Sedimetology and Facies Description of a ...dd 469 474 479 484 489 494 499 504 0 50 100 150 Core Gamma (API) 469 474 484 494 499 504 500 600 700 800 Tool Gamma (cps) 469

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UTh

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CENTRE FOR APPLIED BASIN STUDIES

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TOC Gas Content

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TOC (%)

V, Mo (ppm)

V Mo TOC

Cross plots comparing di�erent total and spectral gamma values. (A) Total gamma ray values measured by handheld gamma tool (RS350), Gamma Scanner (SGR) and calculated gamma ray from XRF tests, respectively, showing a good match with core gamma (LAS). Measurements for core gamma are taken continuously whereas reading in handheld gamma tool, XRF tests and gamma scanner are taken in discrete points. (B), (C), (D) Spectral gamma values measured by mentioned techniques plotted against original spectral gamma values from core showing a reasonable match.

Facies B:Massive or normally gradedbentonite beds

Facies BM: Bivalve-rich mudstone, planar strati�cation

Facies CS: Carbonate-rich silty sand-stone, common bioturbation

Facies CC: Coarse-grained carbonate (limestone), heavily bioturbated

Facies FC:Fine-grained carbonate (limestone), rare bioturbation

Facies FS:Slightly to noncalcareous �ssile shale, rare broken bivalve fragments

Facies FM: Foram, bivalve-rich mudstone,rare ripples

Facies SM:Speckled mudstone with �nely laminated silt-sizedforaminifera grains

Facies MC:Massive with medium to thick parting, noncalcareous mud/claystone.

Facies OM: Organic-rich, �ssile mudstone

0

2

4

cm

Carbonate-rich sandstone

Massive mudstone

Muddy sandstone

Sandstone

Calcareous mudstone

Silty mudstone

Bentonite bed

Missing core

Limestone

Organic-rich mudstone

3-27-1-25W110-34-1-25W18-29-4-29W1 2-11-4-29W1Northwest SoutheastA`A 7105.5m 2524.2m45525.3m

380

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465

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545Datum Base of Fish Scale Sandstone)

Assiniboine Mb.

Keld Mb.

Belle FourcheMb.

Boyne Mb.

mud siltvf f m c

mud siltvf f m c

mud siltvf f m c

mud silt vf f m c

met

ers

GR R GR GR GRRR R

Gammon Mb.

Morden Mb.

met

ers

met

ers

met

ers

These facies are recognized based on grain size, mineralogy, fossil content etc. The mud-dominated facies with the lowest degree of biotur-bation are interpreted as being deposited below storm-wave base in a marine environment. The mud-dominated fossiliferous facies are interpreted to be deposited in a marine shelf environment above storm wave base but below fairweather wave base. These contain planar strati�ed Inocera-mus shell hash beds deposited by storm-induced, higher energy currents reworking the shallow shelf. The sand-dominated facies are comprised of coarse-grain carbonate grains re�ect the shallow-est water facies which, together with the high degree of bioturbation, suggest deposition in a well oxygenated proximal o�shore to lower shore-face setting.Facies OM is more dominant in Morden interval. Facies BM and FM are mostly covering the Keld in-terval. CC facies is occuring on top of the keld and Assiniboine members as resistant, carbonate layers. Facies MC was only detected in the upper Belle Fourche member of the Ashville formation. Facies B or bentonite beds are occuring through the whole section as thick to very thin beds.

B

5

15

25

35

45

55

65

75

468 478 488 498

SiO

2 (%

)

Depth (m)

SiO2CaCO3

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35

468 478 488 498

Al2O

3 (%

)

Depth (m)

0.00

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2.00

2.40

468 478 488 498

K2O

(%)

Depth (m)

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FeS2

(%)

Depth (m)

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468 478 488 498

V (p

pm)

Depth (m)

VTOC (%)

0

10

20

30

40

50

0

0.02

0.04

0.06

0.08

468 478 488 498

Mn

(ppm

)

Depth (m)

MnU

a) b)

e) f)

d)c)

Cross-plots of di�erent elemental compositions vs. depth for the well 3-27-1-25W1. Miner-alogical data are generated by ED-XRF. a) Percentage of SiO2 and CaCO3 versus depth showing the reverse relationship between the two major oxides. b) Values of aluminum oxide versus depth showing the same trend as silica in plot A. c) Showing the values for po-tassium oxide. Note that this trend almost matches the aluminum and silica trends. d) Pyrite content. e) Uranium and manganese, that displays an inverse relationship between the two. f ) TOC percentage plotted along vanadium content as a reducing environment indicative element (TOC data from well report provided by CBM Solutions LTD, 2002).

B-fo

urch

e

A

ssin

iboi

ne

Keld

Mor

den

B-fo

urch

e

A

ssin

iboi

ne

Keld

Mor

den

B-fo

urch

e

A

ssin

iboi

ne

Keld

Mor

den

B-fo

urch

e

A

ssin

iboi

ne

Keld

Mor

den

B-fo

urch

e

Ass

inib

oine

Kel

d

M

ord

en

Carbonate Types of Occurance

Total and Spectral (K, Th, U) Gamma, Geochemistry Overview and Objectives, Stratigraphic Framework Lithologs, Facies and Mineralogy

Stratigraphic nomenclature for the Upper-Cretaceous formations in southwestern Manitoba (Nicolas, 2008). Typical gamma-ray and resistivity well-logs in the well 3-27-1-25W1.

Cret

aceo

us Tu

roni

an

Carli

le

Fm.

Morden Shale

Fave

l Fm

.

Assiniboine Member

Marco Calcarenite

Ceno

man

ian Keld

Member Laurier Limestone Beds

Ashv

ille

Fm.

Belle Fourche Sandstone

Boyne Member

Geophysical well Log (gamma ray and resistivity) with stratigraphic markers for upper Ashville, Favel and Carlile Formations. Facies 1 through 10 are shown in lithology logs.

Area outcrop views. (a) Keld member (Favel formation) outcrop by the Wilson river. (b) Assiniboine member (Favel formation) and its top Marco calcarenite located by theVirmilion river. Also lower part of the Morden is shown on top of the hill. c) Boyne memebr (Carlile formation) and the bentonite beds within the interval.

Shale gas plays are becoming progressively more important in the energy market as gas production from conventional reservoirs decreases. With the advances in exploitation technology gas production from shale has become viable and economic. The first modern exploration of shallow shale gas in Manitoba was initiated by EOG Resources Canada Inc. in 2003. Three shallow wells were drilled in the Waskada Field and perforated in the Assiniboine Member of the Favel Formation (Figure GS-X04-1). These wells did not produce gas and were abandoned in 2006–2007 (Nicolas, 2008). Additionally, in 2006-2007 Tundra Oil and Gas Partnership drilled three wells in Cretaceous shale units; which were also abandoned (Nicolas, 2008).

Based on previous studies southwestern Manitoba is a good candidate for extracting gas from shale formations at shallow depth (Nicolas and Bam-burak, 2009). However, there is need for more studies in order to find the most productive shale intervals in the area and to design the proper techniques for gas extraction. Research in this recently started project will address several of these issues to better understand the shallow shale gas potential of these units. Previous work mainly focused on outcrops, whereas this project integrates these studies with subsurface data, core and well-logs to provide a link between the surface and subsurface where the potential gas resource exists.

This study is being conducted on Upper-Cretaceous formations in southwestern Manitoba including the Upper Ashville, Favel, and Carlile formations. This study examines a number of wells drilled in this area. The goal of this study is to provide information needed to improve exploration in the new and unproven unconventional shallow shale gas play. Detailed subsurface mineralogical and geochemical studies are conducted on cores from a number of wells in this area. The data presented in this work are from well 3-27-1-25W1 located in Waskada oil field.

Core examination, well-log and petrographic analysis are used to investigate the sedimentary structures, grain size, ichnology and bioturbation degree, and consequently to describe the facies scheme. Six main facies are identified ranging from non-calcareous organic mudstone to highly calcar-eous, bioturbated very fine-grained sandstone representing a change from offshore fissile shale to shallow water carbonate-rich lithologies. The biotur-bation intensity varies from rare to moderate representing more distal environmental settings from relatively anoxic to oxic interfaces. Bentonite beds occur at different intervals in the wells indicating volcanic activities during deposition. It may be possible to use these bentonite beds for high resolution dating of the strata as well as for lateral stratigraphic correlations. X-ray Fluorescence, from core and powdered samples, along with X-ray Diffraction are used to identify mineral composition and elemen-tal abundances. One objective is to look at minerals with a link to their types of occurrence within these units. For example, carbonate occurs in three different forms through shale units including; laminae of carbonate foram grains within shale beds, coccolith accumulations and as calcite fiber in thin to thick well -preserved bivalves (Inoceramus) laminae. These different styles of carbonate show rela-tively similar bulk mineralogy. However, each style affects the reser-voir properties and behavior in a different way. It is crucial to conduct mineralogical studies in association with sedimentological observa-tions in order to get the most realistic interpretation, understanding and analysis. Gamma ray values are calculated based on radioactive element concentrations measured through X-ray Fluorescence as well as using a hand-held gamma ray tool (RS 230). Additionally, gamma ray values are acquired using a gamma ray core scanner (SGR). All these gamma measurements are compared with the original high resolution

1. Department of Geoscience, University of Calgary, Calgary, Alberta, 2 .Manitoba Geological Survey, Winnipeg, Manitoba

Mineralogy, Sedimetology and Facies Description of a Potential Cretaceous Shale Gas Play in Western Manitoba Somayeh Hosseininejad1, Per Kent Pedersen1, Ronald James Spencer1, Michelle P. B. Nicolas2

3) Calcareous Clay Clasts2) Calcic Bivalve Fragment Beds 4) Coccolith/Sideritec

d e

1cm

1cm1cm

1cm

1cm 1cm

aa b b

c

a b

c

a

b

1cm

FB

F

FBNC

NC

OM

F500 µm

CC500 µm

500 µm

500 µm250 µm

1 mm1 mm

1) Calcic Foraminifera Laminae

Facies Description

(A) Reducing environment associated elements (V and Mo) plotted against TOC values. vana-dium can be used as a proxy for higher TOC values (Swanson, 1961). (B) TOC values vs. gas content. Note higher concentrations of gas occures at shallower depth with relatively con-stant values of organic matter.

References:Nicolas, M.P.B. 2008: Summary report on petroleum and stratigraphic investigations, southwestern Manitoba; in Report of Activities 2008, Manitoba Science, Technology, Energy and Mines, Manitoba Geological Survey, p. 171–179.Swanson, V.E. 1961: Geology and geochemistry of uranium in marine black shales, a review; United States Geological Survey Professional Paper 356-c, United States Government Printing O�ce, Washington.

(well depth shown in metres)

Study area Located at the SW corner of Manitoba, The location of the 55 km long A-A', NW-SE cross section is indicated.

b c

.

Assiniboine Mb.

Morden Mb.Marco calcareniteKeld Mb.

Boyne Mb.

a

1) Planctic foraminifera occuring within di�erent intervals of the studied strata. (a) Thin to thick foram laminae within the mudstone facies. (b ) Closer microscopic view of a thin foram lamina in shale. (c), (d) and (e) Di�erent foraminifera speices within mudstone. 2) (a) Core veiw of interlaminated Inoceramid shells hashes within dark grey calcareous mudstone. (b) Closer view of prismatic Inoceramid shells. (c) Mi-croscopic view of a red dyed shell. 3) (a) Overall thin section view of a shaly facies. (b), (c) Calcareous and noncalcareous clay clasts in shale (CC) and non-calcareous clay clasts (NC), organic material (OM), forams (F) and phosphatic �sh bones (FB). 4) (a) Coccolith accumulations (pellets) in silty mudstone. (b) Siderite grain in calcareous silty.