Memorandum transmitting the Sample Analysis Results for

United States Environmental Protection Agency

Region 7 Laboratory 25 Funston Road

Kansas City, KS 66115 avso

Date: 8/16/2001

Subject: Transmittal of Sample Analysis Results for ASR #\ 1160

Activity Number: DDW16

Activity Description: Winona Post Company - SA

From: Michael Thomas, Associate Laboratory Director YlA-Regional Laboratory, Environmental Services Division

To: Dave Williams

SUPR/EFLR

OuD<C

Si te : ID #:HCk R r p a l c A3 Other:

This is the sample analysis results transmittal for the above-referenced Analytical Services Request (ASR). The data contained in this transmittal have been approved by the Regional Laboratory. This transmittal contains all of the sample analysis results for this ASR. The Regional Laboratory should be notified within 14 days if any changes are needed to the contents of this report. If you have any questions, comments or data changes, please contact the Laboratory Customer Service Department at 913-551-5295.

cc: Analytical Data File

/LG07+J

160074 SUPERFUND RECORDS

Page 1 of 8

•ASR Number: 1160

Activity Leader: Williams, Dave


Activity Desc: Winona Post Company - SA

Location: Winona

Superfund Name: Winona Post Company

Purpose: Site preliminary assessment

Org: SUPR/EFLR

State: Missouri

Summary of Activity Information

8/16/2001

Phone: (913)551-7625

Type: Superfund/Oil

Site ID: A780 Site OU:

Explanation of Codes, Units and Qualifiers used on this report.

Sample QC Codes: QC Codes identify the type of sample for quality control purposes.

FD Field Sample Field Duplicate

Units: Specific units in which results are reported.

Deg C = Degrees Celsius mg/L = Milligrams per Liter SU = Standard Units (pH) ug/L = Micrograms per Liter umhos/cm = Micromhos per Centimeter

Data Qualifiers: Specific codes used in conjunction with data values to provide additional information on the quality of reported results, or used to explain the absence of a specific value.

(Blank) = Values have been reviewed and found acceptable for use. U = Not detected at or above the reportable level shown.

Page 2 of 8

Activity Number: DDW16 ASR Number: 1160 Sample Information Summary

Activity Desc: Winona Post Company - SA 8/16/2001

Sample QC Matrix Location

External Start Start End End Receipt Number Code Matrix Location Sample No. Date Time Date Time Date

1 Water Wallace property owner - Taken at 07/17/2001 16:00 07/17/2001 16:05 07/19/2001 kitchen sink tap sample

2 - Water Seaman property owner - Taken at spigot near wellhead

07/17/2001 16:30 07/17/2001 16:35 07/19/2001

3 - Water Prewett/renter - Taken from 07/17/2001 17:15 07/17/2001 17:20 07/19/2001 kitchen tap

4- Water Sargent property owner 07/17/2001 17:40 07/17/2001 17:45 07/19/2001 5 - Water Haynes property owner - Taken at

spigot near driveway entrance 07/17/2001 19:15 07/17/2001 19:20 07/19/2001

6 - Water Castellano property owner - Taken 07/17/2001 19:45 07/17/2001 19:50 07/19/2001 at spigot near back dock of house

7 - Water Newsome property owner - 07/17/2001 20:00 07/17/2001 20:05 07/19/2001 Sample taken from well house spigot

8 - Water Sarton property owner - Taken from kitchen tap

07/17/2001 20:15 07/17/2001 20:20 07/19/2001

9 - Water Brawley property owner - Taken at spigot approx. 100 ft. North of house

07/18/2001 10:00 07/18/2001 10:05 07/19/2001

10- Water Foster property owner - Taken from spigot at rear of house

07/18/2001 10:25 07/18/2001 10:30 07/19/2001

10-FD Water Foster property owner - Taken from spigot at rear of house/Field Duplicate location of sample 10

07/18/2001 10:25 07/18/2001 10:30 07/19/2001

11 - Water Russell property owner - Taken from spigot approx. 30 ft. SE of house

07/18/2001 11:05 07/18/2001 11:10 07/19/2001

12- Water Roberts property owner - Taken at 07/18/2001 1 1:30 07/18/2001 11:35 07/19/2001 spigot approx. 150 ft. South of entrance road

1 3 - Water Honeycutt property owner - Taken 07/18/2001 12:00 07/18/2001 12:05 07/19/2001 from spigot located approx. 50 ft. West of home

Page 3 of 8

Activity Number: DDW16 ASR Number: 1160 RLAB Approved Analysis Comments

8/16/2001 Activity Desc: Winona Post Company - SA

Analysis Comments About Results For This Analysis

Herbicides in Drinking Water by GC/EC The contract laboratory received broken sample containers for samples 1160-2, 1160-3, and 1160-7. As a result, another aliquot of each sample was provided by the contract laboratory performing the TPH analysis. Each of the three samples indicated were extracted 1 day past their 14 day holding time. All extracts were analyzed well within their applicable holding time. The actual concentration of the target compound may have been higher than the reported result.

Page 4 of 8

Activity Number: DDW16 ASR Number: 11'60


RLAB Approved Sample Analysis Results

8/16/2001

Analysis / Analyte Units 1 - 2- 3-_ 4-

Conductivity by Field Measurement Conductivity umhos/cm 0.31 0.22 0.34 0.30

Herbicides in Drinking Water by GC/EC Pentachlorophenol ug/L 0.0545 U 0.0545 U 0.0545 U 0.0545 U

pH of Water by Field Measurement pH SU 7.4 7.5 7.4 7.4

Temperature of Water by Field Measurement Temperature Deg C 21.0 20.0 21.0 17.0

TPH Semi-volatile in Water by GC/FID

Extractable TPH mg/L 0.1 U 0.1 U 0.1 U 0.1 U

Page 5 of 8

Activity Number: DDW16 ASR Number: 1 160



8/16/2001

Analysis / Analyte Units 5- 6- 7- 8-


Herbicides in Drinking Water by GC/EC

Pentachlorophenol ug/L 0.0545 U 0.0545 U 0.0545 U 0.0545 U

pH of Water by Field Measurement

pH SU 7.4 7.3 7.3 7.3


TPH Semi-volatile in Water by GC/FID Extractable TPH mg/L 0.1 U 0.1 U 0.1 U 0.1 U

Page 6 of 8

Activity Number: DDW16 ASR Number: 11'60



8/16/2001

Analysis / Analyte Units 9- 10- 10-FD 11-


Herbicides in Drinking Water by GC/EC Pentachlorophenol ug/L 0.0545 U 0.0545 U 0.0545 U 0.0545 U

pH of Water by Field Measurement pH SU 7.6 7.5 7.5 7.7


TPH Semi-volatile in Water by GC/FID Extractable TPH mg/L 0.1 U 0.1 U 0.1 U 0.1 U

Page 7 of 8

Activity Number: DDW16 ASR Number: 1160



8/16/2001

Analysis / Analyte Units 12- 13-

Conductivity by Field Measurement Conductivity umhos/cm 0.37 0.17

Herbicides in Drinking Water by GC/EC Pentachlorophenol ug/L 0.0545 U 0.0545 U

pH of Water by Field Measurement pH SU 7.4 7.8

Temperature of Water by Field Measurement Temperature Deg C 17.0 16.0

TPH Semi-volatile in Water by GC/FID Extractable TPH mg/L 0.1 U 0.1 U

Page 8 of 8

CHAIN OF CUSTODY RECORD ENVIRONMENTAL PROTECTION AGENCY REGION VII

7-EPA-9262(Revised 5/85)

Sample Collection Field Sheet US EPA Region VII

Kansas City, KS

ASR Number: 1160 Sample Number: 1 QC Code: Matrix: Water Tag ID: 1160-1-

Activity Number: DDW16 Activity Leader: Williams, Dave


Location: Winona State: Missouri


Type: Superfund


7xK*yi K.'fcWi onK -W> Location Desc:

External Sample Number:

Expected Cone: Circle One:/Low\Medium High Date Time (24 Hr)

Latitude: ^ Sample Collection: Start *7^ / / 7^/ 0 / jb : Longitude: y TJD.oW End

Laboratory Analyses:

Container Preservative Holding Time Analysis

1 - 128oz amber glass 4 Deg C 7 Days TPH Semi-volatile in Water by GC/FID

1 - 128oz amber glass 4 Deg C 14 Days Herbicides in Drinking Water by GC/EC

Sample Comments:

r,'£on Wallace. 16 0

UU.'<4,C>1A_

(o55%l

573-32-5-4(42-.

N 5 1 - 3 % '

W 2.0.040'

I - 3 2 - f h i ' l e S W i n o n a

4puSt- i5

we-arS t>lc$.

~T~<Jn.y. $ub c~

^ •• 7.4

-fztp ran *1 iTjT,

IA/O U^f

Sample collected by: D. Williams


Kansas City, KS




Location: Winona



State: Missouri Type: Superfund


orl vmr Location Desc:

external Sample Number:

Expected Cone: Circle One: Low Medium High Date Time (24 Hr)

Latitude: Sample Collection: Start ?•/#/ Of )k :^0

Longitude: _9l! J3.MS ' End jJh'Al im?


Container Preservative

1 - 1 28oz amber glass 4 Deg C


Holding Time Analysis

14 Days Herbicides in Drinking Water by GC/EC

7 Days TPH Semi-volatile in Water by GC/FID

Sample Comments:

OWtLi 'Si<wr\<w\ HC t$C,

\A>i'non<\, M,0

Gil- 4-1S4

vrvtas J^vovo L4

Z lo- r uys. old

Te^vp : ^ 0 ° 7-5

Cov\$l \ o - 2-

l£~'2o



Kansas City, KS






Type: Superfund


Location Desc: " T J ^ e r y \ K


Expected Cone: Circle One: Low Medium High

Latitude: 34! 58.' Sample Collection:

Longitude: _3H H '

Date Time (24 Hr)

Start / l*f/C>) 17": (£"

End //7~/Q\ /-f .



1 - 128oz amber glass 4 Deg C





Sample Comments:

W T V e - w e t f - . ?. O. Box 5S-2

toSS<Zi (j>v\tk0.3^

^•0-f~ kni'leg) l/Avion^

~p*vT



Kansas City, KS




Location: Winona





Location Desc:


Date Time (24 Hr) Expected Cone: Circle One: Low Medium High

Latitude: 3k* . Sample Collection: Start 7~/ [ 7 r / ? - : il<)

Longitude: )8-JWtf End








Sample Comments:

Oon SovA&ri/t-

Wi'noAQ* Mb

"W^p. ]74c

1 4 - , l H o. i y,

P

Covicl

j nrr\



Kansas City, KS






:: cdr

Type: Superfund


Location Desc: +JUKT » driytWOM 'ZfrihUife 9 &r>\riwcu External Sample Number:


Latitude: 5 % _ A S a m p l e C o l l e c t i o n : S t a r t I d 3 ^ J H A S "

Longitude: 41° I1.Tq$ End [Joj

Date Time (24 Hr)





Sample Comments:

A^Sth l4^y h -e-i

Wc %by 1 1 0

\aWitxA C55S&

Z l - 3 - 3 2 5 - S & i /

•' 17

1M Condi'. £ > , 3 0

l . ^



Kansas City, KS

ASR Number: 1160 Sample Number: 6 QC Code: Matrix: Water Tag ID: 1160-6-_



Location: Winona





Location Desc: TaJC* <rf\ v\far hajJd- Acer Liou.<



Latitude:

Longitude: 41° K-W

Date Time (24 Hr)

Sample Collection: Start

End 11-/0 I H : 5t> Laboratory Analyses:


1 - 1 28oz amber glass 4 Deg C 14 Days Herbicides in Drinking Water by GC/EC

1 - 1 28oz amber glass 4 Deg C 7 Days TPH Semi-volatile in Water by GC/FID

Sample Comments:

Cashl-lauo

H'C' 131A

| lîO

£?3- 3 25- 2 6 38

p - o

' • 1 3

1-1 °l m'Ws fo r n Vovr fe-fiv


(Atell hyfk : 3 2& -jft. my

on \Nt\]


Kansas City, KS

ASR Number: 1160 Sample Number: 7 QC Code: Matrix: Water Tag ID: 1160-7-_



Location: Winona





Location Desc: -ytee^ iAjel( Lous*.



Latitude: 2^ £9.555' i ° - a -

Longitude: 91 H. old

Date Time (24 Hr)

Sample Collection: Start /Q[

End "7~~ / /7-10\ : OST Laboratory Analyses:







Sample Comments:

DAryl-e- VWsom*C-

fc* 8°I Boy

3-lZ9-<30\&

4^ : I7'C ^ •. 7.3

Cov\Ji \ . o.SS

\ . 1 2 v * f i ' U s

\J\) i hevva



Kansas City, KS




Location: Winona





Location Desc: TcJL&w -hi



Latitude: .59J33' Sample Collection:

Longitude: _9t! J9._eS?

Date Time (24 Hr)

Start *7" l ( T - / 0 ) :IS End ( 20








Sample Comments:

'Sation

Vrcn Boy (33

[A'iho^CX

£ " * 3 - 3 2 5 - 6 2 0 3

\tW7b '• 7-3

C*m$L ' 0-33

kv\ « W 5

V n I p 0 < g V



Kansas City, KS






Type: Superfund


Location Desc: "1gbuA cd~ sygot" l/taut


Date Time (24 Hr) Expected Cone: Circle One: Low Medium High

Latitude: ^ Sample Collection: Start i/H/OJ. 10_:00

Longitude: End / ($ /£ l | ° : C>5~ Laboratory Analyses:







Sample Comments:

PiOSCMaitm

P . O . S o y

\f J I/IA WAy M 0

3

7- k Covy J.\ o. So

M



Kansas City, KS






Type: Superfund


Location Desc:



Latitude: ' Sample Collection:

Longitude: 3£26.m'

Date Time (24 Hr)

Start ^-/ ZlT/Q ( /0 : 25"

End "7~l \%l d J /Q : S6








Sample Comments:

tIpSS~ V ^ ' ^ o H 6

3'°'

cUlUA |

£0hA 0,3^

ip«r

11 rôviA.



Kansas City, KS

ASR Number: 1160 Sample Number: 10 QC Code: FD Matrix: Water Tag ID: 1160-10-FD



Location: Winona





Location Desc: Field Duplicate location of sample 10



Latitude:

Longitude:

Date Time (24 Hr)

Sample Collection: Start *7-/ (%/(u\ jO : 2S"

End 7-/ (%/<> ) I 0.





Sample Comments:



Kansas City, KS






Type: Superfund


Location Desc:



Latitude: 3£ SB. Sample Collection: Start / ( S / 0 / H : OjT

Longitude: Si°- End 1L J0 Laboratory Analyses:




Sample Comments:

My ?iusse|( 324

MX

£ 33- 32.S -

T>\\ CoyuH ' 0>

JL& T- rv\»W5 %voyy> W/kom &')lU / 2 * 'ty

4 on well <rS'M°

, 4- e>yr



Kansas City, KS




Location: Winona





Location Desc:



Latitude: _00.O|5' Sample Collection: start

Longitude: 1 \ ' End H :3S"





Sample Comments:

I(wlir\ %°\ | 125

5 * 3 - 3 2 5

"Wwvb fC

prt : "7.4-o-3*tvdc*.

?v5<fr-l - S * v>\i\e6 Jysw V0,Vi4n.<k. Jir.'lt

3 W) jn -Hwi we'll

Sample collected by: D. Williams ^ j CW"> tAtH&f' o]j/

âyyv2/


Kansas City, KS




Location: Winona





Location Desc



Latitude: 34154 Sample Collection: Start 1V / I /2- : 0O

Longitude: i l!_JEnd IZ OS" Laboratory Analyses:







Sample Comments:

Y 0 • % I4A-]

^ 3 - 3 2 5 - 8 8 H

4^^ \ lb° CL

ft• i% O-lT mil.

^ Y*\\ htfk-V°4T 4^0 .

tL "fft fit*. (sOtzf-Villiams / Sample collected by: D. Williams

Documents

Memorandum transmitting the Sample Analysis Results for