29
U. S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, SCIENCE and ECOSYSTEM SUPPORT DIVISION ATHENS, GEORGL\ 30605-2700 / 4SESD-EIB FEB 2 8 2001 RRFAK- f;.M OTHFR- MEMORANDTIM SUBJECT: Davis Timber Site, Fmal Phase 2 Remedial Investigation Work Plan. Hattiesburg, Mississippi, SESD Project No.01-0300. FROM: THRU: TO: Dan Thoman, Regional Expert '\ Superfund and Air Section Archie Lee, Chief Superfund and Air Sec Amy WiUiams, RPM SSMB Waste Management Division Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi. We will be on site the week of March 5, 2001. Ifyou have any questions or comments, please call me at 706-355-8621. Attachment v^/7-/.rt'•'... t\.:^..<'^...j.../ .- :• . . : FEB 2 7 2001 AFLANTA, GA Gl 2001 10655908

MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

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Page 1: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

U. S. E N V I R O N M E N T A L PROTECTION A G E N C Y R E G I O N 4, SCIENCE and E C O S Y S T E M SUPPORT DIVISION

A T H E N S , G E O R G L \ 30605-2700 /

4SESD-EIB FEB 2 8 2001 RRFAK- f ; . M OTHFR-

MEMORANDTIM

SUBJECT: Davis Timber Site, Fmal Phase 2 Remedial Investigation Work Plan. Hattiesburg, Mississippi, SESD Project No.01-0300.

F R O M :

THRU:

TO:

Dan Thoman, Regional Expert '\ Superfund and Air Section

Archie Lee, Chief

Superfund and Air Sec

A m y WiUiams, R P M S S M B

Waste Management Division

Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber

Site located m Hattiesburg, Lamar County, Mississippi. We will be on site the week of March 5,

2 0 0 1 . I f y o u have any questions or comments , please call m e at 706-355-8621.

Attachment

v^/7-/.rt'•'...

t \ . : ^ . . < ' ^ . . . j . . . / .- :• . . :

FEB 2 7 2001

AFLANTA, GA

Gl 2001

10655908

Page 2: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

us EPA REGION 4 Davis Timber Site

Lamar County Hattiesburg, Mississippi

cc o o

> o o

U.S. ENVIRONMENTAL PROTECTION AGENCY REGION 4, SCIENCE & ECOSYSTEM SUPPORT DIVISION HAZARDOUS WASTE SECTION 980 COLLEGE STATION ROAD ATHENS, GEORGIA 30605-2720

^^<'^°''''%

\V/5

Page 3: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Tunber Site Remedial Investigation Work Plan Draft Phase 2 February 23, 2001

TABLE OF CONTENTS

SECTION PAGE

1.0 FIELD SAMPLING AND ANALYSIS PLAN PHASE 2. 1

1.1 Sample Identification 1

1.2 Impoundment Delineation and Soil/Waste Samphng 3

1.3 Trench Location and Soil/Waste Samplmg 5

1.4 Sediment Sampling 5

1.5 Temporary WeU InstaHation and Sampling 7

2.0 PHASE 2 REMEDIAL INVESTIGATION SAMPLING/DATA

QUALITY OBJECTIVE 8

2.1 General Remedial Investigation Data Quality Objectives 8

2.2 Site Specific Data Quality Objectives 8

2.2.1 Problem 8 2.2.2 Objectives 8 2.2.3 Data Requirements 9 2.2.4 Study Boundaries 9 2.2.5 Contaminant/parameter of Interest 9 2.2.6 Acceptable Decision Error rates 9 2.2.7 Design Optimization 9

3.0 SITE MANAGEMENT PLAN 13

3.1 Field Project Responsibilities 13

3.2 Site Control and Access 14

3.3 Estimated Project Schedule 14

4.0 QUALITY ASSURANCE PROJECT PLAN 15

4.1 Organization and ResponsibiUties. 15

4.2 Sample Collection 15 i

Page 4: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Timber Site Remedial Investigation Work Plan Draft Phase 2 February 23, 2001

TABLE OF CONTENTS

SECTION PAGE

4.3 Analytical Procedures 16

4.4 Field Instrumentation 16

4.5 Sample Contamers 17

4.6 Field Samplmg Equipment and Cleanmg Procedures 17

4.7 Audits... 17

5.0 FIELD HEALTH AND SAFETY PLAN 18

5.1 Purpose 18

5.2 Application 18

5.3 Responsibilities 18

5.4 Training Requhements 19

5.5 Medical Monitoring 19

5.6 Site Safety Considerations 20

5.7 Site Monitormg and Routes Of Exposure 20 5.8 Protective Clothmg ; 20

5.8.1 Protective Clothmg/Gloves 20 5.8.2 Head Gear 22 5.8.3 Eye Protection 22 5.8.4 Boots 22 5.8.5 Resphatory Protection 22

5.9 Emergency Contingency Plan 22

6.0 REFERENCES 23

11

Page 5: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Timber Site Remedial Investigation Work Plan Draft Phase 2 Febmary 23, 2001

LIST OF FIGURES

FIGURE PAGE

1.1 Impoundment Transects 4

1.2 Sediment Sampling Locations 6

111

Page 6: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Timber Site Remedial Investigation Work Plan Draft Phase 2 February 23, 2001

LIST OF TABLES

TABLE PAGE

1.1 Sample Collection Suinmary 2

2.1 Data Quality Objectives - Soil 10

2.1 Data Quality Objectives - Sedunent 11

2.1 Data Quality Objectives - Groundwater 12

5.1 Air Monitoring Action Levels 21

IV

Page 7: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Timber Site Remedial Investigation Work Plan Phase 2 February 23, 2001

LO FIELD SAMPLING AND ANALYSIS PLAN - PHASE 2

Phase 2 ofthe this remedial investigation will include the collection of soil/waste and perched ground water samples from on site and sediment/soil samples fi^om off site. The types and locations of these samples were based on data gaps identified during phase 1 ofthis investigation. The estimated number of samples for phase two is shovsoi in Table 1.1. However, field personnel will be responsible for the final selection ofthe sampling locations which may have a slight impact on the type and number of samples collected. All ofthe samples collected will be analyzed for extractable organic compounds and dioxin/dibenzoflirans. The soil/waste samples collected on site will also be analyzed for poly chlorinated biphenyls (PCBs). The sediment samples collected offsite will be analyzed for total organic carbon and grain size. The site background and physical setting, and an initial site evaluation were presented in the Phase 1 Work Plan. Consequently, they will not be repeated in this document.

1.1 Sample Identification

Samples collected during the project will be designated using an eight digit alphanumeric code in the form of DT-XXX-YYY. The prefix "DT" (for Davis Timber) will be used on all sample designations. The "XXX" represents a three digit alphanumeric sample number corresponding to the sample collection location. The sample collection locations are specified on the Figures presented in sections 1.1 through 1.4 In general, the samples will be numbered as follows:

001-199 - On site sample 201 -299 - Offsite samples 701 - 799 - Replicate (spHt) sample 901 - 999 - QA/QC samples

The last two dighs ofthe repHcate will, in general, correspond to the sample coUection location. For example, sample DT-762-SLA is a repHcate of sample DT-062-SLA

1

Page 8: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Timber Site Remedial Investigation Work Plan Phase 2 February 23, 2001

Sample Description

Soil/waste

Sediment

Table 1.1 Sample Collection Summary Table

Davis Timber Site Hattiesburg, Mississippi

Anticipated Number of Samples Environmental QA/OC

10

8

1 MS/MSD

1 duplicate 1 MS/MSD

Perched Ground Water 1 MS/MSD

Media Number of Samples Environmental QA/QC

Water 1

Soil/Sediment 18

SUBTOTAL 21 4

TOTAL 25

QA/QC samples include duplicate samples and matrix samples. Blanks and spikes for the CLP have not been included.

Page 9: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Timber Site Remedial Investigation Work Plan Phase 2 February 23, 2001

The "YYY" represents the next two or three letters which indicate the sample matrix as specified below:

TW -SD -SL

Temporary Well Sedunent Soil/waste

A third letter will be used with the "SL" designation and will represent the depth from which the sample is collected as specified below:

SLA - 0-6 inches below land Surface (BLS) SLB - 18-24 inches BLS SLC - 4-5feetBLS SLD - 9-10 feet BLS SLE - 14-15 feet BLS SLF - 19-20 feet BLS

Other letter designations may be assigned as conditions warrant.

To insure the continuation ofthe proper numbering sequence throughout the project, the SESD FORMS computer program will be used. The project numbers will be assigned at a later time. The account numbers that will be used by the field personnel through out the field sampling portion of the investigation will be 50102DA4P6CO.

1.2 Impoundment Delineation and Soil/Waste Sampling

The location ofthe fonner on site impoundment was determined during phase 1 ofthis mvestigation; however, the extent was not delineated because the area had been covered with tree bark and wood chips. The south and west borders ofthe impoundment appear to be the edge of the tree bark fill material. The north and east boundaries were not identifiable because the tree bark fill extends over much ofthis portion ofthe site.

The north and east boundaries ofthe impoundment will be delinieated using direct push technology (DPT). A GeoProbe wiH be used to advance boreholes and coUect samples ofthe tree bark fill down into the former unpoundment and through to native material along four transects (see Figure 1.1). Two ofthe transects will be perpendicular to the east boundary and two will be perpendicular to the north boundary. Boreholes will be spaced every 25 feet along the transect until the edge of the impoundment is encountered.

Page 10: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Figure 1.1 Transec Lines Davis Timber, Hattiesburg, MS. 0 100 ^ ^ ^ • ^ ^ ^ M

200 ^^^^^^^

300 400 500 Feet

donnfa/davtsArans

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Davis Timber Site Remedial Investigation Work Plan Phase 2 February 23, 2001

Samples will be coUected from each borehole at five foot intervals until native material is encountered. The tree bark is expected to be between two and twenty feet thick. The former impoundment is expected to be five feet thick. The samples vAW be visually inspected and screened using field PID and FID air monitoring instruments. Up to six samples collected from the tree bark fiU and the fonner impoundment will be submitted for extractable organic compound, PCB's and dioxin/dibenzofuran analyses. Additional boreholes may be advanced along the south and west borders ofthe tree bark fill to verify the extent ofthe former impoundment in those directions.

1.3 Trench Location and Soil/Waste Sampling

Discussions with area residents during the August 22, 2000 public meeting revealed the possibility that trenches were dug along the southem portion ofthe site into which waste pentachlorophenol (PCP) and material from the impoundment was placed and buried. The GeoProbe will be used to advance boreholes in this area to determine if and where trenches may exist. If non native material is encountered, up to four samples from different boreholes will be collected an submitted for extractable organic compound, PCB's and dioxin/dibenzofuran analyses. A Geonics EM-31 may also be used to dehneate the trench boundaries. Grid lines will be set up on a north-south east-west basis with readings taken at 25 foot intervals.

1.4 Sediment Sampling

Sediment samples collected fi'om East and West Mineral Creeks during Phase 1 ofthis investigation indicated that contamhiant concentrations decreased with distance from the site toward Country Club Estates Lake. To further characterize the creeks and defme the areas of contamination, sedunent samples will be collected from 8 additional locations. Four locations wiU be from West Mineral Creek and four locations from East mineral Creek. The locations in East Mineral Creek wiU be spaced every 200 feet dovm stream from phase 1 sample location DT-EMC-SDl. In West Mineral Creek one location v̂ U be between phase 1 locations DT-WL-SD2 and DT-WMC-SDl. The remaining three locations will be spaced every 200 feet down stream fi-om phase Isample location DT-WMC-SDl (see Figure 1.2).

The sediment samples v^ll be collected using a zero to three inch interval below the water-sediment interface. The sediment samples will be analyzed for extractable organic compounds, PCB's, dioxin/dibenzofuran, total organic carbon and grain size.

Page 12: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Figure 1.2 Sediment Sampling Locations Davis Timber, Hattiesburg, MS. 200 400 600 800 1000 Feet

..donnie/davls/sedltx

Page 13: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Tunber Site Remedial Investigation Work Plan Phase 2 Febmary 23, 2001

1.5 Temporary WeU InstaUation and Sampling

During the Phase 1 investigation, h was noted that a perched water table existed in the tree bark fill material over lymg the former unpoundment. To characterize the perched ground water, up to three temporary wells will be installed and sampled during this investigation. The exact location of these temporary wells will be determined in the field. The ground water samples fi-om the temporary weUs will be analyzed for extractable organic compounds, PCBs and dioxin/dibenzofuran.

/

Page 14: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Tunber Site Remedial Investigation Work Plan Phase 2 Febmary 23, 2001

2.0 PHASE 2 REMEDIAL INVESTIGATION SAMPLING/DATA QUALITY OBJECTIVES

2.1 General Remedial Investigation Data Quality Objectives

General remedial investigation sampling objectives as well as the data quality objectives were presented in the Remedial Investigation Work Plan for Phase 1 ofthe Davis Timber Site project. Consequently, they will not be repeated in this document.

2.2 Phase 2 Site Specific Data QuaUty Objectives

2.2.1 Problem

Previous investigations at the Site indicate that on-site soils, perched ground water, and offsite sediments have been contaminated as a result of past facility operations. Elevated levels of dioxin/dibenzofuran isomers, pentachlorophenol (PCP) and extractable organic compounds have been identified but the extent of contamination has not been adequately determined. More specifically, the location ofthe former impoundment has been identified but the size and depth have not been determined. The bark/wood chips overlying the impoundment appear to be holding a significant amount of water which may be contaminated. The contaminant concentration gradients in East and West Mineral Creeks have not been adequately determined and there exists the possibility of waste disposal trenches along the southem border ofthe she.

2.2.2 Objectives

The specific objectives ofthis phase of the investigation include the foUowing:

• Determining the nature of, and the areal and vertical extent of contamination (waste types, concentrations, and, distributions) in the former impoundment and perched groundwater at the Davis Timber Site;

Delineate the contaminant concentration gradients down stream ofthe site in East Mineral Creek and West Mineral Creek.

Determine if waste burial trenches exist on the southern portion ofthe site and if so, determine the waste types, concentrations and distributions.

• I)etemiine if the waste types and concentrations identified exceed Region 4 removal or remediation levels.

Page 15: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Timber Site Remedial Investigation Work Plan Phase 2 Febmary 23, 2001

2.2.3 Data Requirements

Soil/waste, sediment and ground water samples will be required to complete the objectives for phase 2 ofthis mvestigation. Sampling locations wiU be directed to refine the data resuhs from phase 1. Removal and remediation action levels for Region 4 will be developed if any areas exceed regional environmental cleanup goals. Table 2.1 presents the data quality objectives for each media sampled.

2.2.4 Study Boundaries

The study boundaries for this phase ofthe investigation include the Davis Timber site. East Mineral Creek and West Mineral Creek. The contaminants wiU be limited to the compounds contained in the SESDs TCL, TAL, and pesticide target analyte lists. Detection levels will be those obtained with routine analysis.

2.2.5 Contaminant/parameter of Interest

A Hst of contaminants of concem will be prepared as part ofthe Base Line Risk Assessment using data collected during this investigation. Cunently, extractable organic compounds, PCBs and dioxin/dibenzofurans are know to exist at the site. If any contaminants are found to exceed Regional removal/remediation goals, a feasibility study will be conducted to select the appropriate remedy.

2.2.6 Acceptable Decision Error rates

Acceptable decision enor rates will be dependent upon the contaminants of concem developed as part ofthe Base Line Risk Assessment. In order to assure data accuracy, a sufficient number of samples v^ll be collected from the site to determine what, if any contaminants exist at the site. Duplicate samples and quality control samples v̂ all also be collected to vaHdate the field activities and insure that these activities did not introduce contamination or bias sample results. It is expected that 90% of samples collected wUl result m valid results.

2.2.7 Design Optimization

This field investigation has been designed to provide the information necessary to adequately address the stated objectives using a direct-authoritative approach. Data collected during phase 1 identified specific areas contaminated with PCP, extractable organic compounds and dioxin/dibenzofurans. Samples collected during phase 2 v^ll refine the areal extent of these contaminants. Previous sampling resuhs, on she EM surveying, visual observation of Geoprobe samples and air monitoring results during sampling activities will be used to direct sampling locations.

Page 16: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Tunber Site Remedial Investigation Work Plan Phase 2 Febmary 23, 2001

Media:

Location:

Table 2.1 Data Quahty Objectives - Soil

Davis Timber Hattiesburg, Mississippi

Soil, tree bark/wood chip material, waste.

On-she

Data Types: Screening - Site screening using PED and FID air monitoring equipment and visual inspection.

Definitive - Laboratory Analyses for Extractable Organic Compounds, PCBs, Dioxin/dibenzofurans.

Sampling Type: Environmental, Grab samples will be collected utilizing stainless steel hand augers or GeoProbe core tubes, spoons and glass pans.

Field Quality Control Samples: None

Sampling Procedures: See Section 12, United States Environmental Protection Agency, Region 4, Science and Ecosystem Support Division, Environmental Investigations Standard Operating Procedures and Ouality Assurance Manual. May 1. 1996.

Background/control Sample: A control sample will not be collected.

10

Page 17: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Tunber Site Remedial Investigation Work Plan Phase 2 Febmary 23, 2001

Media:

Location:

Table 2. 1 (cont) Data Qualhy Objectives - Sediment

Davis Timber Hattiesburg, Mississippi

Sediment

East Mineral Creek, West Mineral Creek.

Data Types: Screening - none.

Sampling Type:

Definitive - Laboratory Analyses for Extractable Organic Compounds PCBs, Dioxin/dibenzofuran, TOC and grain size.

Environmental, Grab samples will be collected utilizing stainless steel hand augers, scoops, spoons and glass pans.

Field Quality Control Samples:

Sampling Procedures:

2 Duplicates (1 blind and 1 MS/MSD)

See Section 11, United States Environmental Protection Agency, Region 4, Science and Ecosystem Support Division, Environmental Investigations Standard Operating Procedures and Ouality Assurance Manual. May 1, 1996.

Background/control Sample: A control sample wiU not be collected.

11

Page 18: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Timber Site Remedial Investigation Work Plan Phase 2 Febmary 23, 2001

Table 2.1 (cont) Data Qualhy Objectives - Ground Water

Davis Timber Hattiesburg, Mississippi

Media: Perched Ground Water

Location: On Site

Data Types: Screening - pH, Temperature, Specific Conductance, Turbidity.

Definitive - Laboratory Analyses for Extractable Organic Compounds, PCBs, and Dioxin/dibenzofuran.

Sampling Type: Environmental, Grrab Samples Will Be Collected Using Teflon Tubing and Vacuum Jug Assembly.

Field Quality Control Samples: 1 MS/MSD)

Sampling Procedures: See Section 7, United States Environmental Protection Agency, Region 4, Science and Ecosystem Support Division, Environmental Investigations Standard Operating Procedures and Ouality Assurance Manual. May 1, 1996.

Background/control Sample: A control sample wiU not be coUected.

12

Page 19: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Tunber Site Remedial Investigation Work Plan Phase 2 Febmary 23, 2001

3.0 SITE MANAGEMENT PLAN

3.1 Field Project Responsibilities

The overall field investigative/sampling phase ofthe project will be the responsibility of Dan Thoman, the field project manager. Mr. Thoman will be responsible for the following field activities:

• Insuring that all field activities are communicated and coordinated with Amy WiUiams, the Remedial Project Manager (RPM).

• Monitor overall project quality control.

• Monitor health and safety ofthe sampling/investigative personnel.

• Coordinate sample analyses with the laboratory.

The foUowing is a Hsting ofthe personnel that wUl be involved in the field operations at the Davis Timber site and their areas of responsibilities:

Dan Thoman

Amy Williams

Bobby Levws

Field Project Coordinator

Remedial Project Manager

Safety Officer

Milton Henderson GeoProbe Operator

Tim Simpson Field Quality Assurance Coordinator

Brian Striggow Sampling Team Leader

13

Page 20: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Tunber Site Remedial Investigation Work Plan Phase 2 Febmary 23, 2001

The overall management ofthe project is the responsibility ofthe Remedial Project Manager, Amy Williams. Ms. WilHams wiU be responsible for the foUowing activities:

• Coordinating all management activities.

• Arrange for site access.

• Assist in providing for the following services: electricity, water, trash containers and pick-up if necessary.

3.2 Site Control and Access

Areas where sampling activities are taking place will be restricted only to authorized personnel designated by the field project leader (Dan Thoman) and/or the she safety officer (Bobby Lewis).

3.3 Estimated Project Schedule

Field Sampling Investigation— March 5-9 , 2001 Samples sent to CLP or Athens laboratory March 9, 2001 CLP Data Package Sent to Athens QA/QC Section for VaHdation May IS, 2001 Data Cleared and Sent to HWS —- June 8, 2001 Draft Report Completed —- August 30, 2001 Comments on Draft Report September 28, 2001 Final Report Sent to RPM October 30, 2001

14

Page 21: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Timber Site Remedial Investigation Work Plan Draft Phase 2 Febmary 23, 2001

4.0 QUALITY ASSURANCE PROJECT PLAN

Quality assurance (QA) procedures must begin in the planning stage and continue through sample collection, analyses, reporting and final review. The methods that will be used to insure data quality are discussed below.

4.1 Organization and Responsibilities

The Field Project Coordinator has overall responsibUity for field QA. Tim Simpson has been appointed QA coordinator and has the day to day responsibility to insure that prescribed routine qualhy control (QC) procedures are applied and documented in the field.

All laboratory analyses will be conducted by SESD or under the CLP with overall responsibility for laboratory QA resting whh the Branch Chief The Organic Chemistry Section Chief and the Office of Quality Assurance Chief, have the responsibility to insure that prescribed routine QC procedures are applied and documented by SESD or the CLP laboratory.

4.2 Sample CoUection

All samples will be coUected in accordance vwth Section 4 ofthe United States Environmental Protection Agency, Region 4, Science and Ecosystem Support Division, Environmental Investigations Standard Operating Procedures and Oualhy Assurance Manual. May 1, 1996 (2). The quality assurance and quality control procedures described in this manual will insiire that representative samples are collected from the various media sampled. A copy of the manual, in addition to the Work Plan and Field Sampling and Analysis Plan, will be maintained at the field office/command post for reference during all phases ofthe field sampling activities. If any deviations in sampling procedures are used, these deviations wall be recorded in the field log books. The sample collection locations will be surveyed using global positioning system (GPS) equipment

Duplicate samples will be collected weekly for 5 percent ofthe samples collected for each matrix. This v̂ U provide a check for sampling techniques. In addition, when water samples are collected, water trip blanks wdU be prepared v^th organic fi-ee water by the ASB. The trip blanks wiU be transported to the field, handled and stored v^th the samples coUected from the site. This v^ll provide a check to determine if samples may have been contaminated during handling and storage.

15

Page 22: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Timber Site Remedial Investigation Work Plan Draft Phase 2 Febmary 23, 2001

Equipment rinse blanks wiU be coUected, if required, from equipment cleaned on she, using organic free water, at least weekly or more frequently at the request ofthe field quality control coordinator. The equipment rinse blanks will be collected to ensure that the sampling equipment is properly field cleaned.

4.3 Analytical Procedures

^Alljiqfjlte;samp!esm^ andtedioxin/dibenzoftirans:4|Injaddition^,aU^jfA ^sediment:samplesiwiU^be-analyzed;for;/tqtal....^.'•. orgamc .carbon:;;*^ analyses will be cohdii(5ted according to the United States Environmental Protection Agency, Region 4, Science and Ecosystem Support Division, Analytical Support Branch Operations and Ouality Control Manual. December, 1997 (3), or the CLP Statement of Work (SOW). This SOW describes chain of custody, caUbration procedures, routine QC checks, and data validation and reporting; it also describes the laboratory's routine procedures for assessing precision and accuracy. If required, the samples collected for analysis will be booked into the Contract Laboratory Program (CLP) laboratories through the Regional Sample Control Coordinator, to ensure avaUability of space and continuity of data.

4.4 Field Instrumentation

The foUovwng instmments may be used during the remedial investigation at the site:

1. pH meter

2. thermometer 3. specific conductivity meter 4. turbidity meter 5. photo ionization detector 6. combustible gas mdicator 7. oxygen meter S. radiation survey meter 9. organic vapor analyzer 10. water level indicator 11. Geonics EM-31

All calibration procedures utiHzed for these instmments will be performed in accordance wath Appendix D ofthe EISOPQAM (2) or the manufacturers specifications. All calibrations will be recorded in the field log books.

16

Page 23: MEMORANDUM FROM DAN THOMAN, EPA TO AMY ...Attached is the Final Phase 2 Remedial Investigation Work Plan for the Davis Timber Site located m Hattiesburg, Lamar County, Mississippi

Davis Tunber She Remedial Investigation Work Plan Draft Phase 2 Febmary 23, 2001

4.5 Sample Containers

Sample containers used will be in accordance with the requirements specified in Appendix A ofthe EIS0PQAM(2). The following is extracted from the manual and provides a description ofthe analysis, preservatives, and types of containers that wall be used during this sampling mvestigation.

Soil/Sediment Analysis Analvses Container Preservative

Extractable Organics 2 - 8 oz. glass iced, 4°C PCB's Dioxin/dibenzofuran

Water Analvsis Analyses Container Preservative

Extractable Organics 1-1 gallon glass iced, 4°C PCB's Dioxin/dibenzofuran 1-1 gallon glass iced, 4°C

(All containers used for organic samples have Teflon lined caps, and all containers for purgeable organic sample have septum Hds.)

4.6 Field Sampling Equipment and Cleaning Procedures

All samples will be collected with sampling equipment specified and cleaned in accordance with Appendix B ofthe EISOPQAM (2). Any deviation from this wiU be justified and recorded in the field log book. All equipment wash water will be discharged to the ground on site. AU spent isopropanol will be containerized separately from the wash water and disposed of by EPA.

4.7 Audits

Routine audhs of field and laboratory activities will be conducted by the field QA ' Coordinator and by the Organic Chemistry Section Chief Independent field and laboratory audits will be conducted by the Region IV, QA OfBcer or his representative(s). Any problems identified during these audits will be addressed in a memo to the field project coordinator who will then take immediate steps to conect the identified discrepancies.

17

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Davis Tunber Site Remedial Investigation Work Plan Draft Phase 2 Febmary 23, 2001

5.0 FIELD HEALTH AND SAFETY PLAN

5.1 Purpose

The purpose ofthis safety plan is to assign responsibilities, establish personnel protection standards, establish mandatory safety operating procedures, and provide for contingencies that may arise while conducting this remedial investigation. All aspects ofthe field operations must comply with the US-EPA, Region IV, Safety. Health and Environmental Management Program (4) manual which is consistent with US-EPA Orders 1440.2 and 1440.3) and Occupation Safety and Health Administration regulations (29 CFR 1910.120).

5.2 AppUcation

The provisions ofthis safety plan are mandatory for all EPA personnel and personnel under contract to EPA involved with this investigation. Application ofthis safety plan include the sampling and mitigation undertaken on the she or at anv ofF-site areas which may be affected by containination from the site. All visitors (state, contract, EPA persormel, etc.) will be required to abide by these safety procedures. Reflisal to comply vwth the safety guidelines established will result in the visitors being baned from the she or the suspension of work.

5.3 Responsibilities

The field project coordinator (Dan Thoman) and the safety officer Bobby LevAs will have the primary responsibilities for:

1. Assuring that appropriate personnel protection equipment is available and properly utilized by all field operations personnel.

2. Assuring that field personnel are aware ofthe provisions ofthis plan, are instmcted in the work practices necessary to ensure safety, and in planned procedures for dealing with emergencies.

3. Assuring that personnel are aware ofthe potential hazards associated with the site operations.

4. Supervising the monitoring of safety performance by all personnel to ensure that required work practices are employed.

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Davis Timber She Remedial Investigation Work Plan Draft Phase 2 Febmary 23, 2001

5. Assuring personnel have had proper safety training before participating in the investigation and have read the US-EPA, Region IV, Safety. Health and Environmental Management Program manual.

6. Conecting any work practices or conditions that may result in injury to personnel or exposure to hazardous substances.

7. Assuring that proper emergency first aid equipment is available (eye wash station, first aid kit, etc.)

The safety officer will have the ultimate authority on all safety decisions and can suspend project operations if required safety procedures are not used by field personnel. In addition, prior to the initiation of work each day, a safety meeting will be held by the safety officer with field personnel to discuss field safety operations.

5.4 Training Requirements

All field personnel must have received a minimum of 40 hours of initial personnel protection training ofF-site. Personnel must also receive cardiopulmonary resuscitation (CPR) and first aid training prior to she entry (which can be included in the 40 hours of personnel protection training). All personnel that have never worked at a hazardous waste site will be accompanied by an experienced employee for at least 3 days prior to being expected to work at the site without direct safety supervision. All certifications of training wiU be on file with the Science and Ecosystem Support Division safety officer as specified in the US-EPA, Region FV, Safety. Heahh and Environmental Management Program manual prior to site entry.

5.5 Medical Monitoring

Prior to site entry all field investigative personnel must under go a baseline medical examination as specified in the US-EPA, Region IV, Safetv. Health and Environmental Management Program manual.

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Davis Timber Site Remedial Investigation Work Plan Draft Phase 2 Febmary 23, 2001

5.6 Site Safety Considerations

Previous sampling at the site revealed the presence of pentachlorophenol and dioxin/dibenzofiiran isomers m the soil. Hand augers wall be used during the remedial field investigation. It is possible that during these field operations the liberation of irritating and possibly toxic vapors might occur. However, it is felt that the likelihood ofthis occurring is remote. Regardless, the location ofthe nearest phone, the emergency phone numbers and the route to the nearest hospital wiU be placed in each vehicle. It is the responsibility ofthe safety officer to ensure that all field personnel know the route to the hospital and have a copy ofthe emergency phone numbers.

5.7 Site Monitoring and Routes of Exposure

During various phases ofthe sampling activities, the site may be monitored with a photo ionization detector, an organic vapor analyzer (OVA), a radiation survey meter and a combustible gas meter/oxygen meter. It wiU be the safety officer's responsibility to determine what level of monitoring, if any, will be required for each samphng event. Table 5.1 lists the action levels for -each ofthe air monitoring instmments/meters. If readings on the instmments/meters exceed those Hsted in Table 5.1, then the personnel must discontinue field operations and discuss the findings with the safety officer.

It is felt that pentachlorophenol will consthute the greatest known chemical risk to field personnel. Routes of exposure for these compounds would include inhalation, ingestion and dermal contact. The ingestion route represents minimal risks but the inhalation and dermal routes present possible risks. Therefore, the safety officer will determine what levels of protective clothing will be worn by field personnel to eliminate these risks.

5.8 Protective Clothing

Levels of protection refened to in the subsequent sections are defined in the US-EPA, Region IV, Safetv. Health and Environmental Management Program manual.

5.8.1 Protective Clothing/gloves

All personnel wall have Level D protective clothing available to wear. The protective clothing and gloves required to be wom wUl be mandated by the safety officer and may differ from one sampling location to the next.

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Davis Timber Site Remedial Investigation Work Plan Draft Phase 2

, Febmary 23, 2001

Table 5.1 Air Monitoring Action Levels

Davis Timber Site Hattiesburg, Mississippi

INSTRUMENT ACTION LEVEL

PHOTO IONIZATION DETECTOR (10.2 EV LAMP) 5 ppm Above Background

ORGANIC VAPOR ANALYZER 5 ppm Above Background

COMBUSTIBLE GAS METER 20% Lower Explosive Limit

OXYGEN METER Less than 20% Oxygen

RADIATION SURVEY METER Above Background

If any reading on the meters exceed (or is less than for the oxygen meter) the Action Levels listed above then personnel must immediately return to the field office for further instmctions.

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Davis Tunber Site Remedial Investigation Work Plan Draft Phase 2 Febmary 23, 2001

5.8.2 Head Gear

Hard hats will be wom by all personnel when advised by the safety officer.

5.8.3 Eye Protection

AU persormel v^ll be required to wear safety glasses on site as conditions warrant. Face shields and goggles vn\l also be available. Contact lens will not be permitted to be wom at the she.

5.8.4 Boots

Steel toed and steel shank mbber or leather boots will be required to be wom on site.

5.8.5 Respiratory Protection

The respiratory protection that will be made available to field persormel wUl be:

• Five minute air escape capsules (ISI ELSA) • Air purifying respirators (MSA uhra twin)

Only NIOSH/OSHA approved equipment will be used. The safety officer will determine what level of respiratory protection wiU be required for the field personnel by using the air monitoring equipment.

5.9 Emergency Contingency Plan

On-she emergencies could be expected to result from fire, chemical exposure or personnel casualty. If an incident occurs necessitating a response to an emergency, the project leader or safety officer will use the two-way radios to communicate the emergency to personnel on site and/or sound an emergency hom.

The signal will be of at least 5 short blasts (each of about 1 second duration). Personnel on site will immediately discontinue field operations and assemble at a pre-specified location.

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Davis Tunber Site Remedial Site Investigation Work Plan Febmary 23, 2001

6.0 REFERENCES

1. United States Envhonmental Protection Agency, Region 4, Science and Ecosystem Support Division, Davis Timber. Hattiesburg. Mississippi. Remedial Investigation Work Plan. April, 2000.

2. United States Environmental Protection Agency, Region 4, Science and Ecosystem Support Division, Environmental Investigations Standard Operating Procedures and Ouality Assurance Manual. May 1, 1996.

3. United States Envhonmental Protection Agency, Region 4, Science and Ecosystem Support Division, Analytical Support Branch Operations and Quality Control Manual. December, 1997.

4. United States Environmental Protection Agency, Region IV, Safetv. Health and Environmental Management Program Manual. 1998.

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